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196
SUPPORTING DOCUMENT 2. Title Conceptual Design Report, TRUEX Pilot Plant, Project 91E-GFW-153 5. Key Words Project W-153 TRUEX Pilot Plant CDR 7. Abstract 001374 I 1. Total Pages I '1~5 3. Nl..llber 4. Rev No. WHC-SD-Wl53-CDR-001 0 6. Author Name: G. R. Porter Organization/Charge Code 85330 This is the Conceptual Design Report for Project W-153, the TRUEX Pilot Plant at B Pl ant. PPROVED FOR PUBLIC RELEASE ~ --\'-I-Cl l 8. PURPOSE AND USE OF DOCUMENT· This dpCunent $las prepared for use within the U.S. Department of Energy and its contractor~· / lt is to be used only to _perform, direct, / or integrate work unde 1/ _ U.S. Department ·of E .nergy cont~acts. This docunent 7 ·s not approved for public release , until rev} ewed. \ . / ' PATENT STATUS· This docunent copy, since it is t~ ansmitted in advance of patent clear~nce, is made available in confidence solely for use in performance of_ work under contracts with \ the U.S. Department of Energy:, This docunent is not to be published nor its contents otherwise 'qisseminated or used for purposes other than specified above before patent approval for such elease or use has been secured, upon request, from the U.S. Depart~t of Energy, Patent Attorney,, Richland Operations Office, Richland, \ IJA. I DISCLAIMER· This report was prepared as an account of work sponsored by an agency of the United States Governnent. Neither the United States Governnent nor any agency thereof, nor any of their e,rployees, nor any of their contractors, subcontractors or their employees, makes any warranty, express or i~lied, or assunes any legal liability or responsibility for the accuracy, COf1l)leteness, or any third party's use or the results of such use of any information, apparatus, product, or process disclosed, or represents that its use would not infringe privately owned rights. Reference herein to any specific conmercial product, process, or service by trade name, trademark, manufacturer, or otherwise, does not necessarily constitute or i~ly its endorsement, reconmendation, or favoring by the United States Governnent or any agency thereof or its contractors or subcontractors. The views and opinions of authors expressed herein do not necessarily state or reflect those of the United States Governnent or any agency thereof. 9. !~act Level 2 A-6400·073 (7/90) {EF} WEF124 Supporting Docunent (Cover Sheet) ·10. Authorized Manager's Name B. K. Horsager Specify Distribution Limit S L 11. RELEASE STAMP ,- -. ---I I ·,RELEASED .. i l DISTRIBUTION LIMITS i j i I INTERNALONLY_. ; ®jsf'ONSOR LIMITED EXTERNAL _. __ -- _ f MAR -8 --- 1991 ; , 0 _,,_ DATE; ____ . -~..M:::/0 .-.--:;....i...,.=;;.. ___________ _ ..

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Page 1: -I-Cl l

,,,,_.

SUPPORTING DOCUMENT

2. Title

Conceptual Design Report, TRUEX Pilot Plant, Project 91E-GFW-153 5. Key Words

Project W-153 TRUEX Pilot Plant CDR

7. Abstract

001374 I 1. Total Pages I '1~5

3. Nl..llber 4. Rev No.

WHC-SD-Wl53-CDR-001 0

6. Author

Name: G. R. Porter

~L~ Organization/Charge Code 85330

This is the Conceptual Design Report for Project W-153, the TRUEX Pilot Plant at B Pl ant.

PPROVED FOR PUBLIC RELEASE

~--\'-I-Cl l 8. PURPOSE AND USE OF DOCUMENT· This dpCunent $las prepared for use

within the U.S. Department of Energy and its contractor~·/ lt is to be used only to_perform, direct,/ or integrate work unde1/_ U.S. Department ·of E.nergy cont~acts. This docunent7 ·s not approved for public release ,until rev} ewed. \

. / '

PATENT STATUS· This docunent copy, since it is t ~ansmitted in advance of patent clear~nce, is made available in confidence solely for use in performance of_ work under contracts with \ the U.S. Department of Energy:, This docunent is not to be published nor its contents otherwise ' qisseminated or used for purposes other than specified above before patent approval for such elease or use has been secured, upon request, from the U.S. Depart~t of Energy, Patent Attorney,, Richland Operations Office, Richland, \ IJA.

I

DISCLAIMER· This report was prepared as an account of work sponsored by an agency of the United States Governnent. Neither the United States Governnent nor any agency thereof, nor any of their e,rployees, nor any of their contractors, subcontractors or their employees, makes any warranty, express or i~lied, or assunes any legal liability or responsibility for the accuracy, COf1l)leteness, or any third party's use or the results of such use of any information, apparatus, product, or process disclosed, or represents that its use would not infringe privately owned rights. Reference herein to any specific conmercial product, process, or service by trade name, trademark, manufacturer, or otherwise, does not necessarily constitute or i~ly its endorsement, reconmendation, or favoring by the United States Governnent or any agency thereof or its contractors or subcontractors. The views and opinions of authors expressed herein do not necessarily state or reflect those of the United States Governnent or any agency thereof.

9. !~act Level 2

A-6400·073 (7/90) {EF} WEF124 Supporting Docunent (Cover Sheet)

·10. Authorized Manager's Name B. K. Horsager

Specify Distribution Limit S L

11. RELEASE STAMP

,--. ---I I ·,RELEASED .. i

l DISTRIBUTION LIMITS i j i I • INTERNALONLY_. ;

®jsf'ONSOR LIMITED • EXTERNAL _. __ --_ f

MAR - 8 ---1991 ; ,0

_,,_ DATE; ____ . -~..M:::/0 .-.--:;....i...,.=;;.. ____________ ..

.j

Page 2: -I-Cl l

WHC-SD-W-153-CDR-001 Rev. 0

CONCEPTUAL DESIGN REPORT

TRANSURANIC EXTRACTION PILOT PLANT

PROJECT W-153

WESTINGHOUSE HANFORD COMPANY

for the U.S. Department of Energy Richland Operations Office

Richland, Washington

Prepared by Kaiser Engineers Hanford (Wl53CDR)

Contractor Approval

Company . ,.. .. -----..,_

: J .-:1 , ' ' \_/ 1 (~ ~ . v . . ✓ ~---

Westinghou~e Hanford Company ~

Department of Energy Approval

' . ,~~ ~ U. ~~ Energy

1

Construction Division Richland Operations Office

- i -

I Date

-·7 - ' - (.,) . , -~-~---Date

Page 3: -I-Cl l

"-.-··

Chief Designngineer

J/J1dl)y-Project Manager

WHC -SD-W-153-CDR-001 Rev. 0

Wl53CDR

CONCEPTUAL DESIGN REPORT

FOR

TRANSURANIC EXTRACTION PILOT PLANT

PROJECT W-153

Prepared by

KAISER ENGINEERS HANFORD COMPANY Richland, Washington

for

WESTINGHOUSE HANFORD COMPANY

e- 1-10 ~t:1- 2"-qo

~::R!:=.~~~~t:U<..4..A_~~~ $tt/:-~e Date

I' Id/,<> --¢~ -~ -' Date Quali~ering

?;jN/1° S~{k 'bate Classification R~

Date

g -ll(-'!rJ Date

-~ctlte/10 ~-/3 --9"0 .

Date

r/,,/c0 _ ~

Westinghouse Hanford Company

-Projects Department

- ; ; -

APPROVAL

Page 4: -I-Cl l

· . .._.,

WHC -SD-Wl53 -CDR-001 Rev . 0

TABLE OF CONTENTS

I. · INTRODUCTION

II. SUMMARY .. . .

I I I. . JUSTIFICATION

IV. DESCRIPTION OF PROJECT SCOPE

A. SPECIAL EQUIPMENT/PROCESS SYSTEMS (700) 8. DEMOLITION (810) .

V. METHODS OF PERFORMANCE

A. ONSITE ARCHITECT-ENGINEER WORK (WBS 1.0) B. PROCUREMENT STRATEGY (WBS 2.0) ..... . C. ONSITE CONSTRUCTION CONTRACTOR (WBS 3. 1) D. OPERATING CONTRACTOR (WBS 3.3 and 3.4)

VI. REQUIREMENTS AND ASSESSMENTS

A. SAFEGUARDS AND SECURITY . B. HEALTH AND SAFETY ...... . . . C. DECONTAMINATION AND· DECOMMISSIONING D. PROVISIPNS FOR FALLOUT SHELTERS .... . .. . . E. QUALITY ASSURANCE ACTIVITIES/SAFETY CLASSIFICATION F. MAINTENANCE AND OPERATION REQUIREMENTS G. AUTOMATED DATA PROCESSING EQUIPMENT . . . H. ENVIRONMENTAL COMPLIANCE. . . . . . . . .

VII . IDENTIFICATION AND ANALYSIS OF UNCERTAINTIES

A. JET GANG VALVES .. ... .... .. . B. PIPING AND INSTRUMENT DIAGRAM DRAWINGS C. CELL BOUNDARY CONTAINMENT ...... . 0. NEUTRALIZED CURRENT ACID WASTE . .. . E. AQUEOUS MAKEUP . . . . . . . . . . . . F. SUPPLEMENTAL VENTILATION - WESF AMU AREA G. SUPPLEMENTAL FIRE PROTEGTION SYSTEMS H. EMBEDDED PIPING IN 2218 AND 2258 I . UNSTABLE SOLUTIONS

VIII . REFERENCES . .... . . .

- i i i -

1

1

2

10

12 29

32

32 32 33 33

33

33 33 33 34 34 36 37 37

38

38 39 39 39 39 40 40 40 40

40

Page 5: -I-Cl l

#-~-

l ·, \_ , .

U.AOYM. WHC -SD-Wl53 -COR-001 Rev. 0

TABLE OF CONTENTS (Continued}

APPENDICES

Appendix A. Conceptual Project Schedule Appendix B. Cost Estimate Sunmary/Statement of Work Appendix C. Work Breakdown Structure Appendix D. Outline Specifications Appendix E. Energy Conservation Report and Analysis Appendix F. Environmental Protection Evaluation Appendix G. Economic Analysis and Life Cycle Cost Analysis Appendix H. Plant Forces Work Review Appendix I. Physically Handicapped Assessment Appendix J. Instrumentation Identification Appendix K. Equipment Data Sheets

-Appendtx•--<L1-.--1Aqi-riueous Makeup Description- - 221-B Building Appendix M. Sketches

iv

APPAOVAL

Page 6: -I-Cl l

AMU ANL ANSI ASHE

cc CDR CMPO CRT

DACS DOE

FPMCS

FY

HPT HWVP

KEH

LCU ··~,. MRP

; .. · ~ . '• --

NCAW . NCRW NFl>A NPH

OIS

P&ID P&O PFP PUREX ·

QAPP

RL

TBP TRU TRUEX

WAC WHC

WHC -SD-Wl53 -CDR-001 Rev . 0

ACRONYMS

aqueous makeup Argonne National Laboratory American National Standards Institute American Society of Mechanical Engineers

complexant concentrate conceptual design report N-diisobutylcarbamoyl-methylphosphine oxide cathode-ray tube

Data Acquisition and Control System Department of Energy

facility processing monitoring and control system fiscal year

hot pipe trench Hanford Waste Vitrification Plant

Kaiser Engineers Hanford Company

local control unit

Management Requirements and Procedures

neutralized current acid waste neutralized cladding removal waste National Fire Protection Association normal paraffin hydrocarbon

operator interface station

Piping and Instrument Diagram pipe and operating Plutonium Finishing Plant plutonium extraction

Quality Assurance Program Plan

Richland Operations

tributyl phosphate transuranic transuranic extraction

Washington Administrative Code Westinghouse Hanford Company

- V -

APPROVAL

Page 7: -I-Cl l

WHC -SO-Wl53 -CDR-001 Rev . 0

CONCEPTUAL DESIGN REPORT

TRANSURANIC EXTRACTION PILOT PLANT

PROJECT W-153

I. INTRODUCTION .

The transuranic extraction (TRUEX) process has been recommended for the treatment of neutralized cladding removal waste (NCRW), Plutonium Finishing Plant (PFP), and complexant concentrate (CC) waste on the basis of favorable cold laboratory studies completed prior to fiscal year (FY) 1989. During_ FY 1989, laboratory testing with actual waste solutions further confirmed the viability of the process. Neither the TRUEX process nor the f~ed preparation ope rat i ans have been demonstrated in a plant environment. However, the next major step toward application of the technology to double-shell tank waste is the design, fabrication, and operation of a remote pretreatment pilot plant. A study, WHC -SO-WM-ER-058 Rev. 0, completed in FY 1989, concluded that the most suitable location for the TRUEX Pilot Plant would be in the 225-B Building. A feasibility study, ENG-W-90-32, dated March 7, 1990, conducted by Kaiser Engineers Hanford Company (KEH) reconfirmed that conclusion and has shown that the bulk of the sludge washing/dissolution, and solid/liquid separation equipment can be accommodated in Cell 38 of the 221-8 Building while the TRUEX process itself (centrifugal contactors for solvent extraction and · solvent washing) can be accommodated in Cells Band C of the 225-B Building.

II . SUMMARY

This project will provide a system to demonstrate pretreatment of neutralized cladding removal waste (NCRW), Plutonium Finishing Plant (PFP), .and complexant concentrate (CC) waste which will include sludge dissolution, sol id/1 iquid separations, and the transuranic extraction (TRUEX) process. The initial design is geared toward NCRW

Wl53CDR.TD.1825 - 1 -

APPROVAL

09/90

I

- I

I

Page 8: -I-Cl l

_,,,,,.........,..,, i

(·'"-

.. --~ ;.•

WHC-SO -Wl53 -C0R-001 Rev . 0

and it is anticipated that some minor modifications to equipment will

be required to process PFP and CC solids. In addition to providing a facility to aid the design and operation of the full-scale process , the pilot plant will produce feed material for glass waste form qualification (the equivalent of 200 kgs of glass-forming oxides for

each of the waste types) .

Modifications to the 221-B Building and the 225-B Building will be necessary to confirm the TRUEX process. The TRUEX process in the 221-B and 225-B Buildings will be performed as described in figures 1.1 through 1.7. The modification will require a complete renovation of Cell 38 in the 221-B Building and modifications to Cells Band C in the 225-B Building facility, utilizing some existing equipment.

The total estimated cost of this project is $25,100,000.

III. JUSTIFICATION

Conducting pi 1 ot seal e pretreatment demon strati on wi 11 reduce the cost and schedule risk to the TRUEX production facility project by providing a firm basis for full scale design and hands-on experience with the technology and equipment required to operate and maintain the full-scale facility. Scheduled operation of the Hanford Waste Vitrification Plant (HWVP) is dependent on a reliable feed stream of pretreated waste. While it is possible to design a full-scale process from laboratory data, the risks involved in the scale-up, without the support of pilot plant data, are in this case unaccept ­able. Eliminating problems discovered at the pilot plant level would support the full scale design/schedule, thus avoiding process data accumulation that could impact design/schedule of the full -scale-22't-­B Building modifications. In addition, the pilot plant will produce feed material for the hot laboratory and bench-scale glass waste form qualification program being conducted in the 324 Building.

Wl53CDR. TD.1825 - 2 - 09/90

Page 9: -I-Cl l

):a, "tJ CHEMICAL "tJ AOOITI0N

:D

! r-

26

SOLIDS RECYCLE

SLURRY WATER

DECANT

TO TANK FARMS

Ct£MICAL ADDITION

·:u, EXISTING VESSEL

• ~SEL

RCVR TK- 11 -2 ANO/OR TK- l6-J

Tl<- 25-2

STORAGE TK-J6-I • TK-l6-2

CHEMICAL AOOITIOH

41r----... HN03 TK-C-I 15 Gal

DISSOLVER FEED

· FILTER RINSE

COOLING WATCR

DISSOLVER----. OFTCAS

BACKfLUSH AIR

SCljUB WATER

TO VESSEL VOH SYSTEM

T~~:..1 t---~ 50 Gal

CHEIIICAL ADDITION

CHEIIICAL ~ ADOITlbH ~

TO TK-39- 1

F-~-l ,-------p~m,NC

12

FILTER t------1. 9 >-----+t fl~~iE t------~ 1=-a~-1 f~3tt

SOI.IDS

TO VESSEL VENT SYSTEM

10

SOLIDS RCVR

Tl<-l8- 5 225 c.,

CHEMICAL ADDITION

----\54 ---~~lflTE.,.._ ______ -\45 >-----. woL1¥0R M---~ Tl<-Je-6

STORAGE TK- JS-1

225 c.,

TO 212-8

-+-WES!'

COOLING WATER

NIC03 TK-C-2 15 Cal

il:W Tl<-8-l 15 Got

24 21

REVISED 6-29-90

SOLVEHT CLEAN·

UP

SOlVENT STORAGl .---------< CHEMICAL

ADDITION lfb-Cci!i

SOLVEHTM---­EXTRAC·

TION

-@- JTRII'

-;=;@-~9 5CRU4I II ~ 5CRU. 12

PROCESS FLOW DIAGRAM

TRUEX PILOT PLANT

lT1 w I

("") c:::, ;::c I

0 0 __,

;::c CD <

0

Page 10: -I-Cl l

,.;,

l

08/24/90 09:14 Nf

I SiREAH ~ .--~-. ?EAH NA.'£

-

T~. Deg C Pres. ~1a ~ity ml Vo une Liters

Al Grans B GrllllS Ba Grams

Ca GrllllS Ce Grams Cr Gnms

Fe Gnms K Grams La Grams --:m Grams

Grans Mo Grams

Na Grans Nd Grams Ni Grams

Rh Gnms Ru GrllllS Si Grans ------Sr GrllllS Te GrllllS Ti Grans

u Grcl!IS Zn Grams Zr Grams

. "'l: GrllllS · . 35 Grams '·· . 95 Grams -----------Rul06 Grams Sbl25 Grams Csl34 Grans

Csl37 Grams Cel~ Grcl!IS Co60 Grams

Eu154 Grcl!IS EulSS Grans Pu238 Grans --Pu239 Grams Pu240 Gnms Pu241 Grams

Pu242 Grams AmZ41 Grams HZO Grams

I¼+ Grans OH- Grams F- Grmns

Cl- Grams HOZ- Grcl!IS N03- Grans --S04-2 Grans NH3 Grcl!IS C03-2 Gnms

HH03 Grams NH4+ Grams CO2 Grcl!IS • --HOx Grcl!IS ··~ Grams

Grams ·-

H2C204 Grans HEDPA Gr1111S Cli'O Grlll1S --TBP Gr1111S NPH Grns. TOTAL Grcl!IS

1

ADJUSTED FEED

25.0 14 .7

1.2000 8.33E- 02

4. 00E-02 4. 00E-02 1.00E-02

5. 00E-02 l . OOE-10 l.OOE-02

2. 00E-OZ l.63E+OO 4. 00E-02

l . OOE-02 l.OOE-10 1.00E-10

6.30£+00 l.OOE-02 l. OOE-10

2.00E-02 1.00E-02 4.30(-01

l.OOE-10 l.OOE-10 1.00E-10

3.20£-01 l.OOE-10 5.69E+OO

l.OOE-02 4.05£-07 3.71E-07

l.34E-06 8.49£-07 1.45£-07

3.26£-07 2.31E-06 l.42E-08

l.OOE-10 l.OOE-10 1.90E-07

S.31E-04 3.89£-05 4.65£-06

2.lBE-07 l.12E-06 7.60E+Ol

l. OOE-10 4.37E+OO 4.07E+OO

2.00E-02 1.40E-Ol 4.BOE-01

1.00E-02

2.3~-01

2.00E-02

----~ ---

---l.OOE+OZ

2 3

RE'TRIEVAL RE'TRIEVED WATER SLI.DiE -25.0 25.0

14 .7 14 .7 1.0000 1.0500

2. SOE-01 3.33E-Ol

4.00E-02 4. 00E-02 1.00E-02

5.00E-02 l.OOE-10 l . OOE-02

2. 00E-02 l.63E+OO 4. 00E-02

l.OOE-02 1.00£-10 l.OOE-10 ------6.30E+OO 1.00E-02 l.OOE-10

2. 00E-02 l.OOE-02 4.30E-0l

l.OOE-10 1.00£-10 1.00E-10

3.20£-01 1.00E-10 5.69E+OO ---,-----l. OOE-02 4. 05£-07 3.71E-07 ---1.34(-06 8.49E-07 1.45£-07 ---3.26£-07 2.31E-06 l . 42E-08

l.OOE-10 l.OOE-10 1.n-01 ---5.31E-04 3. 89E-05 4.SSE-06 -----2.lBE-07 l.lZE-06

2.SOE+OZ 3.26E+02

1.00E-10 4.37E+OO 4. 07E+OO ------2. 00E-02 l.40E-01 4.SOE-01 --- · 1.00E-02

2.3~-01. ---2.00E-02

---

-----

----2.SOE+02 3.SOE+OZ

APPROVAL FIGURE 1.2

4 5

DECANT ACID

---25.0 25 .0 14.7 14.7

1.0000 1.3505 6. llE-02

---.

------- ---

----

---

3.SSE+Ol

---

---4.70E+Ol

---

~-- . r

6 7

DISSCl.VER DISSCl.VER PRIXlX:T OFFGAS ---

25.0 25 .0 14.7 14.7

1.0965 0.0017 4.81E-Ol l.07E-Ol

WHC-SD-W153~CDR-001 Rev. 0

S1£ET l OF 6

8 9 10

FILTER FILTRATE SOLIDS RINSE ---

25. 0 25 .0 25.0 14.7 14.7 14.7

1. 0338 1.0618 2.0000 9.37E-02 5. 59E-Ol l.57E-02 ---------------6.06£-02 4.24E-02 1.82E-02

4.SSE-02 4.39E-02 4.88E-03 l . 22E-02 l.lOE-02 l.22E-03 ----- -6.1~-02 S. 49E-02 6.lOE-03 1.42£-10 9.91E- ll 4.ZSE-11 l.ZZE-02 l. lOE-02 l.22E-03 ---- ----2. 44£-02 2.20E-02 2.44E-03 l.BlE+OO l.BlE+OO 5.SOE-02 3.BSE-02 1. 6SE-02 ---- --- --l.22E-02 l. lOE-02 1.22E-03 1.22£-10 l.lOE-10 1.22E-ll l.SZE-10 1.06£-10 4.55E-ll -----7.00E+OO 7. 00E+OO 1.06£-02 l.03E-02 3. lBE-04 · 1.14E-10 l.llE-10 3.43E-12 ------ -3. 03E-02 2. 12E-02 9.09E-03 l.SOE-02 l.OSE-02 4.49E-03 5:24E-Ol 4.72£-01 5.24E-02 ---- ------ -----1.ZZE-10 l. lOE-10 l.ZZE-11 l.SZE-10 1.06£-10 4.SSE-11 l.SZE-10 1.06£-10 4.SSE-11 ----------3.65£-01 3. 54E-01 1.lOE-02 l.14E-10 l.llE-10 3.43E-12 6. 62E+OO 6.29E+OO 3.31E-Ol ------ -l.llE-02 l. llE-02 5.47E-07 4.38E-.07 1. 09E-07 5.0lE-07 4. 0lE-07 1. OOE- 07 ---- ------ ------l.79E-06 · l.43E-06 3.57(-07 l.lSE-06 9.lBE-07 2.JOE-07 1.96£-07 l.57E-07 3.92E-08 ---- ------ ------4.41E-07 3.53E-07 8.SlE-08 2.91E-06 2.33E-06 S.82E-07 l.92E-08 l.54E-08 3.84E-09 --- ----- -------1.25£-10 9.99E-11 2. 50€-11 1.25£-10 9.99E-ll 2.SOE-11 2.SOE-07 2. 0SE-07 4.SOE-08 ------6.99E-04 5.73(-04 1.26£-04 S.12E-05 4.20E-05 9.22E-06 6.12E-06 5.0ZE-06 l.lOE-06 ---2. 87E-07 2.JSE-07 S.17E-08 1.32E-06 l.23E-06 9.23(-08 4.49E+02 2.92£-03 9.0SE+Ol 5.l3E+02 2.70E+Ol ----S.87E-Ol . . 6.47E-OI 3.41E-02

4.SZE+OO 4.S2E+OO --- -----2.22£-02 2.22E-02 1.38£-01 1.38E-Ol 5.58E+Ol 5.BSE+Ol 3.CEE+OO --- ---- ---1.llE-02 1.llE-02

S.90E+OO 2.22£-02 2.ZZE-02

1.70E-01 --- ---- ---- -----1.27E-02

6.44E-Ol 1.95£-01 ---- --- -----

2.24E-02 2.24E-02 l.27E-Ol 1.27E-Ol 5.72E-03 5.72£-03 ---- ------- --------- -------

· 2. 61E-02 2.61E-02 2.0BE-02 2.0SE-02

8.2SE+Ol 5.27E+02 l.86E-01 9.67E+Ol 5.93E+02 3.14E+Ol

APPROVAl-

Page 11: -I-Cl l

~

08/24/90 09:14 AM

I STREAM NlH!ER -~ . :£AH IW£

T~. Deg C Press . ~1• Density ml Vo lune Lt ten - ----Al Grams B Grams Ba Grams

Ca Grans Ce Gnms Cr Grans

f'e Grans K Grans La Grans -Hg Gras Mn Grams Mo Grans

Na Grans Nd Grns Nt Grans ----Rh Grams Ru Grams Si Grams

Sr Grans Te Grans Ti Grans ------u Grams Zn Grams Zr Grams ---'C Grans

, -l ~~ Grams Grams

Rul06 Grams Sbl25 Grans Csl34 Grans

Csl37 Grans Cel44 Grams Cc60 Grams --·- -Eul54 Grans Eul55 Grams Pu238 Grams

Pu239 Grams Pu240 Grams Pu241 Grns --Pu242 Grams Am241 Grams HZO Grams -----I+.- Grams OH- Grams F- Grans ----Cl- Grams N02- Grams N03- Grams

S04-2 Grams NH3 Grams C03-2 Grams

HN03 Grams NH4+ Grams CO2 Grams

NOx Grans 'Z Grams J2 Grams -------H2C204 Gran:s HEDPA Grans OflO Grans -- --TBP Gran:s NPH Grams TOTAL Gran:s

11

OiEMICAI. AODITiaf

25.0 14 .7

1.0000

---

--

--

------

-

-· ---

~ ,.

12 13

FILIERED TIU.O TRLEX FEED FEED

25.0 25. 0 14.7 14 . 7

1.0618 1.0618 5.59£-01 5.59£-01 -4.24E-02 4.24E-02 4.39E-02 4.39£-02 l.lOE-02 l.lOE-02

5. 49E-02 5.49E-02 9.91E·ll 9.91£-11 l.lOE-02 l. lOE-02

2.20E-02 2.ZOE-02 l.BlE-+-00 l.BlE-+-00 3.BSE-02 3.BSE-02 ---l.lOE-02 l. lOE-02 l.lOC-10 l.lOE-10 1.06£-10 1.06£-10

7 .OOE-+-00 7.00E-+-00 l.03E-OZ l.03E-02 l.llE-10 l.llE-10

2.12E-02 Z. 12£-02 l.OSE-02 l.OSE-02 4.72E-Ol 4.7ZE-Ol

l.lOE-10 l. lOE-10 1.06£-10 l.06E-10 l. 06£-10 1.06£-10

·3.54E- 01 3.54E-Ol 1.llE-10 1.llE-10 6.29E-+-OO 6.29E-+-OO ---l.llE-02 l.llE-02 4.38£-07 4.38£-07 4.0lE-07 4.0lE-07 ---1.43E-06 l.43E-06 9.l&-07 9.l&-07 l.57E-07 1.57£-07

3.53£-07 3.53E-07 2.33E-06 2.33E-06 l.54E-08 l.54E-QJ

9.99E-ll 9.99E-ll 9.99E-ll 9.99E-ll Z.OSE-07 2.0SE-07

5.73E-04 S. 73E-04 4.ZOE-05 4.ZOC-05 5.02£-06 S.OZE-06

2.35E-07 2.3SE-07 l.23E-06 1.23E-06 5. 13E-+02 5.13E-+02

6.47£-01 6.47E-Ol

4.SZE-+-00 4.52£.00

2.22£-02 2.22£-02 1.38£-01 1.38£-01 5. BSE-t-01 5.BSE+ol

1.llE-02 l.llE-02

2.22£,-02 2.ZZE-02

----- -----2.24E-02 2.24E-OZ l.27E-Ol l.27E-Ol 5. 7ZE-03 5.72E-03 ---2.SlE-02 Z. SlE-02 2.ret-02 2. OSE-02 5.93E+OZ 5.93E+02

APfr~f~3

u 15 16

SOCVENI SPENI EXTRACT. CCXI.ING CCXI.ING

FEED WATER WATER ---25. 0 25 .0 25 . 0 14.7 14.7 14 .7

1.0618 l.0000 l.0000 5.59£- 01 ------4.24E-02 4.39E-02 l . lOE-02 --5.49E-02 9.91£-11 l.lOE- 02 ---2.ZOE-02 l.Slt-+-00 3. BSE- 02 -l.lOE-02 l.lOE-10 1.06£-10

7 .OOE-+-00 1.03E-OZ l . llE-10. ------Z.lZE-02 I.CSE-OZ 4. 7ZE- Ol ----l.IOE-10 l.06E-10 1.06£-10 -------3.S4E-Ol 1.llE-10 6.29E+OO ---- ---- ---l.llE-02 4.38£-07 4.0lt-07 ---l.43E-06 9.l&-07 1.57E-07 ---3.53[-07 -2.33E-06 l.54E-08 ---9.99E-ll 9.99E-ll 2. 05£-07

5.73E-04 4.2!1:-0.S 5.0ZE-06 --- ----2.3SE-07 1.23E-06 5.13E+02

6. 47£-01

4.SZE.00

2.22£-02 1.38£-01 5.8SE+ol ---l.llE-02

---2.ZZE-02

------

----2.24E-02 l.27E-Ol 5.72E-03 ------- ----Z. SlE-02

.

2.0SE-02 5.93E+OZ

Afilrn " \lA6. -

WHC-SD-W153-CDR-001 Rev. 0

S1££T Z OF 6

17 18 19 20

STRIP SCRUB SCRUB TRU #1 #2 PROOUCT

25 . 0 25.0 25. 0 25.0 14 .7 14 .7 14 .7 14 .7

1.0500 1.0800 1.0000 1.0618 2.79E-02 4.47£-02 4.47E-02 4.36E-02 ------ --4.9SE-13

5. 13£-13 1.2&-13 -----6. 41E-13 4. 02E· ll 5. 2&-16 - --- ----5. 13E- 10 Z. llE- 11 2. SZE-02 --- ---l.28E- 13 1.2&- Zl l.OSE-14 ---- -----3.37E-13 4.37E-03 · ~-33E-24 --- --- ---4.49E-09 6.69E-04 5.SlE-12 --------- - ·----1.ZSE-21 l.24E-21 l.24E- 21 --- ---- ---- ----4. l4E-12 l.29E-21 4.02E-04 ------ -----l.02E-14 9.38£- 15 --- ---- ---9.13E-08 l.C7E-17 l.83E- 18 ---4.lZE-18 9.46E-07 l.7SE-19 - ·--·- ---4.91E-ll 4.91E-ll 9.23£- 09 ---2.SSE-05 1.89E-06 2.26E-07 . ------1. 06£-08

2.BZE+ol 4.38E+ol 4. 47E+ol 6.75E-08 4.S7E+ol -- ----6.76E-OZ.

7.3ZE-14 ---3.SOC- 16 2.24E-15

4. 16E-+-OO 1. OlE-12

l.BOC-16

----------

---2.0lE-01 5. 67E-06 l.lSE-+-00

5.69E-OZ ---- --Z.SOE-01-Z.07E- Ol

2.93E+ol 4.83E-t-Ol 4. 47E-t-Ol 4. 63E-t-Ol

.

.-! •

.,...

I

J ~-- j

Page 12: -I-Cl l

I

08/24/90 09:14 AN

SlREJ\14 NlH!ER ,,.-:· , - '.

