gurukashiuniversity.ingurukashiuniversity.in/syllabi/diploma/syllabus/diploma... · web view1st...

GURU KASHI UNIVERSITYGURU GOBIND SINGH COLLEGE OF ENGINEERING & TECHNOLOGY

Diploma (Petrochemicals and Petro Refinery Engineering)

STUDY SCHEME of Petrochemicals and Petro Refinery Engineering

1st Semester

Subject Code Subject Name L T P *Others Credits

120101 Applied Chemistry – I 4 - - 4120102 Applied Mathematics - I 4 - - 4120103 Applied Physics – I 3 - 3120104 English and Communication Skills – I 3 - 3123101 Engineering Drawing – I 2 - 6 4120105 Applied Chemistry – I (Practical) - - 2 1120106 Applied Physics – I (Practical) - - 2 1120107 English and Communication Skills – I

(Practical) - - 2 1120108 General Workshop Practice – I - - 6 3120109 Student Centered Activities - - - -

TOTAL 17 - 18 27



2nd SemesterSubject

Code Subject Name L T P *Others Credits

120202 Applied Mathematics - II 5 - - 5120203 Applied Physics-II 4 - - 4126201 Chemical Engineering Materials 4 - - 4

126202 Introduction to Petrochemical Technology 5 - - 5

126203 Chemical Engineering Drawing 2 - 4 4120206 Applied Physics-II - - 2 1121202 Basic of Information Technology - - 4 2126204 Chemical Engineering Materials - - 2 1120208 General Workshop Practice – II - - 6 3

126205 Introduction to Petrochemical Technology - - 2 1

TOTAL 20 - 20 30



3rd Semester


126301 Chemical Engineering-I (Mechanical Operation) 3 - - 3

125312 Electrical Engineering 2 - - 2126302 Engineering Mechanics-I 3 - - 3126303 General Chemical Technology 3 - - 3123310 Mechanical Engineering 3 - - 3126304 Organic Chemistry 3 - - 3

126305 Chemical Engineering-I (Mechanical Operation) (Practical) - - 2 1

125313 Electrical Engineering (Practical) - - 2 1126306 Engineering Mechanics-I (Practical) - - 2 1

126307 General Chemical Technology (Practical) - - 2 1

123311 Mechanical Engineering (Practical) - - 2 1126308 Organic Chemistry (Practical) - - 2 1126309 Workshop Practice – III - - 6 3

TOTAL 17 - 18 26



4th Semester


126401 Chemical Engineering-II (Fluid flow operation) 4 - - 4

126402 Engineering Mechanics-II 4 - - 4126403 Fertilizer Technology 4 - - 4126404 Physical & Analytical Chemistry. 4 - - 4126405 Process Calculation 3 - - 3

126406 Chemical Engineering-II (Fluid flow operation) (Practical) - - 4 2

126407 Engineering Mechanics-II (Practical) - - 2 1126408 Fertilizer Technology (Practical) - - 2 1

121410 Personal Computer Maintenance and Repair - - 4 2

126409 Physical & Analytical Chemistry. (Practical) - - 2 1

126410 Process Calculation (Practical) - - 2 1TOTAL 19 - 16 27



5th Semester


126501 Chemical Engineering III (Mass Transfer Operation I ) 5 - - 5

126502 Chemical Engineering IV ( Heat Transfer operation ) 4 - - 4

126503 Chemical Engineering Thermodynamics & Kinetics. 4 - - 4

126504 Plant Operation 4 - - 4126505 Petrochemicals Technology 4 - - 4

126506 Chemical Engineering III (Mass Transfer Operation I ) (Practical) - - 2 1

126507 Chemical Engineering IV ( Heat Transfer operation ) (Practical) - - 2 1

126508Chemical Engineering Thermodynamics & Kinetics. (Practical)

- - 2 1

126509 Plant Operation (Practical) - - 2 1

126510 Petrochemicals Technology (Practical) - - 2 1

126511 Project Work-I - - 4 2TOTAL 21 - 14 28



6th Semester


126601 Chemical Engineering V (Mass Transfer Operation II ) 4 - - 4

125601 Basics Of Management 4 - - 4126602 Health Environment & Safety 4 - - 4126603 Polymers Technology and Processing. 4 - - 4126604 Process Instrumentation & Control 3 - - 3

126605 Chemical Engineering V (Mass Transfer Operation II ) (Practical) - - 2 1

126606 Health Environment & Safety (Practical) - - 2 1

126607 Polymers Technology and Processing. (Practical) - - 2 1

126608 Process Instrumentation & Control (Practical) - - 2 1

126609 Project Work –II - - 8 4

TOTAL 19 - 16 27

TOTAL CREDITS:- 165



1ST SEMESTER SYLLABUS

120101 APPLIED CHEMISTRY-I Credits 04 L T P 4 0 0

DETAILED CONTENTSChapter 1. Basic Concepts of Chemistry (10 hrs) 1.1 Units and Dimensions, dimensional formulas- dimensional analysis

principle of homogeneity of dimensions and their limitations, derived units (with special reference to pressure, volume, temperature, density, specific gravity, surface tension, viscosity and conductivity, thermodynamic parameters-significance and applications)

1.2 Matter, element, compound and mixtures, atoms, molecules, ions, symbols and formulae, Atomic mass (A), atomic number (Z) isotopes, isobars, isotones (recapitulation only)

1.3 Mole concept, solution, standard solution, methods to express concentration of solutionMolar mass, molar volume of gases, strength of solutions in grams per liter, morality (M), molality (m), mass and volume percentages and mole fraction

1.4. Chemical equations, thermo-chemical equations, balancing of chemical equations and simple stoichiometric calculations.

1.5 Numerical problems based on mole concept and molarity.

Chapter 2. Atomic Structure, Periodic Table and Chemical Bonding (12 hrs)2.1 Fundamental particles- electrons, protons and neutrons 2.2 Bohr’s model of atom and its limitations (qualitative treatment only).2.3 Wave particle duality and Heisenberg’s uncertainty principle

(elementary idea only)2.4 Modern concept of atom, definition of orbit and orbital’s, shapes of s

and p orbital’s only, quantum numbers (significance only), electronic configuration of elements up to atomic number 30 on the basis of Aufbau Principle, Pauli’s Principle and Hund’s Rule

2.5 Modern periodic law and periodic table, groups and periods.2.6 Classification of elements into s, p, d, and f blocks (periodicity in

properties are excluded)2.7 Chemical bond and cause of bonding. 2.8 Ionic bond, valence bond approach of covalent bond, hybridization

(sp3, sp2 and sp) sigma (σ) and pi (π) bonds.2.9 Metallic bonding – electric, magnetic and dielectric properties based on

Band model

Chapter 3. Water (10 hrs)



3.1 Sources of water, impurities in water (dissolved –gases, salts and suspended), 3.2 Hardness of water, types of hardness, degree of hardness, units of hardness-

ppm, oCl, oFr – numerical problems3.3 Disadvantages of using hard water in domestic and in industries: Laundry

work (action of soap on water), paper, textile and beverage industries.3.4 Boiler feed water and its quality - causes and prevention of

Scale and sludge formation, Priming and foaming Boiler corrosion, Caustic embitterment

3.5 Softening of hard water by Ion exchange process- dematerialized water advantages and limitations of

this method Desalting of sea water by reverse osmosis (RO) methodCalgon process

3.6 Characteristics of drinking water and ICMR, ISI –quality criteria 3.7 Water analysis: Quantitative analysis of hardness by EDTA method, alkalinity, and estimation of total dissolved solids (TDS)-numerical problems3.8 Enlist applications of various kinds of water in engineering and chemical industry.

Chapter 4. Gas laws, Terminology of Thermodynamics and Equilibrium(14 hrs) 4.1 Definition of gas and perfect gas, gas laws- Boyle’s Law, Charles law &

Avogadro’s law, Gas constant (R). 4.2 Terminology of Thermodynamics- thermodynamic system, surroundings,

types of systems, extensive and intensive properties, state of a system, state functions, isothermal, adiabatic reversible, irreversible spontaneous and non spontaneous processes, meaning of ∆E, ∆H, ∆S and ∆G, free energy of spontaneous and non spontaneous processes (mathematical derivations are excluded)

4.3 Elementary idea of zeroth, 1st, 2nd, and 3rd laws of thermodynamics (without mathematical derivation)

4.4 Applications of free energy change (∆G) criteria (in metallurgy and electric work without any mathematical derivation)

4.5 Equilibrium state and its significance statement of Le-Chatelier’s principle, equilibrium constant (K) and its applications..

4.6 Electrolytes, non electrolytes, ionization in aqueous solutions, degree of ionization, ionic product of water (Kw)

4.7 Concept of pH, pH- scale and industrial applications of pH4.8 Definitions - acids, bases, neutralization and acid base titrations,

indicators and choice of indicators for acid base titration.4.9 Buffer (acidic, basic and neutral) solutions, enlist applications of buffer

solution 4.10 Simple numerical problems (only on 4.1, 4.5. 4.6 and 4.7 sections)

Chapter 5. Electrochemistry (10 hrs)



5.1 Electronic concept of oxidation and reduction, redox reactions 5.2 Electrolytes, non-electrolytes and electrolysis, 5.3 Faraday’s Laws of electrolysis and applications in electrometallurgy and

electroplating in automobile5.4 Standard reduction potential (SRP), activity series, electrochemical cell

and their e.m.f5.5 Chemistry of commercial electrochemical cells 5.6 Primary cells - Daniel cell and dry cell

secondary cell - lead acid storage cell, Wetson-cadmium cell, Ni-cad battery, Li battery, Hg – button cell and Ag- button cellFuel cells

Chapter 6. Organic Chemistry (06 hrs)6.1 Tetra covalence of carbon in carbon compounds, catenation (definition only) 6.2 Classification of organic compounds on the bases of functional group6.3 IUPAC nomenclature of simple organic compounds (containing one functional

group only) and their common names (if any)



120102 APPLIED MATHEMATICS – I

Credits:- 05 L T P

5 - -DETAILED CONTENTS

Chapter 1. Algebra (30 hrs)1.1 Complex Numbers: Complex number, representation, modulus and

amplitude. De-movier’s theorem, its application in solving algebraic equation.

1.1 Basics and properties of logarithms and its applications in solving problems related to basic logarithmic formulas.

1.2 Geometrical progression, its nth term and sum of n terms and to infinity. Application of Arithmetic progression and Geometrical progression to Engineering problem such as maximum possible output of the machine, vibration of the spring, finding out capacity of tank etc.

1.3 Partial fractions (linear factors, repeated linear factors, non-reducible quadratic factors excluding repeated factors)

1.5 Permutations and Combinations: Value of npr ncr. Simple problems of formulation of words from given alphabets (with and without repetition), circular permutations etc.

1.6 Binomial theorem (without proof) for positive integral index (expansion and general form); binomial theorem for any index (expansion without proof) first and second binomial approximation with applications to engineering problems

Chapter 2. Trigonometry (25 hrs)2.1 Concept of angles, measurement of angles in degrees, grades and

radians and their conversions. Applications of angles such as angle subtended by an arc, diameter of moon etc.

2.2 T-Ratios of Allied angles (without proof), Sum, difference formulae and their applications (without proof). Product formulae (Transformation of product to sum, difference and vice versa). T-Ratios of multiple angles, sub-multiple angles (2A, 3A, A/2).

2.3 Graphs of Sin x, Cos x, Tan x and ex

2.4 Applications of Trigonometric terms in engineering problems such as to find an angle of elevation, height, distance etc.



Chapter 3. Co-ordinate Geometry (25 hrs)3.1 Cartesian and Polar coordinates (two dimensional), conversion from

cartesian to polar coordinates and vice-versa, distance between two points (cartesian co-ordinates), section formulae

3.2 Area of triangle when its vertices are given, co-ordinates of centroid, in center of a triangle when the vertices are given, simple problems on locus.

3.3 Equation of straight line in various standard forms (without proof), inter section of two straight lines, angle between two lines. Parallel and perpendicular lines, perpendicular distance formula

3.4 General equation of a circle and its characteristics. To find the equation of a circle, given:

Centre and radius Three points lying on it Coordinates of end points of a diameter

3.5 Equation(s) of a straight line, circle, and conics (ellipse, parabola and hyperbola) and their application in solving engineering problems..



120103 APPLIED PHYSICS – I Credits 04 L T P 4 0 0

DETAILED CONTENTSChapter 1. Units and Dimensions (8 hrs)

1.1 Physical quantities 1.2 Units - fundamental and derived units, systems of units (FPS, CGS, MKS and

SI units) 1.3 Dimensions and dimensional formulae of physical quantities 1.4 Dimensional equations and principle of homogeneity, applications to

conversion from one system of units to another, checking the correctness of physical relations and derivation of simple physical relations, limitations of dimensional analysis

1.5 Error in measurement, random and systematic errors1.6 Application of units and dimensions in measuring length, diameter,

Circumference, volume, surface area etc. of metallic and non metallic blocks, wires, pipes etc (at least two each).

Chapter 2. Force and Motion (10 hrs) 2.1Scalar and vector quantities – examples, addition and multiplication (scalar

product and vector product) of vectors 2.2Force, resolution and composition of forces: resultant, parallelogram law of

forces, equilibrium of forces2.3Newton’s Laws of motion: concept of momentum, Newton’s laws of motion and

their engineering applications, derivation of force equation from Newton’s second law of motion; conservation of momentum, impulse. Simple numerical problems

2.4Circular motion: angular displacement, angular velocity and angular acceleration

2.5Relation between linear and angular variables (velocity and acceleration) 2.6Centripetal force (derivation) and centrifugal force with its application such as

banking of roads, bending of cyclist, motion in vertical circle etc 2.7Application of various forces in lifts, cranes, large steam engines and turbines.

