additional monitoring wells drum burial area 1 remedial ... · mr. frank vavra 2 april 20, 1992...

Project No. 87-376 DC O Paul C Rizzo Associates. Inc.April 1992 '• ** ' vL CONSULTANTS

Transmittal

Additional Monitoring WellsDrum Burial Area 1Remedial Investigation/Feasibility Study

Hunterstown Road SiteStraban TownshipAdams County, Pennsylvania

Westinghouse Electric CorporationPittsburgh, Pennsylvania

AR307267

Paul C. Rizzo Associates, Inc.CONSULTANTS

April 20, 1992

Project No. 87-376.12

Mr. Frank VavraU. S. Environmental Protection AgencyRegion III841 Chestnut BuildingPhiladelphia, PA 19107

TRANSMTTTALADDITIONAL MONITORING WELLS

DRUM BURIAL AREA 1REMEDIAL INSTIGATION/FEASIBILITY STUDY

HUNTERSTOWN ROAD SITESTRABAN TOWNSHIP, ADAMS COUNTY, PENNSYLVANIA

Dear Mr. Vavra:

In response to U.S. Environmental Protection Agency (USEPA) comments to theRemedial Investigation Report for the Hunterstown Road Site, Westinghouse ElectricCorporation and Paul C. Rizzo Associates, Inc., designed, installed, and sampled fiveadditional monitoring wells at the Hunterstown Road Site (Figure 1). The projecteddepths and well locations were approved in your letter dated December 14, 1991 toMr. Tim Basilone.

The additional monitoring wells (HMW-15BF, HMW-20AA, HMW-20AB,HMW-21AW, and HMW-21BF) were drilled and installed from January 6, 1992through January 16, 1992. The monitoring well locations are shown on Figure 2. Acopy of the monitoring well installation details and the boring logs for each well isattached. The methods utilized in monitoring well construction were in accordancewith the USEPA approved Sampling and Analysis Plan and Quality Assurance ProjectPlan-Revision 1 (QAPP).

The five additional monitoring wells (HMW-15BF, HMW-20AA, HMW-20AB,HMW-21AW, and HMW-21BF) and nine other monitoring wells associated with DrumBurial Area 1 (HMW-9AW, HMW-9BF, HMW-15AW, HMW-16AW, HMW-16BF,HMW-17AW, HMW-17BF, HMW-20AW, and HMW-20BF) were sampled. Thesampling of the wells was performed by Paul C. Rizzo Associates personnel fromJanuary 27, 1992 through January 29, 1992. As you are aware split samples were also

300 OXFORD DRIVE, MONROEVILLE, PA 15146 PHONE (412) 856-9700 FAX

Mr. Frank Vavra 2 April 20, 1992

collected from monitoring wells HMW-20AA, HMW-20AB, HMW-21AW, and f HMW-21BF by the USEPA oversight consultant. The wells were sampled inconfer mance with the QAPP. The ground water samples collected were analyzed forvolatile organic compounds on the Target Compound List utilizing CLP protocol. Theattached Table 1 contains a summary of the analytical results from the monitoring wellsampling.

It is Westinghouse's understanding that this submittal fulfills item number 4 outlined inyour December 14, 1991 letter to Mr. Tim Basilone. Also, with this submittal,Westinghouse has provided all of the information that you requested in this letter, andthat the Hunterstown Road Site remedial investigation is considered completed andunconditionally approved. Please contact Mr. Basilone if you have any questions onthis submittal.

Respectfully submitted,

William A. BaughmanProject Supervisor

Kenneth J. BirdPrincipal - Remediation Planning

WAB/KJB/smjAttachments

cc: Mr. Timothy Basilone - WestinghouseMr. Matthew Cousino - ENSRMr. Ronald Klinikowski - PADER

113/92

BR3Q7269

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APPENDIX A

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STRABAN TOWNSHIP, ADAMS COUNTY, PENNSYLVANIA

PREPARED FOR

WESTINGHOUSE ELECTRIC CORPORAPITTSBURGH, PENNSYLVANIA

Paul C Rizzo Associates, Inc.CONSULTANTS

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APPENDIX B

AR3073I2

Since 1938WADSWORTH/ALERTLABORATORIES, INC.Sampling, testing, mobile labs

4101 Shuffel Drive N.W. / North Canton, Ohio 44720

3DG NARRATIVE

This narrative pertains to Paul Rizzo and Associates, HunterstownRoad site, project number 87-376 which was completed by^adsworth/ALERT Laboratories. This data package consists ofseventeen samples to be analyzed using' the 3/90 SOW contractlaboratory protocol. The following' is a listing of these samples:

Client ID Laboratory ID

HMW15AW 42759HMW17AW 42760TRPBL1 42761HMM5BF 42762HMW21AW 42763HMK20AA 42765HMW20AB 42766EQB-1 42767HMW21BF 42768HMW21BFD 42769HMW20BF 42770HMW16AW 42771HMW9AW 42772HMW9BF 42773HMW20AW 42774HMW16BF 42775

r3£SSx CORPORATE AND LABORATORY: North Canton, Ohio (216) 497-9396fe\ LABORATORY: Cleveland, Ohio (216) 642-9151

LABORATORY: Pittsburgh, Pennsylvania (412) 826-5477LABORATORY: Tampa, Florida (813) 621-078424-HOURALERT LINE (216)497-9338 fi R 3 Q 7 3 I 3

mlThe following is a listing of the pH value for each volatile watersample as received by the laboratory:

Sample ID EM

HMW15AW 1.0HMW17AW 1.0TRPBL1 5.0HMW15BF 1.0HMW17BF 1.0HMW21AW 1.0HMK20AA 1.0HMW20AB 1.0EQB-1 1.0HMW21BF 1.0HMW21BFD 1.0HMW16AW 1.0HMW9AW 1.0HMW9BF 1.0HMW20AW 1.0HMW16BF 1.0

Software restrictions necessitated the dropping of the "H" prefixfrom the sample numbers in the hardcopy data package.

During the volatile analysis of this SDG, the MS/MSD for sampleMW21AW had recoveries for Trichloroethene outside of QC limits. Theassociated RPDs for this sample were also outside of QC limits. Theabove may be attributed to a matrix effect.

"I certify that this data package is in compliance with the termsand conditions of the contract, both technically and forcompleteness, for other than the conditions detailed above. Releaseof the data contained in this hardcopy data package has beenauthorized by the Laboratory Manager or his designee, as verified bythe following signature."

Ron GibasCLP ManagerFebruary 24, 1992

000001 |JAR3073U

VOLATILES DATA

SR3073I5

VOLATILE QC SUMMARY DATA

""" ' WA.'ii?, VOLATILE ' StS'i c>i •. • .. , ,: . .., v,~...,Y;CD RECOVERY

Lab Name : VVADSWORTH/'ALERT Con t rac c : 6S-D i-OOS5

Lab Code:WADS Case Xo.:S"3~6 SAS Xo . : SDG Xo.:EO.B-l

i EPA1 SAMPLE XO.I

01 ! E03-L02!HMVv9A\V03 IHMWQBF041MW15AW05 1MW15BF06 IMW16AW0"!.MW16BFOS [MWl'AW09! MWl'BF10IMW20AA11 ', MW20AB12 1MW21AW13 IMW21AWMS14IMW21AWMSD15IMW21BF16IMW20AW17 1MW20BFISiTRPBLl19 i VBLK1201VBLK221 ! VBLK322IVBLK423 IW21BFJT 024!251. .„....._.._..26!27! .2S!29!30!

SMC1(TOD*

93102981021029S96

102'10210210210092961001029810010410010210096

.

SMC2(BFB)=

949490949SSS96929494949686869892909696

. 96969496

- - - - - -

SMC3(DCE )=

9084SS969SS6929S981009894SSS696SS92969694929090

- ————

OTHER

_. — „. —

TOTOUT

0000000o000000000000000

._._

OC LIMITSSMC1 (TOD = Toluene-dS (SS-liO)SMC2 (BFB) = Bromof luorobenzene (S.6-115)S.MC3 (DCE) = i.2-Dichloroethane-dl ("6-114)

= Column to be us~eil to flaa recovery values

* Valuer .nit side of contrac: required OC l i m i t s

D System M o n i t o r i n g Compound d i l u t e d out

pag- i oxFOR'.f I I VOA- 1

Pi

SR3073I7

\V'. . 4. '•• \ •'• ••.. - " • r, •• MA v-tvri'i,S.piiK'FTMATk\ A S i'; i' KE* ':b'X:4VL 'I '• 'ATlr P"£i :V /

Lab Name : WADSWoRTH/ALERT • Con t"rac t : 6S-D i-0035

Lab Code: WADS Case N'o.:S~3~6 SAS Xo . : 5DG Xo

la t r i x So i k t- - E PA Sample Xo . : MW 2 i AW

COMPOUXD

1 . 1 -D i ch loroe t heneTrichloroetheneBenzeneTo I ueneChiorobenzene

i

SPIKEADDED(ug/L)

~ i ."1 .~ 1 ." 1 .71.

SAMPLECOXCEXTRATIOX

( ug/L )

39 .130.0.0.0.

MSCOXCEXTRATIOX

( ug/L i

S3.160.58.^ s ~

MS

REC =

624 ~> *s:- -so

oc.LIMITSREC.

6 1 - n 5"1-120-6-12""6-125"5-130

COMPOUXD_ _ _ _ _ „ _ _ _ _ _ _ _ _ _ _ _ _ _ _ - , _ _ _

~1 . 1-DichloroetheneTrichloroetheneBenzeneTo 1 ueneChiorobenzene

SPIKEADDED(ug/L)

"1 .-1."1 .7 i .71 .

...

MSDCONCENTRATION

(ug/L)

100.1"0.6S.65.68.

MSDor'0

REC *

3656*969296

%RPD ±

32*29*16*1"*IS*

QC LRPD

i ii —I 41 11313

:MITSREC.

61-145"1-120"6-12""6-125"5-130

= Column to be used to fiaa recovery and RPD values with an asterisk

* Values outside of OC " l i m i t s

>.PD : 5 o u tor 5 o u t s i d e 1 i m i t s.pike R-JC ,'ive ry: 2 out of 10 o u t r i d e l i m i t - a

COMMENTS: - . . . . - GCC20J

flR3073i8

•vCLA'i ILE' METHOD BLAXK.'-,/'

VBLK1Lab Name:WADSWORTH/ALERT Contract:6S-D1-OOS5

Lab Code: WADS Case N'o.:S"3"6 SAS No.: SDG Xo . : EQB-1

Lab F i l e ID.-VOE196" Lab Sample ID:VBLK1

Date Analyzed: 2/05/92 Time Analyzed:2044

GC Column:DB624 ID: 0.53 (mm) Heated Purge: (Y/X) X

Instrument ID:510000

THIS METHOD BLANK APPLIES TO THE FOLLOWIXG SAMPLES. MS, AND MSD:

COMMENTS:

0102030405060708091011121314151617IS1920212223242526"> 7

282930

EPASAMPLE NO.

MW15AWMW15BFMW17AWMW17BFMW20AAMW20AB

LABSAMPLE ID

427591014276210142760101427631014276510142*66101

LABFILE ID

VOE1968VOE1970VOE19"!VOE1972VOE1976VOE1977

TIMEANALYZED

2119225823330008022"0302

OGOOQ-k

AR3Q73I9page 1 of 4FORM IV VOA 3/90

! VBLK2Lab Name : WADS'WORTH/ALERT Contract : 6S-D 1-008.5 - ! _____.._ _.__.._

Lab Code:WADS Case N'o.:S73"6 SAS No.: SDG Xo.:EQB-l

Lab F i l e ID:VOE19S2 Lab Sample ID:VBLK2

Date Analyzed: 2/06/92 Time Analyzed:1025

GC Column:DB624 ID: 0.53 (mm) Heated Purge: (Y/X) N

Instrument 10:510000

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES. MS. AND MSD

COMMENTS:

o'i02030405060703091011121314151617IS19202122232425261 -

2S2930

EPASAMPLE NO.

MW16BFMW21AWMW21BFW21BF#D '

LABSAMPLE ID

42775101427641014276810142769101

LABFILE ID

VOE1991VOE1983VOE1984VOE1992

TIMEANALYZED

1554110011351630

AR307320p a a e 2 o f 4FORM IV VOA 3/90

. . . . .VOLATILE M'E'rtfbD BLANK SUMMARYVBLK3

Lab Name:WADSWORTH/ALERT Contract:63-Di-0085

Lab Code:WADS Case No.:8~3"6 SAS No.: SDG Xo.:EQ8-I

Lab File ID:VOL99S1 Lab Sample ID:\"BLK3

Date Analyzed: 2/0"/92 Time Analyzed:012 I


Instrument ID:FIXX52

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES. MS. AND MSD:

01020304050607080910111213141516

IS1920212223242526

282930

EPASAMPLE NO.

EOB-1H.MW9BFMW16AWMW21AWMSMW21AWMSDMW2OBFTRPBL1

LABSAMPLE ID

42767101427731014277110142"644276442"7010142*61101

.