... . .::AM NAI£

T911>. Deg C Preu. ~la Oens'ity ml Volune Liters ----Al Grams B Grams 8a Grams -Ca Grams Ca Grans Cr Grams

Fe Grams K Gnms La Grams

~ Grans Grans

Mo Grans -----·-Na Grans Nd Grans Ni Grams

Rh Grans Ru Grans Si Grans --Sr Grans Te GrllllS Ti Grans

u Grans Zn GrllllS Zr Grans -·---.,. GrllllS

JS Grans · Zr"35 Grans

Rul06 GrllllS Sbl25 Gr.ms Csl34 Grns --Csl37 Grans Cel44 Grans Co60 Grns

Eul54 Grams Eul55 Gnms Pu238 Grans

Pu239 GrllllS Pu240 Grans Pu24l Grans

Pu242 Grans Am241 Grams HZO GrllllS

t++- Grams OH- Gnms F- Grams

Cl- Grams HOZ- Grns H03- Grams --S04-2 Grams NK3 Grams C03-2 Grams

Hfl03 Grams NH4+ Grans CO2 Grams

"!Jx Grams GrllllS

/. Grams . . ----H2C204 Grams HEOPA Grmis CMPO GrllllS -------------TBP Gram.

NPH Grams TOTAL Gram

21 22 23

RAFFINATE ~~IC ~~IC FEED -25.0 25.0 25.0

14.7 14 .7 14.7 1.0618 0.7500 0.7500

6.31E-Ol l.~-01 1.39E-Ol

4.24E-02 2.-49£-20 4.39E-02 2.57E-20 l.lOE-02 6.43£-21 ---5.49E-02 3.22E-20 3.30E-ll 2.59E-ll l .10£-0Z 6.92E-25 ---2.20E-02 3.84E-15· l.BlE-+-00 l.OSE-18 l.27E-03 l.llE-02

l. lOE-02 6.43E-21 l.lOE-10 6.43E-29 l.06E-l0 7.66E-l6

7. OOE-+-00 4.41E-22 3.23E-03 2.70E-03 l.llE-10 6.98£-33

2.12E-02 4.BSE-13 9.14E-03 6.56E-04 4.72E-Ol z.nE-19 ---l.lOE-10 . 6.43E-29 l.OSE-10 6.22E-29 l.OSE-10 6.ZZE-29 ------3.54E-Ol 2.0SE-19 l. llE-10 6.49E-29 6.29E-+-OO 4.BSE-11 ---l.llE-02

. 4.3&-07 7.66£-20 4.0lE-07 7.0lE-20

l.25E-06 &.96E-08 9.lBE-07 5.38E-25 l.57E-07 9.l9E-26

3.53E-07 2.07E-25 7.76f.-07 6.ll&-07 l.54E-08 9.00E-27

2.41E-ll 2.68E-ll 2.41E-ll 2.68E-ll l.96E-07 3.13E-l2

5.47E-04 8.76E-09 4.0lE-05 6.42E-10 4.79E-06 7.67E-ll

2.25£-07 3.60E-l2 l. lSE-06 l.07E-l0 5.84E-+-02 l.4SE-01

7 .lSE-01

4.52E-+-OO 4.64E-23 ---2.ZZE-02 2.28E-25 l.38E-Ol 1.42E-24 6.26E-t01 6.43E-22

l.llE-02 l.l4E-25

Z.ZZE-02

~

2.24E-01 3.60E-15 l.27E+OO 6.42E-03 S.72E-02 1.14E-t01 1. 13E-t01 ----2.61E-01 5.20£1-01 5.1SE-tOl 2.0SE-01 4.14E-t0l 4.10£1-01 6.70E+02 l. OSE-+-02 1. 04E-+-02

APP~~ 1_4 WHC-SD-W153-CDR-001 Rev. 0

St£ET 3 OF 6 ... ,

24 25 26 27 28 29 30 IRO l«Jx WNUENSCR SPENI

TRU TO Sil.IDS SCRUBBER CONOEN- CCO..ING CCO..ING PRID.CT Slav.GE RECYCI.! FEED SATE Ii/ATER WATER ------ --- ---25.0 25.0 25.0 25.0 25.0 25 .0 25.0

14 .7 14.7 14.7 14 .7' 14.7 14.7 14 .7 1.0618 1.0618 2.0000 1.0000 1.0000 1.0000 1.0000

-4.36E-02 -4.64E-OZ 2.31E-OZ 1.83E-04 2.92E-06 ------ ---------4.95£-13 1.82E-03 1. 64E-02 S.13E-13 4.BSE-04 4.39£-03 · 1.28E-13 1.22E-04 l.lOE-03 -- ---6.41E-13 6.lOE-04 5.49£ .. 03 4.02E-ll 4.4SE-11 3.82E-ll S.28E-l6 l.22E-04 l.10£-03 --- ---- ---5.l3E-10 2.44E-04 2.ZOE-03 2.llE-11 2. llE-11 2.SZE-02 2.78E-OZ 1.48£-02 --- ---- ---- -----l.ZSE-13 l.22E-04 l. lOE-03 l.28E-21 l.22E-l2 l.lOE-ll l.OSE-14 4.SSE-12 4.09E-ll ------ --- -----3.37E-l3 3.37E-13 4.37E-03 4.40E-03 2.87E-04 5.33E-24 3.43£-13 3.0SE-12 - --- ------ ----4.49£-09 9.09E-04 8. lSE-03 6.69E-04 l.l2E-03 4.04E-03 5.SlE-12 5.24E-03 4.72£-02 ------ ---------l.ZSE-21 l.22E-12 l.lOE-11 1.24E-21 4.SSE-12 4.09E-ll l.24E-21 4.SSE-12 4.09E-ll --------- - ----- -----4.14E-12 l. lOE-03 9.86E-03 1.29E-21 3.43E-13 3.0BE-12 4.02(-04 3.35E-02 2.98E-Ol ---- -------- -1. OZE-14 l.09E-08 9.SSE-08 9.38E-15 1. OOE-08 9.0JE-08 --- ---- --- ---- --·---9.13E-08 1.27E-07 3.22E-07 1. 07E-17 2.30E-08 2.07E-07 l.83E-l8 3.92E-09 3.53E-08 ------4.lZE-18 8. BlE-09- 7.93E-08 9.46E-07 l.OOE-06 5.24E-07 l.79E-19 3.84E-10 3.4SE-09 -4.91E-ll 5. l&E-11 2.2SE-11 4.91E-ll 5. l&-11 2.25£-11 9.23£-09 l.37E-08 4.0SE-08 --- ---2.SSE-05 3.84E-05 1.13E-04 1.89E-06 2.BlE-06 8.30E-06 2.26E-07 3.36E-07 9.92E-07 ---l.06E-08 1.SBE-08 4.6SE-08 6.7SE-08 7.67E-08 8.31E-08 4.57E-t0l 4.84E-t0l 2. 43E-t01 2.92E-03 -------3.41E-03 3.06E-02

7.32E-14 7;32E-14 --- ---- ---3.60E-16 3.SOE-16 2.24E-15 2.24E-15 l.OlE-12 3. 0SE-01 2. 77E-+-OO ---l.BOE-16 1. 80£-16

--- ---l.70E-Ol

- ------ ---l.27E-02

--- ---------- -------- ---- -------S.67E-06 5. 67E-06

5.69E-02 S. 69E-OZ ------ --------- --- ----2. 60E-Ol 2.60E-Ol 2.07E-01 2.07E-Ol 4. 63E-t01 4.93E-t01 2.7SE+Ol l.83E-Ol 2.92E-03

- ~ -

,., .. rnUY~L

Page 13: -I-Cl l

08/Z4/90 09 :14 N4

. L~!REAH NlH!ER

.. ,REAHHM

T~. Deg C Press. ~14 Density ml Volune Liters

Al Grans B Grams Ba Grams

ca Grams Ce Grans Cr Grans --Fe Grans K Grans La Grans --~ Grans

Grams Ho Grams

Na Grams Nd Grams NI Grams

Rh Grans Ru Grams Si Grams --Sr Grams Te Grans Ti Grans

u Grims Zn Grans Zr Grans

. Grams .,o95 Grams Zr95 Grams --------Rul06 Grams Sbl25 GrilfflS CslJ4. GrilfflS

Csl37 Grans Cel44 GrilfflS Co60 GrilfflS --Eul54 Grams EulSS GrilfflS Pu238 Grans -------Pu239 Grns Pu240 Grams Pu241 Grans

Pu242 GrilfflS M1241 Grams H20 Grans

If+ Grams OH- Grams F- Grams

Cl- Grams N02- Grans N03- Grams

S04-2 Grams NH3 Grams C03-2 Grams

HN03 Grams NH4+ Grans CO2 Grams ' ')x Gran:s , Gran:s uz GrllllS ---------H2C204 GrllllS

HEIYA GrllllS 01PO Grans --TBP Grans NPH GrllllS TOTAL Grans

31

NOx ~us ---25.0

14 .7 1.0000

3.31E-03 ---

-------

3.31E+-OO

...

-----3.31[+00

32 33 34 35

SCRlJ!SER SCRL8BER TO FRESH Bl.CMXMC OFFGAS TK-39-1 ORGANIC --- ---25.0 25 .0 25.0 25.0

14.7 14 .7 14.7 14 .7 1.0000 0.0016 1.0000 0.7500

3.33£-03 1.34£-01 3.33(-03 l.40E-03 ---

---

---- -------- ------

------------------- ---

--- ------

---

-----·--3.31[+-00 3.37E-03 3.31E+-OO ---3.34£-04 3.34£-04

----2.0SE-02 2.0SE-02 ----

---· l.70E-0l ---

1.27(-04 3.52E-02 5. 40E-03 ---- ---

l.14E-Ol------ ---5.22(-01 4. lSE-01

3.33E+OO 2.14£-01 3.33E+OO l.OSE+-00 .a ....... ·- ......... ____,.. -

•L , !;--' t

WHC-SD-W153-CDR-001 Rev. 0

St££'T 4 OF 6

36 37 38 39 40 SOCvENI ClEAHI.P CARBONATE CARBONATE SPENT CARBONATE mo ADOlTION ~us CARBONATE WASTE ---------25 .0 25.0 25.0 25 .0 25.0

14.7 14.7 14.7 14 .7 14 .7 0.7500 1.0269 1.0269 1.0269 1.0269

1.39£-01 1.12£-03 2.79E-02 2. 79E-02 l.12E-03 ---2.49E-20 2.57E-20 6.43£-21 --- ------3.22£-20 2.59E-ll 6.92E-25 ----- ---3.84E-15 l.06£-18 l.llE-02 --- ----6.43(-21 6.43E-29 7 .66E-16 --- ------ ----4.41(-22 l.ZBE-02 3.ZlE-01 3.ZlE-01 1.ZBE-02 · 2.70£-03 6.98E-33 --- ---4.BBE-13 6.56£-04 2.77E-19 --- ------6.43(-29 6.22E-29 6.22£-29 ---- ----- -----2.0SE-19 6.49E-29 4.SSE-11 ----7.56£-20 7.0lE-20 ---- -------8.96£-08

· 5.38E-25 9.19(-26 ---2.07E-25 6.0SE-07 9.00£-27 ----2.68(-11 2.68(-11 3.13£-12 ---- ---8.76£-09 6.42E-10 7.67(-11

3.St{-12 1.07(-10 l.4SE-Ol . l.12E+OO 2.79E+Ol 2. 79E+Ol l.12E+OO --- --.- ---4.64E-Z3 --2.28E-25 l.42E-24 6.43E-22

1.14£-25

l.SSE-02 4. l9E-01 4.19E·Ol . l.SSE-02 ------ ---

---·- ----3.St{-15 6.42E-03 l.13(+01

-5.lSE+Ol 4.10£+01 l.04E+02 1.lSE+OO 2.87E+Ol 2.87E+Ol . l.lSE+OO

· 1

I

Page 14: -I-Cl l

08/24/90 09:14 AM

I. S~NueER

EAHNA.'£

-T~. Deg C Press. ~la ~ity ml o une Liters

Al Grans B Grns Ba Grams

Ca GrllllS Ce GrllllS Cr Grns -Fe GrllllS K GrllllS La Grams

~ Grams Grns

Ho GrllllS

Na GrllllS Nd Gram Ni GrllllS -----Rh GrllllS Ru Grams Si Grams

Sr Gr1111S Te ·Grams Ti Grams

u GrllllS Zn Grams -Zr Gr~

, - ..,. Grams 5 Grams

_,:l5 Gram

Rul06 Grarn:s SblZS GrllllS Csl34 Gram --Csl37 Grams Cel44 Grams Co60 Grams

Eul54 Grams Eul55 Gram Pu238 Grams --Pu239 Gram Pu240 Grams Pu241 Grams

Pu242 Grans M1241 Grans H20 Gram

t++- Grams OH- GrllllS F- Grans

Cl- Grams N02- Grams N03- Grams

S04-2 Gram NH3 GrllllS C03-2 Grams

HN03 Grns HH4+ Grams CO2 Grams

NOx Grams , Gram Gram

... ---H2C204 Grams HEOPA Grams 01PO Gram ---TBP Grams NPH Grl!IIIS · TOTAL Grams

,: 41 42 43.

ACID ~ID SPENT AOOITillt SCUJS ACID --

25 .0 25.0 25.0 14 . 7 14.7 14.7

1.1955 1.1955 1.1955 7.SlE-04 l.SSE-02 l.86E-02 --------

---------~

--------

---

- ------

6.09E-01 1.52£+01 1.52£+01

4.62£-03 l.l3E-Ol l.12E-0l

---2. 84E-01 6.93E+OO 6.92E+OO

--- ---- -----

----8.98E-0l 2. 23E+Ol 2. 23E+Ol

44 45 46

ACID NON RNRIC WASTE TRU ------

25.0 25.0 25 .0 '14.7 14.7 14 .7

1.1955 1.0619 1.0619 . 7. 4SE-04 6.33E-0l 6.33E-02

4.24E-02 4.24E-03 4.39E-02 4.39£-03 l.lOE-02 l.lOE-03 --- . 5.49£-02 5.49£-03 3.30E-ll 3.30E-12 1.lOE-02 l.lOE-03

2.20E-02 2.20E-03 l.81E+OO l.81E-0l

. l.27E-03 l.27E-04 ---- ---l.lOE-02 l.lOE-03 l.lOE-10 l.lOE-11 1.06£-10 l.06E-ll ---7.0ZE+OO 7 .02E-0l 3.23E-03 3.23E-04 l.llE-10 1.llE-11 ------2.12E-02 2.12E-03 9.14[-03 9.14E-04 4.72E-0l 4.72E-02

l.lOE-10 l . lOE-11 l.06E-10 l.06E-ll 1.06E-l0 l.06E-ll ---3.54E-0l 3.54E-02 1. llE-10 l . llE-11 6.29E+OO 6.29E-0l

1.llE-02 1.llE-03 4.38E-07 4.38E-08 4.01£:-01 4.0lE-08

l.2SE-06 l.25E-07 9.18£-07 9.l&-08 l.57E-07 1.57[-08

3.53E-Ol 3.53E-08 7.76E-07 7 .76E-08 l.54E-08 l.54E-09 --- ---2.41E-ll 2.41E-12 2.41E-ll 2. 41[-12 l.96E-07 1.96(-08 -----5.47E-04 5.47E-0S 4.0lE-05 4. 0lE-06 4.79E-06 4.79£-07

2.2SE-07 2.2SE-08 l. lSE-06 l.lSE-07

6.09E-Ol 5.85E+02 5.85E+Ol -4.SOE-03 7 .l9E-0l 7.19£-02

. 4.52E+OO 4.52E-0l

2.22E-02 2.22E-03 l.38E.:.01 l.38E-02

2.nE-01 6.29E+Ol' 6.29E+OO --l.llE-02 l.llE-03

l.6&-02 l.liBE-03

2.22E-02 2.22E-03

-

- ----- -----2.24[-01 2.24[-02 l.27E+OO l.27E-0l 5.72E-02 5.72E-03 ----2.61(-01 2.SlE-02 2.08£-01 2.08£-02

8.90E-0l 6.72E+02 6.72E+Ol

-WHC-SD-W153-CDR-001 Rev. 0

S>EET 5 OF 6

47 48 49 so IOI- NOH NOH

TRU TO TRU TO TRU TO TRU TO TIC 31H,Z TIC 25:-1 TAttC FARM 212-B ---

25.0 25. 0 25.0 25 .0 14.7 14.7 14. 7 14 .7

1.0619 1.0619 1.0619 1.0618 6.87E-Ol 7.06E-0l 7.06E-0l 4. 64E-02 ------3.82E-02 3.82E-02 3. 82E-02 l .82E-03 3.9SE-02 3.9SE-02 3.95E-02 4.88E-04 9.88£-03 9.88£-03 9.88£-03 1.22E-04 ---4.94£-02 4.94E-02 4.94E-02 6. lOE-04 2.97E-ll 2.97E-ll 2.97E-ll 4.45E-ll 9.88£-03 9.BBE-03 9.BBE-03 l.22E-04 ----1.9&-02 l .9&-02 l.98£-02 2.44E-04 l.63E+OO l . 63E+OO l. 63E+OO 2.llE-11 l.14E-03 l.14E-03 l.14E-03 2.78£-02 ---- ----9.88£-03 9.BBE-03 9.BBE-03 1.22E-04 9.BBE-11 9.BBE-11 9. BBE-11 l.22E-12 9.SSE-11 9. SSE-11 9. SSE-11 4. 56£-12 --------- -----4.21E+Ol 4.21E+Ol 4.21E+Ol 3.37E-13 2.90E-03 2.90E-03 2.90E-03 4.40E-03 9.97E-ll 9.97E-ll 9.97E-ll 3.43E-13 ---l.91E-02 1.91E-02 l.91E-02 9. 09E-04 8.23E-03 8.23E-03 8.23E-03 l.12E-03 4.25E-0l 4.25E-0l 4.2SE-0l 5.24E-03 -9.BBE-11 9.BBE-11 9.BBE-11 1.22E-12 9.SSE-11 9.5SE-ll 9. 5SE-ll 4.5SE-12 9. SSE-11 9.SSE-11 9.SSE-11 4. SSE-12 --- ------ ---.----3.l9E-0l 3.19£-01 3.l9E-0l l.lOE-03 9.97E-ll 9.97E-ll 9.97E-ll 3.43E-13 5. 66[+00 5. 66[+00 5.66[+00 3.35E-02 ---- --- ------l.OOE-02 l.OOE-02 1. OOE-02 3.94£-07 3.94£-07 3.94£-07 1.09E-08 3.61E-07 3.61E-07 3.61E-07 l.COE-08 --- ------ ----1.lZE-06 l.12E-06 l.l2E-06 l. 27E-07 8.26E-07 8.26E-07 8.26E-07 2.30E- 08 l.41E-07 l.41E-07 l.41E-07 3.92E-09 ---3.17E-07 3.l7E-07 3.17[-07 8.81[-09 6.9&-07 6.9&-07 6.9&-07 l.OOE-06 l.38E-08 l.38E-08 l.38E-08 3.84E-10 ------2.m:-11 2.17E-ll 2.17E-ll 5. lSE- 11 2.17E-ll 2.l7E-ll 2.l7E-ll 5.16£-11 l.76E-07 l.76E-07 l.76E-07 1.37E-08 ---4.93E-04 4.93E-04 4.93E-04 3.84E-0S 3.61E-0S 3.61E-05 3.61E-05 2.SlE-06 4.31E-06 4.31E-06 4.31E-06 3.36E-07 --- ---2.02£-07 2.02E-07 2.02E-07 l.5&-08 l.04E-06 l.04E-06 l.04E-06 7. 67E-08 6.01E+02 6.02E+02 6. 02E-+02 4.84E+Ol ------. . 3.41E-03 l.SSE-+01 l.71E+Ol l.71E+Ol 4.07E+OO 4.07E+OO 4. 07E+OO 7.32E-14

2.00E-02 2.00E-02 2.00E-02 3. 60€-16 l.25E-0l l.69E+Ol 1.69£+01 2.24E-l5 S.66E+Ol 5.66E+Ol 5.66[+01 3.0SE:-01 ------1.011:-02 l. OOE-02 l.OOE-02 l.~-16

l.51E-02 l.SlE-02 1. SlE-02

------- --- -----

2.0lE-01 2. 0lE-01 2.0lE-01 5.67E-06 l.l4E+OO l.14E+OO l. l4E+OO 5.14E-02 5. l4E-02 5. l4E-02 5. 69E-02 ----- ----

·z.3SE-0l 2.35E-0l 2.35E-0l 2. 60€-01 l.87E-0l 1. 87E-0l 1.87(-01 2.07E-0l 7.29E+02 7.49£+02 7 .49E+02 4.93E+Ol

-

Page 15: -I-Cl l

08/24/90 09:14 AH

S7REAH Nl.MIER .

. lJ1 PW£

T~. Deg C Press. ~111 ~ty ml Volune Liters

Al Grams B Grams Ba Grams

Ca 6rllllS Ce Grams Cr GrllllS

Fe Grams IC GrllllS La GrllllS -----~ Grams ·

Grams Mo GrllllS ---Na Grams Nd Grams Ni Grams

Rh GrllllS Ru GrllllS Si Grams

Sr Grns Te Grns Ti Grns -------u Grns Zn Grns Zr Grams ~~.--~,. Grams

Grans ... . ~ ... ;J Grams --Rul06 GrllllS Sbl25 Grams Csl34 Grams

C.sl37 Grams Cel44 Grams Ca60 Grns

Eul54 Grns EulSS Grams Pu238 Grams

Pu239 Grams Pu240 Grams Pu241 Grams

Pu242 Grans MIZ41 Grans H20 Grns

H+ GrlllL'S OH- Grams F- Grims

Cl- Grims N02- Grams N03- GrllllS

504-2 Grams NK3 Grams C03-2 Grns

Him Grns NH4+ Grims CO2 Grams ---------NOx Grams

Grams Grams

- ~ , ·-------------H2C204 Grans HEDPA Grans O'PO . Grams• ----TBP Grams NPH GrllllS TOTAL Grams

r

51 52 53

CLEANED AIR CAUSTIC alGANIC BLEED ADDITlat ---

25.0 25.0 25.0 14.7 14.7 14.7

0.7500 0.0012 1.5300 1.39£-01 3.90E-02 8. 14£-02 ---2.49E-20 2. S7E-20 6.43E-Zl ---3.22E-20 2.59E-ll 6.92E-25

3.84£-15 l.06E-18 l. UE-02 ---6.43E-21 6.43E-29 7.66£-16 --4.41E-22 3.SBE+Ol 2.70E-03 6.9&-33 --4.8&-13 6.56E-04 2.77E-19

6.43E-29 6.22E-29 6.22E-29

2.0SE-19 6.49E-29 4.BSE-11 --- ---- ------7.66£-20 7.0lE-20 ------8.96E-08 5.38E-25 9.19E-26

2.07E-25 6.0SE-07 9.00E-27

2. 613(-11 2. 613(-11 3.13E-12 ---8.76E-09 6.42E-10 7.67E-ll ---3.60E-12 1.07E-10 l.4SE-Ol 6.23E+Ol

2.6SE+Ol 4". 64£-23

2.ZSE-25 l.42E-24 6.43E-22 ---1.14£-25

---7.42E-03

---- ---3.52E-02 l.07E-OZ ------

3.60E-15 6.42(-03 l .13E+Ol ----- ----5. lSE+Ol 4. lOE+Ol 1.04E+OZ 4. 60E-OZ 1.ZSE+OZ

APPM~l.7 WHC-SD-W153-CDR-001 Rev. 0

S>£ET 6 OF 6

54 55 56 57 58 59 60 ,,

FILIER OFFGAS BACXFLUSH AIR OiEHICAL

AIR VENT ADDITION ---- ---25 .0 25.0 25.0 25.0 25 .0 25.0 25.0 14 .7 104.7 14.7 14.7 14 .7 14.7 14.7 0.0007 0.0084 0.0012 1.0000 1.0000 1.0000 1.0000

2.7SE-02 9.99E-02 7.3~-01 1.99£-02 -- ----------

--- -- --------- -- ------ -----

------------ -------- --- -----

-------- --------------- -------

---- ------ -------- ------- ---- ----

--- -------------

--- ------

3.02E-04 1.34£-02 .l.SSE+OO - ---- . . l.SSE+OO

l.613E+Ol

--- ----l.89E-02

--- --- -. ----- - --- ---

6.44(-01 6.44E-01 l.95E-Ol l.95E-01 ------- ---·----- ---- ------

----- --- ---1.92E-OZ 8.39E-Ol 8.52E-Ol l.99E+Ol .. .,_,..,

,_,.r, OVAil -

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IV. DESCRIPTION OF PROJECT SCOPE

The TRUEX Pilot Plant .will provide facilities that are capable of generating data to aid the design and operation of the full-scale process. These facilities include, but are not limited to, vessels for receiving waste transfers from the tank farm, vessels for dissolution of solids, equipment for clarification of dissolver solutions, equipment for extraction of transuranics (TRUs) from the clarified solutions, vessels to accumulate and store product streams, equipment for controlling offgasses from the above, and instrumen­tation to control operations. (The system for transporting waste to the 324 Building is not within the scope of this project, but it must be compatible with the pilot plant liquid waste stream.) The waste form qualification program anticipates a requirement for 200 kg of oxides from each of the three types of waste.

The pilot plant will process three types of feed material: NCRW, PFP, and ~C waste. Stream compositions for processing NCRW are shown on figures 1.1 through 1.7.

The basis for this conceptual design report (CDR) is that NCRW and CC supernate will be delivered to 221-B cell 11 via line 21 from the 244-AR Vault and Tank Farm, respectively, up to 3200 gal of waste stream. It will be stored initially in cell 11, TK-11-2. Plutonium Finishing Plant wastes, while not further addressed in this CDR, are expected to be cask transferred from 200-W to 221-B initially stored in cell· 35, TK-35-2.

Neutralized cladding remova~ waste containing solids will be pumped from TK-11-2 to TK-36-3. It wi]l be settled and decanted in TK-36-3 to accumulate 750 gal of sludge. Decanting is not desirable but may be required if the feed received is too dilute. This sludge will contain most of the radionuclides present in the waste. The balance of the 3,200 gal working volume in this tank will be made up of water that is added in order to help dissolve sodium fluoride. Supernate

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decanted from TK-36-3 will be stored in TK-25-2, which also may contain a maximum working volume of 3,200 gal.

Sludge from TK-36-3 will be jet transferred to a dissolver in cell 38 via lines routed through the hot pipe trench and cell 39 . Sketch ES-0153-MSZ shows interconnections of the affected cells and hot pipe trench. Sketches ES-0153-M32 through ES-0153-M53 shows interconnections with the 221 -8 cells and hot pipe trench.

The products of the process will consist of the solids remaining undissolved after the dissolution step combined with the TRU element concentrate resulting from solvent extraction, and the low-level waste raffi nate from so 1 vent extraction. The l ow-1 eve 1 raffi nate will be suitable for return to the tank farm through existing underground pipelines.

Feed preparation operations will be capable of generating the required yolume of glass plant feed (200 kg of oxides) within a 6-mo operating window for each type of waste. Feed preparation will also be capable· of supporting a continuous solvent extraction run for extended periods.

The solvent extraction feed rate shall be based on the use of 4-cm annular centrifugal contactors with an octyl(phenyl)-N, N-diisobutyl­carbamoyl-methylphosphine oxide (CMPO) and tributyl phosphate {TBP) solvent dissolved in a normal paraffin hydrocarbon {NPH) diluent. Solvent extraction throughput does not necessarily have to match feed preparation throughput .

Feed preparation operations wi l l be capable of sustaining the solvent extraction process either by concurrent operations or advance feed preparation. Advance preparation is preferred to preclude interrup­tion of so 1 vent extraction runs . The p 1 ant wi 11 . be operated on a 24-hr/day, 7-day/wk basis.

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All TRUEX Pilot Plant processes will be operated at ambient tempera­tures. Temperatures will be maintained between 25• C and 40• C.

The equipment purchased and design modifications will be designed for a useful life of 3 yr. New features installed in 221-8 Building and the 225-8 Building will be designed in accordance with Department of Energy {DOE) Order 6430.lA, Division 1300.

The project scope of this CDR is divided into two sections:

221-8 Building {-2-21 B Bu+ld1ng) modifications 225-8 Building<1nooT£ica~ions

A. SPECIAL EQUIPMENT/PROCESS SYSTEMS (700)

1. 221-8 Building ~2:t-B=But-tcting) Modifications

W153CDR.TD.1825

. Equipment Description Cell 38 will contain the dissolution, sludge washing and the solids/liquid separation operations.

The Piping and Instrument Flowsheet for the dissolution process is shown on sketches ES-0153-M34 through ES-0153-M40. (See appendix M for all sketches.)

A structural steel module will be provided to house some of the in-cell equipment. Materials will be selected to be compatible with the acid environment expected to exist in the ce 11 during processing ope rat i ans ( reference figure 2) .

Dissolvers TK-38-L TK-38-2, and TK-38-3 Three dissolvers are available for processing the incoming waste-slurries. Neutralized cladding removal waste will require the use of only one dissolver because of the short dissolver cycle time. Slurry water containing hydrazinium nitrate and concentrated

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acid will be added to the dissolver. Then the appropriate amount of NCRW slurry will be transferred into the dissolver to end up with a 1 M nitric acid solution.

Plutonium Finishing Plant and some CC solids require more concentrated acid during dissolution. Plutonium Finishing Plant and CC are slurried into a dissolver and allowed to settle. The supernates are decanted to a second dissolver tank and held there while the settled solids are dissolved in about 6 M nitric acid. After dissolution, the supernates (and caustic, as required) are added back to adjust the acid concentra­tion to 1 M nitric acid.

The acidificatiun· of waste and dissolution of solids are exothermic and generate off-gasses containing CO2,

N20, ~nd N2• Cooling is required to maintain solution stability and minimize vessel corrosion. Temperatures between 2s• C and 40• C will be maintained.

Filter aid, if required, will be added to the dissolver. Final composition adjustments are also made in the dissolver. Adjustments are made prior to filtration to avoid the introduction or formation of solids in the filtrate.

Filter, F-38-1 The acidified liquors from the filtrate receiver will be clarified by filtration to ensure that an insigni­ficant amount of i nso 1 ub 1 e TRU is fed to so 1 vent extraction. Removal of solids reduces the risk of forming interfacial crud during solvent extraction.

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NORTH

EQUIPTMENT LIST

TK-38-I TK -l8· 2 TK-l8·J TK-l8· 4 TK-J8·5 TK· l8· 6 TK-l8·7 TK-l8·8

DISSOLVER DiSSOLVER DISSOLVER · nLTRATE SOLIDS RAffINATE CONDENSATE NOX COLUMN

:::c :I: n I

Vl C, I

:::c ...... Ul w ~ C, :;o I

0 0 ...... :;o Cl) <

0

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Wl53COR.TD.1825

WHC -SD-Wl53-CDR-001 Rev . 0

Filtrate Receiver, TK-38-4 The filtrate receiver tank will collect clarified solution from filter F-38-1. This tank will feed the three TRUEX feed tanks TK-8-1, TK-B-2, and TK-8-5 located in Cell B of the 225-8 Building facility.

Solids Tank, TK-38-5 Solids remaining on the filter will be flushed into the solids tank. The solids tank will have the capability of recycling the solids to a dissolver or combining the solids with the TRU product from the solvent extraction process for shipment to the 324 Building for waste form qualification studies.

Baffinate Tank, TK-38-6 Raffinate from the solvent extraction process will be collected in the raffinate tank. , The raffinate will be neutralized and routed to TK-36-2 or transferred to the dissolver TK-38~1 for rework.

fil2x Column, TK-38-8 Oxides of nitrogen (NOx) from dissolution and acidification will be scrubbed from the offgas by countercurrent contacting with water in a packed column. If enhanced scrubbing is required, then a solution of caustic will be made available in place of water. The disadvantage of caustic scrubbing is the potential for plugging from relatively insoluble sodium carbonate that is formed from the CO2 in the offgas. In an ~cidic column, the CO2 would not be absorbed. For the pilot plant, a recirculating water system operated on a bat.ch basis wi 11 be employed. The acidic water would be replaced with fresh water when NOx in the effluent gas rises to an unacceptable level.