Chapter 3. Waves and Vibrations (10 hrs) 3.1. Wave motion: transverse and longitudinal wave motion with examples, sound

and light waves, velocity, frequency and wave length of a wave (relationship v = nλ) and their applications

3.2 Wave equation, y = r sine t, phase, phase difference, superposition of waves and their applications.

3.3 Simple Harmonic Motion(SHM): definition, expression for displacement, velocity, acceleration, time period, frequency in S.H.M.

3.4 Free, forced and resonant vibrations with examples



3.5 Acoustics of buildings – reverberation, reverberation time, echo, noise, coefficient of absorption of sound, methods to control reverberation time and their applications

3.6 Ultrasonic – production (magnetostriction and piezoelectric methods) and their engineering and medical applications

Chapter 4 Rotational Motion (6 hrs) 4.1 Concept of translator and rotating motion with examples4.2 Definitions of torque, angular momentum and their relationship 4.3 Conservation of angular momentum (qualitative) and its examples 4.4 Moment of inertia and its physical significance, radius of gyration, Theorems

of parallel and perpendicular axes (statements), Moment of inertia of rod, disc, ring and sphere (Formulae only).

4.5 Application of rotational motions in transport vehicles, trains and aero plane turbine/engine.

Chapter 5 Work, Power and Energy (10 hrs) 5.1 Work: definition and its SI units 5.2 Work done in moving an object on horizontal and inclined plane

(incorporating frictional forces) with its application5.3 Power: definition and its SI units, calculation of power with numerical problems5.4 Energy: Definition and its SI units: Kinetic energy and Potential energy with

examples and their derivation 5.5 Principle of conservation of mechanical energy (for freely falling bodies),

transformation of energy from one form to another with its application 5.6 Friction: concept, types and its engineering applications. 5.7 Application of Friction in brake system of moving vehicles, trains, aero planes

and other objects.

Chapter 6 Properties of Matter (10 hrs) 6.1 Elasticity: definition of stress and strain, different types of modulus of

elasticity, stress – strain diagram, Hooke’s law with its applications6.2 Pressure: definition, its units, atmospheric pressure, gauge pressure, absolute

pressure, U-tube, manometers and barometer gauges and their applications6.3 Surface tension: concept, its units, angle of contact, measurement of surface

tension by capillary tube method, applications of surface tension, effect of temperature and impurity on surface tension

6.4 Fluid motion, stream line and turbulent flow, Equation of Continuity, Bernoulli’s Theorem and their applications.

6.5 Viscosity and coefficient of viscosity: Buoyant force, buoyancy, Stoke’s Law and derivation of terminal velocity, effect of temperature on viscosity and its application in hydraulic systems.

Chapter 7 Thermometry (10 hrs) 7.1 Difference between heat and temperature on the basis of K.E. of molecules 7.2 Principles of measurement of temperature and different scales of

temperature and their relationship



7.3 Resistance thermometers and Pyrometers with their field applications such as Thermocouple, Bi-metallic thermometer.

7.4 Expansion of solids, liquids and gases, coefficient of linear, surface and cubical expansions and relation amongst them

7.5 Modes of transfer of heat (Conduction, convection and radiation with examples)

7.6 Co-efficient of thermal conductivity, determination of thermal conductivity of good conductor (Searle’s method) and bad conductor (Lee’s disc method)

7.7 Application of various systems of thermometry in refrigeration and air-conditioning etc.



120104 ENGLISH AND COMMUNICATION SKILLS - ICredits 03

L T P 0 0 3

DETAILED CONTENTSChapter 1. Facets of Literature (14 hrs)1.1 Short Stories:

Homecoming – R.N. TagoreThe Selfish Giant - Oscar WildeThe Diamond Necklace- Guy- De MaupassanttThe Stick – Justice Surinder Singh

1.2 Prose:I Have A Dream – Martin Luther King On Habits – A. G. GardinerMy struggle for An Education- Booker T WashingtonSeeing People Off – Max Beerbohm

1.3 Poems :Ozymandias – P.B. ShelleyDaffodils – William Wordsworth Stopping by Woods on a Snowy Evening – Robert FrostForefathers- Edmund Blunden

Chapter 2. Grammar and Usage (10 hrs)2.1 Parts of speech:

Nouns PronounsAdjectivesArticlesVerbs AdverbsPrepositions ConjunctionInterjectionIdentifying parts of speechStructures: Verb patterns, Question tags,Subject – Verb agreement (concord)

2.2 Pair of words (Words commonly confused and misused) TensesCorrection of incorrect sentences One word substitution

Chapter 3. Translation (04 hrs)3.1 Glossary of Administrative Terms (English and Hindi)3.2 Translation from Hindi into English

Chapter 4. Paragraph of 100-150 words from outlines (08 hrs)



Chapter 5. Comprehension (04 hrs)Unseen passages of literature, scientific data/graph based for comprehension exercises

Chapter 6. Communication (08 hrs)6.1 Definition, Introduction and Process of Communication 6.2 Objectives of Communication6.3 Notices



123101 ENGINEERING DRAWING - I

Credits:-05 L T P 2 0 6Note:

1. First angle projection is to be followed2. Minimum of 16 sheets to be prepared3. Instructions relevant to various drawings may be given along with

appropriate demonstrations, before assigning drawing practice to students

DETAILED CONTENTSChapter 1. Introduction to Engineering Drawing1.1 Introduction to drawing instruments, materials and layout of drawing sheets.

Chapter 2. Free Hand Sketching and Lettering (03 sheets)2.1 Different types of lines in engineering drawing as per BIS specifications2.2 Practice of vertical, horizontal and inclined lines, geometrical figures such as triangles, rectangles, circles, ellipses and curves, hexagonal, pentagon with the help of drawing instruments.2.3. Free hand lettering (Alphabet and numerals) – lower case and upper case, single stroke, vertical and inclined at 75 degree in different standards, series of 3,5,8 and 12 mm heights in the ratio of 7:4

Chapter 3. Dimensioning Technique (01 sheet)3.1 Necessity of dimensioning, method and principles of dimensioning (mainly theoretical instructions)3.2 Dimensioning of overall sizes, circles, threaded holes, chamfered surfaces, angles, tapered surfaces, holes, equally spaced on P.C.D., counter sink holes, counter bored holes, cylindrical parts, narrow spaces and gaps, radii, curves and arches

Chapter 4. Scales (02 sheets)4.1 Scales - their need and importance (Theoretical instructions).4.2 Drawing of plain and diagonal scales

Chapter 5. Projection (05 sheets)5.1 Theory of projections (Elaborate theoretical instructions)5.2 Projection of Points Production of a point in the first quadrant.

Projection of a point in the third quadrant.5.3 Projection of Straight Line

Line parallel to both the planesLine perpendicular to any one of the reference planeLine inclined to any one of the reference plane.

5.4 Drawing 3 views of given objects (Non-symmetrical objects may be selected for this exercise)



5.5. Drawing 6 views of given objects (Non-symmetrical objects may be selected for this exercise)5.6. Identification of surfaces on drawn views and objects drawn5.7. Exercises on missing lines and viewsNote: At least one sheet in third angle projection

Chapter 6. Sections (02 sheets)6.1 Importance and salient features, Methods of representing sections,

conventional sections of various materials, classification of sections, conventions in sectioning

6.2 Drawing of full section, half section, partial or broken out sections, Offset sections, revolved sections and removed sections.6.3 Drawing of different conventions for materials in section, conventional breaks for shafts, pipes, rectangular, square, angle, channel, rolled sections6.4 Exercises on sectional views of different objects.

Chapter 7. Isometric Views (03 sheets)7.1 Fundamentals of isometric projections (Theoretical instructions)7.2 Isometric views of combination of regular solids like cylinder, cone, cube and prism.



120105 APPLIED CHEMISTRY-I Credits:- 01 L T P 0 0 2LIST OF PRACTICALS

1. Introduction to volumetric analysis, apparatus used in volumetric analysis and molarity based calculations.

2. Preparation of standard solution of oxalic acid {(COOH)2.2H2O} or potassium permanganate (KMnO4) or potassium dichromate (K2Cr2O7)

3. To verify the physical (state, color, odour solubility, boiling and melting points) properties and few chemical properties of ionic (e.g. NaCl) and covalent (kerosene oil or any other such compound may be given) compounds.

4. To determine strength of given solution of sodium hydroxide by titrating against standard solution of oxalic acid using phenolphthalein indicator.

5. To determine total acid number of given oil volumetrically6. To prepare cuprammonium {Cu(NH3)4SO4} and estimate cupric ion in the

given solution of copper sulphate solution by spectrophotometer method..7. To distinguish between aldehyde and ketone by Tollen’s reagent

(benzaldehyde and acetone may be used)8. To verify the first law of electrolysis. (Electrolysis of copper sulphate solution

using copper electrode).9. To prepare iodoform from ethanol or acetone 10. To prepare Bakelite 11. To prepare the Mohr’s salt from ferrous sulphate and ammonium sulphate. 12. Estimation of hardness of water by EDTA method. 13. Estimation of total alkalinity in the given sample of water by titrating against

standard solution of sulfuric acid14. Determination of pH of given solution using pH meter.

120106 APPLIED PHYSICS – I



Credits:- 01 L T P 0 0 2

LIST OF PRACTICALS (to perform minimum ten experiments)

1. To find the diameter of wire using a screw gauge 2. To find volume of solid cylinder and hollow cylinder using a vernier calipers

3. To determine the thickness of glass strip and radius of curvature using a spherometer

4. To verify parallelogram law of forces

5. To find the time period of a simple pendulum and determine the length of second’s pendulum.

6. To find the frequency of a tuning fork by a sonometer

7. To find the velocity of sound by using resonance apparatus at room temperature.

8. To find the Moment of Inertia of a flywheel about its axis of rotation

9. To find the surface tension of a liquid by capillary rise method

10. To determine the atmospheric pressure at a place using Fortin’s Barometer

11. To determine the viscosity of glycerin by Stoke’s method

12. To determine the coefficient of linear expansion of a metal rod

13. To find the coefficient of thermal conductivity of Bakelite sheet (bad conductor) by Lee’s Disc Method

14. To determine the coefficient of thermal conductivity of a copper strip using Searle’s Thermal Conductivity apparatus.



120107 ENGLISH AND COMMUNICATION SKILLS - ICredits 01

L T P

0 0 2

LIST OF PRACTICALS

1. Locating a Book in Library2. To look up words in a Dictionary: meaning and pronunciation of words as

given in the standard dictionary using symbols of phonetics3. To seek information from an Encyclopedia4. Listening pre-recorded English language learning programme 5. Paper reading before an audience (reading unseen passages)6. Study of spelling Rules7. Study of essentials of a good speech to respond and comprehend visual, oral

themes, situations or stimulus and practice before select gathering8. Exercises on use of different abbreviations9. Greetings for different occasions10. Introducing oneself, others and leave taking11. Exercises on writing sentences on a topic



120108 WORKSHOP PRACTICE – I

Credits:-03 L T P

0 0 6DETAILED CONTENTS (PRACTICALS)

The following shops are included in the syllabus: 1. Carpentry and Painting Shop 2. Fitting Shop 3. Electric Shop Note: The contents of various shops prescribed under workshop Practice –I are same as that of General Workshop Practice-I which is common for most of engineering diploma programmes except for Computer Engineering and Information Technology.The instructor is to first explain the introductory part given at the beginning under each shop followed by demonstration and practice by students.1. Carpentry and Painting Shop 1.1 Introduction to various types of wood such as Deodar, Kail, Partal, Teak,

Hollack, Sheesham, Champ, etc. (Demonstration and their identification).1.2 Demonstration, function and use of commonly used hand tools. Care,

maintenance of tools and safety measures to be observed. Job I Marking, sawing, planning and chiseling & their practice

1.3 Introduction to various types of wooden joints, their relative advantages and uses.

Job II Preparation of half lap joint Job III Preparation of Mortise and Tenon Joint

1.4 Demonstration of various methods of painting wooden items. Job IV Preparation of surface before painting including primer coat

Job V Painting Practice by brush/roller/spray2. Fitting Shop 2.1 Introduction to fitting shop tools, common materials used in fitting shop,

Identification of materials. (e.g. Steel, Brass, Copper, Aluminium etc.). Identification of various sections of steel viz. Flat, Angle, Tee, Channel, Bar Girder, Square, Z-Section, etc.

2.2 Description and demonstration of various types of work benches. Holding devices and files. Precautions while doing filing work.Job I Marking of job, use of marking tools and measuring instruments.Job II Filing a dimensioned rectangular or square piece of an accuracy of

0.25mmJob III Filing practice (Production of flat surfaces) Checking by straight edge.

2.3 Description and demonstration of simple operation of hack-sawing, demonstration and description of various types of blades and their specifications, uses and method of fitting the blade. Job IV Making a cutout from a square piece of MS Flat using Hand

hacksaw.3. Electric Shop



3.1 Study, demonstration and identification of common electrical materials such as wires, cables, switches, fuses, ceiling roses, battens, cleats and allied items, tools and accessories.3.2 Study of electrical safety measures and demonstration about use of protective devices.

Job I Identification of phase, neutral and earth of domestic appliances and their connection to two pin/three pin, plugs.

Job II Preparation of a house wiring circuit using fuse, switches, socket, holder, ceiling rose etc. by batten wiring and PVC casing and capping3.3 Study of common electrical appliances such as electric iron, electric kettle, ceiling fan, table fan, electric mixer, electric Geyser, desert cooler etc.3.4 Introduction to the construction of a Lead-acid battery and its working.

