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REMEDIAL INVESTIGATION AND FEASIBILITY STUDY
MARION PRESSURE TREATING COMPANYMARION, UNION PARISH, LOUISIANA
CTTY OF MARIONSUMMARY OF WATER QUALITY ANALYSESCITY OF MARION DRINKING WATER WELLS
Prepared for
U.S. ENVIRONMENTAL PROTECTION AGENCY1445 Ross Avenue
DaUas, TX 75202-2733
Work Assignment No.EPA RegionDate PreparedContract No.Prepared byTetra Tech Project ManagerTelephone No.EPA Work Assignment ManagerTelephone No.
031-RICO-067Z6May 19,200068-W6-0037Tetra Tech EM me.George Allman(214) 740-2029Bartolome J. Canellas(214) 665-6662
900221
CONTENTS
Section Page
I. INTRODUCTION . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1D. DISCUSSION . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1ffl. RESULTS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2IV. FUTUREACTION . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
Attachments
A LOUISIANA DEPARTMENT OF HEALTH & HOSPITALS ANALYTICAL RESULTSB U.S. ENVIRONMENTAL PROTECTION AGENCY ANALYTICAL RESULTSC TETRATECH FIELD LOG BOOK
TABLE
Table Eagfi
1 SUMMARY OF THE RESULTS OF WATER QUALITY ANALYSES . . . . . . . . . . . . . . . . . . 3
li
SUMMARY OF WATER QUALITY ANALYSISCITY OF MARION DRINKING WATER WELLS
L INTRODUCTION
In accordance with instructions from Mr. Bartolome Canellas, U. S. Environmental Protection Agency(EPA) Region 6, Tetra Tech EM Inc. (Tetra Tech) planned and conducted drinking water samplingoperations for the Marion, Louisiana City Water Wells in January 2000. The city of Marion, Louisiana,is located 33.5 miles northwest ofMonroe, Louisiana. The city acquires its water from two water wellslocated less than 1/4 mile from the intersection of State Highway (SH) 551 and SH 33, in Union Parish,Louisiana. The purpose of the sampling activity was to gather preliminary data relative to the groundwater conditions of these wells, which are located within one mile of the Marion Pressure TreatingCompany (MPTC) site. Tetra Tech utilized me services of the EPA's Environmental Services BranchLaboratory in Houston, Texas, for sample analysis.
n. DISCUSSION
Prior to conducting sampling operations, the Tetra Tech project manager contacted Mr. Jimmy Caldwell,Marion City Water Department, to obtain the historical laboratory results of previous drinking watersampling efforts. The Marion City Water Department operates the wells and, collects and tests samplesfrom the wells biannually to ensure compliance with Louisiana drinking water regulations. MarionWater System Well # 1 has a depth of 624 feet in Sparta sand, while Marion Water System Well # 2 is895 feet deep in Wilcox sand. Copies of me record of previous sampling results (Attachment A) wereforwarded to Tetra Tech on December 9,1999. Tetra Tech environmental professionals reviewed thehistorical city water well sampling records supplied by Mr. Caldwell. Historical data obtained from theMarion Water Company records indicate that the wells are in compliance with state regulations.
The Tetra Tech project manager contacted Mr. Caldwell to coordinate me January 2000 sampling effort.Mr. Caldwell met with the Tetra Tech sampling team on January 27,2000, to collect the samples. TetraTech also invited Mr. Ronnie Matte of the Louisiana Department of Environmental Quality (LDEQ) toparticipate in the sampling activities. Mr. Matte also met Tetra Tech personnel and Mr. Caldwell at thesite. Tetra Tech collected me samples on the morning of January 27,2000. In order to support the
S;\RAC\ODA031\DWSAMPLI\JAN200~1.WPD 1
quality control process, Tetra Tech also collected trip blank, field blank, and matrix spike/matrix spikeduplicate samples for analysis. The samples were immediately transported to EPA's EnvironmentalServices Branch Laboratory for analysis.
Samples were analyzed for volatile organic compounds, semi-volatile organic compounds, pesticides,polychlorinated biphenyls, metals, and cyanide; the results are listed at Attachment B. All analyticalresults were reviewed by the quality assurance personnel of the EPA Environmental Services BranchLaboratory. EPA's Houston Laboratory reported analytical results of samples collected in January 2000on March 13, 2000.
in. RESULTS
The LDHH and the OPH regulate the safety and adequacy of drinking water delivered by public watersystems in the State of Louisiana. Tetra Tech environmental professionals reviewed the laboratoryresults of samples collected on January 27,2000, and compared the results with water quality criteriaestablished by LDHH/OPH for drinking water systems. The water quality criteria established byLDHH/OPH for drinking water systems are presented in Table 1.
Laboratory results indicate that drinking water conditions of Marion City Water Wells meet waterquality criteria established by LDHH/OPH for primary drinking water systems in the State of Louisiana.Therefore, the current condition of water quality of Marion City Water Wells presents no evidence thatdrinking water quality in the City of Marion is compromised by constituents present at the MPTC site.
Tetra Tech's report evaluation team contacted Mr. David Reazin, EPA Region 6 Water Division, Mr.Greg Hill of the Louisiana Department of Health and Hospitals (LDHH), and Mr. Lance Broussard of theLDHH Office Of Public Health (OPH) to discuss the historical well records, compliance status, and thewater quality results of samples taken on January 27,2000. Tetra Tech will provide Mr. Reazin, Mr. Hilland Mr. Broussard with copies of the sampling results.
S:\RAC\ODA031\DWSAMPLI\JAN200~1.WPD 2
TABLE 1
SUMMARY OF THE RESULTS OF WATER QUALITY ANALYSESDRINKING WATER WELL SAMPLES, CITY OF MARION
"^rVi'^r;^^1';^!''^^^^
•i};' 'ff Parameter; 'l^:^^:
Antimony
Barium
Calcium
Iron
Magnesium
Potassium
Selenium
Sodium
•f^'r^^^^ipDetected^
'i'.i.^a'MWSW,'^::'".IDUPLICATE
ND
17.0
1,460
74.0
312
1.420
3.4
618,000
concentrations l
'MWSWft^i,
3.7
24.0
1,980
32.0
363
1,580
5.7
735,000
t^l)*^^.' ^1';] '
.ij.MWSW^I.
ND
18.0
1,460
49.0
322
1.440
3.6
560,000
LDHH(OPH)MCL(ug/l)
6.0
2000
NA
300
NA
NA
50
NA
Notes:
LDHHMCLMWSW^NANDOPH
Concentrations of constituents detected in well samples are presented in Table 1. Otheranalyzed constituents were not detected in well samples.Louisiana Department of Health and HospitalsMaximum Concentration LevelsMarion Water System Wellmicrograms per literNot applicableNot detectedOffice of Public Health
S:\RAC\ODA031\DWSAMPLIUAN200~1 .WPD
IV. FUTURE ACTION
Tetra Tech anticipates that sampling of the two city water wells will be repeated during the samplingactivities associated with the Remedial Investigation and Feasibility Study (RI/FS) ground waterinvestigation.
