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December 2007 IAOM Muscat Monday 11/12 - 09:50-10:00 WN # 6 What's New Mixolab device : the complete rheological tool Chopin technologies-France Mr.Charles Loubersac d'Hotel Deputy Export Director

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Page 1: 1- What's new Mixolab - IAOM MIDEAST & AFRICA REGION … ·  · 2016-10-21IAOM Muscat December 2007 Monday 11/12 - 09:50-10:00 WN # 6 What's New Mixolab device : the complete rheological

December 2007IAOM Muscat

Monday 11/12 - 09:50-10:00 WN # 6 What's New

Mixolab device :

the complete rheological tool

Chopin technologies-FranceMr.Charles Loubersac d'Hotel

Deputy Export Director

Page 2: 1- What's new Mixolab - IAOM MIDEAST & AFRICA REGION … ·  · 2016-10-21IAOM Muscat December 2007 Monday 11/12 - 09:50-10:00 WN # 6 What's New Mixolab device : the complete rheological

December 2007IAOM Muscat

Look further…N°173

Page 3: 1- What's new Mixolab - IAOM MIDEAST & AFRICA REGION … ·  · 2016-10-21IAOM Muscat December 2007 Monday 11/12 - 09:50-10:00 WN # 6 What's New Mixolab device : the complete rheological

December 2007IAOM Muscat

Mixolab

A new instrument to measure the dough properties during mixing and heating

Page 4: 1- What's new Mixolab - IAOM MIDEAST & AFRICA REGION … ·  · 2016-10-21IAOM Muscat December 2007 Monday 11/12 - 09:50-10:00 WN # 6 What's New Mixolab device : the complete rheological

December 2007IAOM Muscat

Measurement

• Mixing properties

– Water absorption

– Mixing time

– Stability

– Weakening

• Starch gelatinization

• Enzymatic activity

• Starch retrogradation

Page 5: 1- What's new Mixolab - IAOM MIDEAST & AFRICA REGION … ·  · 2016-10-21IAOM Muscat December 2007 Monday 11/12 - 09:50-10:00 WN # 6 What's New Mixolab device : the complete rheological

December 2007IAOM Muscat

So easy : The Mixer Bowl &

automated water injection

Only 50g

samples

Page 6: 1- What's new Mixolab - IAOM MIDEAST & AFRICA REGION … ·  · 2016-10-21IAOM Muscat December 2007 Monday 11/12 - 09:50-10:00 WN # 6 What's New Mixolab device : the complete rheological

December 2007IAOM Muscat

Operating & maintenance system :

on a remote software

kneader

Sensor

Water tank

Motor

Injection

system

Page 7: 1- What's new Mixolab - IAOM MIDEAST & AFRICA REGION … ·  · 2016-10-21IAOM Muscat December 2007 Monday 11/12 - 09:50-10:00 WN # 6 What's New Mixolab device : the complete rheological

December 2007IAOM Muscat

1 standard protocol…

Page 8: 1- What's new Mixolab - IAOM MIDEAST & AFRICA REGION … ·  · 2016-10-21IAOM Muscat December 2007 Monday 11/12 - 09:50-10:00 WN # 6 What's New Mixolab device : the complete rheological

December 2007IAOM Muscat

A completely

customizable protocol

Maximum test time : 45 hours !

545 min0 minAll times

12°C/min2°C/minCooling gradient

92°C20°CFinal T°C

12°C/min2°C/minHeating gradient

92°C20°CMaximum T°C

60°C20°CMixer T°C

60°C20°CWater T°C

7 Nm0,1 NmTorque

250 rpm55 rpmMixing speed

MaximumMinimumParameters

Page 9: 1- What's new Mixolab - IAOM MIDEAST & AFRICA REGION … ·  · 2016-10-21IAOM Muscat December 2007 Monday 11/12 - 09:50-10:00 WN # 6 What's New Mixolab device : the complete rheological

December 2007IAOM Muscat

Graph interpretation

Page 10: 1- What's new Mixolab - IAOM MIDEAST & AFRICA REGION … ·  · 2016-10-21IAOM Muscat December 2007 Monday 11/12 - 09:50-10:00 WN # 6 What's New Mixolab device : the complete rheological

December 2007IAOM Muscat

Standard graph

torque in Nm

Mixer bowl

temperature

Dough temperature

Time (mn)

Torq

ue

(Nm

)

T°c

(°C

or

°F)

Page 11: 1- What's new Mixolab - IAOM MIDEAST & AFRICA REGION … ·  · 2016-10-21IAOM Muscat December 2007 Monday 11/12 - 09:50-10:00 WN # 6 What's New Mixolab device : the complete rheological

December 2007IAOM Muscat

Protein behaviour

C1

Water Absorption : % of water required for the dough to

produce a torque of 1.1 Nm

Development Time (min) : time to reach the maximum

torque at 30°C

Stability (min) : elapsed time at which the torque produced

is kept at 1.1Nm

For high content protein :

-Higher hydration because more protein molecules

available to catch free water

-Longer stability due to strength of protein molecules, it

needs more energy to modify the network

Page 12: 1- What's new Mixolab - IAOM MIDEAST & AFRICA REGION … ·  · 2016-10-21IAOM Muscat December 2007 Monday 11/12 - 09:50-10:00 WN # 6 What's New Mixolab device : the complete rheological

December 2007IAOM Muscat

Farinograph comparison(Simulator protocol).