Job III Installation of a battery and to connect two or more batteries in series and in parallel.

2nd SEMESTER SYLLABUS

(120202) APPLIED MATHEMATICS-II



Credits 05 L T P

5 - - DETAILED CONTENTS

Chapter 1. Algebra (10 hrs)1.1 Determinants: Elementary properties of determinants up to 3rd order,

consistency of equations, Crammer’s rule.1.2 Matrix: Algebra of matrices, Inverse of a matrix, matrix inverse method

to solve a system of linear equations in 3 variables. 1.3 Application of Matrix in computer programming

Chapter 2. Differential Calculus (24 hrs)

2.1 Definition of function; Concept of limits. Lt xn - an,

Four standard limits x a ---------- x - a Lt Sin x Lt ax - 1 Lt (1+x)1/x

x 0 -------- , x 0 ------- , x 0 x x

2.2 Differentiation of xn , sin x, cos x, tan x, ex, logax (Please take one

example of differentiation by definition)2.3 Differentiation of sum, product and quotient of functions.

Differentiation of function of a function. 2.4 Differentiation of trigonometric inverse functions. Logarithmic

differentiation. Exponential differentiation, Successive differentiation (excluding nth order).

2.5. Application of differential calculus in:: Rate Measures

Errors and increments Maxima and minima Equation of tangent and normal to a curve (for explicit functions only)

Chapter 3. Integral (26 hrs) 3.1 Integration as inverse operation of differentiation with simple examples. 3.2 Simple integration by substitution, by parts and by partial fractions (for linear factors only) 3.3 Evaluation of definite integrals (simple problems)-

π/2 π /2 π/2 Evaluation of ∫ Sinn x. dx, ∫ Cosn x dx , ∫ Sinm x Cosn x dx 0 0 0 using formulae without proof (m and n being positive integers only)

3.4 Applications of integration for : Simple problem on evaluation of area bounded by a curve and axes.



Calculation of volume of a solid formed by revolution of an area about axes. (Simple problems).

To calculate average and root mean square value of a function and Area by Trapezoidal Rule and Simpson’s Rule

Chapter 4. Statistics and Probability (12 hrs) 4.1 Measures of Central Tendency: Mean, Median, Mode with example of daily life. 4.2. Measures of Dispersion: Mean deviation, Standard deviation 4.3. Probability definition and addition law of probability, theorem and

simple numerical problems, General view of normal probability curve (No numericals)

4.4. Explanation of different sampling techniques ( No numericals )

Chapter 5. Differential Equations (08 hrs)5.1 Solution of first order and first degree differential equation by variable

separation method (simple problems) 5.2. Differential equations of homogeneous equation



(120203) APPLIED PHYSICS – II

Credits 04 L T P 4 - -

DETAILED CONTENTS

Chapter 1. Optics (12 hrs) 1.1 Review of basic optics laws: Reflection and Refraction1.2 Refractive index and magnification, image formation in lenses, lens

formulae (thin lens only), power of lens, total internal reflection and their applications

1.3 Simlpe concepts of interference, diffraction , Polarization and their applications like Commercial equipment, optic glasses and its manufacturing and use of Polarimeter in sugarcane industry and distilleries (No explanation required).

1.4 Simple and compound microscope, astronomical telescope, magnifying power and its calculation (in each case) and their applications

Chapter 2. Electrostatics (10 hrs) 2.1 Coulombs law, unit charge and electric lines of force 2.2 Electric flux and Gauss’s Law, Electric field intensity and electric

potential 2.3 Electric field due to point charge, straight charged conductor, plane

charged sheet and charged sphere (Inside and outside the sphere)2.4 Capacitance, types of capacitors, capacitance of parallel plate

capacitor, series and parallel combination of capacitors, Dielectric and its effect on capacitance, and dielectric break down

2.5 Pollution, different types of pollution and polluting agents, Use of Electronics in reducing Air and Water pollution e.g. precipitation of microbes and moisture reparation from air and gases in industry (small explanation only)

Chapter 3. DC Circuits (15 hrs) 3.1 Concept of electricity, various applications of electricity 3.2 Current, voltage, resistance, potential difference and e.m.f, power,

electrical energy and their units, advantages of electrical energy over other forms of energy and Alternating Current and Direct Current

3.3 Ohm’s law and its applications, specific resistance, effect of temperature on resistance, co-efficient of resistance, series and parallel combination of resistors an Resistance, Definitions of Conductance and Super Conducter’s

3.4 Kirchhoff’s laws, Wheatstone bridge principle and its applications 3.5 Heating effect of current and concept of electric power, energy and

their units, related numerical problems and their applications



3.6 Examples of DC Circuits e.g. Various electrical and electronic equipment CRO, T.V., Audio system, Computers (Only examples, no explanations)

Chapter 4. Electromagnetism (10 hrs) 4.1 Magnetic field and its units, magnetic intensity, magnetic lines of force,

magnetic flux and their units 4.2 Permeability and susceptibility and their applications. Electromagnetic

Induction, Lanz’s law and its uses like dynomo, Right hand and left hand rules, Magnetic lines of force due to straight conductor, Solenoid and Circular coil. Force on a current carrying rectangular coil placed in magnetic field and its uses in moving coil galvanometer, electric motor (Concept only). Lorentz force, Force on a current carrying conductor (straight and rectangular)

4.3 Moving coil galvanometer its principle, construction and working. Chapter 5. Semiconductor physics (07 hrs)

5.1 Energy bands, intrinsic and extrinsic semiconductors, p-n junction diode and its characteristics

5.2 Diode as rectifier – half wave and full wave rectifier, semiconductor transistor pnp and npn (concept only)

Chapter 6. Modern Physics (10 hrs)6.1 Lasers: concept of energy levels, ionizations and excitation potentials;

spontaneous and stimulated emission; lasers and its characteristics, population inversion, types of lasers, Helium- Neon and ruby lasers their engineering and medical applications.

6.2 Fibre optics: introduction to optical fiber materials, types, light propagation and applications in communication.



(126201)Chemical Engineering MaterialsCREDITS:-04 L-T-P 4 - -

Chapter 1. Introduction scope of engineering materials, classification of engineering materials, fundamental nature & structure of material, selection of materials

Chapter 2. Engineering properties of materialsMP, BP, Heat capacity, thermal conductivity, Expansion co efficient, thermal insulation, stress, strain, Factors affecting properties of materials

Chapter 3. Metals & AlloysHeat treatment of Steels Mechanical properties of steel, wrought Iron. The analysis of simple Iron Carbon system, Important furnaces for purification of metal. Alloys: Objectives of alloying, properties of alloys, Classification of alloys, approximate compositions. Applications of Nickel steel, chrome steel, Chrome nickel steel, Bronze, brass, Bell metal, Gun metal Monel metal, German silver Duralumin, Bearing metal Hastelloy (i.e. Non ferrous alloys, Copper alloys Aluminium alloys, Nickel base Alloys Lead base alloys) Working pressure for Metal, soldering of metal welding of metal.

Chapter 4. Corrosion & its preventionDefinition, Types of corrosion Electrochemical Corrosion Galvanic corrosion hightemp. Corrosion Factors influencing corrosion methods for protection against corrosion, Laboratory & Plant corrosion test selection of materials.

Chapter 5. Ceramic materialsDefinition properties & application of clay, Fire clay bentonite, Glass, raw material of Glass, mfg. of glass types of glasses their properties & uses Porcelain general properties, Composition and uses, Cement – properties & application.

Chapter 6. Polymer materialsPolymer & their structure Addition & Condensation Polymerisation plastics Definition properties of plastics, classification of plastics, Rubbers – Definition classification, sources, properties & uses of natural & synthetic, rubber, vulcanizing wood, properties, general idea about seasoning its advantage & Limitation.

Chapter 7. LubricantsImportance and classification of lubricants, properties and application of synthetic & semisolid lubricants method of applying lubricants

Chapter 8. Special application materialsInsulation materials properties & application of various electric, thermal, sound, Insulation materials. Adhesives- definition, classification of Adhesives, advantages & limitation of Adhesives.

Chapter 9. Packing materialsObjectives of packaging, requirement of Packaging materials, properties and uses of paper, aluminium foil & card board



(126202) INTRODUCTION TO PETROCHEMICAL TECHNOLOGY



CREDITS:-05 L-T-P 5 - -

Chapter 1. Introduction to Petrochemical Refining Indian Refineries,Their location and capacity Global crude oil producers, Characteristics of crude, Composition, constituents of crude oil Chapter 2. Refining Process of Refining of crude oil to obtain various fractions

Unit operations used in separation processess-Fractionation,Vacuum Distillation List of Hydrocarbons/fractions obtained, their Boiling Ranges and

Their uses Chapter 3. Unit Processess in Refineries: Flow charts,

reactions,DescriptionHydrogeneration,cracking,Alkylation,PolymerisationHydrocracking.Isomerisatiopn,Reforming,Esterifiaction & HydrationsssWaste Treatment

Chapter 4. C1 to C4 Hydrocarbons: C1 Hydrocarbons, Petrochemicals from C1C2 Hydrocarbons, Petrochemicals from C2C3 Hydrocarbons, Petrochemicals from C3C4 Hydrocarbons, Petrochemicals from C4Aromatic Fractions

Chapter 5. Hazard & SafetyHazard in Petrochemical IndustrySafety in Petrochemical Industry

(126203)Chemical Engineering DrawingCREDITS:-04

L-T-P



2 - 4

Chapter 1. Symbols for process flow diagrams utility line diagram, Block

diagrams. Piping & instrumentation diagram.Chapter 2. Sketch of – various types of valvesChapter 3. Sketch of shell & tube heat exchanger Types of heat exchanger

flow arrangement. Tubes & tube shell layout shell & tube side passesChapter 4. Tray tower & packed towerFractionating column – shell, head, support, tray types downcomer, & weirs, flow Pattern on trays feed systems, vapour outlet, Bottom outlet, manhole, ladder, Platform Packed tower – Types of packing, liquid collector, liquid distributor.Chapter 5. Sketch of storage tanks – Fixed roof tank, floating roof tank,

Horton sphereChapter 6. Reaction vessels – Heating & cooling systems, jackets, coils,

agitator, ImpellersChapter 7. Supports & HeadsSupport – Bracket skirt, saddle. Heads – Plain formed head, flared & dished head, shallow dished head, Torispherical dished head elliptical head, Hemispherical head, conical headChapter 8. Sketch of evaporator calendriaChapter 9. Sketch of different types of pumpsChapter 10. Sketch of plate & frame filter press, Rotary filter.

Student will prepare sketch / Drawing on the topics listed. Student on half-imperial size drawing sheet should prepare minimum 10 drawings/ sketches.



(120206) APPLIED PHYSICS- II(PRACTICAL)

Credits 01 L T P - - 2

LIST OF PRACTICALS OF PHYSICS (To perform minimum eight experiments)

1. To find the focal length of convex lens by displacement method.2. To determine the magnifying power of an astronomical telescope

3. To verify ohm’s laws by drawing a graph between voltage and current.

4. To verify laws of resistances in series and in parallel connection.

5. To find resistance of galvanometer by half deflection method

6. To measure very low resistance and very high resistance using Wheat Stone bridge

7. To determine the capacity of a parallel plate capacitor by discharging through a voltmeter and also find out the tine constant of the given capacitor.

8. To draw characteristics of a pn junction diode and determine knee and break down voltages

9. To find wave length of He Ne semiconductor LASER.

10.Use of CRO in plotting AC/DC



(121202)BASICS OF INFORMATION TECHNOLOGYCREDITS:-02

L-T-P - - 4

LIST OF PRACTICALS

1. Given a PC, name its various components and peripherals. List their functions 2. Practice in installing a computer system by giving connection and loading the

system software and application software 3. Exercises on entering text and data (Typing Practice) 4. Installation of operating System viz. Windows XP, Windows 2007 etc..

Features of Windows as an operating system Start Shutdown and restore Creating and operating on the icons Opening closing and sizing the windows Using elementary job commands like – creating, saving, modifying,

renaming, finding and deleting a file Creating and operating on a folder Changing setting like, date, time, colour (back ground and fore ground) Using short cuts Using on line help

5. MS-Word File Management: Opening, creating and saving a document, locating files, copying contents

in some different file(s), protecting files, Giving password protection for a file

Page Set up: Setting margins, tab setting, ruler, indenting Editing a document: Entering text, Cut, copy, paste using toolbars Formatting a document:



Using different fonts, changing font size and colour, changing the appearance through bold/ italic/ underlined, highlighting a text, changing case, using subscript and superscript, using different underline methods

Aligning of text in a document, justification of document ,Inserting bullets and numbering

Formatting paragraph, inserting page breaks and column breaks, line spacing

Use of headers, footers: Inserting footnote, end note, use of comments Inserting date, time, special symbols, importing graphic images, drawing

tools Tables and Borders: Creating a table, formatting cells, use of different border styles, shading in

tables, merging of cells, partition of cells, inserting and deleting a row in a table

Print preview, zoom, page set up, printing options Using Find, Replace options Using Tools like: Spell checker, help, use of macros, mail merge, thesaurus word content

and statistics, printing envelops and lables Using shapes and drawing toolbar, Working with more than one window in MS Word, How to change the version of the document from one window OS to

another Conversion between different text editors, software and MS word

6. MS-Excel Starting excel, open worksheet, enter, edit, data, formulae to calculate

values, format data, create chart, printing chart, save worksheet, switching between different spread sheets

Menu commands: o Create, format charts, organise, manage data, solving problem by

analyzing data, exchange with other applications. Programming with MS-Excel, getting information while working

Work books: o Managing workbooks (create, open, close, save), working in work

books, selecting the cells, choosing commands, data entry techniques, formula creation and links, controlling calculations, working with arrays



Editing a worksheet, copying, moving cells, pasting, inserting, deletion cells, rows, columns, find and replace text, numbers of cells, formatting worksheet

Creating a chart: o Working with chart types, changing data in chart, formatting a

chart, use chart to analyze data Using a list to organize data, sorting and filtering data in list Retrieve data with query: Create a pivot table, customising a pivot table.