LAB •FILE ID

VOL99S3VOL99S"VOL99S5VOL9990VOL9991VOL9984VOL99S2

TIMEANALYZED

0228044303350624065803010154

COMMENTS!

flR30732lpase 3 of 4

FORM IV VGA

'"'''"' ; VOLATu. -lETHOD BLANK bUNr:-;,-... ' •"-;__,_/__j;

VBLK4Lab Name:WADSWORTH/ALERT Contract:6S-D1-OOS5

Lab Code:WADS Case No.:S"3"6 SAS No.: SDG Xo.:EQB-l

Lab F i l e ID:VOL1001 Lab Sample ID:VBLK4

Date Analyzed: 2/0"/92 Time Ana 1 yzed: 1 334

GC Column:DB624 ID: 0.53 (mm) Heated Purge: (Y/N) X

Instrument ID:FINN52

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES. MS. AND MSD:

! EPA! SAMPLE NO.i — — — — — — — - - — — -

01 IHMW9AW02IMW20AW03!04!05!06!0"!03!09!10!11!12!13!14!15!16!1" !18!19!20!21!22!23!24!25!26!27)23!29 !_30!

LABSAMPLE ID

427-210142774101

• ,

LABFILE ID

VOL1002VOL1003

TIMEANALYZED

14101453

OMMENTS:

, f , AR307322pase 4 of 4FORSI IV VGA

•.'. . • VOL^VFLe'•CRG.:^H>: I N'BROMOFLUOROBEXZENE (BFB)

Lab Name:WADSWORTH/ALERT Contract:6S-D1-OOS5

Lab Code:WADS Case No.:S"3"6 SAS No.: SDG No.:EQB-i

Lab F i l e ID:BFBS51E BFB Injection Date: 2/05/92

Instrument 10:51000-0 BF3 Injection Time: 1650

GC Column:DB624 ID: 0.53 (mm) Heated Purge: (Y/X) N

<l

m/e

50

9596

173174175176177

ION ABUNDANCE CRITERIA

S.O - 40.0% of mass 9530.0 - 66.0% of mass 95Base peak. 100% relative abundance5.0 - 9.0% of mass 95Less than 2.0% of mass 17450.0 - 120.0% of mass 954.0 - 9.0% of mass 17493.0 - 101 .0% of mass 1745.0 - 9.0% of mass 176

% RELATIVEABUNDANCE

13.438.6100.0

- ^0.0( 0.0)1"4.05.4( ' 7.3)1

71 ,2( 96.2) 14.9( 6.9)2

ti

1-Value is % mass 174 2-Value is % mass 1"6

ilS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, AND MSD, BLANKS AND STAND.-

! EPA! SAMPLE NO.!— ====s-=-s-

01 ! VSTD200A02IVSTD100A03! VSTD020A04IVSTD010A05! VSTD050A06! VBLK107 IMW15AWOS !MW15BF091.MW17AW10IMW17BF11 1MW20AA121MW20AB13!14!15!16!1"!IS!19!20!"> 1 '- i 1"> !> '

LABSAMPLE ID

VSTD200AVSTD100AVSTD020AVSTD010AVSTD050AVBLK1427591014276210142760101427631014276510142766101

LABFILE ID

VOE1962VOE1963VOE1964VOE1965VOE1966VOE1967VOE1968VOE1970VOE1971VOE 1972VOE19"6VOE 19""

DATEANALYZED

2/05/922/05/922/05/922/05/922/05/922/05/922/05/922/05/922/05/922/06/922/06/922/06/92

TIMEANALYZED

174"18251S591934200920442119225823330008022"0302

P.« i or . BR307323FORM V VOA 3/90

";O:.t'!';i.t Oi'.G.-'..'.: --i Xs'TRUMcNT ;""': ' . RMAXCE '.'nECBROMOFLUOROBENZENE i BFB") '

Lab Name : WADSWORTH/. \LERT Cont-ruet :63-Di-GOS5

1jLab F i l e ID:BFBS52E . BFB I n j e c t i o n Date: 2 / O r / "2

Instrument ID:51000.0 . ~_ .. 5F5 I n j e c t i o n Ti:;ie:03-i


~- RELATIVEm/e ION ABUNDANCE CRITERIA ABUNDANCE

50 S.O - 40. 0': of "mass, 95 - 22.4"5 30.0 - 66.0% of mass 95 42.095 Base peak.96 5.0-9.0%

100% r e l a t i v e abundance 100.0of mass 95 . -r —

173 Less than 2.0% of mass 1"4 0.0( 0.0)1174 50.0 - 120.0% of mass 95175 4.0-9.0%1-6 93.0 - 101177 5.0-9.0%

THIS CI

|W

0102030405060"OS09101 1121314

16

1819201 1_ j.1 •>

64.6of mass 1"4 4 . "( " . 3 ) 1. 0% of mass 174of mass 1~6

60. 3( 93.3)14. 2( - .0)2

1-Value is % mass 174 2-Value is % mass 1"6

IECK APPLIES TO THE FOLLOWING SAMPLES. MS. AND MSD. BLANKS AND STANDARDS

EPASAMPLE NO.

VSTD050CVBLK2MW21AWMW21BFMW16BFW21BFD

————— ... __.__

LABSAMPLE ID

VSTD050CVBLK242"6410i427681014 2 " " 5 1 0 i42*69101

. ..._. ... . _

—————— - -

LABFILE ID

VOE 1980VOE 198 2VOE19S3VOE 1984VOE 1991VOE 1992

._ _ .- , - ... . .. -.

DATEANALYZED

2/06/922/06/922/06/922/06/922/06/922/06/92

.

. . . ————— .

---f — - —

TIMEANALYZED

090310251 100113515541630

•- — — — - — -•-

. „ . ftR3Q732i*n ,\ e e l o ; :•

• ' -•"-''--"--•••• • • • - • • . ; • -• >• BROMOFLUOROBENZENE . ( BFB )

Lab Name:WADSWORTH/ALERT Contract:68-D1-0085

Lab Code:WADS Case No.:S~3*6 SAS No.: SDG No.:EQB-l

Lab F i l e ID:BFB540L BFB Injection Date: 2/06/92

Instrument ID:FINX52 BFB Injection Time:1052

GC Column:DB624 ID: 0.53 (mm) Heated Purge: (Y/N) N

<lm/e

50"59596173174175176177


S.O - 40.0% of mass 9530.0 - 66.0% of mass 95Base peak, 3.00% relative abundance5.0 - 9.0% of mass 95Less than 2.0% of mass 17450.0 - 120.0% of mass 954.0 - 9.0% of mass 17493.0- 101 .0% of mass 1745.0 - 9.0% of mass 176

% RELATIVEABUNDANCE

•} q cJO**.

39."100.06.60.6{ 0.

'"**•*

5.5( 7."I . 1( 9".5.2( 7.

S) 1

5)18) 13 )2

1-Value is % mass 174 2-Value is % mass 176

THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, AND MSD, BLANKS AND STANDARDS

! EPA! SAMPLE NO.

01 ! VSTD050B02 ! VSTD200B03 ! VSTD100B041VSTD020B05 i VSTD010B06!07!08!09!10!11!12!13!14!15!16!17!18!19!20!21!i •> i

LABSAMPLE ID

VSTD050BVSTD200BVSTD100BVSTD020BVSTD010B

LABFILE ID

==============VOL9959VOL9960VOL9961VOL9962VOL9963

'

DATEANALYZED

==========2/06/922/06/922/06/922/06/922/06/92

TIMEANALYZED

10591142122112551328

pa?e 3 of 5 AR307325

CGC3-0

FORM V VOA 3/c><~

. ,VOLATILE ORGANIC INSTRUMENT PERFORMANCE CHECK

BROMOFLUOROBENZENE (BFB)

Lab Name : WADSWORTH/ALERT Con t'r ac t : 6S-D 1 -OOS5

Lab Code:WADS Case No.:S"3"6 SAS No.: SDG No.:EQE-l

Lab F i l e ID:BFB541L BFB Injection Date: 2/06/92

Instrument ID:FINX52 BFB Injection Time:23l2


m/e

50"59596

173174175176177

S.O30.0Base5.0Less50.04.093.05.0


- 40.0% of mass 95- 66.0% of mass 95peak, 100% relative abundance

- 9.0% of mass 95than 2.0% of mass 174- 120.0% of mass 95

- 9.0% of mass 174- 101 .0% of mass 174

- 9.0% of mass 176.

% RELATIVEABUNDANCE

36.960 . "

100.0" .60.5( 0.6)1

85. 15.S( 6.S) 1

33. 9( 98.6)16.3( 7.5)2

1-Value is % mass 174 2-Value is % mass 1~6

THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, AND MSD, BLANKS AND STANDARDS

0102030405060708091011121314151617IS192021i ->

EPASAMPLE NO.

_ _ _ _ _ _ _ _ _ _ _ _VSTD050DVBLK3TRPBL1EOB-1MW20BFMW16AWHMW9BFMW21AWMSMW21AWMSD

LABSAMPLE ID

VSTD050DVBLK342761101427671014277010142771101 .427731014276442764

LABFILE ID

VOL99SOVOL9981VOL99S2VOL9983VOL99S4VOL99S5VOL99S"VOL9990VOL9991

DATEANALYZED

2/06/922/Or/922/0-/922/07/922/07/922/07/922/0~/922/0"/922/0-/92

TIMEANALYZED

231901210154022S03010335044306240658

AR307326pace 4 or r

F,-|u> \l '• I',-! V

VOLATILE -Oi'L.'.:1. I : .• . .-. Yru. ML'XT PERFORMANCE CHECKBROMOFLUOROBENZENE (BFB)

Lab Name:WADSWORTH/ALERT Contract:63-D1-OOS5

Lab CodetWADS Case No.:S~3"6 SAS No.: SDG Xo.:EOB-l

Lab F i l e ID:BFB542L BFB Injection Date: 2/0"/92

Instrument ID:FINN52 BFB Injection Time:1125


m/e

50"59596173174175176177

THIS CI

0102030405060"0809101112131415161"18192021T ~>

% RELATIVEION ABUNDANCE CRITERIA ABUNDANCE

8.0 - 40 .0"o of mass 95 35.130.0 - 66.0% of mass 95 43.2Base peak,5.0 - 9.0%

100% relative abundance 100.0of mass 95 6."

Less than 2.0% of mass 1"4 0.4( 0.6)150.0 - 120.0% of mass 954.0 - 9.0%93.0 - 1015.0 - 9.0%

76.6of mass 174 5.8{ " .6) 10% of mass 174 ~6.S( 100.3)1of mass 176 5 .3( 6.9)2

•

1-Vaiue is % mass 174 2-Value is % mass 1*6

IECK APPLIES TO THE FOLLOWING SAMPLES. MS. AND MSD, BLANKS AND STANDARDS

EPASAMPLE NO.

VSTD050EVBLK4HMW9AWMW20AW

LABSAMPLE ID

VSTD050EVBLK44277210142""4101

_

. LABFILE ID

VOL9999VOL1001VOL1002VOL1003

DATEANALYZED

2/0"/922/0"/922/0"/922/0-/92

"

'

1

TIMEANALYZED

121"133414101453

O' -. <r "7a A.*"

. f AR3Q7327page ? o f :•

FORM V VOA

\UlAtlL£AINTEKi%.^ S'l... •.:'• -.0 ARi '. --AKD R'i :,-.":;: .:;,,.'i •••• '. °~"f r' ." \ '• '•" ' ' ~~ " ' *

Lab Name:WADSWORTH/ALERT Contract:68-D1-0085

Lab Code:WADS Case No.:S7376 SAS No.: SDG No.:EQB-l

Lab F i l e ID: {Standard):VOE1966 Date Analyzed: 2/05/92

Instrument 10:510000 Time Analyzed:2009


1111! _ _ _ _ — _ — — — — _

! 12 HOUR STD! UPPER LIMIT! LOWER LIMIT

! EPA SAMPLE! NO.! _ _ _ _ _ — _ _ _ _ _1 = = - = = = -=: = = --

01 iVBLKl02!MW15AW03!MW15BF04l.MW17.AW051MW17BF06i.MW20AA07 1MW20AB03!k09!flO!I l l -12!13!14!15!16!17!IS!19!20!21!22!

IS 1 (BCM)AREA #

14008128016270041

1324041170461116411149S411215395827105691

_...

-

RT ?

6.577.076.0"

6.576.576.586.586.576.576.57

.

IS2(DFB)AREA *

4898909"9~SO244945

475635424918389388399724410541349024380999

RT *

S.S39.338.33

8.83'8.828.878.878.838.838.83

IS31CBZ)AREA =

481916963832240958

432154391572366723373032381480326774356250

RT =

14.6215. 1214. 12

14.6014.6014.6214.6214.6014.6014.62

.

IS1 (BCM) = BromochloromethaneIS2 (DFB) = 1.4-DifluorobenzeneIS3 (CBZ) = Chlorobenzene-d5

AREA UPPER LIMIT = +100% of internal standard areaAREA LOWER LIMIT = - 50% of internal standard areaRT UPPER LIMIT = +0.50 minutes of internal standard RTRT LOWER LIMIT = -0.50 minutes of internal standard RT

= Column used to flag values outside of QC limits with an astersik* Values outside of QC limits.

! of 4 flR307328FORM VIII VOA 3/90

.uLATILE INTERNAL S I'AN'LM'U. -tl 'A" ' r: :r'T: H'MV*:'->

'Lab Name:WADSWORTH/ALERT Contract:6S-D1-0085

Lab Code:WADS Case No.:873~6 SAS No.: SDG No.:EQB-l

Lab F i l e ID: (Standard):VOE1980 ' Date Analyzed: 2/06/92

Instrument 10:510000 Time Analyzed:0903


iiii

! 12 HOUR STD1 UPPER LIMIT! LOWER LIMIT

! EPA SAMPLE! NO.! ============

01 IVBLK202 IMW21AW03IMW21BF041.MW16BF05!W21BF£D -•"*&'"06!07!08!09!10!11!12!13!14!15!16!17!18!19!20!21!22!

I S 1 { BCM )AREA *

19049538099095248

==========155305137062137132126872131522

RT 4

6.577.076.07

=======6.576.586.586.606.58

IS2(DFB)AREA *

7134601426920356730

553521497404508629458609468955

'

•

RT #

S.S39.338.33

S.S38.87S.S73.878.37

t1

IS3(CBZ)AREA =

6464821292964323241

=====5====

==========

49447"4437934564^243161"44368"

.

RT -

14.6015. 1014. 10

14.6214.6214.6214.6214.62

41

IS1 (BCM) = BromochloromethaneIS2 (DFB) = 1 .4-Dif luorobenzeneIS3 (CBZ) = Chlorobenzene-d5


* Column used to flag values outside of QC l i m i t s with an astersik* Values outside of QC l i m i t s .

HR307329page 2 of 4FORM VI I I VOA 3/90

\0.,.-: L.r, iNTtRXAi. olANDARD AREA AND RT SUMMARY

Lab Name:WADSWORTH/ALERT Contract:6S-D1-OOS5

Lab Code:WADS Case No.:S"3"6 SAS'No.: SDG No.:EQB-l

Lab Fi l e ID (Standard):VOL~980 Date Analyzed: 2/06/92

Instrument ID:FINN52 Time Analyzed:2319


on.02030405i0607|OS;

10!HI.

12!13!14!15!16!17!13!19!20!21!.22 '

12 HOUR STDUPPER LIMITLOWER LIMIT

EPA SAMPLENO.

VBLK3TRPBL1EOB-1MW20BFMW16AWHMW9BFMW21AWMSMW21AWMSD

I S 1 ( BCM )AREA =

232594651811630

'

2266322738192381975320759203322240820710

RT ?

