deutsche akkreditierungsstelle gmbh appendix to ...deutsche akkreditierungsstelle gmbh appendix to...
Post on 06-Jun-2020
8 Views
Preview:
TRANSCRIPT
Deutsche Akkreditierungsstelle GmbH
Appendix to Accreditation Certificate D-PL-14082-01-00
in accordance with DIN EN ISO/IEC 17025:2005
Period of validity: 10 July 2013 to 9 July 2018 Date of issue: 10 July 2013
Holder of certificate:
LUFA-ITL GmbH
Dr.-Hell-Straße 6, 24107 Kiel
Tests in the areas:
Physical, physiochemical, chemical and microbiological analyses of water, waste water,
groundwater, surface water, water of swimming and bathing pools, water of bathing waters,
leachate, sludge, sediments and eluates; selected chemical and microbiological analyses of wastes
and waste eluates;
Chemical and microbiological analyses of drinking of drinking water according to the Drinking
Water Ordinance; analyses of mineral and medicinal water;
Analysis of water and sludge according to BEK 900 (Danish directive concerning quality
requirements in environmental measurements);
Microbiological, biomolecular, physical, physiochemical and chemical analysis of food, feeding
stuff and material of plants and animals;
Organoleptical analyses of food and feeding stuff; macroscopic, physical, chemical and biological
analyses of fertilisers;
Sampling of waste water, untreated and drinking water, water of swimming and bathing pools
and basins, mineral and medicinal water, water of standing waters, of aquifers and flowing
waters, and sewage sludge;
Specialist modules - water and waste
Abbreviations used: see last page
*) Within the * marked testing domains, the laboratory may apply standard or equivalent testing
methods not included in this certificate without prior notice to and approval of DakkS (Deutsche
Akkreditierungsstelle GmbH). The test methods cited are exemplary. The laboratory has a current
list of all test methods in the flexible accreditation domain.
Appendix to Accreditation Certificate D-PL-14082-01-00
Period of validity: 10 July 2013 to 9 July 2018 2/2
**) Within the ** marked testing domains, the laboratory may modify and develop testing
methods without prior notice to and approval of DAkkS (Deutsche Akkreditierungsstelle GmbH).
The testing methods listed are exemplary The test methods cited are exemplary. The laboratory
has a current list of all test methods in the flexible accreditation domain.
Within chapters 1-6 the laboratory is permitted to use the test methods cited here with different
revision levels of the standards, without requiring previous information and approval of the
DAkkS.
2 Analysis of water and sludge according to BEK 900 (Danish directive concerning
quality requirements in environmental measurements)
2.1 Microbiological parameters
ISO 17995
2005-06
Detection and Enumeration of thermotolerant Campylobacter
DIN EN ISO 6222
1999-07
Water quality - Enumeration of culturable micro-organisms -
Colony count by inoculation in a nutrient agar culture medium
DIN EN ISO 7899-2
2000-11
Water quality - Detection and enumeration of intestinal
enterococci - Part 2: Membrane filtration method
DIN EN ISO 16266
2008-05
Detection and Enumeration of Pseudomonas aeruginosa –
membrane filtration method
DS 266
1988-05
Vandundersoegelse. Kvalitativ og kvantitativ bestemmelse af
Salmonella i vand, slam, sediment og jord
Water quality - Qualitative and quantitative determination of
Salmonella in water, sludge, sediment and soil
DS 2255 200-01
Vandundersoegelse - Bestemmelse af coliforme bakterier og termotolerante coliforme bakterier - Fortyndingsmetoden
(MPN-metoden)
Water quality - Enumeration of coliform bacteria and
thermotolerant coliform bacteria - Multiple-tube fermentation
method (Most Probable Number-method)
DS 2256
1983-01
Vandundersoegelse. Bestemmelse af Clostridium perfringens
Water quality - Determination of Clostridium perfringens
DS 2401
1999-07
Miljoeundersoegelse. Bestemmelse af enterokokker.
Kolonitaelling paa fast substrat. Overfladeudsaed
Environmental quality - Enumeration of enterococci - Colony
count on solid medium - Spread plate method
Appendix to Accreditation Certificate D-PL-14082-01-00
Period of validity: 10 July 2013 to 9 July 2018 3/3
DS 3029
2001-11
Enumeration of Legionella – modification of ISO 11731: 1998
SS 28192
1989
Detection and Enumeration of Yeasts and Moulds
Colilert 18/Quanti-Tray Method
from IDEXX
E. coli and coliform bacteria in drinking water and ground water
2.2 Chemical Parameters
M023, M043
DIN EN 25663
1993-11
Water quality; Determination of Kjeldahl nitrogen; Method after
mineralization with selenium
DIN ISO 15923-1
2012-01
Determination of ions by a discrete analysis system and
spectrophotometric detection – Part 1: Ammonium, chloride,
nitrate, nitrite, orthophosphate, silicate and sulfate
(here: Sulfate)
M016, M019, M027
DIN ISO 15705
2003-01
Water quality - Determination of the chemical oxygen demand
index (ST-COD) - Small-scale sealed tube method
Appendix to Accreditation Certificate D-PL-14082-01-00
Period of validity: 10 July 2013 to 9 July 2018 4/4
M009, M011, M012
DIN EN ISO 6878
2004-09
Water quality - Determination of phosphorus - Ammonium
molybdate spectrometric method: digestion
M036
DIN EN ISO 7027
2000-04
Water quality - Determination of turbidity
M026
DIN EN ISO 7393-1
2000-04
Water quality - Determination of free chlorine and total chlorine -
Part 1: Titrimetric method using N,N-diethyl-1,4-phenylene-
diamine
DIN EN ISO 7393-2
2000-04 Berichtigung
2011
Water quality - Determination of free chlorine and total chlorine -
Part 2: Colorimetric method using N,N-diethyl-1,4-phenylene-diamine, for routine control purposes
M035: DS 289
1992-04
Bestemmelse af farvetal (sand farve): Determination of the Colour
index using the Pt-method
DIN EN ISO 7887
2012-04
Water quality - Examination and determination of colour
M037, M038, M039 DIN EN ISO 9963-1
1996-02
Water quality - Determination of alkalinity - Part 1: Determination of total and composite alkalinity
DIN EN ISO 10301
1997-08
Water quality - Determination of highly volatile halogenated
hydrocarbons - Gas-chromatographic methods
DIN EN ISO 10304-1
2009-07
Water quality - Determination of dissolved anions by liquid
chromatography of ions - Part 1: Determination of bromide,
chloride, fluoride, nitrate, nitrite, phosphate and sulfate
M013, M018, M024, M058
DIN EN ISO 11885
2009-09
Water quality - Determination of selected elements by inductively
coupled plasma optical emission spectrometry (ICP-OES)
M010
DIN EN ISO 11905-1
1998-08
Water quality - Determination of nitrogen - Part 1: Method using
oxidative digestion with peroxodisulfate
M008
DIN EN ISO 13395 1996-12