Statistical analysis of data Exchange data with other application: embedding objects, linking to other

applications, import, export document.

7. MS PowerPoint

Introduction to PowerPoint - How to start PowerPoint - Working environment: concept of toolbars, slide layout,

templates etc. - Opening a new/existing presentation - Different views for viewing slides in a presentation: normal,

slide sorter etc.Addition, deletion and saving of slides Insertion of multimedia elements

- Adding text boxes - Adding/importing pictures - Adding movies and sound - Adding tables and charts etc. - Adding organizational chart

Formatting slides - Using slide master - Text formatting - Changing slide layout - Changing slide colour scheme - Changing background - Applying design template

How to view the slide show? - Viewing the presentation using slide navigator - Slide transition - Animation effects etc.

8. Working with MS AccessUnderstanding different data typesCreation of tableEntering data in a table and modify it.Creating simple Queries



9. Internet and its ApplicationsLog-in to internet Navigation for information seeking on internet Browsing and down loading of information from internet Sending and receiving e-mail

- Creating a message - Creating an address book - Attaching a file with e-mail message - Receiving a message - Deleting a message



(126204)Chemical Engineering MaterialsCREDITS:-01 L-T-P

- - 2

Experiments1. Use of metallurgical microscope2. Measurement of corrosion of metal in Acid and alkaline media 3. Measurement of Hardness of metal4. Froth flotation5. Demonstration of

Ceramic materials Plastic materials Lubricants Adhesives Insulation materials Metals & alloys Ores for metals Packaging materials

6. Identification of materials



(120208) WORKSHOP PRACTICE – II Credits 03 L T P - - 6

DETAILED CONTENTS (PRACTICALS)

The following shops are included in the syllabus:

1. Welding Shop 2. Electronic Shop3. Sheet Metal Shop

Note: The contents of various shops prescribed under workshop Practice –I are same as that of General Workshop Practice-I which is common for most of engineering diploma programmes except for Computer Engineering and Information Technology.The instructor is to first explain the introductory part given at the beginning under each shop followed by demonstration and practice by students.

1. Welding Shop

1.1 Introduction to welding and its importance in engineering practice; types of welding; common materials that can be welded, introduction to welding equipment e.g. a.c. welding set, d.c. rectifier, Electrode holder, electrodes and their specifications, welding screens and other welding related equipment and accessories.

1.2 Electric arc welding, (ac. and dc.) precautions while using electric arc welding, Practice in setting current and voltage for striking proper arc.

Job I Practice of striking arc while using electric arc welding set. Job II Welding practice on electric arc welding for making uniform and

straight weld beads

1.3 Various types of joints and end preparation.

Job III Preparation of butt joint by electric arc welding. Job IV Preparation of lap joint by electric arc welding. Job V Preparation of corner joint by using electric arc welding. Job VI Preparation of Tee joint by electric arc welding.

2. Electronic Shop

2.1 Identification and familiarization with the following tools used in electronic shop:



Tweezers, Screw drivers (different sizes), Insulated Pliers, Cutter, Sniper, Philips Screw Driver (Star Screw Driver), L- Keys, Soldering Iron and their demonstration and uses.

2.2 Identification and familiarization with the following electronic instruments:

a) Multimeter analog and digital (Three and half digit) b) Single beam simple CRO, Signal Generator and Function

Generator; function of every knob on the front panel c) Audio-oscillator having sine and square wave output d) Regulated Power supply -- fixed voltage and variable voltage,

single output as well as dual output. Job I Practice in the use of above-mentioned equipment. For this small experimental as set up may be done

2.3 Various types of protective devices such as : Wire fuse, cartridge fuse etc.

2.4 Identification and familiarization with ear phone speaker connector, telephone jacks and similar male and female connectors

2.5 Safety precautions to be observed in the electronic shopNOTE: Demonstration Boards for the above components should be

made. Job II Cut, strip, join and insulate two lengths of wires/ cables (repeat with different types of cables/wires)

Job III Cut, strip, connect/solder/crimp different kinds of wires/ cables (including co-axial and shielded cable) to different types of power/general purpose/Audio Video/Telephone plugs, sockets, jacks, terminals, binding posts, terminal strips, connectors. The tasks should include making complete recording/ playback/ antenna/ speaker leads for common electronic products such as Radio, TV, CD Players, VCD/DVD Players, Cassette Recorder and Players, Hi-Fi equipment, Hand- set, microphone

Job IV Cut, bend, tin component, Leeds, inserts and solder components (resistor, capacitor, diodes, transistors, FETs, IFT coils, ICs etc) on a PCB

3. Sheet Metal ShopIntroduction to sheet metal shop, use of hand tools and accessories e.g. different types of hammers, hard and soft mallet, sheet and wire gauge, necessary allowance required during job fabrication, selection of material.

3.1 Introduction and demonstration of hand tools used in sheet metal shop.3.2 Introduction and demonstration of various machines and equipment used in

sheet metal shop e.g. Shearing Machine, Bar Folder, Burring Machine, Turning Machine, Wiring Machine, Setting Down Machine, Forming Machine , Brake etc.3.3 Introduction and demonstration of various raw materials used in sheet

metal shop e.g. black-plain sheet, galvanized-iron plain sheet, galvanised corrugated sheet, aluminium sheets etc.

3.4 Study of various types of Nuts, Bolts, Rivets, Steel Screws etc.



Job I Shearing practice on a sheet using hand shears. a) Practice on making Single riveted lap joint/Double riveted lap

Joint.b) Practice on making Single cover plate chain type, zig-zag type

and single rivetted Butt Joint



(126205)INTRODUCTION TO PETROCHEMICAL TECHNOLOGY

CREDITS:-01 L-T-P - - 2

Practical:Skills to be developed:Intellectual Skills:

Interpret test resultFollow systemic procedure for handling chemicals

Motor Skills:To handle equipments/instrumentsTo observe physical phenomenon

List of Practical:-1. Determination of Aniline Point.2. Determination of Fire Point, Flash Point.3. Determination of calorific value.4. Determinaton of viscosity index.5. Preparation of Ethyl Acetate by Esterification.6. Preparation of Resin.7. Preparation of Biodiesel by Transesterification.8. ASTM, TVP Distillation.9. Determination of Drop Point.10. Determination of Pour Point.



3RD SEMESTER SYLLABUS

126301 CHEMICAL ENGINEERING–I MECHANICAL OPERATION

Credits:-03 L T P 3 - -Chapters:

1 Introduction - Definition of unit operation & unit process Difference of unit operation & unit process with examples.

2.

a) Characterisation of solid particles – Particle shape sphericty (shape factor) particle size, calculation of equivalent particle diameter, specific surface area, volume surface mean diameter, mass mean diameter, simple calculation of propertiesb) Screening – standard screen series, cumulative analysis, differential analysis, Sieve shaker, Definition of ideal & actual screen capacity and effectiveness of screen. Types of screens- Grizzlies, Trommels, Gyratory screen, Vibrating screens. Simple calculation on capacity and effectiveness of screen

3.

Size reduction (Comminution)a)Criteria for size reduction characterisitics of comminuted products, particle size distribution, energy and power requirement in crushing, work index, laws of crushing, Rittinger's law, Bond's law, Kick's law, Simple calculation of power for size reductionb)Size reduction equipment - Crushers, Jaw crushers, Roll crushers, Angle of nip, Ribbon factor, capacity of Roll crusher, Gyratory crusher, Grinder, Hammer Mill, Ball mill, Attrition mill, Critical speed of Ball mill. Ultrafine grinders - Fluid energy mill cutting machines - Knife cutters, Open and close circuit grinding, Introduction to size enlargement.

4.

Agitation and Mixing of liquids :Definition of agitation & mixing and their Applications. Equipment for agitation, Purposes of agitation, Types of impellers, Propeller, paddle, Turbine Anchor, equation for power consumption in agitation, flow Patterns in agitated tanks, Baffles, Vortex prevention, flow number, Factors affecting agitation. Simple problems on calculation of power in Agitated vessels.

5.Mixing of solids : Purposes of mixing solids & pastes factors affecting selection of equipment, rate of Mixing, mixing index for pastes & powder Principle construction & working of change Can mixer, Kneaders, ribbon blender, Pug mill, Banbury mixer, Muller mixer, Double Cone mixer.

6. Filtration : Definition & application of filtration, factors affecting selection of equipment, Filtration equipment – plate & frame filter press, shell & leaf filter, vacuum filter, rotary drum filter (pre coat), centrifugal Filtration, centrifuge, cartridge filter, filter media & its characteristics, filter aids and methods of application, precoating Principles of cake filtration, constant pressure & constant rate filtration. Filter medium resistance specific cake



resistance simple calculation of and Rm principles, of centrifugal filtration.

7.Sedimentation: Definition – Batch sedimentation rate of Sedimentation height of inter phase & time curve. Flolculation Thickners, Gravity Setting processes. Sink & float method. Differential settling methods, Free & Hindered Settling, definition of Stoke's law, Newton’s Law for terminal settling velocity.

8Separation based on property (solid particles) Definition & application of solid separation, Factors affecting selection of equipment, Froth Floatation, Jigging, Magnetic separation, Electro static precipitator, Cyclone separator, Hydro cyclone, Centrifugal classifier, Bag filter.

9.Conveying of solids( Conveyers) : Vertical & horizontal transport, Belt Chain, screw, pneumatic conveyor Bucket elevator Industrial application of conveying .



125312 ELECTRICAL ENGINEERINGCREDITS:-02

L T P 2 - -

Chapters:1 Introduction

Magnetic circuits, Basic concepts2 A.C. fundamentals3. AC Machines4. D.C. Machines5. Measuring instruments, Types of meters & their application and tariff.6. Introduction to distribution of power

7.Important electronic devices BJT, SCR, TRIAC, DIAC, Photo diode Phototransistors photo voltaic cell LED,Construction, operation, characteristics and application, SCR, Introduction to OPAMP principle & Application of H.F. heating.

8 Digital circuits Logic gate, universal gates Testing of gates of various IC’s like 7400, 7404 etc.

9. Introduction to microprocessor application



126302 ENGINEERING MECHANICS - ICREDITS:-03

L T P 3 - -Unit. Topic

1.Fundamental of Applied MechanicsFundamental unit, Derived units, system of Units, scalar & vector quantities, introduction to applied mechanics.

2. Force – Force characteristics of force, system of forces, fundamental principles of transmissibility effect of force.

3.

Coupling concurrent force systemResultant & equilibrantforce, Equilibrium of aCoplanar concurrent force system, Analytical Method, parallelogram & Lamis theorems Composition and resolution of forces. Bow's Notation Graphical method laws of parallelogramTriangle & polygon of force.

4.Moment & coupleMoment, Types of moment, couple & characteristicOf couple Varignon's theorem of moment. ConditionsOf equilibrium for coplanar non-concurrent forces.

5.

Coplanar non-concurrent forcesParallel force system, resultant of parallel forceSystem by Graphical & analytical method,Resultant of coplanar non concurrent & nonParallel forces by analytical method & graphicalMethod.

6.Support reactionTypes of supports, types of loads, support reaction by graphical and analytical method for simply Supported beam, over hanging beam and roller And hinged beams Reaction of perfect frame.

7.

Centroid – Centre of gravity & moment of inertia Centre of gravity, centroid of composite geometrical Figures, centre of gravity of solid body, modules of selection, moment of inertia radius of gyration, theorem of parallel axis, moment of inertia radius of gyration, theorem of parallel axis, moment of inertia of rectangle, triangle, circle, symmetrical I section & II sections.

8.Friction – Static, dynamic, & limiting friction Rolling & sliding friction, normal reaction, coefficient of friction, angle of friction and angle of repose laws of friction. Friction along various plane ladder friction wedge friction & screw jack friction.



126303 GENERAL CHEMICAL TECHNOLOGYCREDITS:-03

L T P 3 - -



Unit Topics1. Introduction: Concept of chemical industries Flow diagrams & symbols

used in flow Diagram.

2. Inorganic chemical industries: Manufacturing of sulphuric acid, Nitric acid, Hydrochloric acid, Phosphoric acid, their raw Material, properties.

3 Caustic soda & chlore alkali industries: Manufacturing of caustic soda, soda ash, & Chlorine.

4 Plant utilities : Water & its treatment, D.M. water, Boiler water, Air and it uses.

5. Industrial gases : Manufacturing of industrial fuel gases, water gas, producer gas, with properties & application.

6.Natural product industries: Manufacturing of soap, detergent, constituents of Oil, fat & wax, vegetable oil, difference between soap & detergent.

7. Carbohydrate & fermentation industry : Extraction of sugar cane for crystalline sugar Production, starch, ethyl alcohol by fermentation.

8.Pulp paper & Rayon industry: Cellulosic raw materials, manufacturing of paper Pulp sulphite & sulphate pulp process. Manufacturing of paper and viscose rayon.

9. Pharmaceutical Industry: Introduction, Types of drugs, Antibiotics, Classification of drugs based on chemical process.