Hydratation

y = x + 0,0005

R2 = 0,978

48

50

52

54

56

58

60

48 50 52 54 56 58 60

Simulator personnalisé (en %)

Fari

no

(e

n %

)

Temps de développement

y = 1,0001x + 0,0001

R2 = 0,977

0

2

4

6

8

10

12

0 2 4 6 8 10 12

Simulator personnalisé (en min)

Fari

no

(e

n m

in)

Stabilité

y = x - 6E-05

R2 = 0,805

2

4

6

8

10

12

14

16

18

20

2 4 6 8 10 12 14 16 18 20

Simulator personnalisé (en min)

Fari

no

(e

n m

in)

Affaiblissement

y = x + 8E-05

R2 = 0,899

20

40

60

80

100

120

20 40 60 80 100 120

Simulator personnalisé (en UF)

Fari

no

(e

n U

F)

Page 13: 1- What's new Mixolab - IAOM MIDEAST & AFRICA REGION … ·  · 2016-10-21IAOM Muscat December 2007 Monday 11/12 - 09:50-10:00 WN # 6 What's New Mixolab device : the complete rheological

December 2007IAOM Muscat

C2

Minimum torque (Nm) : the minimum value of torque

produced by dough passage subjected to mechanical

and thermal constraints

Weakening (Nm) : difference between the torque at the

end of the holding time at 30°C and the minimum

torque

Protein behaviour

Upon heating, protein linkages are broken and protein

are denatured

Sample A

Sample N Tenacity problems during

Dough manipulation

C2 = 0.46 Nm

C2 = 0.65 Nm

Good breadmaking quality

Good volume

Page 14: 1- What's new Mixolab - IAOM MIDEAST & AFRICA REGION … ·  · 2016-10-21IAOM Muscat December 2007 Monday 11/12 - 09:50-10:00 WN # 6 What's New Mixolab device : the complete rheological

December 2007IAOM Muscat

C3

Peak torque (Nm): the maximum torque produced

during the heating stage

Starch behaviour

The strongly bound crystalline areas of ordinary starch

granules render them insoluble in cold water.

When heating, they will form an opaque suspension,

then translucent (granules swell up and can burst,

amylose and amylopectine get out of starch granules)

and finally a viscous solution = Gelatinization

Page 15: 1- What's new Mixolab - IAOM MIDEAST & AFRICA REGION … ·  · 2016-10-21IAOM Muscat December 2007 Monday 11/12 - 09:50-10:00 WN # 6 What's New Mixolab device : the complete rheological

December 2007IAOM Muscat

C4

Cooking stability (Nm): ratio of the torque after the

holding time at 90°C and the maximum torque during

heating period

Starch behaviour

From the end of gelatinization, only one stress : mixing

-Starch +/- steady

-Amylose and Amylopectine are more free to catch water

-According to high temperature, Amylase & enzymes

break the linkages : viscosity decreases

Page 16: 1- What's new Mixolab - IAOM MIDEAST & AFRICA REGION … ·  · 2016-10-21IAOM Muscat December 2007 Monday 11/12 - 09:50-10:00 WN # 6 What's New Mixolab device : the complete rheological

December 2007IAOM Muscat

C5Setback (Nm): difference between the torque produced

after cooling at 50°C and the one after the heating

period

Starch behaviour

Gel causes the bread to deteriorate (staling)

Upon cooling : gelatinized amylose molecules begin to

re-crystallize, network to form an ordered structure. They

shrink as some of the liquid separates from the gel

= Retrogradation = crumbs firmness = staling

Page 17: 1- What's new Mixolab - IAOM MIDEAST & AFRICA REGION … ·  · 2016-10-21IAOM Muscat December 2007 Monday 11/12 - 09:50-10:00 WN # 6 What's New Mixolab device : the complete rheological

December 2007IAOM Muscat

…to reach a complete information !

Torque

TemperatureTank and dough

C1

Water absorption

Mixing time

Stability

Weakening

C2

Protein

weakening

induced by

temperature C3 C4

C5

PastingCooking

Stability

Retrogradation

Page 18: 1- What's new Mixolab - IAOM MIDEAST & AFRICA REGION … ·  · 2016-10-21IAOM Muscat December 2007 Monday 11/12 - 09:50-10:00 WN # 6 What's New Mixolab device : the complete rheological

December 2007IAOM Muscat

Summary

• The Mixolab is a new tool for a complete characterization of the sample :– Water absorption.– Dough tolerance, stability and elasticity.

– Starch gelatinization and retrogradation.– Enzyme activity.

– Mixing power

• Many settings and calculation possibilities.

• 50g sample.

• Standardized ICC 173

Page 19: 1- What's new Mixolab - IAOM MIDEAST & AFRICA REGION … ·  · 2016-10-21IAOM Muscat December 2007 Monday 11/12 - 09:50-10:00 WN # 6 What's New Mixolab device : the complete rheological

December 2007IAOM Muscat

Summary

• Mixolab brings new testing possibility to the market :• Protein behaviour during heating (C2 in relation with volume).• Pasting properties measured on a dough instead of a batter.• Retro gradation in relation with product shelf life.• Complete testing with only 1 test.• Possibility to work on whole meal flour (time saving on sample

preparation…).

• Various studies are under progress within a very active user group. More application to come up on different products (Durum wheat…) additives (Incl. Fibres, hydrocolloïds…), related to bread making…

Page 20: 1- What's new Mixolab - IAOM MIDEAST & AFRICA REGION … ·  · 2016-10-21IAOM Muscat December 2007 Monday 11/12 - 09:50-10:00 WN # 6 What's New Mixolab device : the complete rheological

December 2007IAOM Muscat

Thank you very much

for your attention

www.chopin.fr