Water quality - Determination of nitrite nitrogen and nitrate
nitrogen and the sum of both by flow analysis (CFA and FIA) and spectrometric detection
Appendix to Accreditation Certificate D-PL-14082-01-00
Period of validity: 10 July 2013 to 9 July 2018 5/5
M034
DIN EN ISO 14403-1
2012-10
Water quality - Determination of total cyanide and free cyanide
using continuous flow analytic
M020, M021 DIN EN ISO 15587-2
2002-07
Water quality - Digestion for the determination of elements in water - Part 2: Nitric acid digestion
DIN EN ISO 15923-1
2012-01
Determination of ions by a discrete analysis system and
spectrophotometric detection – Part 1: Ammonium, chloride,
nitrate, nitrite, orthophosphate, silicate and sulfate
(here: Chloride)
M014, M015, M049
DIN EN ISO 17294-2
2005-02
Water quality - Application of inductively coupled plasma mass
spectrometry (ICP-MS) - Part 2: Determination of 62 elements
DIN EN ISO 17993
2004-03
Water quality - Determination of 15 polycyclic aromatic
hydrocarbons (PAH) in water by HPLC with fluorescence detection
after liquid-liquid extraction
M040
DIN EN 872
2005-04
Water quality - Determination of suspended solids - Method by
filtration through glass fibre filters
DIN EN ISO 12846
2012-08
Water quality – Determination of mercury – method using atom
absorption spectrometry (AAS)
M032, M033
DIN EN 1484
1997-08
Water analysis - Guidelines for the determination of total organic
carbon (TOC) and dissolved organic carbon (DOC)
M017, M042
DIN EN 1899-1
1998-05
Water quality - Determination of biochemical oxygen demand
after n days (BODn) - Part 1: Dilution and seeding method with
allylthiourea acid addition
DIN EN ISO 12673
1999-05
Water quality - Gas chromatographic determination of some
selected chlorophenols in water
M022
DIN EN 25814
1992-11
Water quality; determination of dissolved oxygen by the
electrochemical probe method
M006
DIN EN 26777
1993-04
Water quality; determination of nitrite; molecular absorption
spectrometric method
Appendix to Accreditation Certificate D-PL-14082-01-00
Period of validity: 10 July 2013 to 9 July 2018 6/6
DIN EN 27888
1993-11
Water quality; determination of electrical conductivity
DIN 38404-4 1976-12
German Standard Methods for Analysing of Water, Waste Water and Sludge; Physical and Physical-chemical Parameters (Group C);
Determination of Temperature (C 4)
DIN 38405-4
1985-07
German standard methods for the examination of water, waste
water and sludge; anions (group D); determination of fluoride
(D 4)
M004
DIN 38406-5
1983-10
German standard methods for the examination of water, waste
water and sludge; cations (group E); determination of ammonia-
nitrogen (E 5)
DIN 38407-9
1991-05
German standard methods for the examination of water, waste
water and sludge; substance group analysis (group F);
determination of benzene and some of its derivatives by gas
chromatography (F 9)
M029, M041
DS 204
1980-12
Vandundersoegelse. Toerstof og gloederest
Determination of total residue and total fixed residue in water,
sludge and sediment
DS/R 209
2006-09
Wasseruntersuchung - Fette und Öle - Extraktion mit Tetra-
chlorethen und Messungen mit Infrarot-Spektrophotometrie
DS 217
1991-08
Vandundersoegelse. COD (Oxygenforbrug med kaliumdichromat)
Water analysis - Determination of the chemical oxygen demand
(dicromate method)
M031
DS 236
1977-12
Vandundersoegelse. Aggressivitet over for calciumcarbonat
Water analysis - Stability with respect to calcium carbonate
M030
DS 278
1976-02
Vandundersoegelse. Bestemmelse af sulfid i recipient- og
drikkevand
Water analysis - Determination of sulphide in natural and pure
water
DS 280
1976
Bestimmung von Sulfid in Abwasser: Determination of sulfide in
waste water
Appendix to Accreditation Certificate D-PL-14082-01-00
Period of validity: 10 July 2013 to 9 July 2018 7/7
M002
REFLAB methode 2
2002
Biokemisk oxygenforbrug over 5 doegn (BOD5) pa lavt niveau med
tilsaetning af N-allylthiourea
Biochemical oxygen demand over 5 days (BOD5) at low-level,
adding N-allylthiourea
QMP_504_KI_50_211
2009-12
Prüfung von Trinkwasser auf Geruch, Geschmack und
Geruchsschwellenwert; Determination of smell, taste and
threshold value of smell of drinking water
5 Analysis of feeding stuff, food, materials made from plants and animals
5.1 Preparation and pretreatment of samples*
ASU L 00.00-19/1
2003-12
Analysis of food - Determination of trace elements in food; Part
1: Treatment under pressure
ASU L 01.00-1
2011-06
Analysis of food - General guideline for the preparation of
analytical samples and the preparation of initial suspensions
and decimal dilutions for microbiological analysis - Part 5:
Specific rules for the preparation of milk and milk products
ASU L 02.07-1
1987-06
Analysis of food - Preparation of samples for microbiological
analysis; Method for powdered milk products
ASU L 03.00-1
2011-06
Analysis of food - General guideline for the preparation of
analytical samples and the preparation of initial suspensions
and decimal dilutions for microbiological analysis - Part 5:
Specific rules for the preparation of cheese
ASU L 04.00-1
2011-06
Analysis of food - General guideline for the preparation of
analytical samples and the preparation of initial suspensions
and decimal dilutions for microbiological analysis - Part 5:
Specific rules for the preparation of butter
ASU L 06.00-16
2004-12
Analysis of food - Microbiological analysis of meat and meat
products; Sample preparation
ASU L 42.00-1 2011-06
General guideline for the preparation of analytical samples and the preparation of initial suspensions and decimal dilutions for
microbiological analysis - Part 5: Specific rules for the
preparation of ice cream
Appendix to Accreditation Certificate D-PL-14082-01-00
Period of validity: 10 July 2013 to 9 July 2018 8/8
ASU L 48.01-6
2011-06
Analysis of food - General guideline for the preparation of
analytical samples and the preparation of initial suspensions
and decimal dilutions for microbiological analysis - Part 5:
Specific rules for the preparation of baby and infant formula on
the basis of milk
VDLUFA VII, 2.1.1
2011
Wet digestion under pressure
5.2 Organoleptical characteristic values
ASU L 00.90-6
1997-09
Analysis of food - Organoleptical testing methods; Simple
descriptive test
DLG-Testing stipulations and
test schemes 2011
Sampling and test technology for DLG organoleptic test
DLG-Testing stipulations and
test schemes 2011
Organoleptic evaluation of bread, fine backed goods, cereal
food and confectionery in accordance with DLG test scheme
DLG-Testing stipulations and
test schemes 2011
Organoleptic evaluation of convenience food in accordance
with DLG test scheme.
