4955 yarrow street avda, co 80002
TRANSCRIPT
i
STLSTL Denver4955 Yarrow StreetAvda, CO 80002
TEl: 303 736 0100 Fax: 303 431 7171www.stHnc.com
ANALYTICAL REPORT
URENCO Project
Lot#: D4D030176
Purchase Order 018511-0403003
Frank Bellini/Carl Jackson
Lockwood Greene1500 International DriveSpartanburg, SC 29304
SI DENVER
Project Manager
April 29,2004
Severn Trent LoMWIM Inc.
Table Of ContentsStandard Deliverables
Report Contents Total Numberof Pages
Standard DeliverablesThc Cover Letter and the Report Cover page are considered integralparts of this tdardDeliverablepackage. This report i incompleteunless all pages bniated in this Table of Contents are included
* Table of Contenlts
* Case Narrative
* Executive Summary - Detection Highlights
* Methods Summary
* MethodlAnalyst Summary
* Lot Sample Summary
* Analytical Results
* QC Data Association Summary
* Chain-of-Custody
N:-PMs\Fors\toc suddoc
Lot#: D4D030176
Case NarrativeEnclosed is the report for eight samples received at STL's Denver laboratory on Apri 3, 2004. Theresults included in this report have been reviewed for compliance with STL Denver's Laboratory QualityManual. The test results shown in this report meet all requirements of NELAC and any exceptions arenoted below.
Dilution factors and footnotes have been provided to assist in the interpretation of the results. Eachsample was analyzed to achieve the lowest possible reporting limit within the constraints of the method.In some cases, due to interferences or analytes present at concentrations above the linear calibrationcurve, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilutionrequired.
STL utilizes USEPA approved methods in all analytical work. The samples presented in this report wereanalyzed for the parameters listed on the analytical methods summary page in accordance with themethods indicated. A summary of quality control parameters is provided below.
This report shall not be reproduced except in fiul without the written approval of the laboratory.
Quality Control Sunmmary for Lot D4D030176
Sample Receiving
> The cooler temperature upon receipt at the Denver laboratory was 2.3 C.
> All sample bottles were received in acceptable condition.
Holding Times
> All holding times were met.
Method Blanks
> The analytes Acetone, Naphthalene, and Toluene by Method 8260B were detected in the MethodBlank below the established reporting limits. No corrective action is taken for any values in MethodBlanks that are below the requested reporting limits.
S> All other Method Blanks were within established control limits.
Laboratory Control Samples
> The LCS and LCSD recoveries were above the upper control limits for all compounds except for theDemeton LCSD by Method 8141A. In addition the relative percent difference (RPD) was outsidecontrol Emits for Demeton (total). The associated sample results are still considered valid becausenone of the target compounds were detected.
> The LCS recovery was above the upper control limit for 2,4-D by Mcthod SISlA at 93%. Inaddition the surrogate recovery for DCAA was above the upper control limit for the LCS. Theassociated sample results are still considered valid because 2,4-D was not detected.
> All other Laboratory Control Samples were within established control limits.
Lot#: D4D030176
Matrix Spike (MS) and Matrix Spike Duplicate (MSD)
> The Matrix Spike and Matrix Spike Duplicate recoveries were outside control limits for allcompounds except Ethyl parathion by Method 8141A; for all compounds in the MS by Method8151A; and for Arsenic, Lead, Selenium, and Silver in the MS by Method 601OB. The RPD wasoutside control limits for all Method 6010B metals except Chromium. In addition the surrogaterecovery of DCAA was outside control limits in the MS by Method 8151A Because thecorresponding Laboratory Control Samples and the Method Blank samples were within controllimits, these anomalies may be due to matrix interference.
> The MS/MSD recoveries, surrogate recoveries, and RPD could not be determined for Methods8270C and 808 IA because of the dilutions performed on the samples.
) All other MS and MSD samples were within established control limits.
Organics
> The relative percent difference between the primary and confirmation columns exceeded 40%/. for4,4'-DDD in samples SS-6, SS-9, SS- 1, and SS-12. The lower of the two results is reported.
> Samples SS-13, SS-15, and SS-16 were analyzed at a dilution for Pesticides by Method 80S8A due tothe presence of interfering, non-target compounds. Continuing Calibration Verification (CCV)standards for 4,4'-DDT and Methoxychlor failed when these samples were run without dilution.Therefore, it was necessary to analyze with dilution to obtain passing QC samples. The reportinglimits were raised according to the dilution level. As a result of the dilutions, the surrogaterecoveries could not be determined.
> The surrogate recoveries for DCAA in samples SS-13 and SS-15 were above the upper control limitin Method 815IA. The sample results are still considered valid because no target analytes weredetected.
> The internal standard recoveries for 1,4-Dichlorobenzene-d4 were outside control limits for sampleSS-6 and the MS/MSD performed on this sample by Method 8260B. Because the failed recoverieswere confirmed repeatedly on sample SS-6, matrix effects are confirmed.
> The Continuing Calibration Verification (CCV) standards for Demeton-S, 0,0,0-Triethylphosphorothioate, Dichlorvos, Azinphos-methyl, Mevinphos, Dimethoate, Malathion,Tetrachlorvinphos, and Naled by Method 8141A exceeded the percent difference limits in variousruns and columns. However, the overall mean percent difference is within control limits, therefore,the CCV is also in control and no corrective action was necessary. Additionally, the associatedsamples were non-detect.
> The Continuing Calibration Verification (CCV) standards for Dichloroprop, MCPP, DCAA,Dicamba, Dinoseb, MCPA, and 2,4-DB by Method 8151A exceeded the percent difference limits invarious runs and columns. However, the overall mean percent difference is within control limits,therefore, the CCV is also in control and no corrective action was necessary. Additionally, theassociated samples were non-detect.
> The Continuing Calibration Verification (CCV) standards for Heptachlor, 4,4'-DDE, Endrin, 4,4'-DDD, 4,4'-DDT, DCB, Methoxychlor, Endosulfan 1, Eadrin aldehyde, Endosulfan sulfate, and delta-BHC by Method 8081A exceeded the percent difference limits in various runs and columns.However, the overall mean percent difference is within control limits, therefore, the CCV is also incontrol and no corrective action was necessary. Additionally, the associated samples were non-detect below the reporting limit.
EXECUTVE SUMMARY - Detection H igg
D4D030176
REPORTINGLIMIT
ANALYTTCALME'THODPARAMETER RESULT UNITs
-
8S-2 04/01/04 12:30 001
ArsenicLeadBariumChromiumSilverAcetoneXylenes (total)1,2,4-Trimethylbenzenem-Xylene & p-Xyleneo-XylenePercent Moisture
0.76 B2.8225.90.099 B4.2 J,B0.93 J0.30 J0.56 a0.37 J1.6
1.00.811.01 .01.0205.15.12.52.50.10
mg/kgmg/kgmg/kgmg/kgmg/kgug/kgug/kgug/kgug/kgug/kg
&W8468W8468W846SW8468W8468W8468W846SW846&W846SW846MCAWW
6010B6010B6010B6010B6010B8260B8260B8260B8260B8260B160.3 MOD
SS-6 04/01/04 10:40 002
4,4' -DDD
ArsenicLeadBariumChromiumsilverAcetoneXylenes (total)1,2,4-Trimethylbenzenem-Xylene a p-Xyleneo-XylenePercent Moisture
0.44Qualifiers:
0.76 B
2.2153.10.10 B5.6 J,B1.0 J0.33 J0.73 J0.28 J1.3
1.7JCOL
1.00.811.01.01.0205.15.12.52.50.10
ug/kg
mg/kgmg/kgmg/kgmg/kgmg/kgug/kgug/kgug/kgug/kgug/kgt
SW846 8081A
8W8466W8466W8468W8468W8468W8468W846BW8468W84651(846
DACAWN
6010B6010B6010B6010B6010B8260B8260B8260B8260B8260B160.3 MOD
8S-9 04/01/04 15s15 003
4,4' -DDD
LeadBariumChromiumSilverAcetoneXylenes (total)o-XyleneFluoridePercent Moisture
0.39Qualifiers:
3.3533.40.085 B3.9 .,B0.72 J0.32 J1.0 B1.2
1.7J,COL
0.811.01.01.0205.12.51b0.10
ug/kg
mg/kgmg/kgmg/kgmg/kgug/kgug/kgug/kgmg/kgt
8W846 8081A
8W8468W8468W8468W8466W846
W81466W846SW846MCAWN
6010B6010B6010B6010B8260B8260B8260B9056160.3 MOD
(continued on next page)
EXC1IVE SUNM4ARY - Detection 1ig4light
D4D030176
REPORTINGL3MIT
ANALYTICALMETHODPARAMETER RESULT WNITS
&S-ll 04/01/04 10s00 004
4,4'-DDD
ArsenicLeadBariumChromiumSilverAcetoneSylenes (total)1,2,4-Trimethylbenzenem-Xylene & p-Xyleneo-XyleneFluoridePercent Moisture
0.79Qualifiers:
0.89 B2.8193.40.11 B3.8 J,B0.73 J0.23 J0.43 J0.30 J1.2 B1.3
1.7J,COL
1.00.811.01.01.0205.15.12.52.5100.10
ug/g
mg/kgmg/kgmg/kgmg/kgmg/kgug/kgug/kgug/kgug/kgug/kgmg/kgt
SW846 8081A
SW846SW846SW8468WE468W8468W846SW846SW846SW8468W8468W846MCAWW
6010B6010B6010B6010B6010B8260B8260B8260B8260B826099056160.3 MOD
SS-12 04/01/04 15:40 005
4,41'-DDD
ArsenicLeadBariumChromiumSilverXylenes (total)1,2,4 -Trimethylbenzenem-Xylene & p-Xyleneo-XylenePercent Moisture
0.65Qualifiers:
0.77 B2.7193.50.10 B1.6 i0.45 J1.1 J0.50 J1.5
1.7J,COL
1.00.811.01.01.05.15.12.52.50.10
ug/kg
mg/kgmg/kgmg/kgmg/kgmg/kgug/kgug/kgug/kgug/kgt
5846 8081A
SW846 6010BSW846 6010B8W846 6010B5W846 6010B8W846 6010B8W846 8260B8W846 8260B8W846 8260B8W846 8260BMCAWW 160.3 MOD
8S-13 04/01/04 16:10 006
LeadBariumChromiumXylenes (total)1,2,4-Trimethylbenzenem-Xylene & p-Xyleneo-XylenePercent Moisture
2.6163.01.1 J0.38 J0.82 J0.31 J1.1
0.81 mg/kg1.0 mg/kg1.0 m Mg/kg5.1 ug/kg5.1 ug/kg2.5 ug/kg2.5 ug/kg0.10 k
SW846S8w468WS468W846-8W8468w8468W846MCAWW
6010B6010B60109.8260B8260B8260B8260B160.3 MOD
(Continued on next page)
EXECUTIVE SUMMARY - Detection Eiglights
D4D030176
REPORTINGLIMIT
AhLYTICALMEIHODRESULT UNITS
SS-15 04/01/04 13:10 007
LeadBariumChromiumSilverXylenes (total)1,2,4-Trimethylbenzenem-Xylene & p-Xyleneo-XyleneFluoridePercent Moisture
SS-16 04/01/04 14:4O 008
2.5173.10.10 B
1.1 .0.35 J0.78 J
0.31 J1.0 B1.2
0.811.01.01.05.15.12.52.5100.10
mg/kgmg/kgmg/kgmg/kgug/kgug/kgug/kgug/kgmg/kg
SW846SW846SW846
SW8468W846W8846
8W846SW846SW846McaswK
6010B6010B6010B6010B8260B8260B8260B8260B9056160.3 MOD
ArsenicLeadBariumchromiumSilverXylenes (total)1,2,4-Trimethylbenzenem-Xylene & p-Xylene
o-XyleneNaphthalenePercent Moisture
0.96 B2.9 -243.7
0.11 B
1.4 J0.48 J0.99 .0.44 J0.69 JB,0.81
1.00.811.01.01.05.0'5.02.52.55.00.10
mrg/kgmg/kgmg/kgmg/kgmg/kgug/kgug/kgug/kgug/kgug/kg
SW8468W8468W8468W8466W846SW846
SW8466W846SW846BW846McaWw
601036010B6010B6010B6010B8260B8260B8260B8260B8260B160.3 MOD
METHOD J ANALYSF SUMRMAY
D4D030176
ANALYTICAL3TR'rZTfln
ANALYSTID1]T& T.P
MCAW8W8468W8460W8468W8466W8468W846SW8468846
160.3 MOD6010B7471A8081A8141A8151A8260B8270C9056
Jean CarrierLynn-Anne TrudellRacey OnoMike DobranskySonya DacarHeather DybasDan AppelhansRwanda TodeaAndrita Scofield
0087636645003371008777011595038161001008005716004409
References :
MCAWW wMethods for Chemical Analysis of Water and Wastes",EPA-600/4-79-020, March 1983 and 6ubSequent revisions.
SW846 OTest Methods for Evaluating Solid Waste, Physical/ChemicalMethods*, Third Edition, November 1986 and its updates.
SAMLE SUMMARY
D4D030176
SAMPLED SAMPNO t SAMPLE# CLIENT SAMPLE ID DATE Tn4E
GDHQL 001 SS-2 04/01/04 12:30GDHQX 002 8S-6 04/01/04 lO40G=HQO 003 SS-9 04/01/04 15215GDHQ1 004 88-11 04/01/04 10:00GDHQ2 005 SS-12 04/01/04 15:40GDHQ3 006 SS-13 04/01/04 16,10GDHQ4 007 SS-lS 04/01/04 13:1OGDHQ5 008 SS-16 04/01/04 14:40
NOTE(S)X-lbe maltydeal radu ore e .h e iced above m prmd en ie iov pps.
- Alokdnms amperfomedbefore roidAg sbroaind-44ff esonh cabavesfrnks.Rsultm aoted as 'W on oat detectd stm above bie sated EmIL
rmepour mm ant be reproduced. enxt in Al. wki fte wrm aroVa of die laboratory.-Remus for e Wowing purmnets am new rped on a dry weight baft color. cormasIy. deantyffapout. Iiabi, kyys; odor,
paint miltr est . potost pese mady. rplox potmu1. vepdrr pgravi Vt Oests. sohibIty, dmp-.ai . viscoity. ad wd
METHODS SUMMARY
D4D030176
ANALYTICALPARAMETER METHOD
PREPARATIONMETHOD
Chlorinated Herbicides by GCFluorideInductively Coupled Plasma (ICP) MetalsMercury in Solid Waste (Manual Cold-Vapor)Organochlorine PesticidesOrganophosphorous Compounds by GCPercent MoistureSemivolatile Organic Compounds by GC/MSVolatile Organics by GC/MS
SW8466W846SW8468W846SW846SW846MCANWSW846SW846
815LA90566010B7471A80812k8141A160.3 MOD8270C8260B
8W8466W846SW8468W8468W846
MCAWWSW846SW846
8151A90563050B7471h3550
160.3 MOD3550B5030B/826
References:
MCAW
8W846
'methods for Chemical Analyois of Water and Wastes',EPA-600/4-79-020, March 1983 and subsequent revisions.
"Test Methods for Evaluating Solid Waste, Physical/Chemical
Methods", Third Edition, November 1986 and its updates.
Client Sample ID: 8S-2
GC/MS Volatiles
bot-&le #...sDate Sampled...:Prep Date......:Prep Batch t...sDilution Factor:
D4D030176-00104/01/04 12:3004/12/0441042741
Work Order C...:Date Received..:analysis Date..:Analysis Time..:
GDHQL1AF04/03/0404/12/0413:46
Matrix ......... sOLID
Nethod . ... : 6W846 8260B
PARAMETERAcetoneBenzeneBromodichloromethaneBromoformBromomethane2-Butanone (HEM)carbon tetrachlorideChlorobenzeneChloroetbaneChloroformChloromethaneDibromomethane1,2-Dibromoethane CEDB)1,2-Dichlorobenzene1,3-Dichlorobenzene1,4-DichlorobenzeneDihlorodifluoromethane1,1-Dichloroethane1,2-Dichloroethane1,1-Dichloroethene1,2-Dichloroethene
(total)cis-1,2-Dichloroethenetrans-1,2-Dichloroethene1,2-Dichloropropanecis-1, 3-Dichloropropenetrans-1,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1,1,1,2-Tetrachloroethane1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1,2,4-Trichloro-
benzene
RESULT4.2 J,BNDNDED2NDllDEDEDNDlNDNDNDNDEDNDNDNDNDNDNDND
NDNDNDEDND
NDNDNDNDNDNDNDNDNDND
REPORTINGLIMIT205.15.15.110205.15.11010105.15.15.15.15.1105.15.15.15.1
2.52.55.15.15.15.1205.1205.15.15.15.15.15.1
UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgugtkgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
(Continued on next page)
lDICKHOO GEM
Client SaLMple ID: SS-2
GC/MS Volatiles
Lot-Sanple I...: D4D030176-001 Work Order e...: GDHQL1AA Hatrri .... : SOLID
1,1,1-Trichloroethane1,1,2-TrichloroethaneTrichloroetheneTrichlorofluoromethane1,2,3-TrichloropropaneVinyl chlorideXylenes (total)n-Butylbenzenesec-ButylbenzeneIsopropylbenzene1 2,4-Trimetbylbenzene1,3,5-Trimethylbenzenen-Propylbenzenetert-ButylbenzeneDibromochloromethane2-chlorotoluene4-Chlorotoluene1,2-Dibromo-3-
chloropropane (DBCP)1,3-Dichloropropane2,2-Dichloropropane1,1-Dichloropropenenexachlorobutadiene4-IsopropyltolueneMethyl tert-butyl ether1,2,3-Trichlorobenzenem-Xylene & p-Syleneo-XyleneBromobenzeneBromochloromethbaeNaphthalene
RESULTNDNDNDNDm JND0.93 J7ND0mND0.30 JNDEDIDEDEDNDND
ND
EDEDEDND
0.56 i0.37 JEDEDED
REPORTINGLIMIT5.15.15.1105.15.15.15.15.15.15.15.15.15.15.15.15.110
5.15.15.15.15.1205.12.52.55.15.15.1
UNITSug/kgug/kgug/kg
ug/kgug/kgug/kg
ug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kg
ug/kgug/kgug/kgug/kgug/kg
ag/kgtg/kgug/kgug/kg
ug/kg
SURROGATE
Dibromofluoromethane1,2-Dichloroethane-dt4-BromofluorobenzeneToluene-dB
PERCENT
RECOVERY941029396
RECOVERYLIMITS(71 - 136)(67 - 131)(71 - 124)(77 - 129)
OTE(S) _Rksuand &e on Um skhm bmee auad y .wcId.
I Esz dult. Rem n tkI= 9taRL
B )&eUd blank c m inaro. Th asscat medid blank woubiwm be ft get i t a mprorbk kgd.
WLOD GBE
Client Sample ID: 88-6
GCUMS Volatiles
Lot-Sample C... : D4D030176-002 Work Order g ... 1Date Sampled ... : 04/01/04 10:40 Date Received..sPrep Date ......: 04/12/04 Analysis Date..:Prep Batch 1... : 4104274 Analysis Titae..:Dilution Factor: 1
GDHQX1AA04/03/0404/12/0414:09
Katri ...... : SOLID
Hethod . . : SW846 8260B
PARAMETERAcetoneBenzeneBromodichloromethaneBromofor=Bromomethane2-Butanone (MEK)Carbon tetrachlorideChlorobenzeneChloroethaneChloroformChloromethaneDibromomethane1,2-Dibromoethane (EDB)1,2-Dichlorobenzene1,3-Dichlorobenzene1,4-DichlorobenzeneDichlorodifluoromethane1,1-Dichloroethane1,2-Dichloroethane1,1-Dichloroethene1,2-Dichloroethene
(total)cis-1, 2-Dichloroethenetrans-1,2-Dichloroethene1,2-Dichloropropaneci6 -1,3-Dichloropropenetrans-1,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1,1,1,2-Tetrachioroethane1,1,2,2-TetrachloroetbaneTetrachloroetheneToluene1,2,4-Trichloro-
benzene
RESOaT
5.6 J,BEDNDNDEDlDNDNDEDlDEDD
NDNDNDEDNDEDNDNDND
REPORTINGLIMIT205.15.15.110205.15.11010105.15.15.15.15.1105.15.15.15.1
UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
NDEDNDNDNDNDllDNDNDNDNDNDIDNDND
2.52.55.15.15.15.1205.1205.15.15.15.15.15.1
(Continued on next page)
WM GREENE
Client Sanple mD: SS-6
GC/MS volatiles
Wt-Saiple I...: D4D030176-002 work order I... GDHQX1LA Hatrir .... : SOLID
PARAMETER1,1, 1-Trichloroethane1,1,2-TrichloroethaneTrichloroetheneTrichlorofluoromethane1,2,3-TrichloropropaneVinyl chlorideZylenes (total)n-ButylbenzeneBec-Butylbenzenelsopropylbenzene1,2,4-Trimetylbeanzene1,3,5-Trimethylbenzene
n-Propylbenzenetert-ButylbenzeneDibranochloromethane2-Chforotoluene4-Chlorotoluene1,2-Dibromo-3-
chloropropane (DBCP)1,3-Dichloropropane2,2-Dichloropropane1,1-Dichloropropene
Hexachlorobutadiene4-IsopropyltolueneMethyl tert-butyl ether1,2,3-Trichlorobenzenem-Xylene & p-Xylezeo'-XylenieBromobenzeneBromochloromethaneNaphthalne
RESULTND
VDEDEDDD
ND1.0 LT
ND
NDND0.33 JNDNDNDiDD
IDND
REPORTINmLIMIT5.15.15.1105.15.15.15.15.1
5.1
5.1,5.15.15.15.15.15.110
UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kg
WDNDNDNDNDNDND0.73 ;1Q.28 J
1D1DND
5.15.15.15.15.1205.12.52.55.15.15.1
SURROGATEDibromofluoromethane1,2-Dichloroethane-d44-BromofluorobenzeneToluene-d8
PERCENTRECOVERY98103
9592
RECOVERYLIMITS(71 - 136)(67 - 131)
(71 - 124)(77 - 129)
NOTE(S):Res snd pordn afts bkvc been adused zr t weighbt
I Esntmted iML balt Is less fta RL
B Mcdbd blank ammaina. TIM asoiated medod blak watains Me Irge mlyte at a rontae level.
Client Sample ID: SS-9
GC/hs Volatiles
Lot-Sample i...:Date Sanpled...:Prep Date ...... :Prep Batch I...:Dilution Factor:
D4D030176-00304/01/04 15S:1504/12/0441042741
work Order C..:Date Received..:Analysis Date. .:Analysis Time..:
GDHQ01APL04/03/0404/12/0414:32
Matrix ..... S : OLID
Method . ... : SW846 8260B
PARAMETERAcetoneBenzeneBromodichloromethaneBromoformBroamomethane2-Butanone (MEE)Carbon tetrachlorideChlorobenzeneChloroethaneChloroformChlorometbaneDibromomethane1,2-Dibromoethane (EDB)1,2-Dichlorobenzene1,3-Dichlorobenzene1,4-DichlorobenzeneDichlorodifluoromethane1, 1-Dichloroethane1, 2-Dichloroethane1,1-Dichloroethene1,2-Dichloroethene
(total)cis-1,2-Dichloroethenetrans-1,2-Dichloroethene1,2-Dichloropropanecis-1, 3-Dichloropropenetrans-1,3-DichloropropeneEthylbenzene2-KexanoneMethylene chloride4-Methyl-2-pentanonestyrene1,1,1,2-Tetrachloroethane1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1,2,4-Trichloro-
benzene
RESULT3.9 J,BEDEDNDNDEDNDEDNDEDIDNDNDNDEDNDEDEDEDEDND
NDNDlDEDINDNDNDNDNDEDNDNDNDEDED
REPORTIMG
LIMI205.15.15.110205.15.11010105.1
5.15.15.15.1105.15.15.15.1
2.52.55.15.15.15.1205.120
5.1S.15.15.15.15.1
UNITSugfkgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kguglkguglkgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
(Continued on next page)
I
Client Sample ID: 8S-9
GC/MS Volatiles
Lot-Sample #...: D4D030176-003 Work Order t...: GDHQO1AA Matriz ......... : SOLID
PAEAMETER
1,1,2-Trichloroethane
TrichloroetheneTrichlorofluoromethane1,2,3-TrichloropropaneVinyl chlorideXylenes (total)n-Butylbenzenesec-ButylbenzeneIsopropylbenzene1,2,4-Trimethylbenzene1,3,5-Trimethylbenzenen-Propylbenzenetert-ButylbenzeneDibromochloromethane2-Chlorotoluene4-Chlorotoluene1,2-Dibromo-3-
chloropropane (DBCP)1,3-Dichloropropane2,2-Dichloropropane1,l-DichloropropeneRexachlorobutadiene4-IsopropyltolueneMethyl tert-butyl ether1,2,3-Trichlorobenzenem-Xylene & p-Xyleneo-XyleneBromobenzeneBromochloromethaneNaphthalene
RESULTNDNDNDNDNDWD0.72 JNDNDNDNDNDNDNDNDNDNDND
NDNDDNDNDNDNDND0.32 JNDNDND
REPORTINGLIMIT5.15.15.1105.15.15.15.15.15.15.15.15.15.15.15.15.110
5.15.15.15.15.1205.12.52.55.15.15.1
UNITSug/kgug/kgug/kgug/kgug/kgug/kguglkgug/kguglkgug/kguglkguglkgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kguglkguglkgug/kguglkguglkgug/kguglkgugtkgugtkg
SURROGATEDibromofluoromethaine1, 2-Dichloroethane-d44-BromofluorobenzeneToluene-d8
PERCENTRECOVERY951049296
RECOVERYLIMITS(71 - 136)(67 - 131)(71 - 124)(77 - 129)
NOTE(S):Iur and otlg lmits km ben aiuged br dry weghs.I Egbmted mh. Re* I ess 9i ILI M&odblan ma wa. Tae cae meod blnk cuos btc ge utca armb levd.
