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L1218042
Anchor QEA, LLC
120782-01.01
NEWTOWN CREEK RI
Client:
Project Name:
Project Number:
11/05/12
320 Forbes Boulevard, Mansfield, MA 02048-1806
Lab Number:
Report Date:
508-822-9300 (Fax) 508-822-3288 800-624-9220 - www.alphalab.com
720 Olive Way
Suite 1900
Delaney PetersonATTN:
ANALYTICAL REPORT
Seattle, WA 98101
Certifications & Approvals: NY (11627), CT (PH-0141), NH (2206), NJ NELAP (MA015), RI (LAO00299), PA (68-02089), LA NELAP (03090),FL (E87814), TX (T104704419), WA (C954), DOD (L2217.01), USDA (Permit #P330-11-00109), US Army Corps of Engineers.
(206) 287-9130Phone:
The original project report/data package is held by Alpha Analytical. This report/data package is paginated and should be reproduced only in itsentirety. Alpha Analytical holds no responsibility for results and/or data that are not consistent with the original.
Serial_No:11051209:46
Page 1 of 279
L1218042-01
L1218042-02
L1218042-03
L1218042-04
L1218042-05
L1218042-06
L1218042-07
L1218042-08
L1218042-09
L1218042-10
L1218042-11
L1218042-12
L1218042-13
L1218042-14
L1218042-15
L1218042-16
L1218042-17
L1218042-18
L1218042-19
L1218042-20
L1218042-21
L1218042-22
L1218042-23
L1218042-24
L1218042-25
L1218042-26
L1218042-27
L1218042-28
L1218042-29
L1218042-30
L1218042-31
Alpha Sample ID
TN005SG-000014-20121005
TN005SG-000014-20121005
TN002SG-000011-20121005
TN002SG-000011-20121005
TN003SG-000015-20121005
TN003SG-000015-20121005
TN004SG-000015-20121005
TN004SG-000015-20121005
TN006SG-000015-20121005
TN006SG-000015-20121005
SG-RB-20121006
SG-RB-20121006
HB008SG-000015-20121006
HB008SG-000015-20121006
HB007SG-000015-20121006
HB007SG-000015-20121006
HB006SG-000015-20121006
HB006SG-000015-20121006
HB005SG-000015-20121006
HB005SG-000015-20121006
HB1005SG-000015-20121006
HB1005SG-000015-20121006
HB004SG-000015-20121006
HB004SG-000015-20121006
HB003SG-000015-20121006
HB003SG-000015-20121006
HB002SG-000015-20121006
HB002SG-000015-20121006
HB001SG-000015-20121006
HB001SG-000015-20121006
SG-TB-20121006
Client ID
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Not Specified
Sample Location
NEWTOWN CREEK RI
120782-01.01
Project Name:Project Number:
Lab Number: Report Date:
L121804211/05/12
10/05/12 09:32
10/05/12 09:32
10/05/12 10:41
10/05/12 10:41
10/05/12 11:24
10/05/12 11:24
10/05/12 11:46
10/05/12 11:46
10/05/12 13:16
10/05/12 13:16
10/06/12 09:05
10/06/12 09:05
10/06/12 09:55
10/06/12 09:55
10/06/12 10:45
10/06/12 10:45
10/06/12 11:30
10/06/12 11:30
10/06/12 12:19
10/06/12 12:19
10/06/12 12:19
10/06/12 12:19
10/06/12 13:27
10/06/12 13:27
10/06/12 14:21
10/06/12 14:21
10/06/12 15:05
10/06/12 15:05
10/06/12 15:54
10/06/12 15:54
10/06/12 16:23
Collection Date/Time
Serial_No:11051209:46
Page 2 of 279
L1218042-32
Alpha Sample ID
SRM 1650B
Client ID
Not Specified
Sample Location
10/06/12 12:00
Collection Date/Time
Serial_No:11051209:46
Page 3 of 279
NEWTOWN CREEK RI
120782-01.01
Project Name:
Project Number:
Lab Number:
Report Date:L1218042
11/05/12
Case Narrative
The samples were received in accordance with the Chain of Custody and no significant deviations were encountered during the preparation
or analysis unless otherwise noted. Sample Receipt, Container Information, and the Chain of Custody are located at the back of the report.
Results contained within this report relate only to the samples submitted under this Alpha Lab Number and meet all of the requirements of
NELAC, for all NELAC accredited parameters. The data presented in this report is organized by parameter (i.e. VOC, SVOC, etc.). Sample
specific Quality Control data (i.e. Surrogate Spike Recovery) is reported at the end of the target analyte list for each individual sample,
followed by the Laboratory Batch Quality Control at the end of each parameter. If a sample was re-analyzed or re-extracted due to a
required quality control corrective action and if both sets of data are reported, the Laboratory ID of the re-analysis or re-extraction is
designated with an "R" or "RE", respectively. When multiple Batch Quality Control elements are reported (e.g. more than one LCS), the
associated samples for each element are noted in the grey shaded header line of each data table. Any Laboratory Batch, Sample Specific %
recovery or RPD value that is outside the listed Acceptance Criteria is bolded in the report. Performance criteria for CAM and RCP methods
allow for some LCS compound failures to occur and still be within method compliance. In these instances, the specific failures are not
narrated but are noted in the associated QC table. This information is also incorporated in the Data Usability format for our Data Merger tool
where it can be reviewed along with any associated usability implications. Soil/sediments, solids and tissues are reported on a dry weight
basis unless otherwise noted. Definitions of all data qualifiers and acronyms used in this report are provided in the Glossary located at the
back of the report.
In reference to questions H (CAM) or 4 (RCP) when "NO" is checked, the performance criteria for CAM and RCP methods allow for some
quality control failures to occur and still be within method compliance. In these instances the specific failure is not narrated but noted in the
associated QC table. The information is also incorporated in the Data Usability format of our Data Merger tool where it can be reviewed
along with any associated usability implications.
Please see the associated ADEx data file for a comparison of laboratory reporting limits that were achieved with the regulatory Numerical
Standards requested on the Chain of Custody.
HOLD POLICY
For samples submitted on hold, Alpha's policy is to hold samples free of charge for 30 days from the date the project is completed. After 30
days, we will dispose of all samples submitted including those put on hold unless you have contacted your Client Service Representative and
made arrangements for Alpha to continue to hold the samples.
Please contact Client Services at 800-624-9220 with any questions.
Serial_No:11051209:46
Page 4 of 279
Case Narrative (continued)
NEWTOWN CREEK RI
120782-01.01
Project Name:
Project Number:
Lab Number:
Report Date:L1218042
11/05/12
Volatile Organics
The WG566791-3/4 LCS/LCSD recoveries, associated with L1218042-01, -03, -05, -07, -09, -13, -15, -17,
-19, -21, -23, -25, -27 and -29, are above the individual acceptance criteria for Methylene Chloride (MSD @
153%), Vinyl chloride (MSD @ 134%) and Dichlorodifluoromethane (149%/161%), but within the overall method
allowances. Since all associated samples are non-detect for the affected compounds, no further action was
taken.
Alkylated PAHs
Concentrations for compounds flagged with "G" qualifiers may be biased high due to matrix interference
included in the quantitation.
L1218042-11 was re-analyzed due to quality control failures on the original analysis. The results of the re-
analysis have been reported.
The continuing calibration standard, WG568203-1, had %Ds above the acceptance criteria for Retene at
(29%D) and Benzo(b)fluorene at (29%D); however, they are within the method allowances, therefore no further
action was required.
Saturated Hydrocarbons
The results for n-Octadecane (C18) and n-Nonacosane (C29) are "C" qualified on all detectable results in all
samples, as well as the WG566066-1 Method Blank, due to the positive bias determined to be present in the
samples caused by the co-elution with laboratory standards (i.e. PAH surrogates and/or internal standards).
Concentrations for compounds flagged with "G" qualifiers may be biased high due to matrix interference
included in the quantitation.
Serial_No:11051209:46
Page 5 of 279
Case Narrative (continued)
NEWTOWN CREEK RI
120782-01.01
Project Name:
Project Number:
Lab Number:
Report Date:L1218042
11/05/12
Total Metals
All sediment samples have elevated detection limits for all analytes due to the additional dilutions (10x/50x)
required by the elevated concentrations of target analytes in the samples.
All sediment samples were re-analyzed for Total Tin. In addition, L1218042-11 was re-analyzed for Total
Cobalt.
The WG568940-1 Method Blank, associated with all sediment samples, has a concentration above the
reporting limit for Total Vanadium. Since the associated sample concentrations are greater than 5x the blank
concentration for this analyte, no qualification of the results was performed.
The WG568938-4 MS recovery, performed on L1218042-01, is below the acceptance criteria for Total
Antimony (25%); however, the associated LCS/LCSD recoveries were within criteria.
The WG568940-4 MS recoveries, performed on L1218042-01, are above the acceptance criteria for Total
Aluminum (179%), Calcium (752%) and Iron (384%); however, the spikes do not apply because the sample
concentrations are greater than four times the spike amounts added.
The WG568940-3 Laboratory Duplicate RPDs, performed on L1218042-01, are outside the acceptance
criteria for Total Barium (112%), Cadmium (97%), Calcium (66%), Lead (93%), Selenium (129%) and Thallium
(138%). The elevated RPDs have been attributed to the non-homogeneous nature of the sample utilized for
the laboratory duplicate. In addition, the RPDs are above the acceptance criteria for Total Beryllium (54%) and
Zinc (26%); however, the sample and duplicate results are less than five times the reporting limit. Therefore,
the RPDs are valid.
Total Organic Carbon
All sediment samples were analyzed beyond the QAPP-defined holding time due to a lab oversight; however,
the analysis was performed within the internal laboratory 28-day holding time. In addition, all samples were in
Serial_No:11051209:46
Page 6 of 279
Case Narrative (continued)
NEWTOWN CREEK RI
120782-01.01
Project Name:
Project Number:
Lab Number:
Report Date:L1218042
11/05/12
frozen storage until analysis. The data is released without further action.
The WG566725-3 Laboratory Duplicate RPD, performed on L1218042-01, is outside the acceptance criteria
for Total Organic Carbon-Rep 2 (26%). The elevated RPD has been attributed to the non-homogeneous
nature of the sample utilized for the laboratory duplicate.
Nitrate/Nitrite Nitrogen
The WG567243-3 Laboratory Duplicate RPD, performed on L1218042-01, is outside the acceptance criteria
for Nitrate/Nitrite Nitrogen (30%); however, the sample and duplicate results are less than five times the
reporting limit. Therefore, the RPD is valid.
Total Phosphorus
All samples have elevated detection limits due to the dilutions required to quantitate the results within the
calibration range.
The WG567984-3 MS recovery, performed on L1218042-29, is below the acceptance criteria for Total
Phosphorus (14%); however, the associated LCS is within criteria. The low recovery has been attributed to
sample matrix interference.
Sulfide
All samples have elevated detection limits due to the dilutions required to quantitate the results within the
calibration range.
The WG566113-4 MS recovery, performed on L1218042-07, is above the acceptance criteria for Sulfide
(390%); however, the spike does not apply because the sample concentration is greater than four times the
spike amount added.
Serial_No:11051209:46
Page 7 of 279
Case Narrative (continued)
NEWTOWN CREEK RI
120782-01.01
Project Name:
Project Number:
Lab Number:
Report Date:L1218042
11/05/12
The WG566113-3 Laboratory Duplicate RPD, performed on L1218042-05, is outside the acceptance criteria
for Sulfide (33%). The elevated RPD has been attributed to the non-homogeneous nature of the sample
utilized for the laboratory duplicate.
Percent Soot
All sediment samples were analyzed beyond the QAPP-defined holding time due to a lab oversight; however,
the analysis was performed within the internal laboratory 28-day holding time. In addition, all samples were in
frozen storage until analysis. The data is released without further action.
The WG566732-3 Laboratory Duplicate RPD, performed on L1218042-01, is outside the acceptance criteria
for Percent Soot-Rep 1 (79%). The elevated RPD has been attributed to the non-homogeneous nature of the
sample utilized for the laboratory duplicate.
I, the undersigned, attest under the pains and penalties of perjury that, to the best of my knowledge and belief and based upon my personal inquiry of those responsible for providing the information contained in this analytical report, such information is accurate and complete. This certificate of analysis is not complete unless this page accompanies any and all pages of this report.
Authorized Signature:
Title: Technical Director/Representative Date: 11/05/12
Serial_No:11051209:46
Page 8 of 279
ORGANICS
Serial_No:11051209:46
Page 9 of 279
VOLATILES
Serial_No:11051209:46
Page 10 of 279
FF
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Methyl tert butyl ether
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS-5035 - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
14
2.1
2.1
1.4
4.9
1.4
2.1
1.4
1.4
7.0
1.4
1.4
1.4
1.4
1.4
5.6
1.4
1.4
2.1
1.4
7.0
2.8
2.8
2.8
1.4
2.1
1.4
7.0
7.0
7.0
2.8
11/05/12
TN005SG-000014-20121005Client ID:10/05/12 09:32Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-01Lab ID:
Field Prep: Not SpecifiedMatrix: SedimentAnalytical Method:Analytical Date:Analyst:
1,8260C10/11/12 20:22BN 72%Percent Solids:
MDL
2.8
0.33
0.45
0.39
0.35
0.44
0.57
0.40
0.34
0.60
0.41
0.28
0.54
0.47
0.37
1.6
0.40
0.27
0.26
0.53
1.1
0.81
0.77
0.61
0.46
0.42
0.39
0.51
0.52
0.42
0.92
Serial_No:11051209:46
Page 11 of 279
p/m-Xylene
o-Xylene
cis-1,2-Dichloroethene
Styrene
Dichlorodifluoromethane
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
4-Methyl-2-pentanone
2-Hexanone
Bromochloromethane
1,2-Dibromoethane
1,2-Dibromo-3-chloropropane
Isopropylbenzene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
Methyl Acetate
Cyclohexane
Methyl cyclohexane
Freon-113
Parameter Result
J
J
Dilution Factor
ND
ND
ND
ND
ND
7.9
3.6
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS-5035 - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
2.8
2.8
1.4
2.8
14
50
14
14
14
14
14
7.0
5.6
7.0
1.4
7.0
7.0
28
28
5.6
28
1,2-Dichloroethane-d4
Toluene-d8
4-Bromofluorobenzene
Dibromofluoromethane
105
97
99
103
70-130
70-130
70-130
70-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
TN005SG-000014-20121005Client ID:10/05/12 09:32Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-01Lab ID:
Field Prep: Not Specified
No Tentatively Identified Compounds ND ug/kg 1
Tentatively Identified Compounds
MDL
0.64
0.79
0.36
0.85
2.4
4.5
0.36
5.4
1.9
2.4
1.8
0.50
0.30
2.1
0.27
1.3
1.2
28.
28.
5.6
1.3
Serial_No:11051209:46
Page 12 of 279
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Methyl tert butyl ether
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS-5035 - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
16
2.4
2.4
1.6
5.6
1.6
2.4
1.6
1.6
8.0
1.6
1.6
1.6
1.6
1.6
6.4
1.6
1.6
2.4
1.6
8.0
3.2
3.2
3.2
1.6
2.4
1.6
8.0
8.0
8.0
3.2
11/05/12
TN002SG-000011-20121005Client ID:10/05/12 10:41Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-03Lab ID:
Field Prep: Not SpecifiedMatrix: SedimentAnalytical Method:Analytical Date:Analyst:
1,8260C10/11/12 20:50BN 55%Percent Solids:
MDL
3.2
0.38
0.52
0.45
0.40
0.52
0.66
0.47
0.40
0.70
0.47
0.33
0.62
0.54
0.43
1.8
0.47
0.31
0.30
0.61
1.3
0.94
0.89
0.71
0.53
0.48
0.45
0.59
0.61
0.49
1.1
Serial_No:11051209:46
Page 13 of 279
p/m-Xylene
o-Xylene
cis-1,2-Dichloroethene
Styrene
Dichlorodifluoromethane
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
4-Methyl-2-pentanone
2-Hexanone
Bromochloromethane
1,2-Dibromoethane
1,2-Dibromo-3-chloropropane
Isopropylbenzene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
Methyl Acetate
Cyclohexane
Methyl cyclohexane
Freon-113
Parameter Result
J
J
J
Dilution Factor
ND
ND
ND
ND
ND
33
9.5
6.6
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS-5035 - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
3.2
3.2
1.6
3.2
16
58
16
16
16
16
16
8.0
6.4
8.0
1.6
8.0
8.0
32
32
6.4
32
1,2-Dichloroethane-d4
Toluene-d8
4-Bromofluorobenzene
Dibromofluoromethane
105
96
101
103
70-130
70-130
70-130
70-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
TN002SG-000011-20121005Client ID:10/05/12 10:41Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-03Lab ID:
Field Prep: Not Specified
Dimethyl sulfide NJ9.1 ug/kg 1
Tentatively Identified Compounds
MDL
0.74
0.92
0.41
0.99
2.8
5.2
0.41
6.2
2.2
2.8
2.0
0.58
0.34
2.4
0.31
1.5
1.4
32.
32.
6.4
1.5
Serial_No:11051209:46
Page 14 of 279
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Methyl tert butyl ether
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS-5035 - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
22
3.3
3.3
2.2
7.7
2.2
3.3
2.2
2.2
11
2.2
2.2
2.2
2.2
2.2
8.8
2.2
2.2
3.3
2.2
11
4.4
4.4
4.4
2.2
3.3
2.2
11
11
11
4.4
11/05/12
TN003SG-000015-20121005Client ID:10/05/12 11:24Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-05Lab ID:
Field Prep: Not SpecifiedMatrix: SedimentAnalytical Method:Analytical Date:Analyst:
1,8260C10/11/12 21:17BN 41%Percent Solids:
MDL
4.4
0.52
0.71
0.61
0.55
0.70
0.90
0.64
0.54
0.96
0.64
0.44
0.84
0.74
0.59
2.4
0.63
0.42
0.42
0.83
1.7
1.3
1.2
0.96
0.73
0.66
0.62
0.80
0.83
0.67
1.4
Serial_No:11051209:46
Page 15 of 279
p/m-Xylene
o-Xylene
cis-1,2-Dichloroethene
Styrene
Dichlorodifluoromethane
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
4-Methyl-2-pentanone
2-Hexanone
Bromochloromethane
1,2-Dibromoethane
1,2-Dibromo-3-chloropropane
Isopropylbenzene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
Methyl Acetate
Cyclohexane
Methyl cyclohexane
Freon-113
Parameter Result
J
J
J
Dilution Factor
ND
ND
ND
ND
ND
70
11
14
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS-5035 - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
4.4
4.4
2.2
4.4
22
79
22
22
22
22
22
11
8.8
11
2.2
11
11
44
44
8.8
44
1,2-Dichloroethane-d4
Toluene-d8
4-Bromofluorobenzene
Dibromofluoromethane
104
96
103
104
70-130
70-130
70-130
70-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
TN003SG-000015-20121005Client ID:10/05/12 11:24Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-05Lab ID:
Field Prep: Not Specified
Dimethyl sulfide NJ12 ug/kg 1
Tentatively Identified Compounds
MDL
1.0
1.2
0.56
1.3
3.8
7.1
0.56
8.5
3.0
3.9
2.8
0.78
0.47
3.2
0.42
2.0
1.9
44.
44.
8.8
2.0
Serial_No:11051209:46
Page 16 of 279
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Methyl tert butyl ether
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS-5035 - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
19
2.8
2.8
1.9
6.7
1.9
2.8
1.9
1.9
9.5
1.9
1.9
1.9
1.9
1.9
7.6
1.9
1.9
2.8
1.9
9.5
3.8
3.8
3.8
1.9
2.8
1.9
9.5
9.5
9.5
3.8
11/05/12
TN004SG-000015-20121005Client ID:10/05/12 11:46Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-07Lab ID:
Field Prep: Not SpecifiedMatrix: SedimentAnalytical Method:Analytical Date:Analyst:
1,8260C10/11/12 21:44BN 51%Percent Solids:
MDL
3.8
0.45
0.62
0.53
0.48
0.61
0.78
0.55
0.47
0.83
0.56
0.39
0.73
0.64
0.51
2.1
0.55
0.37
0.36
0.72
1.5
1.1
1.0
0.84
0.63
0.57
0.54
0.69
0.72
0.58
1.2
Serial_No:11051209:46
Page 17 of 279
p/m-Xylene
o-Xylene
cis-1,2-Dichloroethene
Styrene
Dichlorodifluoromethane
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
4-Methyl-2-pentanone
2-Hexanone
Bromochloromethane
1,2-Dibromoethane
1,2-Dibromo-3-chloropropane
Isopropylbenzene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
Methyl Acetate
Cyclohexane
Methyl cyclohexane
Freon-113
Parameter Result
J
J
J
Dilution Factor
ND
ND
ND
ND
ND
57
14
11
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS-5035 - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
3.8
3.8
1.9
3.8
19
68
19
19
19
19
19
9.5
7.6
9.5
1.9
9.5
9.5
38
38
7.6
38
1,2-Dichloroethane-d4
Toluene-d8
4-Bromofluorobenzene
Dibromofluoromethane
105
96
102
104
70-130
70-130
70-130
70-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
TN004SG-000015-20121005Client ID:10/05/12 11:46Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-07Lab ID:
Field Prep: Not Specified
Dimethyl sulfide NJ17 ug/kg 1
Tentatively Identified Compounds
MDL
0.87
1.1
0.49
1.2
3.3
6.2
0.49
7.4
2.6
3.4
2.4
0.68
0.41
2.8
0.37
1.8
1.6
38.
38.
7.6
1.8
Serial_No:11051209:46
Page 18 of 279
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Methyl tert butyl ether
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS-5035 - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
12
1.8
1.8
1.2
4.1
1.2
1.8
1.2
1.2
5.8
1.2
1.2
1.2
1.2
1.2
4.7
1.2
1.2
1.8
1.2
5.8
2.3
2.3
2.3
1.2
1.8
1.2
5.8
5.8
5.8
2.3
11/05/12
TN006SG-000015-20121005Client ID:10/05/12 13:16Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-09Lab ID:
Field Prep: Not SpecifiedMatrix: SedimentAnalytical Method:Analytical Date:Analyst:
1,8260C10/11/12 22:11BN 78%Percent Solids:
MDL
2.3
0.28
0.38
0.32
0.29
0.37
0.48
0.34
0.29
0.51
0.34
0.24
0.45
0.39
0.31
1.3
0.34
0.22
0.22
0.44
0.92
0.68
0.65
0.51
0.39
0.35
0.33
0.42
0.44
0.36
0.77
Serial_No:11051209:46
Page 19 of 279
p/m-Xylene
o-Xylene
cis-1,2-Dichloroethene
Styrene
Dichlorodifluoromethane
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
4-Methyl-2-pentanone
2-Hexanone
Bromochloromethane
1,2-Dibromoethane
1,2-Dibromo-3-chloropropane
Isopropylbenzene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
Methyl Acetate
Cyclohexane
Methyl cyclohexane
Freon-113
Parameter Result
J
Dilution Factor
ND
ND
ND
ND
ND
ND
0.88
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS-5035 - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
2.3
2.3
1.2
2.3
12
42
12
12
12
12
12
5.8
4.7
5.8
1.2
5.8
5.8
23
23
4.7
23
1,2-Dichloroethane-d4
Toluene-d8
4-Bromofluorobenzene
Dibromofluoromethane
104
96
99
104
70-130
70-130
70-130
70-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
TN006SG-000015-20121005Client ID:10/05/12 13:16Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-09Lab ID:
Field Prep: Not Specified
No Tentatively Identified Compounds ND ug/kg 1
Tentatively Identified Compounds
MDL
0.53
0.66
0.30
0.72
2.0
3.8
0.30
4.5
1.6
2.1
1.5
0.42
0.25
1.7
0.22
1.1
1.0
23.
23.
4.7
1.1
Serial_No:11051209:46
Page 20 of 279
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Methyl tert butyl ether
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
3.0
0.75
0.75
0.50
1.8
0.50
0.75
0.50
0.50
2.5
0.50
0.50
0.50
0.50
0.50
2.0
0.50
0.50
0.75
0.50
2.5
1.0
1.0
1.0
0.50
0.75
0.50
2.5
2.5
2.5
1.0
11/05/12
SG-RB-20121006Client ID:10/06/12 09:05Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-11Lab ID:
Field Prep: Not SpecifiedMatrix: WaterAnalytical Method:Analytical Date:Analyst:
1,8260C10/17/12 10:01PD
MDL
0.54
0.22
0.20
0.16
0.30
0.19
0.26
0.18
0.19
0.27
0.16
0.16
0.19
0.16
0.14
0.25
0.19
0.19
0.23
0.26
0.28
0.26
0.22
0.23
0.18
0.21
0.17
0.18
0.19
0.22
0.16
Serial_No:11051209:46
Page 21 of 279
p/m-Xylene
o-Xylene
cis-1,2-Dichloroethene
Styrene
Dichlorodifluoromethane
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
4-Methyl-2-pentanone
2-Hexanone
Bromochloromethane
1,2-Dibromoethane
1,2-Dibromo-3-chloropropane
Isopropylbenzene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
Methyl Acetate
Cyclohexane
Freon-113
Methyl cyclohexane
Parameter Result
J
Dilution Factor
ND
ND
ND
ND
ND
2.2
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
1.0
1.0
0.50
1.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
2.5
2.0
2.5
0.50
2.5
2.5
10
10
10
10
1,2-Dichloroethane-d4
Toluene-d8
4-Bromofluorobenzene
Dibromofluoromethane
106
100
123
98
70-130
70-130
70-130
70-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
SG-RB-20121006Client ID:10/06/12 09:05Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-11Lab ID:
Field Prep: Not Specified
Unknown1 J1.1 ug/l 1
Tentatively Identified Compounds
MDL
0.35
0.33
0.19
0.36
0.30
1.6
0.30
1.9
0.31
0.42
0.58
0.33
0.32
0.33
0.19
0.23
0.22
10.
0.24
0.23
0.29
Serial_No:11051209:46
Page 22 of 279
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Methyl tert butyl ether
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS-5035 - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
35
5.3
5.3
3.5
12
3.5
5.3
3.5
3.5
18
3.5
3.5
3.5
3.5
3.5
14
3.5
3.5
5.3
3.5
18
7.1
7.1
7.1
3.5
5.3
3.5
18
18
18
7.1
11/05/12
HB008SG-000015-20121006Client ID:10/06/12 09:55Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-13Lab ID:
Field Prep: Not SpecifiedMatrix: SedimentAnalytical Method:Analytical Date:Analyst:
1,8260C10/11/12 22:38BN 27%Percent Solids:
MDL
7.1
0.83
1.1
0.98
0.89
1.1
1.4
1.0
0.87
1.5
1.0
0.72
1.4
1.2
0.94
3.9
1.0
0.68
0.67
1.3
2.8
2.0
2.0
1.6
1.2
1.1
0.99
1.3
1.3
1.1
2.3
Serial_No:11051209:46
Page 23 of 279
p/m-Xylene
o-Xylene
cis-1,2-Dichloroethene
Styrene
Dichlorodifluoromethane
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
4-Methyl-2-pentanone
2-Hexanone
Bromochloromethane
1,2-Dibromoethane
1,2-Dibromo-3-chloropropane
Isopropylbenzene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
Methyl Acetate
Cyclohexane
Methyl cyclohexane
Freon-113
Parameter Result
J
J
Dilution Factor
ND
ND
ND
ND
ND
130
22
32
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS-5035 - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
7.1
7.1
3.5
7.1
35
130
35
35
35
35
35
18
14
18
3.5
18
18
71
71
14
71
1,2-Dichloroethane-d4
Toluene-d8
4-Bromofluorobenzene
Dibromofluoromethane
108
99
107
106
70-130
70-130
70-130
70-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
HB008SG-000015-20121006Client ID:10/06/12 09:55Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-13Lab ID:
Field Prep: Not Specified
Dimethyl sulfide NJ36 ug/kg 1
Tentatively Identified Compounds
MDL
1.6
2.0
0.90
2.2
6.1
11.
0.91
14.
4.8
6.2
4.4
1.3
0.76
5.2
0.68
3.3
3.1
71.
71.
14.
3.3
Serial_No:11051209:46
Page 24 of 279
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Methyl tert butyl ether
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS-5035 - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
37
5.6
5.6
3.7
13
3.7
5.6
3.7
3.7
18
3.7
3.7
3.7
3.7
3.7
15
3.7
3.7
5.6
3.7
18
7.4
7.4
7.4
3.7
5.6
3.7
18
18
18
7.4
11/05/12
HB007SG-000015-20121006Client ID:10/06/12 10:45Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-15Lab ID:
Field Prep: Not SpecifiedMatrix: SedimentAnalytical Method:Analytical Date:Analyst:
1,8260C10/11/12 23:05BN 25%Percent Solids:
MDL
7.4
0.87
1.2
1.0
0.93
1.2
1.5
1.1
0.92
1.6
1.1
0.75
1.4
1.2
0.99
4.1
1.1
0.71
0.70
1.4
2.9
2.2
2.1
1.6
1.2
1.1
1.0
1.4
1.4
1.1
2.4
Serial_No:11051209:46
Page 25 of 279
p/m-Xylene
o-Xylene
cis-1,2-Dichloroethene
Styrene
Dichlorodifluoromethane
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
4-Methyl-2-pentanone
2-Hexanone
Bromochloromethane
1,2-Dibromoethane
1,2-Dibromo-3-chloropropane
Isopropylbenzene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
Methyl Acetate
Cyclohexane
Methyl cyclohexane
Freon-113
Parameter Result
J
Dilution Factor
ND
ND
ND
ND
ND
240
20
54
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS-5035 - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
7.4
7.4
3.7
7.4
37
130
37
37
37
37
37
18
15
18
3.7
18
18
74
74
15
74
1,2-Dichloroethane-d4
Toluene-d8
4-Bromofluorobenzene
Dibromofluoromethane
107
100
111
104
70-130
70-130
70-130
70-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
HB007SG-000015-20121006Client ID:10/06/12 10:45Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-15Lab ID:
Field Prep: Not Specified
Dimethyl sulfide NJ28 ug/kg 1
Tentatively Identified Compounds
MDL
1.7
2.1
0.95
2.3
6.4
12.
0.95
14.
5.1
6.6
4.7
1.3
0.80
5.5
0.72
3.4
3.2
74.
74.
15.
3.5
Serial_No:11051209:46
Page 26 of 279
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Methyl tert butyl ether
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS-5035 - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
28
4.2
4.2
2.8
9.8
2.8
4.2
2.8
2.8
14
2.8
2.8
2.8
2.8
2.8
11
2.8
2.8
4.2
2.8
14
5.6
5.6
5.6
2.8
4.2
2.8
14
14
14
5.6
11/05/12
HB006SG-000015-20121006Client ID:10/06/12 11:30Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-17Lab ID:
Field Prep: Not SpecifiedMatrix: SedimentAnalytical Method:Analytical Date:Analyst:
1,8260C10/11/12 23:31BN 34%Percent Solids:
MDL
5.6
0.66
0.91
0.78
0.70
0.90
1.2
0.81
0.69
1.2
0.82
0.57
1.1
0.94
0.75
3.1
0.81
0.54
0.53
1.1
2.2
1.6
1.6
1.2
0.93
0.84
0.79
1.0
1.0
0.86
1.8
Serial_No:11051209:46
Page 27 of 279
p/m-Xylene
o-Xylene
cis-1,2-Dichloroethene
Styrene
Dichlorodifluoromethane
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
4-Methyl-2-pentanone
2-Hexanone
Bromochloromethane
1,2-Dibromoethane
1,2-Dibromo-3-chloropropane
Isopropylbenzene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
Methyl Acetate
Cyclohexane
Methyl cyclohexane
Freon-113
Parameter Result
J
Dilution Factor
ND
ND
ND
ND
ND
270
6.8
60
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS-5035 - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
5.6
5.6
2.8
5.6
28
100
28
28
28
28
28
14
11
14
2.8
14
14
56
56
11
56
1,2-Dichloroethane-d4
Toluene-d8
4-Bromofluorobenzene
Dibromofluoromethane
103
99
106
104
70-130
70-130
70-130
70-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
HB006SG-000015-20121006Client ID:10/06/12 11:30Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-17Lab ID:
Field Prep: Not Specified
Dimethyl sulfide NJ74 ug/kg 1
Tentatively Identified Compounds
MDL
1.3
1.6
0.72
1.7
4.8
9.1
0.72
11.
3.8
5.0
3.5
1.0
0.60
4.2
0.54
2.6
2.4
56.
56.
11.
2.6
Serial_No:11051209:46
Page 28 of 279
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Methyl tert butyl ether
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS-5035 - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
38
5.6
5.6
3.8
13
3.8
5.6
3.8
3.8
19
3.8
3.8
3.8
3.8
3.8
15
3.8
3.8
5.6
3.8
19
7.5
7.5
7.5
3.8
5.6
3.8
19
19
19
7.5
11/05/12
HB005SG-000015-20121006Client ID:10/06/12 12:19Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-19Lab ID:
Field Prep: Not SpecifiedMatrix: SedimentAnalytical Method:Analytical Date:Analyst:
1,8260C10/11/12 23:58BN 26%Percent Solids:
MDL
7.5
0.89
1.2
1.0
0.95
1.2
1.5
1.1
0.93
1.6
1.1
0.76
1.4
1.3
1.0
4.2
1.1
0.72
0.72
1.4
3.0
2.2
2.1
1.6
1.2
1.1
1.1
1.4
1.4
1.2
2.5
Serial_No:11051209:46
Page 29 of 279
p/m-Xylene
o-Xylene
cis-1,2-Dichloroethene
Styrene
Dichlorodifluoromethane
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
4-Methyl-2-pentanone
2-Hexanone
Bromochloromethane
1,2-Dibromoethane
1,2-Dibromo-3-chloropropane
Isopropylbenzene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
Methyl Acetate
Cyclohexane
Methyl cyclohexane
Freon-113
Parameter Result
J
Dilution Factor
ND
ND
ND
ND
ND
580
16
120
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS-5035 - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
7.5
7.5
3.8
7.5
38
140
38
38
38
38
38
19
15
19
3.8
19
19
75
75
15
75
1,2-Dichloroethane-d4
Toluene-d8
4-Bromofluorobenzene
Dibromofluoromethane
104
98
106
105
70-130
70-130
70-130
70-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
HB005SG-000015-20121006Client ID:10/06/12 12:19Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-19Lab ID:
Field Prep: Not Specified
Dimethyl sulfide NJ40 ug/kg 1
Tentatively Identified Compounds
MDL
1.7
2.1
0.96
2.3
6.5
12.
0.97
15.
5.1
6.7
4.7
1.3
0.81
5.6
0.73
3.5
3.3
75.
75.
15.
3.5
Serial_No:11051209:46
Page 30 of 279
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Methyl tert butyl ether
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS-5035 - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
36
5.4
5.4
3.6
13
3.6
5.4
3.6
3.6
18
3.6
3.6
3.6
3.6
3.6
14
3.6
3.6
5.4
3.6
18
7.2
7.2
7.2
3.6
5.4
3.6
18
18
18
7.2
11/05/12
HB1005SG-000015-20121006Client ID:10/06/12 12:19Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-21Lab ID:
Field Prep: Not SpecifiedMatrix: SedimentAnalytical Method:Analytical Date:Analyst:
1,8260C10/12/12 00:25BN 25%Percent Solids:
MDL
7.2
0.85
1.2
1.0
0.91
1.2
1.5
1.0
0.89
1.6
1.0
0.73
1.4
1.2
0.96
4.0
1.0
0.69
0.68
1.4
2.8
2.1
2.0
1.6
1.2
1.1
1.0
1.3
1.4
1.1
2.4
Serial_No:11051209:46
Page 31 of 279
p/m-Xylene
o-Xylene
cis-1,2-Dichloroethene
Styrene
Dichlorodifluoromethane
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
4-Methyl-2-pentanone
2-Hexanone
Bromochloromethane
1,2-Dibromoethane
1,2-Dibromo-3-chloropropane
Isopropylbenzene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
Methyl Acetate
Cyclohexane
Methyl cyclohexane
Freon-113
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
370
38
81
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS-5035 - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
7.2
7.2
3.6
7.2
36
130
36
36
36
36
36
18
14
18
3.6
18
18
72
72
14
72
1,2-Dichloroethane-d4
Toluene-d8
4-Bromofluorobenzene
Dibromofluoromethane
104
99
106
105
70-130
70-130
70-130
70-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
HB1005SG-000015-20121006Client ID:10/06/12 12:19Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-21Lab ID:
Field Prep: Not Specified
Dimethyl sulfide NJ20 ug/kg 1
Tentatively Identified Compounds
MDL
1.6
2.0
0.92
2.2
6.2
12.
0.93
14.
4.9
6.4
4.5
1.3
0.77
5.3
0.70
3.3
3.1
72.
72.
14.
3.4
Serial_No:11051209:46
Page 32 of 279
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Methyl tert butyl ether
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS-5035 - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
26
3.9
3.9
2.6
9.0
2.6
3.9
2.6
2.6
13
2.6
2.6
2.6
2.6
2.6
10
2.6
2.6
3.9
2.6
13
5.2
5.2
5.2
2.6
3.9
2.6
13
13
13
5.2
11/05/12
HB004SG-000015-20121006Client ID:10/06/12 13:27Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-23Lab ID:
Field Prep: Not SpecifiedMatrix: SedimentAnalytical Method:Analytical Date:Analyst:
1,8260C10/12/12 00:52BN 35%Percent Solids:
MDL
5.2
0.61
0.84
0.72
0.65
0.82
1.0
0.75
0.63
1.1
0.76
0.52
0.99
0.87
0.69
2.9
0.74
0.50
0.49
0.98
2.0
1.5
1.4
1.1
0.85
0.77
0.72
0.94
0.97
0.79
1.7
Serial_No:11051209:46
Page 33 of 279
p/m-Xylene
o-Xylene
cis-1,2-Dichloroethene
Styrene
Dichlorodifluoromethane
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
4-Methyl-2-pentanone
2-Hexanone
Bromochloromethane
1,2-Dibromoethane
1,2-Dibromo-3-chloropropane
Isopropylbenzene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
Methyl Acetate
Cyclohexane
Methyl cyclohexane
Freon-113
Parameter Result
J
Dilution Factor
ND
ND
ND
ND
ND
160
16
36
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS-5035 - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
5.2
5.2
2.6
5.2
26
93
26
26
26
26
26
13
10
13
2.6
13
13
52
52
10
52
1,2-Dichloroethane-d4
Toluene-d8
4-Bromofluorobenzene
Dibromofluoromethane
106
98
106
103
70-130
70-130
70-130
70-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
HB004SG-000015-20121006Client ID:10/06/12 13:27Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-23Lab ID:
Field Prep: Not Specified
No Tentatively Identified Compounds ND ug/kg 1
Tentatively Identified Compounds
MDL
1.2
1.5
0.66
1.6
4.5
8.3
0.66
10.
3.5
4.6
3.2
0.92
0.55
3.8
0.50
2.4
2.2
52.
52.
10.
2.4
Serial_No:11051209:46
Page 34 of 279
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Methyl tert butyl ether
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS-5035 - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
33
5.0
5.0
3.3
12
3.3
5.0
3.3
3.3
17
3.3
3.3
3.3
3.3
3.3
13
3.3
3.3
5.0
3.3
17
6.7
6.7
6.7
3.3
5.0
3.3
17
17
17
6.7
11/05/12
HB003SG-000015-20121006Client ID:10/06/12 14:21Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-25Lab ID:
Field Prep: Not SpecifiedMatrix: SedimentAnalytical Method:Analytical Date:Analyst:
1,8260C10/12/12 01:19BN 28%Percent Solids:
MDL
6.7
0.78
1.1
0.93
0.84
1.1
1.4
0.97
0.82
1.4
0.98
0.68
1.3
1.1
0.89
3.7
0.96
0.64
0.63
1.3
2.6
1.9
1.8
1.5
1.1
1.0
0.94
1.2
1.2
1.0
2.2
Serial_No:11051209:46
Page 35 of 279
p/m-Xylene
o-Xylene
cis-1,2-Dichloroethene
Styrene
Dichlorodifluoromethane
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
4-Methyl-2-pentanone
2-Hexanone
Bromochloromethane
1,2-Dibromoethane
1,2-Dibromo-3-chloropropane
Isopropylbenzene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
Methyl Acetate
Cyclohexane
Methyl cyclohexane
Freon-113
Parameter Result
J
Dilution Factor
ND
ND
ND
ND
ND
420
14
91
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS-5035 - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
6.7
6.7
3.3
6.7
33
120
33
33
33
33
33
17
13
17
3.3
17
17
67
67
13
67
1,2-Dichloroethane-d4
Toluene-d8
4-Bromofluorobenzene
Dibromofluoromethane
106
99
109
105
70-130
70-130
70-130
70-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
HB003SG-000015-20121006Client ID:10/06/12 14:21Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-25Lab ID:
Field Prep: Not Specified
Dimethyl sulfide NJ35 ug/kg 1
Tentatively Identified Compounds
MDL
1.5
1.9
0.85
2.0
5.8
11.
0.86
13.
4.5
5.9
4.2
1.2
0.71
4.9
0.64
3.1
2.9
67.
67.
13.
3.1
Serial_No:11051209:46
Page 36 of 279
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Methyl tert butyl ether
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS-5035 - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
28
4.2
4.2
2.8
9.8
2.8
4.2
2.8
2.8
14
2.8
2.8
2.8
2.8
2.8
11
2.8
2.8
4.2
2.8
14
5.6
5.6
5.6
2.8
4.2
2.8
14
14
14
5.6
11/05/12
HB002SG-000015-20121006Client ID:10/06/12 15:05Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-27Lab ID:
Field Prep: Not SpecifiedMatrix: SedimentAnalytical Method:Analytical Date:Analyst:
1,8260C10/12/12 01:46BN 34%Percent Solids:
MDL
5.6
0.66
0.91
0.78
0.71
0.90
1.2
0.82
0.69
1.2
0.83
0.57
1.1
0.95
0.75
3.1
0.81
0.54
0.53
1.1
2.2
1.6
1.6
1.2
0.93
0.84
0.79
1.0
1.0
0.86
1.9
Serial_No:11051209:46
Page 37 of 279
p/m-Xylene
o-Xylene
cis-1,2-Dichloroethene
Styrene
Dichlorodifluoromethane
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
4-Methyl-2-pentanone
2-Hexanone
Bromochloromethane
1,2-Dibromoethane
1,2-Dibromo-3-chloropropane
Isopropylbenzene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
Methyl Acetate
Cyclohexane
Methyl cyclohexane
Freon-113
Parameter Result
J
Dilution Factor
ND
ND
ND
ND
ND
320
9.5
72
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS-5035 - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
5.6
5.6
2.8
5.6
28
100
28
28
28
28
28
14
11
14
2.8
14
14
56
56
11
56
1,2-Dichloroethane-d4
Toluene-d8
4-Bromofluorobenzene
Dibromofluoromethane
104
97
105
103
70-130
70-130
70-130
70-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
HB002SG-000015-20121006Client ID:10/06/12 15:05Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-27Lab ID:
Field Prep: Not Specified
Dimethyl sulfide NJ29 ug/kg 1
Tentatively Identified Compounds
MDL
1.3
1.6
0.72
1.7
4.9
9.1
0.72
11.
3.8
5.0
3.5
1.0
0.60
4.2
0.54
2.6
2.4
56.
56.
11.
2.6
Serial_No:11051209:46
Page 38 of 279
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Methyl tert butyl ether
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS-5035 - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
33
4.9
4.9
3.3
12
3.3
4.9
3.3
3.3
16
3.3
3.3
3.3
3.3
3.3
13
3.3
3.3
4.9
3.3
16
6.6
6.6
6.6
3.3
4.9
3.3
16
16
16
6.6
11/05/12
HB001SG-000015-20121006Client ID:10/06/12 15:54Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-29Lab ID:
Field Prep: Not SpecifiedMatrix: SedimentAnalytical Method:Analytical Date:Analyst:
1,8260C10/12/12 02:13BN 30%Percent Solids:
MDL
6.6
0.77
1.1
0.92
0.83
1.0
1.4
0.95
0.81
1.4
0.96
0.67
1.3
1.1
0.88
3.7
0.95
0.63
0.62
1.2
2.6
1.9
1.8
1.4
1.1
0.99
0.92
1.2
1.2
1.0
2.2
Serial_No:11051209:46
Page 39 of 279
p/m-Xylene
o-Xylene
cis-1,2-Dichloroethene
Styrene
Dichlorodifluoromethane
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
4-Methyl-2-pentanone
2-Hexanone
Bromochloromethane
1,2-Dibromoethane
1,2-Dibromo-3-chloropropane
Isopropylbenzene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
Methyl Acetate
Cyclohexane
Methyl cyclohexane
Freon-113
Parameter Result
J
Dilution Factor
ND
ND
ND
ND
ND
410
7.8
97
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS-5035 - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
6.6
6.6
3.3
6.6
33
120
33
33
33
33
33
16
13
16
3.3
16
16
66
66
13
66
1,2-Dichloroethane-d4
Toluene-d8
4-Bromofluorobenzene
Dibromofluoromethane
103
97
105
104
70-130
70-130
70-130
70-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
HB001SG-000015-20121006Client ID:10/06/12 15:54Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-29Lab ID:
Field Prep: Not Specified
Dimethyl sulfide NJ46 ug/kg 1
Tentatively Identified Compounds
MDL
1.5
1.9
0.84
2.0
5.7
11.
0.84
13.
4.5
5.8
4.1
1.2
0.70
4.9
0.64
3.0
2.8
66.
66.
13.