DLG-Testing stipulations and
test schemes 2011
Organoleptic evaluation of meat products (ham and sausage) in
accordance with DLG test scheme
DLG-Testing stipulations and
test schemes 2011
Organoleptic evaluation of milk and milk products including ice
cream in accordance with DLG test scheme
DLG-Testing stipulations and
test schemes 2011
Organoleptic evaluation of fruit drinks in accordance with DLG
test scheme
DLG-Testing stipulations and
test schemes 2011
Organoleptic evaluation of spirituous and alcoholic mixed
beverages in accordance with DLG test scheme
DLG-Testing stipulations and
test schemes 2011
Organoleptic evaluation water in accordance with DLG test
scheme
5.3 Determination of characteristic values with physical and physiochemical methods
ASU 04.00-14
1996-02
Determination of the hardness of butter
Appendix to Accreditation Certificate D-PL-14082-01-00
Period of validity: 10 July 2013 to 9 July 2018 9/9
ASU L 06.00-2
1980-09
Measurement of the pH value in meat and meat products
ASU L 06.00-8
2010-09
Determination of hydroxyproline content in meat and meat
products
ASU L 06.35-2 (EC)
1984-05
Standards for water content of frozen and deep frozen chicken
and hen; II: Drip method
VDLUFA. VI, C 8.2
2000
Acidity; pH value in milk and milk products
VDLUFA VI, C 25.2
1988
Physical testing methods of butter; Hardness
QMP_504_KI_51_142_x
1997-09
Grill juice loss
5.4 Determination of ingredients
5.4.1 Via gravimetry*
ISO 8262-1
2005-09
Milk products and milk-based foods - Determination of fat
content by the Weibull-Berntrop gravimetric method
(Reference method) - Part 1: Infant foods
ISO 8262-2
2005-09
Milk products and milk-based foods - Determination of fat
content by the Weibull-Berntrop gravimetric method
(Reference method) - Part 2: Edible ices and ice-mixes
ISO 8262-3 2005-09
Milk products and milk-based foods - Determination of fat content by the Weibull-Berntrop gravimetric method
(Reference method) - Part 3: Special cases
DIN EN ISO 1735
2005-05
Gravimetric methods for determination of fat content in milk
and milk products in accordance with SCHMID-BONDZYNSKI-
Ratzlaff
DIN EN ISO 2450
2009-03
Cream - determination of fat content - gravimetric method
(reference method)
DIN EN ISO 3727-1
2002-04
Butter. Determination of moisture, non-fat solids and fat
content - Part 1: Determination of moisture content
DIN EN ISO 3727-2
2002-04
Determination of moisture, non-fat solids and fat content of
butter - Part 2: Determination of non-fat solids
Appendix to Accreditation Certificate D-PL-14082-01-00
Period of validity: 10 July 2013 to 9 July 2018 10/10
DIN EN ISO 8381
2009-03
Gravimetric methods for determination of fat content in milk
and milk products in accordance with RÖSE-GOTTLIEB
ASU L 00.00-18
1997-01 and
Corrigendum
2002-12
Determination of total dietary fibre in food
ASU L 02.06-E/2
1981-01
Dry matter (water contents); Water contents of powdered milk
products
ASU L 06.00-3
2004-07
Determination of dry matter in meat and meat products
ASU L 06.00-4
2007-04
Determination of ash in meet and meat products
ASU L 06.00-6
1980
Determination of total fat content in meat and meat products
VDLUFA III, 6.6.1
1999
Determination of enzyme-soluble organic substance
VDLUFA VI, C 35.3
1985
Dry matter (water content); Sea sand method
VO (EC) 152/2009, III, A
2009-02
Determination of moisture content in feed stuffs
VO(EC) 152/2009, III, H
2009-02
Determination of crude fat
VDLUFA III, 6.1.1
1993
VO(EC) 152/2009, III I
2009-02
Determination of crude fibre (Tecator)
VO(EC) 152/2009, III, M
2009-02
Determination of crude ash
VO(EC) 152/2009, III, N
2009-02
Determination of the ash fraction that is insoluble in
hydrochloric acid
5.4.2 Via Titrimetry*
Appendix to Accreditation Certificate D-PL-14082-01-00
Period of validity: 10 July 2013 to 9 July 2018 11/11
DIN EN ISO 8968-1
2013-04
Milk and milk products - determination of the nitrogen content
and calculation of the crude protein content
ASU L 06.00-5
2010-09
Determination of the table salt content in meet and meat products
ASU L 06.00-7
2007-04
Determination of crude protein content in meat and meat
products
VO(EC) 152/2009, III, C
2009-02
Determination of crude protein content in feeding stuffs
VO(EC) 152/2009, III, Q
2009-02
Determination of chlorine from chlorides
VDLUFA VI, C 10.6.2
1988
Direct determination of inorganic components in milk and milk
products; Chloride in cheese in accordance with ERBACHER
5.4.3 Via photometric and polarimetric methods*
ASU L 02.00-9
2010-09
Determination of lactose and galactose content of milk and
milk products – enzymatic testing method
ASU L 02.00-12
2009-06
Determination of saccharose and glucose in milk products and
ice cream – enzymatic testing method
ASU L 01.00-26/1
2011-01
Determination of L- and D-lactic acid (L- and D- lactate) in milk
and milk products - enzymatic testing method (deviation: also
for feeding stuffs)
VDLUFA III, 12.1.1+2/12.3.1
1976
Determination of carotene and/or xanthophyll upon hot
saponification
VO(EC) 152/2009, III, J
2009-02
Determination of sugar
VO(EC) 152/2009, III, K
2009-02
Determination of lactose
VO(EC) 152/2009, III, L
2009-02
Determination of starch
Appendix to Accreditation Certificate D-PL-14082-01-00
Period of validity: 10 July 2013 to 9 July 2018 12/12
5.4.4 Determination of elements via spectrometric methods*
DIN EN ISO 11885 (E 22)
2009-09
Water quality - Determination of selected elements through
inductively-coupled plasma atomic emission spectrometry (ICP-
OES)
(deviation: Matrix - foodstuffs and feeding stuffs)
