160103 gryphon blend assay

REPORT OF ANALYSIS

TRUE BOILING POINT

DISTILLATION

GRYPHON CRUDE OIL

Job No: 5000 / 65436 Page 1Date: ###

REPORT ON STANDARD ASSAY

Product : Gryphon crude oil

Description on label: Graypen LTD: Dock Road: Grangemounth Docks: Grangemounth : PK3 8TY, UK

Date of sampling : November 18, 2002

Sample received : December 13, 2002

Sample package : Tin drums

Sample volume : 2 x 10 L

Date of testing : December 17, 2002 till January 16, 2003

Job No: 5000/65436 Page 2Date: 1/17/2003

To Whom It May Concern

Product Gryphon crude oilMarked asTerminalSample date 18/11/02Sample Date of receipt 12/13/2002

TBP Distillation Data

FRACTION WT % CUM WT % VOL % CUM VOL%

Gas 0.2 0.2 0.3 0.3 0.0 0.2 0.3C5-60 0.2 0.3 0.2 0.5 160.0 0.3 0.560-160 0.6 0.9 0.5 1.0 237.0 0.9 1.0237-330 1.5 2.4 1.7 2.7 330.0 2.4 2.7330-380 2.0 4.4 2.3 5.0 380.0 4.4 5.0380-450 5.5 9.9 5.9 10.9 450.0 9.9 10.9450-620 21.4 31.4 22.1 32.9 620.0 31.4 32.9620-700 11.8 43.1 11.8 44.7 700.0 43.1 44.7700-1000 33.8 76.9 33.3 78.0 1000.0 76.9 78.0

0.0 0.00.0 0.0

700+ 56.8 100.0 55.1 99.81000+ 23.0 100.0 21.7 99.8

Job No: 5000/65436 Page 3Date: ###

0.0

100.

020

0.0

300.

040

0.0

500.

060

0.0

700.

080

0.0

900.

0

1000

.00.0

10.0

20.0

30.0

40.0

50.0

60.0

70.0

80.0

90.0

True Boiling Point Distillation

Weight % Volume %

Temperature, °C

Pe

rce

nt

Job no.: 5000 / 65436 Page 4Date: 1/16/2003

Fraction: CRUDE OIL

Test Method Unit Result

Density @ 15°C D 5002 g/ml 0.9156API Gravity @ 60°F Calc 22.98Kinematic Viscosity @ 180°F D 445 mm²/s 8.227Kinematic Viscosity @ 210 °F D 445 mm²/s 5.588Micro Carbon Residue D 4530 wt% 1.9Ramsbottom Carbon residue D 524 wt% 1.50Acid Number D 664 mgKOH/g 3.3Sulphur Content D 2622 wt % 0.364Total Nitrogen D 5762 mg/kg 1120Pourpoint D 5853 °F -44Mercaptan sulphur D 3227 mg/kg 6

D 323 psi 0.60Nickel IP 433 mg/kg 2Vanadium IP 433 mg/kg 2Asphaltenes C5 D 6560 wt % 0.54Asphaltenes C7 D 6560 wt % 0.06Water and sediments D 4007 vol % 0.20Water D 4006 vol % 0.2Salt as NaCl D 3230 mg/kg 59Flashpoint, PMCC D 93 °F 140Ash content D 482 wt % 0.030Light Ends IP 344 wt % / vol%

Methane < 0.01 / < 0.01Ethane < 0.01 / < 0.01Propane < 0.01 / < 0.01Iso-Butane < 0.01 / < 0.01n-Butane < 0.01 / < 0.01iso-Pentane < 0.01 / < 0.01n-Pentane < 0.01 / < 0.01

Reid Vapour Pressure at 100 oF

Job no.: 5000 / 65436 Page 5Date: 1/16/2003

Fraction: 237 - 330 °F


Density @ 15°C D 4052 g/ml 0.7930API Gravity @ 60°F D 1298 22.98Sulphur Content D 2622 mg/kg 98Mercaptan Sulphur D 3227 mg/kg 2Hydrogen Sulphide BP 105 mg/kg < 0.5Doctor Test IP 30 negativeNitrogen content D 5762 mg/kg < 3Paraffins, Naphtenes and Aromatics D 5443 wt% -----

n-Paraffins 0.6i-Paraffins 16.3

Olefins < 0.1Naphtenes 69.1Aromatics 13.1

Poly-Naphtenes 0.6> 200 °C 0.3

Copper Corrosion D 130 1ASaturates D 1319 vol% 96.2Aromatics D 1319 vol% 3.0Olefins D 1319 vol% 0.8