10. Manufacture of cement lime, Glass, paint &varnishes

11. Dyes & intermediates : Raw materials, uses, classification of dyes Natural dyes

12. Miscellaneous industries: Agro base chemical industries & pesticides

13. Introduction to coal base, petroleum base& fertilizer industries



123310 MECHANICAL ENGINEERINGCREDITS:-03

L T P

3 - -Chapters:

1. Power transmission systems - Introduction Types of power transmission system, Characteristics of power transmission system, Mechanical drives comparison of various, Mechanical drives.

2. Belt & rope drives - Construction, specification, selection, Application of Belts, V Belts, Rope & Pulley Open & cross belt drives velocity ratio, slip, Methods of minimizing slip, Ratio of tension in the belt, V Belt, Rope drives, Initial tension centrifugal tension, HP transmitted, Belt speed, simple problems based on Belt & rope drives.

3. Chain drivesTypes of chain their selection, Application Constructional feature of roller & silent chains & sprockets, kinematics of chains

4. ClutchesConstructional features of single plate, Multiplate cone and centrifugal clutches

5. Fly WheelsFunction of Fly wheels, Uses of Fly wheels

6. CouplingsSleev or muffle coupling, Flange coupling , Marine type coupling, Flexible coupling, Hook coupling, Selection & application of coupling

7. BrakeIntroduction, types of brake, Calculation of braking torque

8. Gear drivesIntroduction, classification of gears Gear terminology & application, calculation of centre distance, no. of teeth speed ratio for simple gears, compound reverted and epicyclic, gear trains. Construction of single and multistage gear boxes for various types of gear.

9. I.C. Engine – classification of IC engine, two strokes four stroke engine explanation of IHP, BHP machine

10. Boilers & steam engineclassification of boilers, high pressure modern boiler. Accessories & mountings of boiler of steam engine & their components, economizer.

11. Steam turbineclassification of steam turbine, construction and Working of impulse & reaction steam turbine, steam nozzles

12. Mechanical seals



126304 ORGANIC CHEMISTRY

CREDITS:-03 L T P

3 - -

Chapters:

1. Stereo chemistry: Isomerism: geometrical & Optical.

2. Grignard's reagent - Organometalic compounds properties & uses.Girgnard reagent as an important tool for organic synthesis

3.Aliphatic compounds- Chemical reactions involved in methods of preparation, Properties & uses of Ketones, Aldehydes, Halogens carboxylic acids, esters, Aminocompounds.

4.

Aromatic Compounds.Difference between Aliphatic & Aromatic, Chemical reaction involved in preparation of aromatic compounds, properties & uses, Benzene & its homologous, Halogen derivatives of aromatic compounds, e.g. chlorobenzene , sulphonic acid e.g. Benzene sulphonic acid, Aromatic nitro compounds e.g. Nitrobenzene, amino compounds e.g. aniline, Aromatic carboxylic acids e.g. Benzoic acid, Aromatic Aldehydes & Ketones e.g.,Benzaldehyde, Polycylic & Heterocyclic aromatic compounds.

5.

Aromaticity of Benzene: Stability of benzene ring, Nomenclature of Benzene derivatives, reaction, mechanism of aromatic, Substitution electrophilic substitution, Nucleopholic addition Explain- Nitration, Sulphonation, Oxidation Reduction, Halogenation, Amination giving examples.

6 Cycloparaffins, Stability of cyclic compounds



126305 CHEMICAL ENGINEERING–I MECHANICAL OPERATION

CREDITS:-01 L T P

- - 2

Experiments –1. Sieve shaker – cumulative analysis – Differential analysis 2. Roll crusher – calculation of theoretical capacity, Ribbon factor, Angle of nip,

Reduction ratio, Power calculation.3. Ball Mill – calculation of critical speed, operating speed, Application of Rittinger’s law in ball mill.4. Settling rate calculation by sedimentation.5. Calculation of and Rm in vacuum filtration.6. Study of plate & frame filter press, filtration and washing in filter press7. Rate of filtration by gravity filtration.8. Efficiency of separation in froth floatation.9. Calculation of power consumption in agitated vessel. 10.Efficiency of separation in cyclone separator 11.Calculation of viscosity by stokes law using terminal velocity equation.12.Test kick’s law in Jaw crusher.Student should perform minimum 10 experiments.



125313 ELECTRICAL ENGINEERINGCREDITS:-02

L T P

- - 2

Laboratory Exercises 1. R.I. series circuit2. RC series circuit3. Study of starter 4. Speed control / DC motors5. study of CRO & its application6. Testing & application of BJT, SCR, TRAIC, Photo diode photo transistor photo

voltaic cell, LED1. Transistor as an amplifier2. Testing of gates of various IC’s like 7400, 74043. Simple programme using micro processor



126306 ENGINEERING MECHANICS - ICREDITS:-01

L T P

- - 2

Experiments.1. Verification of the following laws:-

Triangular law of forces Parallelogram law of forcesPolygon law of forces

2. To Verify the reaction at the support of simply supported beam3. To find out center of gravity of regular lamine4. To find out center of gravity of irregular lamina5. To determine coefficient of friction b/w three pairs of given surface6. To verify the reactions at the supports of overhanging beam7. To find coefficient of friction for sliding & rolling pair8. To find coefficient of friction for inclined plane9. To find resultant of parallel forces 10. To find resultant of coplaner non parallel,non concurrent forces



126307 GENERAL CHEMICAL TECHNOLOGYCREDITS:-01

L T P

- - 21. Available chlorine in bleaching powder 2. Temporary & permanent hardness in water3. Chloride in water4. Preparation of azodye5. Preparation of Aspirin6. Preparation of Soap7. Preparation of detergent8. Preparation of Boric acid9. Preparation of Alum10. Preparation of nitrobenzene11. Saponification value of oil.12. Properties of boiler feed water and (D.M.water) Minimum 10 experiments should be performed by student.



123311 MECHANICAL ENGINEERINGCREDITS:-01

L T P

- - 21. Troubleshooting in Braking system2. Fault diagnosis in transmission system including clutch,gear drive3. To determine velocity ratio of belt drive system4. Study of various power transmission system5. Study of flywheel6. To study 2 stroke & 4 stroke petrol engine7. To study 2 stroke & 4 stroke diesel engine8. Study of lubricating system of I.C. engine9. Study of various parts of compressor10.Study of - boilers (through industrial visit) - compressors - Steam turbines.



126308 ORGANIC CHEMISTRY CREDITS:-01

L T P

- - 21. Determination of melting point of an organic compound2. Determination of boiling point of an organic compound3. Distingiush between aldehydes & ketones by tollen’s reagent4. Crystallisation of impure sample of any of the following alum , bezoic acid5. Determination of nitrogen,sulphur,chlorine,bromine & iodine in an organic

compound6. Preparetion of iodoform from ethanol or acetone7. Detection of functional groups

(esters,phenolic,amines,carboxylic,nitro,aniline) in simple organic compound8. Separation of two compound mixtures benzoic acid + benzophenone9. Distinguish between aliphatic & aromatic compound10.To Prepare a pure sample of dibenzalacetone from benzaldehyde & acatone



126309 WORKSHOP PRACTICE III

CREDITS:-03 L T P

- - 6

Only demonstration of rolling, making of cylindrical Shell, welding Argon welding, plasma cutting, S S Welding, welding machine, welding Rods, soldering & brazing.



4TH SEMESTER SYLLABUS

126401 CHEMICAL ENGINEERING–II FLUID FLOW OPERATION

CREDITS:-04 L T P

4 - -

Chapters: 1. Introduction : Dimensional analysis – Dimensional equation

Dimensionally Homogeneous equation.Dimensionless groups & their significance

2. Fluid static & its applications: Introduction to statics & dynamics Nature of Fluid, pressure concept, Hydrostatic equilibrium, Barometric equation, Types of fluids Compressible, Incompressible, Manometers, 'U' tube Inclined tube, differential, Continuous gravity Decanter centrifugal decanter simple Calculation of pressure drop in manometer.

3. Fluid flow phenomena: Potential flow Laminar & Turbulent flow, Reynolds experiment velocity gradient & Viscosity, Momentum flux, kinematic viscosity Newtonian and non Newtonian fluids their Examples, Boundary layer separation & Wake formation.

4. Basic equations of fluid flow: Continuity equation of mass balance; Define; Mass velocity, Average velocity Bernoulli’s equation correction factor in Bernoulli’s equation, Kinetic energy correction, correction for fluid friction, pump work in Bernoulli’s equation.

5. Flow of incompressible fluids in pipes (friction in flowing fluid) : Flow of Incompressible fluid in pipes, Hagen poiseuille equation friction factor, relation between skin friction parameters, relation between maximum average velocity. Velocity distribution in pipe, effect of roughness in friction, friction loss from sudden expansion, sudden contraction friction loss in fittings & valves, equivalent, diameter, Hydraulic radius equivalent length, fully developed flow.

6. Flow measurement Orifice meter : Venturimeter, Pitot tube, Rotameter, Weirs and notches, Flow nozzlePrinciple, construction, working installation, Merits & Demerits calculation of flow in meters (simple calculation no derivation of equation.)

7. Transportation of fluids: Pipes, tubes, pipe fittings, specification of Pipes & tubes (schedule number BWG) Joining of pipes & tubes. Valves- Gate valve, Globe valve, plug cock, Ball valve, check Valve, safety valve, Butterfly valve, steam Traps devices for leakage prevention around Moving parts, stuffing box Mechanical seal.

8. Fluid moving machinery:a) Pumps capacity of pumps, Head developed efficiency of pump work done by pump BHP, FHP suction lift, Cavitation & NPSH, simple calculation of power in C.F. pump, performance, Characteristics of C.F. pump, losses in C.F.pump, Principle construction & working of C.F. pump, Installation of C.F.pump, uses of C.F. pump



b) Positive displacement Pumps- (Description & uses), reciprocating pump, Gear pump, plunger pump, vacuum pumps, steam jet ejectors, Acid egg, Air lift pump.c) Fans Blowers & Compressors – Description & uses

9. Fluidisation- Introduction, Concept of fluidisation, types of fluidisation, Application of fluidisation, Minimum porosity, pressure drop in bed, simple problems on fluidisation.

126402 ENGINEERING MECHANICS – IICREDITS:-04

L T P

4 - -



Chapters:1 Linear and angular motion Mechanics, Dynamics, Kinetics and Kinematics

Rectilinear motion displacement, speed velocity, acceleration, equation of Linear action with uniform acceleration, Velocity time diagram angular motion, Rotation, angular displacement angular velocity, angular acceleration, relation between linear and angular motion, equation of angular motion with uniform acceleration.

2 Force Mass Acceleration and work power energy, types of energy, Newton's laws of motion, Relation between force, mass acceleration. Definition of work power, energy, types of energy, conservation of energy.

3. Lifting machines and power transmission Law, definitions, Mechanical advantage, velocity ratio, efficiency, Law of machine, friction in the machine, Maximum efficiency and reversibility machine, some types of lifting machine such as inclined plane, simple wheel and axle, wheel and differential axle, worm and worm wheel and screw jack and their velocity ratio, power transmission, individual drive an drop group drive belt and pulley drive, driver, follower and idler, cross and belt, transmission belt, slips and its consideration, centrifugal tensile gear transmission various types of gear used, gear transmission.

4. Simple stress and strain and elastic constants, elasticity stress, strain, types of stress, working stress, Factor of safety. Young's Modulus of elasticity. Deformation ofbody due to forces acting on it. Principles of superposition stress in bars of varying action and bars of composite section stress due to change in temperature.Linear and lateral strain, Poission's ratio volumetric strain, Bulk modulus. Modulus of rigidity Relation between E.G.K.

5. Bending Moment, shear force and bending stress Definition of bending moment and shear force. S.F. & B.M. diagram cantilever and simply supported beams loaded with point load and U.D.L. point of contraflexure theory of simple bending, assumptions in the theory of simple bending. Bending stress equation.

EquationM F E

--- = --- = ----I Y R

Neutral axis moment of resistance, Distribution of bending stresses in symmetrical and unsymmetrical section.

6. Thin cylindrical and spherical shells.Thin cylindrical and spherical shells, stress in cylindrical stress, design of cylindrical shell change in dimension of cylindrical shell due to internal pressure, thin spherical shell, change in the diameter and volume of thin spherical shell due to internal pressure.

7. Torsion – shafts subjected to Torsion – Deisgn of simple couplings.



126403 FERTILIZER TECHNOLOGYCREDITS:-04

L T P

4 - -Chapters:

1.IntroductionNeed of fertilizer, Types of fertilizers, Merits & Demerits of fertilizers, Natural fertilizers, Application of fertilizers Fertilizer industry in Gujarat, India & World.

2. Nitrogenous fertilisersa) Ammonia sources of Nitrogen & Hydrogen steam reforming, partial oxidation

of RFO, synthesis gas preparation properties, purification and synthesis of ammonia, Ammonia converters.

b) Urea – Physicochemical properties raw material, effect on conversion of process parameters changes, total recycle process steam carbon striping process, Snamprogetti process material of construction of urea reactor.

c) Ammonium Nitrate – Physicochemical and agrochemical properties, manufacturing process material of construction, different neutraliser’s storage & handling.

d) Ammonium Sulphate – Physicochemical properties and agrochemical properties, manufacturing process from Gypsum & as a by-product of caprolactum.

e) Sodium & Potassium Nitrate – Properties & manufacturing process.3. Potassium fertilisers

Significance of it to the plant life natural sources, properties of potash, potassium fertilisers like potassium sulfate, potassium bisulfate, potassium trisulfate, potassium hydroxide potassium chloride.

4. Phosphatic fertilizersSignificance to the plant life, classification sources types of rock phosphate, its composition, mining & processing of rock phosphate, manufacture of simple super phosphate, calcium phosphate, Nitrophosphate . Engg. Problems in different Processes. Concentrated or triple super phosphate, Manufacturing process construction & Working of cyclone mixer.