S:\RAC\ODA031\DWSAMPLIUAN200~1.WPD 4
ATTACHMENT A
LOUISIANA DEPARTMENT OF HEALTH & HOSPITALS ANALYTICAL RESULTSMARION CITY WATER WELL
(Eight Pages)
DEC-09-99 THU 16:06 Mar ion P o l i c e 110F>t .«.- - --.-„ ^._,.^um, . ,-,ui i U.ll'^11 Ln i-nUbtl 1-M <-!-<_ Ht 1UI, |U
From: LOUISIANA DEPT OF HEALTH & HOSPITALSCENTRAL LABORATORY325 LOYOLA AVB. 7th FLOORMEW ORLEANS, LA 70112
September 17, 1996TO: MARION WATER SYSTEM
PWS ID 1111011 PROJECT OB38MITOWN OP MARIONP 0 BOX 216MARION LA 71260
The following analytical results have been obtained for theindicated sample which was submitted to thie laboratory:Sample I.D. AD59622 POC ID: 6JCB-SYRFacility XDi 1111011Point Of Collection: WELL ^1 NEW WELLSample collector: MCCARTNEYSample collection date: 07/15/96 Time; 10:15Lab eubmitbal date; 07/17/96 Time: 16;56
ParameterPAH'S--- ADIPATE8/PHTHALATESSynthetic organic contaminants
Resultsee beloweee bslow
Unite HDLMicrograma/LMicrocrrams/L
D&t& for PAH'S--- ADIPATES/PHTHAIATES Micrograms/L;Coaiponent Naxae /BIS (2-ETHYLHEXYL) PHTHALATEBIS <2-ETHYLHEXYL) ADIPATEBENZO(a)PYREME
ResultNot detectedNot detectedNot detected
Caropon&nfc ICDL3.77.50.05
Data for Synthetic organic contaminants Micrograms/Li
Component NomoDALAPON2,4-DDINOSEBPICLORAMPENTACHLOROPHENOL2,4,5-TP(SILVEX)ATRAZINBALAC3tlLORCHLORDAMEENDRIHHEPTACHLORHBPTACHLOR BPOXIDBHEXACHLOROBBH2EMEHEXACHLOROCYCLOPENfADIENELINDANBMBTHOXYCHLOR
Reeult'Nob detectedNot detectedNot detectedMot detectedNot detectedNot detectedNot detectedNot detectedNot detectedNot detectedNot detectedMot detected.Ndt detectedNot .detectedNot "detectedNot detected
Component HDI»100.060.100.100.160.042.50.230.140.060.0030.0160.0020.120.0071.0
i?^?^ :! ,. ^ ru^ H- r;:1..:. .. 31e292^^... ,.../'"03
i »• ' 'MftRlOK WATER SYSTEM Sample I.D. ABS9622 (continued)Pagei ^September If. 1996
Data for Synthetic organic contaminante (continued):
Coaiponenfc NaaneSIMAZIMETOXAPHENEPCB'slSCftEEH)MJDICARB 8ULPOMEALDICARB SULFOXIDEOXAMrlb(VYDATE).METHOMYLALDIC&RBCARBOFURANDIQUATGLYPHOSATE 'ENDOTHALL
Reeuit Componon-b MDLNo.t. <^efcecced 1.0Koc detecfced 1.0Not d tect dHot detected 0.2Not detected 0.2Hot detected 0.2Noc detected 0.2Not detected 0.2Not detected 0.2Not detected 0.5Not detected 34Not detected 7
Sample conimentB; , . , • . . .
Ptttst resuteiK for voc analysis.
If there are any questions regarding ..this data. please call.
LOUIS P. WALES, JR.''" ;'.LAB SCIENTIST MANAGER
I jW-l?^ 1g. tW," l 7 J?,a i. ^p. ,P o,l, , eg D^ <.,* €
Prom: LOUISIANA DBPT OF HEALTH & HOSPITALSCENTRAL LABORATORY325 LOYOIA AVE. 7fch FLOORMEW ORLEANS, LA 70112
October 3, IS 96To: MARXOM WATER SYSTBM
PWS ID 1111011 PROJECT 0838MITOWN OF MARIONP 0 BOX 216MARION IA 71260
The following analytical results have been obtained for theindicated sample which was (submitted to this laboratory;
ficunple I.D. AB6089E t»OC ID: 8JCC-SYRFacility ID; 1111011Point o£ Collection: WELL ff2 OLD WELLSample collector; MCCARTMEYSarople collection date; 08/19/96 Timet 10:30Lab eubmittal date; 08/21/96 Time: 15:33
Payasieter-PAH'fi--- ADIPATES/PHTaAlATESSynthetic organic contaminante
Resultsee belowsee below
Unite MDLMicrograms/LMicrograias/L
Data for PAH^S---
Conipoxifeat KacieBIS (2-ETHYLHEXYL)BIS (2-ETHYLHBXYL)BENZO(a)PYRENB
PHTHALATEADIPATE
ResultMot detectedNot detectedNot detected
Component WDL3.77.50.05
Data for Synthetic organic oohtiuninantfi Microgranis/L:
Coa^ponent KaiaeDALAPON2,4-DDtHOSEBPICLORAMPEKTACHLOROPHEMOL2.A.5-TP(SILV3BX)ATRAZXNEALACHLORCttLORDANEEKDRXKHEPTACHLORHKPTACHLOR EPOXIDEHBiCACHLOROBfiKZEMBHEXACHLOROCYCLOPENTADIENELTNDANE
^nRTHOXYCHLOR .
ResultNot detectedNot detectedMob detectedNot detectedHot detectedMot detectedKot detectedNot detectedMot detectedNot detectedNot detectedNot detectedNot detectedNot detectedNot detectedMote. detected
Component ISDL100.060.100.100.160.040.300*040.140.0010.0050.0070.0020,040.0070.02
"y-i iij? i w.6: -u, d^ r.'k . ^ « ^^^^T'T^^' »
MARION WITER SYSTEM Sample I.D. AB606?S (continued)t»agei 2October 3, l$96 • • • •
Daita for Synthetic oi?ganio contaxninanfce (continued)»
Cotrtponent NainoSIMA2.XHE .TOXAPHERSPCB'B(SCREfiN)ALDICARB SULFOHBAliDICARB SUL^OXIDBOXAMYL(Vn)ATE)MBTHororx*ALD1CARBCARBOPURANDIQTJATGLYPHOSATEEMDOTHRLI*
Refiult Coinponent; H&1«Not detectefl 0.^7Hot deteoted 0.31Mot detectedNot detected 0.33Not detected. 0.22Not detected 0.23Not detected O.X2Hot detected 0.33Hot detected 0.32Kot detected 0.5Kot Done 34Hot detected 7
Sample cornciente:
FIEASE RESUBHIt FOR VOC t d.WtlOSA'ni MMYSES.
If there are &ny questions regarding this data, pleaee c&ll
LOUIS P. WALES, JR:LAB. SCIENTIST MAMAOER
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ATTACHMENT B
U.S. ENVIRONMENTAL PROTECTION AGENCY ANALYTICAL RESULTSMARION CITY WATER WELL
(44 Pages)
^ UNITED STATES ENVIRONMENTAL PROTECTION AGENCYREGION 6
1445 ROSS AVENUE, SUITE 1200DALLAS. TX 75202-2733
March 21,2000
Ms. Judy Brewster, Marion Town Clerk398 Main StreetMarion, LA71260
Re: former Marion Pressure Treating Company site.Results from town drinking water well samples collected January 2000
Dear Mrs. Brewster:
Please add the following material to the repository of information related to theformer Marion Pressure Treating Company site; and share the information with the townofficials.
Enclosed is the EPA Laboratory "Final Analytical Report" with results for thewater samples collected from the town drinking water wells in January 2000. These areonly the laboratory results. Many are listed as "ND", which means that they were "NotDetected" or found during the analysis. EPA and their contractor's will further evaluatethis data, and will consult with other Federal and State agencies to produce a final reportwith the interpretation of the results.
If there is any question related to this material, you, the Town Officials and or thepublic may contact me at (214) 665-6662.
Sincerely,
Bartolome J. Cafiellas (6SF-LP)
Recycled/Recyclable •Printed with Vegetable 00 Based bite on 100% Recycled Paper (40% Postconsumer)
OT5BCW11 Pagel
United States Environmental Protection AgencyRegion 6 Environmental Services Branch Laboratory
10625 Fallstone, Houston, Texas 77099
Final Analytical Report
Site Name
CERCLIS Number
Marion Pressure Treating
........ LAD008473142
Sample Collection Date ................................... January 27,2000
Laboratory Sample Identification ................................. OT5BCW11
Contact........................................... Bart Canellas (6SF-LT)
Report Date .............................................. March 13,2000
Report Narrative:
Standard procedures for quality assurance and quality control were followed inthe analysis and reporting of the sample results. The results apply only to thesamples tested. This final report should only be reproduced in full.
The laboratory routinely disposes of samples 90 days after all analysis has beencompleted. If you have a need to hold these samples in custody longer than 90days, please send an e-mail to Lany Streck Streck.Larrv(S>epa.aov within thenext 30 days briefly stating your need to hold these samples in custody.