3.1
Serial_No:11051209:46
Page 40 of 279
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Methyl tert butyl ether
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
3.0
0.75
0.75
0.50
1.8
0.50
0.75
0.50
0.50
2.5
0.50
0.50
0.50
0.50
0.50
2.0
0.50
0.50
0.75
0.50
2.5
1.0
1.0
1.0
0.50
0.75
0.50
2.5
2.5
2.5
1.0
11/05/12
SG-TB-20121006Client ID:10/06/12 16:23Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-31Lab ID:
Field Prep: Not SpecifiedMatrix: WaterAnalytical Method:Analytical Date:Analyst:
1,8260C10/17/12 10:36PD
MDL
0.54
0.22
0.20
0.16
0.30
0.19
0.26
0.18
0.19
0.27
0.16
0.16
0.19
0.16
0.14
0.25
0.19
0.19
0.23
0.26
0.28
0.26
0.22
0.23
0.18
0.21
0.17
0.18
0.19
0.22
0.16
Serial_No:11051209:46
Page 41 of 279
p/m-Xylene
o-Xylene
cis-1,2-Dichloroethene
Styrene
Dichlorodifluoromethane
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
4-Methyl-2-pentanone
2-Hexanone
Bromochloromethane
1,2-Dibromoethane
1,2-Dibromo-3-chloropropane
Isopropylbenzene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
Methyl Acetate
Cyclohexane
Freon-113
Methyl cyclohexane
Parameter Result
J
Dilution Factor
ND
ND
ND
ND
ND
2.4
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Volatile Organics by GC/MS - Westborough Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
1.0
1.0
0.50
1.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
2.5
2.0
2.5
0.50
2.5
2.5
10
10
10
10
1,2-Dichloroethane-d4
Toluene-d8
4-Bromofluorobenzene
Dibromofluoromethane
107
101
123
98
70-130
70-130
70-130
70-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
SG-TB-20121006Client ID:10/06/12 16:23Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-31Lab ID:
Field Prep: Not Specified
No Tentatively Identified Compounds ND ug/l 1
Tentatively Identified Compounds
MDL
0.35
0.33
0.19
0.36
0.30
1.6
0.30
1.9
0.31
0.42
0.58
0.33
0.32
0.33
0.19
0.23
0.22
10.
0.24
0.23
0.29
Serial_No:11051209:46
Page 42 of 279
Method Blank AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
10/11/12 18:171,8260CAnalytical Method:
Analytical Date:
11/05/12
Analyst: BN
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Parameter Result
4.2
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
RL
10
1.5
1.5
1.0
3.5
1.0
1.5
1.0
1.0
5.0
1.0
1.0
1.0
1.0
1.0
4.0
1.0
1.0
1.5
1.0
5.0
2.0
2.0
2.0
1.0
1.5
1.0
5.0
5.0
5.0
J ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
UnitsQualifier
Volatile Organics by GC/MS-5035 - Westborough Lab for sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG566791-5
MDL
2.0
0.24
0.32
0.28
0.25
0.32
0.41
0.29
0.25
0.44
0.29
0.20
0.38
0.34
0.27
1.1
0.29
0.19
0.19
0.38
0.78
0.58
0.55
0.44
0.33
0.30
0.28
0.36
0.38
0.30
Serial_No:11051209:46
Page 43 of 279
Method Blank AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
10/11/12 18:171,8260CAnalytical Method:
Analytical Date:
11/05/12
Analyst: BN
Methyl tert butyl ether
p/m-Xylene
o-Xylene
cis-1,2-Dichloroethene
Styrene
Dichlorodifluoromethane
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
4-Methyl-2-pentanone
2-Hexanone
Bromochloromethane
1,2-Dibromoethane
1,2-Dibromo-3-chloropropane
Isopropylbenzene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
Methyl Acetate
Cyclohexane
Methyl cyclohexane
Freon-113
Parameter Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
RL
2.0
2.0
2.0
1.0
2.0
10
36
10
10
10
10
10
5.0
4.0
5.0
1.0
5.0
5.0
20
20
4.0
20
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
UnitsQualifier
Volatile Organics by GC/MS-5035 - Westborough Lab for sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG566791-5
No Tentatively Identified Compounds ND ug/kg
Tentatively Identified Compounds
MDL
0.66
0.46
0.57
0.26
0.61
1.7
3.2
0.26
3.9
1.4
1.8
1.2
0.36
0.21
1.5
0.19
0.92
0.87
20.
20.
4.0
0.93
Serial_No:11051209:46
Page 44 of 279
Method Blank AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
10/11/12 18:171,8260CAnalytical Method:
Analytical Date:
11/05/12
Analyst: BN
Parameter Result RLUnitsQualifier
Volatile Organics by GC/MS-5035 - Westborough Lab for sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG566791-5
1,2-Dichloroethane-d4
Toluene-d8
4-Bromofluorobenzene
Dibromofluoromethane
104
96
100
103
70-130
70-130
70-130
70-130
Surrogate %Recovery QualifierAcceptance
Criteria
MDL
Serial_No:11051209:46
Page 45 of 279
Method Blank AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
10/17/12 07:401,8260CAnalytical Method:
Analytical Date:
11/05/12
Analyst: PD
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Methyl tert butyl ether
Parameter Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
RL
3.0
0.75
0.75
0.50
1.8
0.50
0.75
0.50
0.50
2.5
0.50
0.50
0.50
0.50
0.50
2.0
0.50
0.50
0.75
0.50
2.5
1.0
1.0
1.0
0.50
0.75
0.50
2.5
2.5
2.5
1.0
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
UnitsQualifier
Volatile Organics by GC/MS - Westborough Lab for sample(s): 11,31 Batch: WG567640-5
MDL
0.54
0.22
0.20
0.16
0.30
0.19
0.26
0.18
0.19
0.27
0.16
0.16
0.19
0.16
0.14
0.25
0.19
0.19
0.23
0.26
0.28
0.26
0.22
0.23
0.18
0.21
0.17
0.18
0.19
0.22
0.16
Serial_No:11051209:46
Page 46 of 279
Method Blank AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
10/17/12 07:401,8260CAnalytical Method:
Analytical Date:
11/05/12
Analyst: PD
p/m-Xylene
o-Xylene
cis-1,2-Dichloroethene
Styrene
Dichlorodifluoromethane
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
4-Methyl-2-pentanone
2-Hexanone
Bromochloromethane
1,2-Dibromoethane
1,2-Dibromo-3-chloropropane
Isopropylbenzene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
Methyl Acetate
Cyclohexane
Freon-113
Methyl cyclohexane
Parameter Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
RL
1.0
1.0
0.50
1.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
2.5
2.0
2.5
0.50
2.5
2.5
10
10
10
10
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
UnitsQualifier
Volatile Organics by GC/MS - Westborough Lab for sample(s): 11,31 Batch: WG567640-5
No Tentatively Identified Compounds ND ug/l
Tentatively Identified Compounds
MDL
0.35
0.33
0.19
0.36
0.30
1.6
0.30
1.9
0.31
0.42
0.58
0.33
0.32
0.33
0.19
0.23
0.22
10.
0.24
0.23
0.29
Serial_No:11051209:46
Page 47 of 279
Method Blank AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
10/17/12 07:401,8260CAnalytical Method:
Analytical Date:
11/05/12
Analyst: PD
Parameter Result RLUnitsQualifier
Volatile Organics by GC/MS - Westborough Lab for sample(s): 11,31 Batch: WG567640-5
1,2-Dichloroethane-d4
Toluene-d8
4-Bromofluorobenzene
Dibromofluoromethane
105
102
123
98
70-130
70-130
70-130
70-130
Surrogate %Recovery QualifierAcceptance
Criteria
MDL
Serial_No:11051209:46
Page 48 of 279
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
123
105
106
106
103
96
99
95
96
111
110
107
103
96
102
92
96
102
94
95
153
112
114
115
108
101
104
104
102
125
113
115
109
100
107
94
96
110
100
102
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-139
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
22
6
7
8
5
5
5
9
6
12
3
7
6
4
5
2
0
8
6
7
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
ParameterLCS
%RecoveryLCSD
%Recovery%Recovery
Limits RPD RPD Limits
Volatile Organics by GC/MS-5035 - Westborough Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG566791-3 WG566791-4
Lab Control Sample AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
Qual Qual
Q
Qual
Serial_No:11051209:46
Page 49 of 279
Chloromethane
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Methyl tert butyl ether
p/m-Xylene
o-Xylene
cis-1,2-Dichloroethene
Styrene
Dichlorodifluoromethane
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
118
97
124
128
109
105
105
94
92
94
107
94
96
105
95
149
126
105
110
104
127
102
134
138
119
115
113
96
97
97
110
101
101
111
100
161
126
115
111
106
52-130
57-147
67-130
50-151
65-135
70-130
70-130
70-130
70-130
70-130
66-130
70-130
70-130
70-130
70-130
30-146
54-140
59-130
70-130
70-130
7
5
8
8
9
9
7
2
5
3
3
7
5
6
5
8
0
9
1
2
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
ParameterLCS
%RecoveryLCSD
%Recovery%Recovery
Limits RPD RPD Limits
Volatile Organics by GC/MS-5035 - Westborough Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG566791-3 WG566791-4
Lab Control Sample AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
Qual Qual
Q
Q
Q
Qual
Serial_No:11051209:46
Page 50 of 279
4-Methyl-2-pentanone
2-Hexanone
Bromochloromethane
1,2-Dibromoethane
1,2-Dibromo-3-chloropropane
Isopropylbenzene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
Methyl Acetate
Cyclohexane
Methyl cyclohexane
1,1,2-Trichloro-1,2,2-Trifluoroethane
103
98
113
100
93
91
91
91
105
102
102
112
104
97
120
103
100
98
94
94
104
111
111
123
70-130
70-130
70-130
70-130
68-130
70-130
70-130
70-130
65-130
70-130
70-130
70-130
1
1
6
3
7
7
3
3
1
8
8
9
30
30
30
30
30
30
30
30
30
30
30
30
ParameterLCS
%RecoveryLCSD
%Recovery%Recovery
Limits RPD RPD Limits
Volatile Organics by GC/MS-5035 - Westborough Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG566791-3 WG566791-4
Lab Control Sample AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
1,2-Dichloroethane-d4
Toluene-d8
4-Bromofluorobenzene
Dibromofluoromethane
104
96
97
106
70-130
70-130
70-130
70-130
105
97
96
104
Surrogate Qual%Recovery Qual%RecoveryLCS LCSD
11/05/12
AcceptanceCriteria
Qual Qual Qual
Serial_No:11051209:46
Page 51 of 279
Methylene chloride
1,1-Dichloroethane
Chloroform
Carbon tetrachloride
1,2-Dichloropropane
Dibromochloromethane
1,1,2-Trichloroethane
Tetrachloroethene
Chlorobenzene
Trichlorofluoromethane
1,2-Dichloroethane
1,1,1-Trichloroethane
Bromodichloromethane
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
Bromoform
1,1,2,2-Tetrachloroethane
Benzene
Toluene
Ethylbenzene
Chloromethane
100
99
98
68
97
78
97
100
98
101
99
80
91
75
76
86
104
98
98
99
93
96
95
95
74
96
82
98
95
94
93
97
84
94
81
81
92
103
93
94
95
109
70-130
70-130
70-130
63-132
70-130
63-130
70-130
70-130
75-130
62-150
70-130
67-130
67-130
70-130
70-130
54-136
67-130
70-130
70-130
70-130
64-130
4
4
3
8
1
5
1
5
4
8
2
5
3
8
6
7
1
5
4
4
16
20
20
20
20
20
20
20
20
25
20
20
20
20
20
20
20
20
25
25
20
20
ParameterLCS
%RecoveryLCSD
%Recovery%Recovery
Limits RPD RPD Limits
Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 11,31 Batch: WG567640-3 WG567640-4
Lab Control Sample AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
Qual Qual Qual
Serial_No:11051209:46
Page 52 of 279
Bromomethane
Vinyl chloride
Chloroethane
1,1-Dichloroethene
trans-1,2-Dichloroethene
Trichloroethene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Methyl tert butyl ether
p/m-Xylene
o-Xylene
cis-1,2-Dichloroethene
Styrene
Dichlorodifluoromethane
Acetone
Carbon disulfide
2-Butanone
Vinyl acetate
4-Methyl-2-pentanone
2-Hexanone
112
94
94
97
97
97
98
100
96
83
97
98
97
87
91
105
101
99
77
86
99
132
92
92
93
90
93
95
96
93
89
94
97
88
87
86
107
88
100
86
92
105
39-139
55-140
55-138
61-145
70-130
70-130
70-130
70-130
70-130
63-130
70-130
70-130
70-130
70-130
36-147
58-148
51-130
63-138
70-130
59-130
57-130
16
2
2
4
7
4
3
4
3
7
3
1
10
0
6
2
14
1
11
7
6
20
20
20
25
20
25
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
ParameterLCS
%RecoveryLCSD
%Recovery%Recovery
Limits RPD RPD Limits
Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 11,31 Batch: WG567640-3 WG567640-4
Lab Control Sample AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
Qual Qual Qual
Serial_No:11051209:46
Page 53 of 279
Bromochloromethane
1,2-Dibromoethane
1,2-Dibromo-3-chloropropane
Isopropylbenzene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
Methyl Acetate
Cyclohexane
1,1,2-Trichloro-1,2,2-Trifluoroethane
Methyl cyclohexane
96
100
80
90
87
85
94
104
101
106
93
102
88
87
90
89
100
98
94
96
70-130
70-130
41-144
70-130
70-130
70-130
70-130
70-130
70-130
70-130
3
2
10
3
3
5
6
6
7
10
20
20
20
20
20
20
20
20
20
20
ParameterLCS
%RecoveryLCSD
%Recovery%Recovery
Limits RPD RPD Limits
Volatile Organics by GC/MS - Westborough Lab Associated sample(s): 11,31 Batch: WG567640-3 WG567640-4
Lab Control Sample AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
1,2-Dichloroethane-d4
Toluene-d8
4-Bromofluorobenzene
Dibromofluoromethane
102
100
107
99
70-130
70-130
70-130
70-130
101
100
103
99
Surrogate Qual%Recovery Qual%RecoveryLCS LCSD
11/05/12
AcceptanceCriteria
Qual Qual Qual
Serial_No:11051209:46
Page 54 of 279
SEMIVOLATILES
Serial_No:11051209:46
Page 55 of 279
FF
cis/trans-Decalin
C1-Decalin
C2-Decalin
C3-Decalin
C4-Decalin
Naphthalene
C1-Naphthalenes
C2-Naphthalenes
C3-Naphthalenes
C4-Naphthalenes
2-Methylnaphthalene
1-Methylnaphthalene
Benzothiophene
C1-Benzo(b)thiophene
C2-Benzo(b)thiophene
C3-Benzo(b)thiophene
C4-Benzo(b)thiophene
2,6-Dimethylnaphthalene
Acenaphthylene
Acenaphthene
2,3,5-Trimethylnaphthalene
Fluorene
C1-Fluorenes
C2-Fluorenes
C3-Fluorenes
Dibenzothiophene
4-Methyldibenzothiophene
2,3-Methyldibenzothiophene
1-Methyldibenzothiophene
C1-Dibenzothiophenes
C2-Dibenzothiophenes
Parameter Result
J
J
Dilution Factor
ND
3.59
13.6
19.6
36.1
76.5
48.2
53.0
41.8
31.8
55.7
26.0
3.58
6.15
8.53
13.6
9.20
28.7
209
26.9
6.78
34.4
44.3
66.8
82.8
27.4
19.4
27.6
6.30
61.3
95.6
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
PAHs - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
2.59
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
11/05/12
TN005SG-000014-20121005Client ID:10/05/12 09:32Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-01Lab ID:
Field Prep: Not SpecifiedMatrix: Sediment Extraction Method:
Cleanup Method1:Analytical Method:Analytical Date:Analyst:
1,8270D-SIM(M)10/17/12 14:00MT
ALPHA OP-013
EPA 3611BExtraction Date: 10/12/12 12:37
Cleanup Date1: 10/16/12 72%Percent Solids:
MDL
1.30
1.30
1.30
1.30
1.30
1.49
1.49
1.49
1.49
1.49
1.34
1.63
1.62
1.62
1.62
1.62
1.62
1.23
0.989
0.914
0.848
1.38
1.38
1.38
1.38
1.43
1.43
1.43
1.43
1.43
1.43
Serial_No:11051209:46
Page 56 of 279
C3-Dibenzothiophenes
C4-Dibenzothiophenes
Phenanthrene
2-Methylphenanthrene
2-Methylanthracene
9,4-Methylphenanthrene
C1-Phenanthrenes/anthracenes
C2-Phenanthrenes/anthracenes
C3-Phenanthrenes/anthracenes
C4-Phenanthrenes/anthracenes
Retene
Anthracene
Carbazole
1-Methylphenanthrene
Fluoranthene
Pyrene
C1-Pyrene/fluoranthenes
Benzonaphthothiophene
Benz(a)anthracene
Chrysene
C1-Benzanthracene/chrysenes
C2-Benzanthracene/chrysenes
C3-Benzanthracene/chrysenes
C4-Benzanthracene/chrysenes
Benzo(b)fluoranthene
Benzo(j)+(k)fluoranthene
Benzo(e)pyrene
Benzo(a)pyrene
Perylene
Indeno(1,2,3-cd)pyrene
Dibenz(a,h)+(a,c)anthracene
Benzo(g,h,i)perylene
Parameter Result Dilution Factor
94.7
46.3
270
50.6
60.3
85.9
295
325
170
81.4
ND
161
17.6
56.4
526
1230
1360
190
506
534
713
396
174
75.8
460
555
513
891
146
400
132
414
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
PAHs - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
5.18
Naphthalene-d8
Phenanthrene-d10
Benzo(a)pyrene-d12
76
95
88
50-130
50-130
50-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
TN005SG-000014-20121005Client ID:10/05/12 09:32Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-01Lab ID:
Field Prep: Not Specified
MDL
1.43
1.43
1.72
1.72
1.72
1.72
1.72
1.72
1.72
1.72
1.27
1.07
1.70
1.37
1.65
1.36
1.36
1.45
1.06
1.05
1.05
1.05
1.05
1.05
1.35
1.03
1.07
1.48
1.00
1.41
1.40
1.38
Serial_No:11051209:46
Page 57 of 279
cis/trans-Decalin
C1-Decalin
C2-Decalin
C3-Decalin
C4-Decalin
Naphthalene
C1-Naphthalenes
C2-Naphthalenes
C3-Naphthalenes
C4-Naphthalenes
2-Methylnaphthalene
1-Methylnaphthalene
Benzothiophene
C1-Benzo(b)thiophene
C2-Benzo(b)thiophene
C3-Benzo(b)thiophene
C4-Benzo(b)thiophene
2,6-Dimethylnaphthalene
Acenaphthylene
Acenaphthene
2,3,5-Trimethylnaphthalene
Fluorene
C1-Fluorenes
C2-Fluorenes
C3-Fluorenes
Dibenzothiophene
4-Methyldibenzothiophene
2,3-Methyldibenzothiophene
1-Methyldibenzothiophene
C1-Dibenzothiophenes
C2-Dibenzothiophenes
Parameter Result Dilution Factor
5.24
8.83
30.8
47.0
79.4
183
134
168
136
98.7
157
72.5
8.62
14.1
19.6
29.4
24.7
89.8
633
92.9
20.8
89.5
152
228
217
75.7
70.4
66.9
20.0
184
329
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
PAHs - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
2.23
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
11/05/12
TN002SG-000011-20121005Client ID:10/05/12 10:41Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-03Lab ID:
Field Prep: Not SpecifiedMatrix: Sediment Extraction Method:
Cleanup Method1:Analytical Method:Analytical Date:Analyst:
1,8270D-SIM(M)10/17/12 15:28MT
ALPHA OP-013
EPA 3611BExtraction Date: 10/12/12 12:37
Cleanup Date1: 10/16/12 55%Percent Solids:
MDL
1.12
1.12
1.12
1.12
1.12
1.28
1.28
1.28
1.28
1.28
1.15
1.41
1.40
1.40
1.40
1.40
1.40
1.06
0.852
0.788
0.731
1.19
1.19
1.19
1.19
1.23
1.23
1.23
1.23
1.23
1.23
Serial_No:11051209:46
Page 58 of 279
C3-Dibenzothiophenes
C4-Dibenzothiophenes
Phenanthrene
2-Methylphenanthrene
2-Methylanthracene
9,4-Methylphenanthrene
C1-Phenanthrenes/anthracenes
C2-Phenanthrenes/anthracenes
C3-Phenanthrenes/anthracenes
C4-Phenanthrenes/anthracenes
Retene
Anthracene
Carbazole
1-Methylphenanthrene
Fluoranthene
Pyrene
C1-Pyrene/fluoranthenes
Benzonaphthothiophene
Benz(a)anthracene
Chrysene
C1-Benzanthracene/chrysenes
C2-Benzanthracene/chrysenes
C3-Benzanthracene/chrysenes
C4-Benzanthracene/chrysenes
Benzo(b)fluoranthene
Benzo(j)+(k)fluoranthene
Benzo(e)pyrene
Benzo(a)pyrene
Perylene
Indeno(1,2,3-cd)pyrene
Dibenz(a,h)+(a,c)anthracene
Benzo(g,h,i)perylene
Parameter Result Dilution Factor
268
122
591
155
226
295
1010
1020
474
179
67.8
524
33.8
196
1410
2430
3430
507
1640
1730
2040
1110
496
207
1430
1470
1380
2540
441
1250
420
1270
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
PAHs - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
4.47
Naphthalene-d8
Phenanthrene-d10
Benzo(a)pyrene-d12
69
89
91
50-130
50-130
50-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
TN002SG-000011-20121005Client ID:10/05/12 10:41Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-03Lab ID:
Field Prep: Not Specified
MDL
1.23
1.23
1.48
1.48
1.48
1.48
1.48
1.48
1.48
1.48
1.10
0.921
1.46
1.18
1.42
1.18
1.18
1.25
0.911
0.903
0.903
0.903
0.903
0.903
1.16
0.887
0.922
1.28
0.862
1.21
1.21
1.19
Serial_No:11051209:46
Page 59 of 279
cis/trans-Decalin
C1-Decalin
C2-Decalin
C3-Decalin
C4-Decalin
Naphthalene
C1-Naphthalenes
C2-Naphthalenes
C3-Naphthalenes
C4-Naphthalenes
2-Methylnaphthalene
1-Methylnaphthalene
Benzothiophene
C1-Benzo(b)thiophene
C2-Benzo(b)thiophene
C3-Benzo(b)thiophene
C4-Benzo(b)thiophene
2,6-Dimethylnaphthalene
Acenaphthylene
Acenaphthene
2,3,5-Trimethylnaphthalene
Fluorene
C1-Fluorenes
C2-Fluorenes
C3-Fluorenes
Dibenzothiophene
4-Methyldibenzothiophene
2,3-Methyldibenzothiophene
1-Methyldibenzothiophene
C1-Dibenzothiophenes
C2-Dibenzothiophenes
Parameter Result Dilution Factor
9.65
17.8
59.3
93.3
167
338
241
323
253
172
272
138
15.6
27.1
38.4
54.3
38.6
176
1100
183
39.4
150
272
388
371
144
130
114
36.2
331
535
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
PAHs - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
4.28
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
11/05/12
TN003SG-000015-20121005Client ID:10/05/12 11:24Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-05Lab ID:
Field Prep: Not SpecifiedMatrix: Sediment Extraction Method:
Cleanup Method1:Analytical Method:Analytical Date:Analyst:
1,8270D-SIM(M)10/17/12 16:58MT
ALPHA OP-013
EPA 3611BExtraction Date: 10/12/12 12:37
Cleanup Date1: 10/16/12 41%Percent Solids:
MDL
2.15
2.15
2.15
2.15
2.15
2.46
2.46
2.46
2.46
2.46
2.21
2.70
2.68
2.68
2.68
2.68
2.68
2.03
1.63
1.51
1.40
2.28
2.28
2.28
2.28
2.36
2.36
2.36
2.36
2.36
2.36
Serial_No:11051209:46
Page 60 of 279
C3-Dibenzothiophenes
C4-Dibenzothiophenes
Phenanthrene
2-Methylphenanthrene
2-Methylanthracene
9,4-Methylphenanthrene
C1-Phenanthrenes/anthracenes
C2-Phenanthrenes/anthracenes
C3-Phenanthrenes/anthracenes
C4-Phenanthrenes/anthracenes
Retene
Anthracene
Carbazole
1-Methylphenanthrene
Fluoranthene
Pyrene
C1-Pyrene/fluoranthenes
Benzonaphthothiophene
Benz(a)anthracene
Chrysene
C1-Benzanthracene/chrysenes
C2-Benzanthracene/chrysenes
C3-Benzanthracene/chrysenes
C4-Benzanthracene/chrysenes
Benzo(b)fluoranthene
Benzo(j)+(k)fluoranthene
Benzo(e)pyrene
Benzo(a)pyrene
Perylene
Indeno(1,2,3-cd)pyrene
Dibenz(a,h)+(a,c)anthracene
Benzo(g,h,i)perylene
Parameter Result Dilution Factor
433
214
1030
248
373
506
1720
1640
767
324
129
910
50.1
345
2380
3720
5360
811
2620
2790
3130
1680
789
324
2080
2330
2180
3970
743
2080
703
2060
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
PAHs - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
8.56
Naphthalene-d8
Phenanthrene-d10
Benzo(a)pyrene-d12
65
87
90
50-130
50-130
50-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
TN003SG-000015-20121005Client ID:10/05/12 11:24Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-05Lab ID:
Field Prep: Not Specified
MDL
2.36
2.36
2.83
2.83
2.83
2.83
2.83
2.83
2.83
2.83
2.10
1.76
2.80
2.26
2.72
2.25
2.25
2.39
1.74
1.73
1.73
1.73
1.73
1.73
2.22
1.70
1.76
2.44
1.65
2.32
2.31
2.27
Serial_No:11051209:46
Page 61 of 279
cis/trans-Decalin
C1-Decalin
C2-Decalin
C3-Decalin
C4-Decalin
Naphthalene
C1-Naphthalenes
C2-Naphthalenes
C3-Naphthalenes
C4-Naphthalenes
2-Methylnaphthalene
1-Methylnaphthalene
Benzothiophene
C1-Benzo(b)thiophene
C2-Benzo(b)thiophene
C3-Benzo(b)thiophene
C4-Benzo(b)thiophene
2,6-Dimethylnaphthalene
Acenaphthylene
Acenaphthene
2,3,5-Trimethylnaphthalene
Fluorene
C1-Fluorenes
C2-Fluorenes
C3-Fluorenes
Dibenzothiophene
4-Methyldibenzothiophene
2,3-Methyldibenzothiophene
1-Methyldibenzothiophene
C1-Dibenzothiophenes
C2-Dibenzothiophenes
Parameter Result
J
Dilution Factor
3.39
5.30
16.2
23.5
38.2
123
83.9
101
74.8
50.0
94.3
49.9
5.76
9.32
12.0
17.0
13.8
55.9
238
76.0
10.8
67.8
80.7
105
109
49.2
34.9
37.5
10.4
99.4
141
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
PAHs - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
2.83
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
11/05/12
TN004SG-000015-20121005Client ID:10/05/12 11:46Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-07Lab ID:
Field Prep: Not SpecifiedMatrix: Sediment Extraction Method:
Cleanup Method1:Analytical Method:Analytical Date:Analyst:
1,8270D-SIM(M)10/17/12 18:26MT
ALPHA OP-013
EPA 3611BExtraction Date: 10/12/12 12:37
Cleanup Date1: 10/16/12 51%Percent Solids:
MDL
1.42
1.42
1.42
1.42
1.42
1.62
1.62
1.62
1.62
1.62
1.46
1.78
1.77
1.77
1.77
1.77
1.77
1.34
1.08
0.996
0.924
1.51
1.51
1.51
1.51
1.56
1.56
1.56
1.56
1.56
1.56
Serial_No:11051209:46
Page 62 of 279
C3-Dibenzothiophenes
C4-Dibenzothiophenes
Phenanthrene
2-Methylphenanthrene
2-Methylanthracene
9,4-Methylphenanthrene
C1-Phenanthrenes/anthracenes
C2-Phenanthrenes/anthracenes
C3-Phenanthrenes/anthracenes
C4-Phenanthrenes/anthracenes
Retene
Anthracene
Carbazole
1-Methylphenanthrene
Fluoranthene
Pyrene
C1-Pyrene/fluoranthenes
Benzonaphthothiophene
Benz(a)anthracene
Chrysene
C1-Benzanthracene/chrysenes
C2-Benzanthracene/chrysenes
C3-Benzanthracene/chrysenes
C4-Benzanthracene/chrysenes
Benzo(b)fluoranthene
Benzo(j)+(k)fluoranthene
Benzo(e)pyrene
Benzo(a)pyrene
Perylene
Indeno(1,2,3-cd)pyrene
Dibenz(a,h)+(a,c)anthracene
Benzo(g,h,i)perylene
Parameter Result Dilution Factor
123
61.5
465
83.7
97.3
142
505
459
243
94.5
53.1
267
40.8
104
827
1250
1490
240
772
822
876
468
213
104
624
700
611
1080
246
548
191
555
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
PAHs - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
5.65
Naphthalene-d8
Phenanthrene-d10
Benzo(a)pyrene-d12
65
87
88
50-130
50-130
50-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
TN004SG-000015-20121005Client ID:10/05/12 11:46Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-07Lab ID:
Field Prep: Not Specified
MDL
1.56
1.56
1.87
1.87
1.87
1.87
1.87
1.87
1.87
1.87
1.39
1.16
1.85
1.49
1.80
1.49
1.49
1.58
1.15
1.14
1.14
1.14
1.14
1.14
1.47
1.12
1.17
1.61
1.09
1.53
1.53
1.50
Serial_No:11051209:46
Page 63 of 279
cis/trans-Decalin
C1-Decalin
C2-Decalin
C3-Decalin
C4-Decalin
Naphthalene
C1-Naphthalenes
C2-Naphthalenes
C3-Naphthalenes
C4-Naphthalenes
2-Methylnaphthalene
1-Methylnaphthalene
Benzothiophene
C1-Benzo(b)thiophene
C2-Benzo(b)thiophene
C3-Benzo(b)thiophene
C4-Benzo(b)thiophene
2,6-Dimethylnaphthalene
Acenaphthylene
Acenaphthene
2,3,5-Trimethylnaphthalene
Fluorene
C1-Fluorenes
C2-Fluorenes
C3-Fluorenes
Dibenzothiophene
4-Methyldibenzothiophene
2,3-Methyldibenzothiophene
1-Methyldibenzothiophene
C1-Dibenzothiophenes
C2-Dibenzothiophenes
Parameter Result
J
J
J
J
J
J
G
Dilution Factor
ND
2.16
5.31
8.02
14.2
50.1
29.1
29.8
23.0
16.0
31.7
17.6
2.04
3.57
4.00
7.42
4.18
16.3
106
24.8
4.16
37.0
26.9
35.3
64.3
28.1
13.7
21.1
4.64
45.1
52.0
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
PAHs - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
2.11
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
11/05/12
TN006SG-000015-20121005Client ID:10/05/12 13:16Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-09Lab ID:
Field Prep: Not SpecifiedMatrix: Sediment Extraction Method:
Cleanup Method1:Analytical Method:Analytical Date:Analyst:
1,8270D-SIM(M)10/17/12 21:22MT
ALPHA OP-013
EPA 3611BExtraction Date: 10/12/12 12:37
Cleanup Date1: 10/16/12 78%Percent Solids:
MDL
1.06
1.06
1.06
1.06
1.06
1.21
1.21
1.21
1.21
1.21
1.09
1.33
1.32
1.32
1.32
1.32
1.32
1.00
0.805
0.744
0.690
1.12
1.12
1.12
1.12
1.16
1.16
1.16
1.16
1.16
1.16
Serial_No:11051209:46
Page 64 of 279
C3-Dibenzothiophenes
C4-Dibenzothiophenes
Phenanthrene
2-Methylphenanthrene
2-Methylanthracene
9,4-Methylphenanthrene
C1-Phenanthrenes/anthracenes
C2-Phenanthrenes/anthracenes
C3-Phenanthrenes/anthracenes
C4-Phenanthrenes/anthracenes
Retene
Anthracene
Carbazole
1-Methylphenanthrene
Fluoranthene
Pyrene
C1-Pyrene/fluoranthenes
Benzonaphthothiophene
Benz(a)anthracene
Chrysene
C1-Benzanthracene/chrysenes
C2-Benzanthracene/chrysenes
C3-Benzanthracene/chrysenes
C4-Benzanthracene/chrysenes
Benzo(b)fluoranthene
Benzo(j)+(k)fluoranthene
Benzo(e)pyrene
Benzo(a)pyrene
Perylene
Indeno(1,2,3-cd)pyrene
Dibenz(a,h)+(a,c)anthracene
Benzo(g,h,i)perylene
Parameter Result Dilution Factor
40.8
18.9
427
66.6
26.8
59.3
250
172
81.3
35.3
ND
127
50.7
58.0
973
915
572
141
560
568
349
173
95.2
60.8
497
491
385
594
144
392
124
357
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
PAHs - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
4.22
Naphthalene-d8
Phenanthrene-d10
Benzo(a)pyrene-d12
75
93
86
50-130
50-130
50-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
TN006SG-000015-20121005Client ID:10/05/12 13:16Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-09Lab ID:
Field Prep: Not Specified
MDL
1.16
1.16
1.40
1.40
1.40
1.40
1.40
1.40
1.40
1.40
1.04
0.870
1.38
1.11
1.34
1.11
1.11
1.18
0.860
0.853
0.853
0.853
0.853
0.853
1.10
0.837
0.870
1.20
0.814
1.14
1.14
1.12
Serial_No:11051209:46
Page 65 of 279
cis/trans-Decalin
C1-Decalin
C2-Decalin
C3-Decalin
C4-Decalin
Naphthalene
C1-Naphthalenes
C2-Naphthalenes
C3-Naphthalenes
C4-Naphthalenes
2-Methylnaphthalene
1-Methylnaphthalene
Benzothiophene
C1-Benzo(b)thiophene
C2-Benzo(b)thiophene
C3-Benzo(b)thiophene
C4-Benzo(b)thiophene
2,6-Dimethylnaphthalene
Acenaphthylene
Acenaphthene
2,3,5-Trimethylnaphthalene
Fluorene
C1-Fluorenes
C2-Fluorenes
C3-Fluorenes
Dibenzothiophene
4-Methyldibenzothiophene
2,3-Methyldibenzothiophene
1-Methyldibenzothiophene
C1-Dibenzothiophenes
C2-Dibenzothiophenes
Parameter Result
J
J
J
J
J
J
J
Dilution Factor
3.02
ND
ND
ND
ND
70.8
17.9
6.65
4.58
ND
18.4
11.1
ND
ND
ND
ND
ND
ND
2.52
3.00
ND
7.38
ND
ND
ND
ND
ND
ND
ND
ND
ND
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
PAHs - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
5.81
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11/05/12
SG-RB-20121006Client ID:10/06/12 09:05Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-11Lab ID:
Field Prep: Not SpecifiedMatrix: Water Extraction Method:Analytical Method:Analytical Date:Analyst:
1,8270D-SIM(M)10/17/12 02:12MT
EPA 3510CExtraction Date: 10/10/12 07:46
MDL
2.51
2.51
2.51
2.51
2.51
2.73
2.73
2.73
2.73
2.73
1.55
1.88
2.89
2.89
2.89
2.89
2.89
3.25
2.44
1.56
2.21
2.53
2.53
2.53
2.53
1.66
1.66
1.66
1.66
1.66
1.66
Serial_No:11051209:46
Page 66 of 279
C3-Dibenzothiophenes
C4-Dibenzothiophenes
Phenanthrene
2-Methylphenanthrene
2-Methylanthracene
9,4-Methylphenanthrene
C1-Phenanthrenes/anthracenes
C2-Phenanthrenes/anthracenes
C3-Phenanthrenes/anthracenes
C4-Phenanthrenes/anthracenes
Retene
Anthracene
Carbazole
1-Methylphenanthrene
Fluoranthene
Pyrene
C1-Pyrene/fluoranthenes
Benzonaphthothiophene
Benz(a)anthracene
Chrysene
C1-Benzanthracene/chrysenes
C2-Benzanthracene/chrysenes
C3-Benzanthracene/chrysenes
C4-Benzanthracene/chrysenes
Benzo(b)fluoranthene
Benzo(j)+(k)fluoranthene
Benzo(e)pyrene
Benzo(a)pyrene
Perylene
Indeno(1,2,3-cd)pyrene
Dibenz(a,h)+(a,c)anthracene
Benzo(g,h,i)perylene
Parameter Result
J
J
J
J
Dilution Factor
ND
ND
4.54
ND
ND
ND
ND
4.15
ND
ND
4.18
ND
ND
ND
ND
1.69
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
PAHs - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
Naphthalene-d8
Phenanthrene-d10
Benzo(a)pyrene-d12
85
100
85
50-130
50-130
50-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
SG-RB-20121006Client ID:10/06/12 09:05Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-11Lab ID:
Field Prep: Not Specified
MDL
1.66
1.66
2.76
2.76
2.76
2.76
2.76
2.76
2.76
2.76
2.63
2.17
5.33
4.04
3.05
1.05
1.05
1.37
3.08
1.88
1.88
1.88
1.88
1.88
1.30
2.98
1.91
4.94
3.39
2.11
2.53
1.90
Serial_No:11051209:46
Page 67 of 279
cis/trans-Decalin
C1-Decalin
C2-Decalin
C3-Decalin
C4-Decalin
Naphthalene
C1-Naphthalenes
C2-Naphthalenes
C3-Naphthalenes
C4-Naphthalenes
2-Methylnaphthalene
1-Methylnaphthalene
Benzothiophene
C1-Benzo(b)thiophene
C2-Benzo(b)thiophene
C3-Benzo(b)thiophene
C4-Benzo(b)thiophene
2,6-Dimethylnaphthalene
Acenaphthylene
Acenaphthene
2,3,5-Trimethylnaphthalene
Fluorene
C1-Fluorenes
C2-Fluorenes
C3-Fluorenes
Dibenzothiophene
4-Methyldibenzothiophene
2,3-Methyldibenzothiophene
1-Methyldibenzothiophene
C1-Dibenzothiophenes
C2-Dibenzothiophenes
Parameter Result
J
J
G
J
Dilution Factor
25.3
17.6
62.4
70.3
126
47.2
35.7
95.8
40.8
46.9
37.7
18.3
ND
ND
11.2
24.0
ND
119
90.0
29.0
4.64
36.5
25.4
66.5
178
26.2
13.2
55.0
ND
78.3
89.8
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
PAHs - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
7.30
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
11/05/12
HB008SG-000015-20121006Client ID:10/06/12 09:55Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-13Lab ID:
Field Prep: Not SpecifiedMatrix: Sediment Extraction Method:
Cleanup Method1:Analytical Method:Analytical Date:Analyst:
1,8270D-SIM(M)10/17/12 22:50MT
ALPHA OP-013
EPA 3611BExtraction Date: 10/12/12 12:37
Cleanup Date1: 10/16/12 27%Percent Solids:
MDL
3.67
3.67
3.67
3.67
3.67
4.20
4.20
4.20
4.20
4.20
3.77
4.60
4.58
4.58
4.58
4.58
4.58
3.47
2.79
2.58
2.39
3.90
3.90
3.90
3.90
4.03
4.03
4.03
4.03
4.03
4.03
Serial_No:11051209:46
Page 68 of 279
C3-Dibenzothiophenes
C4-Dibenzothiophenes
Phenanthrene
2-Methylphenanthrene
2-Methylanthracene
9,4-Methylphenanthrene
C1-Phenanthrenes/anthracenes
C2-Phenanthrenes/anthracenes
C3-Phenanthrenes/anthracenes
C4-Phenanthrenes/anthracenes
Retene
Anthracene
Carbazole
1-Methylphenanthrene
Fluoranthene
Pyrene
C1-Pyrene/fluoranthenes
Benzonaphthothiophene
Benz(a)anthracene
Chrysene
C1-Benzanthracene/chrysenes
C2-Benzanthracene/chrysenes
C3-Benzanthracene/chrysenes
C4-Benzanthracene/chrysenes
Benzo(b)fluoranthene
Benzo(j)+(k)fluoranthene
Benzo(e)pyrene
Benzo(a)pyrene
Perylene
Indeno(1,2,3-cd)pyrene
Dibenz(a,h)+(a,c)anthracene
Benzo(g,h,i)perylene
Parameter Result Dilution Factor
158
124
273
42.0
26.4
49.1
204
298
262
188
ND
139
41.4
40.1
1160
1290
700
208
559
798
513
485
449
326
1030
881
774
858
284
817
196
792
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
PAHs - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
14.6
Naphthalene-d8
Phenanthrene-d10
Benzo(a)pyrene-d12
73
96
97
50-130
50-130
50-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
HB008SG-000015-20121006Client ID:10/06/12 09:55Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-13Lab ID:
Field Prep: Not Specified
MDL
4.03
4.03
4.84
4.84
4.84
4.84
4.84
4.84
4.84
4.84
3.58
3.01
4.78
3.86
4.64
3.84
3.84
4.09
2.98
2.95
2.95
2.95
2.95
2.95
3.80
2.90
3.01
4.17
2.82
3.96
3.95
3.88
Serial_No:11051209:46
Page 69 of 279
cis/trans-Decalin
C1-Decalin
C2-Decalin
C3-Decalin
C4-Decalin
Naphthalene
C1-Naphthalenes
C2-Naphthalenes
C3-Naphthalenes
C4-Naphthalenes
2-Methylnaphthalene
1-Methylnaphthalene
Benzothiophene
C1-Benzo(b)thiophene
C2-Benzo(b)thiophene
C3-Benzo(b)thiophene
C4-Benzo(b)thiophene
2,6-Dimethylnaphthalene
Acenaphthylene
Acenaphthene
2,3,5-Trimethylnaphthalene
Fluorene
C1-Fluorenes
C2-Fluorenes
C3-Fluorenes
Dibenzothiophene
4-Methyldibenzothiophene
2,3-Methyldibenzothiophene
1-Methyldibenzothiophene
C1-Dibenzothiophenes
C2-Dibenzothiophenes
Parameter Result
J
J
G
J
Dilution Factor
29.2
20.7
72.6
79.0
150
54.6
40.2
130
50.6
55.9
42.8
20.5
ND
ND
15.0
29.8
ND
172
122
33.7
6.83
50.0
28.4
81.8
213
37.1
18.6
77.6
5.52
107
82.8
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
PAHs - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
8.71
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
11/05/12
HB007SG-000015-20121006Client ID:10/06/12 10:45Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-15Lab ID:
Field Prep: Not SpecifiedMatrix: Sediment Extraction Method:
Cleanup Method1:Analytical Method:Analytical Date:Analyst:
1,8270D-SIM(M)10/18/12 00:18MT
ALPHA OP-013
EPA 3611BExtraction Date: 10/12/12 12:37
Cleanup Date1: 10/16/12 25%Percent Solids:
MDL
4.37
4.37
4.37
4.37
4.37
5.01
5.01
5.01
5.01
5.01
4.49
5.49
5.46
5.46
5.46
5.46
5.46
4.14
3.32
3.07
2.85
4.65
4.65
4.65
4.65
4.80
4.80
4.80
4.80
4.80
4.80
Serial_No:11051209:46
Page 70 of 279
C3-Dibenzothiophenes
C4-Dibenzothiophenes
Phenanthrene
2-Methylphenanthrene
2-Methylanthracene
9,4-Methylphenanthrene
C1-Phenanthrenes/anthracenes
C2-Phenanthrenes/anthracenes
C3-Phenanthrenes/anthracenes
C4-Phenanthrenes/anthracenes
Retene
Anthracene
Carbazole
1-Methylphenanthrene
Fluoranthene
Pyrene
C1-Pyrene/fluoranthenes
Benzonaphthothiophene
Benz(a)anthracene
Chrysene
C1-Benzanthracene/chrysenes
C2-Benzanthracene/chrysenes
C3-Benzanthracene/chrysenes
C4-Benzanthracene/chrysenes
Benzo(b)fluoranthene
Benzo(j)+(k)fluoranthene
Benzo(e)pyrene
Benzo(a)pyrene
Perylene
Indeno(1,2,3-cd)pyrene
Dibenz(a,h)+(a,c)anthracene
Benzo(g,h,i)perylene
Parameter Result Dilution Factor
136
110
366
55.6
32.0
60.4
259
347
255
177
ND
195
59.9
57.4
1900
1860
876
282
764
1070
553
430
473
393
1560
1190
1190
1290
384
1140
274
1130
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
PAHs - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
17.4
Naphthalene-d8
Phenanthrene-d10
Benzo(a)pyrene-d12
70
91
98
50-130
50-130
50-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
HB007SG-000015-20121006Client ID:10/06/12 10:45Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-15Lab ID:
Field Prep: Not Specified
MDL
4.80
4.80
5.77
5.77
5.77
5.77
5.77
5.77
5.77
5.77
4.27
3.59
5.70
4.60
5.54
4.58
4.58
4.87
3.55
3.52
3.52
3.52
3.52
3.52
4.53
3.46
3.59
4.97
3.36
4.73
4.70
4.63
Serial_No:11051209:46
Page 71 of 279
cis/trans-Decalin
C1-Decalin
C2-Decalin
C3-Decalin
C4-Decalin
Naphthalene
C1-Naphthalenes
C2-Naphthalenes
C3-Naphthalenes
C4-Naphthalenes
2-Methylnaphthalene
1-Methylnaphthalene
Benzothiophene
C1-Benzo(b)thiophene
C2-Benzo(b)thiophene
C3-Benzo(b)thiophene
C4-Benzo(b)thiophene
2,6-Dimethylnaphthalene
Acenaphthylene
Acenaphthene
2,3,5-Trimethylnaphthalene
Fluorene
C1-Fluorenes
C2-Fluorenes
C3-Fluorenes
Dibenzothiophene
4-Methyldibenzothiophene
2,3-Methyldibenzothiophene
1-Methyldibenzothiophene
C1-Dibenzothiophenes
C2-Dibenzothiophenes
Parameter Result
J
J
J
J
J
J
J
G
J
J
Dilution Factor
13.2
5.55
17.7
ND
ND
15.0
12.2
33.5
16.8
16.8
11.7
6.18
ND
ND
5.93
13.7
ND
40.8
26.1
9.33
ND
14.8
8.50
22.7
56.4
8.38
4.17
30.2
ND
39.5
18.0
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
PAHs - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
6.16
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
11/05/12
HB006SG-000015-20121006Client ID:10/06/12 11:30Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-17Lab ID:
Field Prep: Not SpecifiedMatrix: Sediment Extraction Method:
Cleanup Method1:Analytical Method:Analytical Date:Analyst:
1,8270D-SIM(M)10/18/12 01:45MT
ALPHA OP-013
EPA 3611BExtraction Date: 10/12/12 12:37
Cleanup Date1: 10/16/12 34%Percent Solids:
MDL
3.09
3.09
3.09
3.09
3.09
3.54
3.54
3.54
3.54
3.54
3.18
3.88
3.86
3.86
3.86
3.86
3.86
2.93
2.35
2.17
2.01
3.28
3.28
3.28
3.28
3.40
3.40
3.40
3.40
3.40
3.40
Serial_No:11051209:46
Page 72 of 279
C3-Dibenzothiophenes
C4-Dibenzothiophenes
Phenanthrene
2-Methylphenanthrene
2-Methylanthracene
9,4-Methylphenanthrene
C1-Phenanthrenes/anthracenes
C2-Phenanthrenes/anthracenes
C3-Phenanthrenes/anthracenes
C4-Phenanthrenes/anthracenes
Retene
Anthracene
Carbazole
1-Methylphenanthrene
Fluoranthene
Pyrene
C1-Pyrene/fluoranthenes
Benzonaphthothiophene
Benz(a)anthracene
Chrysene
C1-Benzanthracene/chrysenes
C2-Benzanthracene/chrysenes
C3-Benzanthracene/chrysenes
C4-Benzanthracene/chrysenes
Benzo(b)fluoranthene
Benzo(j)+(k)fluoranthene
Benzo(e)pyrene
Benzo(a)pyrene
Perylene
Indeno(1,2,3-cd)pyrene
Dibenz(a,h)+(a,c)anthracene
Benzo(g,h,i)perylene
Parameter Result
J
J
J
Dilution Factor
25.5
21.1
86.1
13.2
6.75
13.0
59.4
53.3
45.2
35.8
8.32
40.4
11.9
13.5
337
328
164
54.2
136
205
99.6
72.7
89.3
98.5
262
204
187
209
161
194
48.9
198
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
PAHs - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
12.3
Naphthalene-d8
Phenanthrene-d10
Benzo(a)pyrene-d12
71
99
92
50-130
50-130
50-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
HB006SG-000015-20121006Client ID:10/06/12 11:30Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-17Lab ID:
Field Prep: Not Specified
MDL
3.40
3.40
4.08
4.08
4.08
4.08
4.08
4.08
4.08
4.08
3.02
2.54
4.03
3.25
3.91
3.24
3.24
3.45
2.51
2.49
2.49
2.49
2.49
2.49
3.20
2.44
2.54
3.52
2.38
3.34
3.33
3.27
Serial_No:11051209:46
Page 73 of 279
cis/trans-Decalin
C1-Decalin
C2-Decalin
C3-Decalin
C4-Decalin
Naphthalene
C1-Naphthalenes
C2-Naphthalenes
C3-Naphthalenes
C4-Naphthalenes
2-Methylnaphthalene
