forensic chemistry as scientific and educational specialisation at the jagiellonian university...
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FORENSIC CHEMISTRY FORENSIC CHEMISTRY
AS SCIENTIFIC AND EDUCATIONAL AS SCIENTIFIC AND EDUCATIONAL
SPECIALISATION SPECIALISATION
AT THE JAGIELLONIAN UNIVERSITYAT THE JAGIELLONIAN UNIVERSITY
Paweł Kościelniak
JAGIELLONIAN UNIVERSITY, Faculty of Chemistry
INSTITUTE OF FORENSIC RESEARCH
Cracow, Poland
DEPARTMENT OFANALYTICAL CHEMISTRY
(25)
GROUP OF TOXICOLOGICAL
AND PHARMACEUTICAL
ANALYSIS(5)
GROUP OF ANALYTICAL
FLOW TECHNIQUES
(11)
GROUP OF CHEMOMETRICS
(3)
LABORATORY FOR
FORENSIC CHEMISTRY
LABORATORY FOR FORENSIC CHEMISTRY
- system for capillary electrophoresis (PrinCe 550 CSD, Prince)
- HPLC chromatograph (LaChrom, Merck)
- GC chromatograph (3900, Varian)
- atomic fluorescence spectrometer with hydride generation (AFS 230, Beijing Haiguang Instrument Co.)
- system for microwave digestion (MARS 5X, CEM),
- audiovisual equipment (video-projectors, digital photo-cameras, video-camera, video-recorders)
founded in 2000
Sem. SubjectNo. of hours
lectures classes seminars total
VI
Electronics and automatics 30 30
Optional 60 60
Total 90 90
VII
Electronics and automatics 60 60
Advanced analytical chemistry 45 45
Chemometrics and biometrics 30 15 45
Analysis in forensic chemistry 15 15
Radiometric analysis 30 30
Toxicology 30 30
Flow analysis 15 15
Optional 60 60
Total 225 60 15 300
Sem. SubjectNo. of hours
lectures classes seminars total
VIII
Radiometric analysis 45 45
Forensic toxicology 60 15 75
Criminalistics 15 60 15 90
Low aspects of the forensic expert work 15 15
Student’s report 30 30
Optional 60 60
Total 100 100 100 315
IX
i
X
Laboratory for master thesis 450 450
Seminar for master thesis 60 60
Clinical toxicology 15 15
GLP 15 15
Optional 60 60
Total 90 450 60 600
No. Subject Place
1 Toxicological analysis of drugs IFR
2 Ethanol- selected toxicological and analytical aspects IFR
3 Application of GC/MS method to analysis of drugs in biological materials IFR
4 Determination of inorganic toxicants in biological material IFR
5 Chemical examinations of car paints IFR
6 Chemical examinations of fibers IFR
7 Chemical examinations of gun-shot residuals IFR
8 Chemical examination of inks by TLC IFR
9 Chemical analysis of inks by CE JU
10 Determination of Se and As in biological materials by AFS-HG JU
11 Comparative examination of psychotropic drugs by HPLC and CE JU
12 Profiling of drugs – physicochemical and chemometric examination JU
LABORATORY CLASSES
SubjectAnalytical method
FCh JU IFR
Determination of selected elements at normal levels in biological materials ICP/OES, AAS AAS
Development of novel techniques for preparation of biological samples HPLC, CE
Development of analytical procedures for determination of psychotropic drugs HPLC, CE
Development of analytical procedures for determination of selenium and arsenic in biological materials AFS
Application of Py-GCMS to analysis of criminalistic traces Py-GCMS
Identification and discrimination of paint traces chemometric
methods IR
Examination of questioned documents on the basis of identification of chemical composition of inks CE, LIBS
RESERCH SUBJECTS
PUBLICATIONS
M. Zadrożna, M. Gawlik, B. Nowak, A. Marcinek, H. Mrowiec , S. Walas, R. Wietecha-Posłuszny, P. Zagrodzki, „Antioxidants Activities and Concentration of Selenium, Zinc and Copper in Preterm and IUGR Human Placentas”, J. Trace Elem. Med. Biol., 23, 144-148 (2009).
M. Szafarska, M. Woźniakiewicz, M. Pilch, J. Zięba-Palus, P. Kościelniak, “Computer Analysis of ATR-FTIR Spectra of Paint Samples for Forensic Purposes”, J. Molec. Struct., 924–926, 504–513 (2009).
B. Trzcińska, J. Zięba-Palus, P. Kościelniak, "Application of Microspectrometry in Visible Range to Differentiation of Car Solid Paints for
Forensic Purposes", J. Molec. Struct., 924–926, 393–399 (2009).
R. Wietecha-Posłuszny, J. Dobrowolska, P. Kościelniak, P. Zagrodzki, „Determination of Selenium as a Biomarker of Thyroid Cancer by HG-AFS Method”, Acta Chim. Slov., 56, 441-446 (2009).