Report Approvals:Marvelyn HumphreyDeputy Branch Chief (Acting) Region 6 Laboratory Branch Chief
OT5BCW11 Page 2
United States Environmental Protection Agency( B, Region 6 Environmental Services Branch Laboratory
10625 Fallstone, Houston. Texas 77099
^/ Final Analytical Report
Report Contents
STATION NUMBER________LABORATORY SAMPLE NUMBER_____________PAGE(S)
01 ......................... OT5BCW11-01 ......................... 3-10
02 . . . . . . . . . . . . . . . . . . . . . . . . . OT5BCW11-02 . . . . . . . . . . . . . . . . . . . . . . . . 1 1 - 1 803 . . . . . . . . . . . . . . . . . . . . . . . . . OT5BCW11-03 . . . . . . . . . . . . . . . . . . . . . . . . 19-2604 . . . . . . . . . . . . . . . . . . . . . . . . . OT5BCW11-04 . . . . . . . . . . . . . . . . . . . . . . . . 27-2905 . . . . . . . . . . . . . . . . . . . . . . ' . . . OT5BCW11-05 . . . . . . . . . . . . . . . . . . . . . . . . 30-32QC RESULTS .................................................... 33-42
CHAIN OF CUSTODY . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 43
"V
OT5BCW11 Page 3
U. S. Environmental Protection AgencyRegion 6 Houston Laboratory
Report For Sample Number OT5BCW1101
Source: MARION PRESSURE TREATINGSite Description: -,
Date/Time Received: 1/31/2000 08:30 AM Date Completed 3/10/2000
Date/Time Collected: 1/27/2000 11:26 AM
Sample Type: LIQUID
Comments:
ParameterABN
CN
EMHG
MAA
MICP
P/P
VOA
DescriptionACID/BASE NEUTRALS
CYANIDE
ESAT-MERCURY
GFAAS METALS
ICP METALS
PESTICIDES/POLYCHLORIHATED BIPHEMYLS
VOLATILE ORGANIC ANALYSIS
OT5BCW11 Page 4Volatile Organic Compounds
Method CLP SOW OLM03.2 (low level)
Sample Number OT5BCW11-01
Sample Type: LIQUID
Date Extracted: not extracted
Date Analyzed: 05-Feb-OO
Compound page 1 of 1Chloromethane——————————————————————————Bromomethane——————————————————————————Vinyl Chloride——————————————————————————Chloroethane———————————————————————————Methylene Chloride————————————————————————Acetone——————————————————————————————Carbon Disulfide——————————————————————————1,1 -Dichloroethene—————————————————————————1,1 -Dichloroethane————————————————————————trans-1,2-Dichloroethene—————————————————————cis -1,2-Dichloroethene———————————————————————^l.l———^J^——^^cnioroform————————————————————————————1,2-Dichloroethane—————————————————————————2-Butanone—————————————————————————————1,1.1-Trichtoroethane———————————————————————Carbon Tetrachloride————————————————————————Bromodichloromethane———————————————————————1 2-Dichloropropanecis-1,3-Dichloropropene——————————————————————Trichloroethene———————————————————————————Benzene—————————————————————————————Dibromochloromethane———————————————————————trans-1.3-Dichloropropene—————————————————————1,1,2-Trichloroethane————————————————————————Bromoform————————————————————————————4-Methyl-2-Pentanone———————————————————————2-Hexanone————————————————————————————
1,1,2,2-Tetrachloroethane—————————————————————Toluene——————————————————————————————Chlorobenzene———————————————————————————Ethylbenzene———————————————————————————Styrene—————————————————————————————o-xylene—————————————————————————————m/p-xylene—————————————————————————————
results (ug/l)
NDND
. NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
detection limits1111251111111511111111111
11111111
* "ND" means not detected at the corresponding detection limit
OT5BCW11 Page 5Tentatively Identified Volatile Organic Compounds
Method CLP SOW OLM03.2 (low level)
Sample Number. OT5BCW11-01
Sample Type: LIQUID
Date Extracted: not extracted
Date Analyzed: 05-Feb-OO
Number TICs found: 0
TICNO. CAS NO. COMPOUND NAME*
RTmin.
EST.**CONC.
pg/1
* The compounds listed are tentatively identified by the best match with the NIST/Wiley mass spectral databaseand/or by manual interpretation.
** An estimated concentration is obtained by quantitation using the nearest internal standard. Since no standardwas used for confirmation nor quantitation, a response factor of 1.0 is assumed.
OT5BCW11 Page 6
ORGANIC ANALYSIS DATA6HD-HO Sample NO: OT5BCW11-01
SEMI-VOLATILE COMPOUNDS BY METHOD 625(continuous extractor)
units: ug/L
Date Analyzed: 03-Feb-OO
Sample Type: Liquid
units> ug/L
Compound Name Results* | Del Limits Compound Name Results* | Del Limits
Acenaphthene . . . . . . . . . . . . . . .Acenaphthylene . . . . . . . . . . . . .Anthracene . . . . . . . . . . . . . . . . .Benzole Acid . . . . . . . . . . . . . . .Benzo(a)Anthracene . . . . . . . . .Benzo(a)Pyrene . . . . . . . . . . . . .Benzo(b)Fluoranthene . . . . . . .Benzo(g,b,i)Perylene . . . . . . .Benzo(k)Fluoranthene . . . . . . .Benzyl Alcohol . . . . . . . . . . . . .bis(2-Chloroethoxy)Methane .bis(2-Chloroethyl) Ether . . .bis(2-chloroisopropyl)Etherbis-(2-Ethylhexyl)Phthalate4-Bromophenylphenyl Ether . .Butylbenzylphthalate . . . . . . .Carbazole . . . . . . . . . . . . . . . . . .4-Chloroaniline . . . . . . . . . . . .2-Chloronaphchalene . . . . . . . .2-Chlorophenol . . . . . . . . . . . . .4-Qilorophenylphenyl Ether .4-Chloro-3-Methylphenol . . . .Chrysene . . . . . . . . . . . . . . . . . . .Dibenzofuran . . . . . . . . . . . . . . .Oibenzo(a,h)Anthracene . . . . .1.2-Oichlorobenzene . . . . . . . .1.3-Dlchlorobenzene . . . . . . . .1.4-Dichlorobenzene . . . . . . . .3,3'-Dichlorobenzidine . . . . .3.4-Dichlorophenol . . . . . . . . .Diethylphthai ate . . . . . . . . . . .3,4-Dlmethylphenol . . . . . . . . .DimethylPhthalate . . . . . . . . . .
KDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNONDNDNDND
3
a3
10
8
0.2
8
3
33
10«
2
62
2,4-Dlnltrophenol . . . . . . . . .2,4-Dlnitrotoluene . . . . . . . .2,6-Dinitrotoluene . . . . . . . .4,6-Dlnltro-2-HethylphenolCi-n-Butylphthalate . . . . . . .Di-n-Octyl Phthalate . . . . . .Fluoranthene . . . . . . . . . . . . . .Fluorene . . . . . . . . . . . . . . . . . .Hexachlorobenzene . . . . . . . . .Hexachlorobutadiene . . . . . . .Bexachlorocyclopentadiene .Hexachloroethane . . . . . . . . . .Indeno(1,2,3-cd) Pyrene . . .Isophorone . . . . . . . . . . . . . . . .2-Methylnaphthalene . . . . . . .2-Methylphenol . . . . . . . . . . . .4-Methylpbenol . . . . . . . . . . . .Naphthalene . . . . . . . . . . . . . . .2-Nltroaniline . . . . . . . . . . . .3-Nltroaniline . . . . . . . . . . . .4-Nitroaniline . . . . . . . . . . . .Nitrobenzene . . . . . . . . . . . . . .2-Nltrophenol . . . . . . . . . . . . .4-Hitrophenol . . . . . . . . . . . . .N-Nitrosodiphenylamine . . . .N-Nitroso-Di-n-PropylaminePentachlorophenol . . . . . . . . .Phenanthxene . . . . . . . . . . . . . .Phenol . . . . . . . . . . . . . . . . . . . .Pyrene . . . . . . . . . . . . . . . . . . . .1,2,4-Tricblorobenzene . . . .2.4.5-Trichlorophenol . . . . .2.4.6-Trichlorophenol . . . . .
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNONONDNDNDNDKDNONONDNOND
3066
202
4
2
3
1
5
1038
4
2
6
6
3
88
8
2
10134
6124
3
366
0 KD - Not detected above the listed detection limit.
Analyst Notes: none
{*) NO • Not detected above the listed detection limit.