1-Methylnaphthalene
Benzothiophene
C1-Benzo(b)thiophene
C2-Benzo(b)thiophene
C3-Benzo(b)thiophene
C4-Benzo(b)thiophene
2,6-Dimethylnaphthalene
Acenaphthylene
Acenaphthene
2,3,5-Trimethylnaphthalene
Fluorene
C1-Fluorenes
C2-Fluorenes
C3-Fluorenes
Dibenzothiophene
4-Methyldibenzothiophene
2,3-Methyldibenzothiophene
1-Methyldibenzothiophene
C1-Dibenzothiophenes
C2-Dibenzothiophenes
Parameter Result
J
J
G
J
Dilution Factor
31.0
18.8
60.3
72.4
124
50.7
40.8
119
47.0
49.0
42.5
20.8
ND
ND
14.8
28.6
ND
152
102
27.2
6.05
45.2
24.8
66.7
205
30.4
14.6
56.0
ND
80.2
70.5
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
PAHs - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
8.37
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
11/05/12
HB005SG-000015-20121006Client ID:10/06/12 12:19Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-19Lab ID:
Field Prep: Not SpecifiedMatrix: Sediment Extraction Method:
Cleanup Method1:Analytical Method:Analytical Date:Analyst:
1,8270D-SIM(M)10/18/12 03:12MT
ALPHA OP-013
EPA 3611BExtraction Date: 10/12/12 12:37
Cleanup Date1: 10/16/12 26%Percent Solids:
MDL
4.20
4.20
4.20
4.20
4.20
4.81
4.81
4.81
4.81
4.81
4.32
5.27
5.24
5.24
5.24
5.24
5.24
3.98
3.19
2.95
2.74
4.46
4.46
4.46
4.46
4.61
4.61
4.61
4.61
4.61
4.61
Serial_No:11051209:46
Page 74 of 279
C3-Dibenzothiophenes
C4-Dibenzothiophenes
Phenanthrene
2-Methylphenanthrene
2-Methylanthracene
9,4-Methylphenanthrene
C1-Phenanthrenes/anthracenes
C2-Phenanthrenes/anthracenes
C3-Phenanthrenes/anthracenes
C4-Phenanthrenes/anthracenes
Retene
Anthracene
Carbazole
1-Methylphenanthrene
Fluoranthene
Pyrene
C1-Pyrene/fluoranthenes
Benzonaphthothiophene
Benz(a)anthracene
Chrysene
C1-Benzanthracene/chrysenes
C2-Benzanthracene/chrysenes
C3-Benzanthracene/chrysenes
C4-Benzanthracene/chrysenes
Benzo(b)fluoranthene
Benzo(j)+(k)fluoranthene
Benzo(e)pyrene
Benzo(a)pyrene
Perylene
Indeno(1,2,3-cd)pyrene
Dibenz(a,h)+(a,c)anthracene
Benzo(g,h,i)perylene
Parameter Result Dilution Factor
108
93.6
302
45.1
24.9
50.2
219
282
213
143
ND
156
47.8
52.1
1420
1510
722
231
618
901
445
338
371
338
1250
1010
978
1070
324
974
236
950
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
PAHs - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
16.7
Naphthalene-d8
Phenanthrene-d10
Benzo(a)pyrene-d12
71
92
102
50-130
50-130
50-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
HB005SG-000015-20121006Client ID:10/06/12 12:19Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-19Lab ID:
Field Prep: Not Specified
MDL
4.61
4.61
5.54
5.54
5.54
5.54
5.54
5.54
5.54
5.54
4.10
3.45
5.47
4.42
5.32
4.40
4.40
4.68
3.41
3.38
3.38
3.38
3.38
3.38
4.35
3.32
3.45
4.78
3.23
4.54
4.52
4.44
Serial_No:11051209:46
Page 75 of 279
cis/trans-Decalin
C1-Decalin
C2-Decalin
C3-Decalin
C4-Decalin
Naphthalene
C1-Naphthalenes
C2-Naphthalenes
C3-Naphthalenes
C4-Naphthalenes
2-Methylnaphthalene
1-Methylnaphthalene
Benzothiophene
C1-Benzo(b)thiophene
C2-Benzo(b)thiophene
C3-Benzo(b)thiophene
C4-Benzo(b)thiophene
2,6-Dimethylnaphthalene
Acenaphthylene
Acenaphthene
2,3,5-Trimethylnaphthalene
Fluorene
C1-Fluorenes
C2-Fluorenes
C3-Fluorenes
Dibenzothiophene
4-Methyldibenzothiophene
2,3-Methyldibenzothiophene
1-Methyldibenzothiophene
C1-Dibenzothiophenes
C2-Dibenzothiophenes
Parameter Result
J
J
G
J
Dilution Factor
27.4
18.9
62.6
81.2
122
52.1
40.4
130
45.6
52.4
42.4
20.4
ND
ND
13.4
24.8
ND
177
100
27.3
4.00
43.2
26.9
71.5
189
31.4
15.3
66.6
4.72
89.4
68.7
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
PAHs - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
7.55
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
11/05/12
HB1005SG-000015-20121006Client ID:10/06/12 12:19Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-21Lab ID:
Field Prep: Not SpecifiedMatrix: Sediment Extraction Method:
Cleanup Method1:Analytical Method:Analytical Date:Analyst:
1,8270D-SIM(M)10/18/12 04:38MT
ALPHA OP-013
EPA 3611BExtraction Date: 10/12/12 12:37
Cleanup Date1: 10/16/12 25%Percent Solids:
MDL
3.79
3.79
3.79
3.79
3.79
4.34
4.34
4.34
4.34
4.34
3.90
4.76
4.73
4.73
4.73
4.73
4.73
3.59
2.88
2.66
2.47
4.03
4.03
4.03
4.03
4.16
4.16
4.16
4.16
4.16
4.16
Serial_No:11051209:46
Page 76 of 279
C3-Dibenzothiophenes
C4-Dibenzothiophenes
Phenanthrene
2-Methylphenanthrene
2-Methylanthracene
9,4-Methylphenanthrene
C1-Phenanthrenes/anthracenes
C2-Phenanthrenes/anthracenes
C3-Phenanthrenes/anthracenes
C4-Phenanthrenes/anthracenes
Retene
Anthracene
Carbazole
1-Methylphenanthrene
Fluoranthene
Pyrene
C1-Pyrene/fluoranthenes
Benzonaphthothiophene
Benz(a)anthracene
Chrysene
C1-Benzanthracene/chrysenes
C2-Benzanthracene/chrysenes
C3-Benzanthracene/chrysenes
C4-Benzanthracene/chrysenes
Benzo(b)fluoranthene
Benzo(j)+(k)fluoranthene
Benzo(e)pyrene
Benzo(a)pyrene
Perylene
Indeno(1,2,3-cd)pyrene
Dibenz(a,h)+(a,c)anthracene
Benzo(g,h,i)perylene
Parameter Result Dilution Factor
104
85.8
291
46.0
26.7
55.4
222
269
201
136
ND
159
49.1
47.2
1350
1430
680
222
585
817
429
329
322
265
1200
920
860
936
279
918
236
885
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
PAHs - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
15.1
Naphthalene-d8
Phenanthrene-d10
Benzo(a)pyrene-d12
74
96
92
50-130
50-130
50-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
HB1005SG-000015-20121006Client ID:10/06/12 12:19Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-21Lab ID:
Field Prep: Not Specified
MDL
4.16
4.16
5.00
5.00
5.00
5.00
5.00
5.00
5.00
5.00
3.71
3.11
4.94
3.99
4.80
3.97
3.97
4.23
3.08
3.05
3.05
3.05
3.05
3.05
3.93
3.00
3.12
4.31
2.92
4.10
4.08
4.01
Serial_No:11051209:46
Page 77 of 279
cis/trans-Decalin
C1-Decalin
C2-Decalin
C3-Decalin
C4-Decalin
Naphthalene
C1-Naphthalenes
C2-Naphthalenes
C3-Naphthalenes
C4-Naphthalenes
2-Methylnaphthalene
1-Methylnaphthalene
Benzothiophene
C1-Benzo(b)thiophene
C2-Benzo(b)thiophene
C3-Benzo(b)thiophene
C4-Benzo(b)thiophene
2,6-Dimethylnaphthalene
Acenaphthylene
Acenaphthene
2,3,5-Trimethylnaphthalene
Fluorene
C1-Fluorenes
C2-Fluorenes
C3-Fluorenes
Dibenzothiophene
4-Methyldibenzothiophene
2,3-Methyldibenzothiophene
1-Methyldibenzothiophene
C1-Dibenzothiophenes
C2-Dibenzothiophenes
Parameter Result
J
J
G
J
J
Dilution Factor
19.1
11.7
34.4
36.6
66.3
29.6
23.6
82.5
28.2
26.2
24.9
12.2
ND
ND
8.88
16.8
ND
111
59.4
14.7
1.83
20.3
15.2
37.7
107
13.7
7.74
24.9
3.16
39.7
38.7
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
PAHs - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
5.36
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
11/05/12
HB004SG-000015-20121006Client ID:10/06/12 13:27Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-23Lab ID:
Field Prep: Not SpecifiedMatrix: Sediment Extraction Method:
Cleanup Method1:Analytical Method:Analytical Date:Analyst:
1,8270D-SIM(M)10/18/12 06:04MT
ALPHA OP-013
EPA 3611BExtraction Date: 10/12/12 12:37
Cleanup Date1: 10/16/12 35%Percent Solids:
MDL
2.69
2.69
2.69
2.69
2.69
3.08
3.08
3.08
3.08
3.08
2.76
3.38
3.36
3.36
3.36
3.36
3.36
2.55
2.04
1.89
1.75
2.86
2.86
2.86
2.86
2.96
2.96
2.96
2.96
2.96
2.96
Serial_No:11051209:46
Page 78 of 279
C3-Dibenzothiophenes
C4-Dibenzothiophenes
Phenanthrene
2-Methylphenanthrene
2-Methylanthracene
9,4-Methylphenanthrene
C1-Phenanthrenes/anthracenes
C2-Phenanthrenes/anthracenes
C3-Phenanthrenes/anthracenes
C4-Phenanthrenes/anthracenes
Retene
Anthracene
Carbazole
1-Methylphenanthrene
Fluoranthene
Pyrene
C1-Pyrene/fluoranthenes
Benzonaphthothiophene
Benz(a)anthracene
Chrysene
C1-Benzanthracene/chrysenes
C2-Benzanthracene/chrysenes
C3-Benzanthracene/chrysenes
C4-Benzanthracene/chrysenes
Benzo(b)fluoranthene
Benzo(j)+(k)fluoranthene
Benzo(e)pyrene
Benzo(a)pyrene
Perylene
Indeno(1,2,3-cd)pyrene
Dibenz(a,h)+(a,c)anthracene
Benzo(g,h,i)perylene
Parameter Result Dilution Factor
51.8
47.7
163
25.8
14.0
28.5
125
143
110
83.7
ND
80.5
22.2
27.4
546
709
351
98.2
275
384
234
174
192
166
596
514
454
499
150
455
110
443
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
PAHs - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
10.7
Naphthalene-d8
Phenanthrene-d10
Benzo(a)pyrene-d12
73
97
102
50-130
50-130
50-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
HB004SG-000015-20121006Client ID:10/06/12 13:27Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-23Lab ID:
Field Prep: Not Specified
MDL
2.96
2.96
3.55
3.55
3.55
3.55
3.55
3.55
3.55
3.55
2.63
2.21
3.50
2.83
3.40
2.82
2.82
3.00
2.18
2.17
2.17
2.17
2.17
2.17
2.79
2.13
2.21
3.06
2.07
2.91
2.90
2.85
Serial_No:11051209:46
Page 79 of 279
cis/trans-Decalin
C1-Decalin
C2-Decalin
C3-Decalin
C4-Decalin
Naphthalene
C1-Naphthalenes
C2-Naphthalenes
C3-Naphthalenes
C4-Naphthalenes
2-Methylnaphthalene
1-Methylnaphthalene
Benzothiophene
C1-Benzo(b)thiophene
C2-Benzo(b)thiophene
C3-Benzo(b)thiophene
C4-Benzo(b)thiophene
2,6-Dimethylnaphthalene
Acenaphthylene
Acenaphthene
2,3,5-Trimethylnaphthalene
Fluorene
C1-Fluorenes
C2-Fluorenes
C3-Fluorenes
Dibenzothiophene
4-Methyldibenzothiophene
2,3-Methyldibenzothiophene
1-Methyldibenzothiophene
C1-Dibenzothiophenes
C2-Dibenzothiophenes
Parameter Result
J
J
J
G
J
Dilution Factor
30.6
11.9
40.0
34.4
72.6
46.1
36.4
102
39.9
34.9
38.5
18.9
ND
ND
9.70
22.8
ND
124
80.1
28.6
4.33
41.6
22.7
55.8
156
27.9
12.2
48.3
ND
69.1
52.7
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
PAHs - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
7.43
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
11/05/12
HB003SG-000015-20121006Client ID:10/06/12 14:21Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-25Lab ID:
Field Prep: Not SpecifiedMatrix: Sediment Extraction Method:
Cleanup Method1:Analytical Method:Analytical Date:Analyst:
1,8270D-SIM(M)10/18/12 07:31MT
ALPHA OP-013
EPA 3611BExtraction Date: 10/12/12 14:50
Cleanup Date1: 10/16/12 28%Percent Solids:
MDL
3.73
3.73
3.73
3.73
3.73
4.27
4.27
4.27
4.27
4.27
3.83
4.68
4.66
4.66
4.66
4.66
4.66
3.53
2.84
2.62
2.43
3.96
3.96
3.96
3.96
4.10
4.10
4.10
4.10
4.10
4.10
Serial_No:11051209:46
Page 80 of 279
C3-Dibenzothiophenes
C4-Dibenzothiophenes
Phenanthrene
2-Methylphenanthrene
2-Methylanthracene
9,4-Methylphenanthrene
C1-Phenanthrenes/anthracenes
C2-Phenanthrenes/anthracenes
C3-Phenanthrenes/anthracenes
C4-Phenanthrenes/anthracenes
Retene
Anthracene
Carbazole
1-Methylphenanthrene
Fluoranthene
Pyrene
C1-Pyrene/fluoranthenes
Benzonaphthothiophene
Benz(a)anthracene
Chrysene
C1-Benzanthracene/chrysenes
C2-Benzanthracene/chrysenes
C3-Benzanthracene/chrysenes
C4-Benzanthracene/chrysenes
Benzo(b)fluoranthene
Benzo(j)+(k)fluoranthene
Benzo(e)pyrene
Benzo(a)pyrene
Perylene
Indeno(1,2,3-cd)pyrene
Dibenz(a,h)+(a,c)anthracene
Benzo(g,h,i)perylene
Parameter Result Dilution Factor
70.6
63.4
344
43.6
19.5
44.6
194
220
146
98.3
ND
125
48.6
43.7
1050
1140
543
169
475
666
345
247
283
269
890
782
737
826
245
708
177
704
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
PAHs - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
14.9
Naphthalene-d8
Phenanthrene-d10
Benzo(a)pyrene-d12
71
93
102
50-130
50-130
50-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
HB003SG-000015-20121006Client ID:10/06/12 14:21Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-25Lab ID:
Field Prep: Not Specified
MDL
4.10
4.10
4.92
4.92
4.92
4.92
4.92
4.92
4.92
4.92
3.65
3.06
4.86
3.92
4.72
3.91
3.91
4.16
3.03
3.00
3.00
3.00
3.00
3.00
3.86
2.95
3.07
4.24
2.87
4.03
4.02
3.95
Serial_No:11051209:46
Page 81 of 279
cis/trans-Decalin
C1-Decalin
C2-Decalin
C3-Decalin
C4-Decalin
Naphthalene
C1-Naphthalenes
C2-Naphthalenes
C3-Naphthalenes
C4-Naphthalenes
2-Methylnaphthalene
1-Methylnaphthalene
Benzothiophene
C1-Benzo(b)thiophene
C2-Benzo(b)thiophene
C3-Benzo(b)thiophene
C4-Benzo(b)thiophene
2,6-Dimethylnaphthalene
Acenaphthylene
Acenaphthene
2,3,5-Trimethylnaphthalene
Fluorene
C1-Fluorenes
C2-Fluorenes
C3-Fluorenes
Dibenzothiophene
4-Methyldibenzothiophene
2,3-Methyldibenzothiophene
1-Methyldibenzothiophene
C1-Dibenzothiophenes
C2-Dibenzothiophenes
Parameter Result
J
J
J
G
J
Dilution Factor
23.2
8.53
24.4
30.1
52.5
31.6
25.9
62.6
27.9
25.2
27.9
12.6
ND
ND
8.64
18.1
ND
74.1
50.9
13.1
2.99
20.8
15.3
37.7
98.7
14.2
7.86
26.4
ND
41.3
33.9
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
PAHs - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
5.78
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11/05/12
HB002SG-000015-20121006Client ID:10/06/12 15:05Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-27Lab ID:
Field Prep: Not SpecifiedMatrix: Sediment Extraction Method:
Cleanup Method1:Analytical Method:Analytical Date:Analyst:
1,8270D-SIM(M)10/18/12 08:59MT
ALPHA OP-013
EPA 3611BExtraction Date: 10/12/12 14:50
Cleanup Date1: 10/16/12 34%Percent Solids:
MDL
2.90
2.90
2.90
2.90
2.90
3.32
3.32
3.32
3.32
3.32
2.98
3.64
3.62
3.62
3.62
3.62
3.62
2.75
2.20
2.04
1.89
3.08
3.08
3.08
3.08
3.19
3.19
3.19
3.19
3.19
3.19
Serial_No:11051209:46
Page 82 of 279
C3-Dibenzothiophenes
C4-Dibenzothiophenes
Phenanthrene
2-Methylphenanthrene
2-Methylanthracene
9,4-Methylphenanthrene
C1-Phenanthrenes/anthracenes
C2-Phenanthrenes/anthracenes
C3-Phenanthrenes/anthracenes
C4-Phenanthrenes/anthracenes
Retene
Anthracene
Carbazole
1-Methylphenanthrene
Fluoranthene
Pyrene
C1-Pyrene/fluoranthenes
Benzonaphthothiophene
Benz(a)anthracene
Chrysene
C1-Benzanthracene/chrysenes
C2-Benzanthracene/chrysenes
C3-Benzanthracene/chrysenes
C4-Benzanthracene/chrysenes
Benzo(b)fluoranthene
Benzo(j)+(k)fluoranthene
Benzo(e)pyrene
Benzo(a)pyrene
Perylene
Indeno(1,2,3-cd)pyrene
Dibenz(a,h)+(a,c)anthracene
Benzo(g,h,i)perylene
Parameter Result Dilution Factor
45.4
36.6
130
21.2
12.6
26.3
111
139
89.1
68.4
ND
71.6
18.6
25.2
475
571
289
87.5
232
313
188
137
149
150
447
372
336
370
124
358
89.8
349
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
PAHs - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
11.6
Naphthalene-d8
Phenanthrene-d10
Benzo(a)pyrene-d12
65
93
87
50-130
50-130
50-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
HB002SG-000015-20121006Client ID:10/06/12 15:05Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-27Lab ID:
Field Prep: Not Specified
MDL
3.19
3.19
3.83
3.83
3.83
3.83
3.83
3.83
3.83
3.83
2.83
2.38
3.78
3.05
3.67
3.04
3.04
3.23
2.36
2.34
2.34
2.34
2.34
2.34
3.00
2.29
2.38
3.30
2.23
3.14
3.12
3.07
Serial_No:11051209:46
Page 83 of 279
cis/trans-Decalin
C1-Decalin
C2-Decalin
C3-Decalin
C4-Decalin
Naphthalene
C1-Naphthalenes
C2-Naphthalenes
C3-Naphthalenes
C4-Naphthalenes
2-Methylnaphthalene
1-Methylnaphthalene
Benzothiophene
C1-Benzo(b)thiophene
C2-Benzo(b)thiophene
C3-Benzo(b)thiophene
C4-Benzo(b)thiophene
2,6-Dimethylnaphthalene
Acenaphthylene
Acenaphthene
2,3,5-Trimethylnaphthalene
Fluorene
C1-Fluorenes
C2-Fluorenes
C3-Fluorenes
Dibenzothiophene
4-Methyldibenzothiophene
2,3-Methyldibenzothiophene
1-Methyldibenzothiophene
C1-Dibenzothiophenes
C2-Dibenzothiophenes
Parameter Result
J
J
J
G
J
Dilution Factor
26.7
10.2
29.6
32.5
52.5
37.9
29.7
83.5
32.5
28.0
30.7
15.3
ND
ND
10.1
18.7
ND
105
60.6
16.6
4.42
27.8
19.4
41.3
112
17.3
9.69
40.0
ND
57.2
40.6
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
PAHs - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
6.24
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
11/05/12
HB001SG-000015-20121006Client ID:10/06/12 15:54Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-29Lab ID:
Field Prep: Not SpecifiedMatrix: Sediment Extraction Method:
Cleanup Method1:Analytical Method:Analytical Date:Analyst:
1,8270D-SIM(M)10/18/12 10:26MT
ALPHA OP-013
EPA 3611BExtraction Date: 10/12/12 14:50
Cleanup Date1: 10/16/12 30%Percent Solids:
MDL
3.14
3.14
3.14
3.14
3.14
3.59
3.59
3.59
3.59
3.59
3.22
3.94
3.91
3.91
3.91
3.91
3.91
2.97
2.38
2.20
2.04
3.33
3.33
3.33
3.33
3.44
3.44
3.44
3.44
3.44
3.44
Serial_No:11051209:46
Page 84 of 279
C3-Dibenzothiophenes
C4-Dibenzothiophenes
Phenanthrene
2-Methylphenanthrene
2-Methylanthracene
9,4-Methylphenanthrene
C1-Phenanthrenes/anthracenes
C2-Phenanthrenes/anthracenes
C3-Phenanthrenes/anthracenes
C4-Phenanthrenes/anthracenes
Retene
Anthracene
Carbazole
1-Methylphenanthrene
Fluoranthene
Pyrene
C1-Pyrene/fluoranthenes
Benzonaphthothiophene
Benz(a)anthracene
Chrysene
C1-Benzanthracene/chrysenes
C2-Benzanthracene/chrysenes
C3-Benzanthracene/chrysenes
C4-Benzanthracene/chrysenes
Benzo(b)fluoranthene
Benzo(j)+(k)fluoranthene
Benzo(e)pyrene
Benzo(a)pyrene
Perylene
Indeno(1,2,3-cd)pyrene
Dibenz(a,h)+(a,c)anthracene
Benzo(g,h,i)perylene
Parameter Result Dilution Factor
52.7
43.7
160
27.8
15.6
32.5
137
167
112
70.0
27.0
98.8
22.7
31.8
622
692
374
108
292
389
223
156
179
199
548
472
417
458
153
435
114
430
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
PAHs - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
12.5
Naphthalene-d8
Phenanthrene-d10
Benzo(a)pyrene-d12
71
97
93
50-130
50-130
50-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
HB001SG-000015-20121006Client ID:10/06/12 15:54Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-29Lab ID:
Field Prep: Not Specified
MDL
3.44
3.44
4.14
4.14
4.14
4.14
4.14
4.14
4.14
4.14
3.06
2.57
4.08
3.30
3.97
3.28
3.28
3.49
2.55
2.52
2.52
2.52
2.52
2.52
3.25
2.48
2.58
3.56
2.41
3.39
3.37
3.32
Serial_No:11051209:46
Page 85 of 279
Method Blank AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
10/12/12 18:291,8270D-SIM(M)Analytical Method:
Analytical Date:Extraction Method: EPA 3510CExtraction Date: 10/10/12 07:35
11/05/12
Analyst: MT
cis/trans-Decalin
C1-Decalin
C2-Decalin
C3-Decalin
C4-Decalin
Naphthalene
C1-Naphthalenes
C2-Naphthalenes
C3-Naphthalenes
C4-Naphthalenes
2-Methylnaphthalene
1-Methylnaphthalene
Benzothiophene
C1-Benzo(b)thiophene
C2-Benzo(b)thiophene
C3-Benzo(b)thiophene
C4-Benzo(b)thiophene
2,6-Dimethylnaphthalene
Acenaphthylene
Acenaphthene
2,3,5-Trimethylnaphthalene
Fluorene
C1-Fluorenes
C2-Fluorenes
C3-Fluorenes
Dibenzothiophene
4-Methyldibenzothiophene
2,3-Methyldibenzothiophene
1-Methyldibenzothiophene
C1-Dibenzothiophenes
C2-Dibenzothiophenes
Parameter Result
2.30
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
RL
5.00
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
J ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
UnitsQualifier
PAHs - Mansfield Lab for sample(s): 11 Batch: WG566066-1
MDL
2.16
2.16
2.16
2.16
2.16
2.35
2.35
2.35
2.35
2.35
1.33
1.62
2.48
2.48
2.48
2.48
2.48
2.80
2.10
1.34
1.90
2.18
2.18
2.18
2.18
1.42
1.42
1.42
1.42
1.42
1.42
Serial_No:11051209:46
Page 86 of 279
Method Blank AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
10/12/12 18:291,8270D-SIM(M)Analytical Method:
Analytical Date:Extraction Method: EPA 3510CExtraction Date: 10/10/12 07:35
11/05/12
Analyst: MT
C3-Dibenzothiophenes
C4-Dibenzothiophenes
Phenanthrene
2-Methylphenanthrene
2-Methylanthracene
9,4-Methylphenanthrene
C1-Phenanthrenes/anthracenes
C2-Phenanthrenes/anthracenes
C3-Phenanthrenes/anthracenes
C4-Phenanthrenes/anthracenes
Retene
Anthracene
Carbazole
1-Methylphenanthrene
Fluoranthene
Pyrene
C1-Pyrene/fluoranthenes
Benzonaphthothiophene
Benz(a)anthracene
Chrysene
C1-Benzanthracene/chrysenes
C2-Benzanthracene/chrysenes
C3-Benzanthracene/chrysenes
C4-Benzanthracene/chrysenes
Benzo(b)fluoranthene
Benzo(j)+(k)fluoranthene
Benzo(e)pyrene
Benzo(a)pyrene
Perylene
Indeno(1,2,3-cd)pyrene
Dibenz(a,h)+(a,c)anthracene
Parameter Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
RL
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
ng/l
UnitsQualifier
PAHs - Mansfield Lab for sample(s): 11 Batch: WG566066-1
MDL
1.42
1.42
2.38
2.38
2.38
2.38
2.38
2.38
2.38
2.38
2.26
1.87
4.58
3.47
2.62
0.900
0.900
1.18
2.65
1.62
1.62
1.62
1.62
1.62
1.12
2.56
1.64
4.25
2.91
1.81
2.18
Serial_No:11051209:46
Page 87 of 279
Method Blank AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
10/12/12 18:291,8270D-SIM(M)Analytical Method:
Analytical Date:Extraction Method: EPA 3510CExtraction Date: 10/10/12 07:35
11/05/12
Analyst: MT
Benzo(g,h,i)perylene
Parameter Result
ND
RL
10.0ng/l
UnitsQualifier
PAHs - Mansfield Lab for sample(s): 11 Batch: WG566066-1
Naphthalene-d8
Phenanthrene-d10
Benzo(a)pyrene-d12
94
89
94
50-130
50-130
50-130
Surrogate %Recovery QualifierAcceptance
Criteria
MDL
1.64
Serial_No:11051209:46
Page 88 of 279
Method Blank AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
10/17/12 08:061,8270D-SIM(M)Analytical Method:
Analytical Date:Extraction Method:
Cleanup Method1:
ALPHA OP-013
EPA 3611BExtraction Date: 10/12/12 12:37
11/05/12
Analyst: MT
cis/trans-Decalin
C1-Decalin
C2-Decalin
C3-Decalin
C4-Decalin
Naphthalene
C1-Naphthalenes
C2-Naphthalenes
C3-Naphthalenes
C4-Naphthalenes
2-Methylnaphthalene
1-Methylnaphthalene
Benzothiophene
C1-Benzo(b)thiophene
C2-Benzo(b)thiophene
C3-Benzo(b)thiophene
C4-Benzo(b)thiophene
2,6-Dimethylnaphthalene
Acenaphthylene
Acenaphthene
2,3,5-Trimethylnaphthalene
Fluorene
C1-Fluorenes
C2-Fluorenes
C3-Fluorenes
Dibenzothiophene
4-Methyldibenzothiophene
2,3-Methyldibenzothiophene
1-Methyldibenzothiophene
C1-Dibenzothiophenes
Parameter Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
RL
0.500
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
UnitsQualifier
PAHs - Mansfield Lab for sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG566754-1
Cleanup Date1: 10/16/12
MDL
0.251
0.251
0.251
0.251
0.251
0.287
0.287
0.287
0.287
0.287
0.258
0.315
0.313
0.313
0.313
0.313
0.313
0.238
0.191
0.176
0.164
0.267
0.267
0.267
0.267
0.276
0.276
0.276
0.276
0.276
Serial_No:11051209:46
Page 89 of 279
Method Blank AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
10/17/12 08:061,8270D-SIM(M)Analytical Method:
Analytical Date:Extraction Method:
Cleanup Method1:
ALPHA OP-013
EPA 3611BExtraction Date: 10/12/12 12:37
11/05/12
Analyst: MT
C2-Dibenzothiophenes
C3-Dibenzothiophenes
C4-Dibenzothiophenes
Phenanthrene
2-Methylphenanthrene
2-Methylanthracene
9,4-Methylphenanthrene
C1-Phenanthrenes/anthracenes
C2-Phenanthrenes/anthracenes
C3-Phenanthrenes/anthracenes
C4-Phenanthrenes/anthracenes
Retene
Anthracene
Carbazole
1-Methylphenanthrene
Fluoranthene
Pyrene
C1-Pyrene/fluoranthenes
Benzonaphthothiophene
Benz(a)anthracene
Chrysene
C1-Benzanthracene/chrysenes
C2-Benzanthracene/chrysenes
C3-Benzanthracene/chrysenes
C4-Benzanthracene/chrysenes
Benzo(b)fluoranthene
Benzo(j)+(k)fluoranthene
Benzo(e)pyrene
Benzo(a)pyrene
Perylene
Parameter Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
RL
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
UnitsQualifier
PAHs - Mansfield Lab for sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG566754-1
Cleanup Date1: 10/16/12
MDL
0.276
0.276
0.276
0.331
0.331
0.331
0.331
0.331
0.331
0.331
0.331
0.245
0.206
0.327
0.264
0.318
0.263
0.263
0.280
0.204
0.202
0.202
0.202
0.202
0.202
0.260
0.198
0.206
0.285
0.193
Serial_No:11051209:46
Page 90 of 279
Method Blank AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
10/17/12 08:061,8270D-SIM(M)Analytical Method:
Analytical Date:Extraction Method:
Cleanup Method1:
ALPHA OP-013
EPA 3611BExtraction Date: 10/12/12 12:37
11/05/12
Analyst: MT
Indeno(1,2,3-cd)pyrene
Dibenz(a,h)+(a,c)anthracene
Benzo(g,h,i)perylene
Parameter Result
ND
ND
ND
RL
1.00
1.00
1.00
ug/kg
ug/kg
ug/kg
UnitsQualifier
PAHs - Mansfield Lab for sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG566754-1
Naphthalene-d8
Phenanthrene-d10
Benzo(a)pyrene-d12
79
94
80
50-130
50-130
50-130
Surrogate %Recovery QualifierAcceptance
Criteria
Cleanup Date1: 10/16/12
MDL
0.271
0.270
0.266
Serial_No:11051209:46
Page 91 of 279
Naphthalene
2-Methylnaphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benz(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(j)+(k)Fluoranthene
Benzo(a)pyrene
Indeno(1,2,3-cd)Pyrene
Dibenz(a,h)+(a,c)anthracene
Benzo(ghi)perylene
93
104
97
100
92
95
112
113
118
96
99
94
103
106
104
108
98
90
98
97
101
95
95
112
123
129
96
99
95
103
106
98
100
91
50-130
50-130
50-130
50-130
50-130
50-130
50-130
50-130
50-130
50-130
50-130
50-130
50-130
50-130
50-130
50-130
50-130
3
6
0
1
3
0
0
8
9
0
0
1
0
0
6
8
7
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
ParameterLCS
%RecoveryLCSD
%Recovery%Recovery
Limits RPD RPD Limits
PAHs - Mansfield Lab Associated sample(s): 11 Batch: WG566066-2 WG566066-3
Lab Control Sample AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
Qual Qual Qual
Serial_No:11051209:46
Page 92 of 279
Naphthalene
2-Methylnaphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
84
83
74
86
90
93
86
92
95
90
89
82
91
90
97
91
96
100
50-130
50-130
50-130
50-130
50-130
50-130
50-130
50-130
50-130
7
7
10
6
0
4
6
4
5
30
30
30
30
30
30
30
30
30
ParameterLCS
%RecoveryLCSD
%Recovery%Recovery
Limits RPD RPD Limits
PAHs - Mansfield Lab Associated sample(s): 11 Batch: WG566066-2 WG566066-3
PAHs - Mansfield Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG566754-2 WG566754-3
Lab Control Sample AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
Naphthalene-d8
Phenanthrene-d10
Benzo(a)pyrene-d12
89
90
91
50-130
50-130
50-130
85
90
91
Surrogate Qual%Recovery Qual%RecoveryLCS LCSD
11/05/12
AcceptanceCriteria
Qual Qual Qual
Serial_No:11051209:46
Page 93 of 279
Benz(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(j)+(k)Fluoranthene
Benzo(a)pyrene
Indeno(1,2,3-cd)Pyrene
Dibenz(a,h)+(a,c)anthracene
Benzo(ghi)perylene
69
85
73
86
68
58
52
60
79
90
85
101
86
71
69
74
50-130
50-130
50-130
50-130
50-130
50-130
50-130
50-130
14
6
15
16
23
20
28
21
30
30
30
30
30
30
30
30
ParameterLCS
%RecoveryLCSD
%Recovery%Recovery
Limits RPD RPD Limits
PAHs - Mansfield Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG566754-2 WG566754-3
Lab Control Sample AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
Naphthalene-d8
Phenanthrene-d10
Benzo(a)pyrene-d12
77
94
64
50-130
50-130
50-130
89
98
79
Surrogate Qual%Recovery Qual%RecoveryLCS LCSD
11/05/12
AcceptanceCriteria
Qual Qual Qual
Serial_No:11051209:46
Page 94 of 279
S.R.M. Standard Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
Parameter
11/05/12
% Recovery QC CriteriaPhenanthrene
Fluoranthene
Pyrene
Benz(a)anthracene
Chrysene/Triphenylene
Benzo(b)fluoranthene
Benzo(j)+(k)Fluoranthene
Benzo(e)Pyrene
Benzo(a)pyrene
Perylene
Indeno(1,2,3-cd)Pyrene
Dibenz(a,h)+(a,c)anthracene
Benzo(ghi)perylene
Naphthalene-d8 (Surrogate)
Phenanthrene-d10 (Surrogate)
Benzo(a)pyrene-d12 (Surrogate)
98
91
88
81
89
81
86
93
87
79
101
116
106
73
96
87
67-135
67-135
67-136
68-133
66-138
62-144
60-149
68-134
68-134
56-157
67-135
62-144
68-135
50-130
50-130
50-130
Standard Reference Material (SRM): WG566754-4
Qual
Serial_No:11051209:46
Page 95 of 279
PETROLEUM HYDROCARBONS
Serial_No:11051209:46
Page 96 of 279
FF
n-Nonane (C9)
n-Decane (C10)
n-Undecane (C11)
n-Dodecane (C12)
n-Tridecane (C13)
2,6,10-Trimethyldodecane (1380)
n-Tetradecane (C14)
2,6,10-Trimethyltridecane (1470)
n-Pentadecane (C15)
n-Hexadecane (C16)
Norpristane (1650)
n-Heptadecane (C17)
Pristane
n-Octadecane (C18)
Phytane
n-Nonadecane (C19)
n-Eicosane (C20)
n-Heneicosane (C21)
n-Docosane (C22)
n-Tricosane (C23)
n-Tetracosane (C24)
n-Pentacosane (C25)
n-Hexacosane (C26)
n-Heptacosane (C27)
n-Octacosane (C28)
n-Nonacosane (C29)
n-Triacontane (C30)
n-Hentriacontane (C31)
n-Dotriacontane (C32)
n-Tritriacontane (C33)
n-Tetratriacontane (C34)
Parameter Result
JG
G
JG
J
G
J
C
J
J
J
J
J
Dilution Factor
ND
ND
ND
ND
ND
ND
ND
0.211
ND
ND
ND
ND
ND
0.351
0.155
ND
ND
ND
ND
0.326
ND
0.734
ND
0.197
ND
0.798
0.071
0.242
0.064
0.296
0.113
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Saturated Hydrocarbons by GC-FID - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
0.346
0.346
0.346
0.346
0.346
0.346
0.346
0.346
0.346
0.346
0.346
0.346
0.346
0.346
0.346
0.346
0.346
0.346
0.346
0.346
0.346
0.346
0.346
0.346
0.346
0.346
0.346
0.346
0.346
0.346
0.346
11/05/12
TN005SG-000014-20121005Client ID:10/05/12 09:32Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-01Lab ID:
Field Prep: Not SpecifiedMatrix: Sediment Extraction Method:
Cleanup Method1:Analytical Method:Analytical Date:Analyst:
1,8015D(M)10/20/12 00:35DP
ALPHA OP-013
EPA 3611BExtraction Date: 10/12/12 12:37
Cleanup Date1: 10/16/12 72%Percent Solids:
MDL
0.102
0.110
0.103
0.075
0.095
0.052
0.052
0.041
0.041
0.052
0.114
0.114
0.074
0.069
0.043
0.089
0.049
0.041
0.036
0.044
0.058
0.183
0.051
0.042
0.074
0.230
0.040
0.049
0.044
0.049
0.055
Serial_No:11051209:46
Page 97 of 279
n-Pentatriacontane (C35)
n-Hexatriacontane (C36)
n-Heptatriacontane (C37)
n-Octatriacontane (C38)
n-Nonatriacontane (C39)
n-Tetracontane (C40)
Total Petroleum Hydrocarbons (C9-C40)
DRO (C10-C28)
Parameter Result
J
Dilution Factor
ND
ND
ND
0.088
ND
ND
245
132
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
1
1
1
1
1
1
1
1
Qualifier Units RL
Saturated Hydrocarbons by GC-FID - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
0.346
0.346
0.346
0.346
0.346
0.346
11.4
7.26
ortho-terphenyl
d50-Tetracosane
92
91
50-130
50-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
TN005SG-000014-20121005Client ID:10/05/12 09:32Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-01Lab ID:
Field Prep: Not Specified
MDL
0.060
0.069
0.077
0.081
0.112
0.112
2.51
1.50
Serial_No:11051209:46
Page 98 of 279
n-Nonane (C9)
n-Decane (C10)
n-Undecane (C11)
n-Dodecane (C12)
n-Tridecane (C13)
2,6,10-Trimethyldodecane (1380)
n-Tetradecane (C14)
2,6,10-Trimethyltridecane (1470)
n-Pentadecane (C15)
n-Hexadecane (C16)
Norpristane (1650)
n-Heptadecane (C17)
Pristane
n-Octadecane (C18)
Phytane
n-Nonadecane (C19)
n-Eicosane (C20)
n-Heneicosane (C21)
n-Docosane (C22)
n-Tricosane (C23)
n-Tetracosane (C24)
n-Pentacosane (C25)
n-Hexacosane (C26)
n-Heptacosane (C27)
n-Octacosane (C28)
n-Nonacosane (C29)
n-Triacontane (C30)
n-Hentriacontane (C31)
n-Dotriacontane (C32)
n-Tritriacontane (C33)
n-Tetratriacontane (C34)
Parameter Result
J
G
J
J
J
J
G
G
G
J
C
J
Dilution Factor
ND
ND
ND
ND
ND
ND
0.048
0.678
0.040
0.121
ND
0.231
0.118
0.735
0.531
ND
ND
ND
ND
0.868
ND
2.37
0.269
0.649
ND
0.769
ND
0.674
0.138
0.357
0.460
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Saturated Hydrocarbons by GC-FID - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
0.298
0.298
0.298
0.298
0.298
0.298
0.298
0.298
0.298
0.298
0.298
0.298
0.298
0.298
0.298
0.298
0.298
0.298
0.298
0.298
0.298
0.298
0.298
0.298
0.298
0.298
0.298
0.298
0.298
0.298
0.298
11/05/12
TN002SG-000011-20121005Client ID:10/05/12 10:41Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-03Lab ID:
Field Prep: Not SpecifiedMatrix: Sediment Extraction Method:
Cleanup Method1:Analytical Method:Analytical Date:Analyst:
1,8015D(M)10/20/12 02:06DP
ALPHA OP-013
EPA 3611BExtraction Date: 10/12/12 12:37
Cleanup Date1: 10/16/12 55%Percent Solids:
MDL
0.088
0.095
0.089
0.065
0.082
0.045
0.045
0.036
0.036
0.045
0.098
0.098
0.064
0.060
0.037
0.077
0.042
0.036
0.031
0.038
0.050
0.158
0.044
0.036
0.064
0.198
0.034
0.042
0.038
0.042
0.047
Serial_No:11051209:46
Page 99 of 279
n-Pentatriacontane (C35)
n-Hexatriacontane (C36)
n-Heptatriacontane (C37)
n-Octatriacontane (C38)
n-Nonatriacontane (C39)
n-Tetracontane (C40)
Total Petroleum Hydrocarbons (C9-C40)
DRO (C10-C28)
Parameter Result
J
J
Dilution Factor
0.150
ND
ND
0.264
ND
ND
675
354
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
1
1
1
1
1
1
1
1
Qualifier Units RL
Saturated Hydrocarbons by GC-FID - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
0.298
0.298
0.298
0.298
0.298
0.298
9.83
6.26
ortho-terphenyl
d50-Tetracosane
90
89
50-130
50-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
TN002SG-000011-20121005Client ID:10/05/12 10:41Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-03Lab ID:
Field Prep: Not Specified
MDL
0.052
0.059
0.066
0.069
0.097
0.097
2.16
1.29
Serial_No:11051209:46
Page 100 of 279
n-Nonane (C9)
n-Decane (C10)
n-Undecane (C11)
n-Dodecane (C12)
n-Tridecane (C13)
2,6,10-Trimethyldodecane (1380)
n-Tetradecane (C14)
2,6,10-Trimethyltridecane (1470)
n-Pentadecane (C15)
n-Hexadecane (C16)
Norpristane (1650)
n-Heptadecane (C17)
Pristane
n-Octadecane (C18)
Phytane
n-Nonadecane (C19)
n-Eicosane (C20)
n-Heneicosane (C21)
n-Docosane (C22)
n-Tricosane (C23)
n-Tetracosane (C24)
n-Pentacosane (C25)
n-Hexacosane (C26)
n-Heptacosane (C27)
n-Octacosane (C28)
n-Nonacosane (C29)
n-Triacontane (C30)
n-Hentriacontane (C31)
n-Dotriacontane (C32)
n-Tritriacontane (C33)
n-Tetratriacontane (C34)
Parameter Result
G
J
J
J
J
G
G
J
G
J
C
J
J
Dilution Factor
ND
ND
ND
ND
ND
ND
ND
1.20
0.096
0.189
ND
0.409
0.217
1.24
0.906
0.146
ND
ND
ND
1.10
ND
3.73
0.462
1.16
ND
1.41
0.316
1.30
0.292
0.789
0.756
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Saturated Hydrocarbons by GC-FID - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
0.570
0.570
0.570
0.570
0.570
0.570
0.570
0.570
0.570
0.570
0.570
0.570
0.570
0.570
0.570
0.570
0.570
0.570
0.570
0.570
0.570
0.570
0.570
0.570
0.570
0.570
0.570
0.570
0.570
0.570
0.570
11/05/12
TN003SG-000015-20121005Client ID:10/05/12 11:24Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-05Lab ID:
Field Prep: Not SpecifiedMatrix: Sediment Extraction Method:
Cleanup Method1:Analytical Method:Analytical Date:Analyst:
1,8015D(M)10/20/12 03:36DP
ALPHA OP-013
EPA 3611BExtraction Date: 10/12/12 12:37
Cleanup Date1: 10/16/12 41%Percent Solids:
MDL
0.169
0.182
0.170
0.124
0.156
0.086
0.086
0.068
0.068
0.086
0.188
0.188
0.122
0.114
0.072
0.146
0.081
0.068
0.060
0.073
0.095
0.302
0.084
0.069
0.122
0.380
0.065
0.081
0.072
0.080
0.091
Serial_No:11051209:46
Page 101 of 279
n-Pentatriacontane (C35)
n-Hexatriacontane (C36)
n-Heptatriacontane (C37)
n-Octatriacontane (C38)
n-Nonatriacontane (C39)
n-Tetracontane (C40)
Total Petroleum Hydrocarbons (C9-C40)
DRO (C10-C28)
Parameter Result
J
J
J
J
J
Dilution Factor
0.259
0.359
0.127
0.516
0.246
ND
1260
645
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
1
1
1
1
1
1
1
1
Qualifier Units RL
Saturated Hydrocarbons by GC-FID - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
0.570
0.570
0.570
0.570
0.570
0.570
18.8
12.0
ortho-terphenyl
d50-Tetracosane
88
87
50-130
50-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
TN003SG-000015-20121005Client ID:10/05/12 11:24Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-05Lab ID:
Field Prep: Not Specified
MDL
0.100
0.113
0.127
0.133
0.185
0.185
4.14
2.47
Serial_No:11051209:46
Page 102 of 279
n-Nonane (C9)
n-Decane (C10)
n-Undecane (C11)
n-Dodecane (C12)
n-Tridecane (C13)
2,6,10-Trimethyldodecane (1380)
n-Tetradecane (C14)
2,6,10-Trimethyltridecane (1470)
n-Pentadecane (C15)
n-Hexadecane (C16)
Norpristane (1650)
n-Heptadecane (C17)
Pristane
n-Octadecane (C18)
Phytane
n-Nonadecane (C19)
n-Eicosane (C20)
n-Heneicosane (C21)
n-Docosane (C22)
n-Tricosane (C23)
n-Tetracosane (C24)
n-Pentacosane (C25)
n-Hexacosane (C26)
n-Heptacosane (C27)
n-Octacosane (C28)
n-Nonacosane (C29)
n-Triacontane (C30)
n-Hentriacontane (C31)
n-Dotriacontane (C32)
n-Tritriacontane (C33)
n-Tetratriacontane (C34)
Parameter Result
JG
J
J
G
JG
J
G
J
C
J
J
J
Dilution Factor
ND
ND
ND
ND
ND
ND
ND
0.264
ND
0.061
ND
0.136
ND
0.554
0.283
ND
ND
ND
ND
0.312
ND
1.38
0.173
0.702
ND
1.15
0.142
0.518
0.096
0.564
0.273
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Saturated Hydrocarbons by GC-FID - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
0.377
0.377
0.377
0.377
0.377
0.377
0.377
0.377
0.377
0.377
0.377
0.377
0.377
0.377
0.377
0.377
0.377
0.377
0.377
0.377
0.377
0.377
0.377
0.377
0.377
0.377
0.377
0.377
0.377
0.377
0.377
11/05/12
TN004SG-000015-20121005Client ID:10/05/12 11:46Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-07Lab ID:
Field Prep: Not SpecifiedMatrix: Sediment Extraction Method:
Cleanup Method1:Analytical Method:Analytical Date:Analyst:
1,8015D(M)10/20/12 05:07DP
ALPHA OP-013
EPA 3611BExtraction Date: 10/12/12 12:37
Cleanup Date1: 10/16/12 51%Percent Solids:
MDL
0.112
0.120
0.112
0.082
0.103
0.057
0.057
0.045
0.045
0.057
0.124
0.124
0.081
0.076
0.047
0.097
0.053
0.045
0.039
0.048
0.063
0.199
0.055
0.045
0.081
0.251
0.043
0.053
0.048
0.053
0.060
Serial_No:11051209:46
Page 103 of 279
n-Pentatriacontane (C35)
n-Hexatriacontane (C36)
n-Heptatriacontane (C37)
n-Octatriacontane (C38)
n-Nonatriacontane (C39)
n-Tetracontane (C40)
Total Petroleum Hydrocarbons (C9-C40)
DRO (C10-C28)
Parameter Result
J
Dilution Factor
0.083
ND
ND
ND
ND
ND
383
178
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
1
1
1
1
1
1
1
1
Qualifier Units RL
Saturated Hydrocarbons by GC-FID - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
0.377
0.377
0.377
0.377
0.377
0.377
12.4
7.91
ortho-terphenyl
d50-Tetracosane
88
86
50-130
50-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
TN004SG-000015-20121005Client ID:10/05/12 11:46Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-07Lab ID:
Field Prep: Not Specified
MDL
0.066
0.075
0.084
0.088
0.122
0.122
2.74
1.63
Serial_No:11051209:46
Page 104 of 279
n-Nonane (C9)
n-Decane (C10)
n-Undecane (C11)
n-Dodecane (C12)
n-Tridecane (C13)
2,6,10-Trimethyldodecane (1380)
n-Tetradecane (C14)
2,6,10-Trimethyltridecane (1470)
n-Pentadecane (C15)
n-Hexadecane (C16)
Norpristane (1650)
n-Heptadecane (C17)
Pristane
n-Octadecane (C18)
Phytane
n-Nonadecane (C19)
n-Eicosane (C20)
n-Heneicosane (C21)
n-Docosane (C22)
n-Tricosane (C23)
n-Tetracosane (C24)
n-Pentacosane (C25)
n-Hexacosane (C26)
n-Heptacosane (C27)
n-Octacosane (C28)
n-Nonacosane (C29)
n-Triacontane (C30)
n-Hentriacontane (C31)
n-Dotriacontane (C32)
n-Tritriacontane (C33)
n-Tetratriacontane (C34)
Parameter Result
JG
G
JG
J
G
J
J
C
J
J
J
J
J
Dilution Factor
ND
ND
ND
ND
ND
ND
ND
0.105
ND
ND
ND
ND
ND
0.511
0.137
ND
ND
ND
ND
0.111
ND
0.730
0.068
0.121
ND
0.620
0.052
0.157
0.038
0.255
0.075
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Saturated Hydrocarbons by GC-FID - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
0.281
0.281
0.281
0.281
0.281
0.281
0.281
0.281
0.281
0.281
0.281
0.281
0.281
0.281
0.281
0.281
0.281
0.281
0.281
0.281
0.281
0.281
0.281
0.281
0.281
0.281
0.281
0.281
0.281
0.281
0.281
11/05/12
TN006SG-000015-20121005Client ID:10/05/12 13:16Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-09Lab ID:
Field Prep: Not SpecifiedMatrix: Sediment Extraction Method:
Cleanup Method1:Analytical Method:Analytical Date:Analyst:
1,8015D(M)10/20/12 06:37DP
ALPHA OP-013
EPA 3611BExtraction Date: 10/12/12 12:37
Cleanup Date1: 10/16/12 78%Percent Solids:
MDL
0.083
0.090
0.084
0.061
0.077
0.042
0.042
0.034
0.034
0.042
0.093
0.093
0.060
0.056