J. M. Milczarek, M. Dziadosz, J. Zięba-Palus, “Way to Distinguish Car Paint Traces Based on Epoxy Primer Layers Analysis by Pyrolysis - Gas Chromatography - Mass Spectrometry (Py-GC/MS)”, Chem. Anal., 54, 173-185 (2009.
K. Madej, „Microwave-assisted and Cloud-point Extraction in Dtermination of Drugs and Other Bioactive Compounds”, Trends in
Analytical Chemistry, 28, 436-446 (2009). K. Madej, A. Biedroń, A. Garbacik, „Study of Separation and Extraction Conditions for Five Neuroleptic Drugs by an LLE-HPLC-DAD
Method in Human Plasma”, Journal of Liquid Chromatography & Related Technologies, 32, 3025-3037 (2009).
E. Florek, E. Ignatowicz, W. Piekoszewski, “Effect of Pregnancy and Tobacco Smoke on the Antioxidant Activity of Rutin in an Animal Model”, Pharmacological Reports, 61, 935-940 (2009).
M. Woźniakiewicz, J. Kuczara, P. Kościelniak, „Determination of Fluoxetine in Blood Samples by High-performance Liquid Chromatography Using a Derivatization Reagent”, Chem. Anal. (Warsaw), 54, 667-677 (2009).
R. Wietecha-Posłuszny, T. Lech, P. Kościelniak, “Application of Three Spectrometric Methods to Total Selenium Determination in Post-
mortem Material in a Case of Acute Selenium Compound Poisoning”, J. Forensic Sci., in print. M. Szafarska, R. Wietecha-Posłuszny, M. Woźniakiewicz, C. Hughes, P. Kościelniak, „Influence of Storage Conditions on Ageing of Colour
Dye-Based Inkjet Printing Inks”, Problems of Forensic Sciences, in print
Ph.D. STUDYStudent Subject Defense
Renata Wietecha-Posłuszny Development of the analytical procedure for the selenium determination in human tissues by the AFS-HG technique
2004
Rafał Borusiewicz Examination of arson traces 2004
Joanna Mania Examination of inks by capillary electrophoresis 2005
Michał Woźniakiewicz Analysis of psychotropic drugs by HPLC and CE 2008
Justyna Dobrowolska Elemental analysis of biological materials 2008
Jakub Mielczarek Classification and discrimination of car paint traces 2008
Justyna Dobrowolska Elemental analysis of selected human and animal tissues with toxicological and clinical respects
2009
Małgorzata Szafarska Development of the method for discrimination of printer inks by capillary electrophoresis for criminalistic purposes
2010
Jagoda Majcherczyk Influence of tobacco smoke on pharmacokinetics of citalopram 2011
Aneta Garbacik Novel methods for preparation of biological samples to toxicological analysis 2011
Danuta Dudek-Adamska Trace elements in biological materials 2011
Agnieszka Biedroń Analytical and toxicological examination of selected drugs in biological materials
2012
Paweł Knihnicki Determination of psychotropic drugs in saliva by capillary electroforesis 2012
Tomasz Lachowicz Py-GCMS analysis as a tool in forensic examination of criminalistic traces
2012
Agnieszka Solarz Analysis of printer inks by capillary electrophoresis for criminalistic purposes 2013
PROJECTS
TEMPUS program, project „Transformation of University Chemistry Studies at the Jagiellonian University” (TRUCS); 1997-2000
TEMPUS program, project „National Training Program for Forensic Science Experts” (NATFOSE); 1998-2001
LEONARDO DA VINCI program, project „Vocational Training System in Forensic Sciences - Exchange of Educational Experiences” (VITSFOS-E); 2001-2003
NATO program, project “Sensors for Chemical Weapons Detection Based on Molecularly Imprinted Polymers”; 2004-2005
TEMPUS program, project „Education System in Forensic Sciences for the Republic of Macedonia”, (EDUFORMAK); 2007-2010
Government Grant, project „Application of the Capillary Electrophoresis as a Tool in Criminalistic Examination of Ink Printed Documents”; 2007-2010
Operational Programme 'Innovative Economy', project „Mikro and Nano-systems in Chemistry and Clinical Diagnostics” (MNS-DIAG); 2009-2013
Government Grant, project „The Use of Modern Analytical Instrumentation for Purpose of the Fight Against Crime”; 2010-2013
Laser-induced breakdown spectrometer ((LIBS)
Laser-induced breakdown spectroscopy (LIBS) is a type of atomic emission spectroscopy, which uses a highly energetic laser pulse as the excitation source. The laser is focused to
form a plasma, which atomizes and excites samples.
Price: ~ 45 000 EUR
PLASMA EMMISIONPULSED LASER (1064 nm)
PLASMA PLUME
SAMPLE
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