DIN EN ISO 17294-2 (E 29)
2005-02
Water quality – Application of inductively coupled plasma mass
spectrometry (ICP-MS) - Part 2: Determination of 62 elements
(deviation: Matrix - food stuffs and feeding stuffs, selected
elements)
DIN EN 15510
2007-10
Feeding stuffs - Determination of calcium, sodium, phosphor,
magnesium, potassium, iron, zinc, copper, manganese, cobalt,
molybdenum, arsenic, lead and cadmium by ICP-AES
DIN EN 15621
2012-04
Feeding stuffs - Determination of calcium, sodium, phosphor,
magnesium, potassium, sulphur, iron, zinc, copper, manganese
and cobalt by ICP-AES
VDLUFA III, 10.8.2
2006
Determination of selected elements in plant material and
feeding stuffs with ICP-OES
(Determination in matrix-specific extraction solutions)
VDLUFA III, 17.9.1
2006
Determination of 14 elements in plants, as well as basic feeding
stuffs and complete feeding stuffs by ICP-MS (Determination in matrix-specific extraction solutions)
5.4.5 Determination of organic ingredients via liquid chromatography (LC) methods**
DIN EN 12821
2009-08
Foodstuffs - Determination of vitamin D with HPLC;
determination of cholecalciferol (D3) or ergocalciferol D2)
DIN EN 12822
2000-07
Foodstuffs - Determination of vitamin E with HPLC, α, β, γ and
δ-tocopherols
DIN EN 14122
2003-09
Corrigendum
2012-04
Foodstuffs - Determination of vitamin B1 with HPLC
DIN EN 14152
2003-10
Corrigendum
2012-04
Foodstuffs - Determination of vitamin B2 with HPLC
Appendix to Accreditation Certificate D-PL-14082-01-00
Period of validity: 10 July 2013 to 9 July 2018 13/13
DIN EN 14663
2006-03
Foodstuffs - Determination of vitamin B6 (including glucosidic-
bound compounds) with HPLC
ASU L.00.00-9
1984-11
Examination of foodstuffs - Determination of preservatives in
low-fat foodstuffs
ASU L 40.00-7
1999-11
Corrigendum
2009-11
Determination of saccharide content
(deviation: Use of methods for foodstuffs and feeding stuffs in
general
ASU L 49.00-1
1991-06
Determination of vitamin D in dietetic food
ASU L 49.00-5
2006-12
Determination of tocopheroles and tocatrienoles in dietetic
food
VDLUFA II, 4.11.5; 4. suppl.
1997
Determination of methionine in feeding stuffs with high
chloride
VDLUFA III, 4.11.6
2004
Determination of lysine, methionine and threonine in
commercial amino acid products and premixes
VDLUFA III, 13.6.1
1983
Determination of Choline-Chloride
VDLUFA III, 13.8.1
2007
Determination of vitamin D3 in feeding stuffs; HPLC method
VDLUFA III, 13.9.1
2006
Feeding stuffs - Determination of B vitamins, including nicotinic
acid, HPLC method
VO (EC) 152/2009, IV, A
2009-02
Determination of vitamin A content
VO (EC) 152/2009, IV, B
2009-02
Determination of vitamin E content
VO(EC) 152/2009, III, F
2009-02
Determination of amino acids (except for tryptophane)
VO(EC) 152/2009, III, G
2009-02
Determination of tryptophane
QMP_504_KI_52_020_x
2010-08
Determination of vitamin C (ascorbic acid) in foodstuffs via
HPLC
Appendix to Accreditation Certificate D-PL-14082-01-00
Period of validity: 10 July 2013 to 9 July 2018 14/14
QMP_504_KI_52_021_x
2009-09
Determination of vitamin K1 (phyllocquinone); HPLC method
after DC cleaning
QMP_504_KI_52_022_x
2009-05
Determination of menadione (vitamin K3); HPLC method
QMP_504_KI_52_023_x
2010-08
Determination of preservatives in foodstuffs via HPLC
QMP_504_KI_52_028_x
2009-04
Determination of vitamin K1 (phyllochinon); HPLC with post-
column derivatisation
QMP_504_KI_52_136_x
2011-08
Determination of selected sugars in foodstuffs and beverage
samples with HPLC-ELSD
5.4.6 Determination of organic ingredients via gas chromatography (GC) methods*
ASU L 05.00-16
2010-09
Determination of cholesterole in foodstuffs (gas
chromatography methods)
DGF VI 10a/11a
2000
Gas chromatography: Analysis of fatty acids and fatty acid
distribution
(deviations: Use also is milk fats, without C4 and C6 fatty acid
determination)
VDLUFA III, 5.6.2
1983
Presentation of fatty acid methyl ester for gas chromatographic
determination of the total acid range of feed fats
VDLUFA III, 5.6.2
1983 with DGF C IV 11 D
1998
Determination of eruca acid contents in rape samples
expressed in percent of the total fatty acids
Appendix to Accreditation Certificate D-PL-14082-01-00
Period of validity: 10 July 2013 to 9 July 2018 15/15
5.5 Residues and trace elements
5.5.1 Via photometric methods*
DIN EN ISO 14673-3
2004-05
Determination of the nitrite and nitrate content in milk, Part 3
(deviation: Concentration and production of reagents)
ASU L 00.00-35
1998-09
UV photometric determination of dithiocarbamates and/or
thiuramdisulfides in food of vegetal origin (xanthogenate
method)
ASU L 07.00-12
1990-12
Determination of the nitrite and nitrate content in meat
products
(deviation: Concentration and production of reagents)
VDI 3795 Sheet 1
1976-06
Determination of fluorine contents in biological samples and in
IRMA solutions; Photometric determination
VO (EC) 152/2009, V, A
2009-02
Determination of the content of free and total gossypol
5.5.2 Via electrochemical methods*
DIN EN 16279
2012-09
Feeding stuffs - Determination of fluoride with an ion-selective
electrode (ISE)
5.5.3 Determination of elements via spectrometric methods*
DIN EN ISO 11885 (E 22)
2009-09
Water quality - Determination of selected elements through
inductively-coupled plasma atomic emission spectrometry (ICP-
OES)
(deviation: Matrix - foodstuffs and feeding stuffs)
DIN EN ISO 17294-2 (E 29)
2005-02
Water quality – Application of inductively coupled plasma mass
spectrometry (ICP-MS) - Part 2: Determination of 62 elements