Density @ 15°C D 4052 g/ml 0.8222API Gravity @ 60°F D 1298 40.59Sulphur Content D 2622 mg/kg 0.0145Mercaptan Sulphur D 3227 mg/kg 5Hydrogen Sulphide BP 105 mg/kg < 0.5Nitrogen content D 5762 mg/kg < 3Pour Point D 5950 °F < -76Cloud Point D 5771 °F < -76CFPP IP 309 °F < -76Freezing Point D 2386 °F < -76Kinematic Viscosity @ 70 °F D 445 mm²/s 1.495Kinematic Viscosity @ 100 °F D 445 mm²/s 1.187Aniline Point D 611 °F 117.7Organic Chloride UOP 779 mg/kg < 1Acid Number D 664 mgKOH/g 0.12Saturates D 1319 vol% 88.1Aromatics D 1319 vol% 0.7Olefins D 1319 vol% 11.2

Copper Corrosion D 130 1A

Job no.: 5000 / 65436 Page 6Date: 16/01/03



Density @ 15°C D 4052 g/ml 0.8517API Gravity @ 60°F D 1298 34.56Sulphur Content D 2622 mg/kg 226Mercaptan Sulphur D 3227 mg/kg 2Nitrogen content D 5762 mg/kg < 3Pour Point D 5950 °F < -76Cloud Point D 5771 °F < -76CFPP IP 309 °F < -76Freezing Point D 2386 °F < -76Cetane Index D 976 29.9Kinematic Viscosity @ 70 °F D 445 mm²/s 2.204Kinematic Viscosity @ 100 °F D 445 mm²/s 1.639Smoke Point IP 57 mm 14.5Aniline Point D 611 °F 116.2Copper Corrosion D 130 1ANaphtalenes D1840 vol% 2.46Distillation at Atmospheric Pressure D 86 -----Initial Boiling Point °F 3905 % Recovered °F 39910% °F 40120% °F 40430% °F 40640% °F 40850% °F 41160% °F 41470% °F 41880% °F 42390% °F 42995% °F 435Final Boiling Point °F 443Recovery vol% 98.7Loss vol% < 0.5Acid Number D 664 mgKOH/g 0.26Saturates D 1319 vol% 80.9Aromatics D 1319 vol% 2.8Olefins D 1319 vol% 16.3

Job no.: 5000 / 65436 Page 7Date: 1/16/2003



Density @ 15°C D 4052 g/ml 0.8900API Gravity @ 60°F D 1298 27.40Sulphur Content D 2622 wt% 0.109Nitrogen content D 5762 mg/kg 24Pour Point D 5950 °F < -76Cloud Point D 5771 °F < -76CFPP IP 309 °F < -76Colour D 1500 L 0.5Kinematic Viscosity @ 122 °F D 445 mm²/s 3.114Kinematic Viscosity @ 180 °F D 445 mm²/s 1.914Aniline Point D 611 °F 126.0Copper Corrossion D 130 1AOrganic Chloride UOP 779 mg/kg 1Acid Number D 664 mgKOH/g 1.73Refractive Index at 67 °F D 1747 1.4726Saturates D 1319 vol% 46.6Aromatics D 1319 vol% 37.1Olefins D 1319 vol% 16.3Flash Point D 93 °F 248Water Seperation Index D 3948 70Cetane Index D 976 37.3UOP K Factor UOP 375 11.2Distillation at Atmospheric Pressure D 86 ----Initial Boiling Point °F 4895 % Recovered °F 50410% °F 50620% °F 51130% °F 51540% °F 52150% °F 52960% °F 53770% °F 54780% °F 55990% °F 57495% °F 583Final Boiling Point °F 592Recovery vol% 98.3Loss vol% < 0.5Basic Nitrogen UOP 269 mg/kg 16Wax Content UOP 46 wt% < 0.5