6.336. S35.83

6.376.376.376.376.376.356.376.37

IS2(DFB)AREA =

S6"251"345043363

7936384413760687517073349"36848076178595

RT *

8.5*9.0-S.O"

8.533.57S.5SS.573.5"8.5"8.583.58

IS3(CBZ)AREA =

"4*351494"03*363

6209172561622186395665306604237093267191

RT =

14.1514.6513.65

14. 1514. 1514. 1514. 1514. 1514. 1314. 1514. 15

IS1 (BCM) = BromochloromethaneIS2 (DFB) = 1.4-DifluorobenzeneIS3 (CBZ) = Chlorobenzene-d5


= Column used to flag values outside of QC l i m i t s with an as t er i sk o.--,< ^t* Values out side of QC i imits. mo OH 0 °AR307330

page 3 of 4 - .FORM VI Ir VGA '/on

. . .VOLATILE INTERNAL STANDAi'D AREA AND Rl SUM .-u," "

Lab Name:WADSWORTH/ALERT Contract:63-D 1-0085

Lab CoderWADS Case No.:S73"6 SAS No.: SDG No.:EOS-I

Lab F i l e ID {Standard):VOL9999 Date Analyzed: 2/0"/92

Instrument ID:FINN52 Time Ana 1yzed:121~


O

01020304050607OS09101112131415161"IS19202122

12 HOUR STDUPPER LIMITLOWER LIMIT

EPA SAMPLENO.

VBLK4H.MW9AWMW20AW

I S 1 ( BCM )AREA *

305"!6114215236

276"22849926"26

,

RT i

6.386.385.38

6.376.426.38

IS2(DFB)AREA =

1141*32283565"039

107432108963103734

RT *

8.5S9.08S.OS

8.5"8.603.53

IS3(CBZ)AREA =

9639"192"9448199

85050364*186*81

RT =

14. 1"14.6"13.6"

14.1514.1-14. 1"

TS1 (BCM) = BromochloromethaneIS2 (DFB) = 1.4-DifluorobenzeneI S3 (CBZ) = Chlorobenzene-d5

AREA UPPER LIMIT = +100% of internal standard area •AREA LOWER LIMIT = - 50% of internal standard areaRT UPPER LIMIT = +0.50 minutes of internal standard RTRT LOWER LIMIT = -0.50 minutes of internal standard RT

= Column used to flag values outside of QC l i m i t s with an asterisk.* Values outside of QC l i m i t s . /^/

AR30733Ipage 4 of 4

FORM V I I I VGA 3/90

VOLATILE SAMPLE DATA

AR307332

VOIATILE

Lab Name :WADSWORTH/ ALERT Con t r act : 68-D1 -0085EOB-i i

Lab Code:WADS Case No.:87376 SAS No.: SDG No.:EQB-l

Matrix: (soil/water) WATER Lab Sample ID:42"6"101

Sample wt/vol: 5.00 (g/ml) ML Lab File ID: VOL9983

Level: (low/med) LOW Date Received: 1/30/92

% Moisture: not dec. 0 Date Analyzed: 2/07/92

GC Column:DB624 'ID: 0.53 (mm) Dilution Factor: 1.00

Soil Extract Volume: 0.00 (uL) Soil Aliquot Volume: O.OO(uL)

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L_ Q

74-87-3-------—Chloromethane74-S3-9---------Bromomethane75-01-4———————Vinvl Chloride75-00-3—--—-—Chloroethane75-09-2———————Methvlene Chloride67-64-1 ———— ——Acetone75-15-0———————Carbon Disulfide75-35-4 ———— — — 1, 1-Dichloroethene75-34-3———————1 , 1-Dichloroethane540-59-0——————1,2-Dichloroethene (total )67-66-3 ——————— -Chloroform107-06-2——————1 , 2-Dichloroethane78-93-3 ——————— 2-Butanone71-55-6--—-----1,1.1-Trichloroethane56-23-5———————Carbon Tetrachloride75-27-4—-------Bromodichloromethane78-87-5 — -—————1,2-Dichloropropane10061-01-5-------cis-1, 3-Dichloropropene79-01-6———————Trichloroethene124-48-1--------D i bromochloromethane79-00-5 ———— —— 1, 1 , 2-Trichloroethane71-43-2———————Benzene10061-02-6-- — --trans-1.3-Di ch_lp ropropene75-25-2- — ————Bromoform10 8-10-1 —————— 4-Meth y_l - 2 -JPe n tanone591-78-6——————2-Hexanone _____127-18-4---————Tetrachloroethene79-34-5 —————— -1,1,2. 2-Tetrachloroethane108-88-3 ——————Toluene _____108-90-7- — ———— Chiorobenzene100-41-4- ————— Ethyl benzene100-42-5--------Styre n e1330-20-*--————Xylene (totalI

I.I II.______________________________________________________ I.

FORM I VOA

10. !U10. |U10. |U10. U10. |U69.!10.10. !U10. ! U10. !U10 . i U10.10. |U10. IU10 . I U10. !U_10. !U10. !U10. ! u1010. |u10. JU10. |ul o. ! u10 . ! u10 I .10. ! U1010. ! U1010. ! U1 0 . ! U10. ! U

<l

AR307333 CCCO17

VOLATILE ORGAN I'CS ANALYSIS DAT.-, .sHEETTENTATIVELY IDENTIFIED COMPOUNDS

Lab Name:WADSWORTH/ALERT Contract:68-D1-OOS5

Lab CoderWADS Case No.:87376 SAS No.: SDG No.:EQB-l

Matrix: (soil/water) WATER Lab Sample 10:42767101




GC Column:DB624 ID: 0.53 (mm) Dilution Factor: 1.00


CONCENTRATION UNITS:Number TICs Found: jf I . (ug/L or ug/Kg) UG/L_

CAS NUMBER

i.-79--20-<?2.3.4.5.6.7.3.9.10.11 .12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

COMPOUND NAME

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G2/07/92 2:23:00Sample: 42767101i EG3-1, 5MLConds. : FINN52Formula: VOC Instrument: FINN52 Weight: O. OOOubmitted by: WADS Analyst: JP Acct. No. : 68D10008

A«OUNT=AREA * REF AMNT/<REF AREA * RESP FACT)Resp. fac. from Library Entry

No Name1 BROMOCHLOROMETHANE2 1,4-DIFLUOROBENZENE3 CHLOROBENZENE-D54 CHLOROMETHANE5 BROMOMETHANE6 VINYL CHLORIDE7 CHLOROETHANE8 METHYLENE CHLORIDE9 ACETONE10 CARBON DISULFIDE11 1,1-DICHLOROETHENE12 1,1-DICHLOROETHANE13 1, 2-DICHLOROETHENE (TOTAL)14 CHLOROFORM15 1,2-DICHLOROETHANE16 2-BUTANONE17 1,1, 1-TRICHLOROETHANEIS CARBON TETRACHLORIDE19 VINYL ACETATEO BROMODICHLOROMETHANE21 1,2-DICHLOROPROPANE22 CIS-1,3-DICHLOROPROPENE23 TRICHLOROETHENE24 DIBROMOCHLOROMETHANE25 1,1,2-TRICHLOROETHANE26 BENZENE27 TRANS-1,3-DICHLOROPROPENE28 BROMOFORM29 4-METHYL-2-PENTANONE3O 2-HEXANONE31 TETRACHLOROETHENE32 1,1,2, 2-TETRACHLOROETHANE33 TOLUENE34 CHLOROBENZENE35 ETHYLBENZENE36 STYRENE37 XYLENES38 TOLUENE-0839 BROMOFLUOROBENZENE40 1, 2-DICHLOROETHANE-D441 2-CHLOROETHYL VINYL ETHER42 XYLENE (TOTAL)43 1, 3-DICHLOROBENZENE44 1, 2-DICHLOROBENZENE5 1, 4-DICHLOROBENZENE6 ACROLEIN47 ACRYLONITRILE

AR307336 CGC3.JO

Uo Name'4S TRICHLGRGFLUOROhETHANE49 DICHLORODIFLUORQMETHANE50 CIS-1,2-DICHLOROETHENE

No m/z Scan Time Ref RRT Meth Area(Hght) Amount %Tot1 128 299 6:22 1 l.OOO A BB 19238. 250. OOO NG 13.722 114 403 8:35 2 l.OOO A BB 76O68. 250.000 NG 13.723 117 &64 14:09 3 1.000 A BB 62218. 250.000 NG 13.724 NOT FOUND5 NOT FOUND6 62 45 0:58 1 0.151 A BB 70. 0.872 NG 0.057 64 66 1:24 1 0.221 A BB 34. 0.381 NG O. 02S 84 159 3:23 1 0.532 A*BB 715. 7.733 NG 0.429 43 124 2:39 1 0.415 A BB 13143. 344.596 NG 18.9110 NOT FOUND11 NOT FOUND12 63 216 4:36 1 0.722 A BB 38. 0.174 NG 0.0113 NOT FOUND14 NOT FOUND15 62 359 7:39 1 1.201 A BB 39. 0.161 NG 0.0116 43 290 6:11 1 O. 970 A BB 645. 9.896 NG 0.5417 NOT FOUND18 NOT FOUND19 NOT FOUND20 NOT FOUND21 NOT FOUND22 NOT FOUND23 NOT FOUND24 NOT FOUND25 NOT FOUND26 NOT FOUND27 NOT FOUND28 NOT FOUND29 43 533 11:21 3 0.803 A BB 1058. 4.921 NG 0.2730 NOT FOUND31 NOT FOUND32 NOT FOUND33 91 537 11:26 3 O. 809 A BB 41. 0.146 NG 0.0134 NOT FOUND35 NOT FOUND36 NOT FOUND37 NOT FOUND38 98 532 11:20 3 O. 801 A BB 64632. 244.612 NG 13.4339 95 783 16:41 3 1.179 A BV 56859. 232.546 NG 12.7640 65 354 7:33 1 1.184 A BB 52117. 226.137 NG 12.4141 NOT FOUND42 NOT FOUND43 NOT FOUND44 146 931 19: 5O 3 1. 402 A BB 36. 0. 121 NG 0. 0145 NOT FOUND46 NOT FOUND47 NOT FOUND48 NOT FOUND49 NOT FOUND50 NOT FOUND

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Lab Name :\VADSWORTH/ALERT Contract : 68-D1-OOS5HMW9AW

74-87-3--—————Chior ome t h a n e74-83-9----—---Bromomethane75-01-4———————Vinyl Chloride75-00-3—-—-——Chloroethane75-09-2— —————Methylene Chloride67-64-1------——Acetone75-15-0 ———— — -Carbon Bisulfide75-35-4------—-1.1-Dichloroethene75-34-3——————l ,1-Dichloroethane •" * '540-59-0--- ——— 1,2-Dichloroethene (total)67-66-3———————Chloroform107-06-2- ———— — 1. 2-Dichloroethane78-93-3 —————— — 2-Butanone71-55-6-------—1.1.1-Trichloroethane56-23-5 ——————Carbon Tetrachloride75-27-4---------Bromodichloromethane78-87-5 ——— —— -1.2-Di c h loropropane10061-01-5------cis-l,3-Dichloropropene79-01-6- ————— --Trichloroethene..124-4S-1--- — ---Dibromochlorome thane79-00-5 ——— -——.-1,1.2-Trichloroethane71-43-2 ——————Benzene10061-02-6---—-trans-1,3-Dichloropropene75-25-2-----———Bromoform108-10-1 — - —— — 4-.Methyl-2-Pentanone591-78-6--.--.. - - — 2 -.H exanone127-18-4- — ———— Tetrachloroethene79-34-5- - — - -r--rl. 1.2. 2-Tetra c h 1 o r.oe thane108-88-3----——-Toluene108-90-7——————Chiorobenzene100-41-4---- ---- EJ hv _ 1 b e n_z e n e100-42-5-——: — - - S t .vr_ene___..._1330-20------—-Xylene (total

33. !U33. |U33. !U21. !33. !U3333

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Lab Code:WADS Case No.:ST376 SAS No.: SDG No.:EQB-l

Matrix: (soil/water) WATER Lab Sample 10:42*72101



°o Moisture: not dec. Date Analyzed: 2/07/92


Soil Extract Volume:0 (uL) Soil Aliquot Volume:0 (uL)

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q

,:' - Er.-.•V. v-.E ORGAN i Co ANALYSIS DATA SHEET __TENTATIVELY IDENTIFIED COMPOUNDS

Lab Name:WADSWORTH/ALERT Centract:68-D1-0085H.MW9AW







Soil Extract Volume: 0.00 (uL) Soil Aliquot Volume: 0.00(uL

CONCENTRATION UNITS:Number TICs Found: 0 (ug/L or ug/Kg) UG/L_

CAS NUMBER

1.2.3.4.5.6.7.8.9.10.11 .12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

COMPOUND NAME

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AMQUNT=AREA # REF AMNT/(REF AREA * RESP FACT)Resp. fac. from Library Entry

No Name1 BROMOCHLOROMETHANE2 1,4-DIFLUOROBENZENE3 CHLOROBENZENE-D54 CHLOROMETHANE5 BROMOMETHANE6 VINYL CHLORIDE7 CHLOROETHANE8 METHYLENE CHLORIDE9 ACETONE10 CARBON DISULFIDE11 1,1-DICHLOROETHENE12 1,1-DICHLOROETHANE13 1,2-DICHLOROETHENE (TOTAL)14 CHLOROFORM15 1,2-DICHLO.ROETHANE16 2-BUTANONE17 1,1,1-TRICHLOROETHANE18 CARBON TETRACHLORIDE19 VINYL ACETATE2O BROMODICHLOROMETHANE21 1,2-DICHLOROPROPANE22 CIS-1,3-DICHLOROPROPENE23 TRICHLOROETHENE24 DIBROMOCHLOROMETHANE25 1,1,2-TRICHLORQETHANE26 BENZENE27 TRANS-li3-DICHLORQPRQPENE28 BROMOFORM29 4-METHYL-2-PENTANONE30 2-HEXANONE31 TETRACHLOROETHENE32 1,1,2, 2-TETRACHLOROETHANE33 TOLUENE34 CHLOROBENZENE35 ETHYLBENZENE36 STYRENE37 XYLENES38 TOLUENE-D839 BROMOFLUOROBENZENE40 1,2-DICHLOROETHANE-D441 2-CHLOROETHYL VINYL ETHER42 XYLENE (TOTAL)43 1,3-DICHLOROBENZENE44 1,2-DICHLOROBENZENE45 1,4-DICHLOROBENZENE46 ACROLEIN47 ACRYLONITRILE t