Client Sample ID: SS-lI
GC/MS Volatiles
Lot-Sample ... :Date Sampled...:Prep Date ...... :Prep Batch t...:Dilution Factor:
D4D030176-00404/01/04 10:0004/12/0441042741
Work Order #...:Date Received..:Analysis Date..:Analysis Time..s
GDHQ11AA04/03/0404/12/0414:55
NatriX .... .: SOLID
Method .... : SW846 8260B
PARAMETERAcetone
BenzeneBromodichloromethaneBromoformBromomethane2-Butanone (MEK)Carbon tetracbloride
ChlorobenzeneChloroetbxaechloroform
ChlorometbaneDibromometlane1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene1,3-Dichlorobenzene1,4-DichlorobenzeneDichlorodifluoromethane1,l-Dichloroethane1,2-Dichloroetbane1,1-Dichloroethene1,2-Dichloroethene
(total)cis-1,2-Dichloroethenetrans-1,2-Dichloroethene1,2-Dichloropropanecis-l,3-Dichloropropenetran -1,3-DichloropropeneEthylbenzene2-NexanoneMetbylene chloride4-Methyl-2-pentanoneStyrene1,1,1,2-Tetrachloroethane1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1,2,4-Trichloro-
benzene
RESULT
3.B IBNDNDNDNDND
NDNDNDNDNDEDNDNDNDNDRDNDNDND
REPORTINGLIMIT20
5.15.15.110205.15.11010105.15.15.15.15.1105.15.15.15.1
UTSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
NDNDNDNDNDNDNDNDNDNDNDNDNDNDND
2.52.55.15.15.15.1205.1205.15.15.15.15.15.1
(Continued on next page)
XcKKOOD GREEKE
Client Sample ID: 8S-11
GC/MS Volatiles
Wt-Sample Y...: D4D030176-004 Work Order t...: GDEQ11AP Matrix .. .a SOLID
PARAMETER1,1,l-Trichloroethane1,1,2-TrichloroethaneTrichloroetheneTrichlorofluoromethane1,2,3-TrichloropropaneVinyl chlorideSylenes (total)n-Butylbenzenesec-ButylbenzeneIsopropylbenzene1,2,4-Trimethylbenzene1,3,5-Trimethylbenzenen-Propylbenzenetert-8utylbenzeneDibrocochloromethane2-chlorotoluene4-Chlorotoluene1,2-Dibromo-3-
chloropropane (DBCP)1,3-Dichloropropane
2,2-Dichloropropane1,1-DichloropropeneNexachlorobutadiene4-IsopropyltolueneMethyl tert-butyl ether1,2,3-Trichlorobenzenea-Xylene & p-Xyleneo-XyleneBromobenzeneBromochloromethaneNaphthalene
RESULTNDNDNDNDEDED0.73 JNDNDND0.23 ZEDNDNDNDNDEDND
REPORTINGLIMIT5.15.15.1105.15.15.15.15.15.15.15.1
5.15.15.15.15.110
UNITSug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ugfkgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug1kg
ug/kg
ug/kgug/kg
NDNDNDND
NDEDND0.43 40.30 JNDNDND
5.15.15.15.15.1205.12.52.55.15.15.1
SURROGATEDibromofluoromethane1,2-Dichloroethane-d44-BromofluorobenzeneToluene-d8
PERCENTRECOVERY991039295
RECOVERYLIMITS(71 - 136)(67 - 131)(71 - 124)(77 - 129)
NOTE(S):
R ts, sad eponlg Emhs have be jszW fr dry we k
I Esnaed la& R t s lss 3m EL
B Medod blank c mnhaioo. To associd m hod blan ontains tIe u e o te at a epo bk lvel.
Client Sample ID: 88-12
GC/MS Volatiles
Lot-Sample C...s D4D030176-005 Work Order C...:Date Sampled ...: 04/01/04 15:40 Date Received..:Prep Date ...... s 04/12/04 Analysis Date.. :Prep Batch #...: 4104274 Analysis Time-.:Dilution Factor: I
GDEQ21AA04/03/0404/12/0415:19
Katrix .... SOLID
Nethod.........: SW846 8260B
AcetoneBenzeneBromodichloromethaneBromoformBromomethane2 -Butanone (MEM)Carbon tetrachlorideChlorobenzeneChloroethaneChloroformChloromethaneDibromometbane1,2-Dibromoetbane (BDB)1,2-Dichlorobenzene1,3-Dichlorobenzene1,4-DichlorobenzeneDichlorodifluoromethane1, 1-Dichloroethane1,2-Dichloroethane1,l-Dichloroethene1,2-Dichloroethene
(total)cis-1, 2-Dicbloroethenetrans-1,2-Dichloroethene1,2-Dichloropropaneci-i,3-Dichloropropenetrans-1,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1,1,1,2-Tetrachloroethane1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1,2,4-Trichloro-
benzene
RESULTND
NDNDNDNDNDNDNDNDNDNDNDNDEDNDNDNDNDNDNDND
REPORTINGLIMIT205.25.15.110205.15.11010105.15.15.15.15.1105.15.15.15.1
UNITSug/kgulg/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgUg/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
NDRDaDND1DNDNDNDNDNDNDNDNDEDND
2.52.55.15.15.15.1205.1205.15.15.15.15.15.1
(Continued on next page)
LODD -B
Client Sanple mD. SS-12
GCIKS Volatiles
Lot-Sample #I..: D4D030176-005 Work Order t...: GDHQ21AA
1,1,1-Trichloroethane1,1,2-TrichloroethaneTrichloroetheneTrichlorofluoromethbne1,2,3-TrichloropropaneVinyl chlorideZylenes (total)n-Butylbenzenesec-ButylbenzeneIEopropylbenzene1, 2, 4-Trmtbymbenzene:1,3,5-Trimethylbenzenen-Propylbenzenetert-ButylbenzeneDibromochloromethane2-Chlorotoluene4-Chlorotoluene1, 2-DLbromo-3-
chloropropane (DBCP)1,3-Dichloropropane2,2-Dichloropropane1,L-DichloropropeneHexachlorobutadiene4-I6opropyltolueneMethyl tert-butyl ether1,2,3-Trichlorobenzenem-Kylene & p-Xyleneo0-yleneBromobenzeneBromochloromethane
RESULTNDNDNDEDNDND1.6 JNDNDND0.45 JNDNDNDNDNDNDND
NDEDNDEDNDlDND1.1 J
0.50 JNDEDED
REPORTINGLIMT
5.1
5.1
5.1
10
5.1
5.1
5.1
5.15.15.15.15.1SA.5.15.15.15.110
5.15.15.15.15.1205.12.52.55.15.15.1
Matrix .... . SOLID
UTSug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kg
ug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgugtkgug/kgug/kgug/kgug/kgNaphthalene
SURROGATEDibromofluoromethane1,2-Dichloroethane-d44-BromofluorobenzeneToluene-d8
PERCENTRECOVERY98
1039199
RECOVERYLIMITS(71 - 136)(67 - 131)(71 - 124)
(77 - 129)
om (s) :Rmt md v l4 IIa have ti=e 4uswd fOr dq weigthL
I Essimted Is.aL K~ft is I= tan RL.
Client Sample ID: SS-13
GC/hS Volatiles
Lot-Sample #...:Date Sampled...:Prep Date ...... :Prep Batch #...:Dilution Factor:
D4D030176-00604/01/04 16:1004/12/0441042741
Work Order #... :Date Received. .:AnalysBi Date..:Analysis Tisme..:
GDEQ31AA04/03/0404/12/0415:42
HatriX......... : SOLID
Method ......... : SW846 8260B
PARAMETERAcetoneBenzeneBromzodichloromethaneBromoformBromomethane2-Butanone (MEK)Carbon tetrachlorideChlorobenzeneChloroethaneChloroformChloromethaneDibromometh ane1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene1,3-Dichlorobenzene1,4-DichlorcbenzeneDichlorodifluoromethane1,l-Dichloroethane1,2-Dichloroethane1,1-Dichloroethene1,2-Dichloroethene
(total)cis-1, 2-Dichloroethenetrans-1,2-Dichloroethene1,2-Dichloropropanecis-i,3-Dichloropropenetrans-1 , 3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyi-2-pentanonestyrene1,1,1,2-Tetrachloroethane1,1,2,2-Tetrachloroethane
TetrachloroetheneToluene1,2,4-Trichloro-
benzene
RESULTEDNDEDEDNDNDNDEDNDNDNDNDEDNDNDNDEDIDEDED
kD
REPORTINGLIMIT205.15.15.110205.15.11010105.15.15.15.15.1105.15.15.15.1
UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
EDNDND
EDEDEDEDEDNDNDNDNDEDNDED
2.52.55.15.15.15.1205.1205.15.15.15.15.15.1
(Continued on next page)
WLOD QREEME
Client Sazple ID: SS-13
GC/NS Volatiles
Lot-Sample #...: D4D030176-006 Work Order #...: GDHQ31AA Hatri ...... : SOLID
PARAMETER1,2,1-Trichloroethane1,1,2-TrichloroethaneTrichloroetheneTrichlorofluoromethane1,2,3-Trichloropropanevinyl chlorideZylenes (total)n-Butylbenzenesec-ButylbenzeneIsopropylbenzene1,2,4-Trimethylb e1.3,5-Trimethylbenzenen-Propylbenzenetert-ButylbenzeneDibromochloromethane2-Chiorotoluene4-Chiorotoluene1,2-Dibromo-3-
chloropropane (DBCP)1,3-Dichloropropane2,2-Dichloropropane1,1-DichloropropeneHexachlorobutadiene4-I6opropyltolueneMethyl tert-butyl ether1,2,3-Trichlorobenzeneu-Xylene & p-Myleneo-ZyleneBromobenzeneBromochloromethaneNaphthalene
RESULTND
ND
EDNRD
1.1 JNDNDND
0.38 JNDNDNDNDNDNDND
REPORTINGLIMIT5.15.15.1105.15.15.15.15.15.15.15.15.15.15.15.15.110
UNITSug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kguglkgug/kgug/kgug/kgugifug/kgug/kgug/kg
NDNDNDNDEDNDND0.82 J0.31 ZND
NDND
5.15.15.15.15.1205.12.52.55.15.15.1
SURROGATEDibromofluoromethane1,2-Dichloroethane-d44-BromofluorobenzeneToluene-de
PERCENTRECOVERY94
999293
RECOVERYLIMITS(71 - 136)(67 - 131)(71 - 124)(77 - 129)
FMS) t
Rels and repoi4da mhhave been adjusd for dry %hbL
J Esumftcd rulL Resut is ea M L
client Sample ID: ES-IS
GC/hS Volatiles
lot-Sample #...s D4D030176-007Date Sampled ...: 04/01/04 13:10Prep Date ...... : 04/12/04Prep Batch C...: 4104274Dilution Factors 1
Work order E...:Date Received..:Analysls Date..:Analysis Time..
GDHQ41AA04/03/0404/12/0416:06
Hatrix ..... s OLID
Method . .... : W846 8260B
PARAMTERAcetoneBenzeneBromodichloromethaneBromofoarmBromomethane2-Butanone (MEK)Carbon tetrachlorideChlorobenzeneCbloroethaneChloroformChloromethaneDibrowomethane1,2-Dibromoethane (EDB)1,2-Dichlorobenzene1,3-Dichlorobenzene1,4- DichlorobenzeneDichlorodifluoromethane1, 1-Dichloroethane1,2-Dichloroethane1, 1-Dichloroethene1,2-Dichloroethene
(total)cis-1, 2-Dichloroetbenetrans-1,2-Dichloroethene1,2-DichloropropaneCis-1, 3 -Dichloropropenetrans-1,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1,1,1,2-Tetrachloroethane1,122,2-TetrachloroethaneTetrachloroetheneToluene1,2,4-Trichloro-
benzene
RESULTNDNDNDNDNDNDNDND
NDNDNDNDNDNDNDEDEDhDEDED
REPORTING
205.15.15.110205.15.11010105.15.15.15.15.1105.15.15.1.5.1
UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
NDIDEDNDNDNDNDWDNDEDNDEDNDNDED
2.52.S5.15.15.15.1205.1205.15.15.15.15.15.1
(Continued on next page)
CRWOD
Client Sample ID: 8S-15
GC/HS Volatlles
Lot-Sample I...: D4D030176-007 Work Order #...t GDHQ41AA Matrix........: SOLID
PARAMETER1,1,l-Trichloroethane11, 2-TrichloroethaneTrichloroetheneTrichlorofluoromethane1, 2, 3 -TrichloropropaneVinyl chlorideXylenes (total)n-Butylbenzenesec-ButylbenzeneIsopropylbenzene1,2,4-Trimethylbenzene1,3,5-Trimethylbenzenen-Propylbenzenetert-ButylbenzeneDibromochloromethane2-chlorotoluene4-Chlorotoluene1,2-Dibromo-3-
chloropropane (DBcP)1,3-Dichloropropane2,2-Dichloropropane1,1-DichloropropeneRexachlorobutadiene4-IsopropyltolueneMethyl tert-butyl ether1,2,3-Trichlorobenzenem-Xylene & p-Xyleneo-ZyleneBromoben2zeneBromochloromethaneNaphthalene
RESULTNDNDNDNDNDND1.1 JEDNDND0.35 JNDEDEDEDNDEDND
NDNDNDNDEDNDND
0.78 JT0.31 JNDNDND
REPORTING
LIMIT5.15.15.1105.15.15.L5.15.15.15.15.15.15.15.15.15.110
5.15.15.15.15.1205.12.52.55.15.15.1
UISuglkgug/kgug/kg
ug/kgug/kgug/kguglkgug/kgug/kgug/kguglkgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
SURROGATEDibromofluoromethane1,2-Dichloroethane-d44-BronofluorobenzeneToluene-d8
PERCENTRECOVEY961049495
RECOVEY
LIMITS(71 - 136)(67 - 131)(71 - 124)(77 - 129)
POTE(S)Resok wd .prti llmhs bave been Arustad fJr jy wdehL
I Es-aid resuk. Ret bles dun RL,
Client Sample ID: SS-16
GC/MS Volatiles
Iot-Sample t...: D4DW30176-008 Work Order C...Date Sampled ... : 04/01/04 14:40 Date Received..:Prep Date ...... : 04/12/04 Analysis Date..:Prep Batdh 1 ... : 4104274 Analysis Time..:Dilution Factor: 1
GDIQ51AA04/03/0404/12/0417:16
Matrix ........ : SOLID
Metbod......... : SW846 8260B
PARAMETERAcetoneBenzeneBromodichloromethaneBromoformBrwomzethane,2-Butanone (t=)Carbon tetrachlOrideChlorobenzeneChloroethanchloroformCfhloromethaneDibromomethane1,2-Dibromoetbsule (EDB)1,2-Dicblorobenzene1,3-Dichlorobenzene1,4-DichlorobenzeneDichlorodifluoromethane1,1-Dichloroethane1,2-Dichloroethane1,1-Dichloroethene1.2-Dichloroethene
(total)cis-1,2-Dichloroethenetrans-1,2-Dichloroethene1 2-Dicbloropropanecis-1, 3-Dichloropropenetrans-1,3-DichloropropeneEthylbenzene2-HexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1,1,1,2-Tetrachloroethane1,1,2,2-TetrachloroethaneTetrachloroetheneToluene1,2,4-Trichloro-
benzene
RESULTNDNDNDNDNDEDEDNDNDNDNDEDEDNDNDNDND1DNDEDND
REPORTINGLIMIT205.05.05.010205.05.01010105.05.05.05.05.0105.05.05.05.0
UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
NDhDEDND
NDEDNDNDNDNDNDNDND
NDND
2.52.55.05.05.05.0205.0205.05.05.05.05.05.0
(Continued on next page)
COOD R
Client Sample ID: 8S-16
CC/MS Volatiles
Iot-Bample ...: D4D030176-008
PARAMETER1.1,1-Trichloroethane1,1, 2-Trichloroeth~neTrichloroetheneTrichlorofluoromethane1,2,3-TrichloropropaneVinyl chlorideXylenes (total)n-Butylbenzenesec-ButylbenzeneIsopropylbenzene1,2,4-Trimethylbenzene1,3,5-Trimethylbenzene.n-Propylbenzenetert-ButylbenzencDibremochlorometbane2-Chlorotoluene4-Cblorotoluene1,2-Dibromo-3-
chloropropane (DBCP)1,3-Dichloropropane2,2-Dichloropropane1,1-DichloropropeneNexachlorobutadiene4-IsopropyltolueneMethyl tert-butyl ether1,2,3-Trichlorobenzenem-Xylene & p-Xyleneo-ZyleneBromobenzeneBromochlorcmethaneNaphthalene
Work Order 0...: GDHQ51A&
RES=UTNDNDEDEDNDND1.4 JVDEDND0.48 vTNDNDEDNDJD
EDND
NDNDNDNDNDD
ND0.99 J0.44 JNDND0.69 JB
REPORTINGLIMIT5.05.05.0105.05.0S.05.0S.05.05.05.0S.05.05.05.05.010
5.05.05.05.05.0205.02.52.55.05.05.0
matrix . ... SOLID
UNITSug/kgug/kgug/kgug/kg
Ug/kgug/kg
ug/kgug/kgug/kgtag/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
SURROGATEDibromofluoromethane1,2-Dichloroethane-d44-BromofluorobenzeneToluene-dS
PERCENTRECOVERY971039394
RECOVERYLIMITS(71 - 136)(67 - 131)(71 - 124)(77 - 129)
r8 (SI):R=Ii mad repotdng Eit have been ajd fr dry wegh
I Psdam fes Rulst is Wu Ita ILB MedWd blank ecasnlson The asdated mxthod blank conais dIlw ltget u nate ta m mic level.
Client Sample ID: 6S-2
GC/NS Cemivola
Lat-Saxple t ... :Date Sampled ... :
Date ... .... s
Prep Batch #...:Dilution Factor:
D4D030176-00104/01/04 12:3004/07/0440976211
Work Order I...:Date Received..:Analysia Date.. 3Analysis Tim-e.:
GDHQL1AC04/03/0404/22/0415:54
Matrix . . a SOID
Method......... : 5W846 8270C
PARAMTERAcenaphtheneAcenaphthyleneAcetophenone2-Acetylamlnofluorene4-AminobiphenylAnilineAnthraceneAramiteBeazo(aWanthraceneBenzo(b)fluorantheneBenzo(k)fluorantheneBenzo(ghi)peryleneSenzo(a)pyreneBenzyl alcoholbis(2-Chloroethoxy)
methanebis(2-Chloroethyl)-
etherbis(2-Ethylhexyl)
phthalate4-Bromophenyl phenyl
etherButyl benzyl phthalate4-ChloroanilineChlorobenzilate4-Chloro-3-methylphenol2-Chloronaphthalene2-Chlorophenol4-Chlorophenyl phenyl
etherchryseneDiallateDibenz(a,h)anthraceneDibenzofuranDi-n-butyl phthalate1,2-Dichlorobenzene1,3-Dichlorobenzene1,4-Dichlorobenzene
RESULTEDEDNDIDEDNDIDNDEDRDNDND
NDED
RPORMTILIMIT34034034034001600340340670340340340340340340340
ED 340
340ED
UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kg
ug/kg
ug/kg
ug/kgug/kgug/kguglkgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ND
NDNDNDNDNDNDND
340
340340340340340340340
NDNDEDRDEDND
ED]ND
340670340340340340340340
(Continued on next page)
LOCKOOD GR
Client Sample ID: S-2
GC/MS Semivolatiles
Lot-&aWPle #...: D4D030176-001 Work Order U...: GDHQL1AC atrix ......... : SOLID
PARAMETER3,3'-Dichlorobenzidine2,4-Dichlorophenol2,6-DichlorophenolDiethyl phthalateDimetboate7,12-Dimethylben (a)-
anthracene3,3'-Dimethylbenzidine2,4-DimethylphenolDimethyl phtbalate1,3-Dinitrobenzene4,6-Dinitro-
2-methylphenol2,4-Dinitrophenol2,4-Dinitrotoluene2,6-DinitrotolueneDi-n-octyl phthalateDiphenylamineDisulfotonEthyl methanesulfonateFluorantheneFluoreneHexachlorobenzeneHexachlorobutadieneHexachlorocyclopenta-
dieneHexachloroethaneHexachioropropeneIndeno(1,2,3-cd)pyreneIsodrinI6ophoroneIsosafroleMethapyrilene3-MethylcholanthreneMethyl methanesulfonate2-MethylnaphthaleneMethyl parathion2-Methylphenol3-Methylphenol &
4-MethylphenolHaphtbalene1,4-Naphthoquinone
RESULTEDED
ND
ND
REPORTINGLIMIT1600340340670670670
EDNDEDEDPD
6703403403401600
IDEDNDNDEDNDNDNDVDNDEDIND
160034034034034016003403403403403401600
JNITS
ug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgUg/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kg
EDNDNDNDNDIDNDNDNDNDNDIDID
340340034034034067016006703403401600340340
NDNDND
34016003401-Raphthylamine
(Continued on next page)
Client Sample ID: SS-2
GC/M$ Seuivolatiles
Lot-Sample #...: D4D030176-001 Work Order xI...: GDOQL1AC Hatr i .... : SOLID
PARAMETER2-Haphthylamine2-Nitroaniline3-Nitroaniline4-NitroanilineNitrobenzene2-Nitrophenol4-Nitrophenol4-Nitroquinoline-
l-oxideU-Nitrosodi-n-butylamineH-NitrosodiethylamineU-NitrosodimethylamineU-NitrosodiphenylamineN-Nitrosodi-n-propyl-
amineN-NitrosomethylethylamineK-NitrosomorpholineN-NitrosopiperidineN-Nitrosopyrrolidine5-Nitro-o-toluidineParathionPentachforobenzenePentachloroethanePentachloronitrobenzenePentachlorophenolPhenacetinPhenaithrenePhenolPhorate2-PicolinePronamidePyrenePyridine1,2,4,5-Tetrachloro-
benzene2,3,4,6-Tetrachlorophenol
Thionazino-Toluidine1,2,4-Trichloro-
benzene2,4,5-Trichloro-
phenol2,4,6-Trichloro-
phenol
RESULTN3lDNDNDNDNDEDND
REPORTINGLh:IT34016001600160034034016003400
IDlDNDNDND
340340340340340
NDND1DNDNDEDD
NDIDNDNDRDNDNDNDNDNDNDaD
3403403403406701600340160016001600670
3403401600670670340670340
UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kg
ug/kgug/kgug/kgug/kg
Ug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kg
ug/Icgug/kgug/kgug/kgug/kgug/Jcguglkg
ug/kgug/kgug/kg
ug/kgug/kg
NDNDNDED
16001600670340
340
ND 340
(Continued on next page)
UXS0OD GRESM
Client Bample ID: ES-2
GC/HS Sezivolatiles
LOt-Sample #...t D4D030176-001 Work Order #...: GD0HQL1AC Matri....... s SOLID
PARAMETER.0,0, -Triethylphosphoro-
thioate1,3,5-Trinitrobenzene
RESULTND
REPORTING-LIMIT1600
UNITSug/kg
ug/kg1600
SURROGATE2-FluorophenolPhenol-dSNitrobenzene-dS2-Fluorobiphenyl.2,4,6-TribromophenolTerphenyl-d14
PERCENTRECOVPRY767575697179
RECOVERYLIMITS(28 - 95 )(35 - 90 )(39 - 89 )(35 - 86 )(11 - 111)(30 - 98 )
WOmE(S) XRb and ftpwq lim have ken WdW ro &Y wesk
E
Client Sample ID: SS-6
GC/NS Semivolatiles
Lot-Sample C...: D4D030176-002 Work Order 0...:bate Sanpled.... 04/01/04 10:40 Date Received..:Prep Date...... 04/07/04 Analysis Date..:Prep Batch 1...: 4097621 Analysis Time..:Dilution Factor: 1
GDHQX1AC04/03/0404/22/0416:20
Matrix ... .: SOLID
Method ........ 8W846 8270C
PARAMETERAcenaphtheneAsenaphthyleneAcetophenone2-Acetylaminofluorene4-AminobiphenylAnilineAnthraceneAramite
en o (a)anthraceneBenzo(b)fluorantheneBenzo(k)fluorantheneBenzo(ghi)peryleneEenzo(a)pyreneBenzyl alcoholbis(2-Chloroethoxy)
methanebis(2-Chloroethyl)-
etherbis(2-Ethylhexyl)
phthalate4-Bromophenyl phenyl
etherButyl benzyl phthalate4-ChloroanilineChlorobenzilate4-Chloro-3-methylphenol2-Chloronaphthalene2-Chlorophenol4-Chlorophenyl phenyl
etherChryseneDiallateDibenz(a,h)anthraceneDibenzofuranDi-n-butyl phthalate1,2-Dichlorobenzene1.3-Dichlorobenzene1,4-Dichlorobenzene
RESULTNDNDNDRDEDEDNDEDRDNDNDlDllDRDND
REPORTINGLIMIT33033033033001600330330670330330330330330330330
ED 330
ED 330
MTSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kg
ug/kg
ug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
330
RDNDNDNDNDNDND
330330330330330330330
]DIDNDEDNDEDNDND
330670330330330330330330
(Continued on next page)
LKD GRM
Client Sample IDs SS-6
GCIMS Smivolatiles
. Lot-Sample 0...: D4D030176-002 Work Order #...s GDHQX1AC Hatrix ..... : SOLID
PAFAMER3,3'-Dichlorobenzidine2,4-Dichlorophenol2,6-DichlorophenolDiethyl phthalateDinethoate7,12-Dimethylbenz(a)-
anthracene3,3'-Dimethylbenzidine2,4-DimethylphenolDimetbyl phthalate1,3-Dinitrobenzene4,6-Dinitro-
2-methylphenol2,4-Dinitrophenol2,4-Dinitrotoluene2,6-DinitrotolueneDi-n-octyl phthalateDiphenylamineDisulfotonEthyl methanesulfonateFluorantheneFluoreneEexachlorobenzeneRexachlorobutadieneHexachlorocyclopenta-
dieneHexachloroetbaneHexachloropropeneIndeno(1,2,3-cd)pyreneIsodrinIsophoroneIsosafroleMethapyrilene3-MethylcholanthreneMethyl mnethanesulfonate2-MethylnaphtbaleneMethyl parathion2-Methylphenol3-Methylphenol &
4-MethylphenolNaphthalene1,4-NaphthoqiinoneI-Naphthylamine
RESULTlDlDDD
NDRD
ND
REPORTINGLIMIT1600330330670670
670
NDNDtDNDED
670
3303303301600
NDNDNDNDNDNDNDNDNDNDEDND
160033033033033016003303303303303301600
UNITSug/kgug/kgug/kgug/kgug/kg
ug/kg
ug/kgug/kgug/kgug/kgug/kg
ug/kgug/kguglkgug/kgug/kgug/kguglkgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kg
uglkgug/kgug/kgug/kgug/kgug/kgug/kg
uglkgug/kgug/kg
NDNDNDEDD
NDEDEDNDND
IDND
330330033033033067016006703303301600330330
NDNDED
3301600330
(continued on next page)
Client Sample ID: 8S-6
GC/hS Semivolatiles
Lat-Sample 0...: D4D030176-002 Work Order t...: tDHQX1AC Natrix ........ SOLID
PARM4T2-Kaphthylamine2-Nitroaniline3-Nitroaniline4-KitroanilineNitrobenzene2-Nitrophenol4-Nitrophenol4-Nitroquinoline-
1-oxideN-Nitrosodi-n-butylamineN-NitrooodiethylamineN-NitrosodimethylamineN-NitrosodiphenylamineX-Nitrosodi-n-propyl-
amineN-NitrosomethyletbylamineN-NitrosomorpholineN-NitrosopiperidineN-Nitrosopyrrolidine5-Nitro-o-toluidineParathionPentachlorobenzenePentachloroethanePentachloronitrobenzenePentachlorophenolPhenacetinPhenanthrenePhenolPhorate2-PicolinePronamidePyrenePyridine1,24, 5-Tetrachloro-
benzene2,3,4, 6-TetrachlorophenolThionazino-Toluidine1,2,4-Trichloro-
benzene2,4,5-Trichloro-
phenol
2,4,6-Trichloro-phenol
RESULTNDNDNDEDIDNDEDND
.REPORTINGLIMIT33016001600160033033016003300
EDNDIDEDED
330330330330330
UDNDNDEDNDNDNDNDED13DNDNDEDNDEDNDNDNDND
33033033033067016003301600160016006703303301600670670330670330
UNITSug/kguglkgug/kgug/kgug/kg
ug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kg
ug/kgugtkgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kg
ug/kg
ug/kg
IDEDEDED
16001600670330
330
330
(Continued on next page)
CNOD GR
Client Sample ID: SS-6
GC/KS Semivolatiles
Lot-SaMple #...t D4D030176-002 Work Order *...: GDHQXIAC Matrix.........: SOLID
PARAMETER0,0,0-Triethylphosphoro-
thioate1,3,5-Trinitrobenzene
RESUfLTIND
REPORTINGLIMIT1600
UNITSug/kg
ug/kgID 1600
SURR~OGATE2-Fluorophenolphenol-dSNitrobenzene-d52-Fluorobiphenyl2,4,6-TribromophenolTerphenyl-dl4
PERCENTRECOVERY71717165
RECOVERYLIMITS(28 - 95 )(35 - 90 )(39 - 89 )
(35 - B6 )(11 - 111)(30 - 98 )
6679
NOTE(S):Rewtz wd rqenh4 Etsb Im t= sawd for ft w2I.