Job no.: 5000 / 65436 Page 8Date: 1/16/2003

Fraction: 620-700 °F


Density @ 15°C D 4052 g/ml 0.9153API Gravity @ 60°F D 1298 23.01Sulphur Content D 2622 wt% 0.386Nitrogen content D 5762 mg/kg 324Pour Point D 5950 °F -49Kinematic Viscosity @ 122 °F D 445 mm²/s 9.710Kinematic Viscosity @ 180 °F D 445 mm²/s 4.065Aniline Point D 611 °F 143.3Organic Chloride UOP 779 mg/kg 1Acid Number D 664 mgKOH/g 4.30Refractive Index at 67 °F D 1747 1.4879Flash Point D 93 °F 248Micro Carbon Residue D 4530 wt% < 0.1Ramsbottom Carbon residue D 524 wt% 0.09Cetane Index D 976 39.9UOP K Factor UOP 375 11.4Distillation at Atmospheric Pressure D 86 ----Initial Boiling Point °F 6315 % Recovered °F 63410% °F 63820% °F 64030% °F 64240% °F 64450% °F 64660% °F 64970% °F 65280% °F 65690% °F 66395% °F 670Final Boiling Point °F 674Recovery vol% 97.4Loss vol% 0.4Basic Nitrogen UOP 269 mg/kg 99Wax Content UOP 46 wt% < 0.5

Job no.: 5000 / 65436 Page 9Date: 1/16/2003

Fraction: 700-1000 °F


Density @ 70 °C D 4052 g/ml 0.8895API Gravity @ 60°F D 1298 20.95Sulphur Content D 2622 wt% 0.398Nitrogen content D 5762 mg/kg 1020Pour Point D 5950 °F -17Kinematic Viscosity @ 122 °F D 445 mm²/s 68.85Kinematic Viscosity @ 180 °F D 445 mm²/s 17.17Aniline Point D 611 °F 185.0Acid Number D 664 mgKOH/g 0.78Refractive Index at 67 °F D 1747 1.4949Micro Carbon Residue D 4530 wt% 0.1Ramsbottom Carbon residue D 524 wt% 0.17UOP K Factor UOP 375 11.7Distillation at reduced pressure D 1160 ----Initial Boiling Point °F 7295 % Recovered °F 74310% °F 75620% °F 78430% °F 82240% °F 86550% °F 91260% °F 959Basic Nitrogen UOP 269 mg/kg 336Wax Content UOP 46 wt% 0.6

Job no.: 5000 / 65436 Page 10Date: 1/16/2003

Fraction: 700+


Density @ 70 °C D 4052 g/ml 0.9067API Gravity @ 60°F D 1298 18.22Sulphur Content D 2622 wt% 0.513Nitrogen content D 5762 mg/kg 1930Pour Point D 5950 °F 5UOP K Factor UOP 375 11.8Kinematic Viscosity @ 180 °F D 445 mm²/s 61.52Aniline Point D 611 °F Too darkAcid Number D 664 mgKOH/g 0.77Micro Carbon Residue D 4530 wt% 2.7Ramsbottom Carbon residue D 524 wt% 3.6Distillation at reduced pressure D 1160 ----Initial Boiling Point °F 7215 % Recovered °F 73910% °F 74520% °F 75630% °F 77440% °F 79350% °F 81760% °F 84470% °F 87180% °F 90390% °F 94195% °F 973Final Boiling Point °F 1002Recovery vol% 98Loss vol% 2.0Basic Nitrogen UOP 269 mg/kg 783

Job no.: 5000 / 65436 Page 11Date: 1/16/2003

Fraction: 1000+


Density @ 70 °C D 4052 g/ml 0.9329API Gravity @ 60°F D 1298 14.22Sulphur Content D 2622 wt% 0.675Nitrogen content D 5762 mg/kg 3370Pour Point D 5950 °F 70Kinematic Viscosity @ 180 °F D 445 mm²/s 720.0Aniline Point D 611 °F Too darkAcid Number D 664 mgKOH/g 0.96Ramsbottom Carbon residue D 524 wt% 8.3Basic Nitrogen UOP 269 mg/kg 1590

for BSI INSPECTION NETHERLANDS B.V

Sunill Sewdajal

160103 gryphon blend assay

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