-»-
OT5BCW11 Page 7
ORGANIC ANALYSIS DATA6MD-H Sample NO:OT5BCWU-01 Dace Analyzed: 03-Feb-OO
Sample Type: Liquid
TENTATIVELY IDENTIFIED SEMI-VOLATILE COMPOUNDS BY METHOD 625units: ng/L
RT (lain)
(*) ANALYSTS N01spectral dat
( • * ) Estimated c
CAS «
FE: The compoundsa base or by mar
oncentration is
COMPOUND NAME (*)
NO ABN TIC'S detected in this sample.
3 listed are tentatively identified by the best match with the NISiual interpretation.
based on a Response Factor of 1.0 to the nearest internal scandal
Estimated |Concentration ( • • ) |
ST/EPA/Kiley mass
•d.
OT5BCW11 Page 8
PESTICIDE/PCB ANALYSIS
SAMPLE:SAMPLE TYPE:
GUIDANCE METHOD: OLC02.1
OT5BCW11-01LIQUID
DATE EXTRACTED: 2/2/2000DATE ANALYZED: 2/7/2000
CAS^
319-84-6319-85-7319-86-858-89-976-44-8309-00-21024-57-3949-98-860-57-172-55-972-20-833213-65-972-54-08742193-453494-70-510341-07-850-29-372-43-55103-71-95103-74-28001-35-212674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5
Alpha-BHCBeta-BHCDelta-BHCGamma-BHC (Lindane)HeptachlorAIdrinHeptachlor EpoxideEndosulfan IDieldrin4,4' DDEEndrinEndosulfan II4,4' -DDDEndrin AldehydeEndrin KetoneEndosulfan Sulfate4,4" -DDTMethoxychlorAlpha-ChlordaneGamma- ChlordaneToxapheneArodor 1016Arodor 1221Arodor 1232Arodor 1242Arodor 1248Arodor 1254Arodor 1260
RESULTSNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
DL0.010.010.010.010.010.010.010.010.020.020.020.020.020.020.020.020.020.100.010.011.000.200.400.200.200.200.200.20
ND = NOT DETECTEDDL = DETECTION LIMIT
OT5BCW11 Page 9US EPA REGION 6 LABORATORY
SAMPLED: OT5BCW11-01
SOURCE:MATRIX
ANALYSTS:
PARAMETER
ALUMINUMANTIMONYARSENICBARIUMBERYLLIUMCADMIUMCALCIUMCHROMIUMCOBALTCOPPERIRONLEADMAGNESIUMMANGANESEMERCURYNICKELPOTASSIUMSELENIUMSILVERSODIUMTHALLIUMVANADIUMZINC
MARION PRESSLUQUID
KD. BB, SH
CONCENTRATION
ND3.7ND24NDND
1980NDNDND32ND
363NDNDND
15805.7ND
735000NDNDND
IRE TREATING
DETECTIONLIMIT <=
1002.02.010
2.02.01502.02020252.0150
50.120
10002.010
5002.03020
DATES ANALYZED:14-FEB-OOTO
' UNITS Ml
UG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/L
.-...- UG/LUG/LUG/LUG/L
17-FEB-OO
ETHOD .
200.7200.8200.8200.7200.8200.8200.7200.8200.7200.7200.7200.8200.7200.7245.1200.7200.7200.8200.7200.7200.8200.7200.7
ND: LESS THAN DETECTION LIMIT
'V-
TKRCCTNRCC Laboratory
Report of AnalysisMar 07,2000 9:15AM
OT5BCW11 Page 10
TNRCC Sampler 00Matrix: LIQUIDCollected: 1/27/00 0:00Program: EnvironmentalCollection Site: Marion
Constituent Name
00698
ProtectioPressure
nT
Agencyreating
Group f : 20000224Depth:Received: 02/01/00
Result Unit
Chain of Custody ftStation ID:Collected by:
Prepared Analyzed
Region:
Method<0.02 mg/LCyanide, Total 02/08/00 7:25 335.2
End of Data for TNRCC Sample f: 0000698
Laboratory Approval: —>/) 07-Mar-OO
OT5BCW11 Page 11
U. S. Environmental Protection AgencyRegion 6 Houston Laboratory
Report For Sample Number OT5BCW1102
Source: MARION PRESSURE TREATINGSite Description: —
Date/Time Received: 1/31/2000 08:30 AM Date Completed 3/10/2000
Datemme Collected: 1/27/2000 12:06 PM
Sample Type; LIQUID
Comments:
ParameterABNCNEMHGMAAMICPP/P
VOA
DescriptionACID/BASE NEUTRALSCYANIDE
ESAT-MERCURY
GFAAS METALSICP METALS
PESTICIDES/POLYCHLORIHATED BIPHENYLS
VOLATILE ORGANIC ANALYSIS
OT5BCW11 Page 12Volatile Organic Compounds
Method CLP SOW OLM03.2 (low level)
Sample Number OT5BCW11-02
Sample Type: LIQUID
Date Extracted: not extracted
Date Analyzed: 05-Feb-OO
Compound page 1 of 1Chloromethane——————————————————————————Bromomethane——————————————————————————Vinyl Chloride——————————————————————————Chloroethane———————————————————————————Methylene Chloride———————————————•————————
• Acetone—————————————————————•—————————Carbon Disuffide—————————————————————————1,1-Dichloroethene————————————————————————1,1-Dichloroethane————————————————————————trane.«1 ^—rV^hlfwwH'ir'nr^ --— - ' ,
cis - 1 , 2 - D i c h l o r o e t h e n o — — — — - — • • • • • "•—————————^ L | - ^ — a — -Chloroform——————————————————————————•——1,2-Dichloroethane—————————————————————————2-Butanone———————————————————————————1,1.1 -Trichloroethane————————————————————————^^"srhrtM Tfi r's/^Mftri ft ———
Bromodichloromethane——————————————————————1,2-Dichloropropane———————————————————————cis-1,3-Dichloropropene——————————————————————Trichloroethene——————————————————————————Benzene——————————————————————————————Dibromochloromethane———————————————————————trans-1,3-Dichloropropene—————————————————————1.1,2-Trichtoroethane————————————————————————B romoform—————————————————————————————4-Methyl-2-Pentanone———————————————————————2-Hexanone————————————————————————————
1 4 0 0 "r&tr'B/^hlArAAth^i' r^— ••
Toluene—————————————————————————————Chlocobenzene——————————————————————————Ethylbenzene————————————————————————————Styrene———————————————————————————————
m/o-xylene————————————————————————————
results (ug/1)NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
detection limits11112511111115111111111115511111111
"ND" means not detected at the corresponding detection limit
OT5BCW11 Page 13Tentatively Identified Volatile Organic Compounds
Method CLP SOW OLM03.2 (low level)
Sample Number OT5BCW11-02
Sample Type: LIQUID
Date Extracted: not extracted
Date Analyzed: 05-Feb-OO
Number TICs found: 0
TICNO. CASNO. COMPOUND NAME*
RTmin.
EST.**CONC.
PS/I
• The compounds listed are tentatively identified by the best match with the NIST/Wiley mass spectral databaseand/or by manual interpretation.
** An estimated concentration is obtained by quantitafcon using the nearest internal standard. Since no standardwas used for confirmation nor quantitation, a response factor of 1.0 is assumed.
OT5BCW11 Page 14
ORGANIC ANALYSIS DATA6MD-HO Sample NO: OT5BCW11-02
SEMI-VOLATILE COMPOUNDS BY METHOD 625
(continuous extractor)units: ug/L
Date Analyzed: 03-Feb-OO
Sample Type: Liquid
units: ug/L
Compound Name Results* | Del Limits Compound Name Results* 1 Det Limits
Acenaphthene ...............Acenaphthylene .............Anthracene .................Benzole Acid ...............Benzo(a)Anthracene .........Benzo(a)Pyrene .............Benzo(blFluoranthene .......Benzo(g,h,l)Perylene .......Benzo{k)Fluorantbene .......Benzyl Alcohol .............bis(2-Chloroethoxy)Mettiane .bis(2-Chloroethyl) Btber ...bis(2-chloroisopropyl)Etherbis- (2-EthylhexyDPhthalate4-Bronophenylphenyl Ether ..Butylbenzylpbthalate .......Carbazole ..................4-Cnloroanlllne ............2-Chloronaphtbalene ........2-Chlorophenol .............«-Chlorophenylphenyl Ether .4-Chloro-3-Methylphenol ....Chrysene ...................Dibenzofuran ...............Dibenzo(a,h)Anthracene .....1.2-Dichlorobenzene ........1.3-Dichlorobenzene ........1.4-Dichlorobenzene ........3.3• -Dichlorobenzidlne .....2,4-Dichlorophenol .........Oiethylphthalate ...........2,4-Dlmethylphenol .........OimethylPhthalate ..........