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Scrubber Receiver Tank, TK-38-7 This tank will collect spent scrub liquor from the NOx column. This acidic solution will be transferred to tank TK-39-1. Acidic waste effluent will be used as needed for dissolver makeup water and the balance discharged to the tank farm .

Jumpers Piping jumpers will be designed and fabricated in accordance with SD-RE-0GS-002, "Jumper Design Standard". The plutonium extraction (PUREX)-type nozzles and .connectors will be used for all new pipe connections. Corrosion and erosion allowances will be based on applicable flowsheet conditions and the anticipated duration of the tests. Hanford-type connectors will be utilized whenever existing Hanford male nozzles are in place.

Approximately 155 jumpers will be placed in support of Cell 38. (Refer to sketch ES-0153-M53).

Jumpers will contain major pieces of equipment such as filters, pumps, valves, etc, which will eliminate additional floor space requirements.

Hot Pipe Trench (Refer to sketch ES-0l53-M52, sh 1) Hot pipe trench (HPT) routings will utilize existing pipes in the HPT for~

Neutralized cladding removal waste routings to/from Cells 11 and 25 .

Compl exant concentrate supernates to/from Cells . 11 and 25.

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WHC -SO-Wl53 -COR-001 Rev . 0

Plutonium Finishing Plant waste to/from Cell 35 via Cell 37.

Transuranic extraction feed to/from 225-B Building via Cell 39 .

Operating Gallery Modifications Modifications will be made to existing cold side systems to make up and route the necessary cold chemicals and utility support streams. The following are identified as required services to the cells:

Demineralized water (dilution).

Raw water (cooling).

Steam (jets).

Process air (sparge jets).

Instrument air (air-operated valve control air, instrument dip tubes).

Chemical addition tanks for services to the cell will be provided. The existing aqueous makeup (AMU) tanks will not be utilized. New tanks will be provided to accommodate the following chemical services:

Sodium hydroxide (NaOH).

Nitric acid (HN03).

Fresh organic.

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Oxalic/nitric acid solution (scrub).

Reference AMU support data in Section VII . E and appendices L.

Sampling Sampling requirements for the TRUEX system capabilities in the 221-B Building will be as follows:

Verification sample TK-25-2 Existing Solids sample TK-35- 2 Existing Raffinate sample TK-36-2 Existing Dissolver sample TK-38-1- New Filtrate sample TK-38-4 New

Data Acquisition and Control System (Refer to Figures 3 and 4 . )

.A new centralized Data Acquisition and Control System (DACS) will be installed by this project to control and monitor systems operation. The DACS will utilize state-of­the-art process control and data acquisition at Cell 38 . The DACS will consist of two interconnected systems: the 221-B and 225-B Building's systems. See Electrical section below which discusses the power source. .

The DACS will satisfy the following objectives :

Data acquisition Data analysis Inventory controJ Process control

The DACS will readily interface and share data with the Facility Process Monitoring and Control System (FPMCS).

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S0-W153-CDR-001 REV 0

FIGURE 3 DATA AQUISTION AND CONTROL SYSTEM

CDACSJ ARCHITECTURE

TO/FROM EXISTING 8 PLANT FPMCS

PLANT COMMUNICATION LOOP (TYP) ,--------

PCU (SEE

NOTE 1)

NOTES:

OIS

PRINTER

CABLE (TYP)

8-PLANT .. I• WESF 221-8 225-8

PCU DRIVER

ors

PRINTER

1. REFER TO PROCESS CONTROL UNIT ARCHITECTURE (FIGURE 4) FOR DETAILS.

2. EXACT LOCATIONS TO BE DETERMINED DURING DEFINITIVE DESIGN.

LEGEND LIM - LOOP INTERFACE MODULE ors - OPERATOR INTERFACE STATION PCU - PROCESS CONTROL UNIT

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FIGURE 4: 221-8 PROCESS CONTROL UNIT (PCU) ARCHITECTURE

(

I.

I I (REDUNDANT) LIM LIM

I I (REDUNDANT) -BIM BIM

I I MODULE BUS I

(REpUNDANT)

AMM AMM (REDUNDANT) MFC - MFC

I EXPANDER BUS EXPANDER BUS

ASM TYP ASI TYP TYP OF OF DSO OF OSI ASO -03 3 4 3

· TYP TYP TYP TU TU TU OF TU OF TU OF TU TU

1l

3 4 3

n Jl •I j . l 1 }

' 1 1J

\ y y

8 PLANT PROCESS I/0 SIGNAL FPMCS SEE NOTE 1

NOTES: 1 . PLANT LOOP COMMUNICATION CABLE. 2. EQUIPMENT LIST IS PRELIMINARY. ACTUAL EQUIPMENT REQUIREMENTS

WILL BE IDENTIFIED DURING DEFINITIVE DESIGN.

AMM ASI ASM-03 -SIM ASO OSI oso LIM MFC TU

LEGEND ANALOG MASTER MODULE ANALOG SLAVE INPUT (4-20mA) ANALOG SLAVE MODULE (RTD INPUT) BUS INTERFACE MODULE ANALOG SLAVE OUTPUT (4-20mA) DIGITAL SLAVE INPUT DIGITAL SLAVE OUTPUT LOOP INTERFACE MODULE MULTIFUNCTION CONTROLLER TERMINATION UNIT

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Wl53CDR. TD.1825

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A distributed control system will perform centralized control and operator interface functions normally associated with convent i ona 1 main contra 1 room pane 1 s. These functions will include monitoring, sequential and process control, and alarms.

Two local control units (LCU), one in the 221-B Building, the other in the 225-8 Building, will perform the distri­buted functions, permitting on-line maintenance of various cabinet components. Each cabinet will be capable of stand­alone operation which is essential for operation and moni­toring requirements, especially for critical applications. Those cabinets will house all signal conditioning. Each cabinet will transmit and receive data along the communi­cation link to and from the local DACS operator stations, but will continue to operate stand-alone if communications with the operator stations are lost.

Through dedicated cathode-ray tube (CRT) operator interface stations (0IS)--one dedicated for the 221-B Building control, the other dedicated for the 225-B Building--pilot plant operators will control or monitor equipment operations. A printer adjacent to each console will be provided for permanent record of process events, conditions, alarms, and maintenance required. System configuration security will be ensured using password access.

Instrumentation/Controls (Refer to Table I-New in appendix J.)

For tanks TK-35-1, TK-35-2, TK-36-1, TK-36-2, TK-36-3, TK-38-1 through TK-38-7, and TK-39-1 weight factor (level), specific gravity (density) and pressure and reference cell pressure will be monitored using elec­tronic differential pressure transmitters. Tank

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temperatures will be monitored using 100 ohm platinum resistance temperature detectors, rep 1 acing any existing nickel detectors as needed .

For Cells 38 and 39 sump level will be monitored using electronic differential pressure transmitters. See electrical section below for leak detection.

Open-close control, air-operated valves will be actuated with electric (solenoid operated) pilots.

Jet gang va 1 ves wil 1 be required to perform jet transfer of fluids from one tank to another. Cells 38 and 39 jet gang valves are readily adaptable to remote or manua 1 contra 1 from the DACS. A 11 other ce 11 s require manual o_peration at the cell instrument panel.

During definitive design, selection and location of valve/operator type, with interconnecting controls and monitoring, and utilities requiring either electric and/or air must be selected. Insufficient number of manually operable, or automated remote or manually operated, jet gang valves are available. (See Section VII, Identification and Analysis of Uncertainties).

No new radiation monitoring instrument requirements have been identified.

During definiti~e design, need for and location of any additional instrument pane 1 s or transmitter racks will be determined.

Electrical A Tl el ectri cal work and material wi 11 be in accordance with National Fire Protection Association (NFPA) 70-1990,

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American National Standards . Institute {ANSI), and DOE 6430.lA. In-cell electrical wiring insulation and electrical components will be selected for radiation resistance.

221-8 Building The normal electrical service for the pumps and agitators in Cell 38 will be provided from existing motor control center 19 1 ocated · in the el ectri cal ga 11 ery of the 221-B Building. Power for the LCU, OIS, and printer, which wi 11 be 1 ocated across · from Ce 11 38 in the Operating Galle~y of the ·221-B Building, will be provided from panelboard K located in the operating gallery. Instrumen­tation devices, {i.e., specific gravity, weight factor, differential pressure, and resistance temperature devices) and air-operated valves will be loop-powered from the LCU. Existing leak detection circuits will be modified to

. provide alarm signals at the DACS.

2. 225-B Building (Waste Encapsulation Storage Facility) Modifications

Wl53CDR.TD.1825

Equipment Installation Cells Band C in the 225-B Building will contain the TRUEX feed and solvent extraction systems as shown on sketches ES-0153-M42 through ES-0153-MSl. See sketch ES-0153-MSS, sh 1 and sh 2 for equipment layout.

Transuranic Extraction Feed Tanks, TK-B-1, TK-B-2, and TK-B-5 Existing tanks TK-B-1, TK-B-2, and TK-B-5 will be _used to feed the solvent extraction system. Because tanks TK-B-2 and TK-B-5 are lower than the level of the contactors, the contents of these two tanks will be transferred (via air powered jet) to tank TK-B-1. Tank TK-B-1 feeds the solvent extraction process by gravity flow. Cooling of the process

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will be performed to maintain the solution at the optimum temperature for solvent extraction.

Solvent Storage Tank, TK-C -3 This tank supplies the organic solvent to the solvent extraction and solvent cleanup contactors. The organic solvent consists of octyl (phenyl}-N, CMPO (0.2M) and TBP (1.4M) dissolved in a normal parrafin hydrocarbon (NPH) diluent.

Solvent Extraction Contactors Transuranic elem~nts will be removed from the clarified feed by sol vent extraction. Centrifugal cont actors wil 1 be used for this purpose. The contactors are the 4 cm type similar to Laboratory H-2-96499).

the design developed by Argonne National (AN~) (reference drawings H-2-96495 and Enough contactors will be provided to handle

.flowsheet variations from waste-to-waste. One centrifugal contactor is assumed to be equivalent to a theoretical stage. Pending· further refinements in the flowsheets, a bank of 16 contactors in Cell B, and a bank of four contactors in Cell C will be provided.

After verifying the. nitric acid concentration of the feed and making necessary adjustments, the feed is clarified and fed to the solvent extraction process. The feed tank is sized to permit extended runs (>8 hr). All other flows are proportioned to the feed fl owrate. A dilute o?<a l i c/ni tri c acid solution is used to scrub the organic extract. The scrub solution leaves with the raffinate. Another dilute acid stream containing a complexant is used to strip the TRU elements from the extract into a small volume TRU stream.

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Wl53CDR . TD . 1825

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Strip Tank, TK-B-3 The main purpose of this tank is to collect the TRU product from the solvent extraction system. The tank will also be used to collect liquids from the solvent extraction system when the system is shut down and needs to be drained. Any organic that may be entrained in the aqueous phase will be periodically decanted and transferred to the solvent storage tank. · Aqueous solutions in this tank will be transferred to the solids receiver TK-38-5 (in Cell 38 of 221 -8 Building) .

Solvent Clean-yo ·contactors The stripped solvent is contacted in the solvent cleanup contactors with a sodium carbonate so 1 ut ion to remove organic degradation products followed by ni~ric acid solution to reequilibrate the solvent. The TRUEX solvent is relatively resistant to degradation, but treatment of a

.side stream will be required to maintain solvent quality . The contactors will be the same as those mentioned under solvent extraction contactors.

Sodium Carbonate CNa2C....~l Tank, TK-C-2 This tank supplies a dilute solution of sodium carbonate to the solvent cleanup contactors. This solution is recycled until degradation products reach unacceptable concentra­tions. The contents are then emptied to the raffinate tank, TK-38-6 via the TRU monitor, and replenished with fresh sodium carbonate solution. ·

Nitric Acid CHN03 ) Tan.k, TK-C-1 This tank supplies dilute nitric acid to the solvent c 1 eanup cont actors. This solution is recyc 1 ed until the acidity drops to unacceptable levels. The contents are then emptied to the raffinate tank, TK-38-6 via the TRU monitor, and replenished with fresh acid.

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'

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Transuranic Monitor The TRU monitor will be installed between Cells Band C in the area vacated by the furnace, and tested prior to pilot plant operations as part of a different technology demon­strati on, and then 1 eft in p 1 ace for use by the pi 1 at p 1 ant. Th~sfes.ign--i-s--b~i-ng-mod-tf-i ed- by- KEH to inc 1 ude the necessary nozzles for the pilot plant application.

The low-level waste from the TRUEX process will accumulate in the TRU monitor. When the chamber of the monitor is half full (about 35 gal), it will provide data on the concentration and· isotopic distribution of the TRU content.

Jumpers Tubing jumpers will be designed and fabricated in accordance with SD-RE-DGS-002 "Jumper Design Standard".

_Hot Pipe Trench Routings (Refer to sketch ES-0153-M52, sh 2)

Hot pipe trench routings will utilize existing lines due to the inaccessibility of the 225-B Building's HPT.

Service Gallery Modifications Modifications will be made to existing cold side systems to make up and route the necessary cold chemicals and utility support streams.

Sampling Sample drawing ports are provided on tanks and the connectors as indicated on sketches ES-0153-M42 through ES-0153-MSI. Samples will be drawn in vials using master/slave manipulators, capped and placed in shielded containers for tranlfer from the cells to the analytical chemistry laboratories.

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Aqueous Makeup Reference AMU support data in Secti on VI I. E and appendices L.

Data Acquisition and Control System The 225-8 Bui 1 ding ' s system wi 11 interconnect with the 221-8 Building's system. (See Section IV . , Data Acquisition and Control System.)

Instrumentation/Controls (Refer to Table II-New in appendix J . ) Not only tanks TK-C-1, TK-C-2, TK-C-3, and TK-8-3 weight factor (level), specific gravity (density) and pressure, but also reference cell pressure will be monitored using electronic differential pressure transmitters. . rank temperatures will be monitored using resistance temperature detectors.

See Electrical section below for leak detection .

Jet gang valves will be required to perform jet transfer of fluids from one tank to another.

During definitive design, selection and location of valve/operator type, with interconnecting controls and monitoring, and utilities requiring either electric and/or air must be selected . Insufficient number of manually operable or automated remote manually operated jet gang valves are available. (See Section VII, "Identification and Analysis of Uncertainties".)

New radiation monitoring instrumentation will be provided on cooling water · lines t~ and from cell tanks . in 225-8 Building only.

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Electrical

225-8 Building The norma 1 e 1 ectri ca 1 service for the pumps. 1 ocated in Cells Band C will be provided from either the existing motor contra 1 center or from the existing pane 1 board, depending on the motor size. Power for the LCU, OIS, and printer which will be located in storage pool control room will be provided from one of the existing panelboard. Instrumentation devices (i.e., specific gravity, weight factor, differential pressure, resistance temperature devices), and air~operated valves will be loop-powered from the LCU.

Existing leak detection circuits will be modified to provide alarm signals to the DACS.

A data highway will be necessary to link the LCU in the 225~8 Building with the LCU in the 221-B Building, if an existing route is not available, a penetration will have to be made for conduit routing (possibly in stairwell 109).

Power conditioning will be necessary and is assumed to be provided with the LCUs.

3~ Egyipment/Comoonent/System Safety Classification

Wl53CDR.TD.1825

All interface connections made with existing plant systems will be evaluated at the beginning of definitive design for verification of safety class based on the safety class of the existing system. _

After piping routes and instrument location have been established for the new piping/instrumentation, the consequences of failure will be investigated to document the fact that the new piping or instrumentation will not

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prevent a DOE Order 6430.IA safety class component or system from performing its required function.

If it is determined that corranercial grade items or qua 1 i fi ed suppliers { qua 1 i ty category I c 1 ass i fi cation) are required, KEH Engineering will identify the critical char­acteristic ( s) or Qua 1 i ty Assurance Program requirements for the items, components or structures and prepare a procure­ment specification which will meet the applicable design requirements.

B. DEMOLITION {810}

1. 221-B Building

Wl53CDR .TD . 1825

Disposal of existing remote equipment and cell cleanout activities will be conducted by the 221-B Building operations under procedures to be developed to comply with

.current regulations and requirements for solid-waste burials. Three or more burial boxes may be required to control the dose rate and several of the tanks and/or dunnage will have to be cut up to be placed in the burial boxes.

The items which will be removed from Cell 38 include:

Approximately 80 jumpers.

Twenty-three blank connector (save for future use.) .

Fourteen mechani-c_al dust covers (save for future use) .

Three electrical dust covers (save for future use) .

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Remote flanged type jumper .

EquipmenL

Cesium feed tank (TK-38-1) Cesium waste tank (TK-38-2) Cesium recycle tank (TK-38-3) Eluant receiver (TK-38-4) Ion exchange tower (T-38-5) Cesium concentrator (E-38-6) Condenser (E-38-7) Cesium .product receiver (TK-38-8)

Removable tank dunnage.

Mi see 11 aneous debris, such as 1 oose concrete, free nuts, jumper parts.

Cell 38 Cleanout and Preparation

In-Cell Equipment Removal and disposal of the above listed items will be required. This will be done while 221-B Building is operating so jumper and equipment removal will be dependent upon crane availability.

Following vessel removal, the cell floor will be cleaned as much as practical and all miscellaneous debris disposed of . At the end of tha cleanout, Cell 38 will be empty of all loose items. T~e call will then be ready for flushing, cleaning, and evaluation of the walls and floor conditions for use as Safety Class 2, secondary containment of the process vessels and .piping. The results of this evaluation by the operating contractor may require structural repair of acid-destroyed concrete and sealing of the cell walls and fl oar.

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out-of-Cell Equipment Cold side equipment removal is needed to prepare for installation of new piping and control equipment . This will include the following:

Removal and disposal of Cell 38 instrument and control equipment on the instrument panels and transmitter racks in the Operating Gallery.

Removal and disposal of Pipe and Operating (P&O) Gallery service piping.

2. 225-8 Building TWaste Encapsulation Storage Facility) Disposal of existing remote equipment and cell cleanout activities will be conducted by the 225-8 Building operations personnel under existing procedures and waste disposal techniques. The project cost estimate includes the cost of existing equipment removal, including cost of burial and labor.

Wl53CDR.TD.1825

Approximately 15 tubing jumpers.

Equipment

Waste storage tank, TK-B-4 (Cells Band C) Shield storage tank, TK-C-SA and TK-C-58 (Cell C) Furnace E-8-8 (Cells a and C) Condenser E-8-10 (Cell B) Filter assembly (Cell B) Cell C compactor

Miscellaneous debris, such as di scarded manipulator parts.

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· Cells Band C Cleanout and Preparation Remova 1 and di sposa 1 of the above 1 i sted i terns wi 11 be required. This will be done while 225-8 Building is operating so jumper and equipment removal will depend upon crane, master/slave manipulator, and waste cask availability.

Following vessel removal, the cell floor will be cleaned as much as practical and all miscellaneous debris disposed of . At the end of the cleanout, Cells Band C will be empty of all loose items. The cell will then be ready · for flushing, cleaning, and an ·evaluation of the cell walls and floor for use as a secondary containment for the cell process vessels and piping.

Out-of-Cell Equipment Partially remove and dispose instrument and control equipment for Cells Band C in the Operating Gallery and east transmitter room.

V. METHODS OF PERFORMANCE

A. ONSITE ARCHITECT-ENGINEER WORK (WBS 1.0) The ons ite engineer/constructor contractor wi 11 perform the definitive design, engineering support, and acceptance inspection support on this project .

B. PROCUREMENT STRATEGY (WBS 2.0) The ans ite engi neer/construc.tor contractor wi 11 perform a 11

procurement associated with the project with the exception of 1) connector parts, 2) the DACS with configuration software from the FPMCS vendor, a_nd 3) the centri fuga 1 cont actors. These three items will be procured by the Operating Contractor.

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C. ONSITE CONSTRUCTION CONTRACTOR (WBS 3. 1) ,.- ·· The ans i te construction contractor wi 11 perform the construction

work with the exception of those noted ·in WBS 3.3.

0. OPERATING CONTRACTOR (WBS 3.3 and 3. 4) The operating contractor will perform 1) all demolition associated with in-cell equipment, 2) the fabrication of the centrifugal contactors, 3) the OACS configuration in both 221-8 Building and the 225-8 Building, and 4) the remote installation of in-cell equipment in both 221-8 Building and the 225-8 Building. The operating contractor will provide overall project management during design, procurement, and construction on this project.

VI. REQUIREMENTS AND ASSESSMENTS

A. SAFEGUARDS AND SECURITY This project will have no impact on existing safeguards and security measures. No new measures beyond the current practices will be required.

B. HEALTH AND SAFETY A Preliminary Safety Evaluation will be provided by Westinghouse Hanford Company (WHC). During the construction peri ad, con­struct ion contractors will be required to take all reasonable precautions in the performance of their work to protect the health and safety of their employees, subcontractors, operating contractor, and DOE personnel. At all times, the construction contractor will ensure that the construction area is accessible to emergency vehicles o.r personnel, and that routes for emergency evacuation of personnel are not obstructed.

C. DECONTAMINATION AND DECOMMISSIONING The selection of equipment and materials and the system design 1 ayou_t wi 11 minimize the potent i a 1 for contamination of both

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facilities and personnel during future decontamination and deco11111issioning once the pilot plant operation is complete.

0. PROVISIONS FOR FALLOUT SHELTERS Existing fallout shelters and the 221-B Building will be utilized. No new fallout shelter requirements are needed for this project .

E. QUALITY ASSURANCE ACTIVITIES/SAFETY CLASSIFICATION

1. Quality Assurance Activities

Wl53CDR .TD . 1825

Project activitie·s for all contractors involved in design, procurement, construction, and acceptance will be governed, as applicable, by the requirements of ANSI/American Society of Mechanical Engineers (ASHE) NQA-1 as directed by DOE­Richland Operations (RL) 5700.lA, "Quality Assurance". Minimum project ·quality attributes are documented in the _project functional design criteria and project specific Qua 1 i ty Assurance Program Pl an ( QAPP) . The QAPP wi 11

i-ndicate the project critical characteristics, . corres­ponding safety classification assignments, and programmatic criteria, which are applicable to this project. Additional requirements may be added by appropriate controlling documents during definitive design. The specific quality programmatic requirements, material certifications, qualification/certification of personnel, inspections, examinations/testing, and applicable quality assurance records will be established during definitive design and included in design documents.

Project W-153 will be designed as an installation in an existing facility in accordance with DOE Order 6430 . IA. The facility type has been determined to meet applicable special facility sections for a · nonreactor nuclear facility .

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.-\ .:.

WHC -SD-Wl53 -CDR-001 Rev. 0

Safety classifications are determined through analysis of consequences of failure for the project criteria established in the project functional design criteria and safety analysis documents. Safety Class 3 is the highest level applied to any elements of the proposed facility with the exception of the HEDPA storage enclosure , which will be a Safety Class 2.

Safety Classification of Systems and Equipment

System/Equipment

221-8 8uil ding Transuranic Extraction Tanks Vessel Ventilation System VV 1

Waste Encapsulation and Storage Facility 8/C Cell Tanks Transuranic Monitor

HEDPA Storage Enclosure

Safety Cl ass

3 3

3 3

2

F. MAINT~NANCE AND OPERATION REQUIREMENTS Training of maintenance and operations personnel will be conducted prior to project closeout for a 11 new systems and devices. Cold side utilities will be maintained with methods and equipment currently used at the 221 -8 and 225-8 Buildings . Cell side equipment will be designed with the following maintenance considerations :

Wl53CDR.TD. 1825

Cell 38 equipment will be maintained by employing existing remote mechanical techniques to replace · significant modules.

Band C Cell equipment will be maintained in-situ using the cell master/slave manipulators .

Design of equipment, systems , and components will be standardized to the extent practical to minimize training

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requirements for maintenance personne 1 and to reduce the inventory of spare parts .

G. AUTOMATED DATA PROCESSING EQUIPMENT Automated data processing equipment required for this project is described in Section IV., "Data Acquisition and Control System" .

H. ENVIRONMENTAL COMPLIANCE Design and fabrication of the TRUEX Pilot Plant will be performed in accordance wi~h the following DOE Orders, State and Federal requirements, and national consensus standards. The operating contractor will be responsible for application of all State and Federal permits for discharge streams to the environment.

Wl53CDR .TD.1825

DOE Order 5400.5, "Radiation Protection of the Public and the Environment" .

DOE Order 6430.lA, "General Design Criteria".

DOE Order 5480.4, "Environmental Protection, Safety, and Health Protection Standards" .

DOE Order 5480 . IB, "Environmental Protection, Safety and . Health Protection Program fa~ DOE Operations".

DOE Order 5820.2A, "Radioactive Waste Management".

DOE Order 4700 .A) "Project Management", Title 40 CFR 61 subpart H, "National. Emission Standards for Radionuclied Emissions from Department of Energy Facilities" .

Title 40 CFR 260, "EPA General Regulations for Hazardous Waste Management" (EPA) .

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· ... .....:.,·

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Title 40 CFR 261, "EPA General Regulations for Identifying Hazardous Waste" (EPA).

Title 40 CFR 262, "EPA Regulations for Hazardous Waste Generators" (EPA).

Title 40 CFR 264, "EPA Regulations for Owners and Operators of Penni tted Hazardous Waste Facilities" (EPA).

Title 40 CFR 265, "EPA Interim Standards for Owners and Operators of Permitted Hazardous Waste Facilities" (EPA) .

Washington Administrative Code, WAC 173 -303, "Dangerous Waste Regulations".

Washington Administrative Code, "Implementation of Regulations for Sources".

WAC 173-403, Air ·Contaminant

Washington Administrative Code, WAC 173-216, "State Waste Discharge Permit Program."

ANSI N 42.18, "Specifications and Performance of Onsite Instrumentation for Continuously Monitoring Radioactivity in Effluents".

ANSI N 509, "Nuclear Power Plant Air Cleaning Units and Components (New Construction and Modifications Only)" .

VII . IDENTIFICATION AND ANALYSIS OF. UNCERTAINTIES

A. JET GANG VALVES Existing jet gang valvei are difficult to maintain and many are local manually operated. Some may be nonoperational . Replace­ment . for new 221-8 Building valving will present design and procurement difficulties due to the 1 ack of a standardized

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valving arrangement, valve body and actuator, instrumentation or .--~ automated remote-manual controls approach at this facility .

B. PIPING AND INSTRUMENT DIAGRAM DRAWINGS Piping and Instrument Diagram (P&ID) drawings in this conceptual design report are completed to satisfy the conditions inside of the 221 -B Build·ing cells and the inside of Cells Band C of the 225 -B Building. Further investigation will be requ i red to satisfy the cold side conditions. Instruments, electrical, and piping provided on the cold side could possibly drive certain conditions inside the cells. Completion of the P&IDs will be required to proceed w·ith advanced conceptual.

C. CELL BOUNDARY CONTAINMENT After flushing, cleaning, and evaluating the cell walls and floors by the Operating Contractor, the determination will be made whether- the ce 11 boundaries require st ructura 1 repair and/or sealing.

D. NEUTRALIZED CURRENT ACID WASTE The neutralized current acid waste (NCAW) stream will require interface with project W-153. Joint utilization of some cells in 221-B is a possibility. An interface study will not be conducted until further NCAW information is available. The operating contractor is responsible for the NCAW process routings. This project does not include any costs included with the NCAW process routings.

E. AQUEOUS MAKEUP The AMU level in both the 221-B and 225-8 Buildings have been addressed in appendix L for further review and evaluation in advanced conceptual or definitive design. No cold side piping was conceptualized for pfoject W-153. Parametric cost estimate numb.ers with project C-042 were utilized for cost estimate purposes (reference appendix L) .

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F. SUPPLEMENTAL VENTILATION - WESF AMU AREA The requirements for supplemental ventilation in the AMU areas (e.g., a hood) require further assessment. An allowance for supplemental ventilation equipment is included in the project estimate.

~- SUPPLEMENTAL FIRE PROTECTION SYSTEMS The requirements for modification to existing fire protection systems in WESF in the AMU area and Cells Band C need further assessment. An allowance for supplemental systems · was identified in the cost estimate.

H. EMBEDDED PIPING IN 221B AND 2258 The compatibility of embedded piping with process solutions needs further assessment, as well · as possible fixes where incompatibilities exist.

I . UNSTABLE SOLUTIONS . Recent 1 aboratory work has turned up a potent i a 1 prob 1 em . with solids spontaneously precipitating from solution in dissolved NCRW. The effect of these solids on solvent extraction with centrifugal contactors needs assessments.

VI I I. REFERENCES

1. Functional Design Criteria, "TRUEX Pilot Plant," Project W-153, Westinghouse Hanford Company, Document No. WHC-SD-W153-FDC-001, Rev. o, July 1990.

2. Engineering Study, "TRUEX -~ilot Plant Site Selection," prepared by Westinghouse Hanford Company, Document No. WHC -SD-WM-ER-058, Rev. 0, September 1989.

3. Letter, R. D. Campbell (Kaiser Engineers Hanford Company) to J. D~ Ludowise (Westinghouse Hanford Company), "TRUEX Pilot Plant Design Support," Document No. ENG-W-90-32, March 7, 1990 .

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APPENDIX A

Conceptual Project Schedule

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· ... :·•: .. ,..:.; : ... :• .: ·•

CONSTA WHC

MG MNT SUP?T WHC

~ESIGN(KEHi

~AOC . (KEH)

~AOC . (HHC)

~ Act1,1t1 S.,/Earll DltN

~ 0-lllcol &cthltf

~ Pr•F•N .... l 10l Prl •avl!lon PC EN6A • • 1+r,~

.• ,. ::::r: .