Client Sample mD: SS-9
GCIKMSeiotle
Lot-Sample 0 ... sDate Sampled ... :Prep Date ...... tPrep Batch t ... sDilution Factort
D4D030176-00304/01/04 15:1504/07/0440976211
Work Order 0...:Date Received..:Analysis Date..:Analysis Time..:
GDHQOlAC04/03/0404/22/0416:47
Hatrir ........ z SOLID
Method ..... SW846 8270C
PARAMETERAcenaphtheneAcenaphtbyleneAcetophenone2-Acetylaminofluorene4-AmninobiphenylAnilineAnthraceneAramiteBenzo(a)anthraceneBenzo(b)fluorantheneBenzok) fluorantheneBenzo(ghi peryleneBenzo(a)pyreneBenzyl alcoholbio(2-Chloroethoxy)
methanebisl2-Chloroethyl)-
etherbis(2-Ethylhexyl)
phthalate4-Bromophenyl phenyl
etherButyl benzyl phthalate4-Chloroanilinechlorobenuilate4-Chloro-3-methylphenol2-Chloronaphthalene2-Chlorophenol4-Chlorophenyl phenyl
etherChryseneDiallateDibenz(ah)anthraceneDibenzofuranDi-n-butyl phthalate1,2-Dichlorobenzene1,3-Dichlorobenzene1,4-Dichlorobenzene
RESULIIDNDNDNDNDNDJDNDNDIDSDEDIDlDND
REPORTINGLIMIT33033033033001600330330670330330330330330330330
ND 330
1D 330
UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/igug/kgug/kgug/kgug/kgug/kgug/kg
ug/kg
ug/kg
ug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ND 330
*EDEDEDEDEDEDND
330330330330330330330
RDEDNDEDNDNDED
ND
330670330330330330330330
(Continued on next page)
Client Sample ID: SS-9
GC/hS enlatles
Work Order #...: GDHQO1ACLot-SamPle #...: D4D030176-003 MatriX ..... : SOLID
3,3'-Dichlorobenzidine2,4-Dichlorophenol2,6-DichlorophenolDiethyl phthalateDimethoate7,12-Dimethylbenz(a)-
anthracene3,3'-Dimethylbenzidine2,4-DimethylphenolDimethyl phthalate1,3-Dinitrobenzene4,6-Dinitro-
2-methylphenol2,4-Dinitrophenol2,4-Dinitrotoluene2,6-DinitrotolueneDL-n-octyl phthalateDiphenylamineDisulfotonEthyl methanesulfonateFluorantheneFluoreneHexachlorobenzeneHexachlorobutadieneHexachlorocyclopenta-
dieneNexachloroethaneHexachloropropeneIndeno(1,2,3-cd)pyreneIodrinIsophoroneIsosafroleMethapyrilene3-MethylcholanthreneMethyl methanesulfonate2-MethylnaphthaleneMethyl parathion2-Metbylphenol3-Methylphenol &
4-MethylphenolNaphthalene -1,4-Naphthoquinonel-Naphthylamine
RESULTODtDNDEDEDND
REPORTINGLIMT1600330330670670670
EDVDNDNDND
6703303303301600
NDNDEDNDEDNDEDNDRDNDNDED
160033033033033016003303303303303301600
UNITSug/kgugfkgug/kgug/kgug/kgug/kg
ug/kgugfkgug/kgug/kguglkg
ug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/ksug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kg
NDNDNDNDNDNDND
NDNDNDNDlDND
330330033033033067016006703303301600330330
lNDNDND
3301600330
(Continued on next page)
LOWD GR
Client sazwle ID: ss-9
GC/MS Semivolatiles
lot-S8ample #...: D4D030176-003 Work Order t...: GDHQOIAC Matrr ......... z SOLID
PAMMER2-Naphthylamine2-Nitroaniline3-Nitroaniline4-NitroanilineNitrobenzene2-Nitrophenol4-Nitrophenol4-Nitroquinoline-
l-oxideN-Nitrosodi-n-butylamineN-HitrosodietbylamineN-NitrosodimethylamineN-NitrosodiphenylamineN-Nitrosodi-n-propyl-
amineN-NitrosomethylethylamineN-NitrosomorpholineN-NitrosopiperidineN-Nitrosopyrrolidine5-Nitro-o-toluidineParathionPentachlorobenzenePentachloroethanePentachloronitrobenzenePentachlorophenolPhenacetinPhenanthrene.PhenolPhorate2-PicolinePronamidePyrenePyridine1,2,4,5-Tetrachloro-
benzene2,3,4,6-TetrachlorophenolThionazino-Toluidine1,2,4-Trichloro-
benzene2,4,5-Trichloro-
phenol2,4,6-Trichloro-
phenol
RESULT
NDNDNDNDNDNDNDVD
REPORTINGLIMIT33016001600160033033016003300
EDNDEDNDND.
330330330330330.
NDVD
ND
ND
ND
ND
NDND
NDND
ND
ND
ND
ND
ND
21DND
ND
ED
33033033033067016003301600160016006703303301600670670330670330
Unms
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgugfkgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kg
ug/kg
ug/kg
EDEDND
ND
16001600670330
330
ND 330
(Continued on next page)
Clent Sample ZD: SS-9
Ga/NS Semivolatiles
Lot-Sample 1 ... : D4D030176-003 Work: Order 0.... s GDHQO1AC Hatrix......... : SOLID
PARAMETER00, O-Triethylphosphoro-
thioate1, 3,5 -Trinitrobenzene
RESULTND
REPORTINQLIMIT1600
MTSug/kg
ug/kgND 1600
SURROGATE2-PluoropheiolPhenol-dsNitrobenzene-d52-Fluorcbiphenyl2,4, 6-TribromophenolTerphenyl-d14
PERCENTRECOVERY737473677274
RECOVERYLIMITS(29 - 95 )(35 - 90 )
(39 - 69 )(35 - 86 )(11 - 111)(30 - 98 )
MOE(S) @Rem and prt g riks hame bee mjsod ftw dq WihL
LOslrOOD GR
Client Sample ID: 88-11
GC/S semidvolatiles
Lot-Sample 0... sDate Sampled ... :Prep Date ...... :Prep Batch #...:Dilution Factors
D4D030176-00404/01/04 10:0004/07/0440976211
Work Order #...:Date Received..:Analysis Date..:Analysis Time..:
GDHQ1lAC04/03/0404/22/0417:13
Matrix .... a SOLID
Method .... *....z SW846 8270C
PARAMETERAcenaphtheneAcenaphthyleneAcetophenone2-Acetylaminofluorene4-AminobiphenylAnilineAnthraceneAramiteBenzo (a)nthraceneSenyo (b) fluorantheneBenzo(k)fluorantheneBenzo(ghi)peryleneBenzo(a)pyreneBenzyl alcoholbis(2-Chloroethoxy)
methanebis(2-Chloroethyl)-
etherbis(2-Ethylhexyl)
phthalate4-Bromophenyl phenyl
etherButyl benzyl phthalate4 -hloroanilineChlorobenzilate4-Chloro-3-metbylphenol2-Chloronaphthalene2-Chlorophenol4-Chlorophenyl phenyl
etherChryseneDiallateDibenz(a,h)anthraceneDibenzofuranDi-n-butyl phthalate1,2-Dichlorobenzene1,3-Dichlorobenzene
RESULTVDND
*NDNDNDNDNDNDNDNDNDEDNDNDND
REPORTINGLIMIT33033033033001600330330670330330330330330330330
ND 330
ND 330
UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kg
ug/kg
ug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ND 330
IDNDNDNDNDNDND
330330330330330330330
NDNDNDNDIDNDNDND
3306703303303303303303301,4 -Dichlorobenzene
(Continued on next page)
client Sauple ID: CS-1l
6c/MS ivlatlen
Lot-Sample U...a D4D030176-004 Work Order #. .. GDHQI1AC Matri .... SOLID
PARMETER3,3'-Dichlorobenzidine2,4-Dichlorophenol2,6-DichlorophenolDiethyl phthalateDimethoate7,12-Dimethylbenz(a)-
anthracene3,3'-Dimethylbenzidine2.4-DimethylphenolDimethyl phthalate1,3-Dinitrobenzene4,6-Dinitro-
2-methylphenol2,4-Dinitrzphenol2,4-Dinitrotoluene2,6-DinitrotolueneDi-n-octyl phthalateDiphenylamineDisulfoton,Ethyl methanesulfonateFluorantheneFluoreneHexachlorobenzeneHexachlorobutadieneHexachlorocyclopenta-
dieneHexachloroethaneHexachloropropeneIndeno(1,2,3-cd)pyreneIsodrinIsophoroneIsosafroleMethapyrilene3-MethylcholanthreneMethyl methanesulfonate2-MethylnaphthaleneMethyl parathion2-Methylphenol3-Methylphenol &
4-KethylphenolNaphthalene1,4-Naphthoquinone
I-Naphthylamine
RESULTlNDEDNDNDEDND
REPORTINGLIMIT1600330330670670670
UNITSug/kgug/kgug/kgug/kgug/kguglkg
NDNDNDNDND
6703303303301600
NDNDEDNDNDNDNDNDNDND
EDND
1600330.33033033016003303303303303301600
ug/kgug/kgug/kguglkgug/kg
ug/kgug/kgug/kgug/kguS/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kg
ND
RD
ED
ND
ND
NDND
ND
ND
ED
JIDND
ND
330330033033033067016006703303301600330330
NDND
ND
3301600330
(Continued on next page)
Client Sample ID: SS-11
GC/kS semivolatiles
Lot-Sample *...: D4D030176-004 Work Order #...s GDHQ11AC Katri ......... SOLID
PARAM1ETER2-uaphthylamine2-Nitroaniline3-Nitroaniline4-NitroanilineNitrobenzene2-Nitrophenol4-Nitrophenol4-Nitroquinoline-
1-oxideN-Nitrosodi-n-butylamineN-NitrosodiethylamineN-NitrosodimethylamineN-NitrosodiphenylamineN-Nitrosodi-n-propyl-
amineN-NitrosomethyletbylamineN-NitrosomorpholineN-NitrosopiperidineN-Nitrosopyrrolidine5-Nitro-o-toluidineParathionPentachlorobenzenePentachloroethanePentachloronitrobenzenePentachlorophenolPhenacetinPhenanthrenePhenolPhorate2-PicolinePronamidePyrenePyridine1,2,4,5-Tetrachloro-
benzene2,3,4,6-TetrachlorophenolThionazino-Toluidine1,2,4-Trichloro-
benzene2,4,5-Trichloro-
phenol2,4,6-Trichloro-
phenol
RESULTNDNDND
NDMDND
EDED
REPORTINGLIMIT33016001600160033033016003300
MDEDMD
NDWD
330330330330
330
NDHDNDEDEDNDNDNDNDXDIDNDNDVDNDNDNDNDND
33033033033067016003301600160016006703303301600670670330670330
UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kg
ug/kg
ug/kg
NDND
NDND
1600
1600670330
ED 330
330
(Continued on next page)
Client Sample ID: 6S-11
GCiMS evolaes
Lot-Sample #...: D4D030176-004 Work Order O...: GDHQ11AC Matrix .... : SOLID
PARAMETER00, O-Triethylphosphoro-
thioate1,3, 5-Trinitrobenzene
RESULTND
REPORTINGLIMIT1600
UNITSug/kg
ug/kgND 1600
SURROGATE2-FluorophenolPhenol-d5Nitrobenzene-ds2-Fluorobiphenyl2,4,6-TribromophenolTerphenyl-d14
PERCENTRECOOVRY747574677075
RECOVERYLIMITS(28 - 95 )(35 - 90(39 - 89 )(35 - 86 )(11 - 111)(30 - 98 )
NOTE(B) sRmft azid zeps H have bfen dusd for ft %*kL
wacD GRE
Client Sample ID: SS-12
Cc/Hs Semivolatiles
Lot-Sample C...:Date Sampled...:Prep Date ...... :Prep Batch #...:Dilution. Factor:
D4D030176-00S04/01/04 15:4004/07/0440976211
Work Order 0. . . tDate Received..:Analysis Date..:Analysis Time. . :
GDHQ21AC04/03/0404/22/0417:40
Matrix ..... : SOLID
Method ..... SW846 8270C
PARAMKERAcenaphtheneAcenaphtbyleneAcetophenone2-Acetylaminofluorene4-AminobiphenylAnilineAnthraceneAramiteBenzo (a)anthraceneBenzo(b)fluorantheneBenzo(k) fluorantheneBenzo(ghi)peryleneBenzo(a)pyreneBenzyl alcoholbis(2-chloroethoxy)
methanebis (2-Chloroethyl) -
etherbis(2-Ethylhexyl)
phthalate4-Sromophenyl phenyl
etherButyl benzyl phthalate4-ChloroanilineChlorobenzilate4-Chloro-3-methylphenol2-Chloronaphthalene2-Chlorophenol4-Chlorophenyl phenyl
etherChryseneDiallateDibenz(a,h)anthraceneDibenzofuranDi-n-butyl phthalate1,2-Dichlorobenzene1,3 -Dichlorobenzene1,4-Dichlorobenzene
RESULT
NDNDiDNDNDNDED
IDNDNDNDEDNDED
REPORTINGLIMIT34034034034001600340340670340340340340340340340
340
ND 340
UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kg
ug/kg
ug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kg
ug/kgug/kgug/kgug/kg
ug/kgug/kg
ND 340
NDEDEDEDED2DND
140340340340340340340
NDNDWD21DNDND
ND
ND
340670340340340340340
340
(Continued on next page)
Client Sample ID: &S-12
GC/NS Semivolatiles
Wot-SamPle 0...s D4D030176-005 Work Order #...: 0)HQ21AC Matrix . . s SOLID
PARAMETER3,31-Dichlorobenzidine2,4-Dichlorophenol2,6-DichlorophenolDiethyl phthalateDimethoate7,12-Dimethylbenz(a)-
anthracene3,3'-Dimethylbenzidine2,4-DimethylphenolDimethyl phthalate1,3-Dinitrobenzene4,6-Dinitro-
2-methylphenol2,4-Dinitrophenol2,4-Dinitrotoluene2,6-DinitrotolueneDi-n-octyl phthalateDiphenylamineDisulfotonEthyl methanesulfonateFluorantheneFluoreneHexachlorobenzeneHexachlorobutadieneEexachlorocyclopenta-
dieneHexachloroetbaneNexachloropropeneIndeno(1,2,3-cd)pyreneIsodrinIsophoroneIsosafroleMethapyrilene3-MethylcholanthreneMethyl methanesulfonate2-MethiylaphthaleneMethyl parathion2-Methylphenol3-Methylphenol L
4-Methylphenol
Naphthalene1,4-Naphthoquinonel-Naphthylamine
RESULTNDNDRDVDNDND
REPORTINGLIMIT1600340340670670670
NDNDNDNDED
6703403403401600
NDNDNDNDNDNDNDNDND
NDNDND
160034034034034016003403403403403401600
UWITSug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kg
ug/kg
ug/kgug/kgug/kgug/kgug/kgug/kg
us/kgug/kgug/kgug/kgug/kgug/kg
uglkgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kg
ug/kg
EDNDNDNDNDEDNDNDNDNDNDNDND
340340034034034067016006703403401600340340
NDNDND
3401600340
(Continued on next page)
Client Sample ID: 8S-12
GC/MS Semivolatiles
Lot-Sample 0...: D4D030176-005 Work Order #...: GDHQ21AC Hatr ..... : SOLID
PARAMETER2-Naphthylamine2-Nitroaniline3-Nitroaniline4-NitroanilineNitrobenzene2-Ritrophenol4-Nitrophenol4-vitroquinoline-
I-oxideN-Nitrosodi-n-butylamineN-NitrosodiethylamineN-NitrosodimethylamieN-UitrooodiphenylamineN-Nitrosodi-n-propyl-
amineN-NitrosomethylethylamineN-NitrosomorpholineR-NitrosopiperidineN-Nitrosopyrrolidine5-Nitro-o-toluidineParathionPentachlorobenzenePentachloroethanePentachloronltrobenzenePentachlorophenolPhenacetinPhenanthrenePhenolPhorate2-PicolinePronamidePyrenePyridine1,2,4,5-Tetrachloro-
benzene2,3,4,6-TetrachlorophenolThionazino-Toluidine1,2,4-Trichloro-
benzene2,4,5-Trichloro-
phenol2,4,6-Trichloro-
phenol
RESULTEDEDEDNDNDNDNDND
REPORTINGLIMIT
3401600
1600160034034016003400
NDNDNDNDND
340
340340340340
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
34034034034067016003401600160016006703403401600670670340670340
UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kg
uglkgug/kgug/kgug/kgug/kg
ug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgus/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kg
ug/kg
ug/kg
NDNDNDND
16001600670340
340
340
(Continued on next page)
Client Sample ID: SS-12
GC/MS Semivolatiles
LOt-S0amle #...s D4DO30176-005 work Order #... t GQ2 1AC Matrix ........ : SOLID
PARAMETE
0,0, 0-Trietbylphosphoro-thloate
1,3, 5-Trinitrobenzene
RESULTND
REPORTINGLD1IT1600
UNITSug/kg
ug/kgKD 1600
SURROGATE2-FluorophenolPhenol-dSNitrobenzene-d52-Fluorobiphenyl2,4, 6-TribromophenolTerphenyl-dI4
PERCENT
RECOVERY757575697281
RECOVERYLIMITS(28 - 95 )(35 - 90 )
(39 - 89 )(35 - 86 )(11 - 111)(30 - 98 )
OTE(S):Rm Fonwimtfs have been Justed for dtyw
UCD GREE
Client Sapple ID: SS-13
GC/hS Semivolatiles
Lot-Sanple # ... : D4D030176-006Date Sampled ... : 04/01/04 16:10Prep Date ...... s 04/07/04Prep Batch 1... : 4097621Dilution Factor: 1
Work Order Q. ..Date Received..:Analysis Date..:Analysis Time.. :
GDH231AC04/03/0404/22/0418:07
Matrix .... : SOLID
Method .. . 81(846 8270C
PARAM R
Acenaphthene*Acenaphthylene
Acetophenone2-Acetylaminofluorene4-AminobiphenylAnilineAnthraceneAramiteBenzo(a)anthraceneBenzo(b)fluorantheneBenzo(k)fluorantheneBenzo(ghi)peryleneBenzo(a)pyreneBenzyl alcoholbis(2-Chloroethoxy)
methanebis(2-Chloroethyl)-
etherbis(2-Ethylhexyl)
phthalate4-Bromophenyl phenyl
etherButyl benzyl phthalate4-ChloroanilineChlorobenzilate4-Chloro-3-methylphenol2-Chloronaphthalente2-Chlorophenol4-Chlorophenyl phenyl
etherChryseneDiallateDibenz(a,h)anthraceneDibenzofuranDi-n-butyl phthalate1,2-Dichlorobenzene1,3-Dichlorobenzene1,4-Dichlorobenzene
RESULTNDEDEDEDNDNDEDNDEDNDNDNDEDEDND
REPORTINGLIMIT33033033033001600330330670330330330330330330330
330
330
UNITSuglkgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kcg
ug/kg
ug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ND 330
NDNDNDNDMDImND
330330330330330330330
NDNDEDNDNDNDNDND
330670330330330330330330
(Continued on next page)
Client Sanple mD: SB-13
6c4s Semivolatiles
ot-Sample I...2 D4D030176-006 Work Order #...: GDEQ31AC Matrix .. .: SOLID
PARAMETER3,3'-DJ.chlorobenzidine2,4-Dichlorophenol2,6-DichlorophenolDiethyl phthalateDimethoate7,12-Dimetbylbenz(a)-
anthracene3,3'-Dimethylbenzidine2,4-DimethylphenolDimethyl phthalate1,3-Dinitrobenzene4,6-Dinitro-
2-methylphenol2,4-Dinitrophenol2,4-Dinitrotoluene2,6-DinitrotolueneDi-n-octyl phthalateDiphenylamineDioulfotonEthyl methanesulfonateFluorantheneFluoreneHexachlorobenzeneHexachlorobutadieneHexachlorocyclopenta-
dieneRexachloroetbaneRexachloropropeneIndeno(l,2,3-cd)pyreneIsodrinIsophoroneIsosafroleMethapyrilene3-MethylcholantbreneMethyl methanesulfonate2-MetbylnaphthaleneMethyl parathion2-Methylphenol3-Metbylphenol &
4-MethylphenolNaphthalene1,4-Naphthoquinonel-Naphthylamine
RESULTNDNDNDNDEDND
REPORTINGLIMIT1600330330670670670
MD2DNDNDND
6703303303301600
NDNDNDNDNDIDNDRDNDNDNDHD
160033033033033016003303303303303301600
WNITSug/kgug/kgug/kgug/kgug/kguglkg
ug/kgug/kgug/kgug/kgug/kg
ug/kgugtkgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgugfkgug/kgug/kgug/kg
ug/kgug/kgug/kg
NDNDNDNDNDNDNDNDBDNDEDNDND
330330033033033067016006703303301600330330
NDNDND
3301600330
(Continued on next page)
Client Sample IDt ES-13
aclks Senivolatiles
Lot-&le #...a D4D030176-006
PAAMWETER2 -Naphthylamine2-Nitroaniline3-Nitroaniline4-NitroanilineNitrobenzene2-Nitrophenol4-Nitrophenol4-Nitroquinoline-
Work order t...: GDHQ31AC
RESULTEDNDNDNDNDNDNDND
REPORTINGLIMIT33016001600160033033016003300
Matrix ..... : SOLID
UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgl-oxide
N-Nitrosodi-n-butylamineN-NitrosodiethylrineN-NitrosodimetbylamineK-NItrosodiphenylamineN-Nitrosodi-n-propyl-
amine,N-NitrosaometbylethylamineN-NitrosomorpholineN-NitrosopiperidineV-Nitrosopyrrolidine5-NJitro-o-toluidineParathionPentachlorobenzenePentachloroethanePentachloronitrobenzenePentachlorophenolPhenacetinPhen~athrenePhenolPhorate2-PicolinePronamidePyrenePyridine1,2,4,5-Tetrachloro-
benzene2,3,4,6-TetrachlorophenolThionazino-Toluidine1,2,4-Trichloro-
benzene2,4,5-TrichLoro-
phenol2,4,6-Trichloro-
phenol
NDNDNDNDND
330330330330330
NDNDNDNDNDlDNDNDNDNDNDNDNDNDNDNDNDEDED
330330330
3306701600330160016001600670330330
1600670670330670330
ug/kgug/kgug/kgug/kgug/kg
Ug/kgug/kgug/kguglkgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kguglkgug/kg
ug/kg
ug/kg
NDNDEDND
16001600670330
ED 330
330ED
(Continued on next page)
Client Sample ID: SS-13
GC/MS Semivolatiles
Lot-SaMple I...a D4D030176-006 Work Order 0...: GDHQ31AC Matrix .... : SOLID
RESULTREPORTINGLIMIT1600
ag - - c--oo-
0,0,0-Triethylphosphoro-thioate
1,3,5-Trinitrobenzene
UNITSug/kg
ug/kgND 1600
SURROGATE2-FluorophenolPhenol-dSMitrobenzene-dS2-Fluorabiphenyl2,4,6-TribromophenolTerphenyl-d14
PERCENTRECOVERY757674687083
RECOVERYLIMITS(28 - 95 )(35 - 90 )(39 - 89 )(35 - 86 )(11 - 111)(30 - 98 )
Rehdt and cepoftqdng Minkm bcco asmnd for wdrbL
Client Sample ID: SS-15
GC/HS semivolatiles
Lot-Sample #...: D4D030176-007Date Sampled-: 04/01/04 13:10Prep Date ...... s 04/07/04Prep Batch #...t 4097621Dilution Factors 1
Work Order t...:Date Received..:Analysis Date..:Analysis Time..:
GDHQ4 lAC04/03/0404/22/0418:33
Matrix .... s 8OLID
Method ... .: 6W846 8270C
PARAMETERAcenaphtheneAcenaphthyleneAcetophenone2-Acetylaminofluorene4-AminobiphenylAnilineAnthraceneAramiteBenzo(a)anthraceneBenzo (b) fluorantheneBenzo(k)£luorantheneBenzo(ghi)peryleneBenzo(a)pyreneEenzyl alcoholbis(2-Chloroethoxy)
methanebis(2-Chloroethyl)-
etherbis(2-Ethyihexyl)
phthalate4-8romophenyl phenyl
etherButyl benzyl phthalate4-ChloroanilineChlorobenzilate4-Chloro-3-methylphenol2-Chloronaphthalene2-Chlorophenol4-Chlorophenyl phenyl
etherChryseneDiallateDibenz (a,h)anthraceneDibenzofuranDi-n-butyl phthalate1,2-Dichlorobenzene1,3-Dichlorobenzene1,4-Dichloroben ene
RESULTNDNDNDEDNDNDNDNDNDNDNDNDNDNDND
REPORTING
LIMIT33033033033001600330330670330330330330330330330
ED 330
ND 330
UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kg
ug/kg
ug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ND 330
EDlDNDNDNDNDND
330330330330330330330
NDNDVDNDNDNDND2D
330670330330330330330330
(Continued on next page)
Client Sample ID: SS-15
GC/hs Semivolatiles
Lot-Saizple #...: D4D030176-007 Work Order #...g GDHQ41AC HatriX .. .. : SOLID
PARAMETER3,3'-Dichlorobenzidine2,4-Dichlorophenol2,6-DichlorophenolDiethyl phthalateDimethoate7,12-Dimethylbenz(a)-
anthracene3,31 -Dimethylbenzidine2,4-DitnethylphenolDimethyl phthalate1,3-D W trobenzene4,6-Dinitro-
2-methylphenol2,4-Dinitrophenol2,4-Dinitrotoluene2,6-DinitrotolueneDi-n-octyl phthalateDiphenylamineDivulfotonEthyl methanesulfonateFluorantheneFluoreneNexachlorobenzeneHexachlorobutadieneRexachlorocyclopenta-
dieneHexachloroethaneHexachloropropene
RESULTNDNDNDNDNDND
REPORTINGLIMIT1600330330670670670
NDNDNDNDND
6703303303301600
NDNDlDNDEDNDNDNDNDNDEDND
160033033033033016003303303303303301600
UNITSug/kgug/kgug/kgug/kgug/kgug/kg
us/kgug/kgug/kgu1/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kg
Indeno(1,2,3-cd)pyreneIsodrinIsophoroneIsosafroleMethapyrilene3-MethylcholanthreneMethyl methanesulfonate2-MethylnaphthaleneMethyl parathion2-Methylphenol3-Methylphenol &
4-MethylphenolNaphthalene1,4-Naphthoquinonel-Naphthylamine
NDNDNDND
21DND
ND21DND
NDND
ND11D
330330033033033067016006703303301600330330
NDNDND
3301600330
(Continued on next page)
Client Sample ID: BS-15
GC/MS Semivolatiles
Lot-SaMple 2...: D4D030176-007
PARAMETER2-Naphthylamine2-Nitroaniline3-Nitroaniline4-NitroanilineNitrobenzene2-Nitrophenol4-Nitrophenol4-Nitroquinoline-
l-oxideN-Nitrooodi-n-butylamineN-NitrosodiethylamineN-NitrosodimethylamineN-NitrosodiphenylamineN-Nitrosodi-n-propyl-