NDNONDNDNDNONDNDNDNDNDNDNDHONDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
2
2
210
8
0.2
as
3
3
3
10
6
2
6
2
2,4-Dlnltrophenol . . . . . . . . .2,4-Dinitrotoluene . . . . . . . .2,6-Dinitrotoluene . . . . . . . .4,6-Dinitro-2 -MethylphenolDi-n-Butylphthalate . . . . . . .Di-n-Octyl Phthalate . . . . . .Fluoranthene . . . . . . . . . . . . . .Fluorene . . . . . . . . . . . . . . . . . .Hexachlorobenzene . . . . . . . . .Hexachlorobutadiene . . . . . . .Hexachlorocyclopentadiene .Hexachloroethane . . . . . . . . . .Indeno(l,2,3-cd) Pyrene . . .Isophorone . . . . . . . . . . . . . . . .2-Methylnaphtbalene . . . . . . .2-Methylphenol . . . . . . . . . . . .4-Methylphenol . . . . . . . . . . . .Naphthalene . . . . . . . . . . . . . . .2-Nicroanlline . . . . . . . . . . . .3-Nitroaniline . . . . . . . . . . . .4-Nitroaniline . . . . . . . . . . . .Nitrobenzene . . . . . . . . . . . . . .2-Nitrophenol . . . . . . . . . . . . .4-Nierpphenol . . . . . . . . . . . . .N-Nitrosodiphenylamine . . . .N-MlCroso-Di-n-PropylaminePentachlorophenol . . . . . . . . .Phenanthrene . . . . . . . . . . . . . .Phenol . . . . . . . . . . . . . . . . . . . .Pyrene . . . . . . . . . . . . . . . . . . . .1,2,4-Trichlorobenzene . . . .2.4.5-Trichlorophenol . . . . .2.4.6-Trichlorophenol . . . . .
NDNDNDNDNONDNDNDNDNDNDNDNDKDNDNDNDNDNDNONDNONDNONONDNDNONDNDNDNOND
30
6
6
20
2
4
2
2
1
5
10
38
4
8
2
10
13
4
6
1
2
4
2
3
66
(•) ND - Not detected above the listed detection limit.
Analyst Notes: none
(*) ND - Not detected above the listed detection limit.
OT5BCW11 Page 15
ORGANIC ANALYSIS DATA6MD-H Sample NO:OT5BCW11-02 Date Analyzed: 03-Feb-OO
Sample Type: Liquid
TENTATIVELY IDENTIFIED SEMI-VOLATILE COMPOUNDS BY METHOD 625unite: ug/L
RT (min)
——————————
—————————
( • ) ANALYSTS MOIspectral dat
( • • ) Estimated c
I CAS «
I
——————————
FE: The compoundsa base or by man
oncentration is
COMPOUND NAME (*)
Ho ABN TIC'S detected in this sample.
•
listed are tentatively Identified by the best match with the HISmal interpretation.
based on a Response Factor of 1.0 to the nearest internal standaz
EstimatedConcentration { • • )
ST/EPA/Hiley mass
rd.
OT5BCW11 Page 16
PESTICIDE/PCB ANALYSISGUIDANCE METHOD: OLC02.1
SAMPLE:SAMPLE TYPE:
OT5BCW11-02LIQUID
DATE EXTRACTED: 2/2/2000DATE ANALYZED: 2/7/2000
CAS#
319-84-6319-85-7319-86-858-89-976-44-8309-00-21024-57-3949-98-860-57-172-55-972-20-833213-65-972-54-08742193-453494-70-510341-07-850-29-372-43-55103-71-95103-74-28001-35-212674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5
Alpha-BHCBeta-BHCDelta-BHCGamma-BHC (Lindane)HeptachlorAldrinHeptachlor EpoxideEndosulfan IDieldrin4.4' DDEEndrinEndosutfan II4.4' -DDDEndrin AldehydeEndrin KetoneEndosulfan Sulfate4,4' -DDTMethoxychlorAlpha-ChlordaneGamma- ChlordaneToxapheneAroclor1016Aroclor 1221Aroclor 1232Aroclor 1242Aroclor 1248Aroclor 1254Aroclor 1260
RESULTSNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND .NDNDNDNDNDND
DL0.010.010.010.010.010.010.010.010.020.020.020.020.020.020.020.020.020.100.010.011.000.200.400.200.200.200.200.20
WD=//OF DETECTEDDL = DETECTION LIMIT
OT5BCW11 Page 17US EPA REGION 6 LABORATORY
SAMPLE #:
SOURCE:MATRIX
ANALYSTS:
PARAMETER
ALUMINUMANTIMONYARSENICBARIUMBERYLLIUMCADMIUMCALCIUMCHROMIUMCOBALTCOPPERIRONLEADMAGNESIUMMANGANESEMERCURYNICKELPOTASSIUMSELENIUMSILVERSODIUMTHALLIUMVANADIUMZINC
OT5BCW11-02
MARION PRESSUUQUID
KD.BB, SH
CONCENTRATION
NDNDND18NDND
1460NDNDND49ND
322NDNDND
14403.6ND
560000NDNDND
IRE TREATING
DETECTIONLIMIT <=
1002.02.010
2.02.01502.02020252.0150
50.120
10002.010
5002.03020
DATES ANALYZED:14-FEB-OO TO
UNITS Ml
UG/LUG/LUG/LUG/LUG/LUG/L
• "• UG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/L"UG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/L
17-FEB-OO
ETHOD
200.7200.8200.8200.7200.8200.8200.7200.8200.7200.7200.7200.8200.7200.7245.1200.7200.7200.8200.7200.7200.8200.7200.7
ND: LESS THAN DETECTION LIMIT
TNRCC LaboratoryReport of AnalysisMar 07,2000 9:1 SAM
OT5BCW11 Page 18
TNRCC Sample «: 0000699 Group«: 20000224Matrix: LIQUID Depth:Collected: 1/27/DO 0:00 Received; 02/01/00Program: Environmental Protection AgencyCollection Site: Marion Pressure Treating
Chain of Custody < Region:Station ID:Collected by:
Cyanide, TotalConstituent Name Result_____Unit______Prepared_____Analyzed______Method
<0.02 mg/L 02/08/00 7:25 335.2End of Data for TNRCC Sample S: 0000699
^ ^Laboratory Approval; -^y^________________ 07-Mar-oo
OT5BCW11 Page 19
U. S. Environmental Protection AgencyRegion 6 Houston Laboratory
Report For Sample Number OT5BCW1103
Source: MARION PRESSURE TREATINGSite Description: -,_
Date/Time Received: 1/31/2000 08:30 AM Date Completed 3/10/2000
Date/Time Collected: 1/27/2000 12:12 PM
Sample Type: LIQUID
Comments:
Parameter DescriptionABN ACID/BASE NEUTRALS
CN CYANIDE
EMHG ESAT-MERCORY
MAA GFAAS METALSMICP ICP METALSP/P PESTICIDES/POLYCHLORIKATED BIPHENYLS
VOA VOLATILE ORGANIC ANALYSIS
OT5BCW11 Page 20Volatile Organic Compounds
Method CLP SOW OLM03.2 (low level)
Sample Number OT5BCW11-03
Sample Type: LIQUID
Date Extracted: not extracted
Date Analyzed: 05-Feb-OO
Compound page 1 of 1Chloromethane——————————————————————————Bromomethane——— ——Vinyl Chloride—————————————————————Chloroethane————————————————————————————Methylene Chloride————————————————————————A^otnnft
Carbon Disuffide—————————————————————————11-Dichtoroethene——11-Dichloroethane———————————————————trans-1,2-Dichloroethene—————————————————————ds -1 2-Dichloroethene^l»lo»r<* «•—»Chloroform————————————————————————————
2-Butanone—————————————————————————————1.1,1-Trichloroethane———————————————————————Carbon Tetrachloride———————————————————————Bromodichloro me thane———————————————————————1,2-DichIoropropane————————————————————————ds-1,3-Dichloropropene———————————————————————Trich loroethene———————————————————————————Benzene—————————————————————————————Dibromochloromethane———————————————————————trans-1,3-Dichloropropene—————————————————————1,1,2-Tricnloroethane————————————————————————Brornofomn——————————•—————————————————4-Methyl-2-Pentanone———————————————————————2-Hexanone——————————————————————————————Tetrachloroethene————————————————————————11,2,2-Tetrachloroethane—————————————————————Toluene——————————————————————————————Chlorobenzene———————————————————————————Ethylbenzene———————————————————————————Styrene————;————————————————————————r\ v^flcmJfi —••
m/p-xylene—————————————————————————————
results (ug/l)NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
- NDNDNDNDNDNDNDNDND
detection limits11112511111115111111111115511111111
"ND" means not detected at the corresponding detection limit.