AR3073l*5

15 10. 196 A BB 85. 0.599 NG 0.0231 1 0.236 A BB 4234. 31.555 NG 1.0927 1 O. 538 A BS 16O. 1. 002 NG 0. 03

No Name43 TRICHLDRCiFLUuROMETHANE4? DICHLDRQDIFLUQRGMETHANE50 CIS-1,2-D1CHLQROETHENE

No m/z Scan Time Ref RRT Meth Area(Hght) Amount XTot1 128 301 6:25 1 1.000 A BB 28499. 250.000 NG 8.642 114 404 8:36 2 1.000 A BB 108968. 25O. OOO NG 8.643 117 665 14:10 3 1.000 A BB 86471. 250.000 NG 8.644 NOT FOUND,5 NOT FOUND6 62 59 17 64 71 18 84 162 39 NOT FOUND10 NOT FOUND11 96 119 2:32 1 0.395 A BB 59316. 371.647 NG 12.8412 63 222 4:44 1 0.738 A BB 26225. 70.630 NG 2.4413 96 185 3:56 1 0.615 A BB 46. O. 289 NG 0.0114 NOT FOUND15 62 362 7:43 1 1.203 A BB 437. 1.252 NG 0.0416 43 295 6:17 1 O. 980 A BB 112. 1.220 NG 0.0417 97 324 6:54 2 O. 802 A BB 225662. 628.969 NG 21.7318 NOT FOUND19 NOT FOUND2O NOT FOUND21 NOT FOUND22 NOT FOUND23 130 421 8:58 2 1.042 A BV 27296. 162.295 NG 5.6124 NOT FOUND,25 97 581 12:23 2 1.438 A BB 673. 4.570 NG 0.166 78 357 7:36 2 O. 884 A BB 156. 0.393 NG 0.0127 NOT FOUND28 NOT FOUND29 43 533 11:21 3 0. 8O2 A BB 170O. 6.681 NG 0.2330 NOT FOUND31 NOT FOUND32 NOT FOUND33 NOT FOUND34 NOT FOUND35 NOT FOUND36 NOT FOUND37 NOT FOUND38 98 533 11:21 3 O. 8O2 A BB 91156. 254.668 NG 8.8039 95 784 16:42 3 1.179 A BV 77849. 234.119 NG 8.0940 65 355 7:34 1 1.179 A BB 70456. 2O7. 57O NG 7.1741 NOT FOUND42 NOT FOUND43 146 892 19:00 3 1.341 A BB 79. O. 178 NG 0. Ol44 NOT FOUND45 146 900 19: 1O 3 1.353 A BB 415. O. 866 NG 0.0346 NOT FOUND47 NOT FOUND48 NOT FOUND49 NOT FOUND50 96 281 5: 59 1 0. 934 A BB 2556O. 166. 508 NG 5. 75

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Lab Name:WADSWORTH/ALERT Contract:6S-D1-OOS5H.MW9BF








CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or Ug/Kg) UG/L_ Q

74-87-3————•———Chlorome thane4-83-9---------Bromomethane75-01-4———————Vinvl Chloride75-00-3 —— —— -—Chloroe thane75-09-2———————Methylene Chloride67-64-1 ——————Acetone75-15-0--—————Carbon Disulfide75-35-4- — ———— 1. 1-Dichloroethe.ne75-34-3---------1,1-Dichloroethane540-59-0- ————— 1.2-Dichloroethene (total )67-66-3———————Chloroform107-06-2——————1.2-Di chloroe thane78-93-3- —————— 2-Butanone71-55-6———————1.1.1-Tri chloroe thane56-23-5---—--—Carbon Tetrachloride75-27-4---------Bromodichloromethane78-87-5---------1,2-Dichloropropane10061-01-5---—-cis-l,3-Dichloropropene79-01-6 ——————Trichloroethene124-48-i------—Dibromochloromethane79-00-5 ———— -——1., 1,2-Tri chloroe thane71-43-2———————Benzene10061-02-6————trans-1.3-Dichloropropene75-25-2--- ——— -Bromoform108-10-1 —————— 4-Methyl-2-Pentanone591-78-6- ————— 2-Hexanone127-18-4---———-Tetrachloroethene79-34-5-- ——— - —1,1,2,2-Tetrachloroethane108-88-3-- ————— Toluene108-90-7---———-Chiorobenzene100-41-4- ————— Eth ylbenzene.100-42-5 —————— St.yrene1330-20-7—————Xylene (tota 1J_

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41

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AMQUNT=AREA * REF AMNT/(REF AREA * RESP FACT)Resp. fac. from Library Entry

No Name1 BROMOCHLOROMETHANE2 1,4-DIFLUOROBENZENE3 CHLOROBENZENE-D54 CHLOROMETHANE5 BROMOMETHANE6 VINYL CHLORIDE7 CHLOROETHANEB METHYLENE CHLORIDE9 ACETONE10 CARBON DISULFIDE11 1,1-DICHLOROETHENE12 1,1-D1CHLOROETHANE13 1>2-DICHLQROETHENE <TOTAL)14 CHLOROFORM15 1,2-DICHLOROETHANE16 2-BUTANONE17 1.1,1-TRICHLOROETHANE18 CARBON TETRACHLORIDE19 VINYL ACETATE20 BROMODICHLOROMETHANE21 1,2-DICHLOROPROPANE22 CIS-1,3-DICHLOROPROPENE23 TRICHLOROETHENE24 DIBROMOCHLOROMETHANE25 1,1,2-TRICHLOROETHANE26 BENZENE27 TRANS-1.. 3-DICHLOROPROPENE28 BROMOFORM29 4-METHYL-2-PENTANONE30 2-HEXANONE31 TETRACHLOROETHENE32 1,1,2, 2-TETRACHLOROETHANE33 TOLUENE34 CHLOROBENZENE35 ETHYLBENZENE36 STYRENE37 XYLENES38 TOLUENE-D839 BROMOFLUORQBENZENE40 1.2-DICHLOROETHANE-D441 2-CHLOROETHYL VINYL ETHER42 XYLENE (TOTAL)43 1,3-DICHLOROBENZENE44 1,2-DICHLOROBENZENE45 1,4-DICHLOROBENZENE46 ACROLEIN47 ACRYLONITRILE

AR307362 000046

No Name ' ',,,, "48 TRICHLOROFLUOROML.riANE49 DICHLORODIFLUOROMETHANE50 CIS-1,2-DICHLOROETHENE

No m/z Scan Time Ref RRT Meth Area(Hght) Amount /CTot1 128 298 6:21 1 1.000 A BV 20832. 250. OOO NG 14.532 114 4O2 8:34 2 1.000 A BV 73684. 25O. 000 NG 14.533 117 663 14:08 3 1.000 A BB 60428. 250.000 NG 14.534 NOT FOUND5 NOT FOUND6 NOT FOUND7 NOT FOUNDS NOT FOUND9 43 123 2:37 1 0.413 A BB 10574. 256.039 NG 14.8810 NOT FOUND11 96 112 2:23 1 0.376 A BB 32. 0.292 NG 0.0212 63 218 4: 39 1 O. 732 A BB 38. 0. 161 NG 0. 0113 NOT FOUND14 NOT FOUND15 NOT FOUND16 NOT FOUND17 97 321 6:50 2 0.799 A BB 364. 1.528 NG 0.0918 NOT FOUND19 NOT FOUND20 NOT FOUND21 NOT FOUND22 NOT FOUND23 13O 419 8:56 2 1.O42 A BV 1897. 14. 997 NG O. 8724 NOT FOUND25 NOT FOUND26 NOT FOUND27 NOT FOUND28 NOT FOUND29 43 531 11:19 3 0.801 A BB 1156. 5.536 NG 0.3230 43 611 13:01 3 0.922 A BB 67. 0.464 NG 0.0331 NOT FOUND32 NOT FOUND33 NOT FOUND34 NOT FOUND35 NOT FOUND36 NOT FOUND37 NOT FOUND38 98 530 11:17 3 0.799 A BV 62777. 244.631 NG 14.2239 95 781 16:33 3 1.178 A BB 53742. 226.309 NG 13.1540 65 352 7:30 1 1.181 A BB 55069. 220.668 NG 12.8341 NOT FOUND42 NOT FOUND43 NOT FOUND44 NOT FOUND45 NOT FOUND46 NOT FOUND47 NOT FOUND43 NOT FOUND49 NOT FOUND50 96 279 5:57 1 0.936 A BB 31. 0.312 NG 0.02

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74-8"- 3------ — -Chloromethane74-S3-9---------Bromomethane'5-01-4———————Vinvl Chloride75-00-3 — —— ——Chloroe thane75-09-2 ——— ———Methvlene Chloride67-64-1---------Ac e tone75-15-0——------Carbon Bisulfide75-35-4---—----1,1-Dichloroethene75-34-3 ——————— 1. 1-Dichloroethane540-59-0——————1 ,2-Dichloroethene (total)67-66-3---------Chloroform107-06-2--—----1.2-Pichloroethane78-93-3 ———— ——— 2-Butanone71-55-6---------1,1,1-Trichloroe thane56-23-5--—---—Carbon Tetrachloride'5-2"-4---------Bromodich1oromethane78-8~-5-- —— — —1,2 -Pi chloropropa ne_10061-01-5---—-cis-1.3-Dichloropropene79-01-6———————Trichloroethene124-4S-1--------Dibromochloromethaner9-00-5 ———— ———1 , 1 , 2-Tri chloroe thane1-43-2---------Benzene10061-02-6-—-—trans-1,3-Dichloropropene75-25-2---------Bromoform ___________________IPS-10-1—————— 4-Me t hy l_-_2.-P_e n tanone591-"S-6 —————— 2-Hexanone12"-lS-4——-----Tetrachloroethene79-34-5 -L" - - -~ -_ 1 _,_! ..._2_._ 2_- T.e_t r a chloroethane1Q8-SS-3- — - -r --Jo l.ue n e ... _,. __108-90-"- —————Chiorobenzene100-41-4 —————— Ethy .1 be n z e n e100-42-5-----——Stvrene1330-20-"————Xvlene (total)

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MW15AWLab Name :WADSWORTH/ALERT Cont rac t : 6S-D 1-0085 __.._____._____

Lab Code:WADS Case No.:8'3~(5 SAS No.: SDG Xo.:EQB-1

Matrix: (soil/water) WATER Lab Sample ID:42~59101

Sample wt/vol: 5.00 (g/ml) ML Lab F i l e ID: VOE196S

Level: (iow/med) LOW Pate Received: 1/30/92

% Moisture: not dec. Pate Analyzed: 2/05/92


Soil Extract Volume:0 (uL ) Soil Aliquot Volume:0 (uL

CONCENTRATION UNITS:CAS NO. COMPOUND (ug/L or Ug/Kg) UG/L Q

l»AR307368 000052

VOLATILE ORGrt.-ICS ASAi/i-^' .:....,-. _iiJTENTATIVELY IDENTIFIED COMPOUNDS

MW15AWLab Name:WADSWORTH/ALERT Contract:68-D1-0085

Lab Code:WADS Case No.:8~3~6 SAS No.: SDG No.:EQB-l

Matrix: (soil/water) WATER Lab Sample ID:42~5910l

Sample wt/vol: 5.00 (g/ml) ML Lab File ID: VOE196S






CAS NUMBER

1.o3.4.5.6.7 ..

9 _10.11 .12.13.14.15.16.17.18.19.20.21.22.23.24.25 .26.•> -28.29.30.

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AMOUNT=AREA * REF AMNT/<REF AREA * RESP FACT)Resp. fac. from Library Entry

No Name1 BROMOCHLOROMETHANE2 1,4-DIFLUOROBENZENE3 CHLOROBENZENE-D54 CHLOROMETHANE5 BROMOMETHANE6 VINYL CHLORIDE7 CHLOROETHANE8 METHYLENE CHLORIDE9 ACETONE10 CARBON DISULFIDE11 1, 1-DICHLOROETHENE12 1, 1-DICHLOROETHANE13 1>2-DICHLOROETHENE (TOTAL)14 CHLOROFORM15 1, 2-DICHLOROETHANE16 2-BUTANONE17 1,1,1-TRICHLOROETHANE18 CARBON TETRACHLORIDE19 VINYL ACETATEBO BROMODICHLOROMETHANE21 1,2-DICHLOROPROPANE22 CIS-l,3-DICHLOROPROPENE23 TRICHLOROETHENE24 DIBROMOCHLOROMETHANE25 1, 1,2-TR I CHLOROETHANE26 BENZENE27 TRANS-1,3-DICHLOROPROPENE28 BROMOFORM29 4-METHYL-2-PENTANONE30 2-HEXANONE31 TETRACHLOROETHENE32 1,1,2,2-TETRACHLOROETHANE33 TOLUENE34 CHLOROBENZENE35 'ETHYLBENZENE36 STYRENE37 XYLENES38 TOLUENE-DS39 BROMOFLUOROBENZENE40 1/2-DICHLOROETHANE-D441 2-CHLOROETHYL VINYL ETHER42 XYLENE <TOTAL)43 1,3-DICHLOROBENZENE44 1,2-DICHLOROBENZENE5 1,4-DICHLOROBENZENE

'46 ACROLEIN47 ACRYLONITRILE

000055AR30737I

No Name48 TRICHLOROFLUOROMETHANE49 DICHLORODIFLUOROMETHANE50 CIS-1,2-DICHLOROETHENE

No m/z Scan Time Ref RRT Meth Area(Hght) Amount XTot1 128 303 6:34 1 l.OOO A BB 117046. 25O. 000 NG 13.442 114 4O7 8:49 2 l.OOO A BB 424918. 25O. 000 NG 13.443 117 674 14:36 3 1.000 A BB 391572. 250.000 NG 13.444 NOT FOUND5 NOT FOUND6 NOT FOUND7 NOT FOUND8 NOT FOUND9 43 127 2:45 1 0.419 A BB 86834. 364.152 NG 19.5810 NOT FOUND11 NOT FOUND12 NOT FOUND13 NOT FOUND14 NOT FOUND15 NOT FOUND16 43 292 6:20 1 0.964 A BB 1556. 3.657 NG 0.2017 97 326 7: 04 2 0. 801 A BB 2887. 3. 500 NG 0. 1918 NOT FOUND19 NOT FOUND2O NOT FOUND21 NOT FOUND22 NOT FOUND23 13O 425 9:12 2 1.044 A BB 474. O. 545 NG O. 0324 NOT FOUND25 NOT FOUND26 NOT FOUND27 NOT FOUND28 NOT FOUND29 43 539 11:41 3 0. 8OO A BB 4172. 3.981 NG O. 2130 NOT FOUND31 NOT FOUND32 NOT FOUND33 NOT FOUND34 NOT FOUND35 NOT FOUND36 NOT FOUND37 NOT FOUND38 98 539 11:41 3 0.800 A BB 439862. 255.754 NC 13.7539 95 795 17:13 3 1.180 ABB 360663. 236. 529 NG 12.7240 65 358 7:45 1 1.182 ABB 187761. 240. 996 NG 12.9641 NOT FOUND42 NOT FOUND43 146 903 19:34 3 1. 34O A BB 726. 0.376 NG 0.0244 NOT FOUND45 146 915 19:49 3 1.358 A BB 1565. 0.777 NG 0.0446 NOT FOUND47 NOT FOUND48 NOT FOUND49 NOT FOUND50 NOT FOUND

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Matrix: (soil/water) WATER Lab Sample ID:42"62lOi

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% Moisture: not dec. Date Analyzed: 2/05/92




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75-01-4 —— -75-00-3 —— -75-09-2 —— -67-64-1 —— -"5-15-0 —— •75-1 5-4.----*7 C ^ '1 ^75-34- _>---•

67-66-3 —— -107-06-2---70 Q -} •?