(deviation: Matrix - food stuffs and feeding stuffs, selected
elements)
DIN EN 15510
2007-10
Feeding stuffs - Determination of calcium, sodium, phosphor,
magnesium, potassium, iron, zinc, copper, manganese, cobalt,
molybdenum, arsenic, lead and cadmium by ICP-AES
DIN EN 15621
2012-04
Feeding stuffs - Determination of calcium, sodium, phosphor,
magnesium, potassium, sulphur, iron, zinc, copper, manganese
and cobalt by ICP-AES
Appendix to Accreditation Certificate D-PL-14082-01-00
Period of validity: 10 July 2013 to 9 July 2018 16/16
DIN EN 15763
2010-04
Foodstuffs - Determination of trace elements - Determination
of arsenic, cadmium, mercury, and lead in foodstuffs
inductively coupled plasma mass spectrometry (ICP-MS) in
accordance after wet digestion
(deviation: Without mercury)
DIN EN 16277
2012-09
Animal feeding stuffs - Determination of mercury by cold-
vapour atomic absorption spectrometry (CVAAS) after
microwave pressure digestion (extraction with 65% nitric acid
and 30% hydrogen peroxide);
ASU L 00.00-19/4
1993-08
Determination of trace elements in feeding stuffs; Part 4
Determination of mercury with the cold-vapour atomic
absorption spectrometry (CVAAS) technique
VDLUFA III, 10.8.2
2006
Determination of selected elements in plant material and
feeding stuffs with ICP-OES
(Determination in matrix-specific extraction solutions)
VDLUFA III, 17.9.1
2006
Determination of 14 elements in plants, as well as basic feeding
stuffs and complete feeding stuffs by ICP-MS
(Determination in matrix-specific extraction solutions)
5.5.4 Determination of inorganic residues and trace substances via ion chromatography
(IC) methods*
DIN EN ISO 10304-1
2009-07
Water quality - Determination of dissolved anions via liquid ion
chromatography - Part 1
ASU L 26.00-1
2001-07
Examination of foodstuffs - Determination of the nitrate
content in vegetable products - HPLC/IC methods
5.5.5 Determination of organic residues and trace substances via liquid chromatography
(LC) methods **
DIN EN 15662
2009-02
Foods of plant origin - Determination of pesticide residues via
HPLC-MSMS or GC (QuEChERS method)
ASU L 00.00-76
2002-12
Determination of chlormequat and mepiquat in foodstuffs and
feeding stuffs (HPLC-MS/MS method)
(deviation: Smaller weighted sample, automated sample
injection)
Appendix to Accreditation Certificate D-PL-14082-01-00
Period of validity: 10 July 2013 to 9 July 2018 17/17
Official Journal of the
European Communities,
1864/90,
No. L 179/28
Determination of the glucosinal content in oilseeds by HPLC
IDF 171
1995
Determination of aflatoxin M1 in milk and milk powder via
HPLC cleanup with immuno-affinity column
VDLUFA III, 16.1.2
1993
Determination of aflatoxin B1; official method B: HPLC EC
method VDLUFA method
VDLUFA III, 16.1.4
1993
Determination of alphatoxin B1, extract cleaning with immuno-
affinity column VDLUFA method
VDLUFA III, 16.10.1
1993
Determination of ochratoxin A VDULFA method
VDLUFA III, 16.11.1
2004
Determination of ergosterol HPLC
QMP_504_KI_52_026_x
2011-03
Determination of ochratoxin A upon cleanup on immuno-
affinity column; HPLC method
QMP_504_KI_52_027_x
2011-10
Determination of ethoxyquin (HPLC method)
QMP_504_KI_52_113_x
2011-03
Determination of deoxynivalenol (DON) and zearalenon (ZEA)
in foodstuffs and feeding stuffs (HPLC-MS/MS methods)
QMP_504_KI_52_116_x
2011-03
Determination of Chloramphenicol in foodstuffs and feeding
stuffs (HPLC-MS/MS method)
QMP_504_KI_52_117_x
2011-03O
Determination of acrylamide in foodstuffs (HPLC-MS/MS
methods)
QMP_504_KI_52_123_x
2011-03
Determination of trichothecene (mycotoxins) via HPLC-MSMS
in foodstuffs and feeding stuffs
QMP_504_KI_52_129_x
2011-03
Determination of selected antibiotics in feeding stuffs samples
via HPLC-MSMS (screening multi-method)
Appendix to Accreditation Certificate D-PL-14082-01-00
Period of validity: 10 July 2013 to 9 July 2018 18/18
QMP_504_KI_52_137_x
2012-12
Determination of coumarin in food samples via HPLC-UV
QMP_504_KI_52_145_x
2013-04
Determination of polar pesticides (e.g. ethephon, morpholine)
in fruit and vegetable samples (HPLC-MSMS method)
QMP_504_KI_52_146_x
2013-04
Determination of glyphosate and AMPA as FMOC derivatives
(HPLC-MSMS method)
QMP_504_KI_52_147_x
2013-04
Determination of selected ergo alkaloids in foodstuffs samples
and feeding stuff samples via LC-MSMS
QMP_504_KI_52_148_x
2013-04
Determination of ochratoxin A in foodstuffs samples and
feeding stuffs samples via LC-MSMS
QMP_504_KI_52_149_x
2013-04
Determination of aflatoxins in foodstuffs samples and feeding
stuffs samples via LC-MSMS
5.5.6 Determination of organic residues and trace substances via gas chromatography
methods **
DIN EN 15662
2009-02
Foods of plant origin - Determination of pesticide residues via
HPLC-MSMS or GC (QuEChERS method)
ASU L 00.00-34
2010-09
Modular multi-methods for determination of plant protectant
residues is foodstuffs (Extended new version of DFG
method S 19)
ASU L 00.00-36.2
2004-07
Determination of bromide residues in low-fat foodstuffs,
Part 1: Determination of total bromide
ASU L 00.00-49/2
1999-11 and
Corrigendum
2002-12
Determination of dithiocarbomate and thiram disulfide
residues (gas chromatography method)
deviation: smaller weighted sample, automated sample
injection)
VDLUFA. VII, 3.3.2.4
2011
Determination of polychlorinated dibenzo-p-dioxins (PSDD) and
polychlorinated dibenzofurans (PCDF), and additional selected
coplanar polychlorinated biphenyls (non-ortho PCB) in feeding
stuffs
VDLUFA VII, 3.3.3.2, 1. suppl.