0.035
0.072
0.040
0.034
0.029
0.036
0.047
0.149
0.041
0.034
0.060
0.187
0.032
0.040
0.035
0.040
0.045
Serial_No:11051209:46
Page 105 of 279
n-Pentatriacontane (C35)
n-Hexatriacontane (C36)
n-Heptatriacontane (C37)
n-Octatriacontane (C38)
n-Nonatriacontane (C39)
n-Tetracontane (C40)
Total Petroleum Hydrocarbons (C9-C40)
DRO (C10-C28)
Parameter Result Dilution Factor
ND
ND
ND
ND
ND
ND
165
71.3
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
1
1
1
1
1
1
1
1
Qualifier Units RL
Saturated Hydrocarbons by GC-FID - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
0.281
0.281
0.281
0.281
0.281
0.281
9.28
5.91
ortho-terphenyl
d50-Tetracosane
94
93
50-130
50-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
TN006SG-000015-20121005Client ID:10/05/12 13:16Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-09Lab ID:
Field Prep: Not Specified
MDL
0.049
0.056
0.063
0.066
0.091
0.091
2.04
1.22
Serial_No:11051209:46
Page 106 of 279
n-Nonane (C9)
n-Decane (C10)
n-Undecane (C11)
n-Dodecane (C12)
n-Tridecane (C13)
2,6,10-Trimethyldodecane (1380)
n-Tetradecane (C14)
2,6,10-Trimethyltridecane (1470)
n-Pentadecane (C15)
n-Hexadecane (C16)
Norpristane (1650)
n-Heptadecane (C17)
Pristane
n-Octadecane (C18)
Phytane
n-Nonadecane (C19)
n-Eicosane (C20)
n-Heneicosane (C21)
n-Docosane (C22)
n-Tricosane (C23)
n-Tetracosane (C24)
n-Pentacosane (C25)
n-Hexacosane (C26)
n-Heptacosane (C27)
n-Octacosane (C28)
n-Nonacosane (C29)
n-Triacontane (C30)
n-Hentriacontane (C31)
n-Dotriacontane (C32)
n-Tritriacontane (C33)
n-Tetratriacontane (C34)
Parameter Result
JC
Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.001
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Saturated Hydrocarbons by GC-FID - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
0.001
0.001
0.001
0.001
0.006
0.001
0.001
0.001
0.001
0.001
0.001
0.001
0.001
0.001
0.001
0.001
0.001
0.001
0.001
0.001
0.001
0.006
0.001
0.001
0.001
0.001
0.001
0.001
0.001
0.001
0.001
11/05/12
SG-RB-20121006Client ID:10/06/12 09:05Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-11Lab ID:
Field Prep: Not SpecifiedMatrix: Water Extraction Method:Analytical Method:Analytical Date:Analyst:
1,8015D(M)10/12/12 23:51DP
EPA 3510CExtraction Date: 10/10/12 07:46
MDL
0.0004
0.0001
0.0001
0.0002
0.001
0.0001
0.0001
0.0002
0.0002
0.0002
0.0002
0.0002
0.0002
0.0001
0.0001
0.0002
0.0001
0.0001
0.00005
0.0001
0.0001
0.001
0.0001
0.0001
0.0002
0.0001
0.0001
0.0002
0.0001
0.0002
0.0002
Serial_No:11051209:46
Page 107 of 279
n-Pentatriacontane (C35)
n-Hexatriacontane (C36)
n-Heptatriacontane (C37)
n-Octatriacontane (C38)
n-Nonatriacontane (C39)
n-Tetracontane (C40)
Total Petroleum Hydrocarbons (C9-C40)
DRO (C10-C28)
Parameter Result
J
Dilution Factor
ND
ND
ND
ND
ND
ND
0.035
0.028
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
1
1
1
1
1
1
1
1
Qualifier Units RL
Saturated Hydrocarbons by GC-FID - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
0.001
0.001
0.001
0.001
0.001
0.001
0.038
0.024
ortho-terphenyl
d50-Tetracosane
91
87
50-130
50-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
SG-RB-20121006Client ID:10/06/12 09:05Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-11Lab ID:
Field Prep: Not Specified
MDL
0.0002
0.0002
0.0002
0.0002
0.0002
0.0002
0.006
0.004
Serial_No:11051209:46
Page 108 of 279
n-Nonane (C9)
n-Decane (C10)
n-Undecane (C11)
n-Dodecane (C12)
n-Tridecane (C13)
2,6,10-Trimethyldodecane (1380)
n-Tetradecane (C14)
2,6,10-Trimethyltridecane (1470)
n-Pentadecane (C15)
n-Hexadecane (C16)
Norpristane (1650)
n-Heptadecane (C17)
Pristane
n-Octadecane (C18)
Phytane
n-Nonadecane (C19)
n-Eicosane (C20)
n-Heneicosane (C21)
n-Docosane (C22)
n-Tricosane (C23)
n-Tetracosane (C24)
n-Pentacosane (C25)
n-Hexacosane (C26)
n-Heptacosane (C27)
n-Octacosane (C28)
n-Nonacosane (C29)
n-Triacontane (C30)
n-Hentriacontane (C31)
n-Dotriacontane (C32)
n-Tritriacontane (C33)
n-Tetratriacontane (C34)
Parameter Result
JG
J
J
JG
JG
J
G
J
J
C
J
J
Dilution Factor
ND
ND
ND
ND
ND
ND
ND
0.287
0.251
ND
ND
0.960
ND
0.430
0.409
ND
ND
ND
ND
0.388
ND
3.97
0.747
4.20
0.514
5.34
0.784
4.85
0.592
4.50
5.20
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Saturated Hydrocarbons by GC-FID - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
0.974
0.974
0.974
0.974
0.974
0.974
0.974
0.974
0.974
0.974
0.974
0.974
0.974
0.974
0.974
0.974
0.974
0.974
0.974
0.974
0.974
0.974
0.974
0.974
0.974
0.974
0.974
0.974
0.974
0.974
0.974
11/05/12
HB008SG-000015-20121006Client ID:10/06/12 09:55Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-13Lab ID:
Field Prep: Not SpecifiedMatrix: Sediment Extraction Method:
Cleanup Method1:Analytical Method:Analytical Date:Analyst:
1,8015D(M)10/20/12 08:08DP
ALPHA OP-013
EPA 3611BExtraction Date: 10/12/12 12:37
Cleanup Date1: 10/16/12 27%Percent Solids:
MDL
0.289
0.311
0.291
0.212
0.267
0.146
0.146
0.116
0.116
0.147
0.321
0.321
0.208
0.195
0.122
0.250
0.138
0.116
0.102
0.124
0.163
0.516
0.143
0.117
0.209
0.649
0.112
0.138
0.123
0.137
0.155
Serial_No:11051209:46
Page 109 of 279
n-Pentatriacontane (C35)
n-Hexatriacontane (C36)
n-Heptatriacontane (C37)
n-Octatriacontane (C38)
n-Nonatriacontane (C39)
n-Tetracontane (C40)
Total Petroleum Hydrocarbons (C9-C40)
DRO (C10-C28)
Parameter Result
J
J
J
J
J
J
Dilution Factor
0.820
0.736
0.658
0.733
0.758
0.484
2390
1010
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
1
1
1
1
1
1
1
1
Qualifier Units RL
Saturated Hydrocarbons by GC-FID - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
0.974
0.974
0.974
0.974
0.974
0.974
32.1
20.4
ortho-terphenyl
d50-Tetracosane
94
90
50-130
50-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
HB008SG-000015-20121006Client ID:10/06/12 09:55Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-13Lab ID:
Field Prep: Not Specified
MDL
0.170
0.194
0.216
0.227
0.316
0.316
7.07
4.22
Serial_No:11051209:46
Page 110 of 279
n-Nonane (C9)
n-Decane (C10)
n-Undecane (C11)
n-Dodecane (C12)
n-Tridecane (C13)
2,6,10-Trimethyldodecane (1380)
n-Tetradecane (C14)
2,6,10-Trimethyltridecane (1470)
n-Pentadecane (C15)
n-Hexadecane (C16)
Norpristane (1650)
n-Heptadecane (C17)
Pristane
n-Octadecane (C18)
Phytane
n-Nonadecane (C19)
n-Eicosane (C20)
n-Heneicosane (C21)
n-Docosane (C22)
n-Tricosane (C23)
n-Tetracosane (C24)
n-Pentacosane (C25)
n-Hexacosane (C26)
n-Heptacosane (C27)
n-Octacosane (C28)
n-Nonacosane (C29)
n-Triacontane (C30)
n-Hentriacontane (C31)
n-Dotriacontane (C32)
n-Tritriacontane (C33)
n-Tetratriacontane (C34)
Parameter Result
JG
J
J
JG
JG
J
J
G
J
C
J
J
Dilution Factor
ND
ND
ND
ND
ND
ND
ND
0.382
0.153
ND
ND
1.22
0.298
0.563
0.622
0.358
ND
ND
ND
0.535
ND
4.26
1.21
5.41
0.586
8.05
1.11
6.90
0.893
6.18
6.72
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Saturated Hydrocarbons by GC-FID - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
1.16
1.16
1.16
1.16
1.16
1.16
1.16
1.16
1.16
1.16
1.16
1.16
1.16
1.16
1.16
1.16
1.16
1.16
1.16
1.16
1.16
1.16
1.16
1.16
1.16
1.16
1.16
1.16
1.16
1.16
1.16
11/05/12
HB007SG-000015-20121006Client ID:10/06/12 10:45Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-15Lab ID:
Field Prep: Not SpecifiedMatrix: Sediment Extraction Method:
Cleanup Method1:Analytical Method:Analytical Date:Analyst:
1,8015D(M)10/20/12 14:10DP
ALPHA OP-013
EPA 3611BExtraction Date: 10/12/12 12:37
Cleanup Date1: 10/16/12 25%Percent Solids:
MDL
0.344
0.370
0.347
0.253
0.319
0.175
0.175
0.138
0.138
0.175
0.383
0.383
0.248
0.233
0.146
0.298
0.164
0.139
0.121
0.148
0.194
0.615
0.171
0.140
0.249
0.774
0.133
0.164
0.146
0.163
0.185
Serial_No:11051209:46
Page 111 of 279
n-Pentatriacontane (C35)
n-Hexatriacontane (C36)
n-Heptatriacontane (C37)
n-Octatriacontane (C38)
n-Nonatriacontane (C39)
n-Tetracontane (C40)
Total Petroleum Hydrocarbons (C9-C40)
DRO (C10-C28)
Parameter Result
J
J
J
J
Dilution Factor
1.28
1.17
0.871
0.920
1.04
0.618
3210
1360
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
1
1
1
1
1
1
1
1
Qualifier Units RL
Saturated Hydrocarbons by GC-FID - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
1.16
1.16
1.16
1.16
1.16
1.16
38.3
24.4
ortho-terphenyl
d50-Tetracosane
95
90
50-130
50-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
HB007SG-000015-20121006Client ID:10/06/12 10:45Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-15Lab ID:
Field Prep: Not Specified
MDL
0.203
0.231
0.258
0.271
0.377
0.377
8.43
5.03
Serial_No:11051209:46
Page 112 of 279
n-Nonane (C9)
n-Decane (C10)
n-Undecane (C11)
n-Dodecane (C12)
n-Tridecane (C13)
2,6,10-Trimethyldodecane (1380)
n-Tetradecane (C14)
2,6,10-Trimethyltridecane (1470)
n-Pentadecane (C15)
n-Hexadecane (C16)
Norpristane (1650)
n-Heptadecane (C17)
Pristane
n-Octadecane (C18)
Phytane
n-Nonadecane (C19)
n-Eicosane (C20)
n-Heneicosane (C21)
n-Docosane (C22)
n-Tricosane (C23)
n-Tetracosane (C24)
n-Pentacosane (C25)
n-Hexacosane (C26)
n-Heptacosane (C27)
n-Octacosane (C28)
n-Nonacosane (C29)
n-Triacontane (C30)
n-Hentriacontane (C31)
n-Dotriacontane (C32)
n-Tritriacontane (C33)
n-Tetratriacontane (C34)
Parameter Result
J
J
JG
JG
J
J
JG
J
J
C
J
J
Dilution Factor
ND
ND
ND
ND
ND
ND
ND
ND
0.100
ND
ND
0.386
ND
0.211
0.134
ND
ND
0.111
ND
0.222
ND
0.714
0.430
3.07
0.317
6.06
0.392
2.02
0.303
1.78
2.11
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Saturated Hydrocarbons by GC-FID - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
0.821
0.821
0.821
0.821
0.821
0.821
0.821
0.821
0.821
0.821
0.821
0.821
0.821
0.821
0.821
0.821
0.821
0.821
0.821
0.821
0.821
0.821
0.821
0.821
0.821
0.821
0.821
0.821
0.821
0.821
0.821
11/05/12
HB006SG-000015-20121006Client ID:10/06/12 11:30Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-17Lab ID:
Field Prep: Not SpecifiedMatrix: Sediment Extraction Method:
Cleanup Method1:Analytical Method:Analytical Date:Analyst:
1,8015D(M)10/20/12 15:40DP
ALPHA OP-013
EPA 3611BExtraction Date: 10/12/12 12:37
Cleanup Date1: 10/16/12 34%Percent Solids:
MDL
0.244
0.262
0.245
0.179
0.225
0.124
0.124
0.098
0.098
0.124
0.271
0.271
0.175
0.165
0.103
0.211
0.116
0.098
0.086
0.104
0.137
0.435
0.121
0.099
0.176
0.547
0.094
0.116
0.103
0.116
0.131
Serial_No:11051209:46
Page 113 of 279
n-Pentatriacontane (C35)
n-Hexatriacontane (C36)
n-Heptatriacontane (C37)
n-Octatriacontane (C38)
n-Nonatriacontane (C39)
n-Tetracontane (C40)
Total Petroleum Hydrocarbons (C9-C40)
DRO (C10-C28)
Parameter Result
J
J
J
J
J
J
Dilution Factor
0.280
0.377
0.257
0.487
0.505
0.310
743
266
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
1
1
1
1
1
1
1
1
Qualifier Units RL
Saturated Hydrocarbons by GC-FID - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
0.821
0.821
0.821
0.821
0.821
0.821
27.1
17.2
ortho-terphenyl
d50-Tetracosane
95
92
50-130
50-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
HB006SG-000015-20121006Client ID:10/06/12 11:30Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-17Lab ID:
Field Prep: Not Specified
MDL
0.143
0.163
0.182
0.191
0.267
0.267
5.96
3.55
Serial_No:11051209:46
Page 114 of 279
n-Nonane (C9)
n-Decane (C10)
n-Undecane (C11)
n-Dodecane (C12)
n-Tridecane (C13)
2,6,10-Trimethyldodecane (1380)
n-Tetradecane (C14)
2,6,10-Trimethyltridecane (1470)
n-Pentadecane (C15)
n-Hexadecane (C16)
Norpristane (1650)
n-Heptadecane (C17)
Pristane
n-Octadecane (C18)
Phytane
n-Nonadecane (C19)
n-Eicosane (C20)
n-Heneicosane (C21)
n-Docosane (C22)
n-Tricosane (C23)
n-Tetracosane (C24)
n-Pentacosane (C25)
n-Hexacosane (C26)
n-Heptacosane (C27)
n-Octacosane (C28)
n-Nonacosane (C29)
n-Triacontane (C30)
n-Hentriacontane (C31)
n-Dotriacontane (C32)
n-Tritriacontane (C33)
n-Tetratriacontane (C34)
Parameter Result
JG
J
J
J
JG
JG
J
J
J
J
G
J
J
C
J
Dilution Factor
ND
ND
ND
ND
ND
ND
ND
0.357
0.147
ND
ND
1.10
0.249
0.547
0.595
0.315
ND
ND
0.184
0.520
0.260
4.80
0.792
5.14
0.851
14.0
1.21
6.82
0.806
5.84
6.85
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Saturated Hydrocarbons by GC-FID - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
1.12
1.12
1.12
1.12
1.12
1.12
1.12
1.12
1.12
1.12
1.12
1.12
1.12
1.12
1.12
1.12
1.12
1.12
1.12
1.12
1.12
1.12
1.12
1.12
1.12
1.12
1.12
1.12
1.12
1.12
1.12
11/05/12
HB005SG-000015-20121006Client ID:10/06/12 12:19Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-19Lab ID:
Field Prep: Not SpecifiedMatrix: Sediment Extraction Method:
Cleanup Method1:Analytical Method:Analytical Date:Analyst:
1,8015D(M)10/20/12 17:11DP
ALPHA OP-013
EPA 3611BExtraction Date: 10/12/12 12:37
Cleanup Date1: 10/16/12 26%Percent Solids:
MDL
0.331
0.356
0.333
0.243
0.306
0.168
0.168
0.133
0.133
0.168
0.368
0.368
0.238
0.224
0.140
0.287
0.158
0.134
0.116
0.142
0.187
0.590
0.164
0.134
0.239
0.743
0.128
0.158
0.140
0.157
0.178
Serial_No:11051209:46
Page 115 of 279
n-Pentatriacontane (C35)
n-Hexatriacontane (C36)
n-Heptatriacontane (C37)
n-Octatriacontane (C38)
n-Nonatriacontane (C39)
n-Tetracontane (C40)
Total Petroleum Hydrocarbons (C9-C40)
DRO (C10-C28)
Parameter Result
J
J
J
J
Dilution Factor
1.37
1.17
1.10
1.00
1.05
0.676
2980
1220
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
1
1
1
1
1
1
1
1
Qualifier Units RL
Saturated Hydrocarbons by GC-FID - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
1.12
1.12
1.12
1.12
1.12
1.12
36.8
23.4
ortho-terphenyl
d50-Tetracosane
95
95
50-130
50-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
HB005SG-000015-20121006Client ID:10/06/12 12:19Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-19Lab ID:
Field Prep: Not Specified
MDL
0.195
0.222
0.248
0.260
0.362
0.362
8.10
4.83
Serial_No:11051209:46
Page 116 of 279
n-Nonane (C9)
n-Decane (C10)
n-Undecane (C11)
n-Dodecane (C12)
n-Tridecane (C13)
2,6,10-Trimethyldodecane (1380)
n-Tetradecane (C14)
2,6,10-Trimethyltridecane (1470)
n-Pentadecane (C15)
n-Hexadecane (C16)
Norpristane (1650)
n-Heptadecane (C17)
Pristane
n-Octadecane (C18)
Phytane
n-Nonadecane (C19)
n-Eicosane (C20)
n-Heneicosane (C21)
n-Docosane (C22)
n-Tricosane (C23)
n-Tetracosane (C24)
n-Pentacosane (C25)
n-Hexacosane (C26)
n-Heptacosane (C27)
n-Octacosane (C28)
n-Nonacosane (C29)
n-Triacontane (C30)
n-Hentriacontane (C31)
n-Dotriacontane (C32)
n-Tritriacontane (C33)
n-Tetratriacontane (C34)
Parameter Result
JG
J
J
JG
JG
J
G
J
C
J
Dilution Factor
ND
ND
ND
ND
ND
ND
ND
0.350
0.133
ND
ND
1.11
0.266
0.513
0.576
0.283
ND
ND
ND
ND
ND
4.09
1.22
4.95
0.657
12.5
1.08
6.39
0.946
4.13
6.58
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Saturated Hydrocarbons by GC-FID - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
1.01
1.01
1.01
1.01
1.01
1.01
1.01
1.01
1.01
1.01
1.01
1.01
1.01
1.01
1.01
1.01
1.01
1.01
1.01
1.01
1.01
1.01
1.01
1.01
1.01
1.01
1.01
1.01
1.01
1.01
1.01
11/05/12
HB1005SG-000015-20121006Client ID:10/06/12 12:19Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-21Lab ID:
Field Prep: Not SpecifiedMatrix: Sediment Extraction Method:
Cleanup Method1:Analytical Method:Analytical Date:Analyst:
1,8015D(M)10/20/12 18:41DP
ALPHA OP-013
EPA 3611BExtraction Date: 10/12/12 12:37
Cleanup Date1: 10/16/12 25%Percent Solids:
MDL
0.299
0.321
0.301
0.219
0.276
0.151
0.151
0.120
0.120
0.152
0.332
0.332
0.215
0.202
0.126
0.259
0.142
0.120
0.105
0.128
0.168
0.533
0.148
0.121
0.216
0.671
0.116
0.143
0.127
0.142
0.160
Serial_No:11051209:46
Page 117 of 279
n-Pentatriacontane (C35)
n-Hexatriacontane (C36)
n-Heptatriacontane (C37)
n-Octatriacontane (C38)
n-Nonatriacontane (C39)
n-Tetracontane (C40)
Total Petroleum Hydrocarbons (C9-C40)
DRO (C10-C28)
Parameter Result
J
J
J
J
Dilution Factor
1.20
0.965
0.886
0.879
1.17
0.528
2920
1170
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
1
1
1
1
1
1
1
1
Qualifier Units RL
Saturated Hydrocarbons by GC-FID - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
1.01
1.01
1.01
1.01
1.01
1.01
33.2
21.2
ortho-terphenyl
d50-Tetracosane
96
94
50-130
50-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
HB1005SG-000015-20121006Client ID:10/06/12 12:19Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-21Lab ID:
Field Prep: Not Specified
MDL
0.176
0.200
0.224
0.235
0.327
0.327
7.31
4.36
Serial_No:11051209:46
Page 118 of 279
n-Nonane (C9)
n-Decane (C10)
n-Undecane (C11)
n-Dodecane (C12)
n-Tridecane (C13)
2,6,10-Trimethyldodecane (1380)
n-Tetradecane (C14)
2,6,10-Trimethyltridecane (1470)
n-Pentadecane (C15)
n-Hexadecane (C16)
Norpristane (1650)
n-Heptadecane (C17)
Pristane
n-Octadecane (C18)
Phytane
n-Nonadecane (C19)
n-Eicosane (C20)
n-Heneicosane (C21)
n-Docosane (C22)
n-Tricosane (C23)
n-Tetracosane (C24)
n-Pentacosane (C25)
n-Hexacosane (C26)
n-Heptacosane (C27)
n-Octacosane (C28)
n-Nonacosane (C29)
n-Triacontane (C30)
n-Hentriacontane (C31)
n-Dotriacontane (C32)
n-Tritriacontane (C33)
n-Tetratriacontane (C34)
Parameter Result
JG
J
JG
JG
J
J
G
J
C
J
J
Dilution Factor
ND
ND
ND
ND
ND
ND
ND
0.121
ND
ND
ND
0.624
ND
0.249
0.229
ND
ND
ND
0.091
0.236
ND
2.42
0.516
3.55
ND
7.28
0.606
3.67
0.502
2.21
4.99
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Saturated Hydrocarbons by GC-FID - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
0.714
0.714
0.714
0.714
0.714
0.714
0.714
0.714
0.714
0.714
0.714
0.714
0.714
0.714
0.714
0.714
0.714
0.714
0.714
0.714
0.714
0.714
0.714
0.714
0.714
0.714
0.714
0.714
0.714
0.714
0.714
11/05/12
HB004SG-000015-20121006Client ID:10/06/12 13:27Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-23Lab ID:
Field Prep: Not SpecifiedMatrix: Sediment Extraction Method:
Cleanup Method1:Analytical Method:Analytical Date:Analyst:
1,8015D(M)10/20/12 20:11DP
ALPHA OP-013
EPA 3611BExtraction Date: 10/12/12 12:37
Cleanup Date1: 10/16/12 35%Percent Solids:
MDL
0.212
0.228
0.213
0.156
0.196
0.107
0.107
0.085
0.085
0.108
0.236
0.236
0.153
0.143
0.090
0.184
0.101
0.086
0.075
0.091
0.120
0.378
0.105
0.086
0.153
0.476
0.082
0.101
0.090
0.100
0.114
Serial_No:11051209:46
Page 119 of 279
n-Pentatriacontane (C35)
n-Hexatriacontane (C36)
n-Heptatriacontane (C37)
n-Octatriacontane (C38)
n-Nonatriacontane (C39)
n-Tetracontane (C40)
Total Petroleum Hydrocarbons (C9-C40)
DRO (C10-C28)
Parameter Result
J
J
J
J
Dilution Factor
0.954
0.725
0.426
0.464
0.589
0.423
1780
724
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
1
1
1
1
1
1
1
1
Qualifier Units RL
Saturated Hydrocarbons by GC-FID - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
0.714
0.714
0.714
0.714
0.714
0.714
23.6
15.0
ortho-terphenyl
d50-Tetracosane
96
95
50-130
50-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
HB004SG-000015-20121006Client ID:10/06/12 13:27Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-23Lab ID:
Field Prep: Not Specified
MDL
0.125
0.142
0.159
0.166
0.232
0.232
5.19
3.09
Serial_No:11051209:46
Page 120 of 279
n-Nonane (C9)
n-Decane (C10)
n-Undecane (C11)
n-Dodecane (C12)
n-Tridecane (C13)
2,6,10-Trimethyldodecane (1380)
n-Tetradecane (C14)
2,6,10-Trimethyltridecane (1470)
n-Pentadecane (C15)
n-Hexadecane (C16)
Norpristane (1650)
n-Heptadecane (C17)
Pristane
n-Octadecane (C18)
Phytane
n-Nonadecane (C19)
n-Eicosane (C20)
n-Heneicosane (C21)
n-Docosane (C22)
n-Tricosane (C23)
n-Tetracosane (C24)
n-Pentacosane (C25)
n-Hexacosane (C26)
n-Heptacosane (C27)
n-Octacosane (C28)
n-Nonacosane (C29)
n-Triacontane (C30)
n-Hentriacontane (C31)
n-Dotriacontane (C32)
n-Tritriacontane (C33)
n-Tetratriacontane (C34)
Parameter Result
JG
J
J
JG
JG
J
J
G
J
J
C
J
J
Dilution Factor
ND
ND
ND
ND
ND
ND
ND
0.158
0.148
ND
ND
0.846
ND
0.540
0.300
ND
ND
ND
0.134
0.294
ND
2.92
0.561
3.69
0.563
10.4
0.889
4.91
0.777
3.67
4.80
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Saturated Hydrocarbons by GC-FID - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
0.991
0.991
0.991
0.991
0.991
0.991
0.991
0.991
0.991
0.991
0.991
0.991
0.991
0.991
0.991
0.991
0.991
0.991
0.991
0.991
0.991
0.991
0.991
0.991
0.991
0.991
0.991
0.991
0.991
0.991
0.991
11/05/12
HB003SG-000015-20121006Client ID:10/06/12 14:21Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-25Lab ID:
Field Prep: Not SpecifiedMatrix: Sediment Extraction Method:
Cleanup Method1:Analytical Method:Analytical Date:Analyst:
1,8015D(M)10/20/12 21:41DP
ALPHA OP-013
EPA 3611BExtraction Date: 10/12/12 14:50
Cleanup Date1: 10/16/12 28%Percent Solids:
MDL
0.294
0.316
0.296
0.216
0.272
0.149
0.149
0.118
0.118
0.149
0.327
0.327
0.212
0.199
0.124
0.255
0.140
0.119
0.103
0.126
0.166
0.524
0.146
0.119
0.212
0.660
0.114
0.140
0.125
0.139
0.158
Serial_No:11051209:46
Page 121 of 279
n-Pentatriacontane (C35)
n-Hexatriacontane (C36)
n-Heptatriacontane (C37)
n-Octatriacontane (C38)
n-Nonatriacontane (C39)
n-Tetracontane (C40)
Total Petroleum Hydrocarbons (C9-C40)
DRO (C10-C28)
Parameter Result
J
J
J
J
J
J
Dilution Factor
0.788
0.878
0.607
0.688
0.924
0.653
2190
845
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
1
1
1
1
1
1
1
1
Qualifier Units RL
Saturated Hydrocarbons by GC-FID - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
0.991
0.991
0.991
0.991
0.991
0.991
32.7
20.8
ortho-terphenyl
d50-Tetracosane
95
94
50-130
50-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
HB003SG-000015-20121006Client ID:10/06/12 14:21Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-25Lab ID:
Field Prep: Not Specified
MDL
0.173
0.197
0.220
0.231
0.322
0.322
7.20
4.29
Serial_No:11051209:46
Page 122 of 279
n-Nonane (C9)
n-Decane (C10)
n-Undecane (C11)
n-Dodecane (C12)
n-Tridecane (C13)
2,6,10-Trimethyldodecane (1380)
n-Tetradecane (C14)
2,6,10-Trimethyltridecane (1470)
n-Pentadecane (C15)
n-Hexadecane (C16)
Norpristane (1650)
n-Heptadecane (C17)
Pristane
n-Octadecane (C18)
Phytane
n-Nonadecane (C19)
n-Eicosane (C20)
n-Heneicosane (C21)
n-Docosane (C22)
n-Tricosane (C23)
n-Tetracosane (C24)
n-Pentacosane (C25)
n-Hexacosane (C26)
n-Heptacosane (C27)
n-Octacosane (C28)
n-Nonacosane (C29)
n-Triacontane (C30)
n-Hentriacontane (C31)
n-Dotriacontane (C32)
n-Tritriacontane (C33)
n-Tetratriacontane (C34)
Parameter Result
JG
J
JG
JG
J
J
JG
J
J
C
J
J
Dilution Factor
ND
ND
ND
ND
ND
ND
ND
0.096
ND
ND
ND
0.611
ND
0.227
0.172
ND
ND
ND
0.089
0.200
ND
0.639
0.615
2.73
0.382
6.98
0.539
3.16
0.482
2.38
3.13
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Saturated Hydrocarbons by GC-FID - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
0.770
0.770
0.770
0.770
0.770
0.770
0.770
0.770
0.770
0.770
0.770
0.770
0.770
0.770
0.770
0.770
0.770
0.770
0.770
0.770
0.770
0.770
0.770
0.770
0.770
0.770
0.770
0.770
0.770
0.770
0.770
11/05/12
HB002SG-000015-20121006Client ID:10/06/12 15:05Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-27Lab ID:
Field Prep: Not SpecifiedMatrix: Sediment Extraction Method:
Cleanup Method1:Analytical Method:Analytical Date:Analyst:
1,8015D(M)10/20/12 23:11DP
ALPHA OP-013
EPA 3611BExtraction Date: 10/12/12 14:50
Cleanup Date1: 10/16/12 34%Percent Solids:
MDL
0.228
0.246
0.230
0.168
0.211
0.116
0.116
0.092
0.092
0.116
0.254
0.254
0.164
0.155
0.097
0.198
0.109
0.092
0.080
0.098
0.129
0.408
0.113
0.093
0.165
0.513
0.088
0.109
0.097
0.108
0.122
Serial_No:11051209:46
Page 123 of 279
n-Pentatriacontane (C35)
n-Hexatriacontane (C36)
n-Heptatriacontane (C37)
n-Octatriacontane (C38)
n-Nonatriacontane (C39)
n-Tetracontane (C40)
Total Petroleum Hydrocarbons (C9-C40)
DRO (C10-C28)
Parameter Result
J
J
J
J
J
J
Dilution Factor
0.555
0.535
0.401
0.590
0.618
0.416
1420
550
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
1
1
1
1
1
1
1
1
Qualifier Units RL
Saturated Hydrocarbons by GC-FID - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
0.770
0.770
0.770
0.770
0.770
0.770
25.4
16.2
ortho-terphenyl
d50-Tetracosane
91
89
50-130
50-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
HB002SG-000015-20121006Client ID:10/06/12 15:05Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-27Lab ID:
Field Prep: Not Specified
MDL
0.134
0.153
0.171
0.180
0.250
0.250
5.59
3.33
Serial_No:11051209:46
Page 124 of 279
n-Nonane (C9)
n-Decane (C10)
n-Undecane (C11)
n-Dodecane (C12)
n-Tridecane (C13)
2,6,10-Trimethyldodecane (1380)
n-Tetradecane (C14)
2,6,10-Trimethyltridecane (1470)
n-Pentadecane (C15)
n-Hexadecane (C16)
Norpristane (1650)
n-Heptadecane (C17)
Pristane
n-Octadecane (C18)
Phytane
n-Nonadecane (C19)
n-Eicosane (C20)
n-Heneicosane (C21)
n-Docosane (C22)
n-Tricosane (C23)
n-Tetracosane (C24)
n-Pentacosane (C25)
n-Hexacosane (C26)
n-Heptacosane (C27)
n-Octacosane (C28)
n-Nonacosane (C29)
n-Triacontane (C30)
n-Hentriacontane (C31)
n-Dotriacontane (C32)
n-Tritriacontane (C33)
n-Tetratriacontane (C34)
Parameter Result
JG
J
J
JG
JG
J
J
G
J
J
C
J
J
Dilution Factor
ND
ND
ND
ND
ND
ND
ND
0.121
0.101
ND
ND
0.778
ND
0.292
0.230
ND
ND
ND
0.102
0.271
ND
2.22
0.692
3.32
0.457
9.24
0.723
4.10
0.693
3.40
3.96
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Qualifier Units RL
Saturated Hydrocarbons by GC-FID - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
0.833
0.833
0.833
0.833
0.833
0.833
0.833
0.833
0.833
0.833
0.833
0.833
0.833
0.833
0.833
0.833
0.833
0.833
0.833
0.833
0.833
0.833
0.833
0.833
0.833
0.833
0.833
0.833
0.833
0.833
0.833
11/05/12
HB001SG-000015-20121006Client ID:10/06/12 15:54Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-29Lab ID:
Field Prep: Not SpecifiedMatrix: Sediment Extraction Method:
Cleanup Method1:Analytical Method:Analytical Date:Analyst:
1,8015D(M)10/21/12 00:41DP
ALPHA OP-013
EPA 3611BExtraction Date: 10/12/12 14:50
Cleanup Date1: 10/16/12 30%Percent Solids:
MDL
0.247
0.266
0.249
0.181
0.228
0.125
0.125
0.099
0.099
0.125
0.275
0.275
0.178
0.167
0.104
0.214
0.118
0.100
0.087
0.106
0.139
0.441
0.122
0.100
0.179
0.555
0.096
0.118
0.105
0.117
0.132
Serial_No:11051209:46
Page 125 of 279
n-Pentatriacontane (C35)
n-Hexatriacontane (C36)
n-Heptatriacontane (C37)
n-Octatriacontane (C38)
n-Nonatriacontane (C39)
n-Tetracontane (C40)
Total Petroleum Hydrocarbons (C9-C40)
DRO (C10-C28)
Parameter Result
J
J
J
J
J
Dilution Factor
0.792
0.655
0.570
0.697
0.931
0.570
1680
623
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
1
1
1
1
1
1
1
1
Qualifier Units RL
Saturated Hydrocarbons by GC-FID - Mansfield Lab
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
0.833
0.833
0.833
0.833
0.833
0.833
27.5
17.5
ortho-terphenyl
d50-Tetracosane
96
95
50-130
50-130
Acceptance CriteriaSurrogate % Recovery Qualifier
11/05/12
HB001SG-000015-20121006Client ID:10/06/12 15:54Date Collected:10/08/12Date Received:
Not SpecifiedSample Location:
L1218042-29Lab ID:
Field Prep: Not Specified
MDL
0.145
0.166
0.185
0.194
0.270
0.270
6.05
3.60
Serial_No:11051209:46
Page 126 of 279
Method Blank AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
10/11/12 14:191,8015D(M)Analytical Method:
Analytical Date:Extraction Method: EPA 3510CExtraction Date: 10/10/12 07:35
11/05/12
Analyst: DP
n-Nonane (C9)
n-Decane (C10)
n-Undecane (C11)
n-Dodecane (C12)
n-Tridecane (C13)
2,6,10-Trimethyldodecane (1380)
n-Tetradecane (C14)
2,6,10-Trimethyltridecane (1470)
n-Pentadecane (C15)
n-Hexadecane (C16)
Norpristane (1650)
n-Heptadecane (C17)
Pristane
n-Octadecane (C18)
Phytane
n-Nonadecane (C19)
n-Eicosane (C20)
n-Heneicosane (C21)
n-Docosane (C22)
n-Tricosane (C23)
n-Tetracosane (C24)
n-Pentacosane (C25)
n-Hexacosane (C26)
n-Heptacosane (C27)
n-Octacosane (C28)
n-Nonacosane (C29)
n-Triacontane (C30)
n-Hentriacontane (C31)
n-Dotriacontane (C32)
n-Tritriacontane (C33)
n-Tetratriacontane (C34)
Parameter Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.001
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
RL
0.001
0.001
0.001
0.001
0.005
0.001
0.001
0.001
0.001
0.001
0.001
0.001
0.001
0.001
0.001
0.001
0.001
0.001
0.001
0.001
0.001
0.005
0.001
0.001
0.001
0.001
0.001
0.001
0.001
0.001
0.001
JC
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
UnitsQualifier
Saturated Hydrocarbons by GC-FID - Mansfield Lab for sample(s): 11 Batch: WG566066-1
MDL
0.0003
0.0001
0.0001
0.0001
0.001
0.0001
0.0001
0.0001
0.0001
0.0001
0.0001
0.0001
0.0002
0.0001
0.0001
0.0002
0.0001
0.0001
0.00004
0.0001
0.0001
0.001
0.0001
0.0001
0.0002
0.0001
0.0001
0.0001
0.0001
0.0001
0.0002
Serial_No:11051209:46
Page 127 of 279
Method Blank AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
10/11/12 14:191,8015D(M)Analytical Method:
Analytical Date:Extraction Method: EPA 3510CExtraction Date: 10/10/12 07:35
11/05/12
Analyst: DP
n-Pentatriacontane (C35)
n-Hexatriacontane (C36)
n-Heptatriacontane (C37)
n-Octatriacontane (C38)
n-Nonatriacontane (C39)
n-Tetracontane (C40)
Total Petroleum Hydrocarbons (C9-C40)DRO (C10-C28)
Parameter Result
ND
ND
ND
ND
ND
ND
ND
0.010
RL
0.001
0.001
0.001
0.001
0.001
0.001
0.033
0.021J
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
UnitsQualifier
Saturated Hydrocarbons by GC-FID - Mansfield Lab for sample(s): 11 Batch: WG566066-1
ortho-terphenyl
d50-Tetracosane
95
92
50-130
50-130
Surrogate %Recovery QualifierAcceptance
Criteria
MDL
0.0002
0.0001
0.0002
0.0002
0.0002
0.0002
0.006
0.004
Serial_No:11051209:46
Page 128 of 279
Method Blank AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
10/19/12 18:331,8015D(M)Analytical Method:
Analytical Date:Extraction Method:
Cleanup Method1:
ALPHA OP-013
EPA 3611BExtraction Date: 10/12/12 12:37
11/05/12
Analyst: DP
n-Nonane (C9)
n-Decane (C10)
n-Undecane (C11)
n-Dodecane (C12)
n-Tridecane (C13)
2,6,10-Trimethyldodecane (1380)
n-Tetradecane (C14)
2,6,10-Trimethyltridecane (1470)
n-Pentadecane (C15)
n-Hexadecane (C16)
Norpristane (1650)
n-Heptadecane (C17)
Pristane
n-Octadecane (C18)
Phytane
n-Nonadecane (C19)
n-Eicosane (C20)
n-Heneicosane (C21)
n-Docosane (C22)
n-Tricosane (C23)
n-Tetracosane (C24)
n-Pentacosane (C25)
n-Hexacosane (C26)
n-Heptacosane (C27)
n-Octacosane (C28)
n-Nonacosane (C29)
n-Triacontane (C30)
n-Hentriacontane (C31)
n-Dotriacontane (C32)
n-Tritriacontane (C33)
Parameter Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
RL
0.067
0.067
0.067
0.067
0.067
0.067
0.067
0.067
0.067
0.067
0.067
0.067
0.067
0.067
0.067
0.067
0.067
0.067
0.067
0.067
0.067
0.067
0.067
0.067
0.067
0.067
0.067
0.067
0.067
0.067
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
UnitsQualifier
Saturated Hydrocarbons by GC-FID - Mansfield Lab for sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG566754-1
Cleanup Date1: 10/16/12
MDL
0.020
0.021
0.020
0.015
0.018
0.010
0.010
0.008
0.008
0.010
0.022
0.022
0.014
0.013
0.008
0.017
0.009
0.008
0.007
0.008
0.011
0.035
0.010
0.008
0.014
0.044
0.008
0.009
0.008
0.009
Serial_No:11051209:46
Page 129 of 279
Method Blank AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
10/19/12 18:331,8015D(M)Analytical Method:
Analytical Date:Extraction Method:
Cleanup Method1:
ALPHA OP-013
EPA 3611BExtraction Date: 10/12/12 12:37
11/05/12
Analyst: DP
n-Tetratriacontane (C34)
n-Pentatriacontane (C35)
n-Hexatriacontane (C36)
n-Heptatriacontane (C37)
n-Octatriacontane (C38)
n-Nonatriacontane (C39)
n-Tetracontane (C40)
Total Petroleum Hydrocarbons (C9-C40)DRO (C10-C28)
Parameter Result
ND
ND
ND
ND
ND
ND
ND
0.525
0.338
RL
0.067
0.067
0.067
0.067
0.067
0.067
0.067
2.20
1.40
J
J
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
UnitsQualifier
Saturated Hydrocarbons by GC-FID - Mansfield Lab for sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG566754-1
ortho-terphenyl
d50-Tetracosane
95
97
50-130
50-130
Surrogate %Recovery QualifierAcceptance
Criteria
Cleanup Date1: 10/16/12
MDL
0.011
0.012
0.013
0.015
0.016
0.022
0.022
0.484
0.288
Serial_No:11051209:46
Page 130 of 279
Nonane (C9)
Decane (C10)
Dodecane (C12)
Tetradecane (C14)
Hexadecane (C16)
Octadecane (C18)
Nonadecane (C19)
Eicosane (C20)
Docosane (C22)
Tetracosane (C24)
Hexacosane (C26)
Octacosane (C28)
Triacontane (C30)
Hexatriacontane (C36)
76
85
90
96
103
107
96
99
99
99
98
98
99
96
60
71
80
94
104
108
97
100
100
100
100
99
100
97
50-130
50-130
50-130
50-130
50-130
50-130
50-130
50-130
50-130
50-130
50-130
50-130
50-130
50-130
24
18
12
2
1
1
1
1
1
1
2
1
1
1
30
30
30
30
30
30
30
30
30
30
30
30
30
30
ParameterLCS
%RecoveryLCSD
%Recovery%Recovery
Limits RPD RPD Limits
Saturated Hydrocarbons by GC-FID - Mansfield Lab Associated sample(s): 11 Batch: WG566066-2 WG566066-3
Lab Control Sample AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
o-Terphenyl
d50-Tetracosane
93
89
50-130
50-130
94
90
Surrogate Qual%Recovery Qual%RecoveryLCS LCSD
11/05/12
AcceptanceCriteria
Qual Qual Qual
Serial_No:11051209:46
Page 131 of 279
Nonane (C9)
Decane (C10)
Dodecane (C12)
Tetradecane (C14)
Hexadecane (C16)
Octadecane (C18)
Nonadecane (C19)
Eicosane (C20)
Docosane (C22)
Tetracosane (C24)
Hexacosane (C26)
Octacosane (C28)
Triacontane (C30)
Hexatriacontane (C36)
67
77
75
83
94
96
90
92
92
93
93
93
94
90
77
87
82
89
99
100
94
96
97
98
98
98
99
96
50-130
50-130
50-130
50-130
50-130
50-130
50-130
50-130
50-130
50-130
50-130
50-130
50-130
50-130
14
12
9
7
5
4
4
4
5
5
5
5
5
6
30
30
30
30
30
30
30
30
30
30
30
30
30
30
ParameterLCS
%RecoveryLCSD
%Recovery%Recovery
Limits RPD RPD Limits
Saturated Hydrocarbons by GC-FID - Mansfield Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG566754-2 WG566754-3
Lab Control Sample AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
o-Terphenyl
d50-Tetracosane
91
90
50-130
50-130
94
94
Surrogate Qual%Recovery Qual%RecoveryLCS LCSD
11/05/12
AcceptanceCriteria
Qual Qual Qual
Serial_No:11051209:46
Page 132 of 279
METALS
Serial_No:11051209:46
Page 133 of 279
FF
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
TN005SG-000014-20121005Client ID:10/05/12 09:32Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-01Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Antimony, Total
Silver, Total
0.062
0.682
mg/kg
mg/kg
2
2
0.033
0.033
10/24/12 19:26
10/24/12 19:26
1,6020A
1,6020A
PD
PD
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 72%
MDL
0.006
0.002
Serial_No:11051209:46
Page 134 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
TN005SG-000014-20121005Client ID:10/05/12 09:32Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-01Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Tin, Total 5.14 mg/kg 23.25 10/31/12 15:25 1,6020A PD10/30/12 15:23 EPA 3050B
PrepMethod
Percent Solids: 72%
R
MDL
0.328
Serial_No:11051209:46
Page 135 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
TN005SG-000014-20121005Client ID:10/05/12 09:32Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-01Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Arsenic, Total
Barium, Total
Beryllium, Total
Cadmium, Total
Chromium, Total
Cobalt, Total
Copper, Total
Lead, Total
Manganese, Total
Nickel, Total
Selenium, Total
Thallium, Total
Vanadium, Total
5.18
14.8
0.288
1.06
18.6
3.68
27.8
34.7
161
9.90
1.98
0.509
9.88
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
10
10
10
10
10
10
10
10
10
10
10
10
10
0.162
0.975
0.098
0.065
0.650
0.162
0.650
0.195
0.650
0.325
0.325
0.065
0.325
10/24/12 17:29
10/24/12 17:29
10/24/12 17:29
10/24/12 17:29
10/24/12 17:29
10/24/12 17:29
10/24/12 17:29
10/24/12 17:29
10/24/12 17:29
10/24/12 17:29
10/24/12 17:29
10/24/12 17:29
10/24/12 17:29
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 72%
D2
MDL
0.020
0.250
0.028
0.009
0.152
0.017
0.037
0.063
0.145
0.049
0.081
0.009
0.015
Serial_No:11051209:46
Page 136 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
TN005SG-000014-20121005Client ID:10/05/12 09:32Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-01Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Aluminum, Total
Calcium, Total
Iron, Total
Magnesium, Total
Potassium, Total
Sodium, Total
Zinc, Total
2960
15800
6940
2660
896
3760
54.2
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
50
50
50
50
50
50
50
162
812
325
162
162
162
16.2
10/24/12 16:24
10/24/12 16:24
10/24/12 16:24
10/24/12 16:24
10/24/12 16:24
10/24/12 16:24
10/24/12 16:24
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
PD
PD
PD
PD
PD
PD
PD
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 72%
D
MDL
24.1
98.8
33.5
20.0
24.6
14.0
4.22
Serial_No:11051209:46
Page 137 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
TN002SG-000011-20121005Client ID:10/05/12 10:41Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-03Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Antimony, Total
Silver, Total
0.190
1.83
mg/kg
mg/kg
2
2
0.046
0.046
10/24/12 19:31
10/24/12 19:31
1,6020A
1,6020A
PD
PD
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 55%
MDL
0.008
0.002
Serial_No:11051209:46
Page 138 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
TN002SG-000011-20121005Client ID:10/05/12 10:41Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-03Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Tin, Total 9.52 mg/kg 24.20 10/31/12 15:30 1,6020A PD10/30/12 15:23 EPA 3050B
PrepMethod
Percent Solids: 55%
R
MDL
0.424
Serial_No:11051209:46
Page 139 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
TN002SG-000011-20121005Client ID:10/05/12 10:41Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-03Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Arsenic, Total
Barium, Total
Beryllium, Total
Cadmium, Total
Chromium, Total
Cobalt, Total
Copper, Total
Lead, Total
Manganese, Total
Nickel, Total
Selenium, Total
Thallium, Total
Vanadium, Total
7.94
41.2
0.308
1.04
40.7
5.10
70.1
69.9
305
16.2
0.960
0.180
18.7
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
10
10
10
10
10
10
10
10
10
10
10
10
10
0.223
1.34
0.134
0.089
0.894
0.223
0.894
0.268
0.894
0.447
0.447
0.089
0.447
10/24/12 17:40
10/24/12 17:40
10/24/12 17:40
10/24/12 17:40
10/24/12 17:40
10/24/12 17:40
10/24/12 17:40
10/24/12 17:40
10/24/12 17:40
10/24/12 17:40
10/24/12 17:40
10/24/12 17:40
10/24/12 17:40
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 55%
D2
MDL
0.028
0.343
0.039
0.012
0.210
0.023
0.051
0.086
0.199
0.067
0.111
0.012
0.021
Serial_No:11051209:46
Page 140 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
TN002SG-000011-20121005Client ID:10/05/12 10:41Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-03Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Aluminum, Total
Calcium, Total
Iron, Total
Magnesium, Total
Potassium, Total
Sodium, Total
Zinc, Total
5680
89800
14700
4590
1850
8690
142
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
50
50
50
50
50
50
50
223
1120
447
223
223
223
22.3
10/24/12 16:31
10/24/12 16:31
10/24/12 16:31
10/24/12 16:31
10/24/12 16:31
10/24/12 16:31
10/24/12 16:31
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
PD
PD
PD
PD
PD
PD
PD
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 55%
D
MDL
33.1
136.