amineU-NitrosomethylethylamineN-NitrosomorpholineN-VitrosopiperidineN-NitrosopyrrolidineS-Nitro-o-toluidineParathionPentachlorobenzenePentachloroethanePentachloronitrobenzenePentachlorophenolPhenacetinPhenanthrenePhenolPhorate2-PicolinePronamidePyrenePyridine1,2,4,5-Tetrachloro-
benzene2,3,4,6-TetrachlorophenolThionazino-Toluidine1,2,4-Trichloro-
benzene2,4,5-Trichloro-
phenol2,4,6-Trichloro-
phenol
work Order g...: GDHQ41AC
RESULTNDNDNDPDNDEDEDND
REPORTINGLIMIT33016001600160033033016003300
IDIDEDEDED
330330330330330
EDlND2DNDNDNDNDNDtDNDEDEDEDEDEDNDEDEDND
3303303303306701600
3301600160016006703303301600670670330670330
Matri.i.. . -SOLID
UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kg
ug/kg
NDEDNDED
16001600670330
330
ND 330
(Continued oan next page)
BAWDO G-R
Client Sample mD: SS-15
GC/NS Semivolatiles
1ot-gample U...2 D4D030176-007 Work Order I... : GDH41AC MatriX .... : SOLID
,0,0,0-Triethylphosphoro-thioate
1,3,5-Trinitrobenzene
RESULTND
REPORTINGLIMIT UNITS1600 ug/kg
ND 1600 ug/kg
2-FluorophenolPhenol-d5Nitrobenzene-dS2-Fluorobiphenyl2,4,6-TribromophenolTerphenyl-dH4
N0TE(S):
PERCENTRECOVERY737474676984
RECOVERY
(28 - 95 )(35 - 90 )(39 - 89 )(35 - 86 )(11 - 111)(30 - 98 )
legui Wd ipordz Infhavebeen asWdf~rdiywd~bt
Client Sample ID: 8S-16
aC/MS Semivolatiles
lot-Sample C.. .sDate S.amp... .2Prep Date ...... sPrep Batch #... sDilution Factor:
D4D030176-00804/01/04 14:4004/07/0440976211
Work Order ... :Date Received..Analysis Date..:Analynis Time..s
GDHQ51AC04/03/0404/22/0419:00
Matrix. ...... s SOLID
Method ......... iSW846 8270C
PARAMETER
AcenaphtheneAcenaphtbyleneAcetophenone2-Acetylaminofluorene4-AminobiphenylAnilineAnthraceneAramiteBenzo ()anthraceneBenzob) fluorantheneBenzo (kfluorantheneBenzo(ghi)peryleneBenzo(a)pyrcneBenzyl alcoholbis(2-Chloroetboxy)
methanebis(2-Chloroethyl)-
etherbis(2-Etbylhexyl)
phthalate4-Bromophenyl phenyl
etherButyl benzyl phthalate4-ChloroanilineChlorobenzilate
RESULTRD
RDNDNDRDWDNDNDNDRDNDNDRDNDRD
REPORTINGLIMIT33033033033001600330330670330330330330330330330
ND 330
ND 330
UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kg
ug/kg
ug/kg
ugfkgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ND 330
4-ChlOro-3-methylphenol2-Chloronaphthalene2-Chlorophenol4-Chlorophenyl phenyl
etherChryseneDiallateDibenz(ah)anthraceneDibenzofuranDi-n-butyl phthalate1,2-Dicblorobenzene1,3-Dichlorobenzene1,4-Dichlorobenzene
NDRDNDNDRDEDED
330330330330330330330
VDlDNDNDRDNDlDED
330670330330330330330330
(Continued on next page)
Client Sample ID: 8S-16
GC/kS Semivolatiles
Lot-Sample ... * D4D030176-008
PARAMTER3,3'-DiCblorobenzidine2,4-Dichlorophenol2,6-DichlorophenolDiethyl phthalateDimethoate7,12-Dimethylbenz(a)-
anthracene3,3'-Dimethylbenzidine2,4-Dimethylphenol
Dimethyl phthalate1,3-Dinitrobensene4,6-Dinitro-
2-methylphenol2,4-Dinitrophenol2,4-Dinitrotoluene2,6-DinitrotolueneDi-n-octyl phthalateDiphenylamineDisulf otonEthyl methanesulfonateFluorantheneFluoreneNexachlorobenzeneEexachlorobutadieneNexachlorocyclopenta-
dieneHexachloroethaneRexachloropropeneIndeno(1,2,3-cd)pyreneIsodrinIsophoroneIsosafroleMethapyrilene3-MethylcholanthreneMethyl xetbanesulfonate2-MethylnapbthaleneMethyl parathion2-Methylphenol3-Methylphenol &
4-MethylphenolVaphtbalene1,4-Naphthoquinonel-Naphthylamine
Work Oder #...: GHAC
RESULTNDNDNDNDNDED
REPORTINGLIMIT
1600330330670670670
NDNDEDEDED
6703303303301600
NDEDNDWDND
NDNDNDVDHDNDND
160033033033033016003303303303303301600
MatriX ..... : SOLID
UNITS
ug/kguglkgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kg
NDEDEDNDNDNDNDNDNDNDNDNDND
330330033033033067016006703303301600330330
NDND
ND
3301600330
(continued on next page)
C GRR
Client 8agple mD: 8S-16
GC/HS Semivolatiles
Lot-Sample #...: D4D030176-008 Work Order I.... GDHQSlAC Hatris ..... : SOLID
PARAMERTER2-Naphthylamine2-Nitroanlline3-Nitroaniline4-NitroanilineNitrobenzene2-Nitrophenol4-Nitraphenol4-Nitroquinoline-
I-oxideN-Nitrosodi-n-butylamineN-NitrosodiethylamineN-NitrosodimetbylamineN-NitrosodiphenylamineN-Nitrosodi-n-propyl-
amineU-NitrosomethylethylamineN-NitrosomorpholineN-NitrosopiperidineN-Nitrosopyrrolidine5-Nitro-o-toluidineParathion ,PentachlorobenzenePentachloroethanePentachloronitrobenzenePentachlorophenolPhenacetinPhenanthrenePhenolPhorate2-PicolinePronamidePyrenePyridine1,2,4,5-Tetrachloro-
benzene2,3,4,6-TetrachlorophenolThionazino-Toluidine1,2,4-Trichloro-
benzene2,4,5-Tricbloro-
phenol2,4,6-Trichloro-
phenol
RESULTNDNDNDNDND
NDMD
REPORTING
3301600
160033033016003300
EDNDNDNDIRD
330330330330330
NDND17DNDNDNDNDNDNDNDNDNDVDNDNDNDNDNDND
33033033033067016003301600160016006703303301600670670330670330
UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kg
ug/kgug/kgug/kgug/kg
ug/kg
ug/kg
NDNDIDND
16001600670330
330
ND 330
(Continued on next page)
1OCO -
Client Sample ID: SS-16
GC/MS Evolaes
Lot-Sample I...: a4D030176-008 Work Order #...: GDHQ51AC Matrix.........: SOLID
PARAMETER0,0, 0-Triethyiphosphoro-
thioate1,3,5-Trinitrobenzene
RESULTND
REPORTINGLIMIT1600
UNITSug/kg
ug/kgND 1600
SURROGATE2-Fluorophemol
Phenol-d5Kitrobenzene-ds2-Fluorobiphenyl2,4,6-'TribromophenolTerphenyl-dU4
PERCENTRECOVERYCs
6867636476
RECOVERYLIMITS(28 - 95 )(35 - 90 )(39 - 89 )(35 - 86 )(11 - 111)(30 - 98 )
loTE(a):Rat su rqctg im kae beem Wdjus for dzy wdegbt
Client Samnle ID: S.-2
OCSnvoaie
Wat-Sample t... : D4D030176-001Date Sampled...s 04/01/04 12:30Prep Date ...... s 04/06/04Prep BatcI #... : 4096552Dilution Factor: 1
Work Order #...:Date Received..:Analysis Date..:Analysis Time..
GDHQLMAD04/03/0404/24/0404:06
matrix ..... SoLID
Method .... :. SW46 8081A
Aldrinalpha-BECbeta-BHCdelta-EECgamm-BEC (Lindane]Chlordane (tecbnia4,4'-DDD4,4'-DDE4,4'-DDTDieldrinEndrin
Endrin aldehydeEndosulfan IEndosulfan IIEndosulfan sulfateReptachlorHeptachlor epoxldeHethoxychlorToxaphene
I11)
RESULTHDNDNDHDNDHDNDNDNDNDNDND
NDNDEDNDNDNDNID
REPORTING
1.71.71.71.71.7171.71.71.71.71.71.71.71.71.71.71.73.4170
UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgus/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
SURROGATEDecachlorobiphenylTetrachloro-m-xylene
PERCfETRECOVERY82101
RECOVERYLIMTS(41 - 142)(50 - 127)
NOTHE(S):mb mg *epornAg Inihs hme ber a4jused br diy vcfh.
Client Sample ID: S8-6
GC sezivolatiles
Lot-Sample 8...:Date Sampled...:Prep Date ...... :Prep BatC .... sDilution Fator:
D4D030176-00204/01/04 10:4004/06/0440965521
Work Order t... sDate Received..Analysis Date..:Analysis Time..:
GDHQX1AD04/03/0404/24/0404:35
Matrix ......... : SOLID
Method . .... s W846 808LA
Aldrinalpha-BECbeta-BHCdelta-EHCgamma-BHC (Lindane)Chlordane (technical)4,4'-DMD4,4'-DDE4,4 -DDTDieldrinErerinEndrin aldehydeEndosulfan IEndosulfan !!Endosulfan SulfateHeptachlorIZeptachlor epoxideMethoxychlorToxaphene
RESULTEDNDIDND1IDND0.44 J,TLNDNDVDNDNDNDNDEDNDVDNDND
REPORTINGLIMIT1.71.71.71.71.7171.71.71.71.71.71.7
1.71.71.71.71.73.3170
UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
SURROGATE
DecachlorabiphenylTetrachloro-m-xylene
PERCERTRECOVERY8499
RECOVERYhIMITS(41 - 142)(50 - 127)
MOTE (S):Ieb ad aponWg Nits h be aKhwd AVdy Wcga.
I Estimated rslt. R s t is km don IL.COL Mom4 E. 40% VD etwn pkn nd audmaw *lU= nsul. Ue lwe Of to MO b s NPOtd.
Client Sample ID: 8s-9
GC Semivolatiles
Lot-Sawple C...: D4D030176-003 Work order P...:Date Sampled ... : 04/01/04 15:15 Date Received..:Prep Date ...... s 04/06/04 Analyois Date..:Prep Batch 4 ... s 4096552 Analysis Time..:Dilution Factors 1
GDHQOlAD04/03/0404/24/0405:04
Matrix ....... : OLID
Method.........: SW846 808A
PARAMETERAldrinalpha-BHCbeta-BBCdelta-BHCgamma.-BHC (Lindane:Cblordane (technic,4,44 -W_4,4 '-DDE4,4' -DDTDieldrinEndrinEndrin aldehydeEndosulfan IEndosulfan IIEndosulfan sulfateReptachlorHeptachlor epoxideMethoxychlorToxaphene
3.1)
RESULTNDNDNDNDNDND0.39 67,cJLNDNDNDNDNDEDlNDNDNDNDNDND
REPORTINGLIMIT1.71.71.71.71.7171.71.71.71.71.71.71.71.71.71.71.73.3170
UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
SURROGATEDecachlorobiphenylTetrachloro-m-xylene
PERCENTRECOVERY90105
RECOVERYLIMITS(41 - 142)(50 - 127)
NOTe (S)Rms ad xcp=Wg imhs lua bom mdjusted Slrdy wdglI.
I EF ftu LW ksdt I es k IdRL
COL =r dun 40% RFD belwec prkuq and onrHmado colum euits. The bwe of lhe wo rmb k upomd.
Client Sample m: ES-1l
6C Semivolatiles
Lot-Sample C...:Date Sampled...:Prep Date ..... aPrep Batch #...:Dilution Factort
D4D030176-004 Work order # ... z04/01/04 10:00 Date Received..:04/06/04 Analysis Date..:4096552 Analysis Time..:1
GDHQ11AD04/03/0404/24/0405:32
atrit......... : SOLID
Metbod . .: sBW846 80BIA
PARAMETERAldrinaipha-BECbeta-SHCdelta-BSCgamma-BEC (LindanelChlordane (tecbnici4,4' -DDD4,4'-DDE4,4'-DDTDieldrinEndrinEndrin aldehydeEndosulfan IEndosulfan 1IEndosulfan sulfateHeptachlorReptachlor epoxideMethoxychlorToxaphene
LI)
RESULTNDNDEDNDEDED0.79 TCOLNDEDNDNDEDNDNDNDEDNDNDID
REPORTINGIMI1.71.71.71.71.7171.71.71.71.71.71.71.71.71.71.71.73.3170
UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
SURROGATE
DecachlorobiphenylTetrachloro-m-xylene
PERCENTRECOVERYE399
RECOVERYLUIITS(41 - 142)(50 - 127)
lO= (S):uks aod mpot ENadu kme been u6W 1fo y wdght
I Ednntrd XR= hu g L
O LL Mm tin 40% RFD ben puz cam wnfatn coma rSe TM owe of ti M reums Is UePO
COD GRIM
Client Sanple ID: S5-12
¢C Sedivolatiles
Lot-Sanple #...:Date Sampled...:Prep Date ...... :Prep Batch #...:Dilution Factor:
D4D030176-00504/01/04 15:4004/06/0440965521
Work arder 6...:Date Received..:AnalysiS Date..:Analysie Time..:
GDHQ21lD04/03/0404/24/0406:01
Matrix ..... : SOLID
Method ..... 8W846 8082A
PA=AMETERAldrinalpha-BECbeta-BECdelta-BECgamna- -EC (Lindane)Chlordane (technical)
4,4' -D._4,4'-DDE4,4' -DDTDieldrinEndrinEndrin aldehydeEndosulfan IEndosulfan IIEndosulfan sulfateKeptachlorReptachlor epoxideMethoxychlorToxaphene
RESULT
NDNDNDNDNDND
ND0.65 J,COLEDNDNDNDDD
NDNDNDNDNDNDND
REPORTINGLIMIT1.71.71.71.71.7171.71.71.71.71.71.71.71.71.71.71.73.4170
UNITS
ug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kg
SURROGATEDecacalorobiphenylTetrachloro-m-xylene
PERCENTRECOVERY96109
RECOVERYLIMITS(41 - 142)(50 - 127)
NIOT(s):
R8It wd fepofiq Iit hmac be= 4usd frdry wegbrt.I EPldre raiz. Remuk I kss kn i RL
COLMmV gm111 40% RPD bcw h prhlh awd ewimonf chumm fhc Dhe Iowaofe tw Mcut s k fL
LON RM
Client Sample ID: SS-13
GC Semivolatiles
Lot-Sample t...: D4D030176-006Date 8arpled...s 04/01/04 16:10Prep Date ...... s 04/06/04Prep Batch #...s 4096552
Dilution Factor: 10
Work Order # ... tDate Received..:Analysis Date..:Analynis Time..:
GDHQ3lAD
04/03/0404/27/0411:42
MatriX ..... : SOLID
Method . .... . SW846 8081A
PARPAMTERAldrinalpha-BECbeta-BHCdelta-BECgamma-BEC (Lindane:Chlordane (technici4,4 -DDD4,4' -DDE4,4'-DDTDieldrinEndrinEndrin aldehydeEndosulfan IEadosulfan II
Endosulfan sulfateHeptachlorHeptachlor epoxideMethoxychlorToxaphene
ii)
RESULTVDNDNDND
NDND1TDEDVDNDVDNDNDND
NDNDNDNDND
REPoRTINSLIMIT17171717171701717171717171717171717331700
CNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kguglkgug/kg.
SURROGATEDecachlorobiphenylTetrachloro-m-xylene
PERCENTRECOVERYNC,DILNC,DIL
RECOVERYLIMITS(41 - 142)(50 - 127)
NC Mm ecvcr andlr RPD w kact amculateL
DML TI mcmeo b ae~md or am rqarted de dCM=oor 9k prf== s of befehg aal
Raubs wd q'fn ltse kbme 4fused for try weghL
LOC O GREENE
Client Sanple ID: 5S-15
GC Semivolatiles
Lot-&a6ple 0...: D4D030176-007Date Sampled...: 04/01/04 13:10Prep Date...;..: 04/06/04
Prep Batch 1...: 4096552Dilution Factor: 10
Work Order #...:Date Received..:Analysis Date..:Analysis Time..:
GH41AD04/03/0404/27/0412:11
Hatrix ......... : SOLID
Method, ......... x EW846 8081A
Aldrinalpba-EHCbeta-BHCdelta-BHCgamma-BHC (Lindane)chlordane (technical)4,4 ' -DDD4,4 -DDE4,4 ' -DDTDieldrinEzndrinEndrin aldehydaeEndosulfan IEndosulf an IIEndosulfan sulfateHeptachlorHeptachlor epoxideMetboxychlorToxaphene
RESULTJDNDNDNDEDIDNDNDllDEDIDEDEDIDEDNDNDNDND
REPORTINGLIMIT17171717171701717171717171717171717331700
WITSug/kgug/kgug/kgug/kguglkgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kguglkgug/kgug/kgug/kgug/kg
SURROGATEDecachlorobiphenylTetrachloro-m-xylene
PERCENT
RECOVERY
NC,DIL
HC, DIL
RECOVERYLIMITS
(41 - 142)(50 - 127)
NOTE(6) _NC Ue mcoy andfor RPD were ot eladd.Dl Tw ==zt k ekid or m sq=o dw m Md=k orie pmwam od Ieearh anyom
Xew sad rcpxdng lmb h e be a*tmd br dry we*tL
Client Sample ID: 8S-16
GC Bemivolatiles
Lot-Sample #...: D4D030176-008Date Sampled ... : 04/01/04 14:40Prep Date ...... : 04/06/04Prep Batch 0...s 4096552DilutIn Factor: 10
Work order C...:Date Received..sAnalysi. Date..:Analysis Time..:
GDHQSUM04/03/0404/27/0412:40
Matrix .... : SOLID
Kethod ... .: SN846 8081A
PARAMETERAldrinalpba-BHCbeta-BHCdelta-EECganma-BEC (LindanelChlordane (technlic4,4 '-DDD4 ,4-DDE4,4'-DDTDieldrinEdrinEundrin aldehydeEndosulfan IEndosulfan IIEndosulfan sulfateEeptachlorHeptachlor epoxideFethoxychlorToxaphene
Li)
RESULTEDEDIQDJDEDlD
EDEDEDNDED1DNDND
NDNDNDND
REPORTINGLIMIT17171717171701717171717171717171717331700
UNITS
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kguglkgug/kgug/kgug/kgug/kg
SURROGATEDecachlorobiphenylTetrachloro-m-xylene
PERCENTRECOVERY
NCDILNCDIL
RECOVERYLIMITS(41 - 142)(50 - 127)
NOTE (S):NC Ibe zerowry m=Uor IIPD = " alated.
DIL Ue mnoamaoo k nated or o ,cpord de w dlhnio or de prme= of Weak& amuly
Client Sample ID: 8S-2
GC semivolatiles
Lot-Sample i...:Date Sampled...:Prep Date ...... s
Prep Batdh i ... sDilutioa Factor:
D4D030176-00104/01/04 12:3004/04/0440951251
Work O0e r ... :Date Received..:Analysis Date.. 2Analysis Time...:
GDHQL1AE04/03/0404/12/0413.39
Matrix ... . : SOLID
Method .... : SW846 8141A
PAR7METERAzinphos-methylBolstarChlorpyrifosCoumaphosDemeton (total)DiazinonDichlorvosDimethoateDisulfotonEthopropEthyl parathionFamphurFensulfothionFenthionMalathionMerphosMethyl parathionFevinphosNaled0,0,0-Triethylphosphoro-
thioatePhorateRonnelSulfoteppThionazinTokuthionTrichloronateEPN
RESULTNDNDNDNDNDNDHDEDEDNDNDMDNDNDMDWDkDVDNDND
REPORTINGLIMIT1313131313131313131313131313131313133413
UNITS
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kcgug/kgug/kgug/kgug/kgug/kg
NDNDNDEDNDHD
NDNDND
13G81313131313131313
Demeton-0Demeton-STetrachlorvinphos (Stirophos)
SURROGALTEEthyl Pir4mifosChlormefos
PERCENTRECOVERY7184
RECOVERY
LJMTS(11 - 137)
(37 - 124)
T E(S) :FRft Ed aporbtC Emk have be *Cumd for dry we ht.
Client Sanple ID: 8S-6
OC semivolatiles
Lot-Sample #...:Date Sampled...:Prep Date ...... tPrep atch #... iDilution Factor:
D4D030176-00204/01/04 10:4004/04/0440951251
Work Order 0..:Date Recelved..:Analysis Date..sAnalysis Time..:
GDHQX1AE04/03/0404/12/0414:13
Matrix .. .: OLID
Method ......... SW846 8141A
PARAMETERAzinphos-methylBolstarChlorpyrifosCoumaphosDemeton (total)DiazinonDichlorvosDimethoateDisulfotonEthopropEthyl parathionFamphurpensulfothionFenthionM2lathionMerphos-Methyl parathionMevinphosValed0,0,0-Triethylphosphoro-
thicate
RES=TNDNDNDNDNDNDNDNDIDNDNDNDWDNDNDNDEDNDNDND
REPORTINGLIMIT1313131313131313131313131313131313133313
UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kg
ug/kqug/kgug/kgug/kgug/kgug/kgug/kguglkgug/kg
PhorateRonnelSulfoteppThionazinTokuthionTrichloronateEPNDemeton-0Demeton-STetrachlorvinphos
NDNDIDNDNDNDNDNDNDND
1368131313131.3131.313(Stirophos)
SURROGATEEthyl PirimifosChlormefos
PERCENTRECOVERY7587
RECOVERYLIMTS(11 - 137)(37 - 124)
lmuts w r*orti limis hve been a&Qjusmi br d&y weipg
WO W GREOD
Client Saiple ID: SS-9
GC Semivolatiles
lot-Sample 1 ...aDate Sampled ...:Prep Date ...... sPrep Batch t ...aDilution Factor:
D4D030176-00304/01/04 15:1504/04/04
40951251
Work Order C..: GDHQ0ODate Received..: 04/03janalysis Date..: 04/12i
wnalysis Time..: 14:46
LAE
04!/04
MatriX ..... SOLID
Method .... : SW846 8141A
PARJU4ETERAzinphos-methylBolstar
ChlorpyrifosCoumaphosDemeton (total)DiazinonDichlorvosDimethoateD1AlfotonEthopropEthyl parathionFamphurFensulfothionFenthionMalathionMerphosMethyl parathionMevinphosNaled0,0,0-Triethylphosphoro-
thiLoatePhorateRornelSulfoteppThionazin
RESULTIDNDNDEDEDEDEDNDNDNDEDEDEDNDNDNDND
NDNDIND
REPORTIMLIMIT1313
1313131313131313131313
13131313133313
UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
TokuthionTrichloronateEPNDemeton-ODemeton-STetrachlorvinphos
NDNDNDNDNDNDNDkDNDND
136E1313131313131313(Stirophos)
SURROGATEEthyl PirimifosChlormefos
PERCENTRECOVERY6775
RECOVERYLIMITS(11 - 137)(37 - 124)
NOE(S) :1s and epo eg lmi av been unuted *or d wy dghtL
Client Sample ID: SS-11
GC semivolatiles
bot-Sauple #C..:Date Sampled...:Prep .... ...... s
Prep Batch 9 ... :Dilution Factor:
D4D030176-00404/01/04 10:0004/04/0440951251
Work order 9...sDate Received..:lnalysia Date..:Analysie Time..
GDHQ11AE04/03/0404/12/0415:52
Matrix .. . : SOLD
Method .... : sw846 8141A
PARAMETERAzinphos-methylBolstarchlorpyrifosCoumaphosDemeton (total)DiazinonDichlorvosDimethoateDisulfotonEthopropEthyl parathionFamphurFensulfothionFenthionMalathionMerphosMethyl parathionMevinphosNaled0,0,0-Triethylphosphoro-
thioatePhorateRonnelSulfoteppThionazinTokuthionTrichloronateEPNDemeton-ODemeton-STetrachlorvinphos (Stirophos)
RESULTNDNDNDNDIDNDNDEDNDNDNDNDNDNDNDNDNDNDNDND
REPORTINGLIMIT1313131313131313131313131313131313133313
UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg-ug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
NDNDNDEDEDNDEDED2DND
13681313131313131313
SURROGATEEthyl PirimifosChlormefos
PERCENTRECOVERY7390
RECOVERYLIMITs(11 - 137)(37 - 124)
KTm(S):Resul ad rpong Imits hive been adpftd for by wcigbL
WDZOOD 6REE
Client Sample ID: 8S-12
CC Semivolatiles
Lot-8amQle C. . s
Date Sampled...:
Prep Date ...... s
Prep Batch #...sDilution Factor:
D4D030176-00504/01/04 15:4004/04/0440951251
Work Order t..:Date Received..:Analysis Date..:Analysis Time..:
GDHQ21AE04/03/0404/12/0416s25
Matrix ..... : SOL
Method ...... SW46 8141A
PARAMETERAzinphos-methylBolstarChlorpyrifosCoumaphosDemeton (total)DiazinonDichlorvosDimethoateDisulfotonEthopropEthyl parathionFamphurFensulfothionFenthbonMalathionMerphosMethyl parathionmevinphosNaled0,0, 0-Triethylphosphoro-
thioatePhorateRornelSulfoteppThionazinTokuthionTrichloronateEPSDemeton-0Demeton-STetrachlorvinpbos (Stlro
RESULTiDlDllDEDNDNDNDNDHD
RDNDNDNDNDNDEDNDNDND
IND
REPORTIGLIMIT1313131313131313131313131313131313133413
UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kguglkgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ND
TM
ND
ND
ND
ND
ND
ND
NDNND
13681313131313131313phos)
SURROGATEEthyl PirimifosChlormefos
PERCENTRECOVERY7286
RECOVERYLIMITS(11 - 137)(37 - 124)
NOTE(s):Zmft ad mpw eb nEt hv bm usted fwr dry weiL
Client Sample ID: SS-13
CC Semivolatiles
Lot-Sample #... :Date Sampled...zPrep Date ..... :Prep Batch #...sDilution Factor:
D4D030176-00604/01/04 16:1004/04/0440951251
Work order C...:Date Received.. sanalysis Date..:analysis Time.. i
GDHQ3 1AE04/03/0404/12/0416259
Matrix . .: SOLID
Method . . s 8W846 8141A
PARAMETERAzinphos-methylBoletarChlorpyrifosCoumaphosDemeton (total)DiazinonDichlorvosDimethoateDisulfotonEthopropEthyl parathionFamphurFensulfothionPenthionMalathionMerphosMethyl parathionMevinphosNaled0,0,0-Triethylphosphoro-
thioatePhorate
RESULTEDNDNDNDNDlDNDEDNDNDVDVD1DNDWDNDNDNDNDND
REPORTINGLIMIT1313131313131313131313131313131313133313
UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kguglkg
RonnelSulfoteppThionazinTokuthionTrichloronateEPNDemeton-0Demeton-STetrachlorvimphos
HD
ND
NDEDEDNDNDNDNDND
13
1313131313131313(Stirophos)
SURROGATEEthyl Pirimifoschlormefos
PERCENTRECOVERY
7797
RECOVERYLIMITS(11 - 137)(37 - 124)
NOTE(s):lenas am" pftd Ulu hve be asW dOr dry wrkfL
Client Sample D: SS-15
CC Siivoalatiles
Lt-Sample # ... tDate Sampled...:
Prep Date ...... sPrep Batch t.... :Dilution Factor:
D4D030176-007 Work Order I ... s04/01/04 13:10 Date Reeived..:04/04/04 Analysis Date. .:
4095125 - Analyss Time..:1
GDHQ41AE04/03/0404/12/0417:32
MatriX ..... : SOLID .