5. Compound fertilisersClassification properties, Ammonium phosphate, Diammonium phosphate, Nitrochalk ,trace elements, other ingredients micronutrients.

6. Introduction to bio fertilizers.



126404 PHYSICAL & ANALYTICAL CHEMISTRYCREDITS:-04

L T P

4 - -Chapters:

1. State of matter – Solid Liquid & Gas their properties – Physical properties of liquids types of physical properties & characteristics of each properly. Definition of surface tension, refractive Index, Molar refraction ,specific refraction viscosity ,Molecular viscosity ,surface tension & Viscosity measurement methods, Ostwald Viscosity, stalagmometer.

2. General Gas Laws & Atomic TheoryKinetic theory of gases. Deviation from gas Law, Reduced Vander waal's equation of state, Critical properties, Phenomenon of liquefaction of gases.

3. Ionic equilibria :Introduction sparingly soluble salts, Acids & Bases Hydrolysis, Hydrolysis constant, Buffer Solution, Acid base titrations,

4.Colloids & EmulsionColloids & its various aspects, characteristics of true solutions, suspension & colloidal solution. Classification of colloids difference between Lyophobic, Lyophillic solutions methods, preparation of colloidal solutions, condensation & dispersion methods, purification of colloidal solution, Dialysis ultra filtration, properties of colloidal solution, scattering of light colour charge, Electro osmosis protection, Brownian movement, electrophoresis co-agitation. Phenomenon of emulsion. Definition of Emulsion, types of cleansing action of soap, Advantages of synthetic detergent over alkali Soap, properties & utility of gels.

5. Adsorption : Langmuir's adsorption theorem Gibbs adsorption equation, solid liquid, Liquid – liquid interfaces .

6. Chemical Thermodynamics: Systems, State & state functions, work & heat, First law of thermodynamics, Thermo chemistry, Entropy & free energy, Gibbs-Helmholtz, Clapeyron Equation, Isotherm & Isochore, standard free Energy & its utility Free energy, Temp. Dependence of equilibria:

7. Chemical Kinetics: Classification of reactions. Reaction mechanisms Concentration effect temp. effect, reaction Velocity order of reaction, expression & Determination.



8.Electrometric– methods of analysis : Electrode types of electrode distinguish between Inert electrode working electrode reference electrodevarious electrometric methods. pH metry definition of pH, POH & their relationship, std oxidation potential functions of hydrogen electrode calomel electrode, glass Electrode Ag/AgCl/KCl electrode quinhydrone, Electrode. Problems of pH & POH calculation, Methods of determining pH by pH meter, by pH indicator, By potentiometer methods. Conductometery; definition of conductivity, Galvanic cell, concentration cell, specific, Conductance, cell constant, equivalent Conductance, molecular conductance, Conductivity of water.Conductometry titrations , acid base titration, Precipitation titration replacement titrations. Chromatography– Thin – layer Chromatography, Ion exchange,columnchromatography, Paper chromatography.

9. Qualitative & quantitative analysis: Common ion effect, Ionic product, solubility, solubility product, use of H2 & NH4Cl in qualitative inorganic analysis.



126405 PROCESS CALCULATION

CREDITS:-03

L T P

3 - -Chapters:

1. Dimensions & Units: Introduction. Importance of process calculation, Dimensions & system of units, Fundamental, Quantities, derived quantities conversion to FPS, MKS, & SI system, recommendation for Use of units.

2. Basic chemical calculations : Definition & basic calculations, Mole Atomic Weight, Molecular weight, Equivalent weight, Specific gravity API gravity composition of Solid & liquid weight %, mole %, properties of solution, Raoults law, Henry’s law Normality Molarity molality, gms/lit, PPM, TOC, THOD, BOD, COD.

3. Ideal gas law :Concept derivation of ideal gas, law definition of STP, NTP, Ideal gas law for mixtures Dalton’s law, Amagat’s law, relationship Between Mole %, Vol.%, pressure %, calculation of average molecular weight, density, mole %, Weight %, in SI/MKS system only, equation of State.

4. PsychrometryDefinition of DB and WB temp., Dew point Absolute humidity % humidity, relative Humidity, Humid heat, humid volume, vapour Pressure, partial pressure psychrometric chart Use of psychrometric chart simple problems Based on calculation of psychrometric Properties.

5. Material balance without chemical reactions:Introduction, process flow sheet principles of material simple balance, Recycling & By passing simple Problems based on material balance without Chemical reactions in various unit operations like Distillation Drying Absorption, Evaporation & crystallization extraction Leaching

6. Material balances involving chemical reactions:Introduction Definition of limiting reactant, excess reactant, Yield, conversion, calculation involvingChemical reactions i.e. yield conversion, Composition simple calculation of material balance based on chemical reaction, Electro Chemical reaction

7. Energy balancesa) Introduction- Definition of heat capacity Specific heat, relation

between CP CV & R, Numerical values of gas constant “R” Mean Heat capacity of gases calculation of Enthalpy of gases & gaseous mixture using heat Capacity data. Sensible heat changes in solids & liquids. Calculation of enthalpy of liquids & liquid mixture using heat capacity



of liquids. Calculation of enthalpy of solids.b) Calculation of enthalpy during phase change. Definition of latent heat

of fusion, latent heat of vaporisation, sublimation. Calculation of LHV, Watson equation, effect of temp. on LHV

c) Enthalpy changes accompanying chemical reactions standard heat of formation standard heat of reaction, standard heat of combustion Hess law of constant heat summation, Effect of temperature on heat of reaction, Effect of pressure on heat of reaction.

8. Combustion : Types of fuels, calorific values of fuels, brief idea about ultimate analysis & proximate analysis of solid fuel (coal) simple problems to find calorific value, calculation of air Requirement in combustion, Theoretical air, Excess air composition of fuel gases



126406 CHEMICAL ENGINEERING–II FLUID FLOW OPERATION

CREDITS:-02 L T P

- - 4

Laboratory exercises

1) Calibration of Orifice meter 2) Calibration of Venturimeter3) Calibration of Rotameter4) Verification of Bernoulli’s equation5) Reynolds experiment6) Friction in straight circular pipe 7) Friction in fittings8) Velocity measurement in pilot tube 9) Performance characteristics of C.F. pump10) Demonstration of pipe fittings, pipe, tubes, valves11) Flow in packed column 12) Study of C.F. pump & reciprocating pump, construction/parts Students should perform minimum 10 experiments.

126407 ENGINEERING MECHANICS - II



CREDITS:-01 L T P

- - 2

Experiments

1. To find mechanical advantage,velocity ratio & efficiency of an inclined plane2. To find mechanical advantage,velocity ratio of single purchase crab3. Tensile test on bars of mild steel & aluminium4. Bending test on a steel bar5. Torsion test on specimen of different metals for determining modules of

rigidity6. Impact test on metals

(a) Izod test(b) Charpy test

7. To find Mechanical advantage,velocity ratio & efficiency of screw jack8. To find Mechanical advantage,velocity ratio & efficiency of worm & worm

wheel9. To determine the stiffness of helical spring & to plot graph b/w load &

extension10. Study of various types of belts



126408 FERTILIZER TECHNOLOGYCREDITS:-01

L T P

- - 2

Laboratory Exercises –1. Sampling & sizing of fertilizer.2. To determine nitrogen content in given sample of urea by distillation method.3. To determine total nitrogen content in given sample of ammonium nitrate.4. To determine nitrogen content in given sample by formalin method.5. To determine K2O content in given sample of potash fertilizer.6. To determine P2O5 content in given sample of phosphatic fertilizers.7. To determine moisture content in given sample of urea.8. Preparation of Ammonium Sulfate.9. Preparation of Phosphatic fertilizers. To determine total P2O5 content in

phosphatic fertilizers.



121410 PERSONAL COMPUTER MAINTENANCE AND REPAIRCREDITS:-02

L T P

- - 4 LIST OF PRACTICALS

1. Introduction to Computer hardware and components2. Familiarization with PC assembling and dissembling.3. BIOS configuration and settings.4. Installation of Hard-Disk drive including partitioning and formatting.5. Familiarization with cables i.e. co-axial, UTP and fiber-optic cable and their

installation 6. Installation and configuration of dial-up networking for Broad band internet

7. Installation of Linux OS and other Windows operating systems 8. How to make an E-mail-ID on internet.9. Installation of a printer on different operating systems.10. Virsus – removal and use of vaccines down loads. (Symantec, Norton) etc.11. Installation of

(a) CD or DVD Drive(b) Sound card, Speaker and headphone

12. Recognition of USB port and other parts dike thumb drive or Card Reader etc.13. (a) Replacement of RAM

(b) Replacement of Power Supply



126409 PHYSICAL & ANALYTICAL CHEMISTRYCREDITS:-01

L T P

- - 2

Laboratory Exercises1. Determination of viscosity – By Ostwald viscometer 2. Determination of surface tension stalagmometer 3. Partition co-efficient 4. pH meter pH paper 5. Conductometry titration, HCl, NaOH 6. Conductometry titration NaCl, AgNO3 7. First order and second order kinetics 8. Refractometer



126410 PROCESS CALCULATIONCREDITS:-01

L T P

- - 2

Experiments:-1. Prepare a standard solution(N/25 or M/50) of oxalic acid. With its help

determine the normality (or molarity) & strength of given solution of KMnO4.2. Determine the percentage purity of ferrous sulphate (FeSo4 . 7H2O) in given

solution of known strength (15)3. Determine volumetrically the equivalent weight & the no. of water molecules

of crystallisation in a given sample of oxalic acid COOH.XH2O | COOH Provided N/20(or M/100) KMnO4 solution.4. To determine BOD of given sample5. To determine COD of given sample6. To determine the enthalpy of dissolution of solid cuso4.5H2O in water at room

temperature.7. Estimation of moisture in the given coal sample gravimetrically8. Estimation of ash in the given coal sample gravimetrically 9. Crystallisation of impure sample of Potash alum,K2SO4. Al2(SO4)3.2HH2O The

given solution has been prepared by dissolving O.S.G of an alkali metal permangenate in 500 cm3 of the solution.Determine volumetrically the atomic weight of alkali metal




126501CHEMICAL ENGINEERING III (MASS TRANSFER OPERATION)

CREDITS:-05 L T

P

5 - -

Chapters:1. Introduction – Introduction to Mass transfer Operation. Classification of

mass transfer operation, selection of separation method, Methods of conducting the Mass transfer operation, Factors affecting diffusional operation.

2. Molecular diffusion in fluids - Definition, Fick’s Law, Fick’s second law, Steady State Molecular diffusion in fluids at rest and in laminar flow. Molecular diffusion in gases Steady State diffusion of A through non diffusing B steady state equimolal Counter diffusion, diffusivity of gases effect of Temp. On diffusivity, Molecular diffusion in Liquid: Steady State diffusion of A through non diffusing B steady equimolal counter diffusion Diffusivity of liquids Steady State diffusion of solids.(Note- No derivation of equation use of equation with simple calculation) Uses of molecular diffusion.

3. Mass transfer co-efficientsDefinition of Flux, Mass transfer co-efficient, Brief idea of Mass transfer co-efficient in laminar flow, and turbulent flow Thermal diffusivity. Mass diffusivity, molecular diffusivity, conclusion of penetration theory, film theory, surface renewal theory. Corresponding dimensionless group of Mass Transfer & Heat transfer.

4. Inter Phase Mass TransferEquilibrium & Equilibrium distribution in curve, Briefidea about diffusion between phases definition of local mass transfer coefficient, relation between local & overall M.T. coefficient, material balance SteadyState Cocurrent process, Steady State counter current process define: stage, ideal stage, theoretical stage, Stage efficiency, cascade.

5. Equipment for gas liquid operation(a) gas dispersed equipments, agitated vessels, tray tower, definition of

flooding, loading, priming, tray spacing, tower diameter, down spouts weirs sketch of bubble cap tray Tray tower, Tray arrangements, sieve tray, entrainment, weeping, tray efficiency.

b) Liquid dispersed. Venturi scrubbers, wetted wall towers spray tower & Spray chambers, packed towers, types of packing, Characteristics of packing, sketch of packed tower, Packing arrangement: Random &



Regular packing Support, liquid distribution, flooding & loading Characteristics outline of diameter & pressure drop Calculation for packed tower.

6. Humidification OperationDefinition of various terms, uses of Clausis clapeyron Equation to calculate vapour pressure, vapour pressure curve 0 Define – saturated liquid, super heated liquid Triple point, critical point, critical pressure, critical Temperature, normal boiling point LHV, sensible heat. Vapour – gas mixtures Define – vapour & gas – partial pressure, absoluteHumidity, Molal absolute humidity, difference between saturated Vapour gas mixtures unsaturated Vapour gas mixture, Dry bulb temperature. Relative saturation, Dew point, Humid volume. Humid heat, Enthalpy, Importance of psychrometric chart for Air waterSystem, adiabatic saturation curves, wet bulb temp. Purposes of gas liquid contact operation, water Cooling tower, types, operation, performance, spray Ponds, spray chambers.

7. Absorption & Stripping.Definition of absorption & desorption, use of Solubility and equilibrium solubility curves, two Component system only, effect of temp. & Pressure on solubility, characteristics of ideal solution, Raoults Law, Non ideal solution, Henry’s law, Selection of solvent for absorption, material balance on counter current & cocurrent absorber & Stripper. Equilibrium and operating lines for Absorber & stripper. Minimum liquid/gas Ratio for absorption. Continuous contact equipment.Define – HETP, HTU, NTU Absorption factor, stripping factor Real trays, Simple calculation of MB & Number of stages in absorption, height of tower.