2011
Determination of polynuclear aromatic hydrocarbons (PAH) in
plant material
Appendix to Accreditation Certificate D-PL-14082-01-00
Period of validity: 10 July 2013 to 9 July 2018 19/19
QMP_504_KI_52_046_x
2007-06
KI_52_046_x Determination of selected polychlorinated
biphenyls (PCB) in feeding stuffs, foodstuffs and simultaneously
with the dioxin analysis via GC
QMP_504_KI_52_139_x
2011-09
Determination of chlorophenol residues in solid samples via CS-
MS (QuEChERS method)
5.6 Microbiological and molecular biological examinations of foodstuffs
5.6.1 Determination of the microbiological activity of vitamins with auxotrophic
microorganisms
DIN EN 14131
2003-09
Foodstuffs - microbiological determination of folate
USP 21, 3rd Supplement,
Method 88
1986
Determination of the microbiological activity of biotin (original
title: Biological Tests and Assays - Biotin Assay)
USP 34 Methode 91
2011
Determination of Calcium-D-Pantothenate (original title:
Biological Tests and Assays - Calcium Pantothenate Assay)
USP 34 Methode 171
2011
Determination of the microbiological activity of vitamin B12
(original title: Biological Test and Assays - Vitamin B12 Activity
Assay) (deviation: The concentration of sodium sulphite in the
extraction solution is not adjusted to the weighted sample)
USP 34 Methode 441
2011
Niacin or Niacinamide Assay (Determination of the
microbiological activity of niacin and niacinamide)
(deviation: Extraction with HCI instead of sulphuric acid)
QMP_504_KI_51_009
2013-02
Determination of inosite
QMP_504_KI_51_027
2013-02
Determination of the microbiological activity of choline
5.6.2 Analysis of antibiotics in feeding stuffs via microbiological sensitivity test
QMP_504_KI_51_022
2005-03
Qualitative detection of antibiotics in feeding stuffs -
microbiological diffusion in agar medium
QMP_504_KI_51_024
2005-03
Identification of antibiotics in feeding stuff – microbiological
method - 2005 method (bioautography)
Appendix to Accreditation Certificate D-PL-14082-01-00
Period of validity: 10 July 2013 to 9 July 2018 20/20
5.6.3 Qualitative and quantitative detection of microorganisms via cultural methods*
(identifying bacterial count)
ISO 4831
2006-08
Microbiology - General guidance for the enumeration of
coliforms; Most probable number technique
ISO 4832
2006-02
Microbiology - General guidance for the enumeration of
coliforms; Colony count technique
ISO 4833
2003-06
Microbiology - General guidance for the enumeration of micro
organisms; Colony count technique at 30 °C
ISO 6579
2007-10
Microbiology of food and animal feeding stuffs - Horizontal
method for the detection of Salmonella spp.
ISO 7251
2005-02
Microbiology - General guidance for the enumeration of
presumptive Escherichia coli; Most probable number technique
ISO 13559
2002-11
Butter, fermented milks and fresh cheese - Enumeration of
contaminating microorganisms - Colony-count technique at
30 °C
ISO 15213
2003-05
Microbiology of food and animal feeding stuffs - Horizontal
method for the enumeration of sulphite-reducing bacteria
growing under anaerobic conditions
ISO 15214
1998-08
Microbiology of food and animal feeding stuffs - horizontal
method for the counting of mesophilic lactic acid bacteria -
colony count method at 30°C
ISO 21527-1
2008-07
Microbiology of food and animal feeding stuffs - Horizontal
method for the enumeration of yeasts and moulds - Part 1:
Colony count technique in products with water activity greater
than 0.95
ISO 21527-2
2008-07
Microbiology of food and animal feeding stuffs - Horizontal
method for the enumeration of yeasts and moulds - Part 2:
Colony count technique in products with water activity less
than or equal to 0.95
DIN ISO 21528-1
2009-12
Microbiology of food and feeding stuffs - horizontal method for
detection and enumeration of enterobacteriaceae - part 1:
Detection and enumeration via MPN technique with pre-
enrichment
Appendix to Accreditation Certificate D-PL-14082-01-00
Period of validity: 10 July 2013 to 9 July 2018 21/21
DIN ISO 21528-2
2009-12
Microbiology of food and feeding stuffs - horizontal method for
detection and enumeration of Enterobacteriaceae - part 2:
Colony counting technology
DIN EN ISO 6887-1
1999-04
Microbiology of food and animal feeding stuffs - General
guideline for the preparation of analytical samples and the
preparation of initial suspensions and decimal dilutions for
microbiological analysis - Part 1: General rules for the
preparation initial suspensions and decimal dilutions
DIN EN ISO 6887-5
2011-01
Microbiology of food and animal feeding stuffs - General
guideline for the preparation of analytical samples and the
preparation of initial suspensions and decimal dilutions for
microbiological analysis - Part 5: Specific rules for the
preparation of milk and milk products
DIN EN ISO 6888-1
2003-12
Microbiology of food and animal feeding stuffs - horizontal
method for the enumeration of coagulase-positive
staphylococci (Staphylococcus aureus and other species) - Part
1: Methods with Baird-Parker agar
DIN EN ISO 6888-3
2005-07
Microbiology of food and animal feeding stuffs - horizontal
method for the enumeration of coagulase-positive
staphylococci (Staphylococcus aureus and other species) - Part
3: Detection and MPN method for low bacterial counts
DIN EN ISO 7932
2005-03
Microbiology of food and animal feeding stuffs - horizontal
method for the enumeration of Bacillus cereus - colony
enumeration method at 30°C
(deviation: Use of Bacara agar (AES. AFNOR validated))
DIN EN ISO 7937 2004-11
Microbiology of food and animal feeding stuffs - horizontal method for the enumeration of Clostridium perfringens -
colony enumeration method at 30 °C
DIN EN ISO 11290-1
2005-01
Microbiology of food and feeding stuffs - horizontal method for
detection and enumeration of Listeria monocytogenes - Part 1:
Detection method
(deviation: Tasks in accordance with the ALOA one day method
(AFNOR validated) confirmation with rapid L-mono.)