Project Start ; I0CT90 Pro ect Flnhh: 30N0V95

CZ-· ·

TRUEX PILOT PLANT W-153/SUMMARY SCHEDULE/REV 0

:.•/··•······

Sheet t af t

Dat1 Date: !0CT90 Plat Date: -40CT90

.. ~···· . ~ - ... ·. . --:- .

f n I

1/1 0 I

:£ .. Ill Ill I n 0 JI I

0 0 .. JI I'll <

0

. ···-.·· .. ·····r -· r •

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KAISER ENGINEERS

HANFORD

1.0 ENGINEERING

1.1 DEF.DES. ON-SITE A/E

1.2 ENGR/INSP ON-SITE A/E

1.3 OPERATING CONTRACTOR

2.0 PROCUREMENT

2.1 ON-SITE CONST CONTRACTOR

2.2 OPERATING CONTRACTOR

3.0 CONSTRUCTION

3.1 ON-SITE CONST CONTRACTOR

3 .3 OPERATING CONTRACTOR

3.4 OPERATING MANAGEMENT 0/C

TOTALS BA/BO DOLLARS IN THOUSANDS

BA/BO SCHEDULE

PRO~ECT W-153

TRUEX PILOT PLANT

TOTAL FY 1991 FY 1992 FY 1993 COST 1 I 2 I 3 I 4 1 I 2 I 3 I 4 1 I 2 I 3 I 4

5100 2B00/2BOO 2300/2300

1250 410/410

180 90/90 90/90

610 20/20 150/150 440/440

1950 570/570 1380/1380

7820 4240/4240

6250 1210/1180 2090/2070 1520/1570

1940 310/310 390/390 390/ 390

25100 5000/4970 6400/6380 7000/7050

. '

FY 1994 FY 1995

1 I 2 I 3 I 4 1121314

420/420 420/420

2260/2260 1320/1320

1430/1430

390/390 460/460

4500/4500 2200/2200

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WHC -SD-Wl53 -CDR-001 Rev . 0

APPENDIX B

Cost Estimate Summary/Statement of Work

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.... _

KAISER ENGINEERS HANfORO IIHC JOB NO. 11-153

COST CODE -- ---000

501

700 '--

** KAISER ENGINEERS INTERACT I VE ESTIMATING** TRUEX PILOT PLANT

CONCEPTUAL KEHR01 - PROJECT COST SUMMARY

E SCALA TEO CONTINGENCY DESCRIPTION TOTAL COST X TOT AL ====•••==========::a:::=========== z::.;;;;:;;;;;

-==-- ====•====•= ENG I NEER I NG 5,420,000 20 1,080,000

(ADJUSTED TO MEET DOE 5100-4) -20,000 20,000

BUILDINGS 4,870,000 33 1,630,000

SPECIAL EQUIP/PROCESS SYSTEMS 8,790 , 000 37 3,240,000 (ADJUSTED TO MEET DOE 5100.4) 40,000 30 , 000

PROJECT TOTAL 19,100,000 31 6,000,000

PAGE DATE BY

TOT AL

1 Of 19 11/13/90 09 : 03 : 18 fC DAY

DOLLARS s:.a::;:;;;:a;;;;;;;:

6,500 , 000

6 , 500,000

12,030 , 000 70 , 000

25 , 100,000

• - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -- - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - • - - - - - - - - - - - - - - - - - - - • - - - - - - - - •

TYPE Of REMARKS : ESTIMATE c~.~~~buAL REV. 1 NOVEMBER n, 1990 --::i ~ !i ~ i; -----. -. ,i~-' -\,)"-on-~ IF ll -; · --------------

______ . __ ~fc_Ff _____ .. _ f J rr /4_~ ____ -~ -__ _ _ ~?::::;:~.~~- ___ 11/_1"r/~_v ____________________ _

REV. 0 DATED 10-5-90

•---------------------·----------------·---------------···- - -·--- - - ---·---- - - --- - - --·-----·-·---·-----·-·---- - --- -- ----------------•

(ROUNDED/ADJUSTED TO THE NEAREST " 10,000 / 100,000" - PERCENTAGES NOT RECALCULATED TO RE FLECT ROUNDING)

-··

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KAISER ENGINEERS HANFORD IIESTINGHOUSE HANFORD COMPANY JOB NO . 11-153

IISS

1101 1177 1201 1300

DESCRIPTION -- ---- ---- -------~---=---- ---- ---DEFINITIVE DESIGN - KEH DEFINITIVE DESIGN SUPPORT - KEH E/1 DURING CONSTRUCTION - KEH OACS ENGINEERING/DESIGN - IIHC

SUBTOTAL ENGINEERING

'-----2 11 0 2120 2130

IIHC PROCUREMENT - CONNECTORS KEH PROCUREMENT - EQUIPMENT IIHC PROCUREMENT - OACS

SUBTOTAL 21 PROCUREMENT - B PLANT

2 210 222 0

IIHC PROCUREMENl - CENT. CONTAC l ORS KEH P~OCUR ~MENT - RAO MONITORS

SUBTOTAL . 22

SUBTOTAL 2

PROCUREMENT - IIESF

PROCUREMENT

3 11 0 3120

CF CONSTRUCTION - B PLANT Cf CONSTRUCTION - IIESF

SUBTOTAL 31 Cf CONSTRUCTION

3 . 3320

IIHC CELL 38 - B PLANT B & C CELL - IIESF

SUBTOTA L 33 OPERATING CONTRACTOR

3400 IIHC PROJ. MGMT. & ENG. SUPPORT

SUBTOTAL 3 CONSTRUCTION

PROJECT TOTAL

•• KAISER ENGINEERS INTERACT I VE ESTIMATING•• TRUEX PILOT PLANT

CONCEPTUAL KEHR02 - IIORK BREAKOOIIN STRUCTURE SUMMARY

ESTIMATE SUBTOTAL ~-----=-

3666835 405744 900961 144066

5117606

607402 278816 350100

1236318

466800 155237

622037

1858355

3195562 1767841

4963403

2929117 1015851

3944968

1454200

10362571

ONSITE INDIRECTS

---------0 0 0 0

0

0 0 0

0

0 0

0

0

0 0

0

0 0

0

0

0

0

SUB TOTAL ____ ;:;: ___ _

3666835 405744 900961 144066

5117606

607402 278816 350100

1236318

466800 155237

622037

1858355

3195562 1767841

4963403

2929117 1015851

3944968

1454200

10362571

ESCALATION X TOT AL

4. 10 4 . 10

14. 74 4.50

5.98

4 . 10 9 . 88 7. 33

6.32

7-. 33 9 . 88

7.97

6 . 87

14.38 14 . 38

14.38

11 . 20 11 . 20

11 . 20

10 . 76

-----;;;=: 150340

16636 132796

6463

306255

24903 27547 25662

78112

34216 15337

49553

127665

459524 254216

713740

328062 113776

441838

156472

12 . 66 1312050

2 0 F 19 PAGE DA TE BY

11 / 13/90 09 ; 12:51 fC DAY

SUB TOTAL

3817175 422380

1033757 150549

5423861

632305 306363 375 762

1314430

501016 170574

671590

1986020

3655086 2022057

5677143

325 7 179 1129627

4386806

1610672

11674621

CONTINGENCY X TOTAL

20 20 20 20

763436 84476

205286 30110

20 1083308

25 2 7 35

28

30 30

30

29

158076 8 1212

131517

3 7080 5

150305 5 11 72

201477

5 72282

36 1316336 39 79 1472

37 210/808

40 130287 1 50 564813

43 1867684

20 322134

37 4297626

TOT AL DOLLARS

i:;:;;:5;:a:a:s:

4580610 506656

1239044 180659

6507169

790382 387576 507279

1685237

65132 1 2 21 747

873068

2558305

49 71 4 23 2813529

7784952

4560049 16944 4 0

6254489

1932806

15972247

17,338,532 17,338 , 532 1 , 745,970

10 . 07 19:084 , 502 5 , 953 ,2 16

3 1 25,037 , 721

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KAI SER ENGINEERS HANFORD IJHC JOB NO . ER 0202

1 . DOCUMENTS ANO DRAIJINGS

** KA I SE R ENG I NEE RS IN TERACT I VE ES TI MATING ** TRUEX PILOT PLAN T

CONCEPTUAL KEHR03 · ESTIMATE BASIS SHEET

DOCUMENTS: CONCEPTUAL DESIGN REPORT "TRANSURANIC EXTRAC TION PILO T PLANT" ISSUE O DATED AUGUST 1990.

PAGE DA TE BY

3 0 f 19 10/05 /90 1) : 34 :2 5 FC DAY

DRAWINGS: SK-2-58530 DWG . LIST, SK - 2 - ,8532 THRU SK - 2-58555 PIPING & VESSELS, SK-2 - 58562 THRU SK - 2-58564 ELECTRICAL. SK-2-61688 SHTS . 1 THRU 3 TRU MONITOR.

2. I.ABOR RATES ;:;.:;:;;;;.;;;;:

CURRENT HANFORD BASE RATES AS ISSUED BY KEH (ISSUE # 13, REV. 0, DATED 3 · 1 · 90) INCLUDE FRINGE BENEFITS, LABOR INSURANCE, TAXES ANO TRAVEL WHERE APPLICABLE.

3 . GENERAL REQUIREMENTS/TECHNICAL SERVICES

' . ) ONSITE CONSTRUCTION FORCES GENERAL REQUIREMENTS ANO TECHNICAL SERVICES COSTS ARE I NCLUDED AS A COMPOSITE PERCENTAGE BASED ON THE KEH ESTIMATING FACTOR/BILLING SCHEDULE REVISION 10 DATED JANUARY 02 , 1990 . THE TOTAL COMPOSITE PERCENTAGE APPLIED TO ONSITE CONSTRUCTION FORCES LABOR FOR THIS PROJECT IS 72 TO 79X FOR SHOP WORK ANO 108 TO 115X FOR FIELD ~ORK WHICH IS REfLEC1EO IN THE "OH&P / B & I" COLUMN Of THE ESTIMATE DETAIL.

4. ESCALATION

ESCALATION CALCULATED BY THE HANFORO MATERIAL & LABOR ESCALATION STUDY , JANUARY, 1990.

5 . ROUNDING · LINE ITEMS:

U. S . DEPARTMENT Of ENERGY - DOE ORDER 5100.4 PAGE J - 2 SUBPARAGRAPH CM) , REQUIRES ROUNDING OF A COST ESTIMATE TO $10,000 FOR ITEM COST ANO 5100,000 FOR TOTAL COST . REFERENCE: DOE 5100 . 4, FIGURE 1· 11, DATED 10 - 3 1 -84.

6 . REMARKS

A.) AS Of DECEMBER 1, 1989, QUALITY SUPPORT ANO SAFETY FOR CONSTRUCTION FORCES ARE INCLUDED IN THE CRAFT ADDER.

B. ) All CONSTRUCTION/FABRICATION ACTIVITIES (WITH THE EXCEPTION OF THOSE LISTED IN THE was, APPENDIX C) ARE TO BE PERFORMED BY THE ONSITE CONSTRUCTION CONTRACTOR. IF THIS METHOD OF PERFORMANCE CHANGES, AN ADJUSTMENT WILL BE MADE TO THE ESTIMATE ANO SCHEDULE.

C.) COST INFORMATION FOR CLEANOUT Of CELL 38 IN 221 - 8 ANO B & C CELLS IN 225-8 WAS SUPPLIED BY WHC. ~.) PREVIOUS COST DATA FROM PROJECT C- 042 FFTF FUELS PROCESSING IN PUREX WAS UTILIZED IN COSTING THE COLO SIDE MECHANICAL ,

INSTRUMENTATION, & ELECTRICAL WORK IN 221 - B ANO 225 - 8 . E.) COST FOR OACS (RECEIVED FROM WHC) WAS BASED ON PREVIOUS PROCUREMENT EXPERIENCE WITH THE B·PLANT BAILEY SYSTEM . F.) AN ALLOWANCE (RECEIVED FROM WHC) HAS BEEN HADE FOR SEALING ANO LINING THE CELLS, If THE CONDITION OF THE CELLS POSE A

PROBLEM. KEH'S ESTIMATE IS BASED UPON THE ASSUMPTION THAT THE CONDITION OF THE CELLS (38 S&C) IS ADEQUATE . G.) 400K FOR PROCUREMENT OF CENTRIFUGAL CONTACTORS INCLUDES FABRICATION. H.) THE ESTIMATE (REC'D FORM WHC) FOR CELL CLEANOUT IS BASED ON PRESENT PRACTICES AND DISPOSAL TECHNIQUES . ANY CHANGE IN

DISPOSAL METHODS MAY AFFECT THIS COST. I.) OTP IS NOT INCLUDED IN THIS ESTIMATE . J.) AN ALLOWANCE FOR THE SC2 HEOPA STORAGE CABINET ENCLOSURE IN THE WESF AMU AREA HAS BEEN MADE. K. ) MATERIAL FROM THE COLD SIDE DEMOLITION IS ASSUMED TO BE FREE Of CONTAMINATION (RADIOLOGICALLY OR CHEMICAL). DISPOSAL

WILL BE AT THE CENTRAL LANDFILL. L.) WHC SUPPLIED COSTS FOR THE FOLLOWING :

1. CELL 38 CLEAN·UP, FLUSHING , LINER' FAB & INSTALL IN B- PLANT. 2. 8 & C CELLS CLEAN · UP, EQUIP . INSTALL · WESf. 3. PROJECT MANAGEMENT , PSAR , & ENVIRONMENTAL PERMITTING.

M.) REVIS ED CONCEP TUAL ESTIMATE DATED 10-5·90 TO INCORPORATE NEW ENG I NEERING LIQUIDA TION RAT ES ANO NEW PE RCENTA GE S FO R Cf FIELD CONSTRUCTION .

N . ) REVIS ED ESTIMATE CONTA I NS SEP TE MBE R ESCALATION.

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KAISER ENGINEERS HANFORD ** KAISER ENGINEERS INTERACT IVE ESTIMATING ** PAGE 4 Of 19 \.IESTINGHOUSE HANFORD COMPANY TRUEX PILOT PLANT DA TE 11/13/90 09:12:59 JOB HO .' W - 15 3 CONCEPTUAL BY fC DAY

KE HR04 - COST CODE ACCOUNT SUMMARY

ESTIMATE ONS I TE sue ESCALATION sue CONTINGENCY TOTAL I \.IBS DESCRIPTION SUBTOTAL INDIRECTS TOTAL X TOTAL TOTAL X TOTAL DOLL'ARS

;;. ;: ;;: ------------------------·-·-------

a;:;::,;;.,:;. --------- :;:a:.;•ca..::: ---~- ---=•.&-• a:;.-;a:;:;; ;;; saa c ;.s;.;.:;;;;;ssa. ;:a:•••sas.E

I 000 ENGINEERING

1101 DEFINITIVE DESIGN . KEH 3666835 0 3666835 4. 10 15 034 0 3817175 20 lt,3436 4580610 I 1177 DEFINITIVE DESIGN SUPPORT . KEH 405744 0 405744 4. 10 16636 422380 20 84476 506856 1201 E /I DURING CONSTRUCTION - KEH 900961. 0 900961 14 . 74 132796 103375 7 20 205286 1239044

I "'00 DACS ENGINEERING/DESIGN . WHC 144066 0 144066 4.50 6483 150549 20 30 11 0 180659

'--TOTAL 000 ENGINEERING 5117606 0 5117606 5.98 306255 5423861 20 1083308 6507169

I 501 BUILDINGS

I 3310 WHC CELL 38 - e PLANT 2929117 0 2929117 11 . 20 328062 3 257 179 40 13028 71 4560049 3400 WIIC PROJ. MGMT. ' ENG. SUPPORT 1454200 0 1454200 10 . 76 156472 1610672 20 322134 1932806

TOTAL 501 BUILDINGS I 4383317 0 4383317 11.05 484534 4867851 33 1625005 6492855

700 SPECIAL EQUIP/PROCESS SYSTEMS I 2110 WHC PROCUREMENT - CONNECTORS 607402 0 607402 4 . 10 24903 632305 25 158076 790382

I 2120 KEH PMOCUREMENT - EQUIPMENT 278816 0 278816 9.88 27547 306363 27 81212 387576 2130 WHC PROCUREMENT - DACS 350100 0 350100 7 . 33 25662 375 762 35 131517 507279 2210 WHC PROCUREMENT - CENT. CONTACTORS 466800 0 466800 7 . 33 34216 501016 30 150305 651321 2220 KEH PROCUREMENT - RAO HON I TORS 155237 0 155237 , 9.88 15337 170574 30 51172 221747 - 1 1 0 Cf CONSTRUCT I ON - B PLANT 3195562 0 3195562 14.38 459524 3655086 36 1316336 4971423

20 CF CONSTRUCTION - WESF 1767841 0 1767841 14.38 254216 2022057 39 791472 28135 29 3320 e & C CELL . WESf 1015851 0 1015851 11.20 113776 1129627 50 564813 1694440

TOT Al 700 SPECIAL EQUIP/PROCESS SYSTEMS 7837609 0 7837609 1 2 . 19 955181 8792790 37 3244903 12037697

PROJECT TOTAL 0 1,745,970 5,953,216 17,338,532 17,338,5.32 1Q.07 19,084,502 31 25,037 ,7 21

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KAISER ENGINEERS HANfORD •• KAISER ENGINEERS INTERACT IVE ESTIMATING •• PAGE 5 Of 19 IHSTINGHOUSE HANFORD COMPANY TRUEX PILOT PLANT DA TE 11/13/90 09:13 : 05 JOB NO. 11-·153 CONCEPTUAL BY FC DAY

KEHR05 - ESJIMATE SUMMARY BY CSI DIVISION

ESTIMATE ONSITE SUB ESCALATION SUII CONTINGENCY TOT AL IIIIS DESCklPTION SUBTOTAL INDIRECTS TOTAL X TOT AL TOT AL X TOTAL DOLLARS

= - =:;; - = • • E•a;;~aasm•i;;:sa;•&aa:a5aa.aaa;aa;a; ····••a:a: • ; ... ;£ •••• •••a•a••• :a;; E &: ill; ca.aa;aaa a: aa.c.a:a:aa.sa ....... ., a._••••• aca.a.aa.s • a

ENGINEERING

00 TECHNICAL SERVICES 144066 0 144066 4_50 6483 150549 20 3 0 11 0 180659 22 ENVll!ON ENGRG 48251 0 48251 7 . 35 3547 51798 20 10360 62158 24 STRUCTURAL 6100 0 6100 4 . 10 250 6350 20 1270 7620

FIRE PROT /SAf TY 162565 0 162565 6.41 10413 172978 20 34595 2075 73

28 PIPING/VESSEL 1878493 0 1878493 5.28 99157 1977650 20 395530 2373180 HVAC 46055 0 46055 3 . 45 1588 47643 1 7 8065 55706

29 INSTRUMENT 964504 0 984504 5.20 51221 1035725 20 207145 1242670 31 ELECTRICAL 591961 0 591961 5.29 31300 623261 20 124652 747913 32 SPECIF 35668 0 35668 6.66 2389 38257 20 7652 45909 35 DESIGN ADMJN 32208 0 32208 5.32 1 7 t 4 33922 20 6785 40707 36 SAFETY & RISK ANALYSIS 7800 0 7800 4. 10 320 8120 20 1624 9744 39 ENVJROMENTAL COMPLIANCE 3660 0 3660 4 . 10 150 3810 20 762 4572 40 PROJt:Cl MANAGER 223080 0 223080 4.59 10238 233318 20 46663 279981 4 1 IIORD PROCESSING 12142 0 12142 9.33 1133 13275 20 2655 15930 42 QUALITY ENGINEERING 83280 0 83280 8 . 10 6746 90026 20 18005 108031 44 ACCEPTNCE INSPECTION 118561 0 118561 14.07 16683 135244 20 27049 162293 45 PROJECT PLANNING 67300 0 67300 5 . 91 3975 71275 20 14255 85530 46 EST I MATES 160138 0 160138 6.89 11034 1 711 72 20 34235 205407 49 SUB/PROC 30345 0 30345 13.76 4174 34519 20 6904 41423 62 SURVEY 68800 0 68800 5 . 18 3561 72361 20 14472 86833 63 CONSTR ENGRG 103212 0 103212 4 . 10 4232 107444 20 21489 128933 65 RECORDS MGMT/TURNOVER 47117 0 47117 12.97 6112 53229 20 10645 63874 66 AS-BUILTIHG 166400 0 166400 14.86 24727 191127 20 38225 229352 70 IIORK ORDER 86200 0 86200 4.47 3857 90057 20 18011 108068 74 TRAVEL 9500 0 9500 13. 16 1250 10751 20 2150 12901

JAL ENGINEERING 5117606 0 5117606 5 . 98 306254 5423861 20 1083308 6507169

CONSTRUCT ION

01 GENERAL REQUIRMENTS 156715 0 156715 14.38 22536 179251 25 44813 224063 02 SI TE WORK 2243523 0 2243523 11 . 20 251275 2494798 40 997919 3492716 05 METALS 776 778 0 776 778 12. 71 98725 875503 38 329114 1204617 09 FINISHES 1462 0 1462 14. 50 212 16 74 30 502 2176 11 EQUIPMENT 2938081 0 2938081 9.63 282929 3221010 32 1028982 4249997 15 MECHANICAL 4179551 0 4179551 13. 40 559891 4 739442 4 1 1931128 6670570 16 ELECTklCAL 470616 0 470616 14.38 67675 538291 40 215316 753607 19 WHC PROJECT MANAGEMENT 1454200 0 1454200 10 . 76 156472 1610672 20 322134 1932806

TOT AL CONSTRUCTION 12220926 0 12220926 11.78 1439715 13660641 36 4tl69908 18530552

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KAISER ENGINEERS HANfORO UfSTINGHOUSE HANfORO COMPANY JOB NO. U-153

UBS DESCRIPTION

PIIOJECT lOTAL

--

** KAISER ENGINEERS INTERACTIVE ESTIMATING** TRUEX PILOT PLANT

CONCEPTUAL KEHR05 - ESTIMATE SUMMARY BY CSI DIVISION

ESTIMATE SUBTOTAL .;ac.:a;;;;;;;

17,338,532

ONS I TE INDIRECTS

0

sue TOTAL

17,338,532

ESCALATION l TOTAL

. 1,745,969 10.07

sue TOT Al

\ I

6 0 t 19 PAGE DA TE IIY

11/13/90 09:13:08 FC DAY

CONTINGENCY l TOTAL

TOTAL DOLLARS

19,064,502 5,953,216

31 25,037,721

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I I .

KAISER ENGINEERS HANFORD IJ H C

** KAISER ENGINEERS INTERACTIVE ESTIMATING** lRUEX PILOT PLANT

PAGE DATE BY

7 Of 19 09/27/90 15:34:28 fC DAY JOB NO. fR 0202 CONCEPTUAL

----

KEHR06 - CONTINGENCY ANALYSIS BASIS SHEET

REFERENCE: ESTIMATE BASIS SHEET PAGE 3 Of 19 PAGE 4 & 5 Of 19 COST CODE ACCOUNT SUMMARY

THE U.S. DEPARTMENT Of ENERGY - RICHLAND ORDER 5700.3 "COST ESTIMATING , ANALYSIS ANO STANDARDIZATION" DATED l-27-65, PROVIDES GUIDELINES FOR ESTIMATE CONTING[NCIES. THE GUIDELINE FOR A CONC[PTUAL ESTIMATE SHOULD HAVE AN OVERALL RANGE OF 15 TO 40 X •

CONTINGENCY IS EVALUATED AT THE THIRD COST CODE LEVEL AND SUMMARIZED AT THE PRIMARY AND SECONDARY COST CODE LEVEL OF THE DETAILED COST ESTIMATE.

ENGINEERING

PROCUREMENT

WBS 1 . 1.0 A 15X CONTINGENCY WAS APPLIED TO DEF . DESIGN TO ALLOW FOR CHANGES IN EQUIPMENT DESIGN RESULTING FROM INCREASED REQUIREMENTS.

WBS 1 . 2.0 A 15X CONTINGENCY IJAS APPLIED TO ENG . /INSPECTION TO ALLOW FOR CHANGES IN THE EQUIPMENT FABRICATION OR INSTALLATION RESULTING FROM ADDITIONAL REQUIREMENTS BY QUALITY ASSURANCE OR THE CLIENT.

WBS 1.3.0 A 20X CONTINGENCY IJAS APPLIED TO ALLOW FOR UNRECOGNIZED l&C REQUIREHlNTS ANO ADD ED CONTROL CONFIGERATION COSTS.

AVERAGE ENGINEERING CONTINGENCY 20 X

WBS 2.1. AN AVERAGE Of 28X CONTINGENCY WAS APPLIED TO PROCUREMENT TO ALLOW FOR ANY COST GROWTH DUE TO ADDITIONAL QUALITY ASSURANCE REQUIREMENTS Of THE VENDOR IN THE DESIGN AND OPERATION Of THE TRANSFER PUMPS, AGITATORS, CONTACTORS, AND CONNECTOR PARTS . CONTINGENCY WAS APPLIED DUE TO LIMITED DESIGN INFORMATION OUTLINING THE EQUIPMENTS APPLICATION .

WBS 2.2. AN AVERAGE 30X CONTINGENCY WAS APPLIED TO THE CONTACTORS AND RAD MONITORS TO ALLOW FOR COST DUE TO DESIGN CHANGES OR OPERATING REQUIREMENTS Of THE EQUIPMENT.

AVERAGE PROCUREMENT CONTINGENCY 29 X

CONS TRUCTION WBS 3 . 1 . 0 AN AVERAGE Of 37X CONTINGENCY WAS APPLIED TO ALLOW FOR ANY COST GROWTH TO THE FABRICATION ANO OR INSTALLATION Of THE PROCESS EQUIPMENT DUE TO DESIGN CHANGES OR RADIOLOGICAL CONDITIONS.

WBS 3.3.0 AN AVERAGE Of 43 X CONTINGENCY WAS APPLIED TO WHC CLEANOUT DUE TO THE LIMITED AMOUNT Of INFORMATION AVAILABLE AT THIS TIME CONCERNING EXISTING CONDITIONS.

WBS 3.4.0 20X CONTINGENCY WAS APPLIED FOR THE PROJECT MANAGEMENT FUNCTIONS TO ALLOW FOR SCHEDULE UNCERTAINTIES.

AVERAGE CONSTRUCTION CONTINGENCY 37 X

AVERA GE PROJECT CONTINGENCY 31 X

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KAISER ENGINEERS HANFORD UESTINLHOUSE HANfORD COMPANY JOB NO. U-153

UBS

1101 1177 1201 1300 211 0 2120 2 , i

2 2220 3110 3120 3310 3320 3400

DESCRIPTION

DEFINITIVE DESIGN · KEH DEFINITIVE DESIGN SUPPORT · KEH E/1 DURING CONSTRUCTION · KEH DACS ENGINEERING/DESIGN · UHC UHC PROCUREMENT · CONNECTORS KEH PROCUREMENT · EQUIPMENT WHC PROCUREMENT · DACS WHC PROCUREMENT · CENT. CONTACTORS KEH PROCUREMENT · RAD MONITORS CF CONSTRUCTION B PLANT Cf CONSTRUCTION UESf UHC CELL 36 B PLANT B & C CELL · UESf WHC PROJ . MGMT . & ENG. SUPPORJ

PROJECT TOTAL

** . KAISER ENGINEERS INTERACTIVE ESTIMATING** TRUEX PILOT PLANT

CONCEPTUAL KEHR07 · ONSITE INDIRECT COSTS BY UBS

ESTIMATE SUBTOTAL •==-=•=•=

3666835 405744 900961 144066

_607402 278816 350100 466800 155237

3195562 1767841 2929117 1015851 1454200

CONTRACT ADMINISTRATION X TOTAL

------=== 0.00 0.00 0.00 0 . 00 0.00 0 . 00 0.00 0.00 0.00 0.00 0.00 0.00 0 . 00 0.00

0 0 0 0 0 0 0 0 0 0 0 0 0 0

0

BID PACK PREP.

--==--=-0 0 0 0 0 0 0 0 0 0 0 0 0 0

8 Of 19 PAGE DA TE BY

1 1/13/9 0 09 : 13 :13 FC DAY

OT Hl:R 1 0 T AL INDIRECTS INDIRECTS

=-------= .:..:•.::;;.sJ:a

0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0

0

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STATEMENT OF WORK PROJECT W-153

TRUEX PILOT PLANT CLIENT: Westinghouse Hanford Company W.O. NO.: ER-0813

PREPARED BY: D. P. DeVine DATE: 09-11-90

PROJECT SCOPE Project W-153 will provide a system to demonstrate pretreatment of neutralized cladding removal waste (NCRW) which will include the following operations: sludge washing/dissolution, solid/liquid separation, and the transuranic extraction (TRUEX) process. In addition to providing a facility to aid the design and operation of the full scale process, the pilot plant will produce feed material for glass waste form qualification. Modifications to the 221-B building and the 225-B building will be necessary to confirm the TRUEX process. The bulk of the modifications will be located in cell 38 in the 221-B facility, and cells Band C in the 225-B facility.

Design for this project will be performed by the onsite architect engineer.

REFERENCES

• WHC-SD-Wl53-FDC-001, Rev. O, Functional Design Criteria, TRUEX Pilot Plant, Project W-153, dated September 1990.

• WHC-SD-Wl53-CDR-001, Rev. 0, Conceptual Design Report, TRUEX Pilot Plant, Project W-153, dated September 1990.

• WHC-SD-WM-ER-058, Rev. 0, Engineering Study, TRUEX Pilot Plant Site Selection, dated September 1989.

TASKS

A. Westinghouse Hanford Company (WHC)

WHC will perform the following:

1. Data Acquisition and Control System (DACS) configuration software for both B-Plant and WESF (includes ATP of DACS configuration).

2. Procurement of a) connector heads, b) centrifugal contactors, and c) DACS, for both B-Plant and WESF.

3. Demolition/cleanout of cells 38, B, and C.

SOW-W-153

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Statement of Work Project No. W-153 Page 2

4. Fabrication of centrifugal contactors.

5. Remote installation of all in-cell equipment, in both B-Plant and WESF.

6. Development of all safety documentation (PSAR, etc.).

7. Provide Health Physicist Technicians (HPTs) to support construction.

8. Provide overall project management during design, procurement, and construction of the project.

B. Kaiser Engineers Hanford (KEH) will perform the definitive design for the subject project of which the following activities will be performed:

1. Environmental Engineering (22)

• Provide input regarding environmental issues affecting design. • Review and approve all design documentation .

2. Structural (24)

• Provide input to the utility verification study/report.

3. Fire Protection (26)

• Provide input to the utility verification study/report.

4. Safety Review (26.3)

• Review all design documentation for compliance with current Hanford safety requirements.

5. Piping (27)

SOW-W-153

• Prepare 271 drawings consisting of:

• • • • • •

P&IDs depicting the TRUEX process . Hot pipe trench routings. Hydraulic schematics . Cell arrangements . Cell equipment assemblies and details . Module plans, elevations, sections, and details .

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/ · I\ -~-

Statement of Work Project No. W-153 Page 3

• • •

Remote jumpers . Cold side plans, sections, and details . AMU plans, sections, and details .

• Prepare one procurement specification. • Prepare twelve commercial equipment/material specifications. • Provide input to the construction specification. • Provide input to the utility verification study/report.

6. HVAC (28)

• Provide input to the utility verification study/report.

7. Instrumentation (29)

• Prepare 49 drawings consisting of:

• • • • •

• • • •

Tubing and DACS equipment plans, sections, and details . Instrument panel plans, sections, and details . Transmitter rack plans, sections, and details . Interconnection diagrams •

Provide Prepare Prepare Prepare Provide

input to P&IDs . an input/output list. one procurement specification (DACS) . two commercial equipment/material specification. input to the construction specification .

8. Electrical (31)

SOW-W-153

• Prepare 62 drawings consisting of:

• • • • • • 0

0

0

Power and control plans, sections, and details . One line diagrams . Panelboard/MCC schedules . Wiring diagrams . Elementary diagrams . Conduit schedules/wire run lists . Ladder diagrams. Demolition Plan. AMU support plans, sections, and details.

• Provide input to the utility verification study/report. • Provide input to the construction specification.

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Statement of Work Project No. W- 153 Page 4

9. Specifications (32)

• Format and assemble one construction specification. • Format and assemble two procurement specif1cation. • Format and assemble fourteen commercial equipment/material

specifications.

10. Design Administration (35)

• Provide design discipline coordination. • Provide design progress information to Project Management.

11. Safety Analysis or Risk Assessment (36)

• Ensure that Safety Class designations assigned to equipment and systems are based on valid risk assessments.

• Verify that the design documentation is consistent with the Safety Analysis documents provided by WHC.

12 . Environmental Compliance (39)

• Ensure the TRUEX design conforms to the requirements of RCRA .

13 . Project Management (40)

• Provide daily management of project activities. • Ensure the project technical, budget, and schedule objectives

are met. • Provide single point interface with WHC and DOE. • Provide status updates to WHC and DOE.

14 . Clerical/Word Processing (41)

• Process project correspondence. • Provide word processing services for the construction

specification.

15 . Quality Engineering (42)

SOW-W-153

• Review the baseline documentation to verify QA guidelines and design requirements have been adequately addressed.

• Review the design documents to ensure compliance with the appropriate criteria and procedures.

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Statement of Work Project No. W-153 Page 5

16. Acceptance Inspection (44)

• Prepare an Acceptance Inspection Plan .

17. Project Control (45)

• Set -up budget/schedule, integrating definitive design and construction.

• Maintain cost reports. • Prepare monthly bar chart/S curves. • Progress schedule.

18 . Cost Estimating (46)

• Prepare a final project cost estimate.

19. Procurement (49)

20 .

• Provide design reviews of the procurement and commercial equipment/material specifications.

Survey (62)

• Provide survey data of critical dimensions as input to the piping discipline for as-builting the module.

21. Construction Engineering (63)

• Perform constructability reviews and provide input to the design documents to ensure that a constructable and cost effective design is produced.

22. Records Management (65)

• Provide engineering document control services.

KEH will provide Engineering/Inspection services for the project , of which the fol l owing activities will be performed :

1. Preparation of one Acceptance Test Procedure.

2. Preparation, review, and approval of 477 engineering change notices.

SOW-W-153

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,-, Statement of Work Project No. W-153 Page 6

3. Preparation, disposition, and approval of 106 non-conformance reports.

4. Review and approval of 165 construction submittals.

5. Safety, environmental, and quality engineering support of engineering activities.

6. Acceptance Inspection of construction activities as required by the Acceptance Inspection Plan and Process Control Packages.