71-55-6 —— -56-23-5 —— -75_->- 4f W *> . i

78-87-5 —— -10061-01-5-79-01-6 —— -1 94. — 4. Q— 1 — — -79-00-5 —— -" 1 — 43 — "* — — — •10061-02-6-i T- t 5 ~> — — — -108-10-1 — -

127-18-4 — -79-34-5 —— -iA O O O *>Uo-iso-o---1 H9 — QO — ~ — — .

100-41-4 ——100-42-5 ——1330-20-"—

------Chlorome thane---- — Bromome thane— ----Vinyl Chloride------Chloroe thane------Me thvlene Chloride

------Carbon Disulfide------1 , 1-Dichloroethene------ \ , i-Di chloroe thane———— 1 ,2-Dichloroethene (total)- — ---Chloroform-- — --1 , 2-Pi chloroe thane-- ——— 2-Butanone— ----1 , i . l-Trichloroethane- —— — Carbon Tetrachloride------Bromodi chlorome thane—— --1 , 2-Dichloropropane------cis-1 ,3-Dichloropropene- — —— Trichloroethene------Dibromochl oromet hane— - — -1,1, 2-Tri chloroe thane--- — -Benzene------trans-l,3-Pichloropropene------Bromof orm— —— 4-Methyl-2-Pentanone------2-Hexanone— . . . . . ,•— — — — i e t i acn i oroe t nene

• I ,_,_lCllClCIllwIUCtIlCtIlC

IvJiUtJIIC

------Chiorobenzene--- — -Ethvlbenzene------St vrene------Xylene (total)

10.10.10.10.10.27.10.45.28.

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Lab Code:WADS Case No.:S~3"6 SAS No.: SDG No.:EQB-l

Matrix: (soil/water) WATER Lab Sample IP:42~62101

Sample wt/vol: 5.00 (g/ml) ML Lab Fil e ID: VOE19"0






CAS NUMBER

•2.3.4.5 .6.1 .8.9.10.11 .12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27 .28.29.30.

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AMOUNT=AREA * REF AI1NT/CREF AREA * RESP FACT)Resp. fac. from Library Entry

No Name1 BROMOCHLQROMETHANE2 1i4-DIFLUOROBENZENE3 CHLOROBENZENE-D54 CHLOROMETHANE5 BROMOMETHANE6 VINYL CHLORIDE7 CHLOROETHANE8 METHYLENE CHLORIDE9 ACETONE10 CARBON DISULFIDE11 1,1-DICHLOROETHENE12 1,1-DICHLOROETHANE13 1,2-DICHLOROETHENE (TOTAL)14 CHLOROFORM15 1,2-DICHLOROETHANE16 2-BUTANONE17 1,li1-TRICHLOROETHANE18 CARBON TETRACHLORIDE19 VINYL ACETATE2O BROMODICHLOROMETHANE21 1,2-DICHLOROPRQPANE22 CIS-l,3-DICHLOROPROPENE23 TRICHLOROETHENE24 DIBROMOCHLOROMETHANE25 1,1,2-TRICHLOROETHANE26 BENZENE27 TRANS-1,3-DICHLOROPROPENE28 BROMOFORM29 4-METHYL-2-PENTANONE3O 2-HEXANONE31 TETRACHLOROETHENE32 1,1,2, 2-TETRACHLOROETHANE33 TOLUENE34 CHLOROBENZENE35 ETHYLBENZENE36 STYRENE37 XYLENES38 TOLUENE-D839 BROMOFLUOROBENZENE40 1,2-DICHLOROETHANE-D441 2-CHLOROETHYL VINYL ETHER42 XYLENE (TOTAL)43 1,3-DICHLOROBENZENE44 i,2-DICHLOROBENZENE45 1,4-DICHLOROBENZENE46 ACROLEIN47 ACRYLONITRILE

OQOGG2ftR3Q7378

. . .BB 5O7774. 671 734 NG 23. 45BB 77048. 1057028 NG 3.67

No Name48 TR I CHLOROFLUOROMETHANE49 DICHLORODIFLUOROMETHANE50 C I S-l, 2-DICHLOROETHENE

No m/z Scan Time Ref RRT Meth Area(Hght) Amount XTot1 128 304 6:35 1 1.000 A BB 111641. 25O. 000 NG 8.732 114 409 8:52 2 1.000 A BB 389388. 25O. OOO NG 8.733 117 675 14:37 3 1.000 A BB 366723. 25O. 000 NG 8.734 NOT FOUND5 NOT FOUND6 NOT FOUND7 NOT FOUND8 84 162 3:31 1 0.533 A BB 6298. 9.781 NG 0.349 43 128 2: 46 1 0. 421 A BB 3O226. 132. 894 NG 4. 6410 NOT FOUND11 96 123 2:40 1 0. 4O5 A BB 139635. 225.844 NG 7.8812 63 225 4: 52 1 0. 740 A BB 194293. 139. 604 NG 4. 8713 NOT FOUND14 NOT FOUND15 62 366 7:56 1 1.204 A BB 863. 1.061 NG O. 0416 43 294 6:22 1 0.967 A BB 1108. 2.730 NG O. 1017 97 327 7: 05 2 0. 8OO A BB 5O7774. 671 734 NG 23. 4518 117 327 7:O5 2 0. 80O A19 NOT FOUND20 NOT FOUND i J21 NOT FOUND r ?22 NOT FOUND23 130 426 9:14 2 1.042 A BB 25983. 32.612 NG 1.1424 NOT FOUND25 97 589 12:46 2 1.440 A BB 2497. 3.319 NG O. 1226 NOT FOUND27 NOT FOUND28 NOT FOUND29 43 541 11:43 3 0. SOI A BB 4482. 4.567 NG 0.1630 NOT FOUND31 NOT FOUND32 NOT FOUND33 92 546 1 1 : 50 3 0. 809 A BB 976. 0. 884 NG 0. 0334 NOT FOUND35 NOT FOUND36 NOT FOUND37 NOT FOUND38 98 540 11:42 3 O. 8OO A BB 407677. 253.102 NG 8.8439 95 796 17:15 3 1.179 A BB 347224. 243.146 NG 8.4940 65 360 7:48 1 1.184 A BB 181072. 243.662 NG 8.5141 NOT FOUND42 NOT FOUND43 NOT FOUND44 NOT FOUND45 146 915 19:49 3 1.356 A BB 1747. O. 926 NG O. O346 NOT FOUND47 NOT FOUND48 NOT FOUND49 NOT FOUND50 96 283 6:08 1 O. 931 A BB 30034. 43.924 NG 1.53

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VOLATILE ORGAN I CS ANALYSIS DAT. r.;i£ET

74-87-3 ——————Chlorome thane7.4-83 -9---------Bromome thane75-01-4- ——— ——— Vinyl Chloride75-00-3 ———————Chloroe thane75-09-2 ———— ———Methy.lene. Chloride67-64-1---------Acetone75-15-0———————Carbon Disulfide75-35-4---------1,1-Dichloroethene75-34-3 ——— ———1, l.-D.i ch l_proe t hane540-59-0—————— 1,2-Pichloroethene (total)67-66-3--—-----Chloroform107-06-2 — ————1, 2-Di chloroe thane78-93-3 ————— --2-Bu t_an. o_n_g.__._71-55-6 ——— ———1,1. l-Trichloroethane56-23-5- — - ———Carbon JTetrachloride75-2'T-4---------Brotnodich 1 oromet hane78-87-5---------,1 , 2-Dichloropropane10061-0l-5------cis-1.3-DichIgropropene79-01-6------—r.Tr i chloroe thene.124-48-1 — — — --Dibromochloromethane'9-00-5-—-——--1.1,2-Trichloroethane1-43-2---------B e nzene

._!0.061-02-6---—-trans-1 , 3-Di.chloropropene75-25-2---- — --_-B.romoform108-10-1-—————4-Methvl -2 -Pen t a none59i-"S-D--------2-Hexanone12"- 1 S-4--------Tetrachloroethene:9-34-5-----— --1 . 1 ,.2.i_2_-Te.t r a.ch 1 g roe than e108-88-3 — ————Toluene ..__,___IPS-90-7 —— --——Ch l.o r_gb e n.z e .ne..._100-41-4——————Ethy 1 b e nz en_e.100-42-5 ——— -_--Stvrene1330-20-"—————Xv 1 ene_ It o t a 1

330. ,'U330.!U330.,'U330. !U330. !U_330. |U140330.!Uago.330.If330.|U330. IU260330330.!U330.!U

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Lab Name : WADSWORTH/ALERT Con t rac t : 6S-D1 -OOS5 ____ ...

Lab CoderVVADS Case Xo.:S""3~6 SAS N'o . : SDG Xo.:EQ3-l

Matrix: (soil /water) WATER Lab Sample ID:42"~llOi

Sample wt/vol: 5.00 (s/ml) ML Lab File ID: VOL99S5


% Moisture: not dec. Date Analyzed: 2/0"/92


Soil Extract Vo 1 ume : 0 ( uL ) Soil Aliquot Vo 1 ume : 0 (uL

CONCENTRAT I ON UN ITS:CAS NO. COMPOUND (ug/L or ug/Kg ) UG/L Q

330. It-330. JU330. !f330. I U330. It-330330.!f

ftR307392 000076

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Lab Name:WADSWORTH/ALERT Cont rac t: 6S-D1-OOS5 |____________',

Lab Code: WADS Case No.:ST376 SAS N'o. : SDG No.:EQB-l

Matrix: (soil/water) WATER Lab Sample ID:42""1101

Sample wt/vol: 5.00 (g/ml) ML Lab File ID: VOL99S5






CAS NUMBER

1.2.3.4.5.6.7 .8. ' '9.10.11 .12.13.14.15.16.17.18.19.20.21 .-?->23.24.->=;26.27.28.29.30.

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AMOUNT=AREA * REF AMNT/<REF AREA * RESP FACT)Rssp. fac. from Library Entry

No Name1 BROMOCHLOROMETHANE2 1,4-DIFLUOROBENZENE3 CHLOROBENZENE-D54 CHLOROMETHANE5 BROMOMETHANE6 VINYL CHLORIDE7 CHLOROETHANE8 METHYLENE CHLORIDE9 ACETONE10 CARBON DISULFIDE11 1,1-DICHLOROETHENE12 1,1-DICHLOROETHANE13 1,2-DICHLOROETHENE (TOTAL)14 CHLOROFORM15 1,2-DICHLOROETHANE16 2-BUTANONE17 1,1,1-TRICHLOROETHANEIS CARBON TETRACHLORIDE19 VINYL ACETATE20 BRQMODICHLOROMETHANE21 1,2-DICHLOROPROPANE22 CIS-1,3-DICHLOROPROPENE23 TRICHLOROETHENE24 DIBROMOCHLORDMETHANE25 1,1,2-TRICHLOROETHANE26 BENZENE27 TRANS-1,3-DICHLOROPROPENE23 BROMOFORM29 4-METHYL-2-PENTANONE30 2-HEXANONE31 TETRACHLOROETHENE32 1,1,2, 2-TETRACHLOROETHANE33 TOLUENE34 CHLOROBENZENE35 ETHYLBENZENE36 STYRENE37 XYLENES38 TOLUENE-DS39 BROMOFLUOROBENZENE40 1,2-DICHLDROETHANE-D441 2-CHLOROETHYL VINYL ETHER42 XYLENE (TOTAL)43 1,3-DICHLOROBENZENE44 1,2-DICHLOROBENZENE45 1,4-DICHLOROBENZENE46 ACROLEIN47 ACRYLONITRILE

00007SHR307395

;;jq .2 me • , . - • - - • • . • •48 TRICHLOROFLUOROMETHANE49 DICHLORODIFLUOROMETHANE50 CIS-1,2-DICHLOROETHENE

No m/z Scan Time Ref RRT Meth Area(Hght) Amount /iTot1 128 299 6:22 1 1.000 A BB 20759. 250.000 NG 10.482 114 4O2 3:34 2 l.OOO A BB 78349. 25O. OOO NG 1O. 483 117 664 14: O9 3 l.OOO A BB 65306. 250.000 NG 10.484 NOT FOUND5 NOT FOUND6 NOT FOUND7 NOT FOUNDS NOT FOUND9 43 126 2: 41 1 0. 421 A BV 473. " Kl. 493 NG 0. 4810 NOT FOUND11 96 118 2:31 1 0.395 A BB 2251. 20.594 NG 0.8612 63 221 4: 43 1 0. 739 A BB 73. 0. 310 NG 0. Ol13 NOT FOUND14 NOT FOUND15 NOT FOUND16 43 288 6:08 1 0.963 A BB 299. 4.251 NG 0.1817 97 321 6:50 2 0.799 A BB 9900. 39.079 NG 1.64IS NOT FOUND19 43 237 5:03 2 0.590 A BB 51. 0. 138 NG 0.0120 NOT FOUND21 NOT FOUND22 NOT FOUND23 130 419 8:56 2 1.042 A BB 99241. 737.864 NG 3O. 9224 NOT FOUND25 97 580 12:21 2 1.443 A BB 79. 0.706 NG 0. O326 NOT FOUND27 NOT FOUND28 NOT FOUND29 43 531 11:19 3 0.800 A BB 1061. 4.701 NG 0.2030 NOT FOUND31 164 585 12:28 3 0.881 A BB 32. 0.245 NG 0.0132 NOT FOUND33 NOT FOUND34 112 666 14:11 3 1.003 A BB 49. 0.198 NG 0.0135 NOT FOUND36 NOT FOUND37 NOT FOUND38 98 531 11:19 3 0. 8OO A BB 68253. 246.104 NG 1O. 3139 95 732 16:40 3 1.178 A BB 57006. 222.123 NG 9.3140 65 353 7:31 1 1.181 A BV 53767. 216.203 NG 9.0641 NOT FOUND42 106 731 15:34 3 1.101 A BB 82. 0.543 NG 0.0243 NOT FOUND44 NOT FOUND45 NOT FOUND46 NOT FOUND47 NOT FOUND48 NOT FOUND49 NOT FOUND50 96 279 5:57 1 0.933 A BV 13053. 131.973 NG 5.53

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Lab Name:WADSWORTH/ALERT Contract:68-D1-OOS5MW16BF

74-8'7-3 ——————Chlorome thane"4-83-9---------Bromomethane75-01-4 ——— — -—Vinyl Chloride75-00-3-------—Ch1orge thane75-09-2 ———————Methylene Chloride67-64-1 ———————Acetone75-15-0 — —— -——Carbon Bisulfide75-35-4---------1,1-Di c hloroethene75-34-3 ——— — — -1,1-Dichloroethane540-59-0——————1,2-Dichloroethene (total67-66-3---------Chloroform10?-06-2 ————— --1, 2-Di chloroe thane78-93-3 —— ————— 2-Butanone71-55-6---------1,1,1-Trichloroethane56-23-5—--—-—Carbon Tetrachloride75-27-4---------Bromodichloromethane78-8"-5---------l,2-Pichloropropane_10061-'01-5------cis-1.3-Dichloropropene79-01-6———————Trichloroethene124-48 - 1 ------- -D i b rprnoc h 1 o r ome t hane"9-00-5———————1. 1 , 2-Trichlproe_t_hane_'l-43-2---------Benzene __10061-02-6 - - -.---t ran s-1 . 3-Dich _loropropene._"5-25-2---------Brpmoform

j_0S- 10- l — —— - — 4-Me t hy 1 -2-Pent anone.591-"S-6 ———— —— 2-Hexanone12"-IS-4--—----Tetrachloroethene'9-34-5-------—1.1.2-2-Tetrachloroethane108-SS-j——---—Toluene108-90------——Chiorobenzene100-41-4- — ———— Ethvlbenzene100-42-5 —— ———— Stvrene1330-20-" — — —— Xylene .(.total)

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Lab Code:WADS Case No.:S"3~6 SAS No.: SDG No.:EQB-i

Matrix: (soil/water) WATER Lab Sample ID:42"~5101 .