Method ...... 8W846 8141A
PARAMETERAzinphos-methylBoistarchlorpyrifasCoumaphosDemeton (total)DiazinonDichlorvosDimethoateDisulfotonEthpropEthyl parathionFamphurFensulfothionFenthionMalathionMerphosMethyl parathionMevinphosHaled0,0,0-Triethylphosphoro-
thioatePhorateRonnelSulfoteppThionazinTokuthionTrichloronateEPNDemeton-ODemeton-8Tetrachlorvinphos (Stiro]
RESULTNDNDNDNDRDEDND
NDllDEDND
NDNDND
NDNDEDNDND
hD
NDEDNDNDNDNDNDEDND
REPORTINGLIMIT1313131313131313131313131313131313133313
13681313131313131313
UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgUg/kg
ug/kgug/kgugs/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kCgug/kgug/kgphos)
SURROGATEEthyl PirimifosChlormefos
PERCENTRECOVERY7790
RECOVERYLIMITS(11 - 137)(37 - 124)
MOTE(S) :
Client Sample ID: 8S-16
GC Semivolatiles
Lot-Sample #...:Date Sampled...:Prep Date ...... :Prep Batch t...:Dilution Factor:
D4D030176-008
04/01/04 1MM4004/04/04409512S1
Work order #...:Date Received..:Analysis Date..:Analysis Time..:
GDHQ51AE04/03/0404/12/0418 05
HatriX .. .: SOLID
Hethod .... ... : SW846 6141A
PARA0MTERAzimphos-methylBolstarChlorpyrifosCoumaphosDemeton (total)DiazinonDichlorvosDimethoateDisulfotonEthopropEthyl parathionFamphurFensulfothionFenthionMalathionMerphosMethyl parathionMevinphosNaled0,0,0-Triethylphosphoro-
thioate
RESULTNDNDEDND1NDNDNDND
RDNDNDVDNDNDRDNDNDNDNDWD
REPORTINGLDT1313131313131313131313131313131313133313
uNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
PhorateRonnelSulfoteppThionazinTokuthionTrichloronateEPNDemeton-ODemeton-STetrachlorvinphos
ND
NDNDNDNDNDNDNDNDND
13691313131313131313
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg(Stirophos)
SURROGATEEthyl Pirimifos
Chlormefos
PERCENTRECOVERY7391
RECOVERYLIMITS
(11 - 137)(37 - 124)
NOTE(S):Reml od r'orfg Emm have be idjused Or dry wet.
Client Sample ID: SS-2
GC Seaivolatiles
Lot-Sample ... 2Date Sampled....Prep Date ......:
Prep Batch I...sDilution Factor:
D4D030176-001
04/01/04 12:3004/08/044098553
Work Order #...:Date Received..:Analysis Date..:Analysis Time.-
GDHQL1AF
04/03/0404/13/0419:43
Matrix . .... : SOLID
Method......... : 8W846 8152A
PARAMETER2,4-D2,4-DB2,4,5-T2,4,5-TP (Silvex)DalapoaDicambaDichlorpropDinosebM[CPAHCPP
RESULT
NDNDNDlDIDIDEDNDNDND
REPORTINGLWI8181
20204141811281008100
UNITS
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
SURROGATEDCAA
PERCENTRECOVERY83
RECOVERYIMITS(39 - 96 )
NOTE(s):Resuk ad avofbng lmft bave bee ad~usWe for day wed&.
Client Sample ID: 65-6
GC Bemvolatiles
Lot-Sample t ... s D4D030176-002Date Sampled...: 04/01/04 10:40Prep Date ...... : 04/08/04Prep Batch 1...: 4098553Dilution Factor: 1
Work Order #...:Date Received..:Aialysis Date..:Analysis Tne..*
GDHQX2AF
04/03/0404/13/0420:24
Matrlx.........: SOLID
Method.......2 SW846 8151A
PARAMETER2,4 -D2,4-DB2,*4,5 -T2,4,5-TP (Silvex)DalapoanDicamba,DichlorpropDinoseb?4CPAJ4CPP
RESULTMDE DWDNDWDED
IEDEDEDED
REPORTING
LIMIT81
202041418112
81008100
UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kcgug/kguglkg
SURROGATEDC&A
PERCENTRECOVERY90
RECOVERYLIMITS(39 - 96 M
NOTE(s):Results ad MrpothIg Umkslhave bease adusted for dry wedgta.
Client Sample ID: SS-9
GC Semivolatiles
Lot-SaaPle t...: D4D030176-003Date Sampled ... : 04/01/04 15:15PZep Date ...... s 04/08/04Prep Batch C...: 4098553Dilutioui Factor: 1
Work order #...sDate Received. .Analysis Date..:Analysis Time..:
ODHO01AF04/03/0404/13/0421:05
Matrix .. S. : SLID
Method .... : SW846 8151A
PARAMETER2,4-D2,4-DE2,4,5-T2,4,5-TP (Silvex)DalaponDicauibaDichlorpropDinosebMCPAMCPP
RESULTRDVDEDNDNDND
ND]ND
NDND
REPORTINGLIMIT818120204040811291008100
DNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
SURROGATEDCAA
PERCENTRECOVERY89
RECOVERYLIMITS(39 - 96 )
NOTE(S):
OHD GRENE
Client Sample ID: SS-l1
OC Seinivolaviles
Lot-Sample #...:Date Sampled... 2Prep Date ...... :Prep Batch C...:Dilution Factor:
D4DO30176-00404/01/04 10:0004/08/044098553
Vork Order C..:Date Received..snalysis Date. *:
Analysis Time..:
GDRQ1lAF04/03/0404/13/0421:47
Matrix ..... s SOLID
Metbod ..... SW846 8151A
PARAMETER2,4-D2,4-DB2,4,5-T2,4,5-TP (1ilvex)DalaponDicambaDichlorpropDinosebMCPAMCPP
RESULTNDWDWDNDNDlNDVDNDNDID
REPORTINGLIMIT81e120204141811281008100
UNITSug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
SURROaATEDCAA
PERCENTRECOVERY95
RECOVERYLIMITS(39 - 96 )
IK= CS) :
Client Sanple ID3 E5-12
GC Semivolatiles
Lot-Sample # ... :Date 8ampled ... :Prep Date ...... :Prep Batch I... :Dilution Factor:
D4D030176-005
04/01/04 15:4004/08/04
4098553
1
Work Order 0...: oDHQ21AFDate Received..: 04/03/04
Analysio Date..: 04/13/04
Analysis Time..: 22:29
Matrix ..... : SOLIm
Method ...... 8W846 8151A
PARAMETER2,4-D2,4-DB2,4,S-T2,4,5-TP (SilveX)DalaponDicambaDichlorpropDinosebMCPAMCPP
RESULTNDNDNDNDEDNDNDNDNDND
REPORTINGL8M1T8181
20204141811281008100
UNITSug/kgug/kgug/kgug/kguglkgug/kgug/kgug/kgug/kgug/kg
SURROGATEDCxA
PERCENTRECOVERYE7
RECOVERYLIMITS(39 - 96 )
NOTE(S) :lteS m d rqpoti linus laxc b 1 ted br dy wigh
Client Sample ID: 8S-13
GC semivolatiles
Lot-Sample #...: D4D030176-006Date Sampled.....: 04/01/04 16:10Prep Date .. :.... 04/08/04Prep Batch #...: 4098553Dilution Factor: 1
Wozk Order #...sDate Received..:Analysis Date..tAnalysis Time..:
GDHQ31AF04/03/04
04/13/0423:10
Matrix .. ... : SOLID
Ketbod .... : SW846 815iA
PARAMETER
2,4-D
2,4-DB2,4,5-T2,4,5-TP (Silvex)DalaponDicambaDichlorpropDinosebMCPAKCPP
RESWIdTNDNDMDNDNDNDNDNDEDED
REPORTINGLIMIT81
8120204040el1281008100
UNITSug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kg
SURROGATEDCAA
PERCENTRECOVERY98 *
RECOVERYLIMITS(39 - 96 )
NOTH (S).> Sunapw recovM J Ouside sasfd cmWl liaos
Fesus and veporg limnts hke ben #AusW br wy wel&.
Client Sample TD: SS-15
GC Sesivolatiles
Lot-Sample #...: D4D030176-007Date Sampled ... s 04/01/04 13:10Prep Date ...... s 04/08/04Prep Batch C...: 4098553Dilution Factor: 1
Work Order I...:Date Received..:Analysis Date..:Analysis Time..:
GDHQ42AP04/03/0404/13/0423:51
MatriX ... .: SOLID
Method .... : S W846 8151A
PARAMETER2,4-D2,4-DB2,4,5-T2,4,5-TP (Silvex)DalaponDicambaDichlorpropDinosebMCPAMCPP
RESULTNDNDNDNDND1DNDNDNDND
REPORTINGLIMIT818120204040811281008100
UNITSug/kgug/kgug/kg'ug/kgug/kgug/kgug/kgug/kgug/kgug/kg
SURROGATEDCZA
PERCENTRECOVERY98 *
RECOVERYLnUTS(39 - 96 )
OTE(S) :* Sunsptewyei outdewed ewurl Kinks
Kesiks a repordmg Fu hve kem i baZW fOr b WhL
Client Sample mD: SS-16
6C Seaivolatiles
Lot-Sample 0...:Date Sampled...:Prep Date ......:Prep Batch #...:Dilution Factor:
D4D030176-00804/01/04 14:4004/08/0440985531
Work Order C...:Date Received..:Analysi Date.. :Analysis Time..:
GDHQ51AF04/03/0404/14/0401:15
Matrix ...... : SOLID
Method . . SW846 8151A
PARAMEIER2,4-D2,4-DB2,4,5-T2,4,5-TP (Silvex)DalaponDicambaDichlorpropDinosebMCPAMCPP
RESU[TNDNDNDNDNDND
* ND
NDNDED
REPORTINGLIMIT818120204040
8112
81008100
UNITSug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kg
SURROGATEPERCENTRECOVERY
95
RECOVERY
LIMITS(39 - 96 )
mOTE (S):Rauft a rqwof Emits have be= ausW fo dry wegr.
LO OD GREMEM
Client Sample ID: &S-2
TOERL Metals
lot-SaMple 6...: D4D030176-001Date Sampled...: 04/01/04 12:30 Date Received..: 04/03/04
REPORTINGPARAMETER RESULT LIMIT UNITS METHOD
Prep Batch 1.s:4096254Mercury RD 34 ug/kg 8W846 7471A
Hatr, ....... :
PREPARATICN-ANALYSIS DATE
SOLID
WORKORDER #
_ _ _ _ _ _ _ _ _ _ _ _ _
04/13-04/14/04 GDHQL1AL
Dilutio Factor: 1 Analysis Time..: 11:S4
Prep Batch ... : 4097647Arsenic 0.76 B 2
Diii
Lead 2.8 0Dii
Selenium kD 1Dill
marium 22 1Diii
Cadmium ND 0Dill
Chrolium 5.9 1Dili
silver 0.099 B 1
WOM (S):Rasuk am! qrepdnh lbars km beeu adjuned far dry wei1A.B Eawd euk. less k 9s RL
L. 0 mg/kgaLtion Factor: 1
O.81 mg/kgtioe Factors 1
1.3 mg/kgLtion Factor: 1
.a mg/kgrtion Factor: 1
,.S1 mg/kgLtion Factor: 1
1.0 mg/kgitiax Factors 1
.0 gl/kgItian Factor: 2
5W846 6010BAnalysis Time..: 01.S6
8H846 6010BAnalysis Time.-. 01:56
SW846 6010BAnalysis Time..: 01:56
8W846 6010BAnalysis Time.. : 01256
SW846 6010BAnalysis Time. .: 01:5C
E1846 6010B
Analysis Time..s 01:56
S1846 6010BAnalysis Time..: 01:56
04/09-04/17/04
04/09-04/17/04
04/09-04/17/04
04/09-04/17/04
04/09-04/17/04
04/09-04/17/04
04/09-04/17/04
GMHQLIkP
GMQLrAQ
GDHQL1AR
GDHQL1AN
aEQLUJ
GDHQLIAK
LEOD GREW
Client Sanple IDs 8S-6
* TOL Metal;
Lot-SamPle 8....: D4D030176-002Date Sampled....: 04/01/04 10:40 Date Received..: 04/03/04
REPORTINGPARAMETER RESULT LIMIT UNITS MTOD
Prep Batch 8...: 4096254Mercury ED 33 ug/kg SW846 7471A
Dilution Pactor: 1 Analysis Time..s 12:00
Matrix ......
PREPARATION-ANALYSIS DATE
04/13-04/14/04
SOLID
WORKORDER #
GDHQXlAL
Prep Batch 1... 4097647Arsenic 0.76 B 1.0 mg/kg
Dilution Factors I
Lead 2.2 0.81 mg/kgDilution Factors I
Selenium 1D 1.3 mg/kgDilution Factors 1
Barium 15 1.0 mg/kgDilution Factor: 1
Cadmium ED 0.51 mg/kgDilution Factor: 1
Chrcuium 3.1 1.0 mg/kgDilution Tactors 1
silver 0.10 B 1.0 mg/kg
Dilution Factor: 1
NMTE(S):RIesmulamn epoxg Ims have been 4usd for dry Lw
B EmaiendL Reft bkkm d= RL
8R846 6010BAnalysis Time..x
18(46 6010BAnalysis Time..l
8W846 6010BAnalysis Time..
8H846 6010BAnalysis Time..:
8W846 6010BAnalysis Time..:
81946 6010BAnalysis Time..s
8N846 6010BAnalysis Time..
02:01
02:01
02:01
02:01
02:01
02:01
02:01
04/09-04/17/04
04/09-04/17/04
04/09-04/17/04
04/09-04/17/04
04/09-04/17/04
04/09-04/17/04
04/09-04/17/04
Gnnox2P
GD8Q=2A
GDHQX1AR
eHOX2AG
GDHQXlAH
6HQX1A6
G3HOX3AK
0OHOOD GREEN
Client Sample ID: SS-9
SL metals
Lot-Sample I...: D4D030176-003Date Sampled...: 04/01/04 15:15 Date Received..: 04/03J
REPORTINGPARAMETER RESULT LIMIT UNITS METHC
Prep Batch #...t 4096254Mercury ED 33 ug/kg SW844
Dilution Factor: 1 nalysi
/04
[OD
6 7471AU Time..: 12:02
matrix.....:
PREPARATION-ANALYSIS DATE
04/13-04/14/04
SOLID
WORK
ORDER #
GDHQ01AL
Prep Batch I... 4097647Arsenic ND 1-
Tead 3.3 0.D lul
Selenium ED 1.Dilul
Barium 53 1.Dilui
Cadmium ND 0.Dilul
Chromium 3.4 1.Dulut
silver 0.085 B 1.Dilul
WNr(S):Reks and rpznhg Wmkhe been adjsed for dry w*elgB Enmacd Reu ites ItssdI than RL
.0 mg/kgLion Factors 1
.81 mg/kgtion Vactors 1
.3 mg/kgtion Factors 2
.Q mg/kgtlion Factors 1
.51 mg/kgtion Factors .
.0 mg/kgdton Factor: 1
.0 mg/kgoti Factors I
8W846 6010BAnalyix Time..: 02s:05
S6846 6010BhAalyxis Time.. 02:05
5W846 6010BAnalysic Time..: 02:05
11846 6010BAnalysin Tise..: 02:05
SW846 6010BAnalysis Time..s 02:05
5846 6010BAnalysis Time.., 02:05
53846 60101Analyxis Time..: 02:05
04/09-04/17/04
04/09-04/17/04
04/09-04/17/04
04/09-04/17/04
04/09-04/17/04
04/09-04/17/04
04/09-04/17/04
GDEQOlAP
GDHOOQIA
GDRQO1AR
GDEHOAG
GDEQO1AM
GDED01W
GDQ0OI
LW GRM
Client Sample ID:
TO7hL Ketals
Lot-SaMple t...s D4D030176-004Date Sampled...: 04/01/04 10:00 Date Received..: c
REPORTINGPARAMETER RESULT LIMIT UNITS
Prep Batch .. : 4096254Mercury ED 33 ug/kg
04/03/04
METHOD
matrix ...
PREPARJMIOt-ANALYSIS DATE
04/13-04/14/04
SOLID
WORKORDER #
GDIQUlALSW646 7471Azalysis Tie.. s 12:04Dilutioa Factor: 1 A
Prep Batch ... : 4097647Arsenic 0.89 B I
Lead 2.8 CDilh
Selenilum ED IDlli
Barium 19 1Dill
Cadmium ND a
Dill
cranium 3.4 1Dill
Silver 0.11 B 1Dll
3auss and epwtDg Kmits bave be adaged for dLy wigt
3 Esimted rekd& Ii eW tan RL
.0 mg/kglution Factors 1
0.81 mg/kgatlon Factor: 1
.3 mg/kgatias Factors 1
.0 mg/kgatloa Factors 1
D.51 mg/kgLitla Factor: 1
.0 Mg/kgtiaon Factors 1
1.0 Mg/kgLtlas Factor. 1
91(846 601QBAnalysis Time..s
51(846 6010BAnalysis Time.-:
5W846 6010Banalysis Time.. 3
8846 6010BAnalysix Time..;
8W846 6010BAnalysi Time. .
61846 6010BAalysiu Time.. t
81846 6010BAnalysis Time.:
02:19
02 :19
02:19
02:19
02:19
02:19
02:19
04/09-04/17/04
04/09-04/17/04
04/09-04/17/04
04/09-04/17/04
04/09-04/17/04
04/09-04/17/04
04/09-04/17/04
GMEQ11AP
WDWQ11
GDEQ11AR
GDHQ1IW
GDEQUlAR
GEH11A
GDHWilAi
Client Sample ID: 8S-12
TOTAL Het ls
Lot-Sauple 4...: D4D030176-005Date Sampled...: 04/01/04 15:40 Date Received..: 04/03/04
REPORTINGPARAMETER RESUILT LIMIT UNITS METHOD
Prep Batch 4...: 4096254Mercury ND. 34 ug/kg 6W846 7471A
Dilution Factor: 1 Analysis Time..: 12:06
Matrix .... :
PREPARATION-ANLYSEIS DATE
04/13-04/14/04
SOLID
WOREORDER #
GDHQ21AL
Prep Batch 4097647Arsenic 0.77 B 1.0 mg/kg
Dilution Factor. I
Lean 2.7 0.81 mg/kgDilution Factor: 1
Selenium ID 1.3 mg/kgDilution Factors 1
Barium 19 1.0 mg/kgDilution Factors 1
Cadmium ND 0.51 mg/kgDilution Factor: 1
Crcmitniu 3.5 1.0 mg/kgDilution Factor: 1
Silver 0.10 B 1.0 ng/kgDilution Factor: 1
ZKY (S) gRme bs and epoung Iinhs e km been swtd fbr dry wdghL
B EsiWd resut. Remik k ms dan DL
8N846 6010BAnalysis Time..: 02:24
81846 6010BAnalysis Time..: 02U24
B8146 6010BAnalysis Time. . 02:21
611846 6010BAnalysis Time..: 02:24
8W846 6010BAnalysis Time..: 02:24
S3846 6010BAnalysis Time..i 02M24
83946 6010BAnalysis Tize..t 02:24
04/09-04/17/04 DEHQ22AP
04/09-04/17/04 GDEQ21AQ
04/09-04/17/04 GDHQ21AR
04/09-04/17/04 GD9Q21AG
04/09-04/17/04 GDEQ21AH
04/09-04/17/04 GDQ21M
04/09-04/17/04 G6DQ2IAM
WLCE1O0D GREENE
Client Sample XD: BS-13i
TO= Hetala
Let-Sanple f...s D4D030176-006Date Sampled, ... : 04/01/04 16:10 Date Received..s 04/03/04
REPORTINGPARAMETER RESULT LIMIT UNITS MTOD
Prep Batch 1.: 4096254Mercury wD 33 ug/kg SW846 7471A
Matrix ...... :
PREPARATION-ANALYSIS DATE
04/13-04/14/04
SOLID
WORKORDER #
GDHQ31ALDilution Factort 1 Analysis Time. . 2:08
Prep Batch 1.s:4097647Arsenic 1D I
Dil
Lead 2.6 CDil,
Selenium ED IDill
Barium 16 1Dill
Cadmium ED CDill
Chtmrium 3.0 2
Silver ND 1
Dill
wmO S):ekfh md zqxuwg lts km bhese ajustd to weht.
.. O nmg/kguticn Factor: 1
).81 ug/kgutien Factor: 1
1.3 Mg/kgutioa Factor: 1
I.0 mg/kgution Factor: 1
O. 51 mg/kglution Factor: 1
1.0 mg/kgution FactorS I
.0O mg/kgLtlen Factor: 1
SW846 6010BAnalysis Time-.
01846 6010B1nalysis Time.:
SW846 6010BAnalysis Time..:
511846 6010BMalysis Time..:
SW846 6010BAnalysis Time..t
53846 6010BAnalysis Time..:
SW846 60109Amalymis Time..:
02:28
02:28
02:28
02U28
02:28
02:28
02:28
04/09 -04/17/04
04/09-04/17/04
04/09-04/17/04
04/09-04/17/04
04/09-04/17/04
04/09-04/17/04
04/09-04/17/04
GDHQ3lAP
GMMi31AO
GDHQ31AR
GUQ31AG
GDHQ31AN
GDH~3AJ
GDHQ32.AR
WOCD
Client Sample ID: ES-15
TOTAL Metals
Lot-Sanple #...: D4D030176-007Date Sampled...: 04/01/04 13:10 Date Received..: 04/03/04
MatriX .... : SOLID
REPORTING PREPARATION-ANALYSIS DATE
____
PARAMETER
Prep Batch
Mercury
_ RESULT
1...: 4096254ND
_ LIMIT UNITS
33 ug/kgDilution Factors 1
; METHODWORKORDER #
GDiQ41AL8W846 7471AAnalysiu Time..t 12:10
04/13-04/14/04
Prep Batch ... : 4097647Arsenic ND 1.0 mg/kg
Dilution Factors 1
Lead 2.5 0.81 mg/kgDilution Factors I
Selenium ND 1.3 mg/kgDilution factor: 1
Barium 17 1.0 mg/kgDilution Factora 1
Cadmium ND 0.51 mg/kgDilution Factor: 1
chrmium 3.1 1.0 mg/kgDilution Factor: 1
Silver 0.10 B 1.0 mg/kgDilution Factor. 1
BOTE(S):Reas wd repontb Kwim have been 4and ft day weh.
B Esdiued tre. Resul is Uazn RL.
BW846 6010B3na9lysi Time..1 02:33
SW846 6010BAnalyai. rime.. s02:33
83W846 6010BAnalysis Time.,. a02:33
S1846 6010BAnalysis Time.-a 02:33
S3846 6010Banalysis Time.. i 02:33
8H846 6010BIealyuia TiMe..9 02233
51846 6010 31nalyui Time..: 02:33
04/09-04/17/04
04/09-C4/17/04
04/09-04/17/04
04/09-04/17/04
04/09-04/17/04
C4/09-04/17/04
04/09-04/17/04
GDHQ4lAP
GDEQ41AQ
GDHQ41AR
GD041AG
GDHQ41A
GDR41AJ
GDEHQ41A
Client Sample ID: E8-16
TOTAL Metals
Lot-Sample z...: D4D030176-008Date Sampled...: 04/01/04 14:40 Date Received..: 04/03/1
REPORTINGPARAMETER RESULM LIMIT UNITS METRO]
Prep Batch 0...: 4096254Mercury ID 33 ug/kg 8W846
Dilution Factors 1 Analysis
'0
D
Matrix ..... :
PREPARATION-ANALYSIS DATE
04/13-04/14/04
SOLID
WORKORDER #
GDHQ5lAL7471A
Time..: 12U12
Prep Batch .. : 4097647Arsenic 0.96 B 1.0 mg/g
Dilution Factors 1
Lead 2.9 0.B1 mg/kgDilution Factor: I
Selenium ED 1.3 mg/kgDilution Factor, 1
Barium 24 1.0 mg/kgDilution Factor: 1
Cadmium ED O.50 mg/kgDilution Factors I
Chbrcuum 3.7 1.0 =g/kgDilution Factor: 1
Silver 0.11 B 1.0 mg/kgDilution Factor: 1
MOTE(S):Re uad rqt bngs have beem s#usted for dry weihL3 Esnme resuk Resk k ss duan RL
8R846 6010BAnalysis Time..