7. Preparation of as-built drawings at the completion of construction.

8. Preparation of the project turnover package at project completion.

SOW -W-153

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WHC-SD-W153-CDR-001 Rev. 0

STATEMENT OF WORK

OPERATING CONTRACTOR - PROJECT MANAGEMENT

PROJECT W-153

PREPARED BY: R. L. Louie

I. OBJECTIVES

W.O. NO.: ER-0183

DATE: Seotember 1990

The Operatinq Contractor shall provide project management services to the U.S. Department of Energy-Richland Operations Office (DOE-RL) from definitive design through the completion of construction and project closeout. Project management will include, but is not limited to, overall planning, daily management and technical direction, coordination, control and status reporting for all phases of the project. Before the start of definitive design, the Operating Contractor responsibility and

( authority will be formally documented in a DOE-RL approved Project \...._, Management Plan.

'-.

II. TASKS

A. Genera 1

Provide liaison with the cognizant RL office during the life of the project. Furnish the project information necessary to facilitate surveillance and evaluation of project e1ecution.

1. Provide copies of all project associated correspondence, reports, design drawings, Nonconformance Reports (NCRs), plans and schedules, cost estimates, Quality Assurance (QA) programs and related audits, Engineering Chanqe Notices (ECNs), subcontracts, work orders and supplements, minutes of meetings, test procedures, photographs, etc. All items shall be identified with the project number (W-153).

2. Provide timely notification of meetings, acceptance tests, and final inspections (with agenda when applicable).

3. Provide immediate notification of accidents, incidents, significant problems, work stoppages, etc.

4. Provide data for the Management Review Meeting.

5. Provide responsibility and authority for daily manaoement of the project as provided in the Project Management Plan (PMP).

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WHC-SD-W153- CDR-001 Rev . 0

B. Design

1. Establish pro j ect f i les responsibilities and requirements and disseminate these to project participants.

2. Provide techn i cal d i rection and assistance for design accomplished by the Architect-Engineer (A - E).

3. The Project Cognizant Engineer coordinates and takes the lead technical role in the design review process. Involves the user. site services. operations. maintenance enqineerinq. and process engineering, as necessary, in des i gn reviews. Approves Definitive Design for compliance with the Functional Design Criteria (FDC), project baseline, safety, operability, reliability, enerqy conservat i on, and cost effectiveness. Assures optimum design in terms of cost. safety, reliability, mainta i nability, accuracy, and compliance with applicable codes, standards, criteria. regulations, and Depa r tment of Energy (DOE) Management Directives.

4.

5.

6.

Approve design schedules consistent with project requirements.

Provide and/or concur with engineering reports as required.

Coordinate and integrate environmental, NEPA, permitt i ng and safety assessment act i vities into the project.

7. Update all project documents, control media, reports, schedules, and cost summaries as new information becomes available.

8. Assure that cost effectiveness is stressed in the project design and construction, and that life cycle cost analysis (LCCA). as appropriate, is A basis for design selections and decisions.

9. Participate in the team effort of developing and implementing a comprehensive, integrated project QA and/or Quality Control (QC) and/or inspection plan.

10. Provide information, dat a , records, and guidelines for the special conditions or requirement s that may impact pro j ect cost . i.e., radiation levels, securi t y requirements. escort requirements. etc.

11. Assure preparation of Fair Cost Estimate.

12. Coordinate with the Onsite Construction Contractor to assure constructibility.

J

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WHC-SD-W153- CDR-001 Rev. 0

C. Procurement(Long Lead and Engineered Equipment)

1. Assure procurement plans and schedules are consistent with project schedule requirements.

2. Initiate documentation to procure long lead and engineered equipment.

3. Provide liaison between A-E, program/project coordinators, buyers, and vendors during procurement.

4. Coordinate participation of Quality Assurance, program/project coordinators, and other cognizant personnel during procurement and in-factory acceptance testing activities.

S. Assure th~t comprehensive vendor surveys have been performed within procurement guidelines.

6. Provide overall management of procurement for engineered equipment.

D. Construction

1. Provide techni~al direction and assistance, as applicable, on construction accomplished by Onsile Construction Contractor.

2. Approved construction schedules consistent with project requirements.

3. Provide and/or concur with construction reports as required.

4. Assure industrial and nuclear safely at the construction site.

S. Update all project documents, control media, reports, schedules, and cost summaries as new information becomes available.

6. Provide coordination between operational user and construction forces to minimize interferences and facilitate the construction work. Assure user submittal review as appropriate.

7. Issue excavation and/or drilling and/or tie-in permits and welding and/or cutting permits lo the Onsite Construction Contractor. Approved radiation work procP.dures, if required, initiated by the Onsite Construction Contractor.

8. Review vendors submitlals as required and provide comments to the A­E or buyers.

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WHC-SD-W153-CDR-001 Rev. 0

9. Particioate and concur in final inspection. testing, and acceptance of completed facilities for operation.

10. Support project startup readiness review as required.

11. Assure accurate completion of as-built drawings.

12. Prepare the project close-out documents, and obtain the required approvals.

13. Arrange for disposition and/or storage of project records.

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;

Phase

Design

Procurement

Construction

PROJECT W-153

WHC-SD-W0153-CDR-001 Rev. 0 Page xx of xx

PROJECT MANAGEMENT COST ESTIMATE SUMMARY

Manhours Rate Total

Project Engineer 2745 55.40 $152,040 Cognizant Engineer 2745 55.40 152,040 Management 1370 55.40 75,880 Clerical Support 1370 24.30 33,290

Project Engineer 1370 55.40 '$75,880 Cognizant Engineer 1370 55.40 75,880 Management 915 55.40 50,680 Clerical Support 915 24.30 22,230

Project Engineer 2745 55.40 $152,040 Construction Engineer 2745 55.40 152,040 Cognizant Engineer 2060 55.40 114,090 Management 1370 55.40 75,880 Cleri"cal Support 915 24.30 22,230

Subtotal 22,635 $1,154,200

Costs for development of Preliminary Safety Analysis Report (PSAR) documentation and permitting activities will be funded from the Project Management Work Breakdown Structure and will be managed by the Project Engineer. Estimated cost for PSAR development and permi~ting activities is as follows:

PSAR Development TOTAL PROJECT MANAGEMENT COST

B-xx

$300,000 $1,454,200

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WHC -SD-Wl53 -CDR-001 Rev . 0

APPENDIX C

Work Breakdown Structure

( ' ,.

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WHC -SD-Wl53 -CDR-001 Rev. 0

WORK BREAKDOWN STRUCTURE

1.0 ENGINEERING

I . I Definitive Design (Architect -Engineer)

I.I.I 221-B Building Modifications

1.1. 1. 1 Equipment/Module 1. 1.1 .2 Jumpers 1.1.1.3 Cold Side Piping 1.1.1.4 Cold Side Instm/Elec (221-B Building and

225-B Building)

1.1 .2 225-B Building Modifications

1.1 .2.1 Equipment/Jumpers 1.1.2 . 2 Cold Side Piping 1.1.2 .3 Centrifugal Contactors

1.2 Engineering/Inspection

1.3 •ACS Configuration (Operating Contractor)

2.0 PROCUREMENT

2.1 221-B Building Modifications

2. 1. 1 Connector Head (by operating contractor) 2.1.2 Equipment (Agitators, Condenser, Pumps, DOVs) 2. 1.3 •ACS (by operating contractor)

2.2 225-B Building Modifications

2.2 . 1 Centrifugal Contactors (by operating contractor) 2. 2.2 DACS (by operating contractor)

3.0 CONSTRUCTION

3.1 Onsite Construction Contractor

3.1.1 221 -B Building Modifications

3.1.1.1 Equipment/Module 3.1.1.2 Jumpers 3.1.1.3 Cold Side Piping 3.1.1.4 Cold Side Instm/Elec 3.1.1.5 Cold Side Demolition

C-1

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3.1 .2 225 -B Building Modifications

3.1.2.1 Equipment/Jumpers 3.1 .2 . 2 Cold Side Piping 3. 1.2 .3 Cold Side Instm/Elec 3.1.2.4 Cold Side Demolition

3.3 Operating Contractor

WHC -SD-Wl 53 -CDR-001 Rev . 0

3.3 . 1 Demolition/Cleanout (Cell 38, 225-B Building Cells) 3.3.2 Fabrication of Centrifugal Contactors 3.3.3 Remote installation of in -cell equipment (221-B Building

and 225-B Building)

3.4 Operating Contractor Project Management and Engineering Support

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APPENDIX D

Outline Specifications

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OUTLINE SPECIFICATIONS

DIVISION 5 - METALS

Section 05050 Welding and Inspection

The following codes and standards shall apply in fabrication activities where welding, weld examination, and weld leak testing are involved. This includes qualification of procedures and personnel for welding and nondestructive testing.

1. American Welding Society (AWS) DI.I, Structural Welding Code-Steel: Structural steel fabrication.

a. Welding fabrication requirements.

b. Qualification of welding procedures.

c. Qualification of welding personnel.

d. Nondestructive examination requirements, except personnel requirements. This includes visual examination requirements and acceptance criteria.

2. AWS QCI, Standard for Qualification and Certification of Welding Inspectors: Qualification and certification of visual weld examination personnel.

a. All visual weld examination on structural, stainless sheet/strip/plate steel.

3. ANSI/ASME 831.3, American National Standard Code for Pressure Piping - Chemical Plant and Petroleum Refinery Piping: Process piping systems and miscellaneous piping/tubing systems.

a. Welding fabrication requirements.

b. Nondestructive examination requirements, except personnel requirements.

c. Leak/pressure testing.

4. ASME Boiler and Pressure Vessel Code, Section V, Nondestructive Examination.

a. Nondestructive examination procedural requirements for weld examination.

5. ASME Boiler and Pressure Vessel Code, Section IX, Welding and Brazing Qualifications.

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a. Qualification of welding procedures : Tank fabrication, pipe fabrication, and sheet metal fabrication.

b. Qualification of welding personnel: Tank fabrication, pipe fabrication, and sheet metal fabrication .

6. ASNT Recommended Practice SNT-TC - lA, Personnel Qualification and Certification for Nondestructive Testing: Qualification and certification of nondestructive examination personnel.

a. All nondestructive examination personnel, except for visual weld examination personnel.

Section 05120 Structural Steel

Section

1. Structural steel: Fabricated and erected in accordance with

2.

3.

4.

5.

6.

7.

8.

05500

the American Institute of Steel Construction, Inc (AISC).

Rolled steel shapes and plates: ASTM A 36.

Steel bars and rods: ASTM A 36 .

Bolts: ASTM A 325, Grade A or B.

Nuts: ASTM A 563, Grade A, heavy hex .

Wasners: ASTM F 436.

Expansion anchors: Hilti kwik-bolt fastenin.g system.

Structural tubing: ASTM A 500.

Metal Fabrications

1. Fabricate in accordance with industry standards.

DIVISION 9 - FINISHES

Section 09805 Special Protective Coating

1. Coating: Amercoat 33.

Section 09900 Painting

1. Interior: Semigloss enamel for ferrous metals.

DIVISION 13 - S~ECIAL CONSTRUCTION

Section 13440 Instrumentation

1. Install and interconnect a Bailey Network 90/INFI 90 FPMCS expansion provided by others consisting of the following:

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a. For 221-B Building, one environmentally hardened operator console, one environmentally hardened process control unit (PCU) cabinet housing, input/output (I/0) modules, redundant power supplies, redundant multifunction controllers, redundant communication modules, operator interface station (OIS), printer, calibration equipment, mounting equipment, and associated interconnecting cables for the following approximate I/0 count:

Analog Inputs (4-20 mAdc): 48 Analog Outputs (4-20 mAdc): Spare Analog Inputs (RTD): 7 Digital Outputs (relays rated 3 amp at 120 V ac, 60 Hz): 13 Digital Inputs (rated 3 mA at 120 V ac, 60 Hz): 2

b. For 225-8 Building, one environmentally hardened operator console. One environmentally hardened PCU cabinet housing I/0 modules, redundant power supplies, redundant multifunction controllers, redundant communication modules, driver electronics cabinet, environmentally hardened OIS printer, calibration equip­ment, mounting equipment, and associated interconnecting cables for the following approximate I/0 count:

Analog Inputs (4-20 mAdc): 29 Analog Outputs (4-20 mAdc): Spare Analog Inputs (RTD): 4 Digital Outputs (relays rated 3 amp at 120 V ac, 60 Hz): 54 Digital Inputs (rated 3 mA at 120 V ac, 60 Hz): 18

c. Redundant loop cables.

2. Instrument Panel Equipment

a. Differential pressure transmitter: Rosemount.

b. Diaphragm operated valve: Dahl.

c. Piston-operated valve: Jamesbury with automax actuator .

d. Jet gang valve controls: 6, approximately.

3. In-Cell Equipment

a. Diaphragm operated valve: Dahl.

b. Motor-operated valve: Keystone.

c. Resistance temperature detector: 100 ohm platinum.

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4. Out-of-Cell Equipment

a. Jet gang valve: 15 sets, approximately .

b. Solenoid valves: ASCO .

DIVISION 15 - MECHANICAL

Section 15491 Power Piping Systems

1. The following pipe is considered service piping:

Stainless Steel Carbon Steel Process Air Process Air Steam Condensate Raw Water Raw Water Steam Steam Sanitary Water Instrument Air Instrument Air

ASTM A 312 GR TP 304L ASTM A 106, GR B Carbon steel, threaded Stainless steel , welded Carbon steel, threaded Carbon steel, threaded Stainless steel, welded Carbon steel, threaded Stainless steel, welded Carbon steel, threaded Carbon steel, threaded Stainless steel, welded

Section 15493 Chemical Process Piping Systems

A. Pi ping

1. The following pipe is considered process piping:

Stainless Steel Carbon Steel Chemical Drain Dissolver Off-Gas Exhaust/Vent Exhaust/Vent Exhaust/Vent Demineralized Water 1. 2 M HN03 1. 2 M HN03

Sodium Hydroxide (NaOH) Nitric Acid (HN03 )

Nitric Acid (HN03 )

Organic Carbonate ( CO ) Nitric Acid (RN03 )

Nitric Acid (HN03 )

Precoat Hexahydrate

0-4

ASTM A 312 GR TP 304L ASTM A 106, GR B Stainless steel, welded Stainless steel , welded Carbon steel, threaded Carbon steel , welded Stainless steel, welded Stainless steel, welded Stainless steel, welded Stainless steel tubing with

compression fittings Stainless steel welded Stainless steel welded Stainless steel tubing with

compression fittings Stainless steel welded Stainless steel welded Stainless steel welded Stainless steel tubing with

compression fittings Stainless steel welded Stainless steel welded

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Sample Ut4lity Drain Vessel Off-Gas

WHC -SD -Wl53 -CDR-001 Rev . 0

Stainless steel, welded Stainless steel, welded Stainless steel, welded

2. Perform visual examination on welded systems.

3. Perform pressure testing of process piping in accordance with ANSI 831.3. Perform pressure testing of all service piping in accordance with ANSI 831.1. Instrument air and process air piping shall be pneumatically tested. All other piping shall be hydrostatically tested.

4. Flush or physically inspect piping after installation.

5.. Identify exposed piping as to fluid carried and direction of flow as specified in HPS - 111-M.

DIVISION 16 - ELECTRICAL

Section 16400 Service and Distribution (600-Volt and Below)

1. Exposed Conduit: Rigid steel, IMC or EMT.

2. Conductors:

a. Power/Control Wiring: Copper, 600 volt, THWN/THHN insulation .

b. Specialized Cables: Meet the requirements of their intended use and application.

3. Individual Compartment(s) for Existing MCC: Motor starter units for existing MCC, circuit breaker type with individual control voltage transformer.

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APPENDIX E

Energy Conservation Report and Analysis

Due to the nature of work on this project , an Energy Conservat i on Report and Analysis was not performed. However, the design of the process equipment will minimize energy consumption by use of high efficiency equipment, and wherever possible , circuit balancing and maintenance of a high power factor . ·

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APPENDIX F

Environmental Protection Evaluation

(Furnished by Westinghouse Hanford Company)

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I I

l __ _

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SIGNATURE LIST

SUBJECT : MEMORANDUM -TO-FILE - PROJECT W-1 53, TRANSU RANIC EXTRACTION (TRUEX) PILOT PLANT

Prepared by: 6-M-90 Date

ENVIRONMENTAL DIVISION

0 9054903 Attachment 1 Page 1 Of 6

I have reviewed the attached document and state to the best of my knowledge, that it was prepared in accordance with Department of Energy regulations, Orders, and guidance governing National Environmental Policy Act (NEPA) documentation. I understand that this document will be used by the Department of Energy as a basis for making a NEPA determination regarding the proposed project.

L. E. Borneman Manager Environmental Documentation

PROJECT/PROGRAM

I have reviewed the attached document and state to the best of my knowledge, that the material is true and accurately presented. I understand that this document will be used by the Department of Energy as a basis for making a NEPA determination regarding the proposed project.

Signature

F-1

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,,r~

WHC-SD-Wl53-CDR-001 Rev. 0 9054903

PROPOSED

MEMORANDUM-TO-FILE

SUBJECT: PROJECT W-153, TRANSURANIC EXTRACTION (TRUEX) PILOT PLANT

PROJECT DESCRIPTION

Attachment 1 Page 2 of 6

Future operation of the Hanford Waste Vitrification Plant (HWVP) and the Grout Treatment Facility will be dependent on reliable pretreatment of stored t ank wastes to separate the wastes into high-level and tr~suranic waste for vitrification and low-level waste for grouting . On-schedule operation of the Hanford Waste Vitr i ficat i on Plant (HWVP) is dependent on a reliable feed stream from pretreatment.

The Transuranic Extraction (TRUEX) process has been recommended for the treatment of Neutralized Cladding Removal Waste (NCRW}, Plutonium Finishing Plant (PFP) waste, and Complexant Concentrate (CC) waste on the basis of favorable laboratQry test work. Neither feed preparation operations nor the TRUEX process have been demonstrated in a plant environment. The next major step toward application of the technology to double shell tank waste is the design, ·fabrication, and operation of a remote pretreatment pilot plant. A study has concluded that the most suitable location fqr the TRUEX pilot plant will be in the 200 East Area. Feasibility studies have shown that the bulk of the sludge washing/dissolution, and solid/liquid separation equipment can be accommodated in Cell 38 of 221-B (B Plant) while the TRUEX process itself (cent~ifugal contactors for solvent extraction and solvent washing) can be accommodated in Band C Cells of 225-8, the Waste Encapsulation and Storage Facility (WESF).

This project will provide a system to demonstrate pretreatment of NCRW waste, which will include the following operat i ons: Sludge washing/dissolution, solid/liquid separations, and the TRUEX process. In addition to providing a facility to aid the design and operation of the full scale process, the pi l ot plant will produce feed material for glass waste form qualification (200 kg of oxides for each of the waste forms).

Included in the scope of this project are:

1. Demolition and disposal (as necessary) of the existing equipment i n B Plant Cell 38 and WESF Band C Cells, and the aqueous make up (AMU) areas of B Plant and WESF .

2. Design and construction of the TRUEX Pilot Plant. This includes all vesselsr piping, instrumentation, and cold chemical makeup necessary to safely and efficiently operate the pilot plant process in B Plant Cell 38 and WESF Band C Cells.

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! \

WHC-SD-Wl53-CDR-001 Rev . 0 9054903 Attachment 1 Page 3 of 6

3. Design and construction of interface p1p1ng and instrumentat i on between the Pilot Plant and other B Plant tankage that will be requ i red to transfer retrieved waste to the Pilot Plant and transfer treated waste from the Pil ot Plant.

4. Design and construction of any facility modifications that may be necessary as a result of implementing items 1 through 3.

The TRUEX Pilot Plant will provide facilities that are capable of generating data to aid the design and operation of the full - scal e prricess . These facilities include but are not limited to vessels for receiving was te transfers from the tank farm, vessels for di ssolution of solids , equipment for clarification of dissolver solutions, equ i pment for extraction of transuranics from the clarified solutions, vessels to accumulate and store product streams, equipment for controlling offgasses from the above if required, and instrumentation to control operations. In addition, the pilot plant will produce feed material for the hot lab and bench -scale glass waste form qualification program being conducted in the 324 Building.

The products of the process will consist of two streams: the solids remaining undissolved after the dissolution step will be combined with the transuranic element concentrate resulting from solvent extraction; and the solvent extraction raffinate will be combined with miscellaneous vessel flushes. The transuranic concentrate will be shipped to the 300 Area for waste form qualification studies. The raffinate will be returned to the tank farm through underground pipelines.

The feed rate to the Pilot Plant will be approximately 50 liters of liquids per hour. The waste form ·qualification program anticipates a requirement for 200 kg of oxides from each of the three types of waste material: - NCRW, PFP waste, and CC waste. Feed preparation operations will be capable of generating and shipping the required volume of glass plant feed within a 6 month operating window for each type of waste. The pilot plant will be designed to function for three years.

AFFECTED ENV!R0NMENT

The Transuranic Extraction Pilot Plant (TRUEX) Project is located i n the 200 East Area of the Hanford Site approximately 22 miles northwest of the City of Richland and about 7 miles west from the Columbia River at the closest point. The project location on the 200 Area Plateau is outs i de the projected 100 and 500 year floods. The region is categorized as one of low to moderate seismicity.

The area has a mild climate with annual precipitation of approximately six inches and infrequent periods of high winds (up to 80 miles per hour). Tornadoes are extremely rare, and no violent tornadoes have occurred in the region surrounding Hanford. The probability of a torn~do hitting any given facility on-site is estimated at ten chances in one million during any given year.

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I \

I,

I I I

\ !

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WHC-SD-Wl53-CDR-001 Rev. 0 9054903 Attachment l Page 4 of 6

The sagebrush/cheatgrass-Sandberg's bluegrass vegetative community dominates the Hanford Site . The important shrubs are big sagebrush and rabbitbrush, while the understory is primarily composed of cheatgrass and Sandberg's bl uegrass.

Most mammal species known to inhabit the Hanford Site are small, nocturnal creatures, primarily pocket mice and jackrabbits. Large mammals found on the site are deer and elk, although the elk are almost entirely on the Arid Lands Ecology Reserve. Coyotes and raptors are the primary predators. Grasshoppers are the most conspicuous insects in the community.

Only a few species of small birds nest in the steppe vegetation. Semiannual peaks in avian variety and abundance occur during migration seasons. The State and Federally registered bald eagle is a regular winter visitor to the Hanford Site, and returns during salmon spawning to nest primarily in wooded areas (i.e., between 100-0/DR and 100-H Areas and between 100-H and 100- F Areas). The only two endangered animal species known to occur in the area, the American white pelican and the perigrine falcon, are transient visitors. No species of plant or animal registered as rare, threatened, or endangered are known to depend on the habitat in tha vicinity of the proposed project.

IMPACTS

No significant environmental impacts have been identified for this project. This section provides information on those impacts which have been identified for the proposed Transuranic Extraction Pilot Plant Project.

Because this will be a pilot plant operation with relatively small feed rates to the process, quantities of airborne emissions and liquid effluents produced will be insignificant.

Small amounts of ammonia (NH3) and oxides of nitrogen (NOi) will be generated by processing the wastes. Expected quantities will be well below the trigger levels for these non-radioactive pollutants as stated in the Federal Code of Regulations, Title 40, Part 52.

The B Plant/WESF complex is included in the Radioactive Air Emissions Permit for the Hanford Site from the W~shington State Department of Health. The radiological emissions from the pilot plant are expected to be insignificant and no greater than emissions during the 1980 to 1986 time frame for B Plant/WESF operations.

The only liquid effluents from the process will be spent cooling water and/or steam condensates, which are expected to contain no radionuclides or hazardous wastes. Steam condensate i's normally routed to the 216-8-63 trench, however future plans call for the use of the 216-B-3 pond. Waste cooling water will be sent to the 216-B-3 pond. If either of these waste streams would show a high level of beta activity, it would be diverted to Tank TK-10-1 (in B Plant).

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WHC-SD-W153-CDR-001 Re~Os~go3 Attachmentl Page 5 of 6

Demolition of the existing equipment in B Plant Cell 38 and WESF Band C -~- Cells will produce some radioactively contaminated equipment and materials

which will be disposed of in accordance with all applicable Federal ~nd state waste management regulations and DOE Orders. All wastes will be di sposed of in existing Hanford waste management facilities or approved offsite facilities if required.

Small quantities of nonradioactive and nonhazardous construction scrap may result from construction activities. This scrap will be disposed of in the Hanford Central Landfill or other appropriate disposal site.

Construction activities and pilot plant operations may result in slightly elevated noise levels .

The proposed action will occur within existing buildings in previously disturbed portions of the 200 East Area and no wetlands, wildlife habitat areas, archeological sites, or other cultural resources are located in the vicinity. The 200 Area Plateau does not lie within the 100 or 500 year floodplain.

COORDINATION WITH FEDERAL, STATE, REGIONAL, OR LOCAL PLANS

This activity provides no known conflict with federal, state, regional, or local environmental plans. This project is not part of a larger project that may require an EA or an EIS.

B Plant is currently permitted as an interim status facility under the Washington Administrative Code 173-303-805 and has a Part A Permit Application on file with the Washington State Department of Ecology. A Part B Permit Application will be prepared at a later date in accordance with provisions of the Hanford Federal Facility Agreement and Consent Order (Agreement) . . WESF is not a RCRA permitted facility. Any modifications to the Part A Permit or additional permitting required for the Pilot Plant will be addressed as identified.

The B Plant/WESF complex is included in the Radioactive Air Emissions Permit for the Hanford Site from the Washington State Department of Health. Notification to the state will be required before construction of the pilot plant begins.

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(.. '- .,.

WHC -SD-Wl53-CDR-001 Rev. 0

NATIONAL ENVIRONMENTAL POLICY ACT (NEPA) DETERMINAT ION

9054903 Attachment 1 Page 6 of 6

The potential environmental impacts of this action are clearly insignificant. The project is not a major Federal action significantly affect i ng the quality of the human environment. I therefore determine that neither an Environmental Assessment nor an Environmental Impact Statement is requ i red .

Signatura: ___________ _

Title:

Date:

EH-25 has reviewed this determination and has no objection.

Signature: ___________ _

Date:

cc: M. J. Lawrence, OOE-RL

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APPENDIX G

Economic Analysis and Life Cycle Cost Analysis

Due to the nature of work on this project, an Economic Analysis and Life Cycle Cost Analysis were not performed. There were no other alternatives to consider.

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APPENDIX H

Plant Forces Work Review

(Furnished by Westinghouse Hanford Company)

(Thi's document is currently being revised to reflect the conceptual cost estimate, schedule, method of performance, and work breakdown structure . It will be provided under separate cover.)

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APPENDIX I

Physically Handicapped Assessment

(This project is within the exceptions set out in FPMR subpart 101 -19-604, specifically, the structures provided by this project are not intended for use by the handicapped . )

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APPENDIX J

Instrument Identification

Legend Abbreviations Table I - New Table II - New

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~---- - ----------------- -

LEGEND

Per ISA SS.l 1984

FE flow element FT flow transmitter HS hand switch PI pressure indic~tor TE temperature element

Not per ISA SS.l

DP! DPT EV LOE MC PA PAS PIJC PIJGV SGR SGT WFA WFAS WFI WFR WFT

differential pressure indicator differential pressure transmitter electric operated valve leak detection element manual controller pressure alarm pressure alarm switch pressure indicator jet controller pressure indicator jet gang valve specific gravity recorder specific gravity transmitter weight factor alarm weight factor alarm switch weight factor indicator weight factor recorder weight factor transmitter

ABBREVIATIONS

Per ANSI Yl . l 1972

Unless otherwise noted below

Not per ANSI Yl.l

DACS DOV FPMCS IP J JGV MOV OPR p

data acquisition and control system diaphragm operated valve facility processing monitoring and control instrument panel jet pump jet gang valve motor operated valve operator pump

J-1

WHC -SD-Wl53 - CDR-001 Rev. 0

system

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P&ID piping and instrument diagram POV piston operated valve TB• to be determined TRU transuranic XMTRR transmitter rack

NOTE

WHC-S0 -Wl53 -CDR-001 Rev. 0

1. Tables are preliminary. Actual I/0 and demolition requirements pending completion of P&IOs during definitive design.

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,,~-,\ e"' \ ,,- . ~

Page: No. 1 09/06/90

TABLE I - NEW I/0

MONITOR/ INTERLOCK/

INSTRUMENT DESCRIPTION P&ID DWG LOCATION CONTROL REMARKS

. ES-0153-M35° DOV-38-1-1 TK-38-1 COIL OUTLET CELL 38 EV-38-1-1 NEW/NOZ 216

DOV-38-2-1 TK-38-3 to TK-38-2 ES-0153-M39 CELL 38 EV-38-2-1 NEW/NOZ 258 XFR

DOV-38-2-3 TK-38-2 COIL OUTLET ES-0153-M39 CELL 38 EV-38-2-3 NEW/NOZ 217 DOV-38-3-2 TK-38-3 to TK-38-1 ES-0153-M40 CELL 38 EV-38-3-2 NEW/NOZ 258

XFR DOV-38-3-3 TK-38-3 COIL OUTLET ES-0153-M40 CELL 38 Ev'-38-3-3 NEW/NOZ 258 DOV-38-5-1 TK-38-3 FILTER FEED ES-0153-M36 CELL 38 EV-38-5-lA NEW/NOZ 256 DOV-38-5-2 TK-38-2 FILTER FEED ES-0153-M36 CELL 38 EV-38-5-2 NEW/NOZ 256 DOV-38-5-3 TK-38-1 FILTER FEED ES-0153-M36 CELL 38 EV-38-5-3 NEW/NOZ 256 DOV-38-5-4 FILTRATE TO TK-38-4 ES-0153-M36 CELL 38 EV-38-5-4 NEW/NOZ 221 DOV-38-5-5A/B F-38-1 AIR BACKFLUSH ES-0153-M36 CELL 38 EV-38-5-5A/B NEW/NOZ TBD DOV-38-5-6 F-38-1 ACID BACKFLUSH ES-0153-M36 CELL 38 EV-38-5-1 NEW/NOZ 62 DOV-38-8-1 TK-38-8 COIL OUTL IN ES-0153-M36 OPR GALL EV-38-8-1 NEW/NOZ 216 DOV-E-38-1-2 CONDENSER COIL OUTLET ES-0153-M38 CELL 38 EV-38-1-2 NEW/NOZ 216

G DPI-11-2-2 TK-11-2 PRESS H-2-35311-2 TBD NA EXST/NOZ 38 I

w DPI-25-1-1 TK-25-1 PRESS H-2-60633-1 IP 25A . NA EXST/NOZ TBD DPI-35-0-1 CELL 35 PRESS H-2-35335-2 OPR GALL NA EXST/NOZ 227 DPI-35-1-2 TK-35-1 PRESS H-2-35335-1 IP 35B NA EXST/NOZ 23 DPI-35-2-2 TK-35-2 PRESS H-2-35335-2 OPR GALL NA EXST/NOZ 38 DPI-36-0-1 CELL 36 PRESS H-2-35336-1 OPR GALL NA EXST/NOZ 65 DPI-36-1-1 TK-36-1 PRESS H-2-35336-1 IP 36A NA EXST/NOZ 65 :E:

:c DPI-36-2-1 TK-36-2 PRESS H-2-35336-2 IP· 36B NA EXST/NOZ 62 n

I DPI-36-3-2 TK-36-3 PRESS H-2-35336-3 TBD NA EXST/NOZ 80 V>

DPI-39-0-1 CELL 39 PRESS H-2-35339-1 OPR GALL NA EXST/NOZ 234 0 I

DPT-25-0-1 CELL 25 PRESS H-2-35325-1 IP 25A FPMCS EXST/NOZ 22 :E: I--'