OT5BCW11 Page 21Tentatively Identified Volatile Organic Compounds
Method CLP SOW OLM03.2 (low level)
Sample Number. OT5BCW11-03
Sample Type: LIQUID
Date Extracted: not extracted
Date Analyzed: 05-Feb-OO
Number TICs found:
TICNO. CAS NO. COMPOUND NAME*
RTmin.
EST.**CONC.
V9/1
• The compounds Bsted are tentatively identified by the best match w'rth the NtST/Wiley mass spectral databaseand/or by manual interpretation.
** An estimated concentration is obtained by quantitation using the nearest internal standard. Since no standardwas used for confirmation nor quantitation, a response factor of 1.0 is assumed.
OT5BCW11 Page 22
ORGANIC ANALYSIS DATA6MD-HO Sample OT5BCW11-03 Date Analyzed: 03-Feb-OO
Sample Type: Liquid
SEMI-VOLATILE COMPOUNDS BY METHOD 625(continuous extractor)
units: ug/L units > ug/L
1 Name
teid .................
cohol ...............
oroethyl) Ether .....
AylhexyllRitbalate ..
Eyiphthalate .........
3-Methylphenol ......
thalate .............
hthalate ............
| Results*
....... KDWD
....... SD
....... KD
....... KD
....... SDffr\
....... ND
....... ND
....... ND
....... ND
....... ND
....... ND
....... ND
....... ND
....... ND
....... ND
....... ND
....... ND
....... ND
....... ND
....... ND
....... ND
UT)
....... KDMT^
....... ND
....... ND
....... ND
....... NDMT1
....... MD
Del Limits
1aa
108
o.as884a2
a4B4a4
a488828333
106a62
Codipound Name
2,4-Dinitrophenol ...........
4,6-Dinitro-a-Methylphenol ..Di-n-Butylphthalate .........Di-n-Octyl Phthalate ........
2-Kethylnaphthalene .........2-Methylphenol ..............4-Methylphenol ..............Naphthalene .................2-Nitroaniline ..............3-Nitroaniline ..............4-Nitroaniline ..............
2-Nltrophenol ...............4-Nitrophenol ...............
Pentachlorophenol ...........
Pyrene ......................
| Results* |
......... ND
......... ND
......... ND
......... ND
......... ND
......... ND
......... ND
......... ND
......... ND
......... ND
......... NDMn
......... ND
......... ND
......... ND
......... ND
......... ND........ ND
unMTt
......... ND........ ND........ NO........ ND........ ND........ ND....'.... ND
......... ND........ ND........ ND........ ND........ ND........ ND
Del Limits
306fi
2024221
51038426628882
1013
461
243366
0 KD - Not detected above the listed detection limit.
Analyst Notes: none
(*) ND • Not detected above the listed detection limit.
OT5BCW11 Page 23
ORGANIC ANALYSIS DATA6MD-H Sample NO:OT5BCW11-03 Date Analyzed: 03-Feb-OO
Sample Type: Liquid
TENTATIVELY IDENTIFIED SEMI -VOLATILE COMPOUNDS BY METHOD 625unite: ug/L
EstimatedRT (min) CAS • COMPOUND NAME (*) Concentration (*•) |
16.6 638675 Tricosane 1„.-- „——.„——-—— -——.. . . . . . .„ .——.. . . - . - . . -„————.-——————.————„——.—— -.--——.——17.0 Onknown SC Paraffin a
17.5 Unknown SC Paraffin 1
I
I
(*) ANALYSTS NOTE: The compounda listed are tentatively identified by the best match with the NIST/EPA/oiley mass•pectral data base or by manual interpretation.
(**) Estimated concentration is based on a Response Factor of 1.0 to the nearest internal ctandard.
OT5BCW11 Page 24
PESTICIDE/PCB ANALYSISGUIDANCE METHOD; OLC02.1
SAMPLE:SAMPLE TYPE:
OT5BCW11-03LIQUID
DATE EXTRACTED: 2/2/2000DATE ANALYZED: 2/7/2000
CAS#
319-84-6319-85-7319-86-858-89-976-44-8309-00-21024-57-3949-98-860-57-172-55-972-20-833213-65-972-54-08742193-453494-70-510341-07-850-29-372-43-55103-71-95103-74-28001-35-212674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5
Alpha-BHCBeta-BHCDelta-BHCGamma-BHC (Lindane)HeptachlorAldrinHeptachlor EpoxideEndosulfan IDieldrin4,4' DDEEndrinEndosulfan II4,4' -DDDEndrin AldehydeEndrin KetoneEndosulfan Sulfate4,4' -DDTMethoxychlorAlpha-ChlordaneGamma- ChlordaneToxapheneAroclor1016Arodor 1221Aroclor 1232Arodor 1242Aroclor 1248Arodor 1254Aroclor 1260
RESULTSNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
DL0.010.010.010.010.010.010.010.010.020.020.020.020.020.020.020.020.020.100.010.011.000.200.400.200.200.200.200.20
ND = NOT DETECTEDDL = DETECTION LIMIT
OT5BCW11 Page 25US EPA REGION 6 LABORATORY
SAMPLED
SOURCE:MATRIX
ANALYSTS:
PARAMETER
ALUMINUMANTIMONYARSENICBARIUMBERYLUUMCADMIUMCALCIUMCHROMIUMCOBALTCOPPERIRONLEADMAGNESIUMMANGANESEMERCURYNICKELPOTASSIUMSELENIUMSILVERSODIUMTHALLIUMVANADIUMZINC
OT5BCW11-03
MARION PRESSLLIQUID
KD. BB, SH
CONCENTRATION
NDNDND17NDND
1460NDNDND74ND
312NDNDND
14203.4ND
618000NDNDND
IRE TREATING
DETECTIONUMIT <=
1002.02.010
2.02.01502.02020252.0150
50.120
10002.010
5002.03020
DATES ANALYZED:14-FEB-OOT
UNITS
UG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/LUG/L
•O 17-FEB-OO
METHOD
200.7200.8200.8200.7200.8200.8200.7200.8200.7200.7200.7200.8200.7200.7245.1200.7200.7200.8200.7200.7200.8200.7200.7
ND: LESS THAN DETECTION LIMIT
TNRCC LaboratoryReport of AnalysisMar 07,2000 9:1 SAM
OT5BCW11 Page 26
TNRCC Sample «: 0000700 Group »: 20000224Matrix: LIQUID Depth;Collected: 1/27/00 0:00 Received: 02/01/00Program: Environmental Protection AgencyCollection Site: Marion Pressure Treating
Chain of CustodyStation ID:Collected by:
Region:
Constituent Name Result______Unit______Prepared____Analyzed______MethodCyanide, Total <0.02 mg/L 02/08/00 7:25 335.2
End of Data for TNRCC Sampled 0000700
Laboratory Approval:^^_________________ 07-Mar-oo
OT5BCW11 Page 27
U. S. Environmental Protection AgencyRegion 6 Houston Laboratory
Report For Sample Number OT5BCW1104
Source: MARION PRESSURE TREATINGSite Description: «,
Datemme Received: 1/31/2000 08:30 AM Date Completed 3/10/2000
Date/Time Collected: 1/27/2000 12:30 PM
Sample Type: LIQUID
Comments:
Parameter DescriptionVOA VOLATILE ORGANIC ANALYSIS
OT5BCW11 Page 28Volatile Organic Compounds
Method CLP SOW OLM03.2 (low level)
Sample Number OT5BCW11-04
Sample Type: LIQUID
Date Extracted: not extracted
Date Analyzed: 05-Feb-OO
Compound page 1 of 1Chloromethane———————————————————————————Bromomethane——————————————————————————Wnyl Chloride——————————————————————————Chloroethane———————————————————————————Methylene Chloride—————————————————————————Acetone——————————————————————————————Carbon Disulfide—————————————————————————Il.rv^hlrtmcifhr'n/ft—— •i
1,1-Dichloroethane—————————————————————————trans-1,2-Dichloroethene—————————————————————cis -1,2-Dichloroethene——————————————————————Chloroform————————————————————————————1,2-Dichtoroethane—————————————————————————2-Butanone—————————————————————————————1 11-Trichloroethane————————————————————————Carbon Tetrachloride———————————————————————Bromodichtoromethane————•—————————————————1,2-Oichloropropane————————————————————————cis-1,3-Dichloropropene——————————————————————
Benzene—————————————————————————————Dibromochloromethane———————————————————————trans-1,3-Dichloropropene—————————————————————1 1 OaTri hlftrr^rhthcii'iA———
Bromoform————————————————————————————4-Methyl-2-Pentanone———————————————————————2-Hexanone——————————————————————————————Tetrachloroethene—————————————————————————
Toluene—————————————————————————————Chlorobenzene——————————————————————————Ethylbenzene————————————————————————————Styrene—————————————————————————————
m/n-Yvlianp—————.—————————~——-—.—.—...—.————————
results (ug/1)NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
detection limits11112511111115111111111115511111111
"ND" means not detected at the corresponding detection limit
OT5BCW11 Page 29Tentatively Identified Volatile Organic Compounds
Method CLP SOW OLM03.2 (low level)
Sample Number OT5BCW11-04
Sample Type: LIQUID
Date Extracted:
Date Analyzed:
not extracted
05-Feb-OO
Number TICs found: 0
TICNO. CAS NO. COMPOUND NAME*
RTmin.