126502 CHEMICAL ENGINEERING IV (HEAT TRANSFER OPERATION)

CREDITS:-04 L T

P 4 - -

Chapters:1. Modes of Heat transfer

Introduction, nature of heat flow conduction Convection, radiation, Fourier law of conduction, Newton’s law of convection, Stefan Boltzman law of Radiation.

2. Heat transfer by conductionDefinition – Flux Temp. gradient, Fourier's law Thermal conductivity & its valuation with temp. , Thermal conductivity in solids, liquids & gases Thermal diffusivity, S.S.heat conduction through Single & composite wall, cylinder, sphere, thermal diffusivity.

3. Heat transfer by convectionIntroduction- Rate of heat transfer Heat flux Average temp. Newton's law of convection, Definition of overall H.T.coefficient, individual H.T. coefficient, Concept of Prandtl number, Nusselt number, Grashoff numbers, free, Convection, forced convection, Laminar & Turbulent flow in pipes & tubes – Sider & Tate Equation, Dittus Bolter equation.

4. Heat transfer for condensing vapours(Phase change)a)Boiling – Saturated boiling, pool boiling, Nucleate boiling, Heat flux Vs temperature Drop curve study, factors influencing the rate of heat transfer in boiling, subcooled boiling. b) Condensation- Film type condensation. Dropwise condensation, correlation for heat Transfer coefficient, condensing of super Heated vapours, effect of non condensable Gases on rate & condensation

5. Heat transfer by radiationStefan-Boltzmann’s law for total emissive Power, Heat transfer between bodies, concept of Absorption of emission, Black body, Grey Body, White body, Opaque body, Absorption, Transmission, reflection, emissive power of Black body, Planck’s law, emissivity, Kirchoff’sLaw, radiation shield, calculation of heat loss in atmosphere.



6. Heat transfer equipment.Heat transfer to fluid, concept of cocurrent & counter current flow, temperature range, and Log mean temp. Difference, relation between, Individual & overall HT coefficient, define the terms Heat exchanger, cooler, Heater, Condenser, Evaporator, Reboiler, Vaporiser, double pipe heat exchanger (Hair pin), shell & tube heat exchanger, Types of shell & tube heat exchanger 1-1, 1-2, 2-4. Exchanger, concept of correction Factor of LMTD, condensers Horizontal, vertical, Reboiler, extended surface heat exchanger, plate Type heat exchanger, heat transfer in agitated Vessel, simple calculation of overall H.T.coefficient in heat exchangers & heat transfer area.

7. EvaporationIntroduction- Liquid characteristics, factors affecting selection of evaporator boiling point elevation, heat capacity & economy of an Evaporator, single effect evaporator, multi-effect Evaporator, Types of feed, forward feed, backward feed, effect of heat economy by recompression of vapour, equipment: Short tube evaporator, long tube evaporator, agitated Film evaporator, forced circulation evaporator, Climbing film evaporator, falling film evaporator, Simple problems on single effect evaporator, Calculations (Direct formula).

8. Types of insulationInsulating material, methods of insulation, lagging of steam pipe, critical insulation, thickness, optimum Insulation thickness, simple calculation of Insulation thickness.

9. Tubular furnacesApplication classification & types of tubular furnaces.

10. Different methods of heating & coolinga) Chilled Waterb) Brine waterc) Cooling waterd) Refrigeratione) Hot waterf) Steam water heatingg) Oil heating with (with/without phase change)h) Process stream exchangeri) Molten salt heatersj) Air heaterk) Electric heatingl) Furnace heating.



126503 Chemical Engineering Thermodynamics & Kinetics

CREDITS:-04

L-T-P1. Scope of Thermodynamics First law of Thermodynamics systems &

surroundings Thermodynamic property, state function Internal Energy, Enthalpy, work done, Equilibrium, phase Rule, Types of process, constant volume andConstant pressure process, Heat capacity, SimpleCalculation of KP, KC, KAAY.

2. Second law of Thermodynamics : Statement of thesecond law of Thermodynamics, Mathematicalstatement of second law, Heat Engine,Thermodynamic temperature scale, Entropy,change, Carnot cycle, simple problem on Carnot Cycle.

3. Third law of Thermodynamics: Refrigeration & liquefaction: Carnot refrigeration, The vapour recompression cycle, Compression of refrigeration cycle, selection of Refrigerants, Heat Pump, Liquefaction processes.

4. Introduction to Chemical KineticsDefine – Chemical Kinetics – Rate of chemical Reaction, Factors affecting rate of reactionClassification of chemical reactions, Rate constant Order of reaction, Molecularity of reaction, difference between Molecularity & order of reaction, elementary & non-elementary reactions, Arhenius law of activation energy, Kinetic model, Classification of reactors.

5. Batch reactorConstant volume & constant pressure reactor, Integral method of analysis, differential method of analysis, variable volume reactor, Rate equation.

6. Introduction to reactor design : Flow Pattern, Batch reactor, continuous stirred tank reactor,Plug flow reactor.

7. Catalysis – Catalytic reaction & catalysis characteristics of catalytic reactions, classificationof catalysis, catalyst deactivation, catalyst preparation – Introduction to fixed bed and Fluidised bed reactors.

Chapters:



126504 PLANT OPERATIONCREDITS:-04

L T P

4 - - Chapters:

1. Concept of maintenance theory of failure Accident Record keeping failure or break down failures

2. Organisation check list & for maintenance, preventive maintenance, Types of preventive maintenance, Record of maintenance & their relative usefulness, Modern Management & maintenance techniques.

3. Construction working & operation aspect (include Start up shut down trouble shooting & maintenance) For the equipment’s like valves, pipes, fittings, flow meters pumps & compressor.

4. Construction, working & operation aspects (including start up, shut down trouble shooting & maintenance for equipment’s like size reduction machines, filtration centrifuges & classifiers

5. Construction working & operation aspect (including start up, shut down, trouble shooting & maintenance) for equipment’s such as Heat Exchangers & Evaporators.

6. Construction working & operation aspects (including start up, shut down & trouble shooting & maintenance) for equipment’s such as distillation tower, absorption tower & extractor.

7. Construction working & operation aspect & (includingstart up, shut down trouble shooting & maintenance)For the equipment such as dryers, crystallisers & cooling tower.

8. Construction working & operation aspect (including start up, shut down trouble shooting & maintenance) for various reactors.

9. Trouble shooting in plants (plant emergency) Electricity of cooling water DM water & feed failure, instrument air failure, steam failure, pump failure & remedial actions to be taken.

10. Commissioning Activities



126505 PETROCHEMICALS TECHNOLOGYCREDITS:-04 L T P

4 - -Chapters:

1. Origin formation & composition of petroleum : History, origin and formation of petroleum, world reserves of petroleum Indian petroleum industries types location & capacities development of petroleum refining, composition of petroleum & hemistry of petroleum, Exploration & production of petroleum methods of exploration, drilling, transportation of petroleum products.

2. Petroleum processing data :Evaluation of petroleum, properties of petroleum fractions, Distillation haracteristics, and Important products, properties & test methods: gas, gasoline, Naphtha, kerosene, Diesel, Lube oil, Bitumen significance & methods of testing for above petroleum products.

3. Fractionation of petroleum : Dehydration, Desalting & crude heating of crude – pipe, Still heaters, distillation of petroleum AU, VDU Topping Operation, Blending of gasoline.

4. Treatment techniquesTreatment of LPG, LNG sweetening operation for gases Treatment of gasoline treatment of kerosene treatment of Lube purification of wax.

5. Cracking Introduction, definition of cracking, chemistry & technology Catalytic cracking, catalytic reforming Naphtha cracking, Coking, Alkylation process Isomerisation process, polymer Gasoline Hydrocracking.

6. PetrochemicalsDefinition, History, Major petrochemical products & their Producers in India raw materials for petrochemicals

7. C1 compounds Methanol & formaldehyde

8. C2 compounds Acetylene, Ethylene, vinyl chloride, Ethanol, Acetic acid

9. C3 compoundsPropylene, Acetone & cumin, Acrylonitrate, Acrylic acid, M.M.A.

10. C4 compoundsButadiene, Isobutylene, Butanol

11. AromaticsSolvent extraction, Benzene, toluene, xylene production, Phenol, Benzaldehyde, Terphthalic acid, DMT, Phthalic Anhydride, Maleic anhydride.

12. Lubricating OilsProduction of petroleum waxes, greases, asphalt Bitumen & carbon black.



126506 CHEMICAL ENGINEERING III (MASS TRANSFER OPERATION)

CREDITS:-01 L T

P

- - 2

Laboratory Exercises.

1. Determination of diffusivity of Acetone, Acetic acid, Ethyl alcohol, carbon tetra chloride

2. Diffusion of Acetic acid in water.3. Determination of psychrometric properties of the Air water system 4. Study of packing materials5. Study of Bubble column6. Study of Packed column7. Dissolution of solid in liquid without reaction8. Dissolution of solid in liquid with reaction9. Determination of Mass transfer co-efficient



126507 CHEMICAL ENGINEERING IV (HEAT TRANSFER OPERATION)

CREDITS:-01 L T P

- - 2

Experiments –1. Determination of thermal conductivity of metal, insulation powders. 2. Heat transfer co-efficient in natural convection and forced convection.3. Determination of overall H.T. co-efficient in shell & tube heat exchanger4. Determination of overall H.T. co-efficient in parallel flow and counter flow 5. Determination of overall H.T. co-efficient in condenser 6. Determination of H.T. co-efficient in an agitated tank.7. Study of drop wise & film wise condensation phenomena 8. Calculation of capacity economy in an open pan evaporator 9. Study of H.T. equipment; shell & tube heat exchanger, long tube evaporator 10.Determination of H.T. co-efficient in finned tube exchanger.



126508 CHEMICAL ENGINEERING THERMODYNAMICS & KINETICS

CREDITS:-01 L T P

- - 2

Laboratory Exercises –1. Kinetics of first order2. Kinetics by half-life. 3. Determination of activation energy.4. Integral method of analysis.5. Differential method of analysis6. Study of pilot plant reaction



126509 PLANT OPERATION

CREDITS:-01 L T P

- - 2

Experiments:-1.To determine control valves characterstics.2. To determine response of shell and tube type heat exchanger with PID control3. Study of spray and fluidized bed dyer 4. Study of cooling tower



126510 PETROCHEMICALS TECHNOLOGYCREDITS:-01

L-T-P

- - 2Laboratory Exercises –1. Cleveland open cup (Flash point of Lube oil)2. Flash point in Penskey Martin (closed up) apparatus3. ASTM distillation4. Carbon residue (Conardson method)5. Cloud & Pour point 6. Drop point of grease 7. Penetration number8. Reid vapour pressure9. Smoke point10. Aniline point11. Dielectric strength12. Abel's apparatus13. Redwood viscometer 14. Saybolt viscometer15. Ostwald viscometer 16. Orsat gas analysis A student should perform minimum 10 experiments.



126511 PROJECT WORK - ICREDITS:-02

L T P

- - 4

Some selected topics will be given in a group of 4-5 students. Students will do Literature survey and well be required to present that topic in seminar to be held during the college hours. The topics will be interchanged and all students will have the knowledge of all the topics of seminar work.




126601 CHEMICAL ENGINEERING V MASS TRANSFER OPERATION II

CREDITS:-04

L T P

4 - -Chapters:

1. DistillationVapour liquid equilibria press temp. Concentration diagram, Relative volatility, ideal solutions, Raoult’s law, Flash Vaporisation, differential or simple distillation (Rayleigh equation), steam distillation, vacuum distillation, principles of rectification, Binary system, material balance and energy balance for fractionating column, calculation of ideal stages by McCabe Thiele method, Introduction of feed, location of feed tray, Minimum reflex ratio and infinite reflux ratio, Optimum Reflux ratio, condenser & reboiler heat duty, continuous Contact equipment, HTG, NTG, HOG, NOG, Types of Distillation column. Types of tray, construction & Operation of distillation column.

2. CrystallizationDefinition, crystal forms, crystal geometry, crystallization Equipments, phase diagram, crystal yields, material and Energy balance calculation, Mier’s supersaturation theory and its limitation effect of operating condition on caking of crystals prevention of caking.

3. Membrane separation processesTypes of Membrane – Brief introduction of membrane Separation processes, Reverse osmosis, Micro filtration Ultra filtration, Dialysis, pervaporation, permeation

4. Extraction (Liquid – Liquid)Definition –Field of usefulness, properties of solvent Solvent requirement equilateral triangular diagram, System of three liquids one pair partial soluble system System of three liquids – two pair partially soluble System of two pairs partially soluble liquids with one Solid Effect of temp. and press on solubility diagram, Stagewise contact, calculation for single stage Extraction and multi-stage extraction equipments –Settlers, Mixer setter cascade sieve tray tower Continuous contact Extractor, spray tower, Mechanically Agitated countercurrent extractor pulsed column, Centrifugal extractor.



5. DryingDefinition of various terms, equilibrium, principles of Drying rate of drying curve, Time of drying Batch Drying and continuous drying. Drying equipments Direct dryers and indirect dryers, Tray dryer, Rotary Dryer, Drum dryer, spray dryer.

6. Adsorption and Ion exchangeDefinition- Industrial application, types of adsorption, Adsorption equilibria, equilibrium adsorption of single Vapour & gas mixture in brief, adsorption in liquids, Adsorption of solute from dilute solution Freundlich Equation & its scope, nature of adsorption, xamples, Properties and application of typical adsorption, Adsorption operation of various equipments, Ion Exchange, principles, use of Ion exchange in D.M. water.