Sample wt/vol: 5.00 (g/ml) ML Lab F i l e ID: VOE1991


°S Moisture: not dec. Date Analyzed: 2/06/92

GC Column:DB624 ID: 0.53 (mm) Dilution Factor: 6.~

Soil Extract Volume:0 (uL) Soil Aliquot Volume:0 ( uL)


OOOOS9

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Lab Name:WADSWORTH/ALERT Contract:68-D1-OOS5 !.______

Lab Code: WADS Case N'o.:S"376 SAS Xo. : SDG No.:EQB-l

Matrix: (soi1/water) WATER Lab Sample ID:42"5101

Sample wt/vol: 5.00 (g/ml) ML Lab F i l e ID: VOE1991



GC Column:DB624 ID: 0.53 (mm) Dilution Factor: 6.6"



CAS NUMBER

1 .->3.4.5.6.7 .8.9.10.11 .12.13.14.15.16.17.18.19.20.21 .22.23.24.25.26.0 ~!

28.29.30.

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Data: VOE1991. TI02/06/92 15: 54: 00Samole: 42775101, MW1&EF, 750UL/5MLConds.: 51000OFormula: Instrument: 5100 Weight: 0. 004

i. _ mi t ted by. Analyst: RQ Acct. No. :

AMOUNT=AREA * REF AMNT/CREF AREA * RESP FACT)R < ? _ p . fac. from Library Entry

No Name1 BROMOCHLOROMETHANE2 I/4-DIFLUOROBENZENE3 CHLOROBENZENE-D54 CHLOROMETHANE5 BROMOMETHANE6 VINYL CHLORIDE7 CHLOROETHANE8 METHYLENE CHLORIDE9 ACETONE10 CARBON DISULFIDE11 1,1-DICHLOROETHENE12 1,1-DICHLOROETHANE13 1, 2-DICHLOROETHENE (TOTAL)14 CHLOROFORM15 1,2-DICHLORQETHANE16 2-BUTANONE17 1,1,1-TRICHLOROETHANEIS CARBON TETRACHLORIDE19 VINYL ACETATE20 BROMODICHLOROMETHANE21 1,2-DICHLOROPROPANE22 CIS-1, 3-DICHLOROPROPENE23 TRICHLOROETHENE24 DIBROMOCHLOROMETHANE25 1,1,2-TRICHLORQETHANE26 BENZENE27 TRANS-1,3-DICHLOROFROPENE28 BROMOFORM29 4-METHYL-2-PENTANONE30 2-HEXANONE31 TETRACHLOROETHENE32 1,1,2, 2-TETRACHLOROETHANE33 TOLUENE34 CHLOROBENZENE35 ETHYLBENZENE36 STYRENE37 XYLENES38 TOLUENE-D839 BROMOFLUOROBENZENE40 1,2-DICHLOROETHANE-D441 2-CHLORQETHYL VINYL ETHER42 XYLENE (TOTAL)^3 1,3-DICHLOROBENZENE44 1,2-DICHLQROBENZENE45 1, 4-DICHLOROEENIENE46 ACROLEIN47 ACRYLONITRILE

000092&R307W8

<Mo Name43 TRICHLQRQFUJORQMETHANE43 DICHLDRODIFLUOROMETHANE50 CIS-1, 2-DICHLOROETHENE

N. m/z Scan Time Ref RRT Meth Area(Hght) Amount XTot1 128 305 6:36 1 1.000 A BB 126872. 250.000 NG 10,052 114 4O9 8:52 2 l.OOO A BB 458609. 250.000 NG 10.053 117 675 14:37 3 1,000 A BB 431617. 250.000 NG 10.054 NOT FOUND5 NOT FOUND6 NOT FOUND7 NOT FOUNDS 84 165 3:34 1 0.541 A BB 1583. 2.216 NG 0.099 43 128 2:46 1 0.420 A BB 81756. 280.356 NG 11.2710 76 141 3:03 1 0.462 A BB 5958. 2.884 NG 0.1211 96 125 2:42 1 0.410 A BB 5253. 8.233 NG 0.3312 63 226 4: 54 1 0. 741 A BB 687. 0. 448 NG 0. 0213 NOT FOUND14 NOT FOUND15 NOT FOUND16 NOT FOUND17 97 327 7:O5 2 0. 8OO A BB 20492. 25.665 NG 1.0318 NOT FOUND19 NOT FOUND20 NOT FOUND21 NOT FOUND22 NOT FOUND23 130 426 9:14 2 1.042 A BB 440201. 540.598 NG 21.7424 NOT FOUND25 NOT FOUND26 NOT FOUND27 NOT FOUND28 NOT FOUND29 43 541 11:43 3 0.801 A BB 3930. 3.529 NG 0.1430 NOT FOUND31 NOT FOUND32 NOT FOUND33 NOT FOUND34 NOT FOUND35 NOT FOUND36 NOT FOUND37 NOT FOUND38 98 540 11:42 3 0. SOO A BB 471566. 238.681 NG 9.6039 95 795 17: 13 31. 178 A BB 388913. 237. 542 NG 9. 554O 65 360 7:48 1 1.180 A BB 204932. 228.088 NG 9.1741 NOT FOUND42 NOT FOUND43 NOT FOUND44 NOT FOUND45 NOT FOUND46 NOT FOUND47 NOT FOUND4S NOT FOUND49 NOT FOUND50 96 284 6:09 1 0.931 A BB 121381. 168.682 NG 6.78

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Lab Name:WADSWORTH/ALERT Contract:6S-D1-OOS5MW17 AW

Lab Code:WADS Case No.:S"3~6 SAS No.: SDG No.:EQB-l

Matrix: (soil/water) WATER Lab Sample ID:42"601Q1

Sample wt/vol: 5.00 (g/ml) ML Lab File ID: VOE1971

Level: (Icw/med) LOW Date Received: 1/30/92





74-S7-3-- -----74— 83-Q-------l t — Qj — y — — — — — — —75-01-4 — —— —75-00-3 —————7 C_fiQ_ 0 — ____ _ _

67-64-1 —————75-15-0 — —— —75-35-4 ——————75-34-3 — — ——5 4. 0 _ 5 Q - 0 - -•J w *J -X v/

£ 7 £ fi 1

107-06-2 —————7Q_Q'5_1_ __ _

71-55-6--- ———56-23-5 —————75-27-4 —————7£ — Q7_ ^____-. — _

10061-01-5 ———*7 Q A 1 £. _

124-48-1- — ——79-00-5 ——————71-43-2 ——————10061-02-6 ———

--Bromome thane--Vinyl Chloride--Chloroe thane

1'JwL.ll.yj.wllw VwJJlWJ.iVJ.w

n *— c- uwiiv— Carbon Bisulfide--1 . 1-Di chloroeth'ene--1 , 1-Dichloroethane--1 , 2-Dichloroethene (total)--Chloroform--1 ,2-Dichloroethane--2-Butanone--1 ,1 , 1-Trichloroethane— Carbon Tetrachloride--Bromodi chlorome thane— 1 ,2-Dichloropropane--cis-1-. 3-Dichloropropene— Trichloroethene--Dibromochl oromet hane--1 , 1 ,2-Trichloroethane--Benzene--trans-1 , 3-Dichloropropene

75-25-2---------Bromof orm108-10-1 —————col _~9_(S_____j y i — , o — o — — —1O 7 1 Q -1

— n •; 1 r _ _i y o •+ j — ~ — —t r\ c Q G ^1 n Q Q n — _100-41-4------1 00-4"'-*-----1 V V *T M

1330-20-' ————

--4-Methyl-2-Pentanone--2-Hexanone

i c u i d v_, n i u i u c t n c n c--i , 1 ,2.2-Tetrachloroethane--Toluene--Chiorobenzene--Ethy Ibenzene

t y j. w 11 w— Xylene ( total )

i r\i U .

10.10.10.10.69.10.10.10.10.10.10.10.10.10.10.10.10.10.10.10.

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•"'To'L l i'i-T OKO?,,,.._i ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

Lab Name:WADSWORTK/ALERT Contract:6S-D1-0085MWl'AW

Lab CoderWADS Case No.:87376 SAS No.: SDG No.:EQB-1




<£ Moisture: not dec. 0 Date Analyzed: 2/05/92




O

CAS NUMBER

1 .2.3.4.5.6.7.8.g ^10.11.12.13.14.15.16.17.18.19.20.21.o ->23.24.25.26.27.28.29.30.

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Data: VOE1971. TI02/05/92 23: 33: 00Sample: 42760, MW17AW, 5MLConds. : 51OOOOFormula: Instrument: 51OO Weight: 0. 004Submitted by: Analyst: RQ Acct. No.:

AMOUNT=AREA * REF AMNT/<REF AREA * RESP FACT)Resp. fac. from Library Entry

No Name1 BROMOCHLOROMETHANE2 1, 4-DIFLUOROBENZENE3 CHLQROBENZENE-D54 CHLOROMETHANE5 BROMOMETHANE6 VINYL CHLORIDE7 CHLOROETHANE8 METHYLENE CHLORIDE9 ACETONE10 CARBON DISULFIDE11 1, 1-DICHLOROETHENE12 1, 1-DICHLOROETHANE13 1, 2-DICHLOROETHENE < TOTAL)14 CHLOROFORM15 1, 2-DI CHLOROETHANE16 2-BUTANONE17 1*1, 1-TRICHLOROETHANE18 CARBON TETRACHLORIDE19 VINYL ACETATE20 BROMOD I CHLOROMETHANE21 1,2-DICHLOROPROPANE22 CIS-1, 3-DICHLOROPROPENE23 TRICHLOROETHENE24 D I BROMOCHLOROMETHANE25 1,1, 2-TR I CHLOROETHANE26 BENZENE27 TRANS-1, 3-DICHLOROPROPENE28 BROMOFORM29 4-METHYL-2-PENTANONE30 2-HEXANONE31 TETRACHLOROETHENE32 1,1,2, 2-TETRACHLOROETHANE33 TOLUENE34 CHLOROBENZENE35 ETHYLBENZENE36 STYRENE37 XYLENES38 TOLUENE-D839 BROMOFLUOROBENZENE40 1, 2-DICHLOROETHANE-D441 2-CHLOROETHYL VINYL ETHER42 XYLENE (TOTAL)43 1,3-DICHLOROBENZENE44 1,2-DICHLOROBENZENE45 1,4-DICHLOROBENZENE46 ACROLEIN47 ACRYLONITRILE

000105

No Name48 TRICHLOROFLUOROMETHANE49 DICHLORODIFLUOROMETHANE50 CIS-1,2-DICHLOROETHENE

No m/z Scan Time Ref RRT Meth Area<Hght) Amount r.Tot1 128 3O4 6:35 1 l.OOO A BB 114984. 250.000 NG 13.602 114 4O9 8:52 2 l.OOO A BB 399724. 250.000 NG 13.603 117 675 14:37 3 l.OOO A BB 373032. 250.000 NG 13.604 NOT FOUND5 NOT FOUND6 NOT FOUND7 NOT FOUND8 NOT FOUND9 43 128 2:46 1 0.421 ABB 80270. 342. 662 NG 18.641O NOT FOUND11 NOT FOUND12 NOT FOUND13 NOT FOUND14 NOT FOUND15 NOT FOUND16 NOT FOUND17 97 327 7:05 2 0.800 A BB 2O35. 2.622 NG O. 1418 NOT FOUND19 NOT FOUND20 NOT FOUND21 NOT FOUND22 NOT FOUND23 130 426 9:14 2 1. O42 A BB 1211. 1.481 NG 0. OS24 NOT FOUND25 NOT FOUND26 78 361 7:49 2 O. 883 A BB 3319. 1. 9O4 NG 0.1027 NOT FOUND28 NOT FOUND29 43 540 11:42 3 0. 8OO A BB 3910. 3.916 NG 0.2130 NOT FOUND31 NOT FOUND32 NOT FOUND33 92 546 11:50 3 0.809 A BB 2630. 2.342 NG 0.1334 112 677 14: 4O 3 1. OO3 A BB 6020. 3.513 NG 0.1935 NOT FOUND36 NOT FOUND37 NOT FOUND38 98 540 11:42 3 0. 80O A BB 414174. 252.786 NG 13.7539 95 796 17:15 3 1.179 ABB 336823. 231. 873 NG 12.6140 65 359 7:47 1 1.181 A BB 187206. 244.592 NG 13.3141 NOT FOUND42 NOT FOUND43 NOT FOUND44 NOT FOUND45 146 915 19:49 3 1.356 A BB 1355. 0.706 NG 0.0446 NOT FOUND47 NOT FOUND48 NOT FOUND49 NOT FOUND50 NOT FOUND •

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1A " - - -.- '- L.!-* i AMPLE Nv. ,VOLATILE ORGAN ICS ANALYSIS DATA SHEET

Lab Name:WADSWORTH/ALERT Contract:6S-D1-0085MW17BF

74-83-9---------Bromomethane75-01-4———————Vinyl Chloride75-00-3---————Chloroe thane75-09-2———————Methvlene Chloride67-64-1---------Acetone75-15-0-——————Carbon Bisulfide75-35-4 ———— -—l . 1-Dichloroethene75-34-3-------—1,1-Dichloroethane540-59-0- ——— ——1.2-Dichloroethene (total)67-66-3- ——————Chloroform107-06-2- —— — —1,2-Dichloroethane78-93-3 — ————— -2-Butanone71-55-6---------1,!,1-Trichloroethane56-23-5—-------Carbon Tetrachloride75-27-4---------Bromodi chloromethane78-87-5--—————1, 2-Dichloropropane10061-01-5------cis-1.3-DichIoropropene79-01-6---—-——Trichloroethene124-48-1--------Pibromochloromethane79-00-5----————1,1,2-Trichloroethane71-43-2- ——— ———Benzene10061-02-6—----trans-1.3-Dichloropropene75-25-2-- — ——— -Bromoform108-10-1 ——— - —— 4-Methyl-2-Penta none591-7S-6--- — ---2-Hexanon e127-18-4--------Tetrachloroethene'9-34-5---------l,l,2.2-TetrachIoroethane10S-S8-3--------Toluene108-90-"---—---Chiorobenzene100-41-4--------EthyIbenzene100-42-5--------Styrene1330-20-"- — — — Xylene _i_tp_ta_l.