DIN EN ISO 11290-2
2005-01
Microbiology of food and feeding stuffs - horizontal method for
detection and enumeration of Listeria monocytogenes - Part 2:
Enumeration method
(deviation: Confirmation with rapid L-mono.)
Appendix to Accreditation Certificate D-PL-14082-01-00
Period of validity: 10 July 2013 to 9 July 2018 22/22
DIN EN ISO 13720
2010-12
Meat and meat products - enumeration of presumptive
Pseudomonas spp.
DIN 10113-1
1997-07
Determination of surface colony count on fitment and utensils
in food areas - Part I: Quantitative swab method
DIN 10113-2
1997-07
Determination of surface colony count on fitment and utensils
in food areas - Part II: Semi-quantitative swab method
ASU L 06.00-18
1984-05
Examination of foodstuffs - Determination of the aerobic
enumeration at 30 °C in meat and meat products; spattle
method and poured plate method
ASU L 06.00-19
1984-05
Examination of foodstuffs - Determination of the aerobic
enumeration at 30 °C in meat and meat products; drop plate
method
ASU L 06.00-24
1987-11
Examination of foodstuffs - Determination of
Enterobacteriaceae in meat; spattle method (reference
method)
ASU L 06.00-25
1987-11
Examination of foodstuffs - Determination of
Enterobacteriaceae in meat; drop plate method
ASU L 06.00-40
1997-01
Examination of foodstuffs - Determination of the surface
colony count on meat; destructive method (removal method)
VDLUFA III, 28.1.1
2007
General documented procedure for determination of bacterial
counts via solid nutrient media
VDLUFA III, 28.1.2
2007
Procedure instruction for identification of bacteria, yeasts,
moulds and black fungi as product-typical spoilage indicating indicator germs in feeding stuffs
VDLUFA VI, 7.8.2
1996
Determination of enterococci, colony enumeration method
with kanamycin esculin azide agar
Appendix to Accreditation Certificate D-PL-14082-01-00
Period of validity: 10 July 2013 to 9 July 2018 23/23
VDLUFA VI, 7.13
1996
Determination of the count of thermoduric (thermally-
resistant) microorganisms
Nordisk Metodikkommitté för
Livsmedel. NMKL No. 71, 5.
Ed., 1999
Detection of Salmonella spp. in foodstuffs
QMP_504_KI_51_133
2006-08
Determination of the count of bacillus spores from foodstuffs
Literature method: Literature method Baumgart, J.
Microbiological examination of foodstuffs
QMP_504_KI_51_166
2007-11
Determination of the count of thermophilic microorganisms -
literature method: Literature method Baumgart, J.
Microbiological examination of foodstuffs
5.7 Biochemical examinations of food and feeding stuffs
5.7.1 Analysis of nucleic acids via PCR* (Detection of genetically engineered changes,
microorganisms and other organisms groups)
DIN EN ISO 21570
2006-02
Corrigendum
2007-06
Method for detection of genetically modified organisms and
their products - quantitative based on nucleic acid based
methods, execution in the LightCycler 2
DIN EN ISO 21571
2005-05
Method for detection of genetically modified organisms and
their products - nucleic acid extraction
ASU L 00.00-98
2007-04
Analysis of food and feeding stuffs for the presence of
Salmonella spp., PCR method
ASU L 00.00-122
2008-06
Screening method for detection of genetically modified DNA
sequences in plants
(deviation: Use of the kit, “LightCycler GMO Screening Kit”
(biocetone))
ASU L 23.01-22-1
1998-03
Detection of genetically-modified soybeans.
(deviation: Use of the kit, “Lightcycler GMO Soya Quantification
Kit” (biocetone))
EURL-AP recommended
protocol: 2013-02
Detection of horse DNA using real time PCR
Government of Canada,
MFLP-25: 2006-03
MFLP-26: 2006-02
Analysis of food and feeding stuffs for the presence of shigella
spp., PCR method
Appendix to Accreditation Certificate D-PL-14082-01-00
Period of validity: 10 July 2013 to 9 July 2018 24/24
QMP_504_KI_51_201
2005-01
Isolation of DNA from rapeseed, maize, soy, feeding stuffs and
foodstuffs with the Wizard Magnetic DNA Purification System
for Food (Promega)
QMP_504_KI_51_202
2005-04
Analysis of rapeseed DNA for genetically engineered
modifications via Real Time PCR
QMP_504_KI_51_203
2005-01
Analysis of maize DNA for genetically-engineered changes via
Real Time PRC
QMP_504_KI_51_206
2013-02
Analysis of food and feeding stuffs for the presence of
Salmonella spp., PCR method
QMP_504_KI_51_213
2013-02
PCR detection or PCR confirmation of various pathogenic
bacteria in accordance with literature methods
QMP_504_KI_51_216
2012-10
Analysis of food and feeding stuffs for the presence of Listeria
monocytogenes, PCR method in accordance with Guilbeaud M
et al., J. Appl. Micr. 2005
QMP_504_KI_51_217
2013-03
PCR detection or PCR confirmation of bacterial that are similar
to Clostridium estertheticum and Clostridium estertheticum in
accordance with DM et al., J. Appl. Micr. 2003
QMP_504_KI_51_207
2013-03
Analysis of animal material for the presence of specific DNA of
cattle, pig, sheep, chicken or turkey via Real Time PCR
5.7.2 Determination of toxins, allergens, antibodies, and viruses via immuno-chemical
examination methods*
QMP_504_KI_51_300
2007-01
Quantitative determination of mycotoxins (desoxynivalenol,
Zearalenone, Ochratoxine, aflatoxins) in food and feeding stuffs
due to enzyme immuno assay
QMP_504_KI_51_301
2006-10
Automated determination of anti-Salmonella antibodies in
meat juice or serum due to enzyme immuno assay
QMP_504_KI_51_304
2012-11