DPT-25-1 TK-25-1 PRESS H-2-35325-1 XMTRR 25 FPMCS EXST/NOZ 20 u, w

DPT-25-2 TK-25-2 PRESS H-2-35325-2 XMTRR 25 FPMCS EXST/NOZ 38 I n

DPT-35-0-1 CELL 35 PRESS ES-0153-M33 TBD DACS NEW/NOZ TBD 0 :;:o

DPT-3'5-1-1 TK-35-1 PRESS ES-0153-M33 TBD DACS NEW/NOZ 23 I 0 0 _,

:;:o rt)

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Pa '-cl ~ No . 2 09/ 06/ 90

TABLE I - NEW I/0

MONITOR/ INTERLOCK/

INSTRUMENT DESCRIPTION P&ID DWG LOCATION CONTROL REMARKS

DPT-35-2-1 TK-35-2 PRESS ES-0153-M33 TBD TBD NEW/NOZ 38 DPT-36-0-1 CELL 36 PRESS ES - 0153-M33 TBD DACS NEW/NOZ 65 DPT-36-1-1 TK-36-1 PRESS ES-0153-M33 TBD DACS NEW/NOZ 65 DPT-36-2-1 TK-36-2 PRESS ES-0153-M33 TBD DACS NEW/NOZ 62 DPT-36-3-1 TK-36-3 PRESS ES-0153-M33 TBD DACS NEW/NOZ 80 DPT-38-0-1 CELL 38 PRESS ES-0153-M39 TBD DACS NEW/NOZ 47 DPT-38-1-1 TK-38-1 PRESS ES-0153 - M35 TBD DACS NEW/NOZ 229 DPT-38-1-2 E-38-1 PRESS ES-0153-M38 TBD DACS NEW/NOZ 238 DPT-38-2-1 TK-38-2 PRESS ES-0153-M39 TBD DACS NEW/NOZ 214 DPT-38-3-1 TK-38-3 PRESS ES-0153-M40 TBD DACS NEW/NOZ 80 DPT-38-4-1 TK-38-4 PRESS ES-0153-M34 TBD DACS NEW/NOZ 239 DPT-38-5-1 TK-38-5 PRESS ES-0153-M36 TBD DACS NEW/NOZ 242 DPT-38-6-1 TK-38-6 PRESS ES-0153-M37 TBD DACS NEW/NOZ 249 DPT-38-7-1 TK-38-7 PRESS ES-0153-M38 XMTRR 38 DACS NEW/NOZ 213

c... DPT-38-8-1 DEMISTER DIFF PRESS ES-0153-M38 TBD DACS NEW/NOZ 233 I

.p. DPT-39-0-1 CELL 39 PRESS ES-0153-M41 TBD DACS NEW/NOZ 203 DPT-39-1-1 TK-39-1 PRESS ES-0153-M39 XMTRR 38 DACS NEW/NOZ 23 EV-11-2-1 POV-11-2-1 CONT ES-0153-M32 TBD HS-11-2-1 NEW/NOZ 5 EV-11-2-2 POV-11-2-2 CONT ES-0153-M32 TBD HS-11-2-2 NEW/NOZ 5 EV-11-2-3 POV-11-2-3 CONT ES-0153-M32 TBD HS-11-2-3 NEW/NOZ 5 ::E

EV-38-1-1 DOV-38-1-1 CONT ES-Ol53-M35 OPR GALL HS-38-1-1 NEW/NOZ 216 :c

EV-38-1-2 DOV 38-1-2 CONT ES-0153-M35 OPR GALL HS-38-1-2 NEW/NOZ 216 n I

EV-38-2-1 DOV-38-2-1 CONT ES-0153-M39 OPR GALL HS-38-2-1 NEW/NOZ 258 (/')

Cl

EV-38-2-2 POV-38-2-2 CONT ES-0153-M39 OPR GALL HS-38-2-2 NEW/NOZ 219 I ::E

EV-38-2-3 DOV-38-2-3 CONT ES-0153-M39 OPR GALL HS-38-2-3 NEW/NOZ 217 ...... u,

EV-38-3-2 DOV-38-3-2 CONT ES - 0153-M40 OPR GALL HS-38-3-_2 NEW/NOZ 258 w

EV-38-3-3 DOV-38-3-3 CONT ES-0153-M40 OPR GALL HS-38-3-3 NEW/NOZ 258 I n

EV-38-3-4 POV-38.-3-4 CONT ES-0153-M40 OPR GALL HS-38-3-4 NEW/NOZ 219 Cl ;::o

EV-38-4-1 POV-38-4-1 CONT ES-0153-M34 OPR GALL HS-38-4-1 NEW/NOZ 216 I 0

EV-38-5-1 DOV-38-5-1 CONT ES-0153-M36 OPR GALL HS-38-5-1 NEW/NOZ 256 0 ..... ;::o CD < . 0

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MONITOR/ INTERLOCK/

INSTRUMENT DESCRIPTION P&ID DWG LOCATION CONTROL REMARKS

EV-38-5-2 DOV-38-5-2 CONT ES-0153-M36 OPR GALL HS-38-5-2 NEW/NOZ 256

EV-38-5-5 DOV-38-5-6 CONT ES-0153-M36 OPR GALL HS-38-5-5 NEW/NOZ 62

EV-38-5-5A/B DOV-38-5-5A CONT ES-0153-M36 OPR GALL HS-38-5-5A/B NEW/NOZ TBD

EV-38-6-1 DOV-38-6-1 CONT ES-0153-M37 OPR GALL HS-38-6-1- NEW/NOZ 248

EV-38-8-1 DOV-38-8-1 CONT ES-0153-M38 OPR GALL HS-38-8-1 NEW/NOZ TBD

FT-38-3 TK-38-3 OFFGAS FLOW ES-0153-M40 CELL 38 DACS NEW/NOZ 76

FT-38-4 FILTRATE FLOW .. ES-0153-M36 CELL 38 DACS NEW/NOZ 76

FT-38-6 TK-38-6 OFFGAS FLOW ES-0153-M37 CELL 38 DACS NEW/NOZ 76

HS-11-2-1 EV-11-2-2 CONT ES-0153-M32 TBD CONT NEW HS-11-2-2 EV-11-2-2 CONT ES-0153-M32 TBD CONT NEW HS-11-2-3 EV-11-2-3 CONT ES-0153-M32 TBD CONT NEW HS-38-1-1 EV-38-1-1 CONT ES-0153-M35 DACS CONT NEW HS-38-1-2 EV-38-1-2 CONT ES-0153-M35 DACS CONT NEW

G HS-38-2-1 EV-38-2-1 CONT ES-0153-M39 DACS CONT NEW

I HS-38-2-2 EV-38-2-2 CONT ES-0153-M39 DACS CONT NEW · Ul HS-38-2-3 EV-38-2-3 CONT ES-0153-M39 DACS CONT NEW

HS-38-3-2 EV-38-3-2 CONT ES - 0153-M39 DACS CONT NEW HS-38-3-3 EV-38-3-3 CONT ES-Ol53-M39 DACS CONT NEW HS-38-3-4 EV-38-3-4 CONT ES-0153-M40 DACS CONT NEW HS-38-4-1 EV-38-4-1 CONT ES-0153-M34 DACS CONT NEW HS-38-5-1 EV-38-5-1 CONT ES-0153-M36 DACS CONT NEW :::E:

HS-38-5-2 EV-38-5-2 CONT ES-0153-M36 DACS CONT NEW :::c n

HS-38-5-SA/B EV-38-5-5A/B CONT ES-0153-M36 DACS CONT NEW I (../')

HS-38-6-1 EV-38-6-1 CONT ES-0153-M37 DACS CONT NEW c::, I

J-11-2-1 RETRIEVED SLUDGE ES-0153-M32 CELL 11 JGV-11-2-1 NEW, FOR REF :::E: ....... J-11-2-2 DECANT ES-0153-M32 CELL 11 JGV-11-2-2 NEW, FOR REF Ul

J - 12-1-3 BACKFLUSH TO TK-11-2 ES-0153-M32 CELL 12 JGV-12-1-3 NEW, FOR REF (.,.J I

J-25-1 XFR TO TK-25-2 H-2-35325-1 CELL 25 JGV-25-1-1 EXST, FOR REF n c::,

J-25-2 XFR TO TK-25-1 H-2-35325-2 CELL 25 JGV-25-2-1 EXST, FOR REF :::0 I

J-35-1-1 TK-35-1 TO TK-35-2 H-2-35335-2 CELL 35 JGV-35 - 1-1 EXST, FOR REF 0 0 --'

XFR :::0 It)

< . 0

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TABLE I - NEW I/0

MONITOR/ INTERLOCK/

INSTRUMENT DESCRIPTION P&ID DWG LOCATION CONTROL REMARKS

J-35-2-3 TK-35-2 TO TK-25-2 H-2-35333-2 CELL 35 JGV-35-2-3 EXST, FOR REF J-35-2-4 TK-35-1 TO TK-35-2 H-2-35333-1 CELL 35 JGV-35-2-4 EXST, FOR REF

XFR J-35-2-7 XFR TO TK-36-3 ES-0153-M33 CELL 35 JGV-35-2-1 NEW, FOR REF J-36-1-1 TK-36-1 TO TK-36-2 H-2-35333-1 CELL 36 JGV-36-1-1 EXST, FOR REF

XFR J-36-1-2 XFR TO TK-25-2 ES-0153-M33 CELL 36 JGV-36-1-2 NEW/NOZ 67 J-36-2 TK-36-2 TO TK-36-1 H-2-35333-1 CELL 36 JGV-36-2-1 EXST, FOR REF J-36-3-1 XFR TO TK-38-3 H-2-35336-3 CELL 36 JGV-36-3-1 EXST, FOR REF J-36-3-2 XFR TO TK-36-1 ES-0153-M33 CELL 35 JGV-35-3-2 NEW, FOR REF J-38-1-1 XFR TO TK-38-2,3 ES-0153-M35 CELL 38 JGV-38-1-1 NEW, FOR REF J-38-1-2 XFR TO TK-36-3 ES-0153-M35 CELL 38 JGV-38-1-2 NEW, FOR REF J-38-2-1 XFR TO TK-38-3 ES-0153-M39 CELL 38 JGV-38-2-1 NEW, FOR REF J-38-2-2 XFR TO TK-38-1 ES-0153-M39 CELL 38 JGV-38-2-2 NEW, FOR REF

c... J-38-3-1 XFR TO TK- 38 - 2 ES-0153-M40 CELL 38 JGV-38-3-1 NEW, FOR REF I J-38-4-1 XFR TO BUILDING 225B ES-0153-M34 CELL 38 JGV-38-4-1 NEW, FOR REF 0)

J-38-5-1 SOLIDS RECYCLE ES-0153-M36 CELL 38 JGV-38-5-1 NEW, FOR REF J-38-5-2 TO TK-35-1 ES-0153-M36 CELL 38 JGV-38-5-2 NEW, FOR REF J-38-6-1 NON TRU TO CELL 25 ES-0153-M37 CELL 38 JGV-38-6-1 NEW, FOR REF J-38-7-1 XFR TO TK-39-1 ES-0153-M38 CELL 38 JGV-38-7-1 NEW, FOR REF ~

J-38-7-2 TK-38-8 TO NOx COLUMN ES-0153-M38 CELL 38 JGV-38-7-2 NEW, FOR REF :::c n

J-38-SUMP CELL 38 SUMP JET PUMP ES-0153-M39 CELL 38 JGV-38-SMP NEW, FOR REF I (./)

J-39-SUMP CELL 39 SUMP JET PUMP H-2-35339-1 CELL 39 JGV-39-SUMP EXST J-39-0-1/NOZ 0 I

203 ~

JC-38-1-1 JGV-38-1-1 CONT H-2-35338-2 IP 38B JGV-38-1-1 EXST JC-38-38B-l/NOZ I-' Ul

62 w I

JC-38-1-2 JGV-38-1-2 CONT H-2-35338-1 IP 38D JGV-38-1-2 EXST _JC-38-38D-1/NOZ n 0

56. ;o I

JC-38-2-1 JGV-38-2-1 CONT ES-0153-M39 IP 38F JGV-38-2-1 NEW/NOZ 208 0 0

JC-38-2-2 JGV-38-2-2 CONT ES-0153-M39 IP 38F JGV-38-2-2 NEW/NOZ 236 ..... ;o (I)

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TABLE I - NEW 1/0

MONITOR/ INTERLOCK/

INSTRUMENT DESCRIPTION P&ID DWG LOCATION CONTROL REMARKS

JC-38-3-1 JGV-38-3-1 CONT H-2-35338-5 IP 38F JGV-38-3-1 EXST JC-38-38F-1/NOZ 83

JC-38-4-1 JGV-38-4-1 CONT H-2-35338-3 IP 38F JGV-38-4-1 EXST JC-38-38F-6/NOZ 71

JC-38-5-1 JGV-38-5-1 CONT ES-0153-M38 TBD JGV-38-5-1 NEW/NOZ 236 JC-38-5-2 JGV-38-5-2 CONT H-2-35338-3 IP 38F JGV-38-5-2 EXST JC-38-38F-4/NOZ

73 JC-38-6-1 JGV-38-6-1 CONT ES-0153-M37 TBD JGV-38-6-1 NEW/NOZ 248 JC-38-7-1 JGV-38 - 7-1 CONT ES-0153-M38 TBD JGV-38-7-1 NEW/NOZ 236 JC-38-7-2 JGV-38-7-2 CONT H-2-35338-6 IP 38F JGV-38-7-2 EXST JC-38-38F-3/NOZ

62 JC-38-SUMP JGV-38-SUMP CONT H-2-35338-6 IP ·38F JGV-38-SMP EXST JC-38-0-1/NOZ

208 JC-39-SUMP JGV-39-SUMP CONT H-2-35339-1 IP 39C JGV-39-SUMP EXST JC-39-0-1/NOZ

c.... 203 I JGV-11-2-lA J-11-2-1 CONT ES-0153-M32 TBD MNL OPR NEW/NOZ 29 -..J

JGV-11-2-lB J-11-2-1 CONT ES-0153-M32 TBD MNL OPR NEW/NOZ 29 JGV-11-2-lC J-11-2-1 CONT ES-0153-M32 TBD MNL OPR NEW/NOZ 29 JGV-ll-2-2A J-11-2-2 CONT ES-0153-M32 TBD MNL OPR NEW/NOZ 12 :i:: JGV-ll-2-2B J-11-2-2 CONT ES-0153-M32 TBD MNL OPR NEW/NOZ 12 :c

n JGV-ll-2-2C J-11-2-2 CONT ES-0153-M32 TBD MNL OPR NEW/NOZ 12 I

JGV-12-1-JA J-12-1-3 CONT ES-0153-M32 TBD MNL OPR NEW/NOZ 76 (/)

0

JGV-12-1-3B J-12-1-3 CONT ES-0153-M32 . TBD MNL OPR NEW/NOZ 76 I :i::

JGV-12-1-JC J-12-1-3 CONT ES-0153-M32 TBD MNL OPR NEW/NOZ 76 I-' tTl

JGV-25-lA J-25-1-1 CONT H-2-35325-1 IP 25C MNL OPR EXST/NOZ 12 w I

JGV-25-1B J-25-1-1 CONT H-2-35325-1 IP 25C MNL OPR EXST/NOZ 12 n 0

JGV-25-lC J-25-1-1 CONT H-2-35325-1 IP 25C MNL OPR EXST/NOZ 12 ;o

JGV-25-2A J-25-2-1 CONT H-2-35325-2 IP 250 MNL OPR EXST/NOZ 34 I 0

JGV-25-2B J-25-2-1 CONT H-2-35325-2 IP 250 MNL OPR EXST/NOZ 34 0 _. JGV-25-2C J-25-2-1 CONT H-2-35325-2 IP 250 MNL OPR EXST/NOZ 34 ;o

It)

< . 0

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TABLE I - NEW 1/0

MONITOR/ INTERLOCK/

INSTRUMENT DESCRIPTION P&ID DWG LOCATION CONTROL REMARKS

JGV-35-1-lA J-35-1-1 CONT H-2-35335-2 IP 35C MNL OPR EXST/NOZ 22

JGV-35-1-1B J-35-1-1 CONT H-2-35335-2 IP 35C MNL OPR EXST/NOZ 22

JGV-35-1-lC J-35-1-1 CONT H-2-35335-2 IP 35C MNL OPR EXST/NOZ 22

JGV-35-2-)A J-35-2-3 CONT H-2-35335-2 IP 35C MNL OPR EXST/NOZ 3

JGV-35-2-3B J-35-2-3 CONT H-2-35335-2 IP 35C MNL OPR EXST/NOZ 3

JGV-35-2-)C J-35-2-3 CONT H-2-35335-2 IP 35C MNL OPR EXST/NOZ 3

JGV-35-2-4A J-35-2-4 CONT H-2-35335-1 IP 35B MNL OPR EXST JGV-35-2TO35-1/NOZ 12

JGV-35-2-4B J-35-2-4 CONT H-2-35335-1 IP 35B MNL OPR EXST JGV-35-2TO35-1/NOZ 12

JGV-35-2-4C J-35-2-4 CONT H-2-35335-1 IP 35B· MNL OPR EXST JGV-35-2TO35-1/NOZ

c.... 12 I

co JGV-35-2-7A J-35-2-7 CONT ES-0153-M33 TBD MNL OPR NEW/NOZ 227

JGV-35-2-7B J-35-2-7 CONT ES-0153-M33 TBD MNL CPR NEW/NOZ 227

JGV-35-2-7C J-35-2-7 CONT ES-0153-M33 TBD MNL OPR NEW/NOZ 227

JGV-36-1-lA J-36-1-1 CONT H-2-35336-3 TBD MNL OPR NEW JGV-SPARE/NOZ 78 '

JGV-36-1-1B J-36-1-1 CONT H-2-35336-3 TBD MNL OPR NEW JGV-SPARE/NOZ 78

JGV-36-1-lC J-36-1-1 CONT H-2-35336-3 TBD MNL OPR NEW JGV-SPARE/NOZ 78 ~

JGV-36-1-2A J-36-1-2 CONT ES-0153-M33 TBD MNL OPR NEW/NOZ 67 :c ("")

JGV-36-1-2B J-36-1-2 CONT ES-0153-M33 TBD MNL OPR NEW/NOZ 67 I (./')

JGV-36-1-2C J-36-1-2 CONT ES-0153-M33 TBD MNL OPR NEW/NOZ 67 0 I

JGV-36-2A J-36-2 CONT H-2-35336-2 IP 36B MNL OPR EXST/NOZ 54 ~ ...... JGV-36-2B J-36-2 CONT H-2-35336-2 IP 36B MNL OPR EXST/NOZ 54 u,

JGV-36-2C J-36-2 CONT H-2-35336-2 IP 36B MNL OPR EXST/NOZ 54 w I

JGV-36-3-lA J-36-3-1 CONT H-2-35336-3 IP 36C MNL OPR EXST/NOZ 45 ("")

0

JGV-36-3-1B J-36-3-1 CONT H-2-35336-3 IP 36C MNL OPR EXST/NOZ 45 ::0 I

JGV-36-3-lC J-36-3-1 CONT H-2-35336-3 IP 36C MNL OPR EXST/NOZ 45 0 0 ~

::0 ct> < . 0

-- - ---- - - --- - - - ---- - - --

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TABLE I - NEW l/0

MONITOR/ INTERLOCK/

INSTRUMENT DESCRIPTION P&ID DWG LOCATION CONTROL REMARKS

JGV-36-3-2A J-36-3-2 CONT ES-0153-M33 TBD MNL OPR NEW/NOZ 202

JGV-36-3-2B J-36-3-2 CONT ES-0153-M33 TBD MNL OPR NEW/NOZ 202

JGV-36-3-2C J-36-3-2 CONT ES-0153-M33 TBD MNL OPR NEW/NOZ 202

JGV-38-1-lA J-38-1-1 CONT H-2-35338-2 OPR GALL JC-38-1-1 EXST/NOZ 62

JGV-38-1-1B J-38-1-1 CONT H-2-35338-2 OPR GALL JC-38-1-1 EXST/NOZ 62

JGV-38-1-lC J-38-1-1 CONT H-2-35338-2 OPR GALL JC-38-1-1 EXST/NOZ 62

JGV-38-l-2A J-38-1-2 CONT H-2-35338-4 OPR GALL JC-38-1-2 EXST JGV-38-4-lA/NOZ 56

JGV-38-1-2B J-38-1-2 CONT H-2-35338-4 OPR GALL JC-38-1-2 EXST JGV-38-4-1B/NOZ 56

JGV-38-l-2C J-38-1-2 CONT H-2-35338-4 OPR GALL JC-38-1-2 EXST JGV-38-4-lC/NOZ 56

JGV-38-2-lA J-38-2-1 CONT ES-0153-M39 TBD JC-38-2-1 NEW/NOZ 208

c.... JGV-38-2-1B J-38-2-1 CONT ES-0153-M39 TBD JC-38-2-1 NEW/NOZ 208 I JGV- 38-2-lC J-38-2-1 CONT ES-0153-M39 TBD JC-38-2-1 NEW/NOZ 208

I.O JGV-38-2-2A J-38-2-2 CONT ES-0153-M38 TBD JC-38-2-2 NEW/NOZ 236

JGV-38-2-2B J-38-2-2 CONT ES-0153-M38 TBD JC-38-2-2 NEW/N0Z 236

JGV-38-2-2C J-38-2-2 CONT ES-0153-M38 TBD JC-38-2-2 NEW/N0Z 236

JGV-38-3-lA J-38-3-1 CONT H-2-35338-5 OPR GALL JC-38-3-1 EXST JGV-38-8-lA/NOZ 83 ::E

JGV-38-3-1B J-38-3-1 CONT H-2-35338-5 OPR GALL JC-38-3-1 EXST JGV-38-8-1B/NOZ ::c n

83 I

JGV-38-3-lC J-38-3-1 CONT H-2-35338-5 OPR GALL JC-38-3-1 EXST JGV-38-8-lC/NOZ Vl 0 I

83 ::E

JGV-38-4-lA J-38-4-1 CONT H-2-35:pB-3 OPR GALL JC-38-4-1 EXST JGV-38-2-1/NOZ ' ~ U1

71 w I

JGV-38-4-1B J-38-4-1 CONT H-2-35338-3 OPR GALL JC-38-4-1 EXST JGV-38-2-1/NOZ n 0

71 ;:;o I

JGV-38-4-lC J-38-4-1 CONT H-2-35338-3 OPR GALL JC-38-4-1 EXST JGV-38-2-1/NOZ 0 0

71 --;o ro < . 0

- --· - - -- ---- ------------- ----

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MONITOR/ INTERLOCK/

· INSTRUMENT DESCRIPTION P&ID DWG LOCATION CONTROL REMARKS

JGV-38-5-lA J-38-5-1 CONT ES-0153-M38 TBD JC-38-5-1 NEW/NOZ 236 JGV-38-5-1B J-38-5-1 CONT ES-0153-M38 TBD JC-38-5-1 NEW/NOZ 236 JGV-38-5-lC J-38-5-1 CONT ES-0153-M38 TBO JC-38-5-1 NEW/NOZ 236 JGV-38-5-2A J-38-5-2 CONT ES-0153-M36 TBO JC-38-5-2 NEW/NOZ 73 JGV-38-5-2B J-38-5-2 CONT ES-0153-M36 TBO JC-38-5-2 NEW/NOZ 73 JGV-38-5-2C J-38-5-2 CONT ES-0153-M36 TBO JC-38-5-2 NEW/NOZ 73 JGV-38-6-lA J-38-6-1 CONT ES-0153-M37 OPR GALL JC-38-6-1 NEW/NOZ 248 JGV-38-6-1B J-38-6-1 CONT ES-0153-M37 OPR GALL JC-38-6-1 NEW/NOZ 248 JGV-38-6-lC J-38-6-1 CONT ES-0153-M37 OPR GALL JC-38-6-1 NEW/NOZ 248 JGV-38-7-lA J-38-7-1 CONT ES-0153-M38 TBO JC-38-7-1 NEW/NOZ 236 JGV-38-7-1B J-38-7-1 CONT ES-0153-M38 TBO JC-38-7-1 NEW/NOZ 236 JGV-38-7-lC J-38-7-1 CONT ES-0153-MJB TBO JC-38-7-1 NEW/NOZ 236 JGV-38-7-2A J-38-7-2 CONT ES-0153-M38 TBO JC-38-7-2 NEW/NOZ 62

c_. JGV-38-7-2B J-38-7-2 CONT ES-0153-M38 TBO JC-,-38-7-2 NEW/NOZ 62 I ....... JGV-38-7-2C JC-38-7-2 CONT ES - 0153-MJB TBO JC-38-7-2 NEW/NOZ 62 0

JGV-38-SUMPa J-38-SUMP CONT H-2-35338-6 OPR GALL JC-38-SUMP EXST/NOZ 208 JGV-38-SUMPb J-38-SUMP CONT H-2-35338-6 OPR GALL JC-38-SUMP EXST/NOZ 208 JGV-38-SUMPc J-38-SUMP CONT H-2-35338-6 OPR GALL JC-38-SUMP EXST/NOZ 208 JGV-39-SUMPA J-39-SUMP CONT H-2-35339-1 OPR GALL MNL OPR EXST/NOZ 203 JGV-39-SUMPB J-39-SUMP CONT H-2-35339-1 OPR GALL MNL OPR EXST/NOZ 203 JGV-39-SUMPC JGV-39-SUMP CONT H-2-35339-1 OPR GALL MNL OPR EXST/NOZ 203 ~

LDE-25-0-1 CELL 25 LEAK DET H-2-35325-2 CELL 25 FPMCS EXST/NOZ 9 :::i::: n

LDE-35-1-1 CELL 35 LEAK DET H-2-35335-1 CELL 35 TR 36 EXST/NOZ 26 I (.I)

LDE-36-0-1 CELL 36 LEAK DET H-2-35336-2 CELL 36 TR 36 EXST/NOZ 50 c::, I

MC-11-2-1 JGV-11-2-1 CONT H-2-35311-2 TBO JGV-11-2-1 EXST/NOZ 40 ~ -PI-25-1-1 TK-25-1 PRESS l{-2-35325-1 IP 250 FPMCS EXST/NOZ 25 l.n

PI-25-2-1 TK-25-2 PRESS H-2-35325-1 IP 25B NA EXST/NOZ 211 w I

PIJ-39-SUMP CELL 39 SUMP H-2-35338-6 IP 390 WFI-39-SUMP EXST/NOZ 203 n c::,

PIJC-38-1-1 JC-38-1-1 PRESS H-2-35338-:2 IP 380 MON EXST JC-38-38B-1/NOZ ;;o I

62 0 0 ...... ;;o fl)

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INSTRUMENT DESCRIPTION P&ID DWG LOCATION CONTROL REMARKS

PIJC-38-1-2 JC-38-1-2 PRESS H-2-35338-4 IP 38B MON EXST JC-38-380-1/NOZ 56

PIJC-38-2-1 JC-38-2-1 PRESS ES-0153-M39 TBO MON NEW/NOZ 208 PIJC-38-2-2 JC-38-2-2 PRESS ES-0153-M38 TBD MON NEW/NOZ 236 PIJC-38-3-1 JC-38-3-1 PRESS H-2-35338-5 IP 38F MON EXST JC-38-38F-1/NOZ

83 PIJC-38-4-1 JC-38-4-1 PRESS H-2-35338-3 IP 380 MON EXST

PIJC-38-38F-6/NOZ 71 PIJC-38-5-1 JC-38-5-1 PRESS ES-0153-M38 TBO MON NEW/NOZ 236 PIJC-38-5-2 JC-38-5-2 PRESS H-2-35338-3 IP 38F MON EXST JC-38-JBF-4/NOZ

73 PIJC-38-6-1 JC-38-6-1 PRESS ES-0153-:M36 TBO MON NEW/NOZ 248 PIJC-38-7-1 JC-38-7-1 PRESS ES-0153-M38 TBD MON NEW/NOZ 236

c.... PIJC-38-7-2 JC-38-7-2 PRESS H-2-35338-2 IP 38F MON NEW JC-38-38F-3/NOZ I 62 ,_..

PIJGV-11-2-1 JGV-11-2-1 PRESS ES-0153-M32 ,_.. TBD MON NEW/NOZ 29 PIJGV-11-2-2 JGV-11-2-2 PRESS ES-0153-M32 TBO MON NEW/NOZ 12 PIJGV- 12-1-3 JGV-12-1-3 PRESS ES-0153-M32 TBD MON NEW/NOZ 76

I PIJGV-25C-1 JGV-25-1 PRESS H-2-35325-1 IP 25C MON EXST/NOZ 12 PIJGV-250-1 JGV-25-2 PRESS H-2-35325-2 IP 250 MON EXST/NOZ 34 PIJGV-35-2-7 JGV-35-2-1 PRESS ES-0153-M33 TBO MON NEW/NOZ 227 ::E:

I PIJGV-35-35B-3 JGV-35-2-4 PRESS H-2-35335-1 IP 35B MON EXST/NOZ 12 n

I PIJGV-35-35C-2 JGV-35-2-3 PRESS H-2-35335-2 IP 35C MON EXST/NOZ 3 Vl

C, PIJGV-35-35C-3 JGV-35-1-1 PRESS H-2-35335-2 IP 35C MON EXST/NOZ 22 I

PIJGV-36-1-2 JGV-36-1-2 PRESS ES-0153-M33 TBO MON NEW/NOZ 67 ::E: ,_.. PIJGV-36-3-2 JGV-36-3-2 PRESS ES-0153-M33 TBO MON NEW/NOZ 202 lT1

w PIJGV-36-36A-1 JGV-36-1-1 PRESS H-2-35336-1 IP 36A MON EXST/NOZ 78 I

n PIJGV-36-36B-1 JGV-36-2 PRESS H-2-35336-2 IP 36B MON EXST/NOZ 54 C,

;:o PIJGV-36-36C-1 JGV-36-3-1 PRESS H-2-35336-3 IP 36C MON NEW/NOZ 45 I

0 POV-11-2-1 FROM 244AR ON/OFF ES-0153-M32 CELL 11 EV-11-2-1 NEW/NOZ 5 0

~

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0

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TABLE I - NEW I/0

MONITOR/ INTERLOCK/

INSTRUMENT DESCRIPTION P&ID DWG LOCATION CONTROL REMARKS

I

POV-11-2-2 BACKFLUSH ON/OFF ES-0153-M32 CELL 11 EV-11-2-2 NEW/NOZ 5 .I

POV-11-2-3 TO TK-11-2 ON/OFF ES-0153-M32 CELL 11 EV-11-2-3 NEW/Noz · 5 I

POV-38-2,__2 TK-38-1 to TK-38-2 ES-0153-M39 CELL 38 EV-38-2-2 NEW/NOZ 219 XFR

POV-38-3-4 TK-38-1 to TK-38-3 ES-0153-M40 CELL 38 EV-38-3-4 NEW/NOZ 219 XFR

POV-38-4-1 TK-38-4 REWORK ES-0153-M34 CELL 38 EV-38-4-1 NEW/NOZ 216

POV-38-5-1 F-38-1 SOLIDS OUT ES-0153-M36 CELL 38 EV-38-5-1 NEW/NOZ 221

POV-38-6-1 NON TRU TO CELL 25 ES-0153-M3_7 CELL 38 EV-38-6-1 NEW/NOZ 248

SGR-11-2-1 TK-11-2 DENSITY H-2-35311-2 IP 6 II Y II NA EXST/NOZ 38

SGR-35-1-1 TK-35-1 DENSITY H-2-35335-1 IP 35B SGT-35-1-1 EXST/NOZ 23

SGR-35-2-1 TK-35-2 DENSITY H-3-35335-2 IP 35D SGT-35-2-1 EXST/NOZ 38

SGR-36-1-1 TK-36-1 DENSITY H-2-35336-1 IP 36A SGT-36-1-1 EXST/NOZ 65 c__, SGR-36-2-1 TK-36-2 DENSITY H-2-35336-2 IP 36B SGT-36-2-1 EXST/NOZ 62 I SGR-36-3-1 TK-36-3 DENSITY H-2-35336-3 TBD SGT-36- 3- 1 EXST/NOZ 80

........ N SGR-39-1-1 TK-39-1 DENSITY H-2-35339-1 IP 39A SGT-39-1-1 EXST/NOZ 23

SGT-11-2-1 TK-11-2 DENSITY ES-0153-M32 XMTRR 11 DACS EXST/NOZ 38

SGT-25-1 TK-25-1 DENSITY H-2-35325-1 XMTRR 25 FPMCS EXST/NOZ 20

SGT-25-2 TK-25-2 DENSITY H-2-35325-2 XMTRR 25 FPMCS EXST/NOZ 38

SGT-35-1-1 TK-35-1 DENSITY ES-0153-M33 XMTRR 35 DACS NEW/NOZ 23 ~

SGT-35-1-1 TK-35-1 DENSITY H-2-35335-1 XMTRR 35 SGR-35-1-1 EXST/NOZ 23 I ("")

SGT-35-2-1 TK-35-2 DENSITY H-2-35335-2 XMTRR 35 SGR-35-2-1 EXST/NOZ 38 I Vl

SGT-35-2-1 TK-35-2 DENSITY ES-0153-M33 TBD DACS NEW/NOZ 62 c:::, I

SGT-36-1-1 TK-36-1 DENSITY ES-0153-M32 XMTRR 36 DACS NEW/NOZ 65 ~ ........