46.0
27.6
33.8
19.2
5.80
Serial_No:11051209:46
Page 141 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
TN003SG-000015-20121005Client ID:10/05/12 11:24Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-05Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Antimony, Total
Silver, Total
0.180
3.08
mg/kg
mg/kg
2
2
0.060
0.060
10/24/12 19:32
10/24/12 19:32
1,6020A
1,6020A
PD
PD
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 41%
MDL
0.011
0.003
Serial_No:11051209:46
Page 142 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
TN003SG-000015-20121005Client ID:10/05/12 11:24Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-05Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Tin, Total 16.2 mg/kg 26.56 10/31/12 15:31 1,6020A PD10/30/12 15:23 EPA 3050B
PrepMethod
Percent Solids: 41%
R
MDL
0.662
Serial_No:11051209:46
Page 143 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
TN003SG-000015-20121005Client ID:10/05/12 11:24Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-05Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Arsenic, Total
Barium, Total
Beryllium, Total
Cadmium, Total
Chromium, Total
Cobalt, Total
Copper, Total
Lead, Total
Manganese, Total
Nickel, Total
Selenium, Total
Thallium, Total
Vanadium, Total
10.2
68.5
0.555
1.46
69.8
8.65
122
118
459
26.3
1.53
0.245
32.3
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
10
10
10
10
10
10
10
10
10
10
10
10
10
0.316
1.90
0.190
0.126
1.26
0.316
1.26
0.379
1.26
0.632
0.632
0.126
0.632
10/24/12 17:41
10/24/12 17:41
10/24/12 17:41
10/24/12 17:41
10/24/12 17:41
10/24/12 17:41
10/24/12 17:41
10/24/12 17:41
10/24/12 17:41
10/24/12 17:41
10/24/12 17:41
10/24/12 17:41
10/24/12 17:41
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 41%
D2
MDL
0.039
0.486
0.055
0.017
0.296
0.033
0.071
0.122
0.281
0.095
0.157
0.017
0.029
Serial_No:11051209:46
Page 144 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
TN003SG-000015-20121005Client ID:10/05/12 11:24Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-05Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Aluminum, Total
Calcium, Total
Iron, Total
Magnesium, Total
Potassium, Total
Sodium, Total
Zinc, Total
10000
47500
23800
7410
3000
12600
205
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
50
50
50
50
50
50
50
316
1580
632
316
316
316
31.6
10/24/12 16:32
10/24/12 16:32
10/24/12 16:32
10/24/12 16:32
10/24/12 16:32
10/24/12 16:32
10/24/12 16:32
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
PD
PD
PD
PD
PD
PD
PD
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 41%
D
MDL
46.9
192.
65.2
39.0
47.8
27.2
8.21
Serial_No:11051209:46
Page 145 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
TN004SG-000015-20121005Client ID:10/05/12 11:46Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-07Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Antimony, Total
Silver, Total
0.089
1.13
mg/kg
mg/kg
2
2
0.050
0.050
10/24/12 19:32
10/24/12 19:32
1,6020A
1,6020A
PD
PD
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 51%
MDL
0.009
0.002
Serial_No:11051209:46
Page 146 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
TN004SG-000015-20121005Client ID:10/05/12 11:46Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-07Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Tin, Total 6.06 mg/kg 24.60 10/31/12 15:31 1,6020A PD10/30/12 15:23 EPA 3050B
PrepMethod
Percent Solids: 51%
R
MDL
0.465
Serial_No:11051209:46
Page 147 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
TN004SG-000015-20121005Client ID:10/05/12 11:46Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-07Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Arsenic, Total
Barium, Total
Beryllium, Total
Cadmium, Total
Chromium, Total
Cobalt, Total
Copper, Total
Lead, Total
Manganese, Total
Nickel, Total
Selenium, Total
Thallium, Total
Vanadium, Total
8.17
35.0
0.511
0.583
34.7
7.46
43.8
45.8
424
19.2
0.929
0.152
25.8
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
10
10
10
10
10
10
10
10
10
10
10
10
10
0.225
1.35
0.135
0.090
0.900
0.225
0.900
0.270
0.900
0.450
0.450
0.090
0.450
10/24/12 17:43
10/24/12 17:43
10/24/12 17:43
10/24/12 17:43
10/24/12 17:43
10/24/12 17:43
10/24/12 17:43
10/24/12 17:43
10/24/12 17:43
10/24/12 17:43
10/24/12 17:43
10/24/12 17:43
10/24/12 17:43
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 51%
D2
MDL
0.028
0.346
0.039
0.012
0.211
0.024
0.051
0.087
0.200
0.068
0.112
0.012
0.021
Serial_No:11051209:46
Page 148 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
TN004SG-000015-20121005Client ID:10/05/12 11:46Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-07Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Aluminum, Total
Calcium, Total
Iron, Total
Magnesium, Total
Potassium, Total
Sodium, Total
Zinc, Total
8270
26100
19900
6080
2510
9030
104
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
50
50
50
50
50
50
50
225
1120
450
225
225
225
22.5
10/24/12 16:33
10/24/12 16:33
10/24/12 16:33
10/24/12 16:33
10/24/12 16:33
10/24/12 16:33
10/24/12 16:33
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
PD
PD
PD
PD
PD
PD
PD
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 51%
D
MDL
33.4
137.
46.4
27.8
34.0
19.3
5.85
Serial_No:11051209:46
Page 149 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
TN006SG-000015-20121005Client ID:10/05/12 13:16Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-09Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Antimony, Total
Silver, Total
0.044
0.324
mg/kg
mg/kg
2
2
0.031
0.031
10/24/12 19:33
10/24/12 19:33
1,6020A
1,6020A
PD
PD
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 78%
MDL
0.005
0.001
Serial_No:11051209:46
Page 150 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
TN006SG-000015-20121005Client ID:10/05/12 13:16Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-09Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Tin, Total J2.16 mg/kg 23.57 10/31/12 15:32 1,6020A PD10/30/12 15:23 EPA 3050B
PrepMethod
Percent Solids: 78%
R
MDL
0.360
Serial_No:11051209:46
Page 151 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
TN006SG-000015-20121005Client ID:10/05/12 13:16Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-09Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Arsenic, Total
Barium, Total
Beryllium, Total
Cadmium, Total
Chromium, Total
Cobalt, Total
Copper, Total
Lead, Total
Manganese, Total
Nickel, Total
Selenium, Total
Thallium, Total
Vanadium, Total
J
2.97
9.21
0.137
0.206
11.8
2.85
16.9
19.0
108
7.89
0.268
0.077
7.58
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
10
10
10
10
10
10
10
10
10
10
10
10
10
0.167
1.00
0.100
0.067
0.669
0.167
0.669
0.201
0.669
0.335
0.335
0.067
0.335
10/24/12 17:45
10/24/12 17:45
10/24/12 17:45
10/24/12 17:45
10/24/12 17:45
10/24/12 17:45
10/24/12 17:45
10/24/12 17:45
10/24/12 17:45
10/24/12 17:45
10/24/12 17:45
10/24/12 17:45
10/24/12 17:45
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 78%
D2
MDL
0.021
0.257
0.029
0.009
0.157
0.018
0.038
0.065
0.149
0.050
0.083
0.009
0.015
Serial_No:11051209:46
Page 152 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
TN006SG-000015-20121005Client ID:10/05/12 13:16Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-09Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Aluminum, Total
Calcium, Total
Iron, Total
Magnesium, Total
Potassium, Total
Sodium, Total
Zinc, Total
2190
11900
5170
2070
631
2890
37.1
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
50
50
50
50
50
50
50
167
837
335
167
167
167
16.7
10/24/12 16:34
10/24/12 16:34
10/24/12 16:34
10/24/12 16:34
10/24/12 16:34
10/24/12 16:34
10/24/12 16:34
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
PD
PD
PD
PD
PD
PD
PD
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 78%
D
MDL
24.8
102.
34.5
20.6
25.3
14.4
4.35
Serial_No:11051209:46
Page 153 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
SG-RB-20121006Client ID:10/06/12 09:05Date Collected:10/08/12Date Received:
Matrix: WaterNot SpecifiedSample Location:
L1218042-11Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Aluminum, Total
Antimony, Total
Arsenic, Total
Barium, Total
Beryllium, Total
Cadmium, Total
Calcium, Total
Chromium, Total
Copper, Total
Iron, Total
Lead, Total
Magnesium, Total
Manganese, Total
Nickel, Total
Potassium, Total
Selenium, Total
Silver, Total
Sodium, Total
Thallium, Total
Tin, Total
Vanadium, Total
Zinc, Total
J
J
J
J
J
J
J
J
J
J
ND
ND
ND
0.0002
ND
ND
0.069
0.001
0.001
0.013
0.0002
0.134
0.0008
0.0007
0.068
ND
ND
1.11
0.00001
0.0002
ND
0.005
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
0.100
0.0005
0.0005
0.0005
0.0005
0.0005
0.100
0.001
0.001
0.050
0.0010
0.070
0.0005
0.0005
0.100
0.005
0.0003
0.100
0.00020
0.0005
0.005
0.010
10/23/12 18:19
10/23/12 18:19
10/23/12 18:19
10/23/12 18:19
10/23/12 18:19
10/23/12 18:19
10/23/12 18:19
10/23/12 18:19
10/23/12 18:19
10/23/12 18:19
10/23/12 18:19
10/23/12 18:19
10/23/12 18:19
10/23/12 18:19
10/23/12 18:19
10/23/12 18:19
10/23/12 18:19
10/23/12 18:19
10/23/12 18:19
10/23/12 18:19
10/23/12 18:19
10/23/12 18:19
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
EPA 3020A
EPA 3020A
EPA 3020A
EPA 3020A
EPA 3020A
EPA 3020A
EPA 3020A
EPA 3020A
EPA 3020A
EPA 3020A
EPA 3020A
EPA 3020A
EPA 3020A
EPA 3020A
EPA 3020A
EPA 3020A
EPA 3020A
EPA 3020A
EPA 3020A
EPA 3020A
EPA 3020A
EPA 3020A
PrepMethodMDL
0.023
0.00003
0.0001
0.0001
0.0001
0.0001
0.019
0.0003
0.0003
0.008
0.0001
0.002
0.0001
0.0002
0.006
0.0003
0.00002
0.006
0.00001
0.0001
0.0001
0.001
Serial_No:11051209:46
Page 154 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
SG-RB-20121006Client ID:10/06/12 09:05Date Collected:10/08/12Date Received:
Matrix: WaterNot SpecifiedSample Location:
L1218042-11Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Cobalt, Total J0.00005 mg/l 10.00020 10/23/12 18:49 1,6020A PD10/17/12 12:00 EPA 3020A
PrepMethod
R
MDL
0.00002
Serial_No:11051209:46
Page 155 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
HB008SG-000015-20121006Client ID:10/06/12 09:55Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-13Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Antimony, Total
Silver, Total
0.431
1.89
mg/kg
mg/kg
2
2
0.096
0.096
10/24/12 19:34
10/24/12 19:34
1,6020A
1,6020A
PD
PD
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 27%
MDL
0.017
0.004
Serial_No:11051209:46
Page 156 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
HB008SG-000015-20121006Client ID:10/06/12 09:55Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-13Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Tin, Total 13.8 mg/kg 29.96 10/31/12 15:33 1,6020A PD10/30/12 15:23 EPA 3050B
PrepMethod
Percent Solids: 27%
R
MDL
1.00
Serial_No:11051209:46
Page 157 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
HB008SG-000015-20121006Client ID:10/06/12 09:55Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-13Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Arsenic, Total
Barium, Total
Beryllium, Total
Cadmium, Total
Chromium, Total
Cobalt, Total
Copper, Total
Lead, Total
Manganese, Total
Nickel, Total
Selenium, Total
Thallium, Total
Vanadium, Total
16.4
36.6
0.667
1.68
47.8
8.60
115
128
232
26.5
2.62
0.372
50.7
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
10
10
10
10
10
10
10
10
10
10
10
10
10
0.473
2.84
0.284
0.189
1.89
0.473
1.89
0.567
1.89
0.946
0.946
0.189
0.946
10/24/12 17:47
10/24/12 17:47
10/24/12 17:47
10/24/12 17:47
10/24/12 17:47
10/24/12 17:47
10/24/12 17:47
10/24/12 17:47
10/24/12 17:47
10/24/12 17:47
10/24/12 17:47
10/24/12 17:47
10/24/12 17:47
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 27%
D2
MDL
0.058
0.726
0.082
0.025
0.444
0.050
0.107
0.182
0.421
0.142
0.236
0.026
0.043
Serial_No:11051209:46
Page 158 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
HB008SG-000015-20121006Client ID:10/06/12 09:55Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-13Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Aluminum, Total
Calcium, Total
Iron, Total
Magnesium, Total
Potassium, Total
Sodium, Total
Zinc, Total
11300
5580
34500
8430
3290
24500
312
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
50
50
50
50
50
50
50
473
2360
946
473
473
473
47.3
10/24/12 16:35
10/24/12 16:35
10/24/12 16:35
10/24/12 16:35
10/24/12 16:35
10/24/12 16:35
10/24/12 16:35
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
PD
PD
PD
PD
PD
PD
PD
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 27%
D
MDL
70.1
288.
97.5
58.3
71.5
40.6
12.3
Serial_No:11051209:46
Page 159 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
HB007SG-000015-20121006Client ID:10/06/12 10:45Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-15Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Antimony, Total
Silver, Total
0.635
1.87
mg/kg
mg/kg
2
2
0.099
0.099
10/24/12 19:35
10/24/12 19:35
1,6020A
1,6020A
PD
PD
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 25%
MDL
0.018
0.005
Serial_No:11051209:46
Page 160 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
HB007SG-000015-20121006Client ID:10/06/12 10:45Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-15Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Tin, Total 19.3 mg/kg 210.9 10/31/12 15:34 1,6020A PD10/30/12 15:23 EPA 3050B
PrepMethod
Percent Solids: 25%
R
MDL
1.10
Serial_No:11051209:46
Page 161 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
HB007SG-000015-20121006Client ID:10/06/12 10:45Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-15Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Arsenic, Total
Barium, Total
Beryllium, Total
Cadmium, Total
Chromium, Total
Cobalt, Total
Copper, Total
Lead, Total
Manganese, Total
Nickel, Total
Selenium, Total
Thallium, Total
Vanadium, Total
16.1
40.8
0.715
1.93
52.8
9.32
136
147
215
28.6
3.00
0.442
63.3
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
10
10
10
10
10
10
10
10
10
10
10
10
10
0.478
2.87
0.287
0.191
1.91
0.478
1.91
0.573
1.91
0.956
0.956
0.191
0.956
10/24/12 17:48
10/24/12 17:48
10/24/12 17:48
10/24/12 17:48
10/24/12 17:48
10/24/12 17:48
10/24/12 17:48
10/24/12 17:48
10/24/12 17:48
10/24/12 17:48
10/24/12 17:48
10/24/12 17:48
10/24/12 17:48
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 25%
D2
MDL
0.059
0.734
0.083
0.025
0.448
0.050
0.108
0.184
0.425
0.143
0.238
0.026
0.044
Serial_No:11051209:46
Page 162 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
HB007SG-000015-20121006Client ID:10/06/12 10:45Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-15Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Aluminum, Total
Calcium, Total
Iron, Total
Magnesium, Total
Potassium, Total
Sodium, Total
Zinc, Total
12600
5900
34200
9620
3750
27200
373
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
50
50
50
50
50
50
50
478
2390
956
478
478
478
47.8
10/24/12 16:36
10/24/12 16:36
10/24/12 16:36
10/24/12 16:36
10/24/12 16:36
10/24/12 16:36
10/24/12 16:36
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
PD
PD
PD
PD
PD
PD
PD
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 25%
D
MDL
70.8
291.
98.5
58.9
72.2
41.1
12.4
Serial_No:11051209:46
Page 163 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
HB006SG-000015-20121006Client ID:10/06/12 11:30Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-17Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Antimony, Total
Silver, Total
0.166
0.459
mg/kg
mg/kg
2
2
0.074
0.074
10/24/12 19:36
10/24/12 19:36
1,6020A
1,6020A
PD
PD
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 34%
MDL
0.013
0.003
Serial_No:11051209:46
Page 164 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
HB006SG-000015-20121006Client ID:10/06/12 11:30Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-17Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Tin, Total J4.47 mg/kg 26.69 10/31/12 15:35 1,6020A PD10/30/12 15:23 EPA 3050B
PrepMethod
Percent Solids: 34%
R
MDL
0.675
Serial_No:11051209:46
Page 165 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
HB006SG-000015-20121006Client ID:10/06/12 11:30Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-17Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Arsenic, Total
Barium, Total
Beryllium, Total
Cadmium, Total
Chromium, Total
Cobalt, Total
Copper, Total
Lead, Total
Manganese, Total
Nickel, Total
Selenium, Total
Thallium, Total
Vanadium, Total
14.2
24.8
0.671
0.516
37.5
8.55
39.5
38.8
234
21.8
1.60
0.213
44.2
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
10
10
10
10
10
10
10
10
10
10
10
10
10
0.352
2.11
0.211
0.141
1.41
0.352
1.41
0.422
1.41
0.704
0.704
0.141
0.704
10/24/12 17:50
10/24/12 17:50
10/24/12 17:50
10/24/12 17:50
10/24/12 17:50
10/24/12 17:50
10/24/12 17:50
10/24/12 17:50
10/24/12 17:50
10/24/12 17:50
10/24/12 17:50
10/24/12 17:50
10/24/12 17:50
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 34%
D2
MDL
0.044
0.541
0.061
0.019
0.330
0.037
0.080
0.136
0.313
0.106
0.175
0.019
0.032
Serial_No:11051209:46
Page 166 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
HB006SG-000015-20121006Client ID:10/06/12 11:30Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-17Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Aluminum, Total
Calcium, Total
Iron, Total
Magnesium, Total
Potassium, Total
Sodium, Total
Zinc, Total
11100
2710
32400
6660
2940
16500
116
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
50
50
50
50
50
50
50
352
1760
704
352
352
352
35.2
10/24/12 16:37
10/24/12 16:37
10/24/12 16:37
10/24/12 16:37
10/24/12 16:37
10/24/12 16:37
10/24/12 16:37
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
PD
PD
PD
PD
PD
PD
PD
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 34%
D
MDL
52.2
214.
72.6
43.4
53.2
30.3
9.15
Serial_No:11051209:46
Page 167 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
HB005SG-000015-20121006Client ID:10/06/12 12:19Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-19Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Antimony, Total
Silver, Total
0.531
1.93
mg/kg
mg/kg
2
2
0.095
0.095
10/24/12 19:37
10/24/12 19:37
1,6020A
1,6020A
PD
PD
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 26%
MDL
0.017
0.004
Serial_No:11051209:46
Page 168 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
HB005SG-000015-20121006Client ID:10/06/12 12:19Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-19Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Tin, Total 12.1 mg/kg 29.56 10/31/12 15:36 1,6020A PD10/30/12 15:23 EPA 3050B
PrepMethod
Percent Solids: 26%
R
MDL
0.965
Serial_No:11051209:46
Page 169 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
HB005SG-000015-20121006Client ID:10/06/12 12:19Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-19Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Arsenic, Total
Barium, Total
Beryllium, Total
Cadmium, Total
Chromium, Total
Cobalt, Total
Copper, Total
Lead, Total
Manganese, Total
Nickel, Total
Selenium, Total
Thallium, Total
Vanadium, Total
15.2
37.7
0.673
1.62
48.7
8.37
121
127
212
25.8
2.91
0.392
62.5
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
10
10
10
10
10
10
10
10
10
10
10
10
10
0.454
2.72
0.272
0.182
1.82
0.454
1.82
0.545
1.82
0.908
0.908
0.182
0.908
10/24/12 17:52
10/24/12 17:52
10/24/12 17:52
10/24/12 17:52
10/24/12 17:52
10/24/12 17:52
10/24/12 17:52
10/24/12 17:52
10/24/12 17:52
10/24/12 17:52
10/24/12 17:52
10/24/12 17:52
10/24/12 17:52
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 26%
D2
MDL
0.056
0.697
0.079
0.024
0.426
0.048
0.102
0.175
0.404
0.136
0.226
0.025
0.042
Serial_No:11051209:46
Page 170 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
HB005SG-000015-20121006Client ID:10/06/12 12:19Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-19Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Aluminum, Total
Calcium, Total
Iron, Total
Magnesium, Total
Potassium, Total
Sodium, Total
Zinc, Total
11500
4330
34500
7960
3390
22700
328
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
50
50
50
50
50
50
50
454
2270
908
454
454
454
45.4
10/24/12 16:38
10/24/12 16:38
10/24/12 16:38
10/24/12 16:38
10/24/12 16:38
10/24/12 16:38
10/24/12 16:38
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
PD
PD
PD
PD
PD
PD
PD
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 26%
D
MDL
67.3
276.
93.6
56.0
68.6
39.0
11.8
Serial_No:11051209:46
Page 171 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
HB1005SG-000015-20121006Client ID:10/06/12 12:19Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-21Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Antimony, Total
Silver, Total
0.563
2.00
mg/kg
mg/kg
2
2
0.094
0.094
10/24/12 19:38
10/24/12 19:38
1,6020A
1,6020A
PD
PD
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 25%
MDL
0.017
0.004
Serial_No:11051209:46
Page 172 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
HB1005SG-000015-20121006Client ID:10/06/12 12:19Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-21Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Tin, Total 24.6 mg/kg 219.8 10/31/12 15:38 1,6020A PD10/30/12 15:23 EPA 3050B
PrepMethod
Percent Solids: 25%
R
MDL
2.00
Serial_No:11051209:46
Page 173 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
HB1005SG-000015-20121006Client ID:10/06/12 12:19Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-21Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Arsenic, Total
Barium, Total
Beryllium, Total
Cadmium, Total
Chromium, Total
Cobalt, Total
Copper, Total
Lead, Total
Manganese, Total
Nickel, Total
Selenium, Total
Thallium, Total
Vanadium, Total
15.4
38.1
0.597
1.66
48.5
8.75
123
134
217
27.3
2.78
0.399
61.9
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
10
10
10
10
10
10
10
10
10
10
10
10
10
0.494
2.96
0.296
0.197
1.97
0.494
1.97
0.592
1.97
0.987
0.987
0.197
0.987
10/24/12 17:54
10/24/12 17:54
10/24/12 17:54
10/24/12 17:54
10/24/12 17:54
10/24/12 17:54
10/24/12 17:54
10/24/12 17:54
10/24/12 17:54
10/24/12 17:54
10/24/12 17:54
10/24/12 17:54
10/24/12 17:54
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 25%
D2
MDL
0.061
0.758
0.086
0.026
0.463
0.052
0.112
0.190
0.439
0.148
0.246
0.027
0.045
Serial_No:11051209:46
Page 174 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
HB1005SG-000015-20121006Client ID:10/06/12 12:19Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-21Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Aluminum, Total
Calcium, Total
Iron, Total
Magnesium, Total
Potassium, Total
Sodium, Total
Zinc, Total
11200
4250
33700
8140
3490
23200
328
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
50
50
50
50
50
50
50
494
2470
987
494
494
494
49.4
10/24/12 16:39
10/24/12 16:39
10/24/12 16:39
10/24/12 16:39
10/24/12 16:39
10/24/12 16:39
10/24/12 16:39
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
PD
PD
PD
PD
PD
PD
PD
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 25%
D
MDL
73.2
300.
102.
60.9
74.6
42.4
12.8
Serial_No:11051209:46
Page 175 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
HB004SG-000015-20121006Client ID:10/06/12 13:27Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-23Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Antimony, Total
Silver, Total
0.326
1.56
mg/kg
mg/kg
2
2
0.067
0.067
10/24/12 19:40
10/24/12 19:40
1,6020A
1,6020A
PD
PD
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 35%
MDL
0.012
0.003
Serial_No:11051209:46
Page 176 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
HB004SG-000015-20121006Client ID:10/06/12 13:27Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-23Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Tin, Total 11.2 mg/kg 26.94 10/31/12 15:39 1,6020A PD10/30/12 15:23 EPA 3050B
PrepMethod
Percent Solids: 35%
R
MDL
0.701
Serial_No:11051209:46
Page 177 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
HB004SG-000015-20121006Client ID:10/06/12 13:27Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-23Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Arsenic, Total
Barium, Total
Beryllium, Total
Cadmium, Total
Chromium, Total
Cobalt, Total
Copper, Total
Lead, Total
Manganese, Total
Nickel, Total
Selenium, Total
Thallium, Total
Vanadium, Total
12.9
26.0
0.506
1.31
37.4
7.05
87.6
97.7
178
22.6
2.34
0.282
44.4
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
10
10
10
10
10
10
10
10
10
10
10
10
10
0.360
2.16
0.216
0.144
1.44
0.360
1.44
0.431
1.44
0.719
0.719
0.144
0.719
10/24/12 17:59
10/24/12 17:59
10/24/12 17:59
10/24/12 17:59
10/24/12 17:59
10/24/12 17:59
10/24/12 17:59
10/24/12 17:59
10/24/12 17:59
10/24/12 17:59
10/24/12 17:59
10/24/12 17:59
10/24/12 17:59
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 35%
D2
MDL
0.044
0.552
0.063
0.019
0.337
0.038
0.081
0.139
0.320
0.108
0.179
0.019
0.033
Serial_No:11051209:46
Page 178 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
HB004SG-000015-20121006Client ID:10/06/12 13:27Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-23Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Aluminum, Total
Calcium, Total
Iron, Total
Magnesium, Total
Potassium, Total
Sodium, Total
Zinc, Total
7950
15000
26000
5750
2280
16300
217
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
50
50
50
50
50
50
50
360
1800
719
360
360
360
36.0
10/24/12 16:43
10/24/12 16:43
10/24/12 16:43
10/24/12 16:43
10/24/12 16:43
10/24/12 16:43
10/24/12 16:43
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
PD
PD
PD
PD
PD
PD
PD
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 35%
D
MDL
53.3
219.
74.1
44.3
54.3
30.9
9.34
Serial_No:11051209:46
Page 179 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
HB003SG-000015-20121006Client ID:10/06/12 14:21Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-25Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Antimony, Total
Silver, Total
0.464
1.80
mg/kg
mg/kg
2
2
0.086
0.086
10/24/12 19:41
10/24/12 19:41
1,6020A
1,6020A
PD
PD
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 28%
MDL
0.015
0.004
Serial_No:11051209:46
Page 180 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
HB003SG-000015-20121006Client ID:10/06/12 14:21Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-25Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Tin, Total 11.6 mg/kg 29.13 10/31/12 15:40 1,6020A PD10/30/12 15:23 EPA 3050B
PrepMethod
Percent Solids: 28%
R
MDL
0.921
Serial_No:11051209:46
Page 181 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
HB003SG-000015-20121006Client ID:10/06/12 14:21Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-25Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Arsenic, Total
Barium, Total
Beryllium, Total
Cadmium, Total
Chromium, Total
Cobalt, Total
Copper, Total
Lead, Total
Manganese, Total
Nickel, Total
Selenium, Total
Thallium, Total
Vanadium, Total
14.8
36.6
0.665
1.37
49.6
8.83
112
120
235
26.7
2.96
0.366
57.9
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
10
10
10
10
10
10
10
10
10
10
10
10
10
0.473
2.84
0.284
0.189
1.89
0.473
1.89
0.568
1.89
0.947
0.947
0.189
0.947
10/24/12 18:01
10/24/12 18:01
10/24/12 18:01
10/24/12 18:01
10/24/12 18:01
10/24/12 18:01
10/24/12 18:01
10/24/12 18:01
10/24/12 18:01
10/24/12 18:01
10/24/12 18:01
10/24/12 18:01
10/24/12 18:01
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 28%
D2
MDL
0.059
0.727
0.082
0.025
0.444
0.050
0.107
0.183
0.421
0.142
0.236
0.026
0.043
Serial_No:11051209:46
Page 182 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
HB003SG-000015-20121006Client ID:10/06/12 14:21Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-25Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Aluminum, Total
Calcium, Total
Iron, Total
Magnesium, Total
Potassium, Total
Sodium, Total
Zinc, Total
10600
4510
31700
7430
3200
21400
270
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
50
50
50
50
50
50
50
473
2370
947
473
473
473
47.3
10/24/12 16:44
10/24/12 16:44
10/24/12 16:44
10/24/12 16:44
10/24/12 16:44
10/24/12 16:44
10/24/12 16:44
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
PD
PD
PD
PD
PD
PD
PD
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 28%
D
MDL
70.2
288.
97.6
58.4
71.5
40.7
12.3
Serial_No:11051209:46
Page 183 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
HB002SG-000015-20121006Client ID:10/06/12 15:05Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-27Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Antimony, Total
Silver, Total
0.284
1.46
mg/kg
mg/kg
2
2
0.069
0.069
10/24/12 19:42
10/24/12 19:42
1,6020A
1,6020A
PD
PD
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 34%
MDL
0.012
0.003
Serial_No:11051209:46
Page 184 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
HB002SG-000015-20121006Client ID:10/06/12 15:05Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-27Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Tin, Total 10.1 mg/kg 27.24 10/31/12 15:41 1,6020A PD10/30/12 15:23 EPA 3050B
PrepMethod
Percent Solids: 34%
R
MDL
0.731
Serial_No:11051209:46
Page 185 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
HB002SG-000015-20121006Client ID:10/06/12 15:05Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-27Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Arsenic, Total
Barium, Total
Beryllium, Total
Cadmium, Total
Chromium, Total
Cobalt, Total
Copper, Total
Lead, Total
Manganese, Total
Nickel, Total
Selenium, Total
Thallium, Total
Vanadium, Total
13.3
29.3
0.630
1.00
43.7
7.46
82.2
89.0
219
22.3
2.37
0.278
47.0
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
10
10
10
10
10
10
10
10
10
10
10
10
10
0.350
2.10
0.210
0.140
1.40
0.350
1.40
0.420
1.40
0.701
0.701
0.140
0.701
10/24/12 18:03
10/24/12 18:03
10/24/12 18:03
10/24/12 18:03
10/24/12 18:03
10/24/12 18:03
10/24/12 18:03
10/24/12 18:03
10/24/12 18:03
10/24/12 18:03
10/24/12 18:03
10/24/12 18:03
10/24/12 18:03
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 34%
D2
MDL
0.043
0.538
0.061
0.019
0.329
0.037
0.079
0.135
0.312
0.105
0.174
0.019
0.032
Serial_No:11051209:46
Page 186 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
HB002SG-000015-20121006Client ID:10/06/12 15:05Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-27Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Aluminum, Total
Calcium, Total
Iron, Total
Magnesium, Total
Potassium, Total
Sodium, Total
Zinc, Total
9520
4110
29400
6570
2860
17300
201
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
50
50
50
50
50
50
50
350
1750
701
350
350
350
35.0
10/24/12 16:45
10/24/12 16:45
10/24/12 16:45
10/24/12 16:45
10/24/12 16:45
10/24/12 16:45
10/24/12 16:45
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
PD
PD
PD
PD
PD
PD
PD
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 34%
D
MDL
52.0
213.
72.2
43.2
53.0
30.1
9.10
Serial_No:11051209:46
Page 187 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
HB001SG-000015-20121006Client ID:10/06/12 15:54Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-29Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Antimony, Total
Silver, Total
0.285
1.43
mg/kg
mg/kg
2
2
0.078
0.078
10/24/12 19:43
10/24/12 19:43
1,6020A
1,6020A
PD
PD
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 30%
MDL
0.014
0.004
Serial_No:11051209:46
Page 188 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
HB001SG-000015-20121006Client ID:10/06/12 15:54Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-29Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Tin, Total 10.3 mg/kg 27.70 10/31/12 15:42 1,6020A PD10/30/12 15:23 EPA 3050B
PrepMethod
Percent Solids: 30%
R
MDL
0.777
Serial_No:11051209:46
Page 189 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
HB001SG-000015-20121006Client ID:10/06/12 15:54Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-29Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Arsenic, Total
Barium, Total
Beryllium, Total
Cadmium, Total
Chromium, Total
Cobalt, Total
Copper, Total
Lead, Total
Manganese, Total
Nickel, Total
Selenium, Total
Thallium, Total
Vanadium, Total
14.6
34.2
0.663
1.12
49.1
8.67
96.1
105
262
26.3
2.85
0.322
52.7
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
10
10
10
10
10
10
10
10
10
10
10
10
10
0.424
2.54
0.254
0.169
1.69
0.424
1.69
0.508
1.69
0.847
0.847
0.169
0.847
10/24/12 18:04
10/24/12 18:04
10/24/12 18:04
10/24/12 18:04
10/24/12 18:04
10/24/12 18:04
10/24/12 18:04
10/24/12 18:04
10/24/12 18:04
10/24/12 18:04
10/24/12 18:04
10/24/12 18:04
10/24/12 18:04
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 30%
D2
MDL
0.052
0.651
0.074
0.022
0.397
0.045
0.096
0.164
0.377
0.127
0.211
0.023
0.039
Serial_No:11051209:46
Page 190 of 279
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
SAMPLE RESULTS
HB001SG-000015-20121006Client ID:10/06/12 15:54Date Collected:10/08/12Date Received:
Matrix: SedimentNot SpecifiedSample Location:
L1218042-29Lab ID:
Field Prep: Not Specified
Parameter ResultDilution FactorQualifier Units RL
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
Total Metals - Mansfield Lab
Aluminum, Total
Calcium, Total
Iron, Total
Magnesium, Total
Potassium, Total
Sodium, Total
Zinc, Total
10800
4770
32900
7970
3260
22100
232
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
50
50
50
50
50
50
50
424
2120
847
424
424
424
42.4
10/24/12 16:46
10/24/12 16:46
10/24/12 16:46
10/24/12 16:46
10/24/12 16:46
10/24/12 16:46
10/24/12 16:46
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
PD
PD
PD
PD
PD
PD
PD
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
EPA 3050B
PrepMethod
Percent Solids: 30%
D
MDL
62.8
258.