81846 6010BAnalysis Time..:
SW846 6010BAnalysis Time.. a
8W846 6010BAnalysis Time..:
SW846 6010Banalysis Time..:
811846 6010BAnalysis Time.. :
51846 6010BAnalysis Time. . s
02:37
02a37
02:37
02:37
02:37
02:37
02s37
04/09-04/17/04 GEO51AP
04/09-04/17/04 GEQ51AQ
04/09-04/17/04 GDRQ5lAR
04/09-04/17/04 GD5IAG
04/09-04/17/04 GDH0QS1A
04/09-04/17/04 GDMQSthJ
04/09-04/17/04 GDEQ51AK
I GOD -
Client Sauple ID: 8S-2
General Cbemi try
Lot-Sample #...s D4D030176-001 Work Order #...: GDHQL
Date SaMipled...: 04/01/04 12:30 Date Received..: 04/03/04Matrix........ : SOLI
PARAMETEIFluoride
z RESULT RL UNITS
ED 10 ~ mg/kg
Dilution Factors 1
MEHOD83846 9056valysixs Time..: :53
PREPARITION- PREPANALYSIS DATE BATCH #04/15/04 4107487
Percent moisture 1.6 0.10 tDilution Factors 1
ICMM 160.3 MD 04/19/04nalyuin Time.. 17:3S
4110593
IWOTE(S) :RL Rqofftg Limk
Imks Wz roftd Hfmit lave beem I d forry weight.
Lot-SaMPle t...: D4D030176-002Date SanPled... : 04/01/04 10:40
PARAMETER RESULT
Fluoride SDDilu
Percent Moisture 1.3Dilu
IWO= CS):RL Reporftg Lhk
Resauh wh ft links have kme Imed mr LT .gbt
.CKWOOD -
Client Sauple Th: SS-6
General Cemistry
Work Order 1... : GDHQX HaiDate Received..: 04/03/04
RI; UNITS METHOD
10 mg/kg SW846 9056tion Factors 1 Analyuli Time.. , 16127
0.10 t HMCW 160.3 MODlt4i lactor: 1 Analyst. Time..: 17:35
.ri .... .SOLID
PREPARATION- PREPANALYSIS DATE BATCH #
04/15/04 4107487
04/19/04 4110593
Client Sample ID: CS-9
General Meml try
Lot-Sample #...: D4D030176-003 Work Order q...: GDHQ0
Date Sampled...: 04/01/04 15:15 Date Received..: 04/03/04
HatriX ..... : SOLID
PREPARATION- PREP
ANALYSIS DATE BATCH #PARAMEMT RESULT RL UNITS METHOD
Fluoride 1.0 B 10 09/kgDilution Factors 1
3846 9056Analysix Time. . 16,38
04/15/04 4107487
Percent Noisture 1.2 0.10 %Dilutimn Factors 1
MKMN 160.3 HU 04/19/04Analysi Time.., 17:35
4110593
NME (S):RL Rleponhg Lk
Res deportng bikhav¢eo kJWedfordry wdpL
B Eye; lst k ResSUWth ku OmRL
mD GRAMB
Client Sample ID: 8S-11
Geoxal Chemistry
Lot-SaWple I... : D4D030176-004 Work Order t...: GDHQ1Date Sanpled...: 04/01/04 10:00 Date Received..: 04/03/04
Matrix.........: SOLID
PARAMETER
Mluoride
RESULT
1.2 B
RL UNITS
10 mg/kgDilution Factor: 1
0.10 tDilution Factors 1
PREPARATION- PREP- METHOD ANALYSIS DATE BATCH #
S8E46 9056 04/15/04 4107487anyaly Time..o 1H5O '
MCAUW 160.3 MM 04/19/04 4110593Analyusi Time... 17s35
Percent Moisture 1.3
l0T () v.RL Rupotdng Uhit
Remsui mx! reptifg Nazs live beestdgsped ft dry *bLt.
B sed;Vt Resul Is les Iu DL
LOCo0D. GREEHH
Client Sample IDs SS-12
erl bPM try
Lot-Sample #...s D4D030176-005 Work Order I...s GDHQ2Date Sampled...: 04/01/04 15:40 Date Received..s 04/03/04
HatriX ... .: SOLID
PREPARATPARAMETER
Fluoride
Percent Moisture
RESULT RL UWITS
]w 10 mg/kgDilution Factor: I
1.5 0.10 t
Dilution Factort 1
METHOD ANALYSIS
8W846 9056 04/15/04Analysia Time..: 17t01
HCRNW 160.3 MM 04/19/04Aaly~is TiMe..: 17:35
XON- PREPDATE BATCH #
4107487
4110593
KTH (S) SRL Reponig LUit
ts S rpwft Emhs mh bce Oaen 4ustd frdzy wdgbL
Lot-Sanple I...: D4D030176-006Date SaMpled...: 04/01/04 16:10
PARAMETER RESULT
Fluoride EDDilul
Percent Moioture 1.1Dilul
NOTBW8 sRL Repofiog LhakRe v*s fepotng b kve beaJeld rdry htL
lwCD GR-0 .
Client Sample ID: ss-13
General Chemi try
Work order #...: GDHQ3 MatDate Received..: 04/03/04
RL UNVTS METHOD
10 mg/kg SW846 9056tion Factor: I analysis Time. .3 17:35
0.10 t HKMfW 160.3 MMsti Factors I Analysis TiLe..: 2.7:35
=- ��
niX ... . : SOLID
PREPARATION- PREPANMLYSIS DATE BATCH #
04/15/04 4107487
04/19/04 4110593
IDCKKO -Ra
Client Sanple ID: 5S-35
General Clemistry
Lot-Sample #...: D4D030176-007 Work Order 8...: GDHQ4Date SamPled ... : 04/01/04 13:10 Date Received..: 04/03/04
MatriZ ...... SOLID
PREPARATION- PREPANALYSIS DATE BATCH #Ilz.qTff.'r 10T. TThrrorg mfTEOn
Fluoride 1.0 B 10 mg/IgDilution Vactowi I
51(46 9056natycs TiSm..: 17346
04/15/04 4107487
Percent moisture 1.2 0.10 "Dilution Factort 1
HCMa 160.3 ED 0411914anlysiff Time..: 17:35
43a0593
la= (S) :DL Reporting Unitc
Resutts md reportics limis ham been aCfusted bu dy weighta9 Estlmated result Ranhk I kms gmn RL
OD -E
Client Sample ID: S3-16
General Chemistry
Lot-Swaple t...: D4D030176-008 Work Order #...: GDHO5 Natrix ......... ,: SOLID
Date Sampled...: 04/01/04 14:40 Date Received..: 04/03/04
PREPARATION- PREP
PARAMUETER RESULT RL UNITS METHOD ARJMYSIS DATE BATCH P
Fluoride ND 10 mg/kg 8W846 9056 04/15/04 4107487
Dilution Factors 1 Analyxis Time-: 17:s7
Percent Moisture 0.81 0.10 t !4CAW 160.3 MOD 04/20/04 4111603
Dilutio Jactor 1 Malysis Time : 17:15
RL Repordag LUnitReuIs and rpon 1Mks hke beea a4*e Ibr dry wdghL
QC DATA ASSOCIATION SUMMARY
D4D030176
Sample Preparation and Analysis Control NUmbers
ANALYTICAL LEACH PREPSAMPLE# MATRIX METHOD BEATCH # BATCH # HS RVN#
001 SOLID SW846 9056 4107487 4107237SOLID SW846 7471A 4096254 4096141SOLID 5W846 8141A 4095125 4095022SOLID 8W846 8081A 4096552 4114264SOLID gW846 6260B 4104274 4104174SOLID 8W846 6270C 4097621 4097303SOLID SW846 6010B 4097647 4097320SOLID SW846 8151A 4098553 4099301SOLID MCAW 160.3 ROD 4110593 4111080
002 SOLID SW846 9056 4107487 4107237SOLID SW846 7471A 4096254 4096141SOLID SW846 8141A 4095125 4095022SOLID SW846 8081A 4096552 4114264SOLID 8W846 62609 4104274 4104174SOLID SW846 8270C 4097621 4097303SOLID 8W846 6010B 4097647 4097320SOLID W8W46 8151A 4098553 4098301SOLID MCAKW 160.3 MOD 4110593 4111080
003 SOLID mW846 9056 4107487 4107237SOLID SW846 7471A 4096254 4096141SOLID 6W846 8141A 4095125 4095022SOLID SW846 8081. 4096552 4114264SOLID SW846 8260B 4104274 4104174SOLID SW846 8270C 4097621 4097303SOLID 8W846 6010B 4097647 4097320SOLID 8W846 81511 4098553 4098301SOLID MCAWW 160.3 MOD 4110593 4111080
004 SOLID SW846 9056 4107487 4107237SOLID 8W846 7471. 4096254 4096141SOLID SW846 81412 4095125 4095022SOLID 6W846 80811 4096552 4114264SOLID 8W846 8260B 4104274 4104174SOLID EWS46 8270C 4097621 4097303SOLID 8W846 6010B 4097647 4097320SOLID EW846 8151A 40985S3 4098301SOLID MCAWW 160.3 MOD 4110593 4111080
005 SOLID SW846 9056 4107487 4107237SOLID 6W846 7471A 4096254 4096141SOLID SW846 8141A 4095125 4095022
(Continued on next page)
QC DATA ASSOCATION SUMMARY
IYD030176
Sample Preparation and Analysil.Control NZumbers
ANALYTICAL LEACH PREP
SAMPLE# MRIX METHOD BATCH BATCH * MS R'UN
005 SOLID 8W846 8081A, 4096552 4114264
SOLID 8W846 8260B 4104274 4104174
SOLID 8N846 8270C 4097621 4097303
SOLID SW846 6010B 4097647 4097320
SOLID W8N46 8152A 4098553 4098301
SOLID MCAWW 160.3 MOD 4110593 4111080
006 SOLID 8W846 9056 4107487 4107237
SOLID 8W846 7471A 4096254 4096141
SOLID 8W846 8141A 4095125 4095022
SOLID 8W846 8012A 4096552 4114264
SOLID 6W846 8260B 4104274 4104174
SOLID 8W846 8270C 4097621 4097303
SOLID SW846 6010B 4097647 4097320
SOLID 8W846 8151A 4098553 4098301
SOLID MCAWW 160.3 MOD 4110593 4111080
007 SOLID 6W846 9056 4107487 4107237
SOLID 8W846 7471A 4096254 4096141
SOLID 6W846 8141A 4095125 4095022
SOLID SW846 80811. 4096552 4114264
SOLID S91846 82605 4104274 4104174
SOLID 6W846 8270C 4097621 4097303
SOLID SW846 6010B 4097647 A097320
SOLID SW846 81511. 4098553 4098301
SOLID MCAWW 160.3 MOD 4110593 4111080
008 SOLID 8W846 9056 4107487 4107237
SOLID S8146 74711 4096254 4096141
SOLID 8W846 81411. 4095125 4095022
SOLID SW846 8081. 4096552 4114264
SOLID SW846 8260B 4104274 4104174
SOLID 6W846 8270C 4097621 4097303
SOLID 8W846 60103 4097647 4097320
SOLID SW846 81511 4098553 4098301
SOLID MCANW 160.3 MOD 4111603 4112076
m DE B REPaRT
GC/MS Volatiles
Client Lot #...: D4D030176NB Lot-Sample #: D4D130000-274
Analysis Date..s 04/12/04
Dilution Factor: 1
Work Order #...: GD3FW1AA
Prep Date ...... : 04/12/04
Prep Bateh I... : 4104274
Matrix ......... g SOLID
Analysis Time..: 12:26
PARAMETERAcetoneBenzeneBromodichloromethaneBromofonrmBromomethane2-Butanone (MEN)Carbon tetrachlorideChlorobenzeneChloroethaneChloroformcbioromethaneDibromomethane1,2-Dibromoethane (EDB)1,2-Dichlorobenzene1,3-Dichlorobenzene1,4-DichlorobenzeneDichlorodifluoromethane1,1-Dichloroetbane1,2-Dichloroethane1,1-Dichloroethenei.2-Dichloroethene
(total)ciE-, 12-Dichloroethenetrans-1,2-Dich1oroethene1,2-Dichloropropanecis-1,3-Dichloropropenetrans-1,3-DichloropropeneEthylbenzene2-RexanoneMethylene chloride4-Methyl-2-pentanoneStyrene1,1,1,2-Tetrachloroethane1,1,2.2-TetrachloroethaneTetrachloroetheneToluene
1,2,4-Trichloro-benzene
1,1,1-Trichloroetbane1,1,2-TrichloroethaneTrichloroethene
RESULT3.8 JNDNDNDNDNDND
NDNDNDNDNDNDNDhDNDNDNDNDND
ND
ND
EDNDNDNDllDNDNDNDNDND
ND
ND
NDND
ND
TLIMIT
205.05.05.010205.05.01010105.05.05.05.05.0105.05.05.05.0
2.52.55.05.05.05.0205.0205.05.05.05.05.05.0
5.0 I5.0 15.0 I
UNITS
uglkgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgag/kgug/kgUg/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kg
ug/kgug/kg
ug/kgUg/kg
ug/kg
METHOD6N846 8260BS6846 8260B6W846 82.60BSW846 8260B6WE46 8260B6W846 826038W846 8260BSW846 8260B8W846 82603SW846 8260B8w846 8260BSW846 8260B8w846 8260BSW846 8260B
5W846 8260B5W846 8260B5W846 8260B8W846 8260B8W846 8260B8W846 8260B81846 8260B
8W846 8260B8W846 8260B8W846 82608
S8K46 8260BSW846 8260B8W846 8260BSW846 8260B
8W846 8260BSW846 8260B8W846 8260B
8w846 8260B8W846 8260B
8W846 8260B
6R846 82603
8W846 8260B
8w846 8260B
6w846 8260B8W846 8260B
(Continued on next page)
METOD ELAN RDPORT
GCCkS Volatiles
Client Lot #...: D4D030176 Work Order #...: GD3FW1MA Katr .... : SOLID
PARAMETER
Trichlorofluoromethane1,2,3-TrichloropropaneVinyl chlorideXylenes (total)n-Butylbenzenesec-ButylbenzeneIsopropylbenzene1,2,4-Trimethylbenzene1,3,5-TriMethylbenzenen-Propylbenzenetert-ButylbenzeneDibromochloromethane2-Chlorotoluene4-Chlorotoluene1,2-Dibromo-3-
chloropropane (DBCP)1,3-Dichloropropane2,2-Dichloropropane1,1-DichloropropeneHexcadhlorobutadiene4-IsopropyltolueneMethyl tert-butyl ether1,2,3-Trichlorobenzenem-Xylene & p-Xyleneo-KyleneBromobenzeneEromochloromethane
RESULTED
DEDRDNDNDVDEDNDEDNDNDVDNDND
NDEDIDNDNDNDNDNDMDNDND0.58 J
REPORTINGLIMIT105.05.05.05.05.05.05.05.05.05.05.05.05.010
5.05.05.0
5.05.0205.02.52.55.05.05.0
UNITSug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kg
ug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/i
FETHODSW846 8260B8W846 8260B68)46 8260BSW846 8260B68W46 8260BSW846 826088W846 8260B8IW846 8260BSW846 8260B8W846 8260BSW846 8260B
S8)46 8260B8W846 8260B8W846 8260B8W846 8260B
SW846SW8468W846S8)468W846SW8468W846SW846SW846SW8466W8468(846
8260B8260B826088260B8260B8260B8260B8260B826088260B8260B8260B
SURROGATEDibromofluoromethane1,2-Dichloroethane-d44-BromofluorobenzeneToluene-dS
PERCENTRECOVERY1001059798
RECOVERYLTTS(71 - 136)(67 - 131)(71 - 124)(77 - 129)
cdmd-m am pe-omad b-bm mding aowid simd-offm s a n ca holrd ks
J EsdmB d esuX 1mh k kss d= RL
XiWORATORY CONTROL SAMPLE B7AL1AT( REPORT
GC/mS Volatiles
CliCnt Lot #...: D4D030176LCS Lot-Saiplet: D4D130000-274Prep Date...... : 04/12/04Prep Batch 0....: 4104274Dilution Factor: 1
Work Order #... . GD3FWIAC-LCS atriSx ........ SOLIDGD3FWlhD-LCSD
Analysis Date..: 04/12/04Analysis Time..: 11:40
PARAMETERSenzene,
0Blroene
1, l-Diamroethene
Toluene
Tricbloroethen
PERCENT
RECOVERY9210890105911039310385101
RECOVERYLIMITS
(72 - 121)(72 - 121)(75 - 115)(75 - 115)(60 - 133)(60 - 133)(71 - 117)(71 - 117)(70 - 125)(70 - 125)
BPDRED LIMITS
16
15
13
10
17
METHOD01846 8260B
(0-25) 01846 8260B81846 8260B
(0-25) 8H846 8260B8H846 8260B
(0-25) 61846 8260B61846 8260B
(0-25) 8h846.8260B6H(46 8260B
(0-25) 68146 8260B
SURROGATEDibromofluoromethane
1,2 -Dichloroethane-d4
PERCENTRECOVERY939995106959997100
RECOVERYLIMITS(78 - 118)(78 - 118)(72 - 120)(72 - 120)(76 - 127)(76 - 127)(75 - 120)(75 - 120)
4 -Bromofluorobenzene
Toluene-dS
NOTE (S):Caiwlctlo are pcgmad boe swunfdio kvoi awd-ff hi calmulaW es
, am Fft dwiws bc=n parame
IABORRTORY cNTROLa SAMPL D a= REWOR
GC/HM Volatiles
Clieut Lot #...: D4D030176ICS Lot-Samplet: D4D130000-274Prep Date ...... s 04/12/04Prep Batch #... s 4104274Dilution Pactor: 1
Work Order 6...: GD3FW1AC-LCS Hatri ... . : SOLIDGD3FWlAD-LCSD
Analysis Date..: 04/12/04Analysis Time..: 11:40
SPIKE MEASURED
Benzene
1,1-Difbloroethene
Toluene
Triooe 33en
AMOUNT50.050.0
SO.050.0
50.0
50.0
50.050.0
50.050.0
AMOUNT46.053.845.152.645.351.646.551.442.750.4
UNITSugfkg
ag/kgug/kg
uglkgug/kguglkgug/kguglkg
PERCENTRECOVERY9210890105911039310385101
RPD ETWOD
5846 B260B16 8W846 8260B
8W846 8260B15 81146 8260B
68146 8260B13 O8146 8260B
5846 8260B10 S8146 8260B
S8146 8260B17 81846 8260B
SURROGATE
Dibromoflluorometbane
1,2-Dicbloroethane-dt
4-Bromofluorobenzene
Toluene-dS
PERCENTRECOVERY939995106959997100
RECOVERYLIMITS
(7B - 118)(78 - 118)(72 - 120)(72 - 120)(76 - 127)(76 - 127)(75 - 120)(75 - 120)
Wm (a) ):
hmf ame psened bdome oamnf io o3i towd-off am hb ubted esuk
Boxd pwh 4am awRu d prau
MATRIX SPI SAMPUE3 EVZU9I0Uf REPORT
GC/MS Volatiles
client Lot C...:MS Lot-Sanple #:Date Sampled...:Prep Date ...... s
D4D030176D4D050247-00204/01/04 13:5004/12/04
Work Order C..: GDKHM1-KMSGDKHM1AO-MSD
Date Received..: 04/05/04Analysis Date..: 04/12/04Analysis Time..: 21:10
Matrix .... : SOLID
Prep Batch #...: 4104274Dilution Factor: 1
PARAMETERBekzfene
ctemsnz
1 ,-Dic bloroethene
Toluene
Trichioroethene
PERCENTRECOVERY70725354798671805857
RECOVERYLIMITS(51 - 133)(51 - 133)(28 - 137)(28 - 137)(49 - 134)(49 - 134)(33 - 140)(33 - 140)(46 - 135)(46 - 135)
RPDRPD LIMITS METHOD
SW8463.4 (0-40) 51(46
SK8460.70 (0-40) S846
388469.6 (0-40) 53846
5384612 (0-40) 53846
5K8461.7 (0-40) 5N846
8260B8260B8260B8260B8260B8260B8260B8260B8260B8260B
SURROGATEDibromfluoromethane
1,2-Dichloroethane-d4
4-Bromofluorobenzene
Toluene-dB
PERCENTRECOVERY1031031071108073118119
RECOVERYLIMITS(71 - 136)(71 - 136)(67 - 131)(67 - 131)(71 - 124)(71 - 124)(77 - 129)(77 - 129)
NOTE(S)
BolWd Vit dewtes conurol ptratmot
MM=RZ SPIKE SANPLE DAM REPORT
GC/MS Volatiles
Client Lot S...:MS Lot-Sample I:Date Sampled...sPrep Date ...... :Prep Batch I...sDilution Factor:
D4D030176D4D050247-00204/01/04 13:5004/12/044104274
Work Order I...: GDKHM1X-MSGDEHMlAO--SD
Date Received..: 04/05/04Analysis Date..: 04/12/04Analysis Time..: 21:10
HatriX ..... : SOLID
PARAMETRBenzene
chlorcbenzene
1, 1-Dchloroethene
Toluene
Trichloroethene
SAmLE SP=IEAMOUNT AMT
lD 50.0ED 50.0
ED 50.0ND 50.0ND 50.0ND 50.00.23 50.00.23 50.0ND 50.0ND 50.0
HEASRD
AMOUNT35.036.226.626.839.342.835.640.329.028.5
PERCTUNITS RECVRYug/kg 70ug/kg 72ug/kg 53uglkg 54ug/kg 79ug/kg 86ug/kg 71ug/kg 80uglkg 58mg/kg 57
RPD METHOD0N846 8260B
3.4 01846 8260B38M46 8260B
0.70 SN846 8260B01146 826QB
8.6 S0846 8260BS1846 8260B
12 S0846 8260B38946 8260B
1.7 SN846 8260B
SURROGATEDibromofluoromethane-
1,2 -Dichloroethane-d4
4 -Bromofluorobenzene
PERCENTRECOVERY1031031071108073118119
RECOVERYLIMITS(71 - 136)(71 - 136)(67 - 131)(67 - 131)(71 - 124)(71 - 124)(77 - 129)(77 - 129)
Toluene-de
NxYR f 1 r
Boulpinons am Wefned kfore zwulinc m id rond-off err k cacud gesuk.
Bold Piii denowcs coamrl varmmc
METOD SIAM REPORT
GCINS Seiotle
Client Lot C..: D4D030176
MB Lot-Sanple 4: D4D060000-621
analy5is Date..: 04/22/04Diluticn Factor: 1
Work order .... : GDM57LAA
Prep Date ...... : 04/07/04Prep Batdh 1...s 4097621
Matrix ..... : SOLID
Analysis Time..: 13:41
PAR)METERAcenaphtheneAcenaphthyleneAcetophenone2-Acetylaminofluorene4-AminobiphenylAnilineAnthraceneAramiteBenzo(a)nathraceneBenzo(b)fluorantheneBenzo(k)fluorantheneBenzo(ghi)peryleneBenzo(a)pyreneBenzyl alcoholbiB(2-Chloroethoxy)
methanebis(2-Chloroethyl)-
etherbis (2-Ethylhexyl)
phthalate4-Bromophenyl phenyl
etherButyl benzyl phthalate4-ChloroanilineChlorobenzilate4-Chloro-3-methylphenol2-Chloronaphthalene2-chlorophenol4-Chlorophenyl phenyl
etherChryseneDiallateDibenz(a,h)anthraceneDibenzofuranDi-n-butyl phthalate
1,2-Dichlorobenzene1,3-Dichlorobenzene1,4-Dichlorobenzene3,3'-Dichlorobenzidine2,4-Dichlorophenol
2,6-Dichlorophenol
RESULTNDNDNDNDNDND
NDNDNDDD
NDNDNDND
ED
REPORTINGLIMIT33033033033001600330330660330330330330330330
330
330
ND 330
UNITS
ug/kgu9/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kg
ug/kg
ug/kg
ug/kgug/kgug/kgug/kg
ug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
METHODSW846 8270C
W8)46 8270C8w846 8270C81846 8270C8W846 8270C81846 8270C8W846 8270CSW846 8270C
SW846 8270C6w846 8270C6W846 8270C8w846 8270CSW846 8270CSW846 8270C
6W846 8270C
SW846 8270C
6W846 8270C
6w846 8270C330
NDNDNDNDNDNDND
330330330330330330330
NDNDNDNDNDNDNDNDNDNDND
33066033.03303303303303301600330330
SW8468W8468W846SW846SW846
SW846
8w846
8W8468w846S8846Sw8468w8468W8468W846
8W846
8W846SW846SW846
8270C8270C8270C8270C
8270C8270C
8270C
8270C8270C8270Ce270C8270C8270C8270C8270C
827QC8270C
8270C
(Continued on next page)
I4ETEOD BUMNK REPORT
6CC/s Bemivolatiles
Client Lot I...: D4D030176 Work Order #...: GDM571AA Hatrix .... : SOLID
PARAMETER
Dietbyl phthalateDimethoate7,12-Dimethylbezz(a)-
antbracene3,3'-Dimetbylbenzidine2,4-DimethylphenolDinethyl phthalate1,3-Dinitrobenzene4,6-Dinitro-
2-niethylphenol2,4-Dinitrophenol2,4-Dinitrotoluene2,6-DnintrotolueneDi-n-octyl phthalateDiphenylamineDisulfotonEthyl methanesulfonateFluorantheneFluoreneHexachlorebenzeneHexachlorobutadieneHexachlorocyclopenta-
dieneNexachloroethaneHexachloropropeneIndeno(1,2,3-cd)pyreneIsodrinIsophoroneIsosafroleMethapyrilene3-MethylcholanthreneMethyl methanesulfonate2-MethylnaphtbaleneMethyl parathion2-Methylphenol3-Methylphenol &
4-MethylphenolNaphthalene1,4-Naphthoquinone1-Naphthylamine2-Naphthylamine2-Nitroaniline3-Nitroaniline4-NitroanilineNitrobenzene
RESULTNDNDED
REPORTINILIMIT660660660
NDNDNDNDND
6603303303301600
IDEDNDNDEDEDEDEDIDNDUDND
160033033033033016003303303303303301600
UNITSug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
uglkgug/kg
ug/kgug/kgugfkgug/kgug/kgug/kgug/kgug/kg
SW846SW846SW8468W8468W846
SW846SW846SW846SN146SW8466W8468W846681468W8468W84681W8461SW846
METHODSW846 8270CSW846 8270C
8W846 8270C
8270C8270C8270C8270C8270C
8270C8270C8270C8270C8270C8270C8270C8270C8270C
8270C8270C8270C
NDNDlDVDND
NDNDNDNDNDNDNDND
330330033033033066016006603303301600330330
8W846 8270C
SW846 8270C8W846-8270CSW846 8270CSW846 8270C
6N846 8270C
6W846 8270C8W846 8270C
8W846 8270C8W846 8270C
SW846 8270C8W846 8270C
SW846 8270C
NDlDNDNDEDNDEDND
3301600
330330160016001600330
SW846SW8466W846
SW846SW84688466W8468W846
8270C8270C8270C8270C8270C
8270C8270C
8270C
(Continued on next page)
HEMOD BINK REPORT
GC/MS Bemivolatiles
Client Lot I...: D4D030176 Work Order #...: GDMS71AA. matrix .... : SOLID
PARAMETER2-Nitrophenol4-Nitrophenol4-Nitroquinoline-
1-oxideN-Nitrosodi-n-butylamineN--Nitrosodietb1yamineN-NitrosodimethylamineN-NitrosodiphenylamineN-Nitrosodi-n-propyl-
amineN-BitrosomethyletbylamineN-NitrosomorpholineN-Nitrosopiper&dineN-Nitrosopyrrolidine5-Nitro-o-toluidineParathionPentachlorobenzenePentachloroethanePentachloronitrobenzenePentachlorophenolPhenacetinPhenanthrenePhenolPhorate2-PicolicePronamidePyrenePyridine1,2,4,5-Tetrachloro-benzene
2,3,4,6-TetrachlorophenolThionazino-Toluidine1,2,4-Trichloro-
benzene2,4,5-Trichloro-phenol
2,4,6-Trichloro-phenol
0,0,0-Triethylphosphoro-thioate
1,3,5-Trinitrobenzene
RESULTRDNDND
REPORTIMLIMIT33016003300
IDNDEDNDND
330330330330330
IDEDNDNDNDNDNDNDNDNDlDNDNDED2DNDEDNDND
33033033033066016003301600160016006603303301600660660330660330
ug/kgug/kguzgtkg
ug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kguglkgug/kgug/kgug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kg
ug/kcg
ugtkg
ug/kg
ug/kg
8W846 8270C
SW846 8270CSW846 8270CSW846 8270C
EW846 8270C
8W846 8270CSW846 8270C
EW846 8270CSW846 8270C8W846 8270CSW846 8270C8W846 8270C
8W846 8270C8W846 8270CSW846 8270CSW846 8270CSN846 8270C
8N846 8270CSW846 8270C8W846 8270C8W846 8270C
8W846 8270CSW846 8270C8W846 8270C
8W846 8270C
8W846 8270C8W846 8270C
68846 8270C
-METHODS9846 8270CBW846 8270C
5W846 8270C
EDNDNDND
16001600660330
ND 330
ND 330
5W846 8270C
8W846 8270C
SW846 8270C
8W846 8270C
ND 1600
ND 1600
(Continued on next page)
HIMOD BLMO REPO
GC/S Semaivolatiles
Client Lot #...: D4D030176 Work Order I...: GtM571AA, trix.........: SOLID
REPORTINGT.LTrrq MQTqI MpqweUnn
ADULTS~r- czar--v~
SURROATE2-FluorophenolPhenol-dSNitrobenzene-dS2 -Fluorobiphenyl2,4, 6-TribromophenolTerphenyl-dM4
PERCENTRECOVERY787977736786
RECOVERYLEITS(28 - 95)(35 - 90)(39 - 89)(35 - 86)(11 - 111)(30 - 98)
W0TE(S):CIadatios awe periformd before rcwfig io avoid mdO-ff arm k mi hed cmhLb
LAEORATRY aoNTROi SK14PLE Ey WiT=IO REPORT
GC/MS Sezmvolatiles
Client Lot I...: D4D030176LCS Lot-Sample#: D4D060000-621Prep Date ...... :t 04/07/04Prep Batch 1...s 4097621Dilution Factort 1
Work Order C...: GDM571AC Matrix .... : SOLID
Analysis
Analysis
Date..s 04/22/04Time..: 14:09
PARAMETERAeaephtehne4-Whoro-3-setbylphiendl2- loraphenol1,4-Dichlordbeznzene2,4-Dinitrotoluene4-UitrophenolN-Nitrosodi-n-propyl-
aminePentachlorophenolPhenolPyrene1,2,4-TriChloro-benzene
PERCENTRECOVERY75
797974
797575
RECOVERYLIMITS(49 - 89)(53 - 93)(52 - 92)
(47 - 87)(51 - 98)(37 - 103)(46 - 90)
METHODS8846 8270CSN846 8270C53846 8270C5846 8270CM846 8270CS846 8270CSn846 8270C
77797876
(37 -(52 -(46 -(49 -
96)92)95)89)
SW846SW8468W846R9S46
8270C8270C8270C
8270C
SURROGATE2-FluorophenolPhenol-d5Nitrobenzene-dS2-Fluorobiphenyl2,4,6-TribromophenolTerphenyl-dl4
PERCENTRECOVERY7677
76 .717S81
RECOVERYLIMITS(52 - 92)(52 - 92)(51 - 91)(47 - 88)(48 - 94)(50 - 103)
BOTE(S):Cdlazim oe pfnmed before fomdl w void rmducffamn hI ailated nea1Ls.