SGT-36-2-1 TK-36-2 DENSITY ES-0153-M33 XMTRR 36 DACS NEW/NOZ 223 U1

SGT-36-3-1 TK-36-3 DENSITY ES-0153-M33 TBD DACS NEW/NOZ 80 w I

SGT-38-1-1 TK-38-1 DENSITY ES-0153-M35 XMTRR 38 DACS NEW/NOZ 229 n c:::,

SGT-38-2-1 TK-38-2 DENSITY ES-0153-M39 XMTRR 38 DACS NEW/NOZ 214 ;:o I

SGT-38-3-1 TK-38-3 DENSITY ES-0153-M40 XMTRR 38 DACS NEW/NOZ 80 0 0

SGT:...38-4-1 TK-38-4 DENSITY ES-0153-M34 XMTRR 38 DACS NEW/NOZ 239 _,

;:o 11)

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Page No. 11 09/06/90

TABLE I - NEW I/0

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INSTRUMENT DESCRIPTION P&ID DWG LOCATION CONTROL REMARKS

SGT-38-5-1 TK-38-5 DENSITY ES-0153-M36 TBD DACS NEW/NOZ 242 SGT-38-6-1 TK-38-6 DENSITY ES-0153-M37 XMTRR 38 DACS NEW/NOZ 249 SGT-38-7-1 TK-38-7 DENSITY ES-0153-M38 TBD DACS NEW/NOZ 213 SGT-39-1-1 TK-39-1 DENSITY ES-0153-M39 XMTRR 39 DACS NEW/NOZ 23 SGT-39-1-1 TK-39-1 DENSITY H-2-35339-1 XMTRR 39 SGR-39-1-1 EXST/NOZ 23 TE-11-2-1 TK-11-2 TEMP H-2-35311-2 TK-11-2 TR 11 EXST/NOZ 35 TE-11-2-2 TK-11-2 TEMP H-2-35311-2 TK-11-2 TR 11 EXST/NOZ 35 TE-25-1-1 TK-25-1 TEMP H-2-35325-1 TK-25-1 FPMCS EXST/NOZ 17 TE-25-2-1 TK-25-1 TEMP H-2-35325-2 TK-25-2 FPMCS EXST/NOZ 8 TE-35-1-1 TK-35-1 TEMP H-2-35335-1 TK-35-1 TR 35 EXST NO JMPR/NEW NOZ

27 TE-35-2-1 TK-35-2 TEMP H-2-35335-2 TK-35-2 TR 35 EXST/NOZ 35 TE-36-1-1 TK-36-1-TEMP H-2-35336-1 TK-36-1 TR 36 EXST/NOZ 69

L TE-36-2-1 TK-36-2 TEMP H-2-35336-2 TK-36-2 TR 36 EXST/NOZ 59 I TE-36-3-1 TK- 36-3 TEMP H-2-35336-3 TK-36-3 DACS EXST/NOZ 51 .......

w TE-38-1 TK-38-1 TEMP ES-0153-M35 TK-38-1 DACS NEW/NOZ 59 TE-38-2 TK-38-2 TEMP ES-0153-M39 TK-38-2 DACS NEW/NOZ 44 TE-38-3 TK-38-3 TEMP ES-0153-M40 TK-38-3 DACS NEW/NOZ 77 TE-38-6 TK-38-6-1 TEMP ES-0153-M37 TK-38-6 DACS NEW/NOZ 45

~ TE-38-7 TK-38-7 TEMP ES-0153-M38 CELL 38 DACS NEW/NOZ 51 :r TE-39-1-1 TK-39-1 TEMP H-2-35339-1 TK-39-1 TR 39 EXST/NOZ 26 n

I

TE-E-38-1 E-38-1 OUT TEMP · ES-0153-M38 CELL 38 DACS NEW/NOZ 51 (./')

0

TR-36-1 TK-36-1 TEMP H-2-60640-1 IP 36A TE-36-1-1 _EXST/NOZ 69 I ~

TR-36-2 TK-36-2 TEMP H-2-60640-1· IP 36B TE-36-2-1 EXST/NOZ 59 ...... U"I

TR-36-3 TK-36-3 TEMP H-2-35336-3 TBD TE-36-3-1 EXST/NOZ 51 w I

WFA-38-0-1 CELL 38 SUMP LEVEL AL H-2-35338-6 IP 38D WFAS-38-0-1 EXST/NOZ 208 n WFA-39-0-1 CELL 39 SUMP LEVEL AL H-2-35339-1 IP 39C WFAS-39-0-1 EXST/NOZ 203 0

:;o

WFAS-35-1-1 TK-35-1 LEVEL AL SW H-2-35335-1 OPR GALL WFA-35-1-1 EXST/NOZ 23 I 0

WFAS-38-0-1 CELL 38 SUMP AL SW H-2-35338-6 XMTRR 38 WFA-38-0-1 EXST/NOZ 208 0 _, WFAS-39-0-1 CELL 39 SUMP AL SW H-2-35339-1 XMTRR 39 WFA-39-0-1 EXST/NOZ 203 :;o

l'P < . 0

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Page No. 12 09/06/90

TABLE I - NEW I /0

MONITOR/ INTERLOCK/

INSTRUMENT DESCRIPTION P&ID DWG LOCATION CONTROL REMARKS

WFI-38-SUMP CELL 38 SUMP LEVEL H-2-35338-6 IP 38F WFT-38-0-1 EXST/NOZ 208 WFI-39-SUMP CELL 38 SUMP LEVEL H-2-35339 .:.. 1 IP 39C WFT-39-0-1 EXST/NOZ 203 WFR-11-2-1 TK-11-2 LEVEL H-2-35311-2 IP 6 II y II WFI-11-2-1 EXST/NOZ 38 WFR-35-1-1 TK-35-1 LEVEL H-2-35335-1 IP 35B WFT-35-1-1 EXST/NOZ 23 WFR-35-2-1 TK-35-2 LEVEL ES-0153-M33 IP 35D WFT-35-2-1 EXST/NOZ 38 WFR-36-1-1 TK-36-1 LEVEL H-2-35336-1 IP 36A WFT-36-1-1 EXST/NOZ 65 WFR-36-2-1 TK-36-2 LEVEL H-2-35336-2 IP 36A WFT-36-2-1 EXSTML/NOZ 62 WFR-36-3-1 TK-36-3 LEVEL H-2-35336-3 TBD WFT-36-3-1 EXST/NOZ 80 WFR-39-1-1 TK-39-1 LEVEL H-2-35339-1 IP 39A WFT-39-1-1 EXST/NOZ 23 WFT-25-1 TK-25-1 LEVEL H-2-35325-1 XMTRR 25 FPMCS EXST/NOZ 20 WFT-25-2 TK-25-2 LEVEL H-2-35325-2 XMTRR ·25 FPMCS EXST/NOZ 38 WFT-35-1-1 TK-35-1 LEVEL ES-0153-M33 XMTRR 35 DACS NEW/NOZ 23

c..... WFT-35-1-1 TK-35-1 LEVEL H-2-35335-1 XMTRR 35 WFR-35-1-1 EXST/NOZ 23 I WFT-35-2-1 TK-35-2 LEVEL H-2-35335-2 XMTRR 35 WFR-35-2-1 EXST/NOZ 38

t-' +::. WFT-35-2-1 TK-35-2 LEVEL ES-0153-M33 TBD DACS NEW/NOZ 38

WFT-36-1-1 TK-36-1 LEVEL ES-0153-M33 XMTRR 36 DACS NEW/NOZ 65 WFT-36-2-1 TK-36-2 LEVEL ES-0153-M33 XMTRR 36 DACS NEW/NOZ 62 WFT-36-3-1 TK-36-3 LEVEL ES-0153-M33 TBD DACS NEW/NOZ 80 WFT-38-0-1 CELL 38 SUMP LEVEL H-2-35338-6 XMTRR 38 WFI-38-0-1 EXST/NOZ 208 WFT-38-1-1 TK-38-1 LEVEL ES-0153-M35 XMTRR 38 DACS NEW/NOZ 229 WFT-38-2-1 TK-38-2 LEVEL ES-0153-M39 XMTRR 38 DACS NEW/NOZ 214 ~

::I:

WFT-38-3-1 TK-38-3 LEVEL ES-0153-M40 XMTRR 38 DACS NEW/NOZ 80 n I

WFT-38-4-1 TK-38-4 LEVEL ES-0153-M34 XMTRR 38 DACS NEW/NOZ 239 (/)

0 WFT-38-5-1 TK-38-5 LEVEL ES-0153-M36 TBD DACS NEW/NOZ 242 I

~ WFT-38-6-1 TK-38-6 LEVEL ES-0153-M37 XMTRR 38 DACS NEW/NOZ 249 .......

u, WFT-38-7-1 TK-38-7 LEVEL ES-0153-M38 TBD DACS NEW/NOZ 213 w WFT-39-0-1 CELL 39 SUMP H-2-35339-1 XMTRR 39 WFI-39-0-1 EXST/NOZ 203 I

n WFT-39-1-1 TK-39-1 LEVEL ES-0153-M39 XMTRR 39 DACS NEW/NOZ 23 0

;o I

0 0 _,

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TABLE II - NEW I/0

MONITOR/ INTERLOCK/

INSTRUMENT DESCRIPTION P&ID LOCATION CONTROL REMARKS

DPI-1-18 CELL B PRESS H-2-94501-2 TBD NA DML/NOZ 12 DPI-1-19 CELL C PRESS H-2-94502-2 TBD NA DML/NOZ 1 DPT-B-0-1 CELL B PRESS ES-0153-M44 TBD DACS NEW/NOZ 12 DPT-B-1-1 TK-B-1 PRESS ES-0153-M42 IP Bl DACS NEW/NOZ 8,

DPT-B-2-1 TK-B-2 PRESS ES-0153-M44 TBD DACS NEW/NOZ TBD DPT-B-3-1 TK-B-3 PRESS ES-0153-M46 IP Bl DACS NEW/NOZ TBD DPT-B-5-1 TK-B-5 PRESS ES-0153-M43 TBD DACS NEW/NOZ 16 DPT-C-0-1 CELL C PRESS H-2-94502-2 TBD DACS NEW/NOZ 1 DPT-C-1-1 TK-C-1 PRESS ES-0153-M49 TBD DACS NEW/NOZ TBD DPT-C-2-1 TK-C-2 PRESS ES-0153-M51 TBD DACS NEW/NOZ TBD DPT-C-3-1 TK-C-3 PRESS ES-0153-M48 TBD DACS NEW/NOZ TBD FE-B-1 TRU FEED FLOW ES-0153-M45 CELL B FT-B-3 NEW/NOZ TBD

c... FE-B-2 SOLVENT FEED FLOW ES-0153-M45 CELL B FT-B-4 NEW/NOZ TBD I FT-B-1 TRU FEED FLOW ES-0153-M45 TBD DACS NEW/NOZ TBD ,_..

LTl FT-B-2 SOLVENT IN FLOW ES-0153-M45 TBD DACS NEW/NOZ TBD FT-B-3 SCRUB #1 FEED FLOW ES-0153-M45 TBD DACS NEW/NOZ TBD FT-B-4 SCRUB #2 FEED FLOW ES-0153-M45 TBD DACS NEW/NOZ TBD FT-B-5 STRIP FEED FLOW ES-0153-M45 TBD DACS NEW/NOZ TBD FT-C-1 HN03 IN FLOW ES-0153-M50 CELL C DACS NEW/NOZ TBD FT-C-2 C03 IN FLOW ES-0153-M50 CELL C DACS NEW/NOZ TBD ::i:

:c

FT-C-3 SOLVENT CLEAN FLOW . ES-0153-MSO CELL C DACS NEW/NOZ TBD n I

HS-B-1 CONTACTOR 1 CONT ES-Ol53-M45 DACS CONT NEW l/l c:,

HS-B-10 CONTACTOR 10 CONT ES-0153-M45 DACS CONT NEW I

HS- B-11 CONTACTOR 11 CONT ES-0153-M45 DACS CONT NEW ~ ,_..

HS-B-12 CONTACTOR 12 CONT ES-0153-M45 DACS CONT NEW u, w

HS-B-13 CONTACTOR 13 CONT ES-0153-M45 DACS CONT NEW I n

HS-B-14 CONTACTOR 14 CONT ES-0153-M45 DACS CONT NEW c:, ;::o

HS-B-15 CONTACTOR 15 CONT ES-0153-M45 DACS CONT NEW I 0

HS-B-16 CONTACTOR 16 CONT ES-0153-M45 DACS CONT · NEW 0

ES-0153-M45 DACS CONT _,

HS-B-2 CONTACTOR 2 CONT NEW ;::o l'l)

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0

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Page No. 2 09/14/90

TABLE II - NEW I/0

MONITOR/ INTERLOCK/

INSTRUMENT DESCRIPTION P&ID LOCATION CONTROL REMARKS

HS-B-3 CONT ACTOR 3 CONT ES-0153-M45 DACS CONT NEW HS-B-4 CONT ACTOR 4 CONT ES-0153-M45 DACS CONT NEW HS-B-5 CONT ACTOR 5 CONT ES-0153-M45 DACS CONT NEW HS-B-6 CONT ACTOR 6 CONT ES-0153-M45 DACS CONT NEW HS-B-7 CONT ACTOR 7 CONT ES-0153-M45 DACS CONT NEW HS-B-8 CONTACTOR 8 CONT ES-0153-M45 DACS CONT NEW HS-B-9 CONTACTOR 9 CONT ES-0153-M45 DACS CONT NEW HS-MOV-B-1 MOV-B-1 HND SW ES-0153-M45 DACS CONT NEW/NOZ TBD HS-MOV-B-2 MOV-B-2 HND SW ES-0153-M45 DACS CONT NEW/NOZ TBD HS-MOV-C-1 MOV-C-1 CONT ES-0153-MSO DACS CONT NEW HS-MOV-C-2 MOV-C2 HND SW ES-0153-M50 DACS CONT NEW HS-MOV-C-3 MOV-C3 HND SW ES-0153-M50 DACS CONT NEW HS-MP-1 MP-B-1 HND SW ES-0153-M48 DACS CONT NEW

c..., HS-MP-2 MP-B-2 HND SW ES-1053-M47 DACS CONT NEW I

HS-MP-3 MP-B-3 HND SW ES-0153-M49 DACS CONT NEW ....... 0) HS-MP-4 MP-B- 4 HND SW ES-0153-M49 DACS CONT NEW

HS-MP-5 MP-B-5 HND SW ES-0153-M51 DACS CONT NEW HS-P-B-1 PUMP B-1 HND SW ES-0153-M45 DACS CONT NEW ~

HS-P-B-2 PUMP B-2 HND SW ES-0153-M45 DACS CONT NEW :r n

HS-P-B-3 PUMP B-3 HND SW ES-0153-M45 DACS CONT NEW I (./l

HS-P-B-4 PUMP B-4 HND SW ES-0153-M46 DACS CONT NEW CJ I

HS-P-C-1 PUMP C-1 HND SW ES-1053-M47 DACS CONT NEW ~ I-'

HS-P-C-2 PUMP C-2 HND SW ES-0153-M49 DACS CONT NEW lTl

HS-P-C-3 PUMP C-3 HND SW ES-0153-M49 DACS CONT NEW w I

HS-P-C-4 PUMP C-4 HND SW ES-0153-M50 DACS CONT NEW n CJ

HS-P-C-5 PUMP C-5 HND SW ES-0153-M51 DACS CONT NEW ;:o I

J-B2-1 TK-B-2 TRU FEED ES-0153-M44 CELL B JGV-B2-1 EXST/NOZ 37 0 0

J-B5-1 TRU FEED TO TK-B-1 ES-0153-M43 CELL B JGV-B5-1 NEW/NOZ TBD __,

J-EB-1 CNDSR EB-1 OUTLET ES-0153-M46 TBD JGV-EB-1 NEW/NOZ TBD ;:o 11)

J-EC-1 CNDSR EC-1 OUTLET ES-0153-M48 TBD JGV-EC-1 NEW/NOZ TBD < . 0

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TABLE II - NEW I/0

MONITOR/ INTERLOCK/

INSTRUMENT DESCRIPTION P&ID LOCATION CONTROL REMARKS

JC-B2-1 JGV-B2-1 CONT H-2-94501-2 TBD JGV-B2-1 EXST/NOZ 37 JC-B5-1 JGV-B5-1 CONT ES-0153-M43 TBD JGV-05-1 NEW/NOZ TBD JC-EB-1 JGV-EB-1 CONT ES-0153-M46 TBD J-EB-1 NEW/NOZ TBD JC-EC-1 JGV-EC-1 CONT ES-0153-M48 TBD J-EC-1 NEW/NOZ TBD JGV-B2-lA J-B2-1 CONT H-2-94501-2 CELL B J-B2-1 EXST/NOZ 37 JGV-B2-1B J-B2-1 CONT H-2-94501-2 TBD J-B2-1 EXST/NOZ 37 JGV-B2-lC J-B2-1 CONT H-2-94501-2 TBD J-B2-1 EXST/NOZ 37 JGV-B5-lA J-B5-1 CONT ES-0153-M43 TBD J-B5-1 NEW/NOZ TBD JGV-B5-1B J-B5-1 CONT ES-0153-M43 TBD J-B5-1 NEW/NOZ TBD JGV-B5-lC J-B5-1 CONT ES-0153-M43 TBD J-B5-1 NEW/NOZ TBD JGV-EB-1 J-EB-1 CONT ES-0153-M46 TBD J-EB-1 NEW/NOZ TBD JGV-EC-1 J-EC-1 CONT ES-0153-M48 TBD J-EC-1 NEW/NOZ TBD LE-SUMP-B CELL BLEAK DET H-2-94501-1 CELL B DACS EXST/NOZ 22 LE-SUMP-C CELL C LEAK DET H-2-94502-1 CELL C DACS EXST/NOZ 41

c.... LS-B-1 CONTACTOR 1 LEVEL ES-0153-M45 CELL B DACS NEW/NOZ TBD I ...... LS-B-10 CONTACTOR 10 LEVEL ES-0153-M45 CELL B DACS NEW/NOZ TBD -...J LS-B-11 CONTACTOR 11 LEVEL ES-0153-M45 CELL B DACS NEW/NOZ TBD LS-B-12 CONTACTOR 12 LEVEL ES-0153-M45 CELL B DACS NEW/NOZ TBD LS-B-13 CONTACTOR 13 LEVEL ES-0153-M45 CELL B DACS NEW/NOZ TBD :i;:

LS-B-14 CONTACTOR 14 LEVEL ES-0153-M45 CELL B DACS NEW/NOZ TBD I n

LS-B-15 CONTACTOR 15 LEVEL ES-0153-M45 CELL B DACS NEW/NOZ TBD I (/)

LS-B-16 CONTACTOR 16 LEVEL ES-0153-M45 CELL B DACS NEW/NOZ TBD CJ

LS-B-2 CONTACTOR 2 LEVEL ES-0153-M45 CELL B DACS NEW/NOZ TBD I :i;:

LS-B-3 CONTACTOR 3 LEVEL ES-0153-M45 CELL B DACS NEW/NOZ TBD ...... . lTl

LS-B-4 CONTACTOR 4 LEVEL ES-0153-M45 CELL B DACS NEW/NOZ TBD w I

LS-B-5 CONTACTOR 5 LEVEL ES-0153-M45 CELL B DACS NEW/NOZ TBD n CJ

LS-B-6 CONTACTOR 6 LEVEL ES-0153-M45 CELL B DACS NEW/NOZ TBD ;:o I

LS-B-7 CONTACTOR 7 LEVEL ES-0153-M45 CELL B DACS NEW/NOZ TBD 0

LS-B-8 CONTACTOR 8 LEVEL ES-0153-M45 CELL B DACS NEW/NOZ TBD 0 _,

LS-B-9 CONTACTOR 9 LEVEL ES-0153-M45 CELL B DACS NEW/NOZ TBD ;:o CD < . 0

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TABLE II - NEW I/0

MONITOR/ INTERLOCK/

INSTRUMENT DESCRIPTION P&ID LOCATION CONTROL REMARKS

MC-B2-1 JGV-B2-1 CONT H-2-94501-2 TBD JGV-B2-1 EXST/NOZ 37 MC-B5-1 JGV-B5-1 CONT ES-0153-M43 TBD JGV-B5-1 NEW/NOZ TBD MC-EB-1 JGV-EB-1 CONT ES-Ol53-M46 TBD JGV-EB-1 NEW/NOZ TBD MC-EC-1 JGV-EC-1 CONT ES-0153-M48 TBD JGV-EC-1 NEW/NOZ TBD MOV-B-1 TRU FEED MOV ES-0153-M45 CELL B DACS NEW/NOZ TBD MOV-B-2 SOLVENT FEED MOV ES-0153-M45 CELL B DACS NEW/NOZ TBD MOV-C-1 HN03 SLVT CLN FEED ES-0153-M50 CELL C DACS NEW/NOZ TBD MOV-C-2 C03 SLVT CLN FEED ES-0153-M50 CELL C DACS NEW/NOZ TBD MOV-C-3 USED SLVT FEED ES-0153-M50 CELL C DACS NEW/NOZ TBD MP-B-1 TRU FEED ES-0153-M45 CELL B DACS NEW, FOR REFERENCE MP-B-2 ORGANIC SLVT FEED ES-0153-M45 CELL B DACS NEW, FOR REFERENCE MP-B-3 SCRUB #1 FEED ES-0153-M45 CELL B DACS NEW, FOR REFERENCE MP-B-4 SCRUB #2 FEED ES-0153-M45 CELL B DACS NEW, FOR REFERENCE

c.... MP-B-5 STRIP FEED ES-0153-M45 CELL B DACS NEW, FOR REFERENCE I t-' P-B-1 SLVT RTN TO TK-C-3 ES-0153-M45 CELL B DACS NEW, FOR REFERENCE co

P-B-2 TRU FRAC TO TK-B-3 ES-0153-M45 CELL B DACS NEW, FOR REFERENCE P-B-3 RAFFINATE TO TRU MON ES-0153-M45 CELL B DACS NEW, FOR REFERENCE P-B-4 TK-B-3 DISCH ES-0153-M46 CELL B DACS NEW, FOR REFERENCE P-C-1 TRU MON DISCH ES-1053-M47 CELL B DACS NEW, FOR REFERENCE P-C-2 HN03/C03 MON FEED ES-0153-M49 CELL C DACS NEW, FOR REFERENCE ~

:I: P-C-3 SLVT CLN HN03 RTN ES-0153-M49 CELL C DACS NEW, FOR REFERENCE n

I P-C-4 CLN SLVT TO TK-C-3 ES-0153-M50 CELL C DACS NEW, FOR REFERENCE (/)

0 P-C-5 SLVT CLN C03 RTN ES-0153-M51 CELL C DACS NEW, FOR REFERENCE I

PA-B2-1 JGV-B2-1 ALM SW H-2-94501-2 TBD PAS-B2-1 EXST/NOZ 37 ~ ~

PA-B5-1 JGV-B5-1 PRESS ALM ES-0153-M43 TBD PAS-B5-1 NEW/ NOZ TBD 01 w

PAS-B2-1 JGV-B2-1 PRESS ALM H-2-94501-2 TBD PA-B2-1 EXST/NOZ 37 I n

PAS-B5-1 JGV-B5-1 ALM SW ES-0153-M43 TBD PA-B5-1 NEW/NOZ TBD 0 :;o

PI-B1-1 TK-B-1 PRESS H-2-94501-1 IP Bl NA DML/NOZ 8 I 0

PI-B2-1 TK-B-2 PRESS H-2-94501-2 CELL B NA DML/NOZ 37 0 __, PI-B5-1 TK-B-5 PRESS H-2-94501-1 IP Bl NA DML/NOZ 16

:;o Cl)

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TABLE II - NEW I/0

MONITOR/ INTERLOCK/

INSTRUMENT DESCRIPTION P&ID LOCATION CONTROL REMARKS

PIJC-B2-1 JGV-B2-1 PRESS H-2-94501-2 TBD JGV-B2-1 EXST PI-B2-1/NOZ 37

PIJC-B5-1 JGV-B5-1 PRESS ES-0153-M43 TBD JGV-B5-1 NEW/NOZ TBD PIJC-EB-1 JGV-EB-1 PRESS ES-0153-M46 TBD JGV-EB-1 NEW/NOZ TBD PIJC-EC-1 JGV-EC-1 PRESS ES-0.153-M48 TBD JGV-EC-1 NEW/NOZ TBD PT-B1-1 TK-B-1 PRESS H-2-94501-1 TBD NA DML/NOZ 8 PT-B5-1 TK-B-5 PRESS H-2-94501-1 TBD NA DML/NOZ 16 SGR-B-1-1 TK-B-1 DENSITY H-2-94501-1 TBD SGT-B-1-1 DML SGR-B-5-1 TK-B-5 DENSITY H-2-94501 - 1 IP Bl SGT-B-5-1 DML SGT-B-1-1 TK-B-1 DENSITY H-2-94501-1 IP Bl NA DML/NOZ 9, 10

SGT-B-1-1 TK-B-1 DENSITY ES-0153-M43 TBD DACS NEW/NOZ 9, 10

SGT-B-2-1 TK-B-2 DENSITY ES-0153-M44 TBD DACS NEW/NOZ TBD SGT-B-3-1 TK-B-3 DENSITY ES-0153-M46 TBD DACS NEW/NOZ TBD SGT-B-5-1 TK-B-5 DENSITY H-2-94501-1 TBD NA DML/NOZ 17, 18

c..., SGT-B-5-1 TK-B-5 DENSITY ES-0153-M43 TBD DACS NEW/NOZ 17, 18 I

....... SGT-C-1-1 TK-C-1 DENSITY ES-0153-M49 TBD DACS NEW/NOZ TBD \.0

SGT-C-2-1 TK-C-2 DENSITY ES-0153-M51 TBD DACS NEW/NOZ TBD

SGT-C-3-1 TK-C-3 DENSITY ES-0153-M48 TBD DACS NEW/NOZ TBD TE-B1-1 TK-B-1 TEMP H-2-94501-1 TK-B-1 DACS EXST/NOZ 7A TE-B2-1 TK-B-2 TEMP H-2-94501-1 TK-B-2 DACS EXST/NOZ 70 TE-B3-1 TK-B-3 TEMP ES-0153-M46 TK-B-3 DACS NEW/NOZ TBD ~

:c

TE-B5-1 TK-B-5 TEMP H-2-94501-1 TK-B-5 DACS EXST/NOZ 100A n I

WFR-B1-1 TK-B-1 LEVEL H-2-94501-1 IP Bl WFR-B1-1 DML/NOZ 8, 9 V)

0

WFR-B5-1 TK-B-5 LEVEL H-2-9450;1.-1 IP Bl WFR-B5-1 DML/NOZ 16, 17 I ~

WFT-B-1-1 TK-B-1 LEVEL H-2-94501-1 TBD NA DML/NOZ 8, 9 .......

WFT-B-1-1 TK-B-1 LEVEL ES-0153-M42 TBD DACS NEW/NOZ 8, 9 l1l w

WFT-B-2-1 TK-B-2 LEVEL ES-0153-M44 TBD DACS NEW/NOZ TBD I n

WFT-B-3-1 TK-B-3 LEVEL ES-0153-M46 TBD DACS NEW/NOZ TBD 0 ;o

WFT-B-5-1 TK-B-1 LEVEL H-2-94501-1 TBD NA DML/NOZ 16, 17 I 0

WFT-B-5-1 TK-B-3 LEVEL ES-0153-M43 TBD DACS NEW/NOZ 16, 17 0 -J

WFT-C-1-1 TK-C-1 LEVEL ES-0153-M49 TBD DACS NEW/NOZ TBD ;o ro < . 0

- -- ------ - - ----- - - -

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Page No. 6 09/14/90

INSTRUMENT

WFT-C-2-1 WFT-C-3-1

DESCRIPTION

TK-C-2 LEVEL TK-C-3 LEVEL

~ '. : ... \

TABLE II - NEW I/0

MONITOR/ INTERLOCK/

P&ID LOCATION CONTROL

ES-0153-M52 TBD DACS ES-0153-M48 TBD DACS

REMARKS

NEW/NOZ TBD NEW/NOZ TBD

~ :i: n I

(./) C, I ~ ~ U1 w I

n C, ;::o I

0 0 __,

;::o It)

< . 0

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WHC -SD-Wl53 -CDR-001 Rev . 0

APPENDIX K

Equipment Data Sheets

'• , ._ .·

'-. ·'

Page 111: -I-Cl l

FILTRATE TANK (TK-38-4} Required Volume: Shell Material: Head Material: Wall Thickness: Head Thickness: Tank Height: Tank Width: Tank Length: Corrosion Allowance: Design Temperature: Design Pressure:

WHC -SD-Wl53-CDR-001 Rev . 0

221-B Building, 200 EAST AREA Equipment List

650 ga 1 304L SST 304L SST . 1875 in. .1875 in . 72 in. 48 in . 60 in. .06 in. 10o•F

5 psig

K-1

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WHC-SD -Wl53 -CDR-001 Rev. 0

221-B Building, 200 EAST AREA Equipment List

PROCESS PARAMETERS (TK-38-4)

Maximum Process Temperature: Specific Gravity of Process: Viscosity of Process: Vapor Pressure: Solids Specific Gravity: Characteristics of Solids: _L Soluble

10o•F

1.097 5 Centipoise 1. 5 psi a 2.0

Abrasive Insoluble _L Sticky or Gummy

Pounds of sol\ds/gallon of mixture: Solids Size :

K-2

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WHC -SD -Wl53 -CDR -001 Rev . 0

221-B Building, 200 EAST AREA Equipment List

FILTRATE TANK AGITATOR (A-38-4)

Wetted Parts Material: 304L SST Motor Type: TEFC Type of Mounting: Remote Flange Connection Size: 8 in Type of Seal: Mechanical Type of Agitation: Mixing Design Temperature: 10o•F Corrosion Allowance: . 06 in hp: 1. 75 Speed: 350 - 400 rpm

Note: For process parameters, see page K-2

K-3

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t.-.,- '' \,._.-

WHC -SD -Wl53 -CDR-001 Rev. 0

221-B Building, 200 EAST AREA Equipment List

DISSOLVER TANK (TK-38-1) {Typical for 3)

Required Volume: She 11 Material : Head Material: Wall Thickness: Head Thickness: Tank Height: Tank Width: Tank Length: Corrosion Allowance: Design Temperature: Design Pressure:

650 gal 304L SST 304L SST .250 in .250 in 72 in. 48 in. 60 i n . . 125 in 10o•F

5 psig

K-4

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(

· ........ ·

WHC -SD-W153 -CDR-001 Rev . 0

221-B Building, 200 EAST AREA Equipment List

TK-38-1 PROCESS PARAMETERS

Maximum Process Temperature: Specific Gravity of Process: Viscosity· of the Process: Vapor Pressure: Solids Specific Gravity: Characteristics of Solids: _x_ Soluble

10o•F

1.098 15 Centipoise 1. 5 psi a 2.00

Abrasive Insoluble .L Sticky or Gummy

Pounds of Solids/Gallon of Mixture: TBD Solids Size: TBD

K-5

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WHC -SD -Wl53 -CDR-001 Rev. 0

221-8 Building, 200 EAST AREA Equipment List

DISSOLVER TANK AGITATOR (A -38- 1)

Wetting Parts Material : Motor Type: Type of Mounting: Connection Size: Type of Seal: Type of Agitation: Design Temperature: Corrosion Allowance: hp: Speed:

304L SST TEFC Remote Flange 8 in Mechanical Mixing/Suspension of Solids 10o•F

. 06 in 2.5

350 - 400 rpm

Note: For process parameters, see page K-5.