87.3
52.3
64.0
36.4
11.0
Serial_No:11051209:46
Page 191 of 279
FF
Parameter
Parameter
Result
Result
Dilution Factor
Dilution Factor
Qualifier
Qualifier
Units
Units
RL
RL
Method Blank AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
DateAnalyzed
DateAnalyzed
AnalyticalMethod
AnalyticalMethod
Analyst
Analyst
Date Prepared
Date Prepared
11/05/12
Aluminum, Total
Antimony, Total
Arsenic, Total
Barium, Total
Beryllium, Total
Cadmium, Total
Calcium, Total
Chromium, Total
Cobalt, Total
Copper, Total
Iron, Total
Lead, Total
Magnesium, Total
Manganese, Total
Nickel, Total
Potassium, Total
Selenium, Total
Silver, Total
Sodium, Total
Thallium, Total
Tin, Total
Vanadium, Total
Zinc, Total
Antimony, Total
Silver, Total
J
J
J
J
J
J
J
J
J
J
J
ND
ND
0.0001
0.0001
ND
ND
ND
ND
ND
0.0003
0.009
ND
0.013
0.0004
0.0003
ND
ND
ND
0.017
0.00003
ND
0.001
0.003
ND
ND
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/l
mg/kg
mg/kg
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
2
2
0.100
0.0005
0.0005
0.0005
0.0005
0.0005
0.100
0.001
0.0002
0.0010
0.050
0.001
0.070
0.0005
0.0005
0.100
0.005
0.0003
0.100
0.00020
0.0005
0.005
0.010
0.050
0.050
10/23/12 18:02
10/23/12 18:02
10/23/12 18:02
10/23/12 18:02
10/23/12 18:02
10/23/12 18:02
10/23/12 18:02
10/23/12 18:02
10/23/12 18:42
10/23/12 18:02
10/23/12 18:02
10/23/12 18:02
10/23/12 18:02
10/23/12 18:02
10/23/12 18:02
10/23/12 18:02
10/23/12 18:02
10/23/12 18:02
10/23/12 18:02
10/23/12 18:02
10/23/12 18:02
10/23/12 18:02
10/23/12 18:02
10/24/12 19:24
10/24/12 19:24
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
10/17/12 12:00
10/23/12 10:15
10/23/12 10:15
Total Metals - Mansfield Lab for sample(s): 11 Batch: WG567654-1
Total Metals - Mansfield Lab for sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG568938-1
EPA 3020ADigestion Method:
Prep Information
MDL
MDL
0.023
0.00003
0.0001
0.0001
0.0001
0.0001
0.019
0.0003
0.00002
0.0003
0.008
0.0001
0.002
0.0001
0.0002
0.006
0.0003
0.00002
0.006
0.00001
0.0001
0.0001
0.001
0.009
0.002
Serial_No:11051209:46
Page 192 of 279
Parameter
Parameter
Result
Result
Dilution Factor
Dilution Factor
Qualifier
Qualifier
Units
Units
RL
RL
Method Blank AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
DateAnalyzed
DateAnalyzed
AnalyticalMethod
AnalyticalMethod
Analyst
Analyst
Date Prepared
Date Prepared
11/05/12
Aluminum, Total
Arsenic, Total
Barium, Total
Beryllium, Total
Cadmium, Total
Calcium, Total
Chromium, Total
Cobalt, Total
Copper, Total
Iron, Total
Lead, Total
Magnesium, Total
Manganese, Total
Nickel, Total
Potassium, Total
Selenium, Total
Sodium, Total
Thallium, Total
Vanadium, Total
Zinc, Total
Tin, Total
J
J
J
J
J
J
J
J
J
J
ND
0.014
ND
ND
ND
ND
ND
ND
0.039
2.96
ND
ND
0.068
0.041
2.20
ND
3.39
0.004
0.108
0.388
1.54
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
2
10.0
0.050
0.300
0.030
0.020
50.0
0.200
0.050
0.200
20.0
0.060
10.0
0.200
0.100
10.0
0.100
10.0
0.020
0.100
1.00
5.00
10/24/12 16:22
10/24/12 17:26
10/24/12 17:26
10/24/12 17:26
10/24/12 17:26
10/24/12 16:22
10/24/12 17:26
10/24/12 17:26
10/24/12 17:26
10/24/12 16:22
10/24/12 17:26
10/24/12 16:22
10/24/12 17:26
10/24/12 17:26
10/24/12 16:22
10/24/12 17:26
10/24/12 16:22
10/24/12 17:26
10/24/12 17:26
10/24/12 16:22
10/31/12 15:23
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
1,6020A
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
PD
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/23/12 10:15
10/30/12 15:23
Total Metals - Mansfield Lab for sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG568940-1
Total Metals - Mansfield Lab for sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG570724-1
EPA 3050B
EPA 3050B
Digestion Method:
Digestion Method:
Prep Information
Prep Information
MDL
MDL
1.48
0.006
0.077
0.009
0.003
6.08
0.047
0.005
0.011
2.06
0.019
1.23
0.045
0.015
1.51
0.025
0.860
0.003
0.005
0.260
0.505
Serial_No:11051209:46
Page 193 of 279
Method Blank AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
EPA 3050BDigestion Method:
Prep Information
Serial_No:11051209:46
Page 194 of 279
Aluminum, Total
Antimony, Total
Arsenic, Total
Barium, Total
Beryllium, Total
Cadmium, Total
Calcium, Total
Chromium, Total
Cobalt, Total
Copper, Total
Iron, Total
Lead, Total
Magnesium, Total
Manganese, Total
Nickel, Total
Potassium, Total
Selenium, Total
Sodium, Total
Thallium, Total
Tin, Total
Vanadium, Total
94
92
91
92
87
89
94
90
105
94
90
92
94
90
92
93
87
92
90
88
94
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
80-120
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
ParameterLCS
%RecoveryLCSD
%Recovery%Recovery
Limits RPD RPD Limits
Total Metals - Mansfield Lab Associated sample(s): 11 Batch: WG567654-2 SRM Lot Number: A2METSPIKE
Lab Control Sample AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
Qual Qual Qual
Serial_No:11051209:46
Page 195 of 279
Zinc, Total
Silver, Total
Antimony, Total
Silver, Total
94
91
105
104
-
-
-
-
80-120
80-120
75-125
75-125
-
-
-
-
20
20
20
20
ParameterLCS
%RecoveryLCSD
%Recovery%Recovery
Limits RPD RPD Limits
Total Metals - Mansfield Lab Associated sample(s): 11 Batch: WG567654-2 SRM Lot Number: A2METSPIKE
Total Metals - Mansfield Lab Associated sample(s): 11 Batch: WG567654-3 SRM Lot Number: S3SPIKE
Total Metals - Mansfield Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG568938-2 SRM Lot Number: S3SPIKE
Lab Control Sample AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
Serial_No:11051209:46
Page 196 of 279
Aluminum, Total
Arsenic, Total
Barium, Total
Beryllium, Total
Cadmium, Total
Calcium, Total
Chromium, Total
Cobalt, Total
Copper, Total
Iron, Total
Lead, Total
Magnesium, Total
Manganese, Total
Nickel, Total
Potassium, Total
Selenium, Total
Sodium, Total
Thallium, Total
Vanadium, Total
Zinc, Total
107
92
88
98
97
103
96
103
98
99
95
108
100
97
100
92
107
94
101
103
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
ParameterLCS
%RecoveryLCSD
%Recovery%Recovery
Limits RPD RPD Limits
Total Metals - Mansfield Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG568940-2 SRM Lot Number: A2METSPIKE
Lab Control Sample AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
Serial_No:11051209:46
Page 197 of 279
Tin, Total 112 - 75-125 - 20
ParameterLCS
%RecoveryLCSD
%Recovery%Recovery
Limits RPD RPD Limits
Total Metals - Mansfield Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG570724-2 SRM Lot Number: S3SPIKE
Lab Control Sample AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
Serial_No:11051209:46
Page 198 of 279
Antimony, Total
Silver, Total
0.062
0.682
0.398
1.97
25
96
-
-
-
-
75-125
75-125
-
-
20
20
ParameterNative Sample
MS Found
MS%Recovery
MSD Found
MSD %Recovery
RecoveryLimits RPD
RPD Limits
Total Metals - Mansfield Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 QC Batch ID: WG568938-4 QC Sample: L1218042-01 Client ID: TN005SG-000014-20121005
1.34
1.34
MS Added
Matrix Spike AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
Qual
Q
Qual Qual
Serial_No:11051209:46
Page 199 of 279
Aluminum, Total
Arsenic, Total
Barium, Total
Beryllium, Total
Cadmium, Total
Calcium, Total
Chromium, Total
Cobalt, Total
Copper, Total
Iron, Total
Lead, Total
Magnesium, Total
Manganese, Total
Nickel, Total
Potassium, Total
Selenium, Total
Sodium, Total
Thallium, Total
Vanadium, Total
Zinc, Total
2960
5.18
14.8
0.288
1.06
15800
18.6
3.68
27.8
6940
34.7
2660
161.
9.90
896.
1.98
3760
0.509
9.88
54.2
4100
120
127
61.4
61.0
20600
139
133
155
9390
155
3420
303
138
1590
118
4520
116
135
190
179
90
88
96
94
752
94
101
100
384
94
119
111
100
109
91
119
90
98
106
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
75-125
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
-
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
ParameterNative Sample
MS Found
MS%Recovery
MSD Found
MSD %Recovery
RecoveryLimits RPD
RPD Limits
Total Metals - Mansfield Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 QC Batch ID: WG568940-4 QC Sample: L1218042-01 Client ID: TN005SG-000014-20121005
638
128
128
63.8
63.8
638
128
128
128
638
128
638
128
128
638
128
638
128
128
128
MS Added
Matrix Spike AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
Q
Q
Q
Serial_No:11051209:46
Page 200 of 279
Tin, Total 5.14 22.5 98 - - 75-125 - 20
ParameterNative Sample
MS Found
MS%Recovery
MSD Found
MSD %Recovery
RecoveryLimits RPD
RPD Limits
Total Metals - Mansfield Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 QC Batch ID: WG570724-4 QC Sample: L1218042-01 Client ID: TN005SG-000014-20121005
17.6
MS Added
Matrix Spike AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
Serial_No:11051209:46
Page 201 of 279
Antimony, Total
Silver, Total
Aluminum, Total
Calcium, Total
Iron, Total
Magnesium, Total
Potassium, Total
Sodium, Total
Zinc, Total
0.062
0.682
2960
15800
6940
2660
896.
3760
54.2
0.052
0.603
2910
31200
7190
2610
882
3920
70.7
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
18
12
2
66
4
2
2
4
26
20
20
20
20
20
20
20
20
20
Units RPDParameter Native Sample Duplicate Sample RPD Limits
Total Metals - Mansfield Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 QC Batch ID: WG568938-3 QC Sample: L1218042-01 ClientID: TN005SG-000014-20121005
Total Metals - Mansfield Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 QC Batch ID: WG568940-3 QC Sample: L1218042-01 ClientID: TN005SG-000014-20121005
NEWTOWN CREEK RI
120782-01.01
Project Name:
Project Number:
L1218042Lab Number:
Report Date:
Lab Duplicate AnalysisBatch Quality Control
11/05/12
Qual
Q
Q
Serial_No:11051209:46
Page 202 of 279
Arsenic, Total
Barium, Total
Beryllium, Total
Cadmium, Total
Chromium, Total
Cobalt, Total
Copper, Total
Lead, Total
Manganese, Total
Nickel, Total
Selenium, Total
Thallium, Total
Vanadium, Total
Tin, Total
5.18
14.8
0.288
1.06
18.6
3.68
27.8
34.7
161.
9.90
1.98
0.509
9.88
5.14
4.87
52.7
0.166
0.366
18.4
3.43
29.4
95.2
171
9.15
0.424
0.094
9.84
4.32
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
6
112
54
97
1
7
6
93
6
8
129
138
0
17
20
20
20
20
20
20
20
20
20
20
20
20
20
20
Units RPDParameter Native Sample Duplicate Sample RPD Limits
Total Metals - Mansfield Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 QC Batch ID: WG568940-3 QC Sample: L1218042-01 ClientID: TN005SG-000014-20121005
Total Metals - Mansfield Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 QC Batch ID: WG570724-3 QC Sample: L1218042-01 ClientID: TN005SG-000014-20121005
NEWTOWN CREEK RI
120782-01.01
Project Name:
Project Number:
L1218042Lab Number:
Report Date:
Lab Duplicate AnalysisBatch Quality Control
11/05/12
Q
Q
Q
Q
Q
Q
Serial_No:11051209:46
Page 203 of 279
Aluminum, Total
Calcium, Total
Iron, Total
Magnesium, Total
Sodium, Total
Arsenic, Total
Barium, Total
Chromium, Total
Cobalt, Total
Copper, Total
Lead, Total
Manganese, Total
Nickel, Total
Vanadium, Total
2960
15800
6940
2660
3760
5.18
14.8
18.6
3.68
27.8
34.7
161.
9.90
9.88
2730
15800
7210
2460
3630
4.92
14.7
17.5
3.42
27.8
36.2
158
9.96
10.2
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
8
0
4
8
3
5
1
6
7
0
4
2
1
3
10
10
10
10
10
10
10
10
10
10
10
10
10
10
Units % DParameter Native Sample Serial Dilution RPD Limits
Total Metals - Mansfield Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 QC Batch ID: WG568940-5 QC Sample: L1218042-01 ClientID: TN005SG-000014-20121005
Total Metals - Mansfield Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 QC Batch ID: WG568940-5 QC Sample: L1218042-01 ClientID: TN005SG-000014-20121005
NEWTOWN CREEK RI
120782-01.01
Project Name:
Project Number:
L1218042Lab Number:
Report Date:
Lab Serial Dilution Analysis
Batch Quality Control 11/05/12
Qual
Serial_No:11051209:46
Page 204 of 279
INORGANICS&
MISCELLANEOUS
Serial_No:11051209:46
Page 205 of 279
FF
TN005SG-000014-20121005Client ID:10/05/12 09:32Date Collected:10/08/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1218042-01Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
Total Organic Carbon - Mansfield Lab
General Chemistry - Westborough Lab
General Chemistry - Mansfield Lab
Total Organic Carbon (Rep1)
Total Organic Carbon (Rep2)
Cyanide, Total
pH
Nitrogen, Ammonia
Nitrogen, Nitrate/Nitrite
Nitrogen, Total Kjeldahl
Solids, Total
% Soot (Rep 1)
% Soot (Rep 2)
0.522
0.601
ND
8.0
13
3.7
640
71.9
0.162
0.163
%
%
mg/kg
SU
mg/kg
mg/kg
mg/kg
%
%
%
1
1
1
1
1
1
1
1
1
1
0.010
0.010
1.3
-
10
2.3
190
0.100
0.010
0.010
10/24/12 07:14
10/24/12 07:14
10/18/12 15:39
10/10/12 14:30
10/18/12 21:42
10/16/12 03:35
10/18/12 22:06
10/09/12 16:25
10/24/12 07:14
10/24/12 07:14
1,9060
1,9060
1,9010B/9012A
1,9045C
30,4500NH3-BH
30,4500NO3-F
30,4500N-C
30,2540G
91,-
91,-
NR
NR
JO
ML
AT
DB
AT
KB
NR
NR
Date Prepared
-
-
10/16/12 15:00
-
10/16/12 14:45
10/15/12 01:00
10/16/12 23:45
-
-
-
11/05/12
MDL
0.010
0.010
0.30
NA
1.8
0.39
74.
0.100
NA
NA
Serial_No:11051209:46
Page 206 of 279
FF
TN005SG-000014-20121005Client ID:10/05/12 09:32Date Collected:10/08/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1218042-01Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
General Chemistry - Westborough LabPhosphorus, Total
Sulfide
110
230
mg/kg
mg/kg
1.8
100
12
70
10/18/12 11:00
10/10/12 14:30
30,4500P-E
1,9030B
SD
MP
Date Prepared
-
10/10/12 12:45
11/05/12
D
MDL
3.5
16.
Serial_No:11051209:46
Page 207 of 279
FF
TN002SG-000011-20121005Client ID:10/05/12 10:41Date Collected:10/08/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1218042-03Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
Total Organic Carbon - Mansfield Lab
General Chemistry - Westborough Lab
General Chemistry - Mansfield Lab
Total Organic Carbon (Rep1)
Total Organic Carbon (Rep2)
Cyanide, Total
pH
Nitrogen, Ammonia
Nitrogen, Nitrate/Nitrite
Nitrogen, Total Kjeldahl
Solids, Total
% Soot (Rep 1)
% Soot (Rep 2)
2.05
1.60
ND
7.8
15
6.0
1600
55.4
0.689
0.899
%
%
mg/kg
SU
mg/kg
mg/kg
mg/kg
%
%
%
1
1
1
1
1
1
1
1
1
1
0.010
0.010
1.8
-
13
3.0
250
0.100
0.010
0.010
10/24/12 07:14
10/24/12 07:14
10/18/12 15:40
10/10/12 14:30
10/18/12 21:43
10/16/12 03:39
10/18/12 22:07
10/09/12 16:25
10/24/12 07:14
10/24/12 07:14
1,9060
1,9060
1,9010B/9012A
1,9045C
30,4500NH3-BH
30,4500NO3-F
30,4500N-C
30,2540G
91,-
91,-
NR
NR
JO
ML
AT
DB
AT
KB
NR
NR
Date Prepared
-
-
10/16/12 15:00
-
10/16/12 14:45
10/15/12 01:00
10/16/12 23:45
-
-
-
11/05/12
MDL
0.010
0.010
0.41
NA
2.4
0.51
96.
0.100
NA
NA
Serial_No:11051209:46
Page 208 of 279
FF
TN002SG-000011-20121005Client ID:10/05/12 10:41Date Collected:10/08/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1218042-03Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
General Chemistry - Westborough LabPhosphorus, Total
Sulfide
320
480
mg/kg
mg/kg
4.6
100
42
90
10/18/12 11:00
10/10/12 14:32
30,4500P-E
1,9030B
SD
MP
Date Prepared
-
10/10/12 12:45
11/05/12
D
MDL
12.
20.
Serial_No:11051209:46
Page 209 of 279
FF
TN003SG-000015-20121005Client ID:10/05/12 11:24Date Collected:10/08/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1218042-05Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
Total Organic Carbon - Mansfield Lab
General Chemistry - Westborough Lab
General Chemistry - Mansfield Lab
Total Organic Carbon (Rep1)
Total Organic Carbon (Rep2)
Cyanide, Total
pH
Nitrogen, Ammonia
Nitrogen, Nitrate/Nitrite
Nitrogen, Total Kjeldahl
Solids, Total
% Soot (Rep 1)
% Soot (Rep 2)
2.68
2.49
ND
7.8
26
6.4
3000
41.4
0.599
0.581
%
%
mg/kg
SU
mg/kg
mg/kg
mg/kg
%
%
%
1
1
1
1
1
1
1
1
1
1
0.010
0.010
2.4
-
18
4.0
350
0.100
0.010
0.010
10/24/12 07:14
10/24/12 07:14
10/18/12 15:41
10/10/12 14:30
10/18/12 21:44
10/16/12 03:40
10/18/12 22:08
10/09/12 16:25
10/24/12 07:14
10/24/12 07:14
1,9060
1,9060
1,9010B/9012A
1,9045C
30,4500NH3-BH
30,4500NO3-F
30,4500N-C
30,2540G
91,-
91,-
NR
NR
JO
ML
AT
DB
AT
KB
NR
NR
Date Prepared
-
-
10/16/12 15:00
-
10/16/12 14:45
10/15/12 01:00
10/16/12 23:45
-
-
-
11/05/12
MDL
0.010
0.010
0.55
NA
3.2
0.68
140
0.100
NA
NA
Serial_No:11051209:46
Page 210 of 279
FF
TN003SG-000015-20121005Client ID:10/05/12 11:24Date Collected:10/08/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1218042-05Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
General Chemistry - Westborough LabPhosphorus, Total
Sulfide
540
2500
mg/kg
mg/kg
4.9
100
59
120
10/18/12 11:00
10/10/12 14:32
30,4500P-E
1,9030B
SD
MP
Date Prepared
-
10/10/12 12:45
11/05/12
D
MDL
17.
27.
Serial_No:11051209:46
Page 211 of 279
FF
TN004SG-000015-20121005Client ID:10/05/12 11:46Date Collected:10/08/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1218042-07Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
Total Organic Carbon - Mansfield Lab
General Chemistry - Westborough Lab
General Chemistry - Mansfield Lab
Total Organic Carbon (Rep1)
Total Organic Carbon (Rep2)
Cyanide, Total
pH
Nitrogen, Ammonia
Nitrogen, Nitrate/Nitrite
Nitrogen, Total Kjeldahl
Solids, Total
% Soot (Rep 1)
% Soot (Rep 2)
1.29
1.20
ND
7.9
16
6.2
1500
50.5
0.338
0.208
%
%
mg/kg
SU
mg/kg
mg/kg
mg/kg
%
%
%
1
1
1
1
1
1
1
1
1
1
0.010
0.010
1.8
-
14
3.3
290
0.100
0.010
0.010
10/24/12 07:14
10/24/12 07:14
10/18/12 15:43
10/10/12 14:30
10/18/12 21:45
10/16/12 03:41
10/18/12 22:09
10/09/12 16:25
10/24/12 07:14
10/24/12 07:14
1,9060
1,9060
1,9010B/9012A
1,9045C
30,4500NH3-BH
30,4500NO3-F
30,4500N-C
30,2540G
91,-
91,-
NR
NR
JO
ML
AT
DB
AT
KB
NR
NR
Date Prepared
-
-
10/16/12 15:00
-
10/16/12 14:45
10/15/12 01:00
10/16/12 23:45
-
-
-
11/05/12
MDL
0.010
0.010
0.43
NA
2.4
0.56
110
0.100
NA
NA
Serial_No:11051209:46
Page 212 of 279
FF
TN004SG-000015-20121005Client ID:10/05/12 11:46Date Collected:10/08/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1218042-07Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
General Chemistry - Westborough LabPhosphorus, Total
Sulfide
400
1000
mg/kg
mg/kg
4.9
100
48
99
10/18/12 11:00
10/10/12 14:32
30,4500P-E
1,9030B
SD
MP
Date Prepared
-
10/10/12 12:45
11/05/12
D
MDL
14.
22.
Serial_No:11051209:46
Page 213 of 279
FF
TN006SG-000015-20121005Client ID:10/05/12 13:16Date Collected:10/08/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1218042-09Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
Total Organic Carbon - Mansfield Lab
General Chemistry - Westborough Lab
General Chemistry - Mansfield Lab
Total Organic Carbon (Rep1)
Total Organic Carbon (Rep2)
Cyanide, Total
pH
Nitrogen, Ammonia
Nitrogen, Nitrate/Nitrite
Nitrogen, Total Kjeldahl
Solids, Total
% Soot (Rep 1)
% Soot (Rep 2)
J
5.09
4.78
0.47
8.0
ND
2.9
360
77.8
0.047
0.047
%
%
mg/kg
SU
mg/kg
mg/kg
mg/kg
%
%
%
1
1
1
1
1
1
1
1
1
1
0.010
0.010
1.2
-
9.1
2.1
190
0.100
0.010
0.010
10/24/12 07:14
10/24/12 07:14
10/18/12 15:44
10/10/12 14:30
10/18/12 21:46
10/16/12 03:41
10/18/12 22:10
10/09/12 16:25
10/24/12 07:14
10/24/12 07:14
1,9060
1,9060
1,9010B/9012A
1,9045C
30,4500NH3-BH
30,4500NO3-F
30,4500N-C
30,2540G
91,-
91,-
NR
NR
JO
ML
AT
DB
AT
KB
NR
NR
Date Prepared
-
-
10/16/12 15:00
-
10/16/12 14:45
10/15/12 01:00
10/16/12 23:45
-
-
-
11/05/12
MDL
0.010
0.010
0.29
NA
1.6
0.36
73.
0.100
NA
NA
Serial_No:11051209:46
Page 214 of 279
FF
TN006SG-000015-20121005Client ID:10/05/12 13:16Date Collected:10/08/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1218042-09Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
General Chemistry - Westborough LabPhosphorus, Total
Sulfide
130
35
mg/kg
mg/kg
2
2
13
1.3
10/18/12 11:00
10/10/12 14:33
30,4500P-E
1,9030B
SD
MP
Date Prepared
-
10/10/12 12:45
11/05/12
D
MDL
3.6
0.29
Serial_No:11051209:46
Page 215 of 279
FF
HB008SG-000015-20121006Client ID:10/06/12 09:55Date Collected:10/08/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1218042-13Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
Total Organic Carbon - Mansfield Lab
General Chemistry - Westborough Lab
General Chemistry - Mansfield Lab
Total Organic Carbon (Rep1)
Total Organic Carbon (Rep2)
Cyanide, Total
pH
Nitrogen, Ammonia
Nitrogen, Nitrate/Nitrite
Nitrogen, Total Kjeldahl
Solids, Total
% Soot (Rep 1)
% Soot (Rep 2)
3.73
4.11
ND
7.7
120
9.8
8100
26.7
0.066
0.084
%
%
mg/kg
SU
mg/kg
mg/kg
mg/kg
%
%
%
1
1
1
1
1
1
1
1
1
1
0.010
0.010
3.6
-
28
6.2
520
0.100
0.010
0.010
10/24/12 07:14
10/24/12 07:14
10/18/12 15:44
10/10/12 14:30
10/18/12 21:46
10/16/12 03:42
10/18/12 22:11
10/09/12 16:25
10/24/12 07:14
10/24/12 07:14
1,9060
1,9060
1,9010B/9012A
1,9045C
30,4500NH3-BH
30,4500NO3-F
30,4500N-C
30,2540G
91,-
91,-
NR
NR
JO
ML
AT
DB
AT
KB
NR
NR
Date Prepared
-
-
10/16/12 15:00
-
10/16/12 14:45
10/15/12 01:00
10/16/12 23:45
-
-
-
11/05/12
MDL
0.010
0.010
0.83
NA
5.0
1.0
200
0.100
NA
NA
Serial_No:11051209:46
Page 216 of 279
FF
HB008SG-000015-20121006Client ID:10/06/12 09:55Date Collected:10/08/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1218042-13Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
General Chemistry - Westborough LabPhosphorus, Total
Sulfide
650
5500
mg/kg
mg/kg
4.7
200
88
370
10/18/12 11:00
10/10/12 14:34
30,4500P-E
1,9030B
SD
MP
Date Prepared
-
10/10/12 12:45
11/05/12
D
MDL
25.
84.
Serial_No:11051209:46
Page 217 of 279
FF
HB007SG-000015-20121006Client ID:10/06/12 10:45Date Collected:10/08/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1218042-15Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
Total Organic Carbon - Mansfield Lab
General Chemistry - Westborough Lab
General Chemistry - Mansfield Lab
Total Organic Carbon (Rep1)
Total Organic Carbon (Rep2)
Cyanide, Total
pH
Nitrogen, Ammonia
Nitrogen, Nitrate/Nitrite
Nitrogen, Total Kjeldahl
Solids, Total
% Soot (Rep 1)
% Soot (Rep 2)
4.34
4.40
ND
7.7
120
7.3
6500
25.4
0.094
0.091
%
%
mg/kg
SU
mg/kg
mg/kg
mg/kg
%
%
%
1
1
1
1
1
1
1
1
1
1
0.010
0.010
3.9
-
28
6.5
580
0.100
0.010
0.010
10/24/12 07:14
10/24/12 07:14
10/18/12 15:45
10/10/12 14:30
10/18/12 21:47
10/16/12 03:43
10/18/12 22:11
10/09/12 16:25
10/24/12 07:14
10/24/12 07:14
1,9060
1,9060
1,9010B/9012A
1,9045C
30,4500NH3-BH
30,4500NO3-F
30,4500N-C
30,2540G
91,-
91,-
NR
NR
JO
ML
AT
DB
AT
KB
NR
NR
Date Prepared
-
-
10/16/12 15:00
-
10/16/12 14:45
10/15/12 01:00
10/16/12 23:45
-
-
-
11/05/12
MDL
0.010
0.010
0.91
NA
5.1
1.1
220
0.100
NA
NA
Serial_No:11051209:46
Page 218 of 279
FF
HB007SG-000015-20121006Client ID:10/06/12 10:45Date Collected:10/08/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1218042-15Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
General Chemistry - Westborough LabPhosphorus, Total
Sulfide
680
5800
mg/kg
mg/kg
5
200
98
390
10/18/12 11:00
10/10/12 14:35
30,4500P-E
1,9030B
SD
MP
Date Prepared
-
10/10/12 12:45
11/05/12
D
MDL
28.
88.
Serial_No:11051209:46
Page 219 of 279
FF
HB006SG-000015-20121006Client ID:10/06/12 11:30Date Collected:10/08/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1218042-17Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
Total Organic Carbon - Mansfield Lab
General Chemistry - Westborough Lab
General Chemistry - Mansfield Lab
Total Organic Carbon (Rep1)
Total Organic Carbon (Rep2)
Cyanide, Total
pH
Nitrogen, Ammonia
Nitrogen, Nitrate/Nitrite
Nitrogen, Total Kjeldahl
Solids, Total
% Soot (Rep 1)
% Soot (Rep 2)
2.85
2.31
ND
7.7
96
9.3
4300
34.3
0.070
0.068
%
%
mg/kg
SU
mg/kg
mg/kg
mg/kg
%
%
%
1
1
1
1
1
1
1
1
1
1
0.010
0.010
2.9
-
21
4.8
430
0.100
0.010
0.010
10/24/12 07:14
10/24/12 07:14
10/18/12 15:46
10/10/12 14:30
10/18/12 21:51
10/16/12 03:43
10/18/12 22:15
10/09/12 16:25
10/24/12 07:14
10/24/12 07:14
1,9060
1,9060
1,9010B/9012A
1,9045C
30,4500NH3-BH
30,4500NO3-F
30,4500N-C
30,2540G
91,-
91,-
NR
NR
JO
ML
AT
DB
AT
KB
NR
NR
Date Prepared
-
-
10/16/12 15:00
-
10/16/12 14:45
10/15/12 01:00
10/16/12 23:45
-
-
-
11/05/12
MDL
0.010
0.010
0.67
NA
3.8
0.82
160
0.100
NA
NA
Serial_No:11051209:46
Page 220 of 279
FF
HB006SG-000015-20121006Client ID:10/06/12 11:30Date Collected:10/08/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1218042-17Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
General Chemistry - Westborough LabPhosphorus, Total
Sulfide
660
1700
mg/kg
mg/kg
4.6
100
67
140
10/18/12 11:00
10/10/12 16:48
30,4500P-E
1,9030B
SD
MP
Date Prepared
-
10/10/12 12:45
11/05/12
D
MDL
19.
33.
Serial_No:11051209:46
Page 221 of 279
FF
HB005SG-000015-20121006Client ID:10/06/12 12:19Date Collected:10/08/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1218042-19Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
Total Organic Carbon - Mansfield Lab
General Chemistry - Westborough Lab
General Chemistry - Mansfield Lab
Total Organic Carbon (Rep1)
Total Organic Carbon (Rep2)
Cyanide, Total
pH
Nitrogen, Ammonia
Nitrogen, Nitrate/Nitrite
Nitrogen, Total Kjeldahl
Solids, Total
% Soot (Rep 1)
% Soot (Rep 2)
4.68
5.10
ND
7.8
140
12
7100
25.5
0.121
0.136
%
%
mg/kg
SU
mg/kg
mg/kg
mg/kg
%
%
%
1
1
1
1
1
1
1
1
1
1
0.010
0.010
3.8
-
27
6.5
540
0.100
0.010
0.010
10/24/12 07:14
10/24/12 07:14
10/18/12 15:47
10/10/12 14:30
10/18/12 21:52
10/16/12 03:44
10/18/12 22:16
10/09/12 16:25
10/24/12 07:14
10/24/12 07:14
1,9060
1,9060
1,9010B/9012A
1,9045C
30,4500NH3-BH
30,4500NO3-F
30,4500N-C
30,2540G
91,-
91,-
NR
NR
JO
ML
AT
DB
AT
KB
NR
NR
Date Prepared
-
-
10/16/12 15:00
-
10/16/12 14:45
10/15/12 01:00
10/16/12 23:45
-
-
-
11/05/12
MDL
0.010
0.010
0.90
NA
4.9
1.1
210
0.100
NA
NA
Serial_No:11051209:46
Page 222 of 279
FF
HB005SG-000015-20121006Client ID:10/06/12 12:19Date Collected:10/08/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1218042-19Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
General Chemistry - Westborough LabPhosphorus, Total
Sulfide
680
6000
mg/kg
mg/kg
4.8
100
94
200
10/18/12 11:00
10/10/12 16:49
30,4500P-E
1,9030B
SD
MP
Date Prepared
-
10/10/12 12:45
11/05/12
D
MDL
26.
44.
Serial_No:11051209:46
Page 223 of 279
FF
HB1005SG-000015-20121006Client ID:10/06/12 12:19Date Collected:10/08/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1218042-21Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
Total Organic Carbon - Mansfield Lab
General Chemistry - Westborough Lab
General Chemistry - Mansfield Lab
Total Organic Carbon (Rep1)
Total Organic Carbon (Rep2)
Cyanide, Total
pH
Nitrogen, Ammonia
Nitrogen, Nitrate/Nitrite
Nitrogen, Total Kjeldahl
Solids, Total
% Soot (Rep 1)
% Soot (Rep 2)
4.39
4.05
ND
7.8
140
9.8
7000
25.2
0.141
0.193
%
%
mg/kg
SU
mg/kg
mg/kg
mg/kg
%
%
%
1
1
1
1
1
1
1
1
1
1
0.010
0.010
3.7
-
29
6.6
560
0.100
0.010
0.010
10/24/12 07:14
10/24/12 07:14
10/18/12 15:48
10/10/12 14:30
10/18/12 21:52
10/16/12 03:45
10/18/12 22:17
10/09/12 16:25
10/24/12 07:14
10/24/12 07:14
1,9060
1,9060
1,9010B/9012A
1,9045C
30,4500NH3-BH
30,4500NO3-F
30,4500N-C
30,2540G
91,-
91,-
NR
NR
JO
ML
AT
DB
AT
KB
NR
NR
Date Prepared
-
-
10/16/12 15:00
-
10/16/12 14:45
10/15/12 01:00
10/16/12 23:45
-
-
-
11/05/12
MDL
0.010
0.010
0.87
NA
5.3
1.1
220
0.100
NA
NA
Serial_No:11051209:46
Page 224 of 279
FF
HB1005SG-000015-20121006Client ID:10/06/12 12:19Date Collected:10/08/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1218042-21Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
General Chemistry - Westborough LabPhosphorus, Total
Sulfide
610
7000
mg/kg
mg/kg
4.7
200
93
400
10/18/12 11:00
10/10/12 17:08
30,4500P-E
1,9030B
SD
MP
Date Prepared
-
10/10/12 12:45
11/05/12
D
MDL
26.
89.
Serial_No:11051209:46
Page 225 of 279
FF
HB004SG-000015-20121006Client ID:10/06/12 13:27Date Collected:10/08/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1218042-23Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
Total Organic Carbon - Mansfield Lab
General Chemistry - Westborough Lab
General Chemistry - Mansfield Lab
Total Organic Carbon (Rep1)
Total Organic Carbon (Rep2)
Cyanide, Total
pH
Nitrogen, Ammonia
Nitrogen, Nitrate/Nitrite
Nitrogen, Total Kjeldahl
Solids, Total
% Soot (Rep 1)
% Soot (Rep 2)
3.64
3.88
ND
7.8
56
8.8
5100
35.3
0.182
0.184
%
%
mg/kg
SU
mg/kg
mg/kg
mg/kg
%
%
%
1
1
1
1
1
1
1
1
1
1
0.010
0.010
2.8
-
21
4.7
410
0.100
0.010
0.010
10/24/12 07:14
10/24/12 07:14
10/18/12 15:50
10/10/12 14:30
10/18/12 21:53
10/16/12 03:48
10/18/12 22:17
10/09/12 16:25
10/24/12 07:14
10/24/12 07:14
1,9060
1,9060
1,9010B/9012A
1,9045C
30,4500NH3-BH
30,4500NO3-F
30,4500N-C
30,2540G
91,-
91,-
NR
NR
JO
ML
AT
DB
AT
KB
NR
NR
Date Prepared
-
-
10/16/12 15:00
-
10/16/12 14:45
10/15/12 01:00
10/16/12 23:45
-
-
-
11/05/12
MDL
0.010
0.010
0.65
NA
3.7
0.80
160
0.100
NA
NA
Serial_No:11051209:46
Page 226 of 279
FF
HB004SG-000015-20121006Client ID:10/06/12 13:27Date Collected:10/08/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1218042-23Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
General Chemistry - Westborough LabPhosphorus, Total
Sulfide
570
3400
mg/kg
mg/kg
4.8
100
68
140
10/18/12 11:00
10/10/12 16:50
30,4500P-E
1,9030B
SD
MP
Date Prepared
-
10/10/12 12:45
11/05/12
D
MDL
19.
32.
Serial_No:11051209:46
Page 227 of 279
FF
HB003SG-000015-20121006Client ID:10/06/12 14:21Date Collected:10/08/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1218042-25Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
Total Organic Carbon - Mansfield Lab
General Chemistry - Westborough Lab
General Chemistry - Mansfield Lab
Total Organic Carbon (Rep1)
Total Organic Carbon (Rep2)
Cyanide, Total
pH
Nitrogen, Ammonia
Nitrogen, Nitrate/Nitrite
Nitrogen, Total Kjeldahl
Solids, Total
% Soot (Rep 1)
% Soot (Rep 2)
J
4.43
4.52
1.2
7.7
82
9.6
6600
27.8
0.179
0.168
%
%
mg/kg
SU
mg/kg
mg/kg
mg/kg
%
%
%
1
1
1
1
1
1
1
1
1
1
0.010
0.010
3.5
-
26
6.0
520
0.100
0.010
0.010
10/24/12 07:14
10/24/12 07:14
10/18/12 15:52
10/10/12 14:30
10/18/12 21:54
10/16/12 03:48
10/18/12 22:18
10/09/12 16:25
10/24/12 07:14
10/24/12 07:14
1,9060
1,9060
1,9010B/9012A
1,9045C
30,4500NH3-BH
30,4500NO3-F
30,4500N-C
30,2540G
91,-
91,-
NR
NR
JO
ML
AT
DB
AT
KB
NR
NR
Date Prepared
-
-
10/16/12 15:00
-
10/16/12 14:45
10/15/12 01:00
10/16/12 23:45
-
-
-
11/05/12
MDL
0.010
0.010
0.82
NA
4.6
1.0
200
0.100
NA
NA
Serial_No:11051209:46
Page 228 of 279
FF
HB003SG-000015-20121006Client ID:10/06/12 14:21Date Collected:10/08/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1218042-25Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
General Chemistry - Westborough LabPhosphorus, Total
Sulfide
640
4600
mg/kg
mg/kg
4.9
100
88
180
10/18/12 11:00
10/10/12 16:50
30,4500P-E
1,9030B
SD
MP
Date Prepared
-
10/10/12 12:45
11/05/12
D
MDL
25.
40.
Serial_No:11051209:46
Page 229 of 279
FF
HB002SG-000015-20121006Client ID:10/06/12 15:05Date Collected:10/08/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1218042-27Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
Total Organic Carbon - Mansfield Lab
General Chemistry - Westborough Lab
General Chemistry - Mansfield Lab
Total Organic Carbon (Rep1)
Total Organic Carbon (Rep2)
Cyanide, Total
pH
Nitrogen, Ammonia
Nitrogen, Nitrate/Nitrite
Nitrogen, Total Kjeldahl
Solids, Total
% Soot (Rep 1)
% Soot (Rep 2)
J
3.61
3.43
0.67
7.9
77
8.5
5300
33.5
0.161
0.189
%
%
mg/kg
SU
mg/kg
mg/kg
mg/kg
%
%
%
1
1
1
1
1
1
1
1
1
1
0.010
0.010
2.7
-
21
5.0
410
0.100
0.010
0.010
10/24/12 07:14
10/24/12 07:14
10/18/12 15:53
10/10/12 14:30
10/18/12 21:55
10/16/12 03:49
10/18/12 22:19
10/09/12 16:25
10/24/12 07:14
10/24/12 07:14
1,9060
1,9060
1,9010B/9012A
1,9045C
30,4500NH3-BH
30,4500NO3-F
30,4500N-C
30,2540G
91,-
91,-
NR
NR
JO
ML
AT
DB
AT
KB
NR
NR
Date Prepared
-
-
10/16/12 15:00
-
10/16/12 14:45
10/15/12 01:00
10/16/12 23:45
-
-
-
11/05/12
MDL
0.010
0.010
0.64
NA
3.8
0.84
160
0.100
NA
NA
Serial_No:11051209:46
Page 230 of 279
FF
HB002SG-000015-20121006Client ID:10/06/12 15:05Date Collected:10/08/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1218042-27Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
General Chemistry - Westborough LabPhosphorus, Total
Sulfide
500
3800
mg/kg
mg/kg
4.9
100
73
150
10/18/12 11:00
10/10/12 16:51
30,4500P-E
1,9030B
SD
MP
Date Prepared
-
10/10/12 12:45
11/05/12
D
MDL
20.
33.
Serial_No:11051209:46
Page 231 of 279
FF
HB001SG-000015-20121006Client ID:10/06/12 15:54Date Collected:10/08/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1218042-29Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
Total Organic Carbon - Mansfield Lab
General Chemistry - Westborough Lab
General Chemistry - Mansfield Lab
Total Organic Carbon (Rep1)
Total Organic Carbon (Rep2)
Cyanide, Total
pH
Nitrogen, Ammonia
Nitrogen, Nitrate/Nitrite
Nitrogen, Total Kjeldahl
Solids, Total
% Soot (Rep 1)
% Soot (Rep 2)
4.07
3.95
ND
7.8
110
9.2
6500
29.8
0.278
0.270
%
%
mg/kg
SU
mg/kg
mg/kg
mg/kg
%
%
%
1
1
1
1
1
1
1
1
1
1
0.010
0.010
3.2
-
23
5.6
490
0.100
0.010
0.010
10/24/12 07:14
10/24/12 07:14
10/18/12 15:54
10/10/12 14:30
10/18/12 21:56
10/16/12 03:50
10/18/12 22:20
10/09/12 16:25
10/24/12 07:14
10/24/12 07:14
1,9060
1,9060
1,9010B/9012A
1,9045C
30,4500NH3-BH
30,4500NO3-F
30,4500N-C
30,2540G
91,-
91,-
NR
NR
JO
ML
AT
DB
AT
KB
NR
NR
Date Prepared
-
-
10/16/12 15:00
-
10/16/12 14:45
10/15/12 01:00
10/16/12 23:45
-
-
-
11/05/12
MDL
0.010
0.010
0.76
NA
4.2
0.95
190
0.100
NA
NA
Serial_No:11051209:46
Page 232 of 279
FF
HB001SG-000015-20121006Client ID:10/06/12 15:54Date Collected:10/08/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1218042-29Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
General Chemistry - Westborough LabPhosphorus, Total
Sulfide
610
5200
mg/kg
mg/kg
4.6
100
77
170
10/18/12 11:00
10/10/12 16:52
30,4500P-E
1,9030B
SD
MP
Date Prepared
-
10/10/12 12:45
11/05/12
D
MDL
22.
38.