10 . ! u10 . i.10. !U10 . .' U10. !U62.! B29. !i o.! u10i o.! u10. ! u10. !u10. !u10. i u10. ! u10. JU10. ! u10 . I U10. |U10 . j U10. !U10. ! u1 0 . ! U1010. ! U10. ! u10. JU10. ! u10. ! u1010 . .' U10. ! ui o.! u

Lab CoderWADS _ Case No.:?"376 SAS No.: SDG No.:EQB-l

Matrix: (soil/water) WATER Lab Sample ID:42'763101

Sample wt/voi: 5,00 (g/ml) ML Lab File ID: VOE1972






BR307U25 000i09

• JL-ATH.E ORGAN ICS ANALYSIS DATA SHEET _______TENTATIVELY IDENTIFIED COMPOUNDS !

I MW17BFLab Name:WADSWGRTH/ALERT Con t rac t : 68-D1-0035 ',______

Lab Code:WADS Case No.:S73~6 SAS No.: SDG No.:EQB-l

Matrix: (soi1/water) WATER Lab Sample ID:42763101







CAS NUMBER

1.2.3.4.5.6.1 .8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.


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Data: VOE1972. TI02/06/92 0:08:00Sample: 42763, MW17BF, 5MLConds.: 51OOOOFormula: Instrument: 51OO Weight: O. 004Submitted by: Analyst: RQ Acct. No. :

AMOUNT=AREA * REF AMNT/(REF AREA * RESP FACT)Resp. fac. from Library Entry

No Name1 BROMOCHLOROMETHANE2 I. 4-DIFLUOROBENZENE3 CHLOROBENZENE-D54 CHLOROMETHANE5 BROMOMETHANE6 VINYL CHLORIDE7 CHLOROETHANE8 METHYLENE CHLORIDE9 ACETONE1O CARBON DISULFIDE11 1,1-DICHLOROETHENE12 1, 1-DICHLOROETHANE13 1«2-DICHLOROETHENE (TOTAL)14 CHLOROFORM15 1,2-DICHLOROETHANE16 2-BUTANONE17 1,1,1-TRICHLOROETHANE18 CARBON TETRACHLORIDE19 VINYL ACETATE2O BROMODICHLOROMETHANE21 1,2-DICHLOROPROPANE22 CIS-1,3-DICHLOROPROPENE23 TRICHLOROETHENE24 DIBROMOCHLOROMETHANE25 1,1,2-TRICHLOROETHANE26 BENZENE27 TRANS-1,3-DICHLOROPROPENE28 BROMOFORM29 4-METHYL-2-PENTANONE3O 2-HEXANONE31 TETRACHLOROETHENE32 1,1,2,2-TETRACHLORQETHANE33 TOLUENE34 CHLOROBENZENE35 ETHYLBENZENE36 STYRENE37 XYLENES38 TOLUENE-D839 BROMOFLUOROBENZENE4O 1,2-DICHLOROETHANE-D441 2-CHLOROETHYL VINYL ETHER42 XYLENE (TOTAL)43 1,3-DICHLOROBENZENE44 1,2-DICHLOROBENZENE45 1,4-DICHLOROBENZENE46 ACROLEIN47 ACRYLONITRILE

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N o N e > - . « - '43 TRI'wriLOROFLUOROMETHANE49 DICHLORODIFLUOROMETHANE50 CIS-1,2-DICHLOROETHENE

No m/z Scan Time Ref RRT Meth Area(Hght) Amount XTot1 128 303 6:34 1 1.000 A BB 112153. 250. OOO NG 12.702 114 4O8 8: SO 2 1.000 A BB 41O541. 25O. OOO NO 12.703 117 674 14:36 3 1.000 A BB 381480. 250.000 NG 12.704 NOT FOUND5 NOT FOUND6 NOT FOUND7 NOT FOUND8 84 162 3:31 1 0.535 A BB 2019. 3.121 NG 0.169 43 127 2:45 1 0.419 A BB 70245. 307.436 NG 15.6210 76 139 3:01 1 0.459 A BB 259969. 145.110 NG 7.3711 NOT FOUND12 NOT FOUND13 NOT FOUND14 NOT FOUND15 NOT FOUND16 43 292 6: 2O 1 O. 964 A BB 2O28. 4.975 NG O. 2517 97 325 7:02 2 0.797 A BB 945. 1.186 NG 0.0618 NOT FOUND19 NOT FOUND20 NOT FOUND21 NOT FOUND22 NOT FOUND23 13O 425 9:12 2 1.O42 A BB 1945. 2.315 NG 0.1224 NOT FOUND,25 NOT FOUND

78 36O 7:48 2 0.882 A BB 3719. 2.078 NG O. 1127 NOT FOUND28 NOT FOUND29 43 540 11:42 3 0. 8O1 A BB 4765. 4.667 NG 0.2430 NOT FOUND31 NOT FOUND32 NOT FOUND33 92 545 11: 48 3 O. 809 A BB 5470. 4. 763 NG 0. 2434 112 677 14:40 3 1. OO4 A BB 5255. 2.999 NG O. 1535 1O6 706 15:18 3 1.047 A BB 23O9. 3. 28O NG O. 1736 NOT FOUND37 106 706 15:18 3 1.047 A BB 23O9. 2.379 NG O. 1238 98 539 11:41 3 0.800 A BB 424563. 253.389 NG 12.8839 95 795 17:13 3 1.180 A BB 348022. 234.277 NG 11.914O 65 358 7:45 1 1.182 A BB 182247. 244.124 NG 12.4141 NOT FOUND42 106 743 16:06 3 1.102 A BB 728. 0.711 NG O. 0443 146 9O4 19:35 3 1.341 A BB 491. 0.261 NG O. 0144 NOT FOUND45 146 915 19:49 3 1.358 A BB 1468. 0.748 NG O. 0446 NOT FOUND47 NOT FOUND48 NOT FOUND49 NOT FOUND5O NOT FOUND

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• s..- "';; I,* *%-:*.. «3A "'-: J E?A SAMPLE .\0.VOLATILE ORGAN" ICS ANALYSIS DATA SHEET _____________________

\ MW20AALab Name:WADS\VORTK/ALERT Contract : 6S-D1-0085 !______

74-87-3——---——Chloromethane74-83-9---—----Bromomethane75-01-4———————Vinyl Chloride75-00-3-——————Chloroethane75-09-2——--—-Methylene Chloride67-64-1 ——— —— —Acetone75-15-0———————Carbon Disulfide75-35-4--- —— -—1,1-Dichloroethene75-34-3--- — --—1 .1-Dichloroethane540-59-0 —— ———— 1,2-Dichloroethene (total)67-66-3—-------Chloroform107-06-2- —— — — 1,2-Dichloroethane78-93-3 ———— —— 2-Butanone71-55-6 ——— --——1,1,1-Trichloroethane56-23-5——-—-—Carbon Tetrachloride75-27-4---------Bromodichloromethane78-87-5---------1,2-Dichloropropane10061-01-5------cis-1.3-Dichloropropene79-01-6----—---Trichloroethene124-48-l--------Dibromochloromethane79-00-5 —— ---——1,1,2-Trichloroethane71-43-2———————Benzene10061-02-6-———trans-1,3-Dichloropropene75-25-2----------Bromof orm108-10-1——————4-Methyl-2-Pentanone591-"8-6 —— --- — 2-Hex anone127-lS-4--------Tetrachloroethene79-34-5-—---—-1.1.2,2-Tetrachloroethane108-88-3---——--Toluene108-90-7———---Chiorobenzene100-41-4————'• — Ethyl b e nzen e.100-42-5 — —— — -Stvrene1330-20---------Xylene (tg tali.

10.10. !U10 . ! U10. !U10. !U64. ! B10. !U10.10.10.1010 . ! U10. |U_10. ! U10. !U1Q . ! Uio.it;10. !10. !i o.! u10. ! u10. ! U10. I U10 . i U10. i U101010.: u10 . ! U10. U1010. ! U10 . ! U

Lab CoderWADS Case No.:8T376 SAS No.: SDG No.:EQB-l


Sample wt/vol: 5.00 (g/ml) ML Lab File ID: VOE19T6


°S Moisture: not dec. Date Analyzed: 2/06/92




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••,-•>,.• ?/-\ *r<& •: • -; -.!t?- ' HEA SA.VPiFVOLATlLt OKvj.iNiCS AXAL'ib-S DATA SHEET ______

TENTATIVELY IDENTIFIED COMPOUNDS! MW20AA

Lab Name:WADS\VORTH/ALERT Con tract : 6S-D1-OOS5 ,'


Matrix: (soil/water) WATER Lab Sample ID:42765101






CONCENTRATION UNITS:Number TICs Found:. 0 (ug/L or ug/Kg) UG/L_

CAS NUMBER

1.2.3.4.5.6.7.S.g _10.11.12.13.14.15.16.17.18.19.20.21."i o23.24.25.26.27.28.29.30.

COMPOUND NAME

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Data: VOE1976. TI02/06/92 2:27:00Sample: 42765, MW2OAA, 5MLConds. : 510000Iormula: Instrument: 5100 Weight: 0. 004ubmitted by: Analyst: RQ Acct. No. :


No Name1 BROMOCHLOROMETHANE2 1,4-DIFLUOROBENZENE3 CHLOROBENZENE-D54 CHLOROMETHANE5 BROMOMETHANE6 VINYL CHLORIDE7 CHLOROETHANE8 METHYLENE CHLORIDE9 ACETONE1O CARBON DISULFIDE11 1,1-DICHLOROETHENE12 1,1-DICHLOROETHANE13 1,2-DICHLOROETHENE (TOTAL)14 CHLOROFORM15 1,2-DICHLOROETHANE16 2-BUTANONE17 1,1,1-TRICHLOROETHANE18 CARBON TETRACHLORIDE9 VINYL ACETATEO BROMODICHLOROMETHANE21 1,2-DICHLOROPROPANE22 CIS-l, 3-DICHLOROPROPENE23 TRICHLOROETHENE24 DIBROMOCHLOROMETHANE25 1,1,2-TRICHLOROETHANE26 BENZENE27 TRANS-1, 3-DICHLOROPROPENE28 BROMOFORM29 4-METHYL-2-PENTANONE30 2-HEXANONE31 TETRACHLOROETHENE32 1,1,2, 2-TETRACHLOROETHANE33 TOLUENE34 CHLOROBENZENE35 ETHYLBENZENE36 STYRENE37 XYLENES38 TOLUENE-DS39 BROMOFLUOROBENZENE40 1,2-DICHLOROETHANE-D441 2-CHLOROETHYL VINYL ETHER42 XYLENE <TOTAL)43 1,3-DICHLOROBENZENE44 1,2-DICHLOROBENZENE5 1,4-DICHLOROBENZENE

"46 ACROLEIN47 ACRYLONITRILE 000121

AR3Q7i*37

No Name48 TRICHLOROFLUOROMETHANE49 DICHLORODIFLUOROMETHANE50 CIS-l, 2-DICHLOROETHENE

No m/z Scan Time Ref RRT Meth Area(Hght) Amount XTot1 128 3O3 6:34 1 l.OOO A BB 95827. 25O. OOO NG 13.662 114 408 8:50 2 l.OOO A BB 349024. 250.000 NG 13.663 117 674 14:36 3 1.000 A BB 326774. 250.000 NG 13.664 NOT FOUND5 NOT FOUND6 NOT FOUND7 NOT FOUND8 84 164 3:33 1 O. 541 A BB 5018. 9. O79 NG O. 509 43 127 2: 45 1 O. 419 A BB 62O22. 317. 693 NG 17. 3510 NOT FOUND11 NOT FOUND12 NOT FOUND13 NOT FOUND14 NOT FOUND15 NOT FOUND16 43 293 6:21 1 O. 967 A BB 481. 1.381 NG O. 0817 97 326 7: O4 2 O. 799 A BB 1437. 2. 121 NG O. 1218 NOT FOUND19 NOT FOUND20 NOT FOUND21 NOT FOUND22 NOT FOUND23 NOT FOUND24 NOT FOUND25 NOT FOUND26 78 360 7:48 2 0.882 A BB 521. O. 342 NG O. 0227 NOT FOUND28 NOT FOUND29 43 540 11:42 3 O. 8O1 A BB 8331. 9.526 NG 0.5230 NOT FOUND31 NOT FOUND32 NOT FOUND33 92 545 11: 48 3 0. 809 A BB 922. 0. 937 NG O. 0534 NOT FOUND35 NOT FOUND36 NOT FOUND37 NOT FOUND38 98 539 11:41 3 O. 800 A BB 365972. 254.987 NG 13.9339 95 795 17:13 3 1.180 ABB 300250. 235. 956 NG 12.8940 65 359 7:47 1 1.185 A BB 157944. 247.614 NC 13.5341 NOT FOUND42 NOT FOUND43 NOT FOUND44 NOT FOUND45 146 914 19:48 3 1.356 A BB 1854. 1.103 NG 0.0646 NOT FOUND47 NOT FOUND48 NOT FOUND49 NOT FOUND50 NOT FOUND