Allergen analysis: Quantitative determination of residues of
hazelnut, peanut, almond egg, ß-lactoglobulin, casein and
gluten in food through enzyme immuno assay
Appendix to Accreditation Certificate D-PL-14082-01-00
Period of validity: 10 July 2013 to 9 July 2018 25/25
6 Examinations of fertilisers
6.1 Sample preparation
VO(EC) 2003/2003, IV, 3.1.1
2003-10
Extraction of the phosphorus soluble in mineral acids
VO(EC) 2003/2003, IV, 3.1.2
2003-10
Extraction of the phosphorus that can be dissolved in a
2% solution of antacid
VO(EC) 2003/2003, IV, 3.1.3
2003-10
Extraction of the phosphorus that can be dissolved in a
2% solution of citric acid
VO(EC) 2003/2003, IV, 3.1.4
2003-10
Extraction of the phosphorus that can be dissolved in neutral
ammonium citrate
VO(EC) 2003/2003, IV, 3.1.5.2
2003-10
Extraction of the phosphorus that can be dissolved at room
temperature in accordance with Permanent
VO(EC) 2003/2003, IV, 3.1.6
2003-10
Extraction of the water-soluble phosphorus
VO(EC) 2003/2003, IV, 8.1
2003-10
Extraction of total calcium, total magnesium and total sodium,
as well as the total sulphur in the form of sulphate
VO(EC) 2003/2003, IV, 8.3
2003-10
Extraction of water-soluble calcium, magnesium and sodium, as
well as the total sulphur in the form of sulphate
VO(EC) 2003/2003, IV, 9.1
2003-10
Extraction of total trace nutrient substances
VO(EC) 2003/2003, IV, 10.2 2003-10
Extraction of water-soluble trace nutrient substances
VDLUFA II, 4.1.2
2004
Determination the of antacid soluble phosphate, extraction
VDLUFA II, 4.1.3
1995
Determination of the citric acid soluble phosphate, extraction
VDLUFA II, 4.1.5
1995
Determination of the alkaline ammonium citrate soluble
phosphate in accordance with Petermann, extraction
VDLUFA II, 4.1.7
1995
Determination of the water soluble phosphate, extraction
Appendix to Accreditation Certificate D-PL-14082-01-00
Period of validity: 10 July 2013 to 9 July 2018 26/26
VDLUFA II, 6.1.1
2004
Determination of mineral soluble calcium: Manufacturing of
the analysis solutions
VDLUFA II, 6.1.2
2004
Determination of total calcium in fertilisers with organic
fractions: Manufacturing of the analysis solutions
VDLUFA II, 6.1.3
1999
Determination of water-soluble calcium in mineral fertilisers:
Manufacturing of the analysis solutions
VDLUFA II, 7.1
2008
Magnesium: Manufacturing of the analysis solutions
VDLUFA II, 7.3.1.2
2008
Extraction of water-soluble sulphur that can be present in
different forms
VDLUFA II, 9.5.1
2004
Chemical digestion with aqua regia
6.2 Physiochemical characteristic values
DIN EN 12176 (S 5)
1998-06
Characterisation of sludge - determination of the pH value
DIN EN 12880 (S 2a)
2001-02
Characterisation of sludges - determination of the dry residue
and the water content
VDLUFA II, 6.3
1995
Determination of the alkaline effective components in calcium
fertilisers
VDLUFA II, 6.4
1995
Determination of the reactivity of carbonic acid calcium
fertilisers
VDLUFA II, 6.5.1
2008
Determination of sieve passage of fertilisers, dry method
VDLUFA II, 6.5.2
1995
Determination of sieve passage of moist or clumped fertilisers,
wet method
VDLUFA II, 10.1
1999
Determination of loss on ignition
Appendix to Accreditation Certificate D-PL-14082-01-00
Period of validity: 10 July 2013 to 9 July 2018 27/27
6.3 Inorganic chemical parameters
DIN EN ISO 11885 (E 22)
2009-09
Water quality - Determination of selected elements through
inductively-coupled plasma atomic emission spectrometry
(ICP-OES)
(Determination in matrix-specific extraction solutions)
DIN EN ISO 17294-2 (E 29)
2005-02
Water quality – Application of inductively coupled plasma mass
spectrometry (ICP-MS) - Part 2: Determination of 62 elements
(Determination in matrix-specific extraction solutions)
VO(EC) 2003/2003, IV, 2.1
2003-10
Determination of ammonium nitrogen
VO(EC) 2003/2003, IV, 2.3.2
2003-10
Determination of total nitrogen in nitrate-containing calcium
cyanamide
VO(EC) 2003/2003, IV, 3.2
2003-10
Determination of phosphorus in the extracts (gravimetric as
Quinolinium Molybdophosphate)
VO(EC) 2003/2003, IV, 4.1
2003-10
Determination of water-soluble potassium
VDLUFA II, 3.2.1
1995
Determination of ammonium nitrogen
VDLUFA II, 3.4.1
1995
Determination of nitrate nitrogen
VDLUFA II, 3.5.2.3
2004
Determination of total nitrogen with the presence of nitrate,
reduction of the nitrate fraction with iron powder and
Tin-(II)-chloride
VDLUFA II, 3.5.2.4
1995
Determination of total nitrogen with the presence of nitrate,
reduction of the nitrate fraction with chrome powder
VDLUFA II, 4.2.2
1995
Determination of the phosphate in solutions and extracts
VDLUFA II, 4.2.4
2007
Determination of Ca, K, Mg, Na, P, S and Cl as main and
secondary fractions in fertilisers, ICP-OES method
VDLUFA II, 5.1.2
1995
Determination of mineral soluble potassium, production of the
analysis solution
VDLUFA II, 5.1.3
1995
Determination of total potassium, production of the analysis
solution
Appendix to Accreditation Certificate D-PL-14082-01-00
Period of validity: 10 July 2013 to 9 July 2018 28/28
VDLUFA II, 5.2.1
2004
Determination of potassium (gavimetric method with sodium
tetraphenylboron)
VDLUFA II, 8.10
2007
Determination of micro nutrients in fertiliser extracts:
ICP-OES method
6.4 Organic-chemical parameters
VO(EG) 2003/2003, IV, 2.5
2003-10
Biuret in urea, photometric
VDLUFA II, 3.9.1
1999
Determination of biuret
top related