Serial_No:11051209:46
Page 233 of 279
FF
SRM 1650BClient ID:10/06/12 12:00Date Collected:10/08/12Date Received:
Parameter ResultDilution Factor
Matrix: Sediment
Not SpecifiedSample Location:
L1218042-32Lab ID:
Qualifier Units RL
SAMPLE RESULTS
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
Field Prep:
DateAnalyzed
AnalyticalMethod Analyst
Not Specified
Total Organic Carbon - Mansfield Lab
General Chemistry - Mansfield Lab
Total Organic Carbon (Rep1)
Total Organic Carbon (Rep2)
% Soot (Rep 1)
% Soot (Rep 2)
1.73
1.76
5.52
6.96
%
%
%
%
1
1
1
1
0.010
0.010
0.010
0.010
10/24/12 07:14
10/24/12 07:14
10/24/12 07:14
10/24/12 07:14
1,9060
1,9060
91,-
91,-
NR
NR
NR
NR
Date Prepared
-
-
-
-
11/05/12
MDL
0.010
0.010
NA
NA
Serial_No:11051209:46
Page 234 of 279
FF
Parameter ResultDilution FactorQualifier Units RL
Method Blank AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
DateAnalyzed
AnalyticalMethod Analyst
Date Prepared
11/05/12
Sulfide
Total Organic Carbon (Rep1)
Total Organic Carbon (Rep2)
% Soot (Rep 1)
% Soot (Rep 2)
Nitrogen, Nitrate/Nitrite
Cyanide, Total
Cyanide, Total
Nitrogen, Ammonia
Nitrogen, Total Kjeldahl
Phosphorus, Total
J
ND
ND
ND
ND
ND
ND
ND
ND
1.4
ND
ND
mg/kg
%
%
%
%
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
1
1
1
1
1
1
1
1
1
1
1
0.50
0.010
0.010
0.010
0.010
1.0
0.94
0.94
7.5
150
5.0
10/10/12 14:29
10/24/12 07:14
10/24/12 07:14
10/24/12 07:14
10/24/12 07:14
10/16/12 03:32
10/18/12 15:34
10/18/12 15:34
10/18/12 21:40
10/18/12 22:04
10/18/12 11:00
1,9030B
1,9060
1,9060
91,-
91,-
30,4500NO3-F
1,9010B/9012A
1,9010B/9012A
30,4500NH3-BH
30,4500N-C
30,4500P-E
MP
NR
NR
NR
NR
DB
JO
JO
AT
AT
SD
10/10/12 12:45
-
-
-
-
10/15/12 01:00
10/16/12 15:00
10/16/12 15:00
10/16/12 14:45
10/16/12 23:45
-
General Chemistry - Westborough Lab for sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG566113-1
Total Organic Carbon - Mansfield Lab for sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG566725-1
General Chemistry - Mansfield Lab for sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG566732-1
General Chemistry - Westborough Lab for sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG567243-1
General Chemistry - Westborough Lab for sample(s): 01,03,05,07,09,13,15,17,19,21 Batch: WG567329-1
General Chemistry - Westborough Lab for sample(s): 23,25,27,29 Batch: WG567330-1
General Chemistry - Westborough Lab for sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG567349-1
General Chemistry - Westborough Lab for sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG567493-1
General Chemistry - Westborough Lab for sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG567984-1
MDL
0.11
0.010
0.010
NA
NA
0.02
0.22
0.22
0.01
0.04
1.4
Serial_No:11051209:46
Page 235 of 279
Sulfide
pH
Nitrogen, Nitrate/Nitrite
Cyanide, Total
Cyanide, Total
Nitrogen, Ammonia
Nitrogen, Total Kjeldahl
88
100
98
110
112
99
101
-
-
-
112
110
-
-
75-125
99-101
90-110
80-120
80-120
83-115
84-115
-
-
-
2
2
-
-
25
20
35
35
20
26
ParameterLCS
%RecoveryLCSD
%Recovery%Recovery
Limits RPD RPD Limits
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG566113-2
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG566203-1
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG567243-2
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21 Batch: WG567329-2 WG567329-3
General Chemistry - Westborough Lab Associated sample(s): 23,25,27,29 Batch: WG567330-2 WG567330-3
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG567349-2
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG567493-2
Lab Control Sample AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
Qual Qual Qual
Serial_No:11051209:46
Page 236 of 279
Phosphorus, Total 103 - 52-148 - 20
ParameterLCS
%RecoveryLCSD
%Recovery%Recovery
Limits RPD RPD Limits
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 Batch: WG567984-2
Lab Control Sample AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
Serial_No:11051209:46
Page 237 of 279
Sulfide
Total Organic Carbon (Rep1)
Total Organic Carbon (Rep2)
% Soot (Rep 1)
% Soot (Rep 2)
Nitrogen, Nitrate/Nitrite
Cyanide, Total
Cyanide, Total
Nitrogen, Ammonia
1000
0.522
0.601
0.162
0.163
3.7
ND
ND
110
1100
2.71
2.93
1.23
1.33
170
14
25
1300
390
118
123
93
93
93
100
90
90
-
-
-
-
-
-
13
24
-
-
-
-
-
-
-
98
90
-
70-130
75-125
75-125
75-125
75-125
80-120
65-135
65-135
55-144
-
-
-
-
-
-
7
4
-
25
25
25
25
25
20
35
35
20
ParameterNative Sample
MS Found
MS%Recovery
MSD Found
MSD %Recovery
RecoveryLimits RPD
RPD Limits
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 QC Batch ID: WG566113-4 QC Sample: L1218042-07 Client ID: TN004SG-000015-20121005
Total Organic Carbon - Mansfield Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 QC Batch ID: WG566725-4 QC Sample: L1218042-01 Client ID: TN005SG-000014-20121005
General Chemistry - Mansfield Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 QC Batch ID: WG566732-4 QC Sample: L1218042-01 Client ID: TN005SG-000014-20121005
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 QC Batch ID: WG567243-4 QC Sample: L1218042-01 Client ID: TN005SG-000014-20121005
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21 QC Batch ID: WG567329-4 WG567329-5 QC Sample: L1218042-01 Client ID: TN005SG-000014-20121005
General Chemistry - Westborough Lab Associated sample(s): 23,25,27,29 QC Batch ID: WG567330-4 WG567330-5 QC Sample: L1218042-23 Client ID: HB004SG-000015-20121006
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 QC Batch ID: WG567349-4 QC Sample: L1218042-29 Client ID: HB001SG-000015-20121006
25.8
1.85
1.95
1.14
1.26
180
14
28
1300
MS Added
Matrix Spike AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
Qual
Q
Qual Qual
Serial_No:11051209:46
Page 238 of 279
Nitrogen, Total Kjeldahl
Phosphorus, Total
6500
610
19000
720
102
14
-
-
-
-
43-160
75-125
-
-
26
20
ParameterNative Sample
MS Found
MS%Recovery
MSD Found
MSD %Recovery
RecoveryLimits RPD
RPD Limits
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 QC Batch ID: WG567493-4 QC Sample: L1218042-29 Client ID: HB001SG-000015-20121006
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 QC Batch ID: WG567984-3 QC Sample: L1218042-29 Client ID: HB001SG-000015-20121006
12500
782
MS Added
Matrix Spike AnalysisBatch Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
11/05/12
Q
Serial_No:11051209:46
Page 239 of 279
Solids, Total
Sulfide
pH
Total Organic Carbon (Rep1)
Total Organic Carbon (Rep2)
% Soot (Rep 1)
% Soot (Rep 2)
Nitrogen, Nitrate/Nitrite
29.8
2500
8.0
0.522
0.601
0.162
0.163
3.7
30.1
1800
8.0
0.614
0.779
0.070
0.154
5.0
%
mg/kg
SU
%
%
%
%
mg/kg
1
33
0
16
26
79
6
30
10
25
5
25
25
25
25
20
Units RPDParameter Native Sample Duplicate Sample RPD Limits
General Chemistry - Mansfield Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 QC Batch ID: WG565958-1 QC Sample: L1218042-29 Client ID: HB001SG-000015-20121006
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 QC Batch ID: WG566113-3 QC Sample: L1218042-05 Client ID: TN003SG-000015-20121005
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 QC Batch ID: WG566203-2 QC Sample: L1218042-01 Client ID: TN005SG-000014-20121005
Total Organic Carbon - Mansfield Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 QC Batch ID: WG566725-3 QC Sample: L1218042-01 Client ID: TN005SG-000014-20121005
General Chemistry - Mansfield Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 QC Batch ID: WG566732-3 QC Sample: L1218042-01 Client ID: TN005SG-000014-20121005
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 QC Batch ID: WG567243-3 QC Sample: L1218042-01 Client ID: TN005SG-000014-20121005
NEWTOWN CREEK RI
120782-01.01
Project Name:
Project Number:
L1218042Lab Number:
Report Date:
Lab Duplicate AnalysisBatch Quality Control
11/05/12
Qual
Q
Q
Q
Q
Serial_No:11051209:46
Page 240 of 279
Nitrogen, Ammonia
Nitrogen, Total Kjeldahl
Phosphorus, Total
110
6500
610
110
6500
600
mg/kg
mg/kg
mg/kg
0
0
2
20
26
20
Units RPDParameter Native Sample Duplicate Sample RPD Limits
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 QC Batch ID: WG567349-3 QC Sample: L1218042-29 Client ID: HB001SG-000015-20121006
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 QC Batch ID: WG567493-3 QC Sample: L1218042-29 Client ID: HB001SG-000015-20121006
General Chemistry - Westborough Lab Associated sample(s): 01,03,05,07,09,13,15,17,19,21,23,25,27,2 QC Batch ID: WG567984-4 QC Sample: L1218042-29 Client ID: HB001SG-000015-20121006
NEWTOWN CREEK RI
120782-01.01
Project Name:
Project Number:
L1218042Lab Number:
Report Date:
Lab Duplicate AnalysisBatch Quality Control
11/05/12
Serial_No:11051209:46
Page 241 of 279
S.R.M. Standard Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
Parameter
11/05/12
% Recovery QC CriteriaTotal Organic Carbon (Rep1)
Total Organic Carbon (Rep2)
96
111
75-125
75-125
Standard Reference Material (SRM): WG566725-2
Qual
Serial_No:11051209:46
Page 242 of 279
S.R.M. Standard Quality Control
Project Name:
Project Number:
Lab Number:
Report Date:
NEWTOWN CREEK RI
120782-01.01
L1218042
Parameter
11/05/12
% Recovery QC Criteria% Soot (Rep 1)
% Soot (Rep 2)
100
100
75-125
75-125
Standard Reference Material (SRM): WG566732-2
Qual
Serial_No:11051209:46
Page 243 of 279
*Values in parentheses indicate holding time in days
L1218042-01A
L1218042-01B
L1218042-01D
L1218042-01E
L1218042-01F
L1218042-01G
L1218042-01H
Amber 100ml unpreserved
Amber 250ml unpreserved
Glass 60mL unpreserved
Amber 250ml unpreserved
Glass 60mL unpreserved
Vial MeOH preserved split
Vial Water preserved split
E
E
A
E
E
A
A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
1.7
1.7
2.1
1.7
1.7
2.1
2.1
Y
Y
Y
Y
Y
Y
Y
Absent
Absent
Absent
Absent
Absent
Absent
Absent
A
D
B
C
E
Absent
Absent
Absent
Absent
Absent
CoolerCustody SealCooler Information
NEWTOWN CREEK RI
120782-01.01
A2-FE-6020T(180),A2-PB-6020T(180),A2-BA-6020T(180),A2-NI-6020T(180),A2-SB-6020T(180),A2-ZN-6020T(180),A2-K-6020T(180),A2-CR-6020T(180),A2-TL-6020T(180),A2-AS-6020T(180),A2-CO-6020T(180),A2-MN-6020T(180),A2-BE-6020T(180),A2-CD-6020T(180),A2-V-6020T(180),A2-MG-6020T(180),A2-PREP-3050:2T(180),A2-SE-6020T(180),A2-AG-6020T(180),A2-AL-6020T(180),A2-CA-6020T(180),A2-CU-6020T(180),A2-NA-6020T(180),A2-PREP-3050:1T(180),A2-SN-6020T(180)
A2-SHC(14),A2-ALKPAH(14),A2-SOOT(28),A2-TS(7),A2-TOC-9060-2REPS(28)
8260HLW(14)
TCN-9010(14),TKN-4500(28),TPHOS-4500(28),PH-9045(1),NO3/NO2-4500(28),NH3-4500(28)
SULFIDE-9030(7)
8260HLW(14)
8260HLW(14)
Project Name:
Project Number:
L1218042Lab Number:
Report Date:
Sample Receipt and Container Information
Container ID Container Type Cooler pHTempdeg C Pres Seal
Container Information
Analysis(*)
11/05/12
Were project specific reporting limits specified? YES
Reagent H2O Preserved Vials Frozen on: NA
Serial_No:11051209:46
Page 244 of 279
*Values in parentheses indicate holding time in days
L1218042-01I
L1218042-01X
L1218042-02A
L1218042-02B
L1218042-03A
L1218042-03B
L1218042-03D
L1218042-03E
L1218042-03F
L1218042-03G
L1218042-03H
L1218042-03I
L1218042-03X
L1218042-04A
L1218042-04B
Vial Water preserved split
Amber 500ml unpreserved
Amber 500ml unpreserved
Plastic 250ml unpreserved
Amber 100ml unpreserved
Amber 250ml unpreserved
Glass 60mL unpreserved
Amber 250ml unpreserved
Glass 60mL unpreserved
Vial MeOH preserved split
Vial Water preserved split
Vial Water preserved split
Amber 500ml unpreserved
Amber 500ml unpreserved
Plastic 250ml unpreserved
A
E
E
E
E
E
A
E
E
A
A
A
E
E
E
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
2.1
1.7
1.7
1.7
1.7
1.7
2.1
1.7
1.7
2.1
2.1
2.1
1.7
1.7
1.7
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
NEWTOWN CREEK RI
120782-01.01
8260HLW(14)
A2-AG-6020T(180)
SUB-GEOTESTING(28)
SUB-BROOKS(28)
A2-FE-6020T(180),A2-PB-6020T(180),A2-BA-6020T(180),A2-NI-6020T(180),A2-SB-6020T(180),A2-ZN-6020T(180),A2-K-6020T(180),A2-CR-6020T(180),A2-TL-6020T(180),A2-AS-6020T(180),A2-CO-6020T(180),A2-MN-6020T(180),A2-BE-6020T(180),A2-CD-6020T(180),A2-V-6020T(180),A2-MG-6020T(180),A2-PREP-3050:2T(180),A2-SE-6020T(180),A2-AG-6020T(180),A2-AL-6020T(180),A2-CA-6020T(180),A2-CU-6020T(180),A2-NA-6020T(180),A2-PREP-3050:1T(180),A2-SN-6020T(180)
A2-SHC(14),A2-ALKPAH(14),A2-SOOT(28),A2-TS(7),A2-TOC-9060-2REPS(28)
8260HLW(14)
TCN-9010(14),TKN-4500(28),TPHOS-4500(28),PH-9045(1),NO3/NO2-4500(28),NH3-4500(28)
SULFIDE-9030(7)
8260HLW(14)
8260HLW(14)
8260HLW(14)
A2-AG-6020T(180)
SUB-GEOTESTING(28)
SUB-BROOKS(28)
Project Name:
Project Number:
L1218042Lab Number:
Report Date:
Container ID Container Type Cooler pHTempdeg C Pres Seal
Container Information
Analysis(*)
11/05/12
Serial_No:11051209:46
Page 245 of 279
*Values in parentheses indicate holding time in days
L1218042-05A
L1218042-05B
L1218042-05D
L1218042-05E
L1218042-05F
L1218042-05G
L1218042-05H
L1218042-05I
L1218042-05X
L1218042-06A
L1218042-06B
Amber 100ml unpreserved
Amber 250ml unpreserved
Glass 60mL unpreserved
Amber 250ml unpreserved
Glass 60mL unpreserved
Vial MeOH preserved split
Vial Water preserved split
Vial Water preserved split
Amber 500ml unpreserved
Amber 500ml unpreserved
Plastic 250ml unpreserved
E
E
A
E
E
A
A
A
E
E
E
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
1.7
1.7
2.1
1.7
1.7
2.1
2.1
2.1
1.7
1.7
1.7
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
NEWTOWN CREEK RI
120782-01.01
A2-FE-6020T(180),A2-PB-6020T(180),A2-BA-6020T(180),A2-NI-6020T(180),A2-SB-6020T(180),A2-ZN-6020T(180),A2-K-6020T(180),A2-CR-6020T(180),A2-TL-6020T(180),A2-AS-6020T(180),A2-CO-6020T(180),A2-MN-6020T(180),A2-BE-6020T(180),A2-CD-6020T(180),A2-V-6020T(180),A2-MG-6020T(180),A2-PREP-3050:2T(180),A2-SE-6020T(180),A2-AG-6020T(180),A2-AL-6020T(180),A2-CA-6020T(180),A2-CU-6020T(180),A2-NA-6020T(180),A2-PREP-3050:1T(180),A2-SN-6020T(180)
A2-SHC(14),A2-ALKPAH(14),A2-SOOT(28),A2-TS(7),A2-TOC-9060-2REPS(28)
8260HLW(14)
TCN-9010(14),TKN-4500(28),TPHOS-4500(28),PH-9045(1),NO3/NO2-4500(28),NH3-4500(28)
SULFIDE-9030(7)
8260HLW(14)
8260HLW(14)
8260HLW(14)
A2-AG-6020T(180)
SUB-GEOTESTING(28)
SUB-BROOKS(28)
Project Name:
Project Number:
L1218042Lab Number:
Report Date:
Container ID Container Type Cooler pHTempdeg C Pres Seal
Container Information
Analysis(*)
11/05/12
Serial_No:11051209:46
Page 246 of 279
*Values in parentheses indicate holding time in days
L1218042-07A
L1218042-07B
L1218042-07D
L1218042-07E
L1218042-07F
L1218042-07G
L1218042-07H
L1218042-07I
L1218042-07X
L1218042-08A
L1218042-08B
Amber 100ml unpreserved
Amber 250ml unpreserved
Glass 60mL unpreserved
Amber 250ml unpreserved
Glass 60mL unpreserved
Vial MeOH preserved split
Vial Water preserved split
Vial Water preserved split
Amber 500ml unpreserved
Amber 500ml unpreserved
Plastic 250ml unpreserved
E
E
A
E
E
A
A
A
E
E
E
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
1.7
1.7
2.1
1.7
1.7
2.1
2.1
2.1
1.7
1.7
1.7
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
NEWTOWN CREEK RI
120782-01.01
A2-FE-6020T(180),A2-PB-6020T(180),A2-BA-6020T(180),A2-NI-6020T(180),A2-SB-6020T(180),A2-ZN-6020T(180),A2-K-6020T(180),A2-CR-6020T(180),A2-TL-6020T(180),A2-AS-6020T(180),A2-CO-6020T(180),A2-MN-6020T(180),A2-BE-6020T(180),A2-CD-6020T(180),A2-V-6020T(180),A2-MG-6020T(180),A2-PREP-3050:2T(180),A2-SE-6020T(180),A2-AG-6020T(180),A2-AL-6020T(180),A2-CA-6020T(180),A2-CU-6020T(180),A2-NA-6020T(180),A2-PREP-3050:1T(180),A2-SN-6020T(180)
A2-SHC(14),A2-ALKPAH(14),A2-SOOT(28),A2-TS(7),A2-TOC-9060-2REPS(28)
8260HLW(14)
TCN-9010(14),TKN-4500(28),TPHOS-4500(28),PH-9045(1),NO3/NO2-4500(28),NH3-4500(28)
SULFIDE-9030(7)
8260HLW(14)
8260HLW(14)
8260HLW(14)
A2-AG-6020T(180)
SUB-GEOTESTING(28)
SUB-BROOKS(28)
Project Name:
Project Number:
L1218042Lab Number:
Report Date:
Container ID Container Type Cooler pHTempdeg C Pres Seal
Container Information
Analysis(*)
11/05/12
Serial_No:11051209:46
Page 247 of 279
*Values in parentheses indicate holding time in days
L1218042-09A
L1218042-09B
L1218042-09D
L1218042-09E
L1218042-09F
L1218042-09G
L1218042-09H
L1218042-09I
L1218042-09X
L1218042-10A
L1218042-10B
Amber 100ml unpreserved
Amber 250ml unpreserved
Glass 60mL unpreserved
Amber 250ml unpreserved
Glass 60mL unpreserved
Vial MeOH preserved split
Vial Water preserved split
Vial Water preserved split
Amber 500ml unpreserved
Amber 500ml unpreserved
Plastic 250ml unpreserved
E
E
A
E
E
A
A
A
E
E
E
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
1.7
1.7
2.1
1.7
1.7
2.1
2.1
2.1
1.7
1.7
1.7
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
NEWTOWN CREEK RI
120782-01.01
A2-FE-6020T(180),A2-PB-6020T(180),A2-BA-6020T(180),A2-NI-6020T(180),A2-SB-6020T(180),A2-ZN-6020T(180),A2-K-6020T(180),A2-CR-6020T(180),A2-TL-6020T(180),A2-AS-6020T(180),A2-CO-6020T(180),A2-MN-6020T(180),A2-BE-6020T(180),A2-CD-6020T(180),A2-V-6020T(180),A2-MG-6020T(180),A2-PREP-3050:2T(180),A2-SE-6020T(180),A2-AG-6020T(180),A2-AL-6020T(180),A2-CA-6020T(180),A2-CU-6020T(180),A2-NA-6020T(180),A2-PREP-3050:1T(180),A2-SN-6020T(180)
A2-SHC(14),A2-ALKPAH(14),A2-SOOT(28),A2-TS(7),A2-TOC-9060-2REPS(28)
8260HLW(14)
TCN-9010(14),TKN-4500(28),TPHOS-4500(28),PH-9045(1),NO3/NO2-4500(28),NH3-4500(28)
SULFIDE-9030(7)
8260HLW(14)
8260HLW(14)
8260HLW(14)
A2-AG-6020T(180)
SUB-GEOTESTING(28)
SUB-BROOKS(28)
Project Name:
Project Number:
L1218042Lab Number:
Report Date:
Container ID Container Type Cooler pHTempdeg C Pres Seal
Container Information
Analysis(*)
11/05/12
Serial_No:11051209:46
Page 248 of 279
*Values in parentheses indicate holding time in days
L1218042-11A
L1218042-11B
L1218042-11C
L1218042-11D
L1218042-11E
L1218042-11G
L1218042-11H
L1218042-11I
L1218042-12B
L1218042-13A
Plastic 500ml HNO3 preserved
Amber 1000ml unpreserved
Amber 1000ml unpreserved
Amber 1000ml unpreserved
Amber 1000ml unpreserved
Vial HCl preserved
Vial HCl preserved
Vial HCl preserved
Plastic 250ml unpreserved
Amber 100ml unpreserved
D
D
D
D
D
A
A
A
D
B
<2
7
7
7
7
N/A
N/A
N/A
N/A
N/A
1.9
1.9
1.9
1.9
1.9
2.1
2.1
2.1
1.9
1.9
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
NEWTOWN CREEK RI
120782-01.01
A2-FE-6020T(180),A2-PB-6020T(180),A2-BA-6020T(180),A2-NI-6020T(180),A2-SB-6020T(180),A2-ZN-6020T(180),A2-K-6020T(180),A2-CR-6020T(180),A2-TL-6020T(180),A2-AS-6020T(180),A2-CO-6020T(180),A2-MN-6020T(180),A2-BE-6020T(180),A2-CD-6020T(180),A2-PREP-3020(180),A2-V-6020T(180),A2-MG-6020T(180),A2-SE-6020T(180),A2-AG-6020T(180),A2-AL-6020T(180),A2-CA-6020T(180),A2-CU-6020T(180),A2-NA-6020T(180),A2-SN-6020T(180)
A2-SHC(7)
A2-SHC(7)
A2-ALKPAH(7)
A2-ALKPAH(7)
8260(14)
8260(14)
8260(14)
SUB-BROOKS(28)
A2-FE-6020T(180),A2-PB-6020T(180),A2-BA-6020T(180),A2-NI-6020T(180),A2-SB-6020T(180),A2-ZN-6020T(180),A2-K-6020T(180),A2-CR-6020T(180),A2-TL-6020T(180),A2-AS-6020T(180),A2-CO-6020T(180),A2-MN-6020T(180),A2-BE-6020T(180),A2-CD-6020T(180),A2-V-6020T(180),A2-MG-6020T(180),A2-PREP-3050:2T(180),A2-SE-6020T(180),A2-AG-6020T(180),A2-AL-6020T(180),A2-CA-6020T(180),A2-CU-6020T(180),A2-NA-6020T(180),A2-PREP-3050:1T(180),A2-SN-6020T(180)
Project Name:
Project Number:
L1218042Lab Number:
Report Date:
Container ID Container Type Cooler pHTempdeg C Pres Seal
Container Information
Analysis(*)
11/05/12
Serial_No:11051209:46
Page 249 of 279
*Values in parentheses indicate holding time in days
L1218042-13B
L1218042-13D
L1218042-13E
L1218042-13F
L1218042-13G
L1218042-13H
L1218042-13I
L1218042-13X
L1218042-14A
L1218042-14B
L1218042-15A
L1218042-15B
L1218042-15D
L1218042-15E
L1218042-15F
L1218042-15G
L1218042-15H
L1218042-15I
Amber 250ml unpreserved
Glass 60mL unpreserved
Amber 250ml unpreserved
Glass 60mL unpreserved
Vial MeOH preserved split
Vial Water preserved split
Vial Water preserved split
Amber 500ml unpreserved
Amber 500ml unpreserved
Plastic 250ml unpreserved
Amber 100ml unpreserved
Amber 250ml unpreserved
Glass 60mL unpreserved
Amber 250ml unpreserved
Glass 60mL unpreserved
Vial MeOH preserved split
Vial Water preserved split
Vial Water preserved split
B
A
B
B
A
A
A
B
B
B
B
B
A
B
B
A
A
A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
1.9
2.1
1.9
1.9
2.1
2.1
2.1
1.9
1.9
1.9
1.9
1.9
2.1
1.9
1.9
2.1
2.1
2.1
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
NEWTOWN CREEK RI
120782-01.01
A2-SHC(14),A2-ALKPAH(14),A2-SOOT(28),A2-TS(7),A2-TOC-9060-2REPS(28)
8260HLW(14)
TCN-9010(14),TKN-4500(28),TPHOS-4500(28),PH-9045(1),NO3/NO2-4500(28),NH3-4500(28)
SULFIDE-9030(7)
8260HLW(14)
8260HLW(14)
8260HLW(14)
A2-AG-6020T(180)
SUB-GEOTESTING(28)
SUB-BROOKS(28)
A2-FE-6020T(180),A2-PB-6020T(180),A2-BA-6020T(180),A2-NI-6020T(180),A2-SB-6020T(180),A2-ZN-6020T(180),A2-K-6020T(180),A2-CR-6020T(180),A2-TL-6020T(180),A2-AS-6020T(180),A2-CO-6020T(180),A2-MN-6020T(180),A2-BE-6020T(180),A2-CD-6020T(180),A2-V-6020T(180),A2-MG-6020T(180),A2-PREP-3050:2T(180),A2-SE-6020T(180),A2-AG-6020T(180),A2-AL-6020T(180),A2-CA-6020T(180),A2-CU-6020T(180),A2-NA-6020T(180),A2-PREP-3050:1T(180),A2-SN-6020T(180)
A2-SHC(14),A2-ALKPAH(14),A2-SOOT(28),A2-TS(7),A2-TOC-9060-2REPS(28)
8260HLW(14)
TCN-9010(14),TKN-4500(28),TPHOS-4500(28),PH-9045(1),NO3/NO2-4500(28),NH3-4500(28)
SULFIDE-9030(7)
8260HLW(14)
8260HLW(14)
8260HLW(14)
Project Name:
Project Number:
L1218042Lab Number:
Report Date:
Container ID Container Type Cooler pHTempdeg C Pres Seal
Container Information
Analysis(*)
11/05/12
Serial_No:11051209:46
Page 250 of 279
*Values in parentheses indicate holding time in days
L1218042-15X
L1218042-16A
L1218042-16B
L1218042-17A
L1218042-17B
L1218042-17D
L1218042-17E
L1218042-17F
L1218042-17G
L1218042-17H
L1218042-17I
L1218042-17X
L1218042-18A
L1218042-18B
Amber 500ml unpreserved
Amber 500ml unpreserved
Plastic 250ml unpreserved
Amber 100ml unpreserved
Amber 250ml unpreserved
Glass 60mL unpreserved
Amber 250ml unpreserved
Glass 60mL unpreserved
Vial MeOH preserved split
Vial Water preserved split
Vial Water preserved split
Amber 500ml unpreserved
Amber 500ml unpreserved
Plastic 250ml unpreserved
B
B
B
B
B
A
B
B
A
A
A
B
B
B
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
1.9
1.9
1.9
1.9
1.9
2.1
1.9
1.9
2.1
2.1
2.1
1.9
1.9
1.9
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
NEWTOWN CREEK RI
120782-01.01
A2-AG-6020T(180)
SUB-GEOTESTING(28)
SUB-BROOKS(28)
A2-FE-6020T(180),A2-PB-6020T(180),A2-BA-6020T(180),A2-NI-6020T(180),A2-SB-6020T(180),A2-ZN-6020T(180),A2-K-6020T(180),A2-CR-6020T(180),A2-TL-6020T(180),A2-AS-6020T(180),A2-CO-6020T(180),A2-MN-6020T(180),A2-BE-6020T(180),A2-CD-6020T(180),A2-V-6020T(180),A2-MG-6020T(180),A2-PREP-3050:2T(180),A2-SE-6020T(180),A2-AG-6020T(180),A2-AL-6020T(180),A2-CA-6020T(180),A2-CU-6020T(180),A2-NA-6020T(180),A2-PREP-3050:1T(180),A2-SN-6020T(180)
A2-SHC(14),A2-ALKPAH(14),A2-SOOT(28),A2-TS(7),A2-TOC-9060-2REPS(28)
8260HLW(14)
TCN-9010(14),TKN-4500(28),TPHOS-4500(28),PH-9045(1),NO3/NO2-4500(28),NH3-4500(28)
SULFIDE-9030(7)
8260HLW(14)
8260HLW(14)
8260HLW(14)
A2-AG-6020T(180)
SUB-GEOTESTING(28)
SUB-BROOKS(28)
Project Name:
Project Number:
L1218042Lab Number:
Report Date:
Container ID Container Type Cooler pHTempdeg C Pres Seal
Container Information
Analysis(*)
11/05/12
Serial_No:11051209:46
Page 251 of 279
*Values in parentheses indicate holding time in days
L1218042-19A
L1218042-19B
L1218042-19D
L1218042-19E
L1218042-19F
L1218042-19G
L1218042-19H
L1218042-19I
L1218042-19X
L1218042-20A
L1218042-20B
Amber 100ml unpreserved
Amber 250ml unpreserved
Glass 60mL unpreserved
Amber 250ml unpreserved
Glass 60mL unpreserved
Vial MeOH preserved split
Vial Water preserved split
Vial Water preserved split
Amber 500ml unpreserved
Amber 500ml unpreserved
Plastic 250ml unpreserved
B
B
A
B
B
A
A
A
B
B
B
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
1.9
1.9
2.1
1.9
1.9
2.1
2.1
2.1
1.9
1.9
1.9
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
NEWTOWN CREEK RI
120782-01.01
A2-FE-6020T(180),A2-PB-6020T(180),A2-BA-6020T(180),A2-NI-6020T(180),A2-SB-6020T(180),A2-ZN-6020T(180),A2-K-6020T(180),A2-CR-6020T(180),A2-TL-6020T(180),A2-AS-6020T(180),A2-CO-6020T(180),A2-MN-6020T(180),A2-BE-6020T(180),A2-CD-6020T(180),A2-V-6020T(180),A2-MG-6020T(180),A2-PREP-3050:2T(180),A2-SE-6020T(180),A2-AG-6020T(180),A2-AL-6020T(180),A2-CA-6020T(180),A2-CU-6020T(180),A2-NA-6020T(180),A2-PREP-3050:1T(180),A2-SN-6020T(180)
A2-SHC(14),A2-ALKPAH(14),A2-SOOT(28),A2-TS(7),A2-TOC-9060-2REPS(28)
8260HLW(14)
TCN-9010(14),TKN-4500(28),TPHOS-4500(28),PH-9045(1),NO3/NO2-4500(28),NH3-4500(28)
SULFIDE-9030(7)
8260HLW(14)
8260HLW(14)
8260HLW(14)
A2-AG-6020T(180)
SUB-GEOTESTING(28)
SUB-BROOKS(28)
Project Name:
Project Number:
L1218042Lab Number:
Report Date:
Container ID Container Type Cooler pHTempdeg C Pres Seal
Container Information
Analysis(*)
11/05/12
Serial_No:11051209:46
Page 252 of 279
*Values in parentheses indicate holding time in days
L1218042-21A
L1218042-21B
L1218042-21D
L1218042-21E
L1218042-21F
L1218042-21G
L1218042-21H
L1218042-21I
L1218042-22A
L1218042-22B
Amber 100ml unpreserved
Amber 250ml unpreserved
Glass 60mL unpreserved
Amber 250ml unpreserved
Glass 60mL unpreserved
Vial MeOH preserved split
Vial Water preserved split
Vial Water preserved split
Amber 500ml unpreserved
Plastic 250ml unpreserved
A
A
A
A
A
A
A
A
A
A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
2.1
2.1
2.1
2.1
2.1
2.1
2.1
2.1
2.1
2.1
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
NEWTOWN CREEK RI
120782-01.01
A2-FE-6020T(180),A2-PB-6020T(180),A2-BA-6020T(180),A2-NI-6020T(180),A2-SB-6020T(180),A2-ZN-6020T(180),A2-K-6020T(180),A2-CR-6020T(180),A2-TL-6020T(180),A2-AS-6020T(180),A2-CO-6020T(180),A2-MN-6020T(180),A2-BE-6020T(180),A2-CD-6020T(180),A2-V-6020T(180),A2-MG-6020T(180),A2-PREP-3050:2T(180),A2-SE-6020T(180),A2-AG-6020T(180),A2-AL-6020T(180),A2-CA-6020T(180),A2-CU-6020T(180),A2-NA-6020T(180),A2-PREP-3050:1T(180),A2-SN-6020T(180)
A2-SHC(14),A2-ALKPAH(14),A2-SOOT(28),A2-TS(7),A2-TOC-9060-2REPS(28)
8260HLW(14)
TCN-9010(14),TKN-4500(28),TPHOS-4500(28),PH-9045(1),NO3/NO2-4500(28),NH3-4500(28)
SULFIDE-9030(7)
8260HLW(14)
8260HLW(14)
8260HLW(14)
SUB-GEOTESTING(28)
SUB-BROOKS(28)
Project Name:
Project Number:
L1218042Lab Number:
Report Date:
Container ID Container Type Cooler pHTempdeg C Pres Seal
Container Information
Analysis(*)
11/05/12
Serial_No:11051209:46
Page 253 of 279
*Values in parentheses indicate holding time in days
L1218042-23A
L1218042-23B
L1218042-23D
L1218042-23E
L1218042-23F
L1218042-23G
L1218042-23H
L1218042-23I
L1218042-23X
L1218042-24A
L1218042-24B
Amber 100ml unpreserved
Amber 250ml unpreserved
Glass 60mL unpreserved
Amber 250ml unpreserved
Glass 60mL unpreserved
Vial MeOH preserved split
Vial Water preserved split
Vial Water preserved split
Amber 500ml unpreserved
Amber 500ml unpreserved
Plastic 250ml unpreserved
C
C
A
C
C
A
A
A
C
C
C
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
1.8
1.8
2.1
1.8
1.8
2.1
2.1
2.1
1.8
1.8
1.8
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
NEWTOWN CREEK RI
120782-01.01
A2-FE-6020T(180),A2-PB-6020T(180),A2-BA-6020T(180),A2-NI-6020T(180),A2-SB-6020T(180),A2-ZN-6020T(180),A2-K-6020T(180),A2-CR-6020T(180),A2-TL-6020T(180),A2-AS-6020T(180),A2-CO-6020T(180),A2-MN-6020T(180),A2-BE-6020T(180),A2-CD-6020T(180),A2-V-6020T(180),A2-MG-6020T(180),A2-PREP-3050:2T(180),A2-SE-6020T(180),A2-AG-6020T(180),A2-AL-6020T(180),A2-CA-6020T(180),A2-CU-6020T(180),A2-NA-6020T(180),A2-PREP-3050:1T(180),A2-SN-6020T(180)
A2-SHC(14),A2-ALKPAH(14),A2-SOOT(28),A2-TS(7),A2-TOC-9060-2REPS(28)
8260HLW(14)
TCN-9010(14),TKN-4500(28),TPHOS-4500(28),PH-9045(1),NO3/NO2-4500(28),NH3-4500(28)
SULFIDE-9030(7)
8260HLW(14)
8260HLW(14)
8260HLW(14)
A2-AG-6020T(180)
SUB-GEOTESTING(28)
SUB-BROOKS(28)
Project Name:
Project Number:
L1218042Lab Number:
Report Date:
Container ID Container Type Cooler pHTempdeg C Pres Seal
Container Information
Analysis(*)
11/05/12
Serial_No:11051209:46
Page 254 of 279
*Values in parentheses indicate holding time in days
L1218042-25A
L1218042-25B
L1218042-25D
L1218042-25E
L1218042-25F
L1218042-25G
L1218042-25H
L1218042-25I
L1218042-25X
L1218042-26A
L1218042-26B
Amber 100ml unpreserved
Amber 250ml unpreserved
Glass 60mL unpreserved
Amber 250ml unpreserved
Glass 60mL unpreserved
Vial MeOH preserved split
Vial Water preserved split
Vial Water preserved split
Amber 500ml unpreserved
Amber 500ml unpreserved
Plastic 250ml unpreserved
C
C
A
C
C
A
A
A
C
C
C
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
1.8
1.8
2.1
1.8
1.8
2.1
2.1
2.1
1.8
1.8
1.8
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
NEWTOWN CREEK RI
120782-01.01
A2-FE-6020T(180),A2-PB-6020T(180),A2-BA-6020T(180),A2-NI-6020T(180),A2-SB-6020T(180),A2-ZN-6020T(180),A2-K-6020T(180),A2-CR-6020T(180),A2-TL-6020T(180),A2-AS-6020T(180),A2-CO-6020T(180),A2-MN-6020T(180),A2-BE-6020T(180),A2-CD-6020T(180),A2-V-6020T(180),A2-MG-6020T(180),A2-PREP-3050:2T(180),A2-SE-6020T(180),A2-AG-6020T(180),A2-AL-6020T(180),A2-CA-6020T(180),A2-CU-6020T(180),A2-NA-6020T(180),A2-PREP-3050:1T(180),A2-SN-6020T(180)
A2-SHC(14),A2-ALKPAH(14),A2-SOOT(28),A2-TS(7),A2-TOC-9060-2REPS(28)
8260HLW(14)
TCN-9010(14),TKN-4500(28),TPHOS-4500(28),PH-9045(1),NO3/NO2-4500(28),NH3-4500(28)
SULFIDE-9030(7)
8260HLW(14)
8260HLW(14)
8260HLW(14)
A2-AG-6020T(180)
SUB-GEOTESTING(28)
SUB-BROOKS(28)
Project Name:
Project Number:
L1218042Lab Number:
Report Date:
Container ID Container Type Cooler pHTempdeg C Pres Seal
Container Information
Analysis(*)
11/05/12
Serial_No:11051209:46
Page 255 of 279
*Values in parentheses indicate holding time in days
L1218042-27A
L1218042-27B
L1218042-27D
L1218042-27E
L1218042-27F
L1218042-27G
L1218042-27H
L1218042-27I
L1218042-27X
L1218042-28A
L1218042-28B
Amber 100ml unpreserved
Amber 250ml unpreserved
Glass 60mL unpreserved
Amber 250ml unpreserved
Glass 60mL unpreserved
Vial MeOH preserved split
Vial Water preserved split
Vial Water preserved split
Amber 500ml unpreserved
Amber 500ml unpreserved
Plastic 250ml unpreserved
C
C
A
C
C
A
A
A
C
C
C
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
1.8
1.8
2.1
1.8
1.8
2.1
2.1
2.1
1.8
1.8
1.8
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
NEWTOWN CREEK RI
120782-01.01
A2-FE-6020T(180),A2-PB-6020T(180),A2-BA-6020T(180),A2-NI-6020T(180),A2-SB-6020T(180),A2-ZN-6020T(180),A2-K-6020T(180),A2-CR-6020T(180),A2-TL-6020T(180),A2-AS-6020T(180),A2-CO-6020T(180),A2-MN-6020T(180),A2-BE-6020T(180),A2-CD-6020T(180),A2-V-6020T(180),A2-MG-6020T(180),A2-PREP-3050:2T(180),A2-SE-6020T(180),A2-AG-6020T(180),A2-AL-6020T(180),A2-CA-6020T(180),A2-CU-6020T(180),A2-NA-6020T(180),A2-PREP-3050:1T(180),A2-SN-6020T(180)
A2-SHC(14),A2-ALKPAH(14),A2-SOOT(28),A2-TS(7),A2-TOC-9060-2REPS(28)
8260HLW(14)
TCN-9010(14),TKN-4500(28),TPHOS-4500(28),PH-9045(1),NO3/NO2-4500(28),NH3-4500(28)
SULFIDE-9030(7)
8260HLW(14)
8260HLW(14)
8260HLW(14)
A2-AG-6020T(180)
SUB-GEOTESTING(28)
SUB-BROOKS(28)
Project Name:
Project Number:
L1218042Lab Number:
Report Date:
Container ID Container Type Cooler pHTempdeg C Pres Seal
Container Information
Analysis(*)
11/05/12
Serial_No:11051209:46
Page 256 of 279
*Values in parentheses indicate holding time in days
L1218042-29A
L1218042-29B
L1218042-29D
L1218042-29E
L1218042-29F
L1218042-29G
L1218042-29H
L1218042-29I
L1218042-29X
L1218042-30A
L1218042-30B
L1218042-31A
L1218042-31B
Amber 100ml unpreserved
Amber 250ml unpreserved
Glass 60mL unpreserved
Amber 250ml unpreserved
Glass 60mL unpreserved
Vial MeOH preserved split
Vial Water preserved split
Vial Water preserved split
Amber 500ml unpreserved
Amber 500ml unpreserved
Plastic 250ml unpreserved
Vial HCl preserved
Vial HCl preserved
C
C
A
C
C
A
A
A
C
C
C
A
A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
1.8
1.8
2.1
1.8
1.8
2.1
2.1
2.1
1.8
1.8
1.8
2.1
2.1
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Y
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
Absent
NEWTOWN CREEK RI
120782-01.01
A2-FE-6020T(180),A2-PB-6020T(180),A2-BA-6020T(180),A2-NI-6020T(180),A2-SB-6020T(180),A2-ZN-6020T(180),A2-K-6020T(180),A2-CR-6020T(180),A2-TL-6020T(180),A2-AS-6020T(180),A2-CO-6020T(180),A2-MN-6020T(180),A2-BE-6020T(180),A2-CD-6020T(180),A2-V-6020T(180),A2-MG-6020T(180),A2-PREP-3050:2T(180),A2-SE-6020T(180),A2-AG-6020T(180),A2-AL-6020T(180),A2-CA-6020T(180),A2-CU-6020T(180),A2-NA-6020T(180),A2-PREP-3050:1T(180),A2-SN-6020T(180)
A2-SHC(14),A2-ALKPAH(14),A2-SOOT(28),A2-TS(7),A2-TOC-9060-2REPS(28)
8260HLW(14)
TCN-9010(14),TKN-4500(28),TPHOS-4500(28),PH-9045(1),NO3/NO2-4500(28),NH3-4500(28)
SULFIDE-9030(7)
8260HLW(14)
8260HLW(14)
8260HLW(14)
A2-AG-6020T(180)
SUB-GEOTESTING(28)
SUB-BROOKS(28)
8260(14)
8260(14)
Project Name:
Project Number:
L1218042Lab Number:
Report Date:
Sent to GeoTesting Express
Sent to Brooks Rand Lab
Sent to GeoTesting Express
Sent to Brooks Rand Lab
L1218042-02A
L1218042-02B
L1218042-04A
L1218042-04B
Container ID Container Type Cooler pHTempdeg C Pres Seal
Container Information
Analysis(*)
11/05/12
Container Comments
Serial_No:11051209:46
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*Values in parentheses indicate holding time in days
NEWTOWN CREEK RI
120782-01.01
Project Name:
Project Number:
L1218042Lab Number:
Report Date:
Sent to GeoTesting Express
Sent to Brooks Rand Lab
Sent to GeoTesting Express
Sent to Brooks Rand Lab
Sent to GeoTesting Express
Sent to Brooks Rand Lab
Sent to Brooks Rand Lab
Sent to GeoTesting Express
Sent to Brooks Rand Lab
Sent to GeoTesting Express
Sent to Brooks Rand Lab
Sent to GeoTesting Express
Sent to Brooks Rand Lab
Sent to GeoTesting Express
Sent to Brooks Rand Lab
Sent to GeoTesting Express
Sent to Brooks Rand Lab
Sent to GeoTesting Express
Sent to Brooks Rand Lab
Sent to GeoTesting Express
Sent to Brooks Rand Lab
Sent to GeoTesting Express
Sent to Brooks Rand Lab
Sent to GeoTesting Express
Sent to Brooks Rand Lab
L1218042-06A
L1218042-06B
L1218042-08A
L1218042-08B
L1218042-10A
L1218042-10B
L1218042-12B
L1218042-14A
L1218042-14B
L1218042-16A
L1218042-16B
L1218042-18A
L1218042-18B
L1218042-20A
L1218042-20B
L1218042-22A
L1218042-22B
L1218042-24A
L1218042-24B
L1218042-26A
L1218042-26B
L1218042-28A
L1218042-28B
L1218042-30A
L1218042-30B
Container ID Container Type Cooler pHTempdeg C Pres Seal
Container Information
Analysis(*)
11/05/12
Container Comments
Serial_No:11051209:46
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Report Format: DU Report with "J" Qualifiers
GLOSSARY
Project Name:
Project Number:
Lab Number:
Report Date:
L1218042NEWTOWN CREEK RI
120782-01.01 11/05/12
Acronyms
EPA
LCS
LCSD
LFB
MDL
MS
MSD
NA
NC
NI
RL
RPD
SRM
Environmental Protection Agency.
Laboratory Control Sample: A sample matrix, free from the analytes of interest, spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes.Laboratory Control Sample Duplicate: Refer to LCS.
Laboratory Fortified Blank: A sample matrix, free from the analytes of interest, spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes.Method Detection Limit: This value represents the level to which target analyte concentrations are reported as estimated values, when those target analyte concentrations are quantified below the reporting limit (RL). The MDL includes any adjustments from dilutions, concentrations or moisture content, where applicable.Matrix Spike Sample: A sample prepared by adding a known mass of target analyte to a specified amount of matrix sample for which an independent estimate of target analyte concentration is available. Matrix Spike Sample Duplicate: Refer to MS.