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Lab Name:WADSWORTH/ALERT Contract:6S-D1-0085MW20AB

74-87-3———————-Chl oromet hane74-83-9---------Bromomethane75-01-4———————Vinyl Chloride75-00-3———————Chloroe thane75-09-2----—---Methylene Chloride67-64-1-——————Acetone75-15-0-——————Carbon Disulfide75-35-4--—--—-1,1-Dichloroethene75-34-3-- — ---—1 ,1-Dichloroethane540-59-0-- —— - — 1,2-Dichloroethene (total)67-66-3 ———— -——Chloroform107-06-2— ———— 1, 2-Di chloroe thane78-93-3 ——————— 2-Butanone71-55-6————— —1.1, 1-Trichloroethane56-23-5-——---—Carbon Tetrachloride75-27-4---------Bromodichloromethane78-87-5 ——————— 1, 2-Dich Ip. r op r opane10061-01-5------cis-1.3-Dichloropropene79-01-6——————Trichloroethene124-48-l--------Dibromochloromethane79-00-5 — - — - — -1.1,2-Trichloroe thane71-43-2———————Benzene10061-02-6——:——trans-1,3-Dichloropropene75-25-2 ————— --Bromoform108-10-1 —————— 4-Methyl-2-Pentanone591-78-6--- ———— 2-Hexanone127-18-4----—--Tetrachloroethene79-34-5---------l.l,2.2-Tetrachloroethane108-88-3———————Toluene108-90-7——-----Chiorobenzene100-41-4 ——— ——— Ethyl benzene100-42-5 ——— —— - J tvrene1330-20-"—————Xylene (total)

10. ! U10.10. |U10. JU10. !U65. ! B10 . ! U1010 . ! U10 . ! U10. !U10 . ! U10 . ! U10. ! U10. !U10 . ! U10. ! U10. ! U30. !10. ! U10. ! U10. !U10. iU10. |u10. IU10. |u_i o. ! u10. !U_10. ! u10. !u1010i o.; u

Lab Code:WADS Case No.:S7376 SAS No.: SDG N"o.:EQB-l

Matrix: (soil/water) WATER Lab Sample ID:42~66101



* Moisture: not dec. Date Analyzed: 2/06/92




000125AR307I.M

"•' " :' VOLATILE ORGAN ICS AN'ALYSio ' ;.,,.. iTENTATIVELY IDENTIFIED COMPOUNDS

Lab Name:WADSWORTH/ALERT Contract:6S-D1-OOS5MW20AB









CAS NUMBER

1.2.3.4.5.6.7.S.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.


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Data: VOE1977. TI02/06/92 3:02:00Sample: 42766, MW20AB, 5MLConds. : 510000Formula: Instrument: 510O Weight: 0. 004Submitted by: Analyst: RQ Acct. No.:


toNo Name1 BROMOCHLOROMETHANE2 I/4-DIFLUOROBENZENE3 CHLOROBENZENE-D54 CHLOROMETHANE5 BROMOMETHANE6 VINYL CHLORIDE7 CHLOROETHANE8 METHYLENE CHLORIDE9 ACETONE10 CARBON DISULFIDE11 li 1-DICHLOROETHENE12 1,1-DICHLOROETHANE13 1, 2-DICHLOROETHENE (TOTAL)14 CHLOROFORM15 1,2-DICHLOROETHANE16 2-BUTANONE17 1,1,1-TRICHLOROETHANE18 CARBON TETRACHLORIDE19 VINYL ACETATE20 BROMODICHLOROMETHANE21 1,2-DICHLOROPROPANE22 CIS-1,3-DICHLOROPROPENE23 TRICHLOROETHENE24 DIBROMOCHLOROMETHANE25 1, 1, 2-TRICHLOROETHANE26 BENZENE27 TRANS-1,3-DICHLOROPROPENE28 BROMOFORM29 4-METHYL-2-PENTANONE30 2-HEXANONE31 TETRACHLOROETHENE32 1,1,2, 2-TETRACHLOROETHANE33 TOLUENE34 CHLOROBENZENE35 ETHYLBENZENE36 STYRENE37 XYLENES38 TOLUENE-D839 BROMOFLUOROBENZENE40 1,2-DICHLOROETHANE-D441 2-CHLOROETHYL VINYL ETHER42 XYLENE (TOTAL)43 1,3-DICHLOROBENZENE44 1,2-DICHLOROBENZENE45 1,4-DICHLOROBENZENE46 ACROLEIN47 ACRYLONITRILE OQOl^S

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No Name48 TRICHLOROFLUOROMETHANE49 DICHLORODIFLUOROMETHANE50 CIS-l.2-DICHLOROETHENE

No m/z Scan Time Ref RRT Meth Area(Hght) Amount XTot1 128 303 6:34 1 l.OOO A BB 1O5691. 250. OOO NG 12.462 114 4O8 8: SO 2 l.OOO A BB 38O999. 25O. OOO NG 12.463 117 675 14:37 3 l.OOO A BB 356250. 250. OOO NG 12.464 NOT FOUND5 NOT FOUND6 NOT FOUND7 NOT FOUND8 84 163 3: 32 10. 538 A BB 4524. 7. 422 NG 0. 379 43 127 2: 45 1 O. 419 A BB 69847. 324. 385 NG 16. 161O NOT FOUND11 NOT FOUND12 NOT FOUND13 NOT FOUND14 83 319 6:55 1 1.053 A BB 1340. 1. O75 NG O. 0515 NOT FOUND16 NOT FOUND17 97 326 7:04 2 O. 799 A BB 1847. 2. 497 NG 0. 1218 NOT FOUND19 NOT FOUND20 NOT FOUND21 NOT FOUND22 NOT FOUND23 13O 426 9:14 2 1. O44 A BB 118291. 151. 74O NG 7.5624 NOT FOUND5 NOT FOUND6 78 360 7: 48 2 O. 882 A BB 6735. 4. O54 NG O. 2O27 NOT FOUND28 NOT FOUND29 43 541 11:43 3 O. 8O1 A BB 6886. 7.222 NG 0.3630 NOT FOUND31 NOT FOUND32 NOT FOUND33 92 545 11:48 3 0. 8O7 A BB 10280. 9.584 NG 0.4834 NOT FOUND35 1O6 706 15:18 3 1.046 A BB 2785. 4.236 NG O. 2136 NOT FOUND37 106 706 15:18 3 1.046 A BB 2785. 3.073 NG O. 1538 98 540 11: 42 3 0. 800 A BB 395573. 252. 807 NG 12. 6039 95 796 17:15 3 1.179 A BB 328845. 237.045 NG 11.8140 65 359 7:47 1 1.185 A BB 172163. 244.716 NG 12.1941 NOT FOUND42 1O6 744 16:07 3 1. 1O2 A BB 1O44. 1.092 NG 0.0543 NOT FOUND44 NOT FOUND45 146 915 19:49 3 1.356 A BB 1932. 1.054 NG 0.0546 NOT FOUND47 NOT FOUND48 NOT FOUND49 NOT FOUND50 96 282 6: 07 1 0. 931 A BB 3368. 5. 203 NG 0. 26

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1A ' EPA SAV/PLE NO.VOLAiiLE ORGAN ICS ANALYSIS DATA SHEET

Lab Name:WADSWORTH/ALERT Centract:6S-D1-OOS5MW20AW

74-87-3———————Chlorome thane74-83-9-—--——-Bromomethane75-01-4———————Vinvl Chloride75-00-3———————Chloroe thane75-09-2———————Methylene Chloride67-64-1---------Acetone75-15-0———————Carbon Disu 1 f i de75-35-4 —— ————— 1, 1-Dichloroethene75-34-3———————1, 1-Dichloroethane540-59-0 — ————— 1, 2-Dichloroethene (total)67-66-3———————Chloroform107-06-2——————1, 2-Di chloroe thane78-93-3 ——————— 2-Butanone71-55-6-------—1,1,1-Trichloroethane56-23-5-——----Carbon Tetrachloride75-27-4---------Bromodichloromethane78-87-5---------1,2-Dichloropropane10061-01-5————cis-1,3-Dichloropropene79-01-6 ——————Trichloroethene124-48-1----—--Dibromochloromethane79-00-5 ———————1,1,2-Tri chloroe thane71-43-2--———--Benzene10061-02-6————trans-l,3-Dichloropropene75-25-2-——————Bromoform108-10-1——————4-.Methyl-2-Pentanone591-78-6 ——— — — 2-Hexanone127-18-4——————Tetrachloroethene"9-34-5 — - — ———1.1,2.2-Tetrachloroethane108-88-3 ——————Toluene108-90-"--———Chiorobenzene100-41-4- — - — --Ethyl benzene100-42-5 ———— —— Styrene1330-20-"—-----Xvlene (total)

50. !U50. !U50. !U50. !U50. !U94.!50. !U

50. !U1450. !U50. !U50. !U50. !U50. iU50. !U50. !U50. iU

730. !50. !U50. ! U50. !U50. !U50. |U50. !U50. !U50. |U5 c.: u50. !U50. !Uso. ;u50. ! U50. iU

Lab Code:WADS Case No.:87376 SAS No.: SDG No.:EQB-1

Matrix: (soil/water) WATER Lab Sample ID:427"M101





Soil Extract Volume:0 (uL) Soil Aliquot Volume:0 (uL


C00134ftR307l*5Q

• ,'GLA? ;Ll:''ORGANics ANALYSIS DATA SHEET" .""TENTATIVELY IDENTIFIED COMPOUNDS

Lab Name:WADSWORTH/ALERT Contract:6S-D1-OOS5MW^OAW


Matrix: (soil/water) WATER Lab Sample ID:42774101







CAS NUMBER

1.2.3.4.5.6.7.S.9.10.11 .12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.

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Data: VOL1003.TIOS/07/92 14:53.00Sample: 42774101, MWZOAW, 1ML/5MLC one's. : FINN52ormula: VOC Instrument: FINN52 Weight: 0.000famitted by: WADS Analyst: JP Acct. No. : 68D10008

AMOUNT=AREA * REF AMNT/(REF AREA # RESP FACT)Resp. fac. from Library Entry

No Name1 BROMOCHLGRQMETHANE2 1, 4-DIFLUQR05ENZENE3 CHLOROBENZENE-D54 CHLOROMETHANE5 BROMOMETHANE6 VINYL CHLORIDE7 CHLOROETHANES METHYLENE CHLORIDE9 ACETONE10 CARBON DISULFIDE11 1, 1-DICHLOROETHENE12 i, 1-DICHLOROETHANE13 1,2-DICHLOROETHENE (TOTAL)14 CHLOROFORM15 1,2-DICHLOROETHANE16 2-BUTANONE17 1,1,1-TRICHLOROETHANE18 CARBON TETRACHLORIDE9 VINYL ACETATEO BROMODICHLOROMETHANE

li2-DICHLOROPROPANE22 CIS-1, 3-DICHLOROPROPENE23 TRICHLOROETHENE24 DIBROMOCHLOROMETHANE25 1,1,2-TRICHLOROETHANE26 BENZENE27 TRANS-1, 3-DICHLOROPROPENE28 BROMOFORM29 4-METHYL-2-PENTANONE30 2-HEXANONE31 TETRACHLOROETHENE32 1,1,2,2-TETRACHLOROETHANE33 TOLUENE34 CHLOROBENZENE35 ETHYLBENZENE36 STYRENE37 XYLENES38 TOLUENE-DS39 BROMOFLUOROBENZENE40 1,2-DICHLOROETHANE-D441 2-CHLOROETHYL VINYL ETHER42 XYLENE (TOTAL)43 1,3-DICHLOROBEN2ENE44 1,2-DICHLOROBENZENE5 1,4-DICHLOROBENZENE

"46 AC ROLE INACRYLON,TRILE 000137

No Name45 TRICHLOROFLuOROMEThr.,«£49 DICHLORODIFLUOROMETHANE50 CIS-1,2-DICHLDRDETHENE

No m/z Scan Time Ref RRT Meth Area(Hght) Amount y.Tot1 128 300 6:23 1 1.000 A BB 26726. 250.000 NG 10.722 114 403 8:35 2 1.000 A BB 103784. 250.000 NG 10.723 117 665 14:10 3 1.000 A BV 86781. 250.000 NG 10.724 NOT FOUND5 NOT FOUND6 NOT FOUND7 NOT FOUND3 NOT FOUND9 43 124 2:39 1 0.413 A BB 4234. 93.677 NG 4.0210 NOT FOUNDII 96 114 2:26 1 0.380 A BB 67. 0.448 NG O. 0212 NOT FOUND13 NOT FOUND14 NOT FOUND15 NOT FOUND16 43 293 6:15 1 O. 977 A BV 168. 1.951 NG O. OS17 97 323 6:53 2 0. 8O1 A BB 2641. 7.729 NG 0.3318 NOT FOUND19 NOT FOUND20 NOT FOUND *21 63 439 9:21 2 1.O89 A BB 50. O. 308 NG O. 0122 NOT FOUND23 130 420 8:57 2 1.042 A BB 116592. 727.851 NG 31.2224 NOT FOUND25 97 578 12:19 2 1.434 A BB 37. 0.264 NG O. 0126 78 356 7:35 2 O. 883 A BB 575. 1.523 NG 0.0727 NOT FOUND28 NOT FOUND29 43 533 11:21 3 O. 8O2 A BB 1641. 6.426 NG O. 2830 NOT FOUND31 NOT FOUND32 NOT FOUND33 91 537 11:26 3 0.808 A BB 2846. 7.517 NG 0.3234 NOT FOUND35 106 696 14:50 3 1.047 A BB 588. 4.784 NG O. 2136 NOT FOUND37 106 696 14:50 3 1.047 A BB 588. 3.168 NG 0.1438 98 532 11: 2O 3 O. 8OO A BB 91831. 255.636 NG 10.9739 95 783 16:41 3 1.177 A BB 77481. 232.180 NG 9.964O 65 353 7:31 1 1.177 A BB 693O3. 217.718 NG 9.3441 NOT FOUND42 106 732 15:36 3 1.101 A BB 1083. 5.635 NG 0.2443 146 889 18:56 3 1.337 A BB 56. 0.126 NG 0.0144 NOT FOUND45 146 900 19:10 3 1.353 A BB 69. 0.143 NG 0.0146 NOT FOUND47 NOT FOUND48 NOT FOUND49 NOT FOUND5O 96 2SO 5: 5S 1 O. 933 A BB 2068. 14.365 NG 0.62to

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additional monitoring wells drum burial area 1 remedial ... · mr. frank vavra 2 april 20, 1992...

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