K-6

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\

WHC -SO -Wl53 -COR-001 Rev . 0

221-B Building, 200 EAST AREA Equipment Li st

DISSOLVER TANK TRANSFER PUMP (P -38- 1}

Required Flow Rate: Specific Gravity of Process: Viscosity of Process: Vapor Pressure of Process : Total Dynamic Head: Type of Flow: _x_ Newtonian

Non-Newtonian Corrosion Allowance:

5 gpm See Process See Process See Process 60 ft of H20

. 06 in

Parameters Parameters Parameters

Type of Mounting : Remote Flange Motor Type: TEFC hp: 1/3 Speed: 1770 Voltage: 115 V

Note: for process parameters see page K-5.

K-7

(Sh K-5) (Sh K-5) (Sh K-5)

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WHC -SD-Wl53 -CDR -001 Rev. 0

221-B Building, 200 EAST AREA

DISSOLVER TANK COOLING COIL:

Required Heat Transfer Rate: Cooling Water Temperature In: Cooling Water Temperature Out: Cooling Coil Line Size: Cooling Coil Diameter: Cooling Water Flow Rate:

Cooling Coil Material:

Equipment List

TBD 75°F

as·F l in. sch 80 S pipe 42 in TBO

304 L SST

K-8

Page 119: -I-Cl l

I t .

tqui pment Li st

DISSOLVER TANK FILTER (F-38- 1}

Filter Rating: Filter Flow Rate: Filter Type: Design Pressure: Design Temperature: Design Pressure Drop:

5 Micron 2 gpm max Cartridge 20 psig (Filter housing) 10o•F

5 psig max

Note: For process parameters, see page K-5.

K-9

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r _._ ..... _ I • '-- ··

SOLIDS TANK (TK-38-5)

Required Volume : She 11 M.a teri al : Head Material: Wa 11 Thickness: Head Thickness: Tank Height: Tank Diameter: Corrosion Allowance: Design Temperature: Design Pressure:

WHC -SD-Wl53 -CDR -00 1 Rev . 0

221-B Building, 200 EAST AREA Equipment List

225 gal 304L SST 304L SST . 1875 in . 1875 in 78 in . 30 in. .06 in 10o•F

5 psig

K-10

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221-B Building, 200 EAST AREA Equipment Li st

TK-38-5 PROCESS PARAMETERS

Maximum Process Temperature: Specific Gravity of Process: Viscosity of the Process: Vapor Pressure: Solids Specific Gravity: Characteristics of Solids:

_x_ Soluble

10o•F

1.2 (after dissolution) 15 centipoise 1. 5 psi a 2.00

Abrasive Insoluble _X_ Sticky or Gummy

Pounds of Solids/Gallon of Mixture: TBD Solids Size: TBO

K-11

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221-8 Building, 200 EAST AREA

Equipment List

SOLIDS TANK AGITATOR (A-38-5}

Wetted Parts Material : Motor Type: Type of Mounting: Connection Size: Type of Seal: Type of Agitation: Design Temperature: Corrosion Allowance: hp: Speed:

304L SST TEFC Remote Flange 8 in Mechanical Dissolution 1oo·F . 06 in 2.5 350 - 400 rpm

Note: For process parameters, see page K-11.

K-12

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RAFFINATE TANK (TK-38-6)

Required Volume: Shell Material: Head Material: Wall Thickness: Head Thickness: Tank Height: Tank Diameter: Corrosion Allowance: Design Temperature: Design Pressure:

( '

\

WHC -SD -Wl53 -C0R-001 Rev . 0

221-B Building, 200 EAST AREA Equipment List

225 gal 304L SST 304L SST .1875 in . . 1875 in. 78 in. 30 in. .06 in. 10o•F

5 psig

K-13

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WHC -SO-Wl53-COR-001 Rev. 0

221-B Building, 200 EAST AREA Equipment List

TK-38-6 PROCESS PARAMETERS:

Maximum Process Temperature: Specific Gravity of Process: Viscosity of Process: Vapor Pressure:

10o•F

1.097 5 Centipoise 1. 5 psi a

K- 14

I

I

I I I I I

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WHC -SD -Wl53-CDR-001 Rev . 0

221-B Building, 200 EAST AREA Equipment List

SCRUBBER RECEIVER TANK (TK-38-7}

Required Volume: She 11 Materi a 1 :

Head Material: Wall Thickness: Head Thickness: Tank Height: Tank Width: Tank Length: Corrosion Allowance: Design Temperature: Design Pres.sure:

50 gal 304L SST 304L SST .1875 in. .1875 in. 36 in. 30 in. 42 in. . 08 in. 10o•F

5 psig

K-15

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221-B Building, 200 EAST AREA Equipment List

TK-38-7 PROCESS PARAMETERS

Maximum Procass Temperature : Specific Gravity of Process: Viscosity of Process: Vapor Pressure:

1oo·F 1.00 10 Centipoise 1. 5 psi a

K-16

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.,·-,._

. -·:--

NOx Column (TK-38-8)

WHC -SD -W153 -CDR-001 Rev. 0

221-B Building, 200 EAST AREA Equipment List

Design C02/NOx Flow Rate: TBD Column Type: Scrub Water Flow Rate: Air Bleed Flow Rate: She 11 Materi a 1 : Head Material: Wa 11 Thickness: Head Thickness: Column Height: Column Diameter: Corrosion Allowance: Design Temperature: Design Pressure: Design Vacuum:

Packed Bed Absorber TBD TBD 304L SST

304L SST . 1875 in. .1875 in. TBD TBD . 06 in. 10o•F

5 psig 28 in. WC= .49 in hg

K-17

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WHC-SD -Wl 53 -COR-001 Rev . 0

221-B Building, 200 EAST AREA Equipment List

NOx COLUMN DEMISTER (0-38- 1)

Required Liquid Volume (Below Demister Pad): Shell Material : 304L SST Head Material: 304L SST Shell Thickness: .322 in Head Thickness: .322 in Tank Height: 12 in

Tank Diameter: Corrosion Allowance: Design Temperature: Design Pressure: Vapor Flow: Vapor Density: Liquid Density: Liquid Viscosity: Demister Pad Material: Demister Pad Thickness: Demister Pad Manufacturer: Demister Pad Style :

8.63 in . 01 i h.

10o•F

5 psig TBD

TB• 62. 4 l bm/ft3

5 Centipoise 304L SST 4 in. York Co. Inc. Style 431

K-1 8

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221-B Building. 200 EAST AREA Equipment List

DISSOLVER OFFGAS CONDENSER {E -38-1)

Offgas Entering Temperature: Offgas Exit Temperature: Cooling Water Entering Temperature: Cooling Water Exit Temperature : Latent Heat (Process Vapors): Non-Condensables (Process): Process Vapor to be Condenser : Design Temperature: Shell Side: 220°F Design Pressure: Shell Side: 5 psig Shell Material: Tube Material: Baffle Material : Corrosion Allowance:

22o•F go•F

75°F as·F Btu/lbm NOx, CO2 1bm/hr H20 1 bm/hr

Tube Side: 100°F

Tube Side: 100 psig 300 Series SST 300 Series SST 300 Series SST . 01 in.

K- 19

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225-8 Building - 200 EAST AREA

SOLVENT RETURN PUMP (P-B -1)

Required Flow Rate: Specific Gravity of Process Viscosity of Process Vapor Pressure of Process Total Dynamic Head: Type of Flow: -1._ Newtonian

Non-Newtonian Corrosion Allowance : Motor Type:

_. hp: Speed: Voltage:

PROJECT EQUIPMENT LIST

B-CELL

0-20 gph

See Process Parameters (Sh K-21) See Process Parameters (Sh K-21) See Process Parameters (Sh K-21) 8 ft of H20

. 01 in TEFC 1/6

1725 rpm llSV

K-20

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225-B Building - 200 EAST AREA PROJECT EQUIPMENT LIST

B-CELL

SOLVENT RETURN PUMP PROCESS PARAMETERS:

Maximum Solvent Temperature: Specific Gravity of Solvent: Viscosity of Solvent: Vapor Pressure of Solvent:

10o•F

.750 2 Centipoise 1 psia

K-21

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;:: ' . \. ., .

WHC -SD -Wl53 - CDR-001 Rev. 0

225-8 Building - 200 EAST AREA PROJECT EQUIPMENT LIST

TRU FRACTION PUMP (P -8-2)

Requi~ed Flow Rate: Specific Gravity of Process Viscosity of Process Vapor Pressure of Process Total Dynamic Head: Type of Flow: _x_ Newtonian

Non-Newtonian Corrosion Allowance: Motor Type: hp:

Speed: Voltage:

8-CELL

0-20 gph See Process Parameters (Sh K-23) See Process Parameters (Sh K-23) See Process Parameters (Sh K-23) 10 ft H20

.01 in

TEFC

1/6 1725 rpm 115 V

K-22

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225-B Building - 200 EAST AREA PROJECT EQUIPMENT LIST

B-CELL

TRU FRACTION PUMP PROCESS PARAMETERS:

Maximum Process Temperature: Specific Gravity of Process: Viscosity of Process: Vapor Pressure:

10o•F

1.097 5 Centipoise 1. 5 psi a

K- 23

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WHC -SD-Wl53 -CDR-001 Rev . 0

-225-8 Building - 200 EAST AREA

PROJECT EQUIPMENT LIST

CONTACTOR RAFFINATE PUMP (P -8-3}

Required Flow Rate: Specific Gravity of Process: Viscosity of Process: Vapor Pressure of Process: Total Dynamic Head: Type of Flow: _X_ Newtonian

Non-Newtonian Corrosion Allowance: Motor Type: hp: ·Speed: Voltage :

B-CELL

0-20 gph See Process See Process See Process 8 ft H20

.01 in TEFC

1/6

1725 rpm 115 V

K- 24

Parameters Parameters Parameters

(Sh K-25) (Sh K-25) (Sh K-25)

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B-CELL

CONTACTOR RAFFINATE PUMP PROCESS PARAMETERS

Maximum Process Temperature: Specific Gravity of Process: Viscosity of the Process: Vapor Pressure:

. ~------ -

10o•F

1.097 5 Centipoise 1. 5 psi a

K- 25

. I !

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( '

'.

'··

WHC -SD-Wl53 -CDR-001 Rev . 0

225-8 Building - 200 EAST AREA PROJECT EQUIPMENT LIST

B-CELL

SOLVENT RETURN PUMP HEAD TANK (HTK-8-1) (TYP of 6)

Required Volume: 1 gal She 11 Materi a 1 : 304L SST Head Material: 304L SST Wall Thickness: . 237 in. Head Thickness: .237 in. Tank Height: 15 in. Tank Diameter: 4. 50 in. Corrosion Allowance: .01 in. Design Temperature: 100°F Design Pressure : 5 psig

K-26

Page 137: -I-Cl l

STRIP TANK (TK-8-3)

Required Volume:

I She 11 Material :

I. Head Material: Wall Thickness: Head Thickness: Tank H~ight: Tank Diameter: Corrosion Allowance: Design Temperature: Design Pressure:

WHC -SD-Wl53 -CDR-001 Rev . 0

225-B Building - 200 EAST AREA PROJECT EQUIPMENT LIST

B-CELL

15 gal 304L SST 340L SST . 250 in. (Sch 20 pipe) .250 in. (Light weight) 33 in. 12 in. . 06 in. 10o•F

5 psig

K-27

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,..,-: .... I

' \ .. _ .. ·

WHC -SD -Wl53-CDR-001 Rev . 0

225-B Building - 200 EAST AREA PROJECT EQUIPMENT LIST

STRIP TANK PUMP (P-8-4)

Required Flow Rate: Specific Gravity of Process Viscosity of Process Vapor Pressure of Process Total Dynamic Head: Type of Flow: _x_ Newtonian

Non-Newtonian Corrosion Allowance : Motor Type: hp: Speed : Voltage :

8-CELL

0-30 gph See Process See Process See Process 8 ft of H20

. 01 in TEFC 1/6

1725 rpm 115V

K-28

Parameters (Sh K-29) Parameters (Sh K-29) Parameters (Sh K-29)

-- - - - ------

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WHC -SD-Wl53 -CDR-00 1 Rev . 0

225-B Building - 200 EAST AREA PROJECT EQUIPMENT LIST

STRIP TANK PUMP PROCESS PARAMETERS :

Maximum Process Temperature: Specific Gravity of Process: Viscosity of the Process: Vapor Pressure:

B-CELL

10o•F

1.097

5 Centipoise 1. 5 psia

K-29

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225-B Building - 200 EAST AREA PROJECT EQUIPMENT LIST

C-CELL

SOLVENT STORAGE TANK <TK-C-3)

Required Volume: Shell Material: Head Material: Wall Thickness: Head Thickness: Tank Height : Tank Diameter: Corrosion Allowance : Design Temperature : Design Pressure :

15 gal 304L SST 304L SST

. 250 in. (Sch 20 pipe)

.250 in. (Light weight Pipe Cap) 33 in . 12 3/4 in . . 06 in. 10o•F

5 psig

K- 30

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WHC-SD-Wl53 -CDR -00 1 Rev . 0

225- B Building - 200 EAST AREA PROJECT EQUIPMENT LIST

C-CELL C03 STORAGE TANK (TK-C -2) Required Volume: 15 gal

304L SST 304L SST

She 11 Materi a 1 : Head Material: Wall Thickness: Head Thickness: Tank Height: Tank Diameter: Corrosion Allowance: Design Temperature: Design Pressure:

. 250 in. (Sch 20 pipe)

. 250 in. (Light weight) 33 in.

12 3/4 in. .06 in. 10o•F

5 ps ig

K-31

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WHC -SD -Wl53 -CDR -001 Rev . 0

225-B Building - 200 EAST AREA PROJECT EQUIPMENT LIST

C-CELL

TRU MONITOR FEED DISCHARGE PUMP (P-C-1}

Required Flow Rate: Specific Gravity of Process Viscosity of Process Vapor Pressure of Process Total Dynamic Head: Type of Flow : _x_ Newtonian

Non-Newtonian Corrosion Allowance: Motor Type: hp:

Speed: Voltage :

0-20 gpm

See Process Parameters (Sh K-33) See Process Parameters (Sh K-33) See Process Parameters (Sh K-33)

8 ft H20

.01 in TEFC 1/6 1725 rpm 115 V

K-32

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225-B Building - 200 EAST AREA PROJECT EQUIPMENT LIST

PUMP P-C-1 PROCESS PARAMETERS Maximum Process Temperature : Specific Gravity of Process : Viscosity of Process: Vapor Pressure:

C-CELL

K-33

10o•F

1.097 max . 5 Centipoise 1. 5 psi a

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225-B Building - 200 EAST AREA PROJECT EQUIPMENT LIST

HN0~3 STORAGE TANK PUMP (P-C-2) Required 'Flow Rate: Specific Gravity of Process: Viscosity of Process: Vapor Pressure of Process: Total Dynamic Head: Type of Flow: _x_ Newtonian

Non-Newtonian Corrosion Allowance: Motor Type : hp: Speed: Voltage:

C-CELL

K-34

0-20 gph

See Process Parameters (Sh K-35) See Process Parameters (Sh K-35) See Process Parameters (Sh K-35) 8 ft H20

. 01 in TEFC 1/6

1725 rpm 115 V

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C

WHC -SD -W153 -CDR -001 Rev . 0

225-B Building - 200 EAST AREA PROJECT EQUIPMENT LIST

PUMP P-C-2 PROCESS PARAMETERS Maximum Process Temperature: Specific Gravity of Process : Viscosity of Process: Vapor Pressure :

C-CELL

1oo·F 1.20

2 Centipoise 1. O psi a

K-35

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225-B Building - 200 EAST AREA PROJECT EQUIPMENT LIST

HN03/SOLVENT CLEAN-UP PUMP (P-C-3) Required Flow Rate: Specific Gravity of Process : Viscosity of Process: Vapor Pressure of Process: Total Dynamic Head: Type of Flow: _x_ Newtonian

Non-Newtonian Corrosion Allowance: Motor Type: hp: Speed: Voltage:

C-CELL

K-36

0-20 gph

See Process Parameters (Sh K-37) See Process Parameters (Sh K-37) See Process Parameters (Sh K-37) 3 ft OF H20

.01 in TEFC li6

1725 rpm 115 V

- I

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225-B Building - 200 EAST AREA PROJECT EQUIPMENT LIST

PUMP P-C -3 PROCESS PARAMETERS Maximum Process Temperature: Specific Gravity of Process : Vi scosity of Process: Vapor Pr~ssure :

C-CELL

10o•F

1.20 1 Cent i poise 1. O psi a

K- 37

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)

I -

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WHC -SD -Wl53 -CDR -001 Rev . 0

225-B Building - 200 EAST AREA PROJECT EQUIPMENT LIST

SOLVENT CLEAN-UP PUMP (P-C-4} Required Flow Rate: Specific Gravity of Process: Viscosity of Process: Vapor Pressure of Process: Total Dynamic Head: Type of Flow: _x_ Newtonian

Non-Newtonian Corrosion Allowance: Motor Type : hp: Speed : Voltage:

C-CELL

0-20 gph See Process Parameters (Sh K-39) See Process Parameters (Sh K-39) See Process Parameters {Sh K-39) 8 ft H20

. 01 in TEFC 16

1725 rpm 115 V

K- 38

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WHC -SD -W153 -CDR -001 Rev . 0

225-B Building - 200 EAST AREA PROJECT EQUIPMENT LIST .

PUMP P-C-4 PROCESS PARAMETERS Maximum Process Temperature: Specific Gravity of Process : Viscosity or Process : Vapor Pressure :

C-CELL

10o•F

. 750 2 Centipoise 1. O psi a

K-39

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£03/SOLVENT CLEAN-UP PUMP (P -C- 5) Required Flow Rate : Specific Gravity of Process : Vjscosity of Process: Vapor Pressure of Process : Total Dynamic Head: Type of Flow : _x_ Newtonian

Non -Newtonian Corrosion Allowance : Motor Type : hp : Speed: Voltage :

C-CELL

0-20 gph See Process Parameters (Sh K-41) See Process Parameters (Sh K-41) See Process Parameters (Sh K-41)

8 ft H20

. 01 i n TEFC

1/6

1725 rpm 115 V

K-40

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225-B Building - 200 EAST AREA PROJECT EQUIPMENT LIST

PUMP P-C-5 PROCESS PARAMETERS Maximum Process Temperature: Specific Gravity of Process : Viscosity of Process: Vapor Pressure:

C-CELL

10o•F

1. 027 2 Centipoise 1. a ps; a

K-41

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APPENDIX L

Aqueous Makeup Description - 221-B and 225-B Buildings

. ~ .;

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WHC -SD -Wl53 -CDR-001 Rev . 0

AMU DESCRIPTION UPGRADES

221 -B Building AMU

221-B Building AMU is located on the third floor of 271-8. At present, eight tanks (TK-H-309, 310, 311, 312, 313, 314, 315, and 316) are identified to be upgraded by Project W-004 to support Neutralized Current Acid Waste (NCAW) operations. These tanks are located on the west side of the AMU. All tanks are 600 gal.

The chemicals to be used in these AMU tanks are nitric acid (12.2M), sodium hydroxide (19M), sodium ni trite and miscellaneous utility tank contents. ·

The scope of project W-004 will i nclude upgrading the floor (west end) , secondary containment, and instrumentation (to include level alarm and leak detection and temperature mon i toring) as well as electrical motor control centers for vessel agitators.

The scope of work identified in Project W-OlOH is to provide new spill containment and spill prevention measures for the storage tanks in the 211 -8 Chemical Tank Farm and the 221-B Operating Gallery Scale Tanks.

One of the scale tanks to be upgraded is TK-39A (60 gal) which can be utilized by the TRUEX Pilot Plant.

The project is also providing an overflow containment tank (TK-25) for sodium nitrite from scale tank TK-25A (400 gal).

The transfer pump station located at cell 40 in the 221-B Building Operating Gallery has not been used in years. The pumps are wrapped in plastic with a plexiglass shield covering them. The pump currently has a direct overflow to the chemical sewer. An interlock with the 225-8 BuildiMg receiving tank does not exist. If this system is not upgraded, operators will be required to hand carry nitric ac id to the . 225 - B Building AMU and pour it into the appropriate tanks. Special handling requirements for safety reasons will require operators to be dressed in acid suit and breathing contained fresh air .

225-8 Building AMU

The 225 -8 Building AMU is located on the second floor . There is a total of 11 tanks in the 225-8 Building AMU area. Table 1 identifies tanks, sizes and the chemical that was contained within each tank .

TABLE 1

Tank Chemical Capacity (gal)

TK-201 Tri-sodium phosphate 600 TK-202 Tri-sodium phosphate 600 TK-203 Sodium Hydroxide 50 TK -204 Nitric Acid 50

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I

TK-205 TK-206 TK-207 TK -208 TK-209 TK-210 TK-212

Hydrochloric Acid Hydrochloric Acid Sodium Hydroxide Phosphoric Acid Not Used Demineralized Water Sodium Hydroxide

WHC -SD-Wl53 -CDR-001 Rev . 0

30 5

100 so 50

1000 5

The current condition of the 225-8 Building AMU does not meet the environmental regulations to provide secondary containment to prevent spills from entering the chemical sewer and ensure incompatible chemicals shall not be mixed. Instrumentation would need to be upgraded accordingly to meet these environmental regulations also.

No projects have been identified to upgrade the 225-8 Building AMU . However, it would be necessary to provide the upgrades discussed in the 225-8 Building AMU Chemical Usage/Upgrades section for the TRUEX Pilot Plant.

221-8 Building AMU Chemical Usage/Upgrades

The chemicals to be used in the 221-B Building AMU for the TRUEX Pilot Plant are nitric acid, sodium hydroxide, sodium nitrite, and miscellaneous chemicals {oxalic acid, hydrazine and diatomaceous earth). The amount of nitric acid to be used per batch is identified in Table 2. The amount of sodium hydroxide and sodium nitrite will be used on an as needed basis for neutralization purposes.

The upgrades to existing systems are identified below by the chemical usage. The extent of these upgrades would include modifications to existing scale tanks and modifications to the pump transfer station in the 221-B Building. Additional chemical utility tanks with containment would be needed to make up miscellaneous chemicals. Two options are presented for the nitric acid usage in the 221-B Building. A flow diagram of the upgrades is outlined in Figure 1.

1. Nitric Acid Usage Seventy-nine gal of 12.2 M HN03 is required for each feed batch of 600 gal.

Option 1 - Upgrade Scale Tank {TK-38A) {400 gal)

Upgrade Instrumentation to include level and leak alarm detection.

Provide MOV on feed line to scale tank interlocked with high l i quid 1 eve l .

Provide jumpers to tanks (TK-38-1, 2, and 3).

TK-38A will receive nitric acid through header H-309 from TK-H-309 in the 221-B Building AMU .

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, I

\ .. ..

WHC-SD -Wl53 -CDR-001 Rev . 0

Option 2 - Utilize Scale Tank (TK-39A) (60 gal) which is upgraded in Project WOlO.

Provide Jumpers to Tanks (TK-38-1, 2, and 3)

TK-39A will receive nitric acid through header H-309 from TK-H-309 in the 221-B Building AMU.

2. Sodium Nitrite Sodium nitrite will be available in tanks TK-H-315, and 316 . The sodium nitrite header runs from TK-H-315, and 316 to scale tanks located between cells 24 and 29. The upgrade requirements for the use of sodium nitrite will be as. follows:

Extend the sodium nitrite header (h-315/316) to cell 36 to utilize scale tank (TK-36A).

Reroute overflow piping and drain p1p1ng from TK-36A in operating gallery to containment tank (added by project WOIO) in pipe gallery at cell 25.

3. Nitric Acid to Filter Dilute nitric acid (IM) will be needed as a filter flush. 12.2M ni tric acid will be able to use the same scale tank routing as the nitric acid usage. ·The upgrade necessary for this system will involve a jumper provided from the appropriate scale tank to the filter in cell 38.

4. Nitric Acid Transfer to the 225-B Building Nitric Acid header H-309 runs over to the 225-B Building AMU. A pump station is located in the pipe gallery of the 221-B Building at cell 40.

Upgrade/replace pump located in 221-B Building with interlock controls and manual shutoff in 225-B Building.

Provide instrumentation (level alarms/interlocks) to 225-B Building feed tanks and pump .

Provide secondary containment for pump, 225-B Building receiver tank and spill control/diversion capability .

5. Sodium Hydroxide Sodium hydroxide will be used to neutralize the raffinate solution in TK-38-6. Sodium hydroxide will be stored in TK-310 and TK-311 in the 221-B Building AMU . . These tanks will be accessed for sodium hydroxide . Upgrades to be in place, should consist of the following:

Provide sodium hydroxide header tie-in to scale tank TK-39A Provide jumper from scale tank TK -39A to TK -38-6

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I

6.

WHC -SD -Wl53 -CDR -001 Rev . 0

Oxalic Acid Oxalic acid will be added to the dissolver tanks (TK-38-1/2/3) . This chemical addition would be necessary for the PFP flowsheet. The upgrade proposed is to add a chemical utility tank with containment to tie-in to the scale tank TK-39A with jumpers provided to the dissolver tanks.

7. Hydrazine Hydrazine may be added to the dissolver tanks (TK-38-1/2/3) to oxidize N02 , thus eliminating evolution of NOx from the dissolver tanks. An upgrade would be required to add a chemical utility tank with containment to tie-in ta the scale tank TK-39A with jumpers provided to the dissolver tanks.

8. Diatomaceous Earth Diatomaceous earth would be used for precoating the filter in cell 38. The 221-8 Building would be required to mix up diatomaceous earth in the chemical utility tanks for other uses. TRUEX pilot plant would be able to access the chemical utility tanks (TK-313 and TK-314). The utility tank header connects to scale tank TK-39A. A jumper would need to be provided to the filter located in cell 38. ·

225-8 Building AMU Chemical Usage/Upgrades

The chemicals to be used in the 225-8 Building AMU are nitric acid, oxalic acid, l-hydroxyethane-1, 1-diphosphonic acid, (HEDPA), sodium carbonate, octyl (phenyl)-N,N-diisobutyl carbamoylmethylphosphine oxide, (CMPO), normal paraffin hydrocarbon, (NPH) and tributylphosphate, (TBP). The amounts of the chemicals have been calculated by using the amount of solids in one dissolver batch of 600 gal. These calculations can be found in Table 2.

A minimum of five agitator tanks will be required. Minimum tank sizes should be specified 20% larger than chemical need. All tanks will require secondary containment to contain 110% of the tank contents. An additional tank of 50 gal will be needed to contain just water. All tanks will require upgrades to instrumentation (level alarms, leak detection). Metering pumps or flowmeters with automatic controls should be provided to meter chemicals to cells. Backflow preventers will need to be in place. Connections to wall nozzles will need to be hard piped from tanks and jumper ties will need to be made in cell tanks. Sufficient redundancy of tanks containing strip, scrub No. 1, and scrub No. 2 solutions will need to be provided to ensure the duration of campaigns is longer than one 600 gal batch of 3.5 days.

Additional storage tanks with metering pumps will need to be provided for a 1 yr supply of TBP (60 gal) and NPH (70 gal). A water wash tank should be provided to wash the TBP to eliminate monobutyl and dibutyl degradation products in the fresh organic solvent which extracts transurancies and go to the aqueous waste stream. (This stream would then go to grout instead glass.) A nitric acid receiver tank will also need to be prov ided to feed the agitated tanks.

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.r'°"'• >

( \. ........

Tank

Strip

WHC -SD -Wl53 -CDR -001 . Rev. 0

Current operations allow the vessel ventilation header to vent through to the roof with no filtration. This may need to be altered due to zon i ng requirements, {225-8 Building AMU is designated potentially contaminated) .

Special ventilation for mixing organic may need to be provided {hood with minimum face velocity 150 ft/min, actual face velocity is dependent upon toxicity of chemicals found in ASHRAE standards).

Additional fire protection may need to be provided for the organic solvent. The addition will be dependent upon the location of the organic solvent and component tanks .

A flow diagram and components are identified in Figure 2. Specific tank information can be found in Table 3 summarizing sizes, tie-ins, and components. tanks are identified by the chemical stream name.

TABLE 3

Component Batch Size (gal ) Tie- ins Tank Size

H20/HEDPA 25 . 1 H20 50 gal

Scrub No. 1 H20/H2C20t.f'HN03 40 . 1 H20/HN03 50 gal

Scrub No. 2 H20 40 .1 H20 50 gal

Carbonate H20/NaC03 1.056 H20 15 gal Scrub

Acid Scrub H20/HN03 0. 704 H20/HN03 15 gal

Organic CMPO/TBP/NPH 1.29 TBP/NPH 15 gal Solvent

Conclusions and Recommendations

In addition to the upgrades identified, the following conclusions and recommendations are provided.

The TRUEX Pilot Plant will be able to take advantage of the upgrades provided by the two 221 -8 Building projects, thus prov iding minimal additional upgrades. The preferred alternative for the nitric acid upgrade i s option 1, since it would eliminate cross -contamination of chemicals, water flushes and more than one acid transfer for one process batch.

Only two chemical utility tanks are currently available for use in the 221 -8 Building AMU. Three miscellaneous chemicals are required for use in the TRUEX Pilot Plant. The chemical utility tanks wi ll also be dedicated for 221-8 Building use. Therefore, it is recommended that additional chemical utility tanks be added to supplement the AMU system.

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The nitric acid pump station is required due to the safety aspects. The special operator handling requirements would be eliminated if a header receiver tank located in the 225-B Building could be utilized to meter acid to the appropriate agitator tanks.

The currently available resources within the 225- B Building AMU do not fit with the requirements for the necessary chemicals and tank sizes needed to support the TRUEX Pilot Plant. Due to the limited space available for expansion, it may be required to remove existing equipment.

It might be possible to upgrade TK-205 once used for HCl which has local ventilation already on the tank. Verification of the existing ventilation at the tank would need to be ascertained ta ensure adequacy.

TK-204 the nitric acid tank which has a connection from 221-8 Building header H-309 may be utilized as an acid receiving tank. From the receiving tank, the tie-ins can be made to the mixing tanks. Secondary containment and instrumentation upgrades to TK-204 will also be necessary.

The 225-B Building AMU will also have to be evaluated for dry chemical storage ta include NaC03 , HEDPA, H2C204 and CMPO.

L-6

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Page 160: -I-Cl l

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Page 161: -I-Cl l

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APPENDIX M

Sketches

Page 162: -I-Cl l

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INDEX NO. , ... , ...

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TITLE

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Page 163: -I-Cl l

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Page 164: -I-Cl l

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Page 166: -I-Cl l

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~ff/() 'tVI Pa ge 1 of _I_ ENGINEEtllNG DATA TRANSMITTAL

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Impact Level (F) Reason for Transmittal (G) Disposit ion (H) & (I)

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I 3. Information 6. Dist (Receipt Ack now. Required) 3. Disapproved w /comment 6. Receipt acknow ledged

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I ~- 19. 20. 21. DOE APPROVAL (if required) I Ltr No. ..

W!lt;E~ '!f:!/fio ~Ktki 1ffe.!1t • Approved --- oghizanm,;et • Approved w /comments Authorized Representative Date e

[ Originator for Receiving Organization Engineer's Manager • Disapproved w /comments

BD-7400- 172 (2 /89)