EST-CONC.
tig/l
* The compounds listed are tentatively identified by the best match w'rth the NIST/Wiley mass spectral databaseand/or by manual interpretation.
** An estimated concentration is obtained by quantitation using the nearest internal standard. Since no standardwas used for confirmation nor quantitation, a response factor of 1.0 is assumed.
OT5BCW11 Page 30
U. S. Environmental Protection AgencyRegion 6 Houston Laboratory
Report For Sample Number OT5BCW1105
Source: MARION PRESSURE TREATINGSite Description: -g
Date/Time Received: 1/31/2000 08:30 AM Date Completed 3/10/2000
Date/Time Collected: 1/27/2000 01:00 PM
Sample Type: LIQUID
Comments:
Parameter DescriptionVOA VOLATILE ORGANIC ANALYSIS
•?-
OT5BCW11 Page 31Volatile Organic Compounds
Method CLP SOW OLM03.2 (low level)
Sample Number OT5BCW11-05
Sample Type: LIQUID
Date Extracted: not extracted
Date Analyzed: 05-Feb-OO
Compound page 1 of 1Chtoromethane——————————————————————————Brornomethane——————————————————————————Vinyl Chloride——————————————————————————Chloroethane———————————————————————————Methylene Chloride—————————————————————————Acetone—————————————————————————————Carbon Disulfide—————————————————————————1,1 -Dichloroethene—————————————————————————1,1 -Dichloroethane—————————————————————————trans-1,2-Dichloroethene—————•——————————————cis -1,2-Dichloroethene———————————————————————^^« • »- -Chloroform—————————————————————————————1,2-Dichloroethane————————————————————————2-Butanone———————————————————————————1.1,1 -Trichloroethane———————————————————————Carbon Tetrachtoride———————————————————————Bromodichloromethane——————————————————————1,2-Dichtoropropane————————————————————————ds-1,3-Dichloropropene——————————————————————Trichloroethene———————————————————————————R&I^^AF*^ ^k^ • u — ^ — — — — — — k
Dibromochloromethane——————————————————:———trans-1.3-Dichloropropene—————————————————————1.1,2-Trichloroethane————————————————————————Bromofonn————————————————————————————4-Methyl-2-Pentanone——————————————————————2-Hexanone—————————————————————————————Tetrachloroethene————————————————————————1.1,2,2-Tetrachloroethane—————————————————————Toluene—————————————————————————————Chlorobenzene————"—————————————————————Ethylbenzene————————————————————————————Styrene——————————————————————————————
m/p-xylene—————————————————————————————
results (ug/l)NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNONDNDNDNDNDNDNDNDND
- NDNDNDND
detection limits11112511111115111111111115511111111
"ND" means not detected at the corresponding detection limit
OT5BCW11 Page 32Tentatively Identified Volatile Organic Compounds
Method CLP SOW OLM03.2 (low level)
Sample Number. OT5BCW11-05
Sample Type: LIQUID
Date Extracted:
Date Analyzed:
not extracted
05-Feb-OO
Number TICs found: 0
TICNO. CAS NO. COMPOUND NAME*
RTmin.
EST."CONC.
PS/I
* The compounds listed are tentatively identified by the best match with the NIST/Wiley mass spectral databaseand/or by manual interpretation.
** An estimated concentration Is obtained by quantitation using the nearest internal standard. Since no standardwas used for confirmation nor quantitation, a response factor of 1.0 is assumed.-
OT5BCW11 Page 33
WATER VOLATILE SYSTEM MONITORING COMPOUND RECOVERY
Instrument ID:Set Number OT5BCW11
System 5-HP 5972
Method: CLPSOWO
Set Name: MARION PRES Column Info: 0.25 -HP-624
010203040506070809
EPASAMPLE NO.
OT5BCW11-BLKOT5BCW11-DLOT5BCW11-01OT5BCW11-01 MOT5BCW11-01 MOT5BCW11-02OT5BCW11-03OT5BCW11-04OT5BCW11-05
SMC1(DCE) «
10310398
10010197
10298
101
SMC2(TOL) H-
102106959999
1001009899
SMC3(BFB) #
1021069498
1011009798
101
TOTOUT
000000000
SMC1 (DCE)SMC2 (TOL)SMC3 (BFB)
1,2-Dichloroethane-d4Toluene-dSBromofluorobenzena
QC LIMITS(76-114)(88-110)(86-115)
ff Column to be used to flag recovery values* Values outside of contract required QC limitsD System Monitoring Compound diluted out
page 1 of 1
OT5BCW11 Page 34
WATER VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY
Set Name: MARION PRESSURE TRE Lab File: V50F0509.DMethod: CLPSOWOEPA Sample No.OTSBCW11-01
Set Number OT5BCW11Sample Type: LIQUID
COMPOUND1,1-DichloroetheneTrichloroetheneBenzeneTolueneChlorobenzene
SPIKEADDEDM)
5050505050
SAMPLECONCENTRATION
(ug/i)0.00.00.00.00.0
MSCONCENTRATION
W)5247504848
MS%
REC<1
10494
1009696
QCLIMITSREC.
61 - 14571 - 17076- 12776- 12575- 130
COMPOUND-1,1-DichloroetheneTrichloroetheneBenzeneTolueneChlorobenzene
SPIKEADDED
frig/I)5050505050
MSDCONCENTRATION
W)4746514948
MSD%
REC<?9492
1029896
%RPD#
102220
QCLRPD
14141 11313
IMITSREC.