7. LeachingDefinition of various terms, preparation of solid, Temp. of leaching methods of operation, unsteady state Operation. In place leaching, Heap leaching, calculation for single stage leaching, stage efficiency, equipments Percolation tank, Shank system Agitated vessels,Bollman extractor.



125601BASICS OF MANAGEMENTCREDITS:-04

L T P

4 - -Chapters:1. Introduction:

Definition and concept of Management, functions of management viz. planning, organizing, staffing, coordinating, controlling; Various areas of management: Human Resource Management (HRM): recruitment, training, retraining and compensation policies; Financial Management: payback period, Net Present Value (NPV), Internal Rate of Return (IRR), profitability ratio, cost benefit analysis; Materials Management: economic order quantity, re-order point, safety stock, Just-in-Time Technique of Materials Management; Marketing Management: necessity, advertisement, print media, electronic media, sales promotion

2. Structure of Industrial OrganizationConcept and structure of an organization, hierarchical management structure (top, middle and lower level management) and functional management structure.

3. LeadershipConcept, importance, types and qualities of a good leader

4. MotivationConcept and importance of motivation - drives and incentives, intrinsic and extrinsic motivation, brief about theories of motivation.

5. Ethics and ValuesIntroduction, importance of attitude, values and ethical behaviour. Professional ethics – its need and development

6. Customer Relationship Management (CRM)Need, various types of customers, customer satisfaction, life- long customer, Customer Satisfaction Index (CSI) and its significance

7. Legal Aspects of Business8. Elementary knowledge of Income Tax, Sales Tax, Excise Duty, Provident

Fund, Employees State Insurance Act.a) Labour welfare schemes, systems of wage payment, incentivesb) Salient features of Factory Act 1948 with special reference to health,

safety and welfare measures, working hours, annual leave with wages, Payment of Wages Act 1936, Minimum Wages Act 1948

c) Intellectual Property Rights (IPR), concept, definitions, infringements related to patents, copyright, trademark

7. Introduction to Total Quality Management (TQM) and steps to achieve this. 8. MIS: Concept, importance and steps for its development 9. ill effect of drugs10.Knowing Drug Abuse.

Type of Drugs used and their ill effects. Consequences of drug abuse.



Symptoms and Prevention Rehabilitation

11.Traffic Laws.12.Importance of knowing traffic laws and safe driving

Traffic rules Controlling road rage among young drivers Law regarding traffic Social responsibility towards injured in case of road

accidents.

126602 HEALTH ENVIRONMENT & SAFETY



CREDITS:-04 L T P

4 - -

Chapters:1. Introduction to safety: Definition of safety, Importance

Of safety in chemical industries, safety of the organisation, industrial plant layout for safety. Safety measures introduction of various safety organisations like National safety council ILO etc. society & safety advantages of safety.

2. Hazards: Types of hazards, chemical hazardsI) Chemical hazards – classification, occupational healthhazards, causes of occupational diseases & poisoningprevention of diseases control of chemical hazards –safety factors color codes & symbols for safety inChemical industries.ii) Mechanical hazardsiii) Electrical hazardsiv) Radiation hazardsv) Noise and vibrating hazards

3. Hazards of fire and explosion: Theory of fire & explosions, definition, flammability, fire & pond fire explosion types of fire, fire extinguishing agents, types of fire, fire protection in industries, fixed installation monitors, alarms and fire fighting activities.

4. Protective equipments: Protective equipments for head, ears, eyes, face and respiratory. Organs hands feet etc. and there maintenance.

5. Safe handling of hazardous chemicals: Chemical reactions & properties of hazardous chemicals like chlorine, Ammonia, caustic soda sulfuric acid, hydrochloric acid Nitric acid carbon monoxide phosgene LPG transportation of hazardous chemicals, storage of hazardous chemicals, Hazop / Hazan study disposal of hazardous chemicals.

6. Health & Safety hazards: Toxicology, pressure related safety, temperature related Safety.

7. Loss prevention & Techniques for HazardIdentification – Hazard operability & disaster planningBasic principles, keywords, procedure safety regulation & Safety audits, check list, safety techniques, first aid,Emergency.

8. Industrial Acts: Introduction factory acts, Industrial Disputes Act, Boiler Act, Pollution Control Act, ESI Act, Workmen’s Compensation Act. Industrial Safety, Introduction, Causes of accidents, Types of accidents, safety procedures, safety during maintenance, operation, safety. Permit system.

9. Environment: Concept of environment, components of environment, Ecological aspects of environment.

10. Pollution: Water pollution, Air pollution, Noise pollution, Radioactive pollution.



11. Global environmental problems: Introduction, acid rain, greenhouse effect, and ozone layer depletion. Measures against global problems.

12. Energy conservation: Conventional & non-conventional energy sources of energy. Renewable & non-renewable energy sources re use of water.



126603 POLYMERS TECHNOLOGY AND PROCESSING

CREDITS:-04

L T P

4 - -Chapters:

1. Introduction: What are Polymer, History, and structure of Polymer, Molecular Weight and its determination.

2. Chemistry of polymerization: Different types of polymerization, chain polymerization, and Free radical polymerization.

3. Polymerization methods: Bulk polymerization, Solution polymerization, Suspension Polymerization, emulsions polymerization, and melts polymerization, Polycondensation.

4. Chemical and geometrical structure of polymer molecules: Microstructure based on chemical structure, Microstructure based on geometrical structure, Introduction to polymer blends, polymer compounds Glass transition temp.

5. Individual polymers: Introduction classification of plastics raw materials. Manufacturing process for the products like Polyethylene, High density polyethylene, Linear Low-density polyethylene. Polyvinylchloride, polystyrene Polypropylene, Engineering Plastics like, ABS, PMMA, TEFLON, Polycarbonates

6. Rubbers: Classification rubbers, natural rubber, synthetic rubber like SBR, Polybutadiene, Polyethylene, Propylene & Butyl rubber, Nitrile rubber, Neoprene rubber, reclaim rubber, applications of rubber.

7. Resins for Adhesives & protective coating: Introduction, Phenol formaldehyde, Amino resins, polyester resin, Alkyd resins, Epoxy resin, polyurethene resins, polyamide resins, vinyl resins, vinyl alcohol resins, vinylidene resins, styrene resins, acrylic resins, protective coatings

8. Fiber & Film : Introduction, properties of fiber, cellulosic fiber, polyamide fiber, polyester fiber, acrylic fiber, and inorganic fiber like glass Carbon. Films : Viscose & cellulose acetate, polyolefins, PVC

9. Plastics processing processing of thermoplastics, Processing of thermosets, and Processing of plastics and recent developments.

10. Quality control: Identification of plastics, Testing of plastics.



126604 PROCESS INSTRUMENTATION & CONTROLCREDITS:-03

L T P

3 - -Chapters:

1. Introduction : Importance of instrumentationBasic concept of measurement, system Configuration, methods of measurement, Elements of measurementFunctional elements of an instrument, (block Diagram). Functions of an instrument, static Characteristics & dynamic characteristics Transducers – Definition - classification of Transducers, one application of each transducers With sketch Measurement of physical Quantities using transducer with simple Diagram like temp., pressure, flow, level, Thickness, speed, strain, pH value.

2. Temperature MeasurementIntroduction, Temperature scales, expansion, thermometer, filled system, thermometers, sources of errors infilled system thermometers, Thermoelectric temperature measurement (Thermocouple), principles of thermoelectricity, See Back, Peltier Thomson effect, classification of thermocouple (types), their composition range, lead wires for Thermocouple, Thermal well, Resistance thermometer (PRT) Pyrometry, Laws of radiation, Radiation receiving element and Radiation pyrometer, Optical pyrometer, Calibration of temperature measuring instruments, their merits and demerits.

3. Pressure MeasurementIntroduction, Manometers, Elastic type, Bourden tube Diaphragm, Bellows, Bellgauges, Indicating element for pressure gauge, Differential pressure meter, Electrical type: strainguauge, potentiometric press, transducer, capacitive pressure transducer, Reluctive pressure transducers, LVDT, Servo, piezoelectric, pressure switches, measurement of vacuum, Mcleodgauge, Thermal conductivity gauge, ionization gauge, Measuring pressure in corrosive fluids, calibration of pressure measuring instruments, Maintenance and repair of pressure measuring instruments, Merits and demerits of pressure measuring instruments and their application.

4. Flow MeasurementIntroduction, methods of flow measurement, inferential flow meters, variable head meters, variable areas meters, magnetic flow meter, Turbine meter, target meter, thermal flow meter, Vortex flow meter, Quantity flow meters, Nutating disc meter, Oscillating piston type, Rotating Vane, Reciprocating piston, Lobed impeller type flow meter

5. a) Measurement of head & levelIntroduction, Methods of level measurement, Direct and Indirect methods, hook type, sight glass, Hydraulic transmission, Float type level indicators, float and shaft, float and tape, Magnetic float gauge, pressure gauge method,



air bellows, Diaphragm, Air purge (Bubbler method), Liquid purge, electrical methods: conductivity method, resistance method, capacitance method, ultrasonic method, radiation level detector, level measurement in corrosive environments, servicing of level measuring instruments, level measurement in pressure vessel, level of dry solids.b) Miscellaneous MeasurementDensity measurement, Hydrometer method, Displacement meter, Air purge method, Viscosity measurement, continuous viscosity meter, Humidity measurement, Psychrometer method, Hygrometer method, pH measurement.

6. a) Indicating & Recording instrumentsIntroduction, types of recorders, strip chart recorder, circular chart recorder, X-Y recorder, their merits, demerits and application.b) Telemetering systemsElectrical or electronic telemetering systems, voltage telemetering, current telemetering systems, pneumatic telemetering system.

7. Introduction to process control : Automatic process control, its merits & demerits. Incentives for chemical process control, aspects of process control system, Hardware for a process control system.

8. Open Loop control systems : Dynamic behaviour of first order and second order system, Forcing functions, step, impulse, Ramp, siunusoidal Transfer, Function, Physical Examples, first order systems thermometer,Pure capacity element, Liquid level Mixing process, TimeConstant second order system interacting and non interacting. Systems Mercurry Manometer Terms related to underdamped, System Damping coefficient Decay ratio overshoot rise time, Transportation lag.

9. Closed loop control systems: Feedback and feed forward control system, Servo Regulatory Control system, Development of block diagram.

10. Process control application: Process control in distillation column, Heat exchanger, Reactor, (Batch type) control systems with multiple loops, cascade control, Ratio control, selective control, split range control, Adaptive control. Final control element, control element, control valve, Classification, valve actuator, valve position, characteristics of control valves.

11 Control actions & controllers: Types of control actions – P, PI, PD, PID, Types of controllers – Hydraulic, pneumatic, electronic etc.On-Off controller P, PI, PD & PID controllers.

12Analog to digital & digital to analog controllers: Digital computer control, Introduction to DCS, Evolution of DCS, merits & demerits, basic architecture of DCS, Hierachy in DCS system Introduction to PLC.



126605 CHEMICAL ENGINEERING V(MASS TRANSFER OPERATION II)

CREDITS:-01 L T P

- - 2

Experiments –1. Verification of Rayliegh equation2. Vapour liquid equilibrium data3. Steam distillation4. Vacuum distillation5. Single stage – Liquid – Liquid extraction6. Three stage – Liquid – Liquid extraction7. Batch drying 8. Single stage leaching9. Binodal curve & Tieline10.Adsorption on charcoal.



126606 HEALTH ENVIRONMENT & SAFETY

CREDITS:-01 L-T-P

- - 2

Laboratory exercises –1. Demonstration of different types of fire extinguishers 2. Demonstration of various personal protective diseases 3. Determination of important parameters governing quality of water 4. (Analysis of water) TDS, pH, DO, turbidity, Acidity & Alkalinity CO, CO2, & SO2, Cl2 5. BOD & COD in liquid effluent 6. Measurement of noise level7. Measurement of humidity8. Study of color codes for different pipe lines 9. Determination of Air pollutants

126608 PROCESS INSTRUMENTATION & CONTROLCREDITS:-01

L-T-P



- - 2

List of experiments1. Determination of time constant of thermocouple with and without sheath2. Manometer dynamics3. First order mixing process (Time constant) 4. Non interacting tanks 5. Integrating element6. Study of controllers7. Application of process control - Case study in Laboratory boiler8. Study of controller gain.

126609 PROJECT WORK - IICREDITS:-04

L-T-P

- - 8



Based on the theoretical knowledge and laboratories during five semesters, the student is required to prepare project work report. This is supplemented by four weeks of in-plant training/plant visit during final year. The student has to submit a training report for which separate weightage is given.Making use of the above, the student will be given any one of the Chemical Product For which the report is to be prepared by him in the following format:

1. Introduction (a) Objective (b) Application including market survey.2. Properties (a) Raw material (b) Products (c) Byproducts3. Chemistry / Mechanism of the process.4. Different processes used in the industry5. Selection of the process technology6. Description of the process selected.7. Material balance / Energy balance - simple calculation for production of It on

some basis.8. Simple Equipment design - Calculation of height, diameter, thickness of Any one

of the major chemical equipment and its detailed drawing.9. Operation : Operation of chemical plant, start up, shutdown procedure,

Maintenance aspect.10.Safety of the process equipment.11.Process Instrumentation Diagram - Instrumentation and process control 12.Details of any one of the major chemical equipment.13.Cost estimation.14.Entrepreneurship and management aspect of the project. Conclusion (a) Results

(b) Usefulness in the industry (c) Interpretation.

gurukashiuniversity.ingurukashiuniversity.in/syllabi/diploma/syllabus/diploma... · web view1st...

Documents