BMd pri deotu oz lpume
ZEORATORY CXTROL SAMPLE nac REPORT
GC/MS Semivolatiles
Client Iot 0...: D4D030176IC Lot-Sample#: D4D060000-621Prep Date ...... s 04/07/04Prep Batch 1... : 4097621Dilution Factor: 1
work Order ... : GDM571AC
Znalysis Date..: 04/22/04Analysis Time..: 14:08
Matrix ...... : SOLID
Acenapih en4-Chloro-3-methylphenol2-chiorophenol1, 4-Dibo ez2, 4-Dinitrotoluene4-NitrophienolN-Nitrosodi-n-propyl-
amine
Phenol
Pyrene1,2,4-TriduLoro-
benzene
SPIKEAMOUNT3300495049503300330049503300
4950495033003300
MEASUREDAMOUNT2470393039202450262037202490
3830392025902520
UNITSug/kguglkgugftug/kgug/kgug/kgug/kg
ug/kgug kgugWug/kg
PERCENTRECOVERY75797974797575
METHODSN846 8270C9N846 8270C8(846 8270C8W846 8270C81(46 8270CSH846 8270C81846 8270C
77797876
81(94681(94681(84681(846
8270C8270C8270C8270C
SURROGATE
2-FluorophenolPhenol-d5Nitrobenzene-d52-Fluorobiphenyl2,4,6-TribromophenolTerphenyl-d14
PERCENTRECOVERY7677767175at
RECOVERYLIMITS
(52 - 92)(52 - 92)(51 - 91)(47 - 98)(48 - 94)(50 - 103)
NOTE(S):Ckunih= am perfmed kebforoxmug so ate smmdoff scm In hk ualW rcfs}old pAU d&wW atrl param
MATRa Spin 8W EVLXIO1 RFPRT
GC/MS Semivolatiles
Client Lot 0... sD4D030176MS Lot-Sanple tt D4D020177-001Date Sampled...: 04/01/04 09:4Prep Date ...... s04/07/04Prep Batch #...s 4097621Dilution Factor: 5
Work Order C...:
5 Date Received..:Analysis Date..:Pnalysis Time..
GDE20 LhX-MSGDE201A0 -MSD04/02/0404/22/0420:45
atri...... ... SOLID
Acenaphthene
4-Chloro-3-gethylpbenol
2- hlophrznol
1, 4-Dicblorobenzene
2,4-Diflitrotoluene
4-Nitrxphenol
N-Nitrosodi-n-prxpyl-amine
PERCENTRECOVERYMCDILNCDILNCDILNCDILDC,DILNC,DIhDC,DILNC,DILNC,DrLNC,DILNC,DILNC DILNCDXL
HCDIL
RECOVERYLIMITS(25 - 101)(25 - 101)(32 - 97)(32 - 97)(29 - 95)(29 - 95)(34 - 81)(34 - 81)(31 - 105)(31 - 105)(10 - 128)(10 - 128)(33 - 91)
RPDRPDLIMITS METHOD
0N846 8270C(0-40) 81846 8270C
S8846 8270C(0-40) 8N846 8270C
S1846 8270C(0-40) m846 8270C
E8146 8270C(0-40) 61846 8270C
61846 0270C(0-40) SW846 9270C
E8846 8270C(0-40) S8846 8270C
81846 8270C
(33 - 91) (0-40) S146 8270C
Pentachloropbenol
Phenol
Pyrene
1,2,4-Trichloro-benzene
HCDIDLWC, DILNC, DXLNC, DILKCIDILNCUDILNC. DIL
(10(10(34(34(13(13(33
- 101)
- 101)- 93)
- 93)
- 105)
- 105)
- 88)
S1846(0-40) 5846
51846(0-40) S5946
S1146(0-40) SR846
81(46
8270C8270C8270C8270C8270C8270C8270C
NC,DIL (33 - 88) (0-40) S8846 8270C
SURROGATE2-Fluorophenol
Phenol-dS
Nitrobenzene-ds
2-Fluorobiphenyl
2,4,6-Tribromophenol
PERCENTRECOVERYNC,DILNC, DILNC,DILNCDILNC,DILNC, DLNC, DILNC,DILNC,DILNCDIL
RECOVERYLIMITS(28 - 95)(28 - 95)(35 - 90)(35 - 90)(39 - 89)(39 - 89)(35 - 86)(35 - 86)(11 - 111)(11 - 111)
(Continued on next page)
MATRIX SPIKE SAMPLE EVAWAITICO REPORT
GC/KS Semivolatiles
Client Lot I.,.: D4D030176MS Lot-Sample #: D4D020177-001
Work Order * ... : GDE201AX-MSGDE201AO-MSD
Matrix.........: SOLID
PERCENTSURROGATE RECOVERY
RECOVERYLIMITS
Terphenyl-dl4 KC,DILRC, DIL
(30 - 98)(30 - 98)
OTE (S):
calulaons am perboed borte nuaDt s0 to avoid md-off a b causatd madtL
Dom pdzt 4amoes reuro param m~NC The ncoveuy uIor RPD sm not calcslad.DIL Te coie"atnion h estimated or rti reporsed due to dilution or dfe prese of bmfatSh ayes
}ATRIK m SAMPLE DATA REPORT
GC/MS Semivolatiles
Clielt Lot #...:
uS Lot-Sample #:Date Sampled...:Prep Date .. :...
D4DC30176 Work Order #... :D4D020177-001
04/01/04 09:45 Date Received..:04/07/04 Analysis Date.. s
GDE201AX-MSGDE201AO -MSD04/02/0404/22/04
matrix ......... : SOLID
Prep Batch 1...: 4097621Dilution Factor: 5
Analysis Time.. : 20:45
PARAMETERA hene
4-hloro-3-methylphenol
2-Chlorophenol
1,4-Dichlorobenzene
2,4-Dinitrotoluene
4-Hitrophenol
N-Nitrosodi-n-propyl-amine
SAMPLE SPIKE MEASRD
AMOUNT AIT AMOUNTND 0.0RD 0.0
ND 0.0RD 0.0RD 0.0ID 0.0ND 0.0RD 0.0RD 0.0ED 0.0ID 0.0WD 0.0RD 0.0
UNITS
Uw/gug/kgug9/kuglkgug/ksug9/kugl/guglkgug/kgug/kgug9/kug/kgUg/kg
PERCETRECVRYNCD3hNCUDILNCEDIhNCDILNCDILNC,DILIDICMDLNCDILNCDILXC,DILNCDILNC,DIL
NICDIK
NC,DIL
RPD METHOD51146 8270C8H846 8270C51146 8270CS5846 8270C68W46 8270CS1846 8270C81146 8270C51846 8270CSW846 8270C5846 8270CS5846 8270CS8146 8270CS1846 8270C
5846 8270CWD 0.0
Pentadblorophenol
Phenol
NDEDNDND
ImJNDNM
ND
0.00.00.00.00.00.00.0
0.0
ug/kg
ug/kgug/kgug/kgug/kg
uglkgug/kg
ug/kg
NC.DILNCDILNCDILXCDILHCDILNC,DI3LNC,DIL
NC,DXL
5W846SW1468H846S884681146S8146
81846
8270C8270C8270C8270C8270C8270C8270C1,2,4-Trichioro-
benzeneS81146 8270C
SURROGATE2-Fluorophenol
Phenol-d5
Nitrobenzene-d5
2-Fluorobiphenyl
2,4*6-Tribromophenol
PERCENTRECOVERYNC.DILNCDIL
NC,DILNCDILNC, DILNC,DIL
NC.DILNCDILNC,DIL
KC,DIL
RECOVERY
LIMITS(28 - 95)(28 - 95)(35 - 90)
(35 - 90)(39 - 89)(39 - 89)(35 - 86)(35 - 86)(11 - 111)
(11 - 111)
(Continued on next page)
NATRZK m SAME Dfl REPOtT
CC/M Semivolatiles
Client Lot #...: D4D030176HS Lot-Sample #: D4D020177-001
Work Order ... : GDE201AX-MSODE201AO-MSD
atriX......... SOLID
PERCTETRECOVERYv_
RECOVERYLIMITS
(30 - 98)(30 - 98)
Terphenyl-dl4 CCDILNC,DIL
NOTE(S) :C<muda am pafd befoe zmmuing so miod bind-off arm hi alaced seftBold Viml denote cantrol param terNC The cvery mdor PD we mot Idud.DIL The co ccradon Es asmud or ut rpoeed due oiDd or dAe-p of iterfeting alycm
ETHO B REPORT
GC semivolatiles
Client Lot ... : WDD030176HB Lot-Sample 0: D4D050000-552
Alnalysis Date..: 04/28/04Dilutimn Factor: 1
Work Order # ... s GDJSX1AA
Prep Date ..... : 04/06/04Prep Batch 1...t 4096552
Matrix ..... : SOLID
Analysis Tioe..: 13:34
PARAMETER
Aldrin
alpba-BHC
beta-EHC
delta-BEC
gamia-EXC (Lindane)
Chlordane (technical)
4,4 -DDD
4,4'-DDE
4,4'-DDT
Dieldrin
Endrin
Endrin aldehyde
Endosulfan I
Endosulfan II
Endosulfan sulfate
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
RESULTND
NDNDNDNDNDNDNDNDEDNDND2EDNDNDND
ND
REPORTINGLIaT1.71.71.71.71.7171.71.71.71.71.71.71.71.71.71.71.73.3170
UNITS
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgu/kg
ME=TOD8W846 8081ASW846 B08SASW846 8081A8W846 8081ASW846 808616W846 80BlASW846 8082A5W846 8081A8W846 8081A8W846 8081ASW846 8081A
E8846 8081ASW846 8081A8W846 8081ASW846 8081ASW846 8081ASW846.80812EW846 8081ASw846 80812A
SURROGATEDecachlorobiphenylTetrachloro-m-xylene
PERCENTRECOVERY136106
RECOVERYLMaTS(41 - 142)(50 - 127)
NOTE(S):
LABOPAUY ONTROL SaMPE EVABWLTIO REPORT
GC Semivolatiles
Client Lot t...: D4D030176WCS Lot-Sauplet: D4D050000-552Prep Date ...... s 04/06/04Prep Batch 1...: 4096552Dilution Factor: 2
PARAMETERAldringamna-DMC (Idndane)4,4 -DDTDieldrinEndrinHetahl or
Work Order t... : GDJ8X1AC MatriX ......... SOLID
Analysia Date..: 04/24/04Analysis Tim..: 02:12
PERCENTRECOVERY10198107106121101
RECOVERY
LIMITS(72 - 113)(71- 112)(66 - 125)(76 - 115)(73 - 124)(68 - 123)
METHOD51(84651(84651(84691(4651(4651(846
9081A~8082ASOSlA.SO81.A80811
08B1&
DecachlorobiphenylTetracbloro-mn-xylene
PERCENTRECOVERY12698
RECOVERYLIMITS(66 - 128)
(65 - 119)
07E (S):caiaii2dow ar performed More rocaUnDg to xavod udoff aosn h lcubed resuaslsold prv denomes couM par s
IABORATMY CONTROL - DATA REPORT
GC semivalatiles
Client Lot #... a D4D030176LCS Lot-Sample#: D4D050000-S52Prep Date ...... : 04/06/04Prep Batch 0...' :4096552Diluticu Factor: 1
Work Order 0...: GDJ8X1AC Matrix .... : SOLID
Analysis Date..: 04/24/04Analysiz Time..: 02:12
PARAMETERWAri
gama-BEC (T.4nan )4, 4 ' -DDTDieldrinEndrin
IHeptacbor
SPIKEAMOWNT
16.716.716.716.716.7
16.7
MEASUREDAMOUNT16.8
16.3
17.817.720.216.9
UNITSug/kguglkgugIkgugkcgug/kgug/kg
PERCENT
RECOVERY10198107106121101
METHOD8W846 808ka8W846 8081281846 8081AS8146 8081A81846 808125846 8081A
SURROGATEDecachlorobiphenyl
Tetrachloro-m-xylene
PERCENTRECOVERY12698
RECOVERY
(66 - 128)
(65 - 119)
NOTE(S) :hdk =ons we pernwed befote frdh 10 aoid =nd-off h .b ah renft.
Bod pt denoes a8mw pzirma
HATI m SAMPL EVAXADMON RE'ORT
GC Semivolatiles
Client Lot 0...: D4D030176NS Lot-SamPle #: D4D010150-002Date Sampled ... : 03/29/04 08:04Prep Date ...... : 04/06/04
Prep Batch C..: 4096552Dilution Factor: 1
Work Order 0...:
Date Received..:analysis Date..:Analysis Time..:
GET271AD-HSGET271AE-MSD03/30/0404/24/0403:09
KatriX .... : SOLID
PARAMETERAldrin
gama-BUC (Lindane)
4,4'-DDT
Dieldrin
Endrin
Eleptachior
PERCENTRECOVERYNCDILNC,DILNC,DILNC,DILHC,DILNC,DILNC,DILNC,DILnc,nxr
JC, DNC,DImNCDIL
RECOVERYLIMITS156 - 117)
(56 - 117)
(55 - 122)
(55 - 122)(47 - 132)
(47 - 132)
(57 - 117)(57 - 117)
(56 - 130)
(56 - 130)(41 - 134)
(41 - 134)
RPDRPDLIMITS METHOD
S6846 1(0-30) 61146 1
8W846 I(0-30) 8N146 1
81846 1(0-30) 81846 I
S6846 I(0-30) 8N846 1
51846 I(0-30) 6R846 I
81146 1(0-30) 61846 1
8081A8081A0 8IA
3081A3081A3081A8081A3082k3081A3081A3081A3081A
SURROGATEDecachlorobiphenyl
Tetrachloro-m-xylene
PERCENTRECOVERYNC,DIL
NCDILNC,DILSC,DIL
RECOVERYLIMITS(41 - 142)(41 - 142)(50 - 127)
(50 - 127)
NOTEs) :C& u a-e pefmed btefort ounding W aiod mound-offerwrs i aa ned mblc
BoUl pft denoes corol paraemmNC De cay nd/or RPD ah. mm acuW.DIL The kwnaW= b adiued or Wot repoeW due to diklon or bc preseof ofberfing xrmyos
GC semivolatiles
Client Lot # ... s D4D030176MS Lot-Sawple #: D4D010150-002Date Saqpled ... : 03/29/04 08s04Prep Date ...... : 04/06/04Prep Batch 1 ... : 4096552Dilution Factor: 1
Work Order # ... :
Date Received..:Analysis Date..sAnalysis Time..
GET271AD-MSGET271AE-MSD03/30/0404/24/0403:09
Matrix......... : SOLID
PARAMETERAldrin
gamma-BBC (Lindane)
4,4 ' -DT
Dieldrin
Eadrin
SAMPLE SPIKE MEASRDAMOUNT AMT AMOUNT
MDMDND1DNDRD
NDJlDRD
ND
t1NITS
ug/kguglkg
ug/kgng/kgw9/k9ug/kguglkgug/kugfkguglkgug/kg
PERCNTRECVRYNC,DnLNC,DILNC,DILNC,DILNCDILNC,DILXC,DILNC,DMNC,DILXC, DELNCDILNC,DIL
RPD METHODS8846 8081k81146 0081A81846 8081A81846 8081A5816 083LA
M846 8081O81846 80lA
6W846 808LaS1846 8081k8W846 8081L81846 B081hSH846 8081A
SURROGATEDecachlorobiphenyl
Tetrachloro-m-xylene
PERCOEfTRECOVERYNC,DILNC,DILNCDILNC,DIL
RECOVERYLIMITS(41 - 142)(41 - 142)(50 - 127)(50 - 127)
NOTE (S):
Bol pdt deote swcor pmers
NC lie enray aydeor RPD were e cakulntc
DIL The ceauzd= hadmaed or = rqwnad due w dlldo atr pere o f efd ng valyt
METHOD IRTUK REPORT
GC Semivolatiles
Client Lot C...: D4D030176
HB Lot-Sample #: D4D040000-125
Analysis Date..: .04/12/04
Dilution Factor: 1
PARAMETERAziDphos-methylBolstarChlorpyrifosCoumaphosDemeton (total)DiazinonDichlorvosDimethoate
DisulfotonEthopropEthyl parathionFamphurFensulfothionFenthionMalathionMerphosMethyl parathion
14evinphosNaled00, 0-Triethylphosphoro-
thioatePhorateRonnelSulfoteppThionazinTokuthionTrichloronateEPNDemeton-ODemeton-STetrachlorvinphos (Stirop
Work Order #...: GDHT41kA
Prep Date ...... : 04/04/04Prep Batch ... : 4095125
Matrix .... : SOLID
Analysis Time..: 07:01
RESULTNDNDNDIDNDNDNDNDND
NDNDNDNDNDNDNDNDNDNDND
REPORTINGLDMIT1313131313131313
131313131313131313133313
UNITS
ug/kgug/kgug/kgug/kguglkgug/kgug/kgug/kgug/kgug/kgug/kg,ug/kgug/kgug/kgug/kgug/kg.ug/kgug/kgug/kgug/kg
ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
METHODSW846 I8W846 I
8W846 ISW846 I
8W846 ISW846 ISW846 I
8W846 1
SW846 1
8W846 ISW846 I
8W846 18W846 1SW846 1
8W846 18W846 1SW846 I
SW846 i8W846 1
8W846 9
SW846 15846 I
8W846 18W846 1
8W846 18W846 I
8W846 E
8W846 ISW846 I
SW846 8
B141AB141h8141A8141A8141A3141k3141A314LA
3141A8141A3141A8141A8141A8141A8141A8141A8141A8141A1141A1141A
1141h1141A1141A1141k1141A8141A8141A8141AB141A141A
NDND
ND
ND
ND
ND
ND
ND
ND
ND
13671313131313131313
SURROGATEEthyl Pirimifoschlormefos
PERCENrRECOVERY7076
RECOVERYLIMITS(11 - 137)(37 - 124)
NM re(s)Cdcaahwoo ame pero=We beore rowdlg o avoid rood-off mrom In clulatda Ecufta.
1ABORATORY CORJROL SAMPLE EVALUATION REPORT
GC semivolatiles
Client Lot C..: D4D030176
LCS Lot-Sauple#: D4D040000-125Prep Date ........ 04/04/04Prep Batch #...: 4095125Dilution Factor: I
Work Order C...: GDHT41AC-LCS Matrix ..... : SOLIDGDHT41AD-LCSD
Analysis Date-.: 04/12/04Analysis Time..: 07:35
PARAMETERDemta (total)
Diazinan
Etbyl parathion
Halathion
Methyl parathion
Pborate
PERCENTRECOVERY
116 a32 p175 a180 a138 a166 a168 a165 a151 a171 a160 a135 a
RECOVERYLIMITS
(27 - 104)(27 - 104)(60 - 13S)(60 - 135)(74 - 127)(74 - 127)(64 - 138)(64 - 138)(72 - 108)(72 - 108)(58 - 106)(58 - 106)
RPDRPD LIMITS METHOD
51846113 (0-40) C8146
5118463.0 (0-40) 81846
C814619 (0-40) CR846
681461.5 (0-40) 81846
8184612 (0-40) R8846
R884617 (0-401 C8846
8141A8141A814118141A8142A8141A8141A8141k8141k8141A8141k8141k
SURROGATE
Ethyl Pirimifos
Chlormefos
PERCENTRECOVERY
88763E4
RECOVERYLIMITS(36 - 118)(36 - 118)(59 - 112)(59 - 112)
NOTE(S) sCdlaldo are perfolud before moift ao d rund-offerroIn cd ulated resufr .
3ld ;dnf denoe Gooftot punmers
p RlWve pere dIfferarce GRPD) k emswde nated cntl Wm
t Spiked uyce scoovery h eutaide awed cowtol limits.
LABORATORY aCITTOL SMLE DATA REPORT
GC Siivlti
Client Lot f...:WCS Lot-Sanplet:Prep Date ...... sPrep Batch I... :Dilution Factor:
D4D030176D4D040000-125
04/04/0440951251
Work Order Y... : GDHT41AC-LCS Matrix ......... 2: SOLIDGDHT41AD-LCSD
AnalySiS Date..: 04/12/04knalyuis Time..: 07:35
SPIKE =EAZUREDPARAMETERDemeton (total)
Diazzmen
Ethyl parathion
Malathion
Methyl parathion
Ehorate
AM6666.766.766.766.766.766.766.766.766.766.766.766.7
AMOUNT77.2 a21.6 p116 a120 a91.9 a111 a112 a110 a101 a114 a106 a90.1 a
UNITS
Wlkgug/kgugkgUI/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg
PERCENTRECOVERY11632175180138166168165151171160135
RPD METHOD81846 8141A
113 21846 8141A2W846 8141A
3.0 61846 8141A61146 8141A
19 6N846 8141-A2W846 8141A
1.5 6W846 8141A6w846 8141A
12 S2846 8141AS8146 8141-A
17 81846 8141A
Ethyl Pirimifos
Chlormefos
PERCENTRECOVERY88768384
RECOVERYLIMITS(36 - 118)(36 - 118)(59 - 112)(59 - 112)
NOTE(CS) :Caitmo ae perbfod before wning lo avoid round-off ero hin alaculed 1mdis
Bold pFrmt des cocro pameter
p Relstive pee dffeco (D) E oumside aaed cootrol ihmis.
a Spiked aIMly cimoveij k outside azwed enabunlimi
MRTRZ SPTIKESMPLE EVALU&TION REPORT
GC Semivolatiles
Client Lot C...: DtKS Lot-Sample 6: DDate Sampled...: Os'Prep Date ...... s04Prep Batch 6...: 4sDilution Factor: 1
1D0301761C230295-008
Work Order C..:
1/22/041/04/04O95125
09:45 Date Received..:Analysis Date..:Analysis Time..s
GCQ2E1DC-MSGCQ2ElDD-HSD03/23/0404/12/0409:47
Matrix .... . s OLID
PARAMETER
Demeton (total)
Dniznion
Ethyl parathion
Malathion
Methyl parathion
Phorate
PERCENTRECOVERY227 a207 a228 a214 a170170184 a186 a177 a179 a201 a193 a
RECOVERYLIMTS(33 - 131)(33 - 131)(20 - 168)(20 - 168)(20 - 175)(20 - 175)(42 - 148)(42 - 148)(35 - 129)(35 - 129)(20 - 145)(20 - 145)
RPDRPD LIMITS HETHOD
81(469.3 (0-40) 81(846
S18466.4 (0-40) 61846
8W8460.26 (0-40) 61846
91(461.3 (0-40) 51846
9W8461.0 (0-40) 6W(846
818464.0 (0-40) S;8146
8142A8141A8141A8141A8141A8141A8141A8141A8141k8141h8141A8141A
SURROGATEEthyl Pirimifos
Chlormefos
PERCENTRECOVERY8078106100
RECOVERYLIMITS(11 - 137)(1t - 137)(37 - 124)(37 - 124)
NOTE(S)):Caladam amc pomed befrouendig so awd wund-off a in eakulatd ets.ld prA dees coned panmems
a SpIked anyed ecv= keulut aced ceaml limbs.