61 - 14571 - 17076- 12776- 12575- 130
ft Column to be used to flag recovery and RPD values with an asterisk* Values outside of QC limitsRPD: 0 out of 5 outside limitsSpike Recovery: 0 out of 10 outside limitsCOMMENTS:
Lab Name:
Lab Code:
- 2CWATER SEM1VOLATILE SURROGATE RECOVERY
US EPA REGION 6 LABORATORY Contract:
OT5BCW11 Page 35
SiteNam Marion Pr SASNo.: Act.#: OTCW11
010203040506
Sample No.:OCW11-BLKOCW11-01OCW11-01MSOCW11-01MSDOCW11.02OCW11-03
S12FP #
696875657574
S2PHL #
716776677875
S32CP #
757282698079
S4DCB «
626371606868
S5NBZ #
827685708482
S6FBP#
867781698279
S7TBP #
848491808899
S8TPH #
898380708388
TOT •OUT
000000
81 2FP52 PHL53 2CP54 DCB55 NBZ56 FBP57 TBP58 TPH
QC LIMITS2-Fluorophenol (surrt) (30-106)Phenol-dS (surr2) (27-112)2-Chlorophenol-d4 (surr3) (39-105)1 -Dichlorobenzene-(14(sun4) (42-103)Nitrobenzene-dS (surr5) (29-121)2-Fluoroblphenyl (SUITS) (36-111)2,4,6-Tribromophenol (surr7) (29-129)(114-Terphenyl (surr8) (39-135)
# Column to be used to flag recovery values* Values outside of contract required QC limitsD Surrogate diluted out
page 1 of 1 FORM II SV-1 3/90
3C OT5BCW11 Page 36WATER SEMIVOLAT1LE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY
Lab Name:Lab Code:
US EPA REGION 6 LABORATORY Contract:SiteNam Marion Pr SASNo.: OTCW11 Act.#:
Matrix Spike- Sample No.: OCW11-01
COMPOUNDPhenol2-ChlorophenoI1,4-DichlorobenzeneN-Nitroso-di-propylamine1,2,4-Trichlorobenzene4-Chloro-3-methylphenolAcenaphthene4-Nitrophenol2,4-DinitrototuenePentachlorophenotPyrene
SPIKEADDED(ug/L)
1010
5.05.05.010
5.0105.0105.0
SAMPLECONCENTRATION
(ug/L)0.00.00.00.00.00.00.00.00.00.00.0
MSCONCENTRATION
(ug/L)6.37.22.82.83.17.13.46.13.57.74.0
MS%
REC#6372565662716861707780
QCLIMITSREC.
40- 9747- 9841 - 9426- 1 1 141 • 9932- 10941 - 10432- 13041 • 10640 - 13652- 122
COMPOUNDPhenol2-ChlorophenoI1,4-DichlorobenzeneN-Nitroso-di-propylamine1,2,4-Trichloroben2ene4-Chloro-3-methylphenolAcenaphthene4-Nitrophenol2,4-DinitrotoluenePentachloropheno!Pyrene
SPIKEADDED(ug/L)
10105.05.05.0105.0105.0105.0
MSDCONCENTRATION
(ug/L)5.66.12.42.42.86.22.95.63.17.03.4
MSD%
REC#5661484856625856627068
%RPD#
121715151014169
121016
QCLRPD
2926245025394333343022
IMITSREC.
40 - 9747 - 9841 - 9426 - 1 1 141 - 9932 - 10941 - 10432 - 13041 - 10640 - 13652 - 122
# Column to be used to flag recovery and RPD values with an asterisk• Values outside of QC limitsRPD: 0 out of 11 outside limitsSpike Recovery: 0 out of 22 outside limitsCOMMENTS:
FORM III SV-1 3/90
OT5BCW11 Page 37
PESTICIDE/PCB SURROGATE REPORTU.S. ENVIRONMENTAL PROTECTION AGENCY
HOUSTON LABORATORY BRANCH
INSTRUMENT: GC7 (HP-689<nCOLUMNS: DB-35MS COLUMNS: DB-5MSCOLUMN LENGTH: 30m COLUMN LENGTH (m): 30mCOLUMN ID: 0.32mm COLUMN ID (mm): 0.32mm
EPA SAMPLE NUMBER
OT5BCW11-BLKOT5BCW11-01MSOT5BCWI1-01MSDOT5BCW11-01OT5BCW11-02OT5BCW11-03
TCMX%REC
638081778380
DCB% REC
1029597919691
TCMXOut
000000
DCB Out
000000
Q.C. LIMITS-WATERWARNING 61-94 60-114ACTION 52-103 47-127
• a Values outside ofQC Kmlts
N.D. = CAN NOT DETECTED DUE TO INTERFERENCES
OT5BCW11 Page 38
WATER PESTICIDE MATRIX SPIKE / MATRIX SPIKE DUPLICATE REPORT
Lab Name: U.S. EPA Houston Lab6MD-HOLab Code:
Matrix Spike - EPA Sample No.:Date Extracted: 2/2/00Date Analyzed: __2/7/00
Case No.: __________OT5BCW11-01. 01MS, 01MSD
COMPOUND
LINDANEHEPTACHLORALDRINDIELDRINENDRINDDT
spike
(ug/ml)
0.05000.05000.05000.10000.10000.1000
concentration in• Sample
(rg/mi I000000
MSRECOVERY
( "9/ml 1
0.03670.03170.03730.07600.08460.0769
MS%
REC#
73.4%63.5%74.5%75.0%84.6%76.9%
QC.LimitsREC.
56-12340-13140-12052-12656-12138-127
COMPOUND
LINDANEHEPTACHLORALDRINDIELDRINENDRINDDT
spike
(yg/ml)
0.05000.05000.05000.10000.10000.1000
MSDRECOVERY
("gl0.03650.02960.0371
. 0.07390.08320.0826
MSD•/.
REC
73.0%59.2%74.2%73.9%83.2%82.6%
%RPDS
0.5%6.9%0.4%1.5%1.7%7.2%
QCLRPD
152022182127
JmttsREC.
56-12340-13140-12052-12656-12138-127
# = column to be used to flag recovery and RPD values with an asterisk
* e values outside of QC limits
OT5BCW11 Page 39Quality Control Report - Metals Laboratory
Site Name: MARION PRESSURE TREATINGSample«: OT5BCW1101
Date Received:. Date Reported:
31-Jan-OO25-Feb-OO
Quality Control for Sample Numbers: OT5BCW1101-03AQ (DWMCLS)
105%96°/o87%99%96%
Sb 123AS 75Be 9Cd 111Cr 52Pb 208Se 82Tl 205
Comments:
27533.530.534.533.637.033.836.8
27533.331.234.433.737.533.537.8
DLDLDLDLDLDLDLDL
0.00.62.30.30.31.30.92.7
0.92 104%95%95%101%102%102%98%99%
106%92% 1.43
105%
ALL SAMPLES AND SPIKES @ 1:4 DILUTIONAN ADDITIONAL 10 ug/l WAS ADDED TO THE SPIKE & SPIKE DUP
DL0 Detection Limits
Acceptable Percent Recovery Range = 75-125%Acceptable Relative Percent Difference = < 20
OT5BCW11 Page 40U.S. EPA Region 6 Laboratory
Quality Control Report - Metals Laboratory
Site Name: MARION PRESSURE TREATINGSample«: OT5BCW1101
Date Received:Date Reported:
QuaBty Control for Sample Numbers: OT5BCW1101-03 AQ HSL
31-Jan-OO25-Feb-OO
Comments: a) ANALYTICAL ADD ON OF DIGESTED PREP BLANK WAS 1 1 3 % FOR Cu
DL= Detection Limits
Acceptable Percent Recovery Range = 75-125%Acceptable Relative Percent Difference = < 20
2/15/00Data File:Method File:Sample Table
13:09CN021500CN
File: CN021500
Standard Set #1 OT5BCW11 Page 41
S2Concentration
Peak66 545836 109814 86097 52432 61750 0000
Value0.50000.25000.10000.05000.02000.0000
Calc0.49130.26410.10540.05070.0140-0.0055
Coefficients;Intercept :Slope :Std Dev :Corr Coef :R^2 :
-0.0055130.0074660.009614770.9989960.997994
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PRQJ.NO. j PROJECT N A M E ~ " ' " ] ] / / A./ / / / " '
^-^3 I /W; P/^(/^ Trec^ NO. ///^y//SAWLERS.CT< ./ n w / / r^f^y / /^^/^J^________ coN. A)/^^^ REMARKS
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ReUdfluished by: «rMiucJ Date/Time Received by:/yig»wrur»/ Relinquished by: ^niww; Date/Time Received by: (S f»«n»/«;
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Relinquished by: (SifimunI Date /Time Received foyLaboratpfy by: i Dite /Time Remarks_________ , I | ' >gfe ^^ , , ^SMppedby: ^e.^fey lAirbmNumbe / igy C l / &T ok
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