Re hs an qoti i hasve bee u W or dry we
ATRIX 8P SAMPLE DA.A REPORT
GC Semivolatiles
Client Lot I ... :MS [ct-Sample #sDate Saxpled...:Prep Date ...... :Prep Batch U ... :Dilutioa Factor:
D4D030176D4C230295-00803/22/04 09:4504/04/0440951251
Work Order #...:
Date Received..:Analysis Date..:Analysis Time..:
GCQ2E1DC-MSGCQ2E1DD-MSD03/23/0404/12/0409:47
Matrix .... : SOLID
PARAMETERDeMeton (total)
Diaziflon
Ethyl parathio
Halathion
Hethyl parathio
Phorate
SAMPLEAMOUNTEDIDND
DD
NDNDEDND
llDN9DED
SPIKEAMT93.093.093.093.093.093.093.093.093.093.093.093.0
MEASRDAMOUNT UNITS
211 ug/kg192 ug/kg212 ug/kt199 ug/kg158 ug/kg158 ug/kg171 Ug/kg173 ug/kg164 ug/kg166 ug/kg187 ug/kg180 ug/kg
PERCUTRECURY RPD METHOD227 a 51846 8141A207 a 9.3 81846 8141A228 a SW846 8141A214 a 6.4 51846 81412170 S5846 8142k170 0.26 5S146 8141A184 a SR846 8l41A186 a 1.3 51146 81412177 a 5N846 8141A179 a 1.0 5846 8141a201 a Sn846 8141A193 a 4.0 511846 8141A
SURROGATEEthyl Pirimifos
Chlormefos
PERCENTRECOVERY8078106100
RECOVERYLIMITS(11 - 137)(11 - 137)(37 - 124)(37 - 124)
NOT(Ss):Cd cuim ave peformed before mut w mid round-4ff hi cacuted r!wBold primdenoe co=o parmee
a Spiked yte emovay k de = Ued contol Wmhs.Resks cmd odg i ends hr bftn aduised dry we!&.
MTED SLIM REPRT
GC Semivolatiles
Client Lot I...: D4D030176HB Lot-Sample f. D4D070000-553
Analysis Date..: 04/13/04
Dilution Factor: 1
Work Order ... :DQR1AA
Prep Date ...... : 04/08/04Prep Batch U ... : 4098553
Matrix .... D : SOLI
Analysis TiMe..t 17:39
PARAMETER2,4-D2,4-DB2,4,5-T2,4,5-TP (Silvex)DalaponDicambaDichlorprop
DinosebMCPAMKPP
RESULTEDNDNDNDNDNDND
NDNDND
REPORTINGLIMIT80
2020204040801280008000
UNITS
ug/kgug/kgug/kgVg/kg
ug/kgug/kgug/kgug/kgug/kgug/kg
METHODS8146 8151A8W846 8151A
SW846 8151A8W846 8151A
81846 815LASW846 8151A8W846 8151ASN846 8151ASW846 8151ASW846 8151A
SURROGATEDCAA
PERCENTRECOVERY
96
RECOVERYTL TS
(39 - 96)
NOTE (S):
Cakuafig- am Paned bfore MiUing I uoid rou-Off C= in Chk ta rMU.
IUBORAT= CcETROL SMPWL EVLUMICN REPORT
GC Semivolatiles
Client Lot ... : D4D030176WS Lot-Sanpleft D4D070000-553Prep Date ...... : 04/08/04Prep Batch 1...: 4098553Dilution Factor: 1
Work Order #... : GDQMRLAC-LCS Matrix......... : SOLIDGDQNRIAD-LCSD
Analysis Date..: 04/13/04Analysis Time..: 18:20
PARAMETER2,4-D
2,4,5-T
2,4,5-TP (Silvez)
PERCENTRECOVERY93 a89111108112110
RECOVERYLIMITS
(26 - 92)(26 - 92)(26 - 115)(26 - 115)(31 - 114)(31 - 114)
RPDRPD LIMITS METHOD
5N846 M152A5.1 (0-40) SH846 8151A
SW846 8151A2.6 (0-40) 5W846 8151A
SW846 8151A2.1 (0-40) BW846 8151A
SURROGATEDCAA
PERCENTRECOVERY102 *
95
RECOVERYLIMITS(39 - 96)(39 - 96)
OTE (S):Omdadons are pertmed before gmdhg to void rowd-ofrfavrs in cabAmed maUL
BNO pft dene p== Imtm
a Spikd oye mvay bmide d sonirolmi
* Surwgpe recoveay iontfde aed ano vmhL
aCOROL SAMPLE DA REPORT
GC Semivolatiles
Client LOt #.. .: D4D030176
LCS Lot-Samle$: D4D070000-553Prep Date ...... z 04/08/04Prep Batch 1... : 4098553Dilution Factor: 1
Work Order #...s GDQNRAC-LCS Matrix .... : SOLID
GDQNR1AD-LCSDAnalysis Date..: 04/13/04Analysis Time..: 16:20
SPIKE MEASMUR PERCENTPARAMETER2,4-D
2,4,5-T
2,'I5-TP (Silvex)
AMo=64.064 .16. 016.016.016.0
AMOUNT59.8 a56.817.717.318.017.6
MITS RECOVERY
Ug/g 93ug/kg 89ug/kg 111
g/kg 108ug/kg 112ug/kg 110
RPD METWODS8846 8151k
5.1 51846 8151A81846 8151A
2.6 91(846 8151A61(846 8151k
2.1 SR846 8151k
SURROSATEDCAA
PERCENTRECOVERY102 *95
RECOVERYLIMITS(39 - 96)(39 - 96)
NOTE (S) :azuais wre pufamd bfort toung D avoid mmd offem In icatmiat re
Bd prm dems contro l pam
a S4&d msIyte evey I oude sae mo imit.
* Suwmgae ery k ouie atwd Wvtt lins
3: BP= MPW EVMALU=TI REPORT
GC Semivolatiles
Client Lot E...: D4D030176NS Lot-Sample t: D4D070249-001Date SaMpled ... : 04/05/04Prep Date ...... : 04/08/04Prep Batch 0 ... : 4098553Dilution Factor: -I
Work Order #...:
Date Received..sAnalysis Date..:Analysis Time. .:
GDPJ4LhJ-MSGDPJ41hX-MSD04/07/0404/14/0402:38
matrix ... .: SOLID
2,4-D
2,4,5-T
2,4,5-TP (Silver)
PERCENTRECOVERY103 a81121 a103120 a101
RECOVERYIMIS(26 - 92)(26 - 92)
(26 - 115)(26 - 115)(31 - 114)(31 - 114)
RPDRPD LIMITS _ METHOD
8K84623 (0-40) EW846
884616 (0-40) 81(846
8W84617 (0-40) 8846
815LASISlA8LMIA8152A8151A8152A
SURROGATEDCRA
PERCENTRECOVERY103 *88
RECOVERYLIMTS(39 - 96)(39 - 96)
NOTE(8):Cdca ire am pefxed efore ,imdi to m smd-off aors IamW ed ruft
aom pd 4e ames con pummm
a Sp&ed mnslym memM k oteide Ktd corl lmft.
Lurropte movay Iks ou e mat contol Slts
MATRIX S SANPLE DN REPORT
GC Semivolatiles
Client Lot # ... I D4D030176 Work Order C...:NS lot-Sample #: D4D070249-001Date Sampled ... : 04/05/04 . Date Received..:Prep Date ...... : 04/08/04 tAnalysis Date..:Prep Batch # ... : 4098553 Analysis Time..Dilution Factor: 1
GDPJ41AJ-MSGDPJ41AK-4SD04/07/0404/14/0402:38
Matrix......... : SOLID.
2,4-D
2,4,5-T
2,4, 5-TP (Silvex)
SAMPLE SPIKEAMOUNT ANTED 64.0RD 64.0MD 16.0MD 16.0MD 16.0WD 16.0
MEASRDAMOT65.652.119.416.519.216.2
UNITSug9/kug/kgug/kgug/kgugl/guglkg
PERCNTRECVRY103 a81121 a103120 a101
RPD METHODSnB46 1
23 8W846 I8WB46 1
16 5846 I5W846 1
17 0S846 I
MLIABISIA815IAB15LABiSIA8151A
SURROGATEDCAA
PERCENTRECOVERY103 *
se
RECOVERYLIMITS(39 - 96)(39 - 96)
BME(S):Chwuhfio we perfomed before oundl lo avoid mnd-offom h calmlated emsults.ld prim dauen trol prametrs
a Spiked NWe recovezy is outside oaed r ntrol I Wm* Surroe rcovay I Suidted conro EM
=MTD BLANK REPORr
TOTAL metals
Client Lot # ... : D4D030176 H atri r .S....... s SOLID
REPORTINGLIMIT
PREPARATION- WORKMETHOD ANALYSIS DATE ORDER IPAIZMrDTER PRASTTU UNIqiS
HB Lot-SampleMercury
#: D4DOS0000-254 Prep Batch 0...:ND 33 ug/kg
Dilutio Factor: 1Analysus Time. . 11:44
4096254SW846 7471A 04/13-04/14/04 GDH7J1AP
BB Lot-SanpleArsenic
4: D4D060000-647 Prep Batch ...: 4097647ND 1.0 mg/kg SW846 6010B
Dilution Factor: 1Analysis Time..s 01:24
04/09-04/17/04 GDM8G1AC
Lead ND 0.80 mg/kgDilution Factor: 1Analysis Time..: 01:24
6W846 6010B
EW846 6010B
04/09-04/17/04 GDMSG180
04/09-04/17/04 GDM8G1ANSelenium 1.3DilutionAnalysis
mg/kgFactor: 1Tize. .s 01s24
Barium ND 1.0DilutionAnalysis
Mg/kgractort 1Time..: 01:24
SW846 6010B 04/09-04/17/04 GDMsQlAD
Cadmium
Chromium
Silver
ED 0.50 mg/kgDilution Factors 1Aalyssl Time..2 01:24
1.0 mg/kgDilution Factor: 1Analysis Time.. 01s24
1.0 mg/kgDilution Factor: 1Analysis Time..s 01:24
SW846 6010B
SW846 6010B
SW846 6010B
04/09-04/17/04 GDM$GLAF
04/09-04/17/04 GDM8G1AG
04/09-04/17/04 GDM3GlAPND
NOS(S) :Caeuadows ae perforted before rodng t0 avod rond-off em In calhm msus.
LASORATORY CONTROL SMPLE EVALMWIO RE ORT
TOTAL Metals
Client Lot 6-..: D4D030176
PERCENT RECOVERYPARAMETER RECOVERY LIMITS METHOD
WS Lot-Samplef: D4D050000-254 Prep Batch #...: 4096254Mercury 90 (82 - 113) SW846 7471A
Dilution Factor: 1 Analysis
LCS Lot-Sanple#: D4DO60000-647 Prep Batch #...t 4097647Arsenic 89 (80 - 111) SW846 6010B
Dilution Factors I Analysis
Lead 91 (80 - 116) SW846 6010BDilution Factors I Analysis
Selenium 88 (80 - 112) SW846 6010BDilution Factors 1. Analysis
Barium 97 (80 - 117) SW846 6010BDilution Factors 1 Analysis
Cadmium 88 (80 - 119) SW846 6010BDilution Factor: 1 Analysis
Chromium 94 (80 - 120) 8W846 6010BDilution Factor: 1 Analysis
Silver 93 (80 - 109) SW846 6010BDilustion Factor: 1 Analysis
NOTE(S) IlcaUos am padmed bcore rounding l *void vound-off ans In cadIand asulm
Matrix . .3: SOLID
PREPARATION-ANALYSIS DATE WORK ORDER #
04/13-04/14/04 GDH7J1AC
Time..: 11s46
04/09-04/17/04 GDHSO1AVTime..s 01229
04/09-04/17/04 GDM8G1A4Time..: 01s29
04/09-04/17/04 GDM8GLA7Time.. s 01s29
04/09-04/17/04 GDM8GlAWTime. . 01m29
04/09-04/17/04 GDMSGlAOTise..: 01:29
04/09-04/17/04 GDMSGlAlTime.. 3 01:29
04/09-04/17/04 GDMtGlABTime.. a Gls29
LABORATORY OaOaT , SLIE DATh REPORT
TOTAL metals
Client Lot C....: D4D030176 Hatris .... D.... : SOLID
SPIKE MEASURED PERCNT PRBPARATION- WORKPARAMETER AMOUNT AMOUNT UNITS RECVRY METHOD ANALYSIS DATE ORDER #
LCS Lot-Saxzplef: D4DO50000-254 Prep Batch 4...: 4096254Mercury 833 750 ug/kg 90 SW846 7471A 04/13-04/14/04 GDH7J1AC
Dilution Factor: 1 Analysis Time. . s 1s46
LCS Lot-Sample#: D4D060000-647 Prep Batch C..: 4097647Arsenic 200 177 mglkg 89 8W846 6010B 04/09-04/17/04 GDM8G1AV
Dilution Factors 1 Analysls Time..: 01s29
Lead 50.0 45.6 mg/kg 91 BW846 6010B 04/09-04/17/04 GDM8GlA4Dilution Factor: 1 Analysis TLe...s 01:29
Selenium 200 177 mg/kg 88 SW846 6010B 04/09-04/17/04 GDM8G1A7
Dilution Factor: I Analysis Time..: 0M29
Barium 200 193 mg/kg 97 EW846 6010B 04/09-04/17/04 GDM8G1AWDilution Factor: 1 Analysis Time..: 01:29
Cadmium 5.00 4.40 mg/kg 88 £W846 6010B 04/09-04/17/04 GDM8G1A0
Dilution Factor: 1 Analysis Time : 01:29
Chromium 20.0 19.7 mg/kg 94 6W846 6010B 04/09-04/17/04 GDM8G1A1Dilution Factors 1 Analysis Time..S 01:29
Silver 5.00 4.65 mg/kg 93 8846 6010B 04/09-04/17/04 GDM8G1ASDilution Factors 1 Analysis Tine. s 01:29
Cah0A;1ns at purkmed betor :ouing to 1od lwudoffawn b culamd remkl
KA7TR BP SAMPLE EVMDhUlION REPORT
TOTAL metals
Client Lot #...z D4D030176Date Sampled...: 03/29/04
Matrix ..... : SOLIDDate Received..: 03/30/04
PERCENT RECOVERY RPD
PARAMETER RECOVERY LIMITS RPD LIMITS METHODPREPARATION- WORKANALYSIS DATE ORDER #
US Lot-Sample #:Mercury 104
93
D4C300294-001 Prep Batch #...: 4096254(82 - 113) SW846 7471A
(82 - 113) 10 (0-20) SW846 7471ADilution Factort 1.Analyuis Tim. .i lSO*0
04/13-04/14/04 GC7TP1CE04/13-04/14/04 GC7TP1CF
NMO(S):cao am prfofmeld berore mmdlgs loD r found-offmon in ccW zesusb
Resits and apoxdn Imhs bs been aeumd for dry weg&.
MQdTRIX SPIKE SAMPLE DA32L REPORT
TOTAL Metals
Client Lot #... : D4D030176Date Sampled...: 03/29/04
HatriX .. O...... : SOLIDDate Received..: 03/30/04
SAMPLE SPIKE MEASRD PERCHTPARPAMETER AMOUNT AMT AMOUNT UNITS RECVRY RPD METHOD
PREPARATIORq-ANALYSIS DMTR
WORKORDER #
4S Lot-Sanple #: D4C300294-001 Prep Batch C...: 4096254Mercury
44 96644 966
1050 ug/kg 104945 ug/kg 93
Dilution Factors 1Analysis Time.- llt50
8W846 7471A10 5W846 7471A
04/13-04/14/04 GC7TP1CE04/13-04/14/04 GC7TP1CF
NOTE S) sCdadatms am parfowat before bauad tI &vol mid-cIT uors In Caad rwkLcs.
Reisuht wxd rwqg labw have ben bd r dI y wdgbL
M19TRIX SPI SAPLE EVULUWIM RE 'T
TOTL Metals
Client Lot t...: D4D030176Date Sampled...: 04/01/04 09:45 Date Received..: 04/02/04
PERCENT RECOVERY RPDPARAM4ETER RECOVERY LIMITS RPD LIMITS METHOD
HatriX ..... : SOLID
PREPARATION-ANALYSIS DATE
WORKORDER #
FS lot-Sample #: D4D020177-001 Prep Batch 1...: 4097647
Arsenic 44 N76 *
Lead 44 N79 *
Selenium
Barium
Cadmium
46 N77 *
52112 *
4072 *
(76 - 111) 6W846 6010B(76 - 111) 52 (0-30) 8W846 60103
Dilution Factor: 1uaalyzis Time..-: 0142
(70 - 200) SW846 6010B(70 - 200) 54 (0-40) SW846 6010B
Dilution factor: 1Analysis Tie..: 01:42
(76 - 104) 5W846 6010B(76 - 104) 51 (0-30) SW846 6010B
Dilution Factor: 1
Analysis Time..: 01:42
(52 - 159) 8W846 6010B(52 - 159) 53 (0-30) 8W846 6010B
Dilution Factor: 1Analysiu Time..s 01:42
(40 - 130) EW846 6010B(40 - 130) 56 (0-30) SW846 6010B
Dilution Factor: 1Analysis Time..: 01:42
(70 - 200) 5W846 6010B(70 - 200) 8.6 (0-40) SW846 6010B
Dilution Factor: 1
Asalydsi Time..s O:sU
04/09-04/17/04 GDE201A3
04/09-04/17/04 GDE201A4
04/09-04/17/04 GDE201CJ
04/09-04/17/04 GDE201CK
04/09-04/17/04 GDE201CO
04/09-04/17/04 GDB201CR
04/09-04/17/04 GDB201AS04/09-04/17/04 GDE201A6
04/09-04/17/04 GDE2O1A904/09-04/17/04 GDE201CA
04/09-04/17/04 GDE201CC04/09-04/17/04 GDE201CD
Cbromium 136119
silver 45 N79 *
(75(75
- 141)
- 141) 51 (0-30)Dilution Factor: 1
Analysis Time..s :1:42
S1846 601GB8W846 6010B
04/09-04/17/04 GDE201CTP4/09-04/17/04 GDE201CU
OTE8(s):Caiahdo at paftmed befot =oimdk So aoi wmd-offcomn In c tdaed smu.N Spikd acyfe ioery k oude aculed 1am EmRb -d repordg Hmmt be beenl a e for dry wdL
* Rd-ve peceat diffnce (M1D) Is oi cud co im
HLTRIX SPUR SAMPLE DATA REP(RT
TOTAL Metals
Client Lot t...:Date Slampled'.'.:.2
D4D03017604/01/04 09:45 Date Received..: 04/02/04
Matrix ..... ,.2 SOLID
SAMPLE SPIKE HEASRD PERCNTPARAMETER AMOUNT AMT AMOUNT UNITS RECVRY RPD METHOD
PREPARATION- WORKAULLYSIS DATE ORDER #
MS Lot-SampleArsenic
t: D4D020177-001 Prep Batch C...: 4097647
1.7 2071.7 207
92.6 N Mg/kg 44158 * Mg/kg 76
Dilution Factor: 1Azalysiu Tie. .: 01:42
S1W846 6010B52 SW846 6010B
04/09-04/17/04 GDE201A304/09-04/17/04 GDE2O1A4
Lead2.12.1
51.7 25.0 N mg/kg51.7 43.2 * mg/kg
Dilution Factor: 1
4479
SW846 6010B54 SW846 6010B
04/09-04/17/04 GDE201CJ04/09-04/17/04 GDE201CK
Analysis Time..s 01:42
SeleniumRD 207ND 207
94.9 N Mg/kg160 * Mg/kg
Dilution Factort 1
4677
SW846 6010B51 SW846 6010B
04/09-04/17/04 GDE2O1oQ04/09-04/17/04 GDE201CR
Analynis Time..1 01342
Barium67 20767 207
173 mg/kg 52298 * mg/kg 112
Dilution Factor: 1
Analysis Time..: 01:42
8W846 6010B53 SW846 6010B
04/09-04/17/04 GDE201A504/09-04/17/04 (WE201A6
Cadmium
ND 5.17 2.09 mg/kgND 5.17 3.73 * mg/kg
Dilution Factor: 1.
4072
8w846 6010B56 SW846 6010B
04/09-04/17/04 GDE201A904/09-04/17/04 GDE201CZ
Analysis Time..: 01:42
chromium
Silver
13 20.7 40.8 mg/kg 13613 20.7 37.5 mg/kg 119
Dilution Factors 1Analysis Time..S 01i42
SW846 6010B8.6 8W846 6010B
8W846 6010B51 SW846 6010B
04/09-04/17/04 GDE201CC04/09-04/17/04 GDE201CD
04/09-04/17/04 GDE201CT04/09-04/17/04 GDE201CU
0.18 5.17 2.53 N mg/kg0.18 5.17 4.24 * Mg/kg
Dilution Factors I
4579
Analysis Time..: 01:42
(Continued on next page)
1 SPIKE SAMPLE Do REPORT
TOTAL Msetals
Client Lot t... : D4D030176Date Sampled...: 04/01/04 09:45 Date Received..: 04/02/04
Matrix......... SOLID
NOB (S) :Cadatim art pformed beoe rodiaI lo amid Timuoffsenm In Alcuned n k.
N Spiked ayte Scowy k outse d cowoAll EAits.Resu and epordag Et he bma rend for dry wAti.
* kebaw parw diffau= IR) I oumd iwezd cowuL imis.
BA A So REPOR
General cht try
Client Lot f...: D4D030176 Matrix.........: SOLnM
PARAMETER
Fluoride.
REPORTING PREPARATION- PREP
RESULT LIAIT UNITS METHOD ANALYSIS DATE BATCH #Work Order #: GECK61MA MB Lot-Sample #: D4D160000-487
ED 10 mg/kg SW846 9056 04/15/04 4107487Dilutiml Factors 1Analysis TLme. . s 15:42
IO=E(S):Cakuladous eperfd before ouiog o ovoi toed-off erws b caadawdwekt
IJOaTaOr CONTOL SAIE EVALUAI REPORT
General Malitry
Lot-Sample I...: D4D030176 Matrix.........: SOLID
PARAMETERFluoride
PERCENT RECOVERY RPD PREPARATION- PREPRECOVERY LIMITS RPD LIMITS METhOD AIMLYSIS DATE BATCE #
WO#:GECM61AC-LCS/GECK61AD-LCSD LCS Lot-Sample#: D4D160000-48798 (90 - 110) 5W846 9056 04/15/04 4107487100 (90 - 110) 1.9 (0-10) SW846 9056 04/15/04 4107487
Diltutl Factors 1 Analysis Jime..t 15:20
NOTE (S):uCkkdudarPafrmgefbr tounag u avoid wrawudsoffan kcalcuIated rut.
LBEnRAT= WRWL SAMPLE DL REPORT
General Chemistry
Lot-Sample if...: D4D030176 Matrix......... SOLID
PARAMETERFluoride
SPIKE MEASURED PERCNTAMOUNT AMOUNT UNITS RECVRY RPD METHOD
WO#:GECM61AC-LCS/GECM61=D-LCSD40.0 39.3 mg/kg 98 SW846 !40.0 40.0 mg/kg 100 1.9 SW846 !
Dilution Factors I Analysis I
LCS?0569056
PREPARATION- PREPANALYSIS DATE BATCH #
Lot-Sample#: D4D160000-48704/15/04 4107i8704/15/04 4107487
rize..% 15X20
NOT ES):CaIcU ns we petfrmed befare rounding o avoid Iund-of a. In =haih rena.
MhTRIX SPIKE SAMPLE EVJXCLK1IN REPORT
General Cintry
Client Lot #...: D4D030176Date Sampled...: 04/01/04 12:30 Date Received..: 04/03/04
MatriX .... : SOLID
PARAMETERFluoride
PERCENT RECOVERY RPDRECOVERY LIMITS RPD LIMITS METHOD
WO#: GDHQL1AV-MS/GDHQL1AW-MSD94 (80 - 120) SW846 905694 (90 - 120) 0.48 (0-10) SW846 9056
Dilution Factor: 1Analysis Time..: 16X05
PREPARATION- PREPANALYSIS DATE BATCH #
MS Lot-Sample #s D4D030176-0o104/15/04 410748704/15/04 4107487
DO (S):Ca3toIs are pefoted before wudingso avoid owtd-off wos k cakuated mweks.
Rem ad epoialimbharebeeadustcdfrdzyweight
MAT=R SPK SATEW DM REPORT
eneral cbzMatry
Client Lot t...: D4D030176 SOLMatri.SIDDate Sampled ... : 04/01/04 12:30 Date Received..: 04/03/04
SAMPLE SPIKE MEASRD PERCNT PREPARATION- PREPPARAMETER AMOUNT AMT AMOUNT UNITS RECVRY RPD HMEHOD ANALYSIS DATE BATCH #Fluoride WO#: GDHQL1AV-KS/GDHQL1AW-MSD MS Lot-Sample #: D4D030176-001
ND 50.8 48.4 mg/kg 94 6W846 9056 04/15/04 4107487ND 50.8 48.6 mg/kg 94 0.48 SW846 9056 04/15/04 4107487
Dilution aCtor: IAnalysis Time..: 16s05
OTR (S):Ckbtiow arm perfbmed before rutmdhl a S id ,amd-off am in mab-ed rm*s
SAMPLE DUPLICTE EVAItIOK ZKPORT
General CeMistry
Client Lot # ... : D4D030176 Work Order @... : GD51-SMP HatriGD518-DUP
Date Sampled ... : 04/12/04 14:30 Date Received..: 04/14/04% Misture ..... : 20
DUPLICATE RPDPARAM RESULT RESULT UWITS RPD LIMIT METHODPercent Moisture SD Lot-Sample $ I
20 19 t 8.6 (0-20) MCMA 160.3 MOD
.x : SOLID
PREPARATION-ANALYSIS DATEW D140295-00104/19/04
PREPBATCH #
4110593Dilutin Facort 1 AnalyuiE TieW..3 17t3S
NO (S):Wzlaiu am pmfonwd tetbre wcumh ID avoid md-off ros hI akcad mike
Rmz ad a ouig linihs hame bcen a4uted fr dry wekhL
vFJPTE D CPLrc2M EALARi REPORT
General mistry
Client Lot #...: D4D030176 Work Order I...: GDSHQ-SMP matrix .....: SOLIDD8IHQ-DUP
Date Sampled...: 04/09/04 12:15 Date Received..: 04/15/04t Hoisture ..... : 21
DUPLICATE RPD PREPARATION- PREPPARPM RESULT RESULT UNITS RPD LIMIT METHOD 1NPLYSIS DATE BATCH #Percent Moisture SD Lot-Sample #: D4DD50302-001
21 19 t 9.9 (0-20) MCAKW 160.3 MOD 04/20/04 4111603Dilutian Factor: 1 Analysis Time..1 17:15
SAMPLE DUPLCA EVAUTX REPORr
Geoa <aiemiSt
Client lot I...: D4D030176 Work Order I...: GEFXS-MP Hatri ....... : SOLIDGEFXS-DUP
Date Sapled... : 04/14/04 13:20 Date Received..: 04/19/04t Moisture.....: 14
DUPLICATE RPD PREPARATION- PREPPARAM RESULT RESULT UNITS RPD LIMIT METHOD ANALYSIS DATE BATCH $Percent Moisture SD Lot-Sample #: D4D190181-013
14 15 t 6.5 (0-20) KCAWW 160.3 MOD 04/20/04 4111603Dilutti Factor: 1 Analysi sTe. T s 17315
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