Not Applicable.
Not Calculated: Term is utilized when one or more of the results utilized in the calculation are non-detect at the parameter's reporting unit.Not Ignitable.
Reporting Limit: The value at which an instrument can accurately measure an analyte at a specific concentration. The RL includes any adjustments from dilutions, concentrations or moisture content, where applicable.Relative Percent Difference: The results from matrix and/or matrix spike duplicates are primarily designed to assess the precisionof analytical results in a given matrix and are expressed as relative percent difference (RPD). Values which are less than five times the reporting limit for any individual parameter are evaluated by utilizing the absolute difference between the values; although the RPD value will be provided in the report.Standard Reference Material: A reference sample of a known or certified value that is of the same or similar matrix as the associated field samples.
-
-
-
-
-
-
-
-
-
-
-
-
-
Terms
Analytical Method: Both the document from which the method originates and the analytical reference method. (Example: EPA 8260B is shown as 1,8260B.) The codes for the reference method documents are provided in the References section of the Addendum.
Data Qualifiers
A
B
C
D
E
G
H
I
M
NJ
-
-
-
-
-
-
-
-
-
-
Spectra identified as "Aldol Condensation Product".
The analyte was detected above the reporting limit in the associated method blank. Flag only applies to associated field samples that have detectable concentrations of the analyte at less than five times (5x) the concentration found in the blank. For MCP-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank. For DOD-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte at less than ten times (10x) the concentration found in the blank AND the analyte was detected above one-half the reporting limit (or above the reporting limit for common lab contaminants) in the associated method blank. For NJ-Air-related projects, flag only applies to associated field samples that have detectable concentrations of the analyte above the reporting limit.Co-elution: The target analyte co-elutes with a known lab standard (i.e. surrogate, internal standards, etc.) for co-extracted analyses.Concentration of analyte was quantified from diluted analysis. Flag only applies to field samples that have detectable concentrations of the analyte.Concentration of analyte exceeds the range of the calibration curve and/or linear range of the instrument.
The concentration may be biased high due to matrix interferences (i.e, co-elution) with non-target compound(s). The result should be considered estimated.The analysis of pH was performed beyond the regulatory-required holding time of 15 minutes from the time of sample collection.
The RPD between the results for the two columns exceeds the method-specified criteria; however, the lower value has been reporteddue to obvious interference.Reporting Limit (RL) exceeds the MCP CAM Reporting Limit for this analyte.
Presumptive evidence of compound. This represents an estimated concentration for Tentatively Identified Compounds (TICs), where the identification is based on a mass spectral library search.
1 The reference for this analyte should be considered modified since this analyte is absent from the target analyte list of the originalmethod.
-
Footnotes
Serial_No:11051209:46
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Report Format: DU Report with "J" Qualifiers
Project Name:
Project Number:
Lab Number:
Report Date:
L1218042NEWTOWN CREEK RI
120782-01.01 11/05/12
Data Qualifiers
P
Q
R
RE
-
-
-
-
The RPD between the results for the two columns exceeds the method-specified criteria.
The quality control sample exceeds the associated acceptance criteria. For DOD-related projects, LCS and/or Continuing CalibrationStandard exceedences are also qualified on all associated sample results. Note: This flag is not applicable for matrix spike recoverieswhen the sample concentration is greater than 4x the spike added or for batch duplicate RPD when the sample concentrations are lessthan 5x the RL. (Metals only.)Analytical results are from sample re-analysis.
Analytical results are from sample re-extraction.
J
ND
-
-
Estimated value. The Target analyte concentration is below the quantitation limit (RL), but above the Method Detection Limit (MDL) or Estimated Detection Limit (EDL) for SPME-related analyses. This represents an estimated concentration for Tentatively Identified Compounds (TICs).Not detected at the method detection limit (MDL) for the sample, or estimated detection limit (EDL) for SPME-related analyses.
Serial_No:11051209:46
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Alpha Analytical performs services with reasonable care and diligence normal to the analytical testinglaboratory industry. In the event of an error, the sole and exclusive responsibility of Alpha Analyticalshall be to re-perform the work at it's own expense. In no event shall Alpha Analytical be held liablefor any incidental, consequential or special damages, including but not limited to, damages in any wayconnected with the use of, interpretation of, information or analysis provided by Alpha Analytical.
We strongly urge our clients to comply with EPA protocol regarding sample volume, preservation, cooling,containers, sampling procedures, holding time and splitting of samples in the field.
LIMITATION OF LIABILITIES
1
30
91
Test Methods for Evaluating Solid Waste: Physical/Chemical Methods. EPA SW-846. Third Edition. Updates I - IIIA, 1997.
Standard Methods for the Examination of Water and Wastewater. APHA-AWWA-WPCF. 18th Edition. 1992.
Analysis of Soot by Accardi-Dey, Gschwend, 2003; Gustafsson (et. al.), 1997.
Project Name:
Project Number:
Lab Number:
Report Date:
L1218042NEWTOWN CREEK RI
120782-01.01
REFERENCES
11/05/12
Serial_No:11051209:46
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Certificate/Approval Program SummaryLast revised August 3, 2012 – Mansfield Facility
The following list includes only those analytes/methods for which certification/approval is currently held.For a complete listing of analytes for the referenced methods, please contact your Alpha Customer Service Representative.
Connecticut Department of Public Health Certificate/Lab ID: PH-0141.
Wastewater/Non-Potable Water (Inorganic Parameters: pH, Turbidity, Conductivity, Alkalinity, Aluminum, Antimony, Arsenic, Barium, Beryllium, Boron, Cadmium, Calcium, Chromium, Cobalt, Copper, Iron, Lead, Magnesium, Manganese, Mercury, Molybdenum, Nickel, Potassium, Selenium, Silver, Sodium, Strontium, Thallium, Tin, Titanium, Vanadium, Zinc, Total Residue (Solids), Total Suspended Solids (non-filterable). Organic Parameters: PCBs, Organochlorine Pesticides, Technical Chlordane, Toxaphene, Acid Extractables, Benzidines, Phthalate Esters, Nitrosamines, Nitroaromatics & Isophorone, PAHs, Haloethers, Chlorinated Hydrocarbons, Volatile Organics.)
Solid Waste/Soil (Inorganic Parameters: pH, Aluminum, Antimony, Arsenic, Barium, Beryllium, Cadmium,Calcium, Chromium, Hexavalent Chromium, Cobalt, Copper, Iron, Lead, Magnesium, Manganese, Mercury, Molybdenum, Nickel, Potassium, Selenium, Silver, Sodium, Thallium, Titanium, Vanadium, Zinc, Total Organic Carbon, Corrosivity, TCLP 1311, SPLP 1312. Organic Parameters: PCBs, Organochlorine Pesticides, Technical Chlordane, Toxaphene, Volatile Organics, Acid Extractables, Benzidines, Phthalates, Nitrosamines,Nitroaromatics & Cyclic Ketones, PAHs, Haloethers, Chlorinated Hydrocarbons.)
Florida Department of Health Certificate/Lab ID: E87814. NELAP Accredited.
Non-Potable Water (Inorganic Parameters: SM2320B, SM2540D, SM2540G.)
Solid & Chemical Materials (Inorganic Parameters: 6020, 7470, 7471, 9045. Organic Parameters: EPA 8260,8270, 8082, 8081.)
Air & Emissions (EPA TO-15.)
Louisiana Department of Environmental Quality Certificate/Lab ID: 03090. NELAP Accredited.
Non-Potable Water (Inorganic Parameters: EPA 180.1, 245.7, 1631E, 3020A, 6020A, 7470A, 9040, 9050A, SM2320B, 2540D, 2540G, 4500H-B, Organic Parameters: EPA 3510C, 3580A, 3630C, 3640A, 3660B, 3665A,5030B, 8015D, 3570, 8081B, 8082A, 8260B, 8270C, 8270D.)
Solid & Chemical Materials (Inorganic Parameters: EPA 1311, 3050B, 3051A, 3060A, 6020A, 7196A, 7470A,7471B, 7474, 9040B, 9045C, 9060. Organic Parameters: EPA 3540C, 3570, 3580A, 3630C, 3640A, 3660,3665A, 5035, 8015D, 8081B, 8082A, 8260B, 8270C, 8270D.)
Biological Tissue (Inorganic Parameters: EPA 6020A. Organic Parameters: EPA 3570, 3510C, 3610B, 3630C, 3640A, 8270C, 8270D.)
Air & Emissions (EPA TO-15.)
New Hampshire Department of Environmental Services Certificate/Lab ID: 2206. NELAP Accredited.
Non-Potable Water (Inorganic Parameters: EPA 180.1, 1631E, 6020A, 7470A, 9040B, 9050A, SM2540D, 2540G, 4500H+B, 2320B, 3020A, . Organic Parameters: EPA 3510C, 3630C, 3640A, 3660B, 8081B, 8082A, 8270C, 8270D, 8015D.)
Solid & Chemical Materials (Inorganic Parameters: SW-846 1311, 3050B, 3051A, 6020A, 7471B, 9040B, 9045C. Organic Parameters: SW-846 3540C, 3580A, 3630C, 3640A, 3660B, 3665A, 8270C, 8015D, 8082A, 8081B.)
New Jersey Department of Environmental Protection Certificate/Lab ID: MA015. NELAP Accredited.
Non-Potable Water (Inorganic Parameters: SW-846 1312, 3020A, SM2320B, SM2540D, 2540G, 4500H-B, EPA 180.1, 1631E, SW-846 7470A, 9040C, 6020A, 9050A. Organic Parameters: SW-846 3510C, 3580A, 3630C, 3640A, 3660B, 3665A, 8015D, 8081B, 8082A, 8270C, 8270D)
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Solid & Chemical Materials (Inorganic Parameters: SW-846 1311, 1312, 3050B, 3051A, 6020A, 7471B, 7474,9040B, 9040C, 9045C, 9045D, 9060. Organic Parameters: SW-846 3540C, 3570, 3580A, 3630C, 3640A, 3660B, 3665A, 8081B, 8082A, 8270C, 8270D, 8015D.)
Atmospheric Organic Parameters (EPA 3C, TO-15, TO-10A, TO-13A-SIM.)
Biological Tissue (Inorganic Parameters: SW-846 6020A. Organic Parameters: SW-846 8270C, 8270D, 3510C, 3570, 3610C, 3630C, 3640A)
New York Department of Health Certificate/Lab ID: 11627. NELAP Accredited.
Non-Potable Water (Inorganic Parameters: SM2320B, SM2540D, 6020A, 1631E, 7470A, 9050A, EPA 180.1, 3020A. Organic Parameters: EPA 8270C, 8270D, 8081B, 8082A, 3510C.)
Solid & Hazardous Waste (Inorganic Parameters: EPA 6020A, 7471B, 7474, 9040C, 9045D. Organic Parameters: EPA 8270C, 8270D, 8081B, 8082A, 1311, 3050B, 3580A, 3570, 3051A.)
Air & Emissions (EPA TO-15, TO-10A.)
Pennsylvania Certificate/Lab ID: 68-02089 NELAP Accredited
Non-Potable Water (Inorganic Parameters: 1312, 1631E, 180.1, 3020A, 6020A, 7470A, 9040B, 9050A, 2320B, 2540D, 2540G, SM4500H+-B. Organic Parameters: 3510C, 3580A, 3630C, 3640A, 3660B, 3665A, 8015D, 8081B, 8082A, 8270C, 8270D .)
Solid & Hazardous Waste (Inorganic Parameters: EPA 1311, 3051A, 6020A, 7471B, 7474 9040B, 9045C, 9060.Organic Parameters: EPA3050B, 3540C, 3570, 3580A, 3630C, 3640A, 3660B, 3665A, 8270C, 8270D, 8081B,8015D, 8082A.)
Rhode Island Department of Health Certificate/Lab ID: LAO00299. NELAP Accredited via NJ-DEP.
Refer to NJ-DEP Certificate for Non-Potable Water.
Texas Commission of Environmental Quality Certificate/Lab ID: T104704419-08-TX. NELAP Accredited.
Solid & Chemical Materials (Inorganic Parameters: EPA 6020, 7470, 7471, 1311, 9040, 9045, 9060. Organic Parameters: EPA 8015, 8270, 8081, 8082.)
Air (Organic Parameters: EPA TO-15)
Virginia Division of Consolidated Laboratory Services Certificate/Lab ID:460194. NELAP Accredited.
Non-Potable Water (Inorganic Parameters:EPA 3020A, 6020A, 245.7, 9040B. Organic Parameters: EPA 3510C,3640A, 3660B, 3665A, 8270C, 8270D, 8082A, 8081B, 8015D.)
Solid & Chemical Materials (Inorganic Parameters: EPA 6020A,7470A,7471B,9040B,9045C,3050B,3051, 9060.Organic Parameters: EPA 3540C, 3580A, 3630C, 3640A, 3660B, 3665A, 3570, 8270C, 8270D, 8081B, 8082A,8015D.)
Washington State Department of Ecology Certificate/Lab ID: C954. Non-Potable Water (InorganicParameters: SM2540D, 180.1, 1631E.)
Solid & Chemical Materials (Inorganic Parameters: EPA 6020, 7470, 7471, 7474, 9045C, 9050A, 9060. OrganicParameters: EPA 8081, 8082, 8015, 8270.)
U.S. Army Corps of Engineers
Department of Defense, L-A-B Certificate/Lab ID: L2217.01.
Non-Potable Water (Inorganic Parameters: EPA 6020A, SM4500H-B. Organic Parameters: 3020A, 3510C,8270C, 8270D, 8270C-ALK-PAH, 8270D-ALK-PAH, 8082A, 8081B, 8015D-SHC, 8015D.)
Solid & Hazardous Waste (Inorganic Parameters: EPA 1311, 3050B, 6020A, 7471A, 9045C, 9060, SM 2540G, ASTM D422-63. Organic Parameters: EPA 3580A, 3570, 3540C, 8270C, 8270D, 8270C-ALK-PAH, 8270D-ALK-PAH 8082A, 8081B, 8015D-SHC, 8015D.
Air & Emissions (EPA TO-15.)
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Analytes Not Accredited by NELAP Certification is not available by NELAP for the following analytes: 8270C: Biphenyl. TO-15: Halothane, 2,4,4-Trimethyl-2-pentene, 2,4,4-Trimethyl-1-pentene, Thiophene, 2-Methylthiophene, 3-Methylthiophene, 2-Ethylthiophene, 1,2,3-Trimethylbenzene, Indan, Indene, 1,2,4,5-Tetramethylbenzene, Benzothiophene, 2-Methylnaphthalene, 1-Methylnaphthalene.
Serial_No:11051209:46
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Certificate/Approval Program Summary Last revised August 16, 2012 - Westboro Facility
The following list includes only those analytes/methods for which certification/approval is currently held.
For a complete listing of analytes for the referenced methods, please contact your Alpha Customer Service Representative.
Connecticut Department of Public Health Certificate/Lab ID: PH-0574. NELAP Accredited Solid Waste/Soil. Drinking Water (Inorganic Parameters: Color, pH, Turbidity, Conductivity, Alkalinity, Chloride, Free Residual Chlorine, Fluoride, Calcium Hardness, Sulfate, Nitrate, Nitrite, Aluminum, Antimony, Arsenic, Barium, Beryllium, Cadmium, Calcium, Chromium, Copper, Iron, Lead, Magnesium, Manganese, Mercury, Nickel, Selenium, Silver, Sodium, Thallium, Zinc, Total Dissolved Solids, Total Organic Carbon, Total Cyanide, Perchlorate. Organic Parameters: Volatile Organics 524.2, Total Trihalomethanes 524.2, 1,2-Dibromo-3-chloropropane (DBCP) 504.1, Ethylene Dibromide (EDB) 504.1, 1,4-Dioxane (Mod 8270). Microbiology Parameters: Total Coliform-MF mEndo (SM9222B), Total Coliform – Colilert (SM9223, Enumeration and P/A), E. Coli. – Colilert (SM9223, Enumeration and P/A), HPC – Pour Plate (SM9215B), Fecal Coliform – MF m-FC (SM9222D), Fecal Coliform-EC Medium (SM 9221E). Wastewater/Non-Potable Water (Inorganic Parameters: Color, pH, Conductivity, Acidity, Alkalinity, Chloride, Total Residual Chlorine, Fluoride, Total Hardness, Silica, Sulfate, Sulfide, Ammonia, Kjeldahl Nitrogen, Nitrate, Nitrite, O-Phosphate, Total Phosphorus, Aluminum, Antimony, Arsenic, Barium, Beryllium, Boron, Cadmium, Calcium, Chromium, Hexavalent Chromium, Cobalt, Copper, Iron, Lead, Magnesium, Manganese, Mercury, Molybdenum, Nickel, Potassium, Selenium, Silver, Sodium, Strontium, Thallium, Tin, Titanium, Vanadium, Zinc, Total Residue (Solids), Total Dissolved Solids, Total Suspended Solids (non-filterable), BOD, CBOD, COD, TOC, Total Cyanide, Phenolics, Foaming Agents (MBAS), Bromide, Oil and Grease. Organic Parameters: PCBs, Organochlorine Pesticides, Technical Chlordane, Toxaphene, Acid Extractables (Phenols), Benzidines, Phthalate Esters, Nitrosamines, Nitroaromatics & Isophorone, Polynuclear Aromatic Hydrocarbons, Haloethers, Chlorinated Hydrocarbons, Volatile Organics, TPH (HEM/SGT), CT- Extractable Petroleum Hydrocarbons (ETPH), MA-EPH, MA-VPH. Microbiology Parameters: Total Coliform – MF mEndo (SM9222B), Total Coliform – MTF (SM9221B), E. Coli – Colilert (SM9223 Enumeration), HPC – Pour Plate (SM9215B), Fecal Coliform – MF m-FC (SM9222D), Fecal Coliform – A-1 Broth (SM9221E), Enterococcus - Enterolert. Solid Waste/Soil (Inorganic Parameters: pH, Sulfide, Aluminum, Antimony, Arsenic, Barium, Beryllium, Boron, Cadmium, Calcium, Chromium, Hexavalent Chromium, Cobalt, Copper, Iron, Lead, Magnesium, Manganese, Mercury, Molybdenum, Nickel, Potassium, Selenium, Silver, Sodium, Thallium, Tin, Vanadium, Zinc, Total Cyanide, Ignitability, Phenolics, Corrosivity, TCLP Leach (1311), SPLP Leach (1312 metals only), Reactivity. Organic Parameters: PCBs, PCBs in Oil, Organochlorine Pesticides, Technical Chlordane, Toxaphene, CT-Extractable Petroleum Hydrocarbons (ETPH), MA-EPH, MA-VPH, Dicamba, 2,4-D, 2,4,5-T, 2,4,5-TP(Silvex), Dalapon, Volatile Organics (SW 8260), Acid Extractables (Phenols) (SW 8270), Benzidines (SW 8270), Phthalates (SW 8270), Nitrosamines (SW 8270), Nitroaromatics & Cyclic Ketones (SW 8270), PAHs (SW 8270), Haloethers (SW 8270), Chlorinated Hydrocarbons (SW 8270). ) Maine Department of Human Services Certificate/Lab ID: 2009024. Drinking Water (Inorganic Parameters: SM9215B, 9222D, 9223B, EPA 180.1, 353.2, SM2130B, 2320B, 2540C, 4500Cl-D, 4500CN-C, 4500CN-E, 4500F-C, 4500H+B, 4500NO3-F, EPA 200.7, EPA 200.8, 245.1, EPA 300.0. Organic Parameters: 504.1, 524.2.) Wastewater/Non-Potable Water (Inorganic Parameters: EPA 120.1, 1664A, 350.1, 351.1, 353.2, 410.4, 420.1, SM2320B, 2510B, 2540C, 2540D, 426C, 4500Cl-D, 4500Cl-E, 4500CN-C, 4500CN-E, 4500F-B, 4500F-C, 4500H+B, 4500Norg-B, 4500Norg-C, 4500NH3-B, 4500NH3-G, 4500NO3-F, 4500P-B, 4500P-E, 5210B, 5220D, 5310C, 9010B, 9040B, 9030B, 7470A, 7196A, 2340B, EPA 200.7, 6010B, 200.8, 6020, 245.1, 1311, 1312, 3005A, Enterolert, 9223D, 9222D. Organic Parameters: 608, 624, 625, 8081A, 8082, 8330, 8151A, 8260B, 8270C, 3510C, 3630C, 5030B, ME-DRO, ME-GRO, MA-EPH, MA-VPH.) Solid Waste/Soil (Inorganic Parameters: 9010B, 9012A, 9014A, 9030B, 9040B, 9045C, 6010B, 7471A, 7196A, 9050A, 1010, 1030, 9065, 1311, 1312, 3005A, 3050B. Organic Parameters: ME-DRO, ME-GRO, MA-EPH, MA-VPH, 8260B, 8270C, 8330, 8151A, 8081A, 8082, 3540C, 3546, 3580A, 3630C, 5030B, 5035.) Massachusetts Department of Environmental Protection Certificate/Lab ID: M-MA086. Drinking Water (Inorganic Parameters: (EPA 200.8 for: Sb,As,Ba,Be,Cd,Cr,Cu,Pb,Ni,Se,Tl) (EPA 200.7 for: Ba,Be,Ca,Cd,Cr,Cu,Na,Ni) 245.1, (300.0 for: Nitrate-N, Fluoride, Sulfate); (EPA 353.2 for: Nitrate-N, Nitrite-N); (SM4500NO3-F for: Nitrate-N and Nitrite-N); 4500F-C, 4500CN-CE, EPA 180.1, SM2130B, SM4500Cl-D, 2320B, SM2540C, SM4500H-B. Organic Parameters: (EPA 524.2 for: Trihalomethanes, Volatile Organics); (504.1 for: 1,2-Dibromoethane, 1,2-Dibromo-3-Chloropropane), EPA 332. Microbiology Parameters: SM9215B; ENZ. SUB. SM9223; ColilertQT SM9223B; MF-SM9222D.) Non-Potable Water (Inorganic Parameters:, (EPA 200.8 for: Al,Sb,As,Be,Cd,Cr,Cu,Pb,Mn,Ni,Se,Ag,Tl,Zn); (EPA 200.7
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for: Al,Sb,As,Be,Cd,Ca,Cr,Co,Cu,Fe,Pb,Mg,Mn,Mo,Ni,K,Se,Ag,Na,Sr,Ti,Tl,V,Zn); 245.1, SM4500H,B, EPA 120.1, SM2510B, 2540C, 2340B, 2320B, 4500CL-E, 4500F-BC, 426C, SM4500NH3-BH, (EPA 350.1 for: Ammonia-N), LACHAT 10-107-06-1-B for Ammonia-N, SM4500NO3-F, 353.2 for Nitrate-N, SM4500NH3-BC-NES, EPA 351.1, SM4500P-E, 4500P-B,E, 5220D, EPA 410.4, SM 5210B, 5310C, 4500CL-D, EPA 1664, SM14 510AC, EPA 420.1, SM4500-CN-CE, SM2540D. Organic Parameters: (EPA 624 for Volatile Halocarbons, Volatile Aromatics),(608 for: Chlordane, Toxaphene, Aldrin, alpha-BHC, beta-BHC, gamma-BHC, delta-BHC, Dieldrin, DDD, DDE, DDT,Endosulfan I, Endosulfan II, Endosulfan sulfate, Endrin, Endrin Aldehyde, Heptachlor, Heptachlor Epoxide, PCBs-Water), (EPA 625 for SVOC Acid Extractables and SVOC Base/Neutral Extractables), 600/4-81-045-PCB-Oil. Microbiology Parameters: (ColilertQT SM9223B; Enterolert-QT: SM9222D-MF.) New Hampshire Department of Environmental Services Certificate/Lab ID: 200307. NELAP Accredited. Drinking Water (Inorganic Parameters: SM 9222B, 9223B, 9215B, EPA 200.7, 200.8, 300.0, SM4500CN-E, 4500H+B, 4500NO3-F, 2320B, 2510B, 2540C, 4500F-C, 5310C, 2120B, EPA 332.0. Organic Parameters: 504.1, 524.2.) Non-Potable Water (Inorganic Parameters: SM9222D, 9221B, 9222B, 9221E-EC, EPA 3005A, 200.7, 200.8, 245.1, SW-846 6010B, 6010C, 6020, 6020A, 7196A, 7470A, SM3500-CR-D, EPA 120.1, 300.0, 350.1, 350.2, 351.1, 353.2, 410.4, 420.1, 426C, 1664A, SW-846 9010B, 9030B, 9040B, SM2120B, 2310B, 2320B, 2540B, 2540D, 4500H+B, 4500CL-E, 4500CN-E, 4500NH3-H, 4500NO3-F, 4500NO2-B, 4500P-E, 4500-S2-D, 5210B, 5220D, 2510B, 2540C, 4500F-C, 5310C, 5540C, LACHAT 10-204-00-1-A, LACHAT 10-107-06-2-D, 3060A. Organic Parameters: SW-846 3510C, 3630C, 5030B, 8260B, 8270C, 8270D, 8330, EPA 624, 625, 608, SW-846 8082, 8082A, 8081A, 8081B, 8151A, 8330, 8270C-SIM, 8270D-SIM.) Solid & Chemical Materials (Inorganic Parameters: SW-846 6010B, 6010C, 7196A, 7471A, 1010, 1030, 9010, 9012A, 9014, 9030B, 9040B, 9045C, 9050, 9065,1311, 1312, 3005A, 3050B, 3060A. Organic Parameters: SW-846 3540C, 3546, 3050B, 3580A, 3630C, 5030B, 5035, 8260B, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8330, 8151A, 8015B, 8015C, 8082, 8082A, 8081A, 8081B.) New Jersey Department of Environmental Protection Certificate/Lab ID: MA935. NELAP Accredited. Drinking Water (Inorganic Parameters: SM9222B, 9221E, 9223B, 9215B, 4500CN-CE, 4500NO3-F, 4500F-C, EPA 300.0, 200.7, 200.8, 245.1, 2540C, SM2120B, 2320B, 2510B, 5310C, SM4500H-B. Organic Parameters: EPA 332, 504.1, 524.2.) Non-Potable Water (Inorganic Parameters: SM5210B, EPA 410.4, SM5220D, 4500Cl-E, EPA 300.0, SM2120B, 2340B, SM4500F-BC, EPA 200.7, 200.8, 351.1, LACHAT 10-107-06-2-D, EPA 353.2, SM4500NO3-F, 4500NO2-B, EPA 1664A, SM5310B, C or D, 4500-PE, EPA 420.1, SM510ABC, SM4500P-B5+E, 2540B, 2540C, 2540D, 2540G, EPA 120.1, SM2510B, SM2520B, SM15 426C, 9222D, 9221B, 9221C, 9221E, 9222B, 9215B, 2310B, 2320B, 4500NH3-H, 4500-S D, EPA 350.1, 350.2, SW-846 1312, 7470A, 5540C, SM4500H-B, 4500SO3-B, SM3500Cr-D, 4500CN-CE, EPA 245.1, SW-846 9040B, 3005A, 3015, EPA 6010B, 6010C, 6020, 6020A, 7196A, 3060A, SW-846 9010B, 9030B. Organic Parameters: SW-846 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 3510C, EPA 608, 624, 625, SW-846 3630C, 5030B, 8015C, 8081A, 8081B, 8082, 8082A, 8151A, 8330, 1,4-Dioxane by NJ Modified 8270, 8015B, NJ EPH.) Solid & Chemical Materials (Inorganic Parameters: SW-846, 6010B, 6010C, 6020, 6020A, 7196A, 3060A, 9010B, 9030B, 1010, 1030, 1311, 1312, 3005A, 3050B, 7471A, 7471B, 9014, 9012A, 9040B, 9040C, 9045C, 9045D, 9050A, 9065, 9251. Organic Parameters: SW-846 8015B, 8015C, 8081A, 8081B, 8082, 8082A, 8151A, 8330, 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 3540C, 3546, 3580A, 3630C, 5030B, 5035L, 5035H, NJ OQA-QAM-025 Rev.7, NJ EPH.) New York Department of Health Certificate/Lab ID: 11148. NELAP Accredited. Drinking Water (Inorganic Parameters: SM9223B, 9222B, 9215B, EPA 200.8, 200.7, 245.2, SM5310C, EPA 332.0, SM2320B, EPA 300.0, SM2120B, 4500CN-E, 4500F-C, 4500NO3-F, 2540C, SM 2510B. Organic Parameters: EPA 524.2, 504.1.) Non-Potable Water (Inorganic Parameters: SM9221E, 9222D, 9221B, 9222B, 9215B, 5210B, 5310C, EPA 410.4, SM5220D, 2310B-4a, 2320B, EPA 200.7, 300.0, SM4500CL-E, 4500F-C, SM15 426C, EPA 350.1, SM4500NH3-BH, EPA 351.1, LACHAT 10-107-06-2, EPA 353.2, SM4500-NO3-F, 4500-NO2-B, 4500P-E, 2540C, 2540B, 2540D, EPA 200.8, EPA 6010B, 6010C, 6020, 6020A, EPA 7196A, SM3500Cr-D, EPA 245.1, 245.2, 7470A, SM2120B, LACHAT 10-204-00-1-A, 4500CN-CE, EPA 1664A, EPA 420.1, SM14 510C, EPA 120.1, SM2510B, SM4500S-D, SM5540C, EPA 3005A, 3015, 9010B, 9030B. Organic Parameters: EPA 624, 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 625, 608, 8081A, 8081B, 8151A, 8330, 8082, 8082A, EPA 3510C, 5030B.) Solid & Hazardous Waste (Inorganic Parameters: EPA 1010, 1030, EPA 6010B, 6010C, 7196A, 7471A, 7471B, 9012A, 9014, 9065, 9050A, EPA 1311, 1312, 3005A, 3050B, 9010B, 9040C, 9045D. Organic Parameters: EPA 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8015B, 8015C, 8081A, 8081B, 8151A, 8330, 8082 8082A, 3540C, 3546, 3580, 3580A, 5030B, 5035A-H, 5035A-L.)
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North Carolina Department of the Environment and Natural Resources Certificate/Lab ID : 666. (Inorganic Parameters: SM2310B, 2320B, 4500Cl-E, 4500Cn-E, 9014, Lachat 10-204-00-1-X, 1010A, 1030, 4500NO3-F, 353.2, 4500P-E, 4500SO4-E, 300.0, 4500S-D, 5310B, 5310C, 6010C, 6020A, 200.7, 200.8, 3500Cr-B, 7196A, 245.1, 7471A, 7471B, 1311,1312. Organic Parameters: 608, 8081B, 8082A, 624, 8260B, 625, 8270D, 8151A, 8015C, 504.1, MA-EPH, MA-VPH.) Drinking Water Program Certificate/Lab ID: 25700. (Inorganic Parameters: Chloride EPA 300.0. Organic Parameters: 524.2) Pennsylvania Department of Environmental Protection Certificate/Lab ID : 68-03671. NELAP Accredited. Drinking Water (Inorganic Parameters: 200.7, 200.8, 245.2, 300.0, 332.0, 2120B, 2320B, 2510B, 2540C, 4500-CN-CE, 4500F-C, 4500H+-B, 4500NO3-F, 5310C. Organic Parameters: EPA 524.2, 504.1) Non-Potable Water (Inorganic Parameters: EPA 120.1, 1312, 3005A,3015, 3060A, 200.7, 200.8, 410.4, 1664A, SM2540D, 5210B, 5220D, 4500-P,BE, 245.1, 300.0, 3501., 350.2, 353.2, 420.1, 6010B, 6010C, 6020, 6020A, 7196A, 7470A, 9010B, 9030B, 9040B, Lachat 10-107-06-2-D, NJ-EPH, 2120B, 2310B, 2320B, 2340B, 2510C, 2540B, 2540C, 3500Cr-D, 436C, 4500CN-CE, 4500Cl-E, 4500F-B, 4500F-C, 4500H+-B, 4500NO2-B, 4500NO3-F, 4500S-D, 4500SO3-B, 5310BCD, 5540C. Organic Parameters: EPA 3510C, 3630C, 5030B, 625, 624, 608, 8081A, 8081B, 8082, 8082A, 8151A, 8260B, 8270C, 8270D, 8330, 8015B, ) Solid & Hazardous Waste (Inorganic Parameters: EPA 350.1, 1010, 1030, 1311, 1312, 3005A, 3050B, 3060A, 6010B, 6010C, 6020A, 7196A, 7471A, 7471B, 9010B, 9012A, 9014, 9040B, 9045C, 9050, 9065, SM 4500NH3-BH, 9030B, 9038, 9251. Organic Parameters: 3540C, 3546, 3580A, 3630C, 5035, 8015B, 8015C, 8081A, 8081B, 8082, 8082A, 8151A, 8260B, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8330, NJ-EPH.) Rhode Island Department of Health Certificate/Lab ID: LAO00065. NELAP Accredited via NJ-DEP. Refer to MA-DEP Certificate for Potable and Non-Potable Water. Refer to NJ-DEP Certificate for Potable and Non-Potable Water. Texas Commisson on Environmental Quality Certificate/Lab ID: T104704476-09-1. NELAP Accredited. Non-Potable Water (Inorganic Parameters: EPA 120.1, 1664, 200.7, 200.8, 245.1, 245.2, 300.0, 350.1, 351.1, 353.2, 410.4, 420.1, 6010, 6020, 7196, 7470, 9040, SM 2120B, 2310B, 2320B, 2510B, 2540B, 2540C, 2540D, 426C, 4500CL-E, 4500CN-E, 4500F-C, 4500H+B, 4500NH3-H, 4500NO2B, 4500P-E, 4500 S2¯D, 510C, 5210B, 5220D, 5310C, 5540C. Organic Parameters: EPA 608, 624, 625, 8081, 8082, 8151, 8260, 8270, 8330.) Solid & Hazardous Waste (Inorganic Parameters: EPA 1311, 1312, 9012, 9014, 9040, 9045, 9050, 9065.) Virginia Division of Consolidated Laboratory Services Certificate/Lab ID: 460195. NELAP Accredited. Drinking Water (Inorganic Parameters: EPA 200.7, 200.8, 300.0, 2510B, 2120B, 2540C, 4500CN-CE, 245.2, 2320B, 4500F-C, 4500F-C, 4500NO3-F, 5310C. Organic Parameters: EPA 504.1, 524.2.) Non-Potable Water (Inorganic Parameters: EPA 120.1, 1664A, 200.7, 2..08, 245.1, 300.0, 3005A, 3015, 1312, 6010B, 6010C, 3060A, 353.2, 420.1, 6020, 6020A, SM4500S-D, SM4500-CN-CE, Lachat 10-204-00-1-X, 7196A, 7470A, 9010B, 9040B, 2310B, 2320B, 2510B, 2540B, 2540C, 3500Cr-D, 426C, 4500Cl-E, 4500F-B, 4500F-C, 4500PE, 510AC, 5210B, 5310B 5310C, 5540C. Organic Parameters: EPA 3510C, 3630C, 5030B, 8260B, 608, 624, 625, 8081A, 8081B, 8082, 8082A, 8151A, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8330, ) Solid & Hazardous Waste (Inorganic Parameters: EPA 1010A, 1030, 3060A, 3050B, 1311, 1312, 6010B, 6010C, 6020, , 7196A, 7471A, 7471B, 6020A, 9030B, 9010B, 9012A, 9014 9040B, 9045C, 9050A, 9065. Organic Parameters: EPA 5035, 3540C, 3546, 3550, 3580, 3630C, 8260B, 8015B, 8015C, 8081A, 8081B, 8082, 8082A, 8151A, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8330.) Department of Defense, L-A-B Certificate/Lab ID: L2217. Drinking Water (Inorganic Parameters: SM 4500H-B. Organic Parameters: EPA 524.2, 504.1.) Non-Potable Water (Inorganic Parameters: EPA 200.7, 200.8, 6010B, 6010C, 6020, 6020A, 245.1, 245.2, 7470A, 9040B, 9010B, 180.1. 300.0, 332.0, 6860, 353.2, 410.4, 9060, 1664A, SM 4500CN-E, 4500H-B, 4500NO3-F, 4500CL-D, 5220D, 5310C, 2130B, 2320B, 2540C, 3005A, 3015, 9010B, 9056. Organic Parameters: EPA 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8330A, 8082, 8082A, 8081A, 8081B, 3510C, 5030B, MassDEP EPH, MassDEP VPH.)
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Solid & Hazardous Waste (Inorganic Parameters: EPA 200.7, 6010B, 6010C, 7471A, 6860, 1311, 1312, 3050B, 7196A, 9010B, 9012A, 9040B, 9045C, 3500-CR-D, 4500CN-CE, 2540G, Organic Parameters: EPA 8260B, 8260C, 8270C, 8270D, 8270C-SIM, 8270D-SIM, 8330A/B-prep, 8082, 8082A, 8081A, 8081B, 3540C, 3546, 3580A, 5035A, MassDEP EPH, MassDEP VPH.) The following analytes are not included in our current NELAP/TNI Scope of Accreditation: EPA 8260B: Freon-113, 1,2,4,5-Tetramethylbenzene, 4-Ethyltoluene. EPA 8330A: PETN, Picric Acid, Nitroglycerine, 2,6-DANT, 2,4-DANT. EPA 8270C: Methyl naphthalene, Dimethyl naphthalene, Total Methylnapthalenes, Total Dimethylnaphthalenes, 1,4-Diphenylhydrazine (Azobenzene). EPA 625: 4-Chloroaniline, 4-Methylphenol. Total Phosphorus in a soil matrix, Chloride in a soil matrix, TKN in a soil matrix, NO2 in a soil matrix, NO3 in a soil matrix, SO4 in a soil matrix. EPA 9071: Total Petroleum Hydrocarbons, Oil & Grease.
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ENVIRONMENTAL SAMPLE CHAIN OF CUSTODY~ ~ANCHOR'/..., OEA~305 W Grand Ava Sullo 300, Monlvolo, Now Jer.oy 07545; ph: 201.930.9890
Client: Newtown Creek Group Project: Newtown Creek
COCID:
Sample Custodian:
Lab:
AAL-20121 006-164742
Ib
Alpha Analytical Labs
cocCollected # LabSample Field Sample ID Matrix Containers Analytical Program ac'Number Date Time
001 TN005SG-000014.20121005 SE 10/05/2012 09:32 B Newtown Creek Surface Sediment 0002 TN002SG-000011-20 121005 SE 10/05/2012 10:41 8 Newtown Creek Surface Sediment 0003 TN003SG-000015-20121005 SE 10/05/2012 11:24 8 Newtown Creek Surface Sediment 0
<t 004 TN004SG.000015-20121005 SE 10/05/2012 11:46 8 Newtown Creek Surface Sediment 0/0 005 TN006SG.000015.20121 005 SE 10/05/2012 13:16 8 Newtown Creek Surface Sediment 0
I 12 006 SG.RB.20121006 wa 10/06/2012 09:05 9 Newtown Creek Rinse Blank Sediment Surface 0N 007 HB008SG.000015.20121006 SE 10/06/2012 09:55 8 Newtown Creek Surface Sediment 0(c" 008 HB007SG-000015.20121 006 SE 10/06/2012 10:45 8 Newtown Creek Surface Sediment 0Cb 009 HB006SG-000015-20121 006 SE 10/06/2012 11:30 8 Newtown Creek Surface Sediment 0;;. 010 HB005SG.000015.20121 006 SE 10/06/2012 12:19 8 Newtown Creek Surface Sediment 0Itt 011 HB1005SG.000015-20121006 SE 10/06/2012 12:19 7 Newtown Creek Surface Sediment 0
02"" 012 HB004SG.000015-20121 006 SE 10/06/2012 13:27 8 Newtown Creek Surface Sediment 0,Z~ 013 HB003SG.0000 15-20 121006 SE 10/06/2012 14:21 8 Newtown Creek Surface Sediment 0,t6 014 HB002SG-000015-20121 006 SE 10/06/2012 15:05 8 Newtown Creek Surface Sediment 0!fJ 015 HB001 SG.000015.20121 006 SE 10/06/2012 15:54 8 Newtown Creek Surface Sediment 0I 016 SG.TB.20121 006 WQ 10/06/2012 16:23 2 Newtown Creek Trip Blank 0
<1,I,{;L -':>,ll,{'1.-Zt.1,3,25).1,2Q.}
Comment:
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SAMPLE_CUSTO
LAB_QC COC_ID DIANNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006.164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-2"0121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL.20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006.164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 Ib
TURN_A CONTAINROUND_ TAT_UN I ER_COUTIME T NT-1 DAYS 130 DAYS 030 DAYS 130 DAYS 145 DAYS 045 DAYS 130 DAYS 030 DAYS 030 DAYS 037 DAYS 130 DAYS 030 DAYS 030 DAYS 030 DAYS 130 DAYS 030 DAYS 130 DAYS 030 DAYS 1-1 DAYS 130 DAYS 030 DAYS 130 DAYS 145 DAYS 045 DAYS 130 DAYS 030 DAYS 030 DAYS 037 DAYS 130 DAYS 030 DAYS 030 DAYS 030 DAYS 130 DAYS 030 DAYS 130 DAYS 030 DAYS 1-1 DAYS 130 DAYS 030 DAYS 130 DAYS 145 DAYS 045 DAYS 130 DAYS 030 DAYS 030 DAYS 037 DAYS 130 DAYS 030 DAYS 030 DAYS 030 DAYS 130 DAYS 030 DAYS 130 DAYS 030 DAYS 1-1 DAYS 1
METHODNAASTM D7263ASTM D422EPA 6010B/6020EPA 8015 modified, AlphaEPA 8270-SIM mod, Alpha SEPA 90450SM4500NH3-BHEPA 9010BEPA 1631MSM4500N03-FGustafsson, et aI., 1997SM4500P-ESM4500Norg-CEPA 9060EPA 9030BEPA 160.3EPA 8260BNAASTM 07263ASTM 0422EPA 601OB/6020EPA 8015 modified, AlphaEPA 8270-SIM mod, Alpha SEPA 9045DSM4500NH3-BHEPA 9010BEPA 1631MSM4500N03-FGustafsson, et aI., 1997SM4500P-ESM4500Norg-CEPA 9060EPA 9030BEPA 160.3EPA 8260BNAASTM D7263ASTM D422EPA 601OB/6020EPA 8015 modified, AlphaEPA 8270-SIM mod, Alpha SEPA 90450SM4500NH3-BHEPA 9010BEPA 1631MSM4500N03-FGustafsson, et aI., 1997SM4500P-ESM4500Norg-CEPA 9060EPA 9030BEPA 160.3EPA 8260BNA
Page 1 of 5
SAMPLE_ SAMPLEMATRIX DATE 31ME TEST_REQUEST
SE 10/6/2012 15:54 ArchiveSE 10/6/2012 15:54 DensitySE 10/6/2012 15:54 GrainsizeSE 10/6/2012 15:54 Metals, totalSE 10/6/2012 15:54 n-alkanes & isoprenoids (inc. DRO & TPH)SE 10/6/2012 15:54 PAHs & alkyl PAHsSE 10/6/2012 15:54 pHSE 10/6/2012 15:54 Sediment AmmoniaSE 10/6/2012 15:54 Sediment Cyanide, TotalSE 10/6/2012 15:54 Sediment MercurySE 10/6/2012 15:54 Sediment Nitrate/NitriteSE 10/6/2012 15:54 Soot CarbonSE 10/6/2012 15:54 Sediment Phosphorus, TotalSE 10/6/2012 15:54 SedimentTKNSE 10/6/2012 15:54 Sediment TOCSE 10/6/2012 15:54 SulfideSE 10/6/2012 15:54 Total SolidsSE 10/6/2012 15:54 VOCsSE 10/6/2012 15:05 ArchiveSE 10/6/2012 15:05 DensitySE 10/6/2012 15:05 GrainsizeSE 10/6/2012 15:05 Metals, totalSE 10/6/2012 15:05 n-alkanes & isoprenoids (inc. DRO & TPH)SE 10/6/2012 15:05 PAHs & alkyl PAHsSE 10/6/2012 15:05 pHSE 10/6/2012 15:05 Sediment AmmoniaSE 10/6/2012 15:05 Sediment Cyanide, TotalSE 10/6/2012 15:05 Sediment MercurySE 10/6/2012 15:05 Sediment Nitrate/NitriteSE 10/6/2012 15:05 Soot CarbonSE 10/6/2012 15:05 Sediment Phosphorus, TotalSE 10/6/2012 15:05 Sediment TKNSE 10/6/2012 15:05 Sediment TOCSE 10/6/2012 15:05 SulfideSE 10/6/2012 15:05 Total SolidsSE 10/6/2012 15:05 VOCsSE 10/6/2012 14:21 ArchiveSE 10/6/2012 14:21 DensitySE 10/6/2012 14:21 GrainsizeSE 10/6/2012 14:21 Metals, totalSE 10/6/2012 14:21 n-alkanes & isoprenoids (inc. ORO & TPH)SE 10/6/2012 14:21 PAHs & alkyl PAHsSE 10/6/2012 14:21 pHSE 10/6/2012 14:21 Sediment AmmoniaSE 10/6/2012 14:21 Sediment Cyanide, TotalSE 10/6/2012 14:21 Sediment MercurySE 10/6/2012 14:21 Sediment Nitrate/NitriteSE 10/6/2012 14:21 Soot CarbonSE 10/6/2012 14:21 Sediment Phosphorus, TotalSE 10/6/2012 14:21 Sediment TKNSE 10/6/2012 14:21 Sediment TOCSE 10/6/2012 14:21 SulfideSE 10/6/2012 14:21 Total SolidsSE 10/6/2012 14:21 VOCsSE 10/6/2012 13:27 Archive
FIELD_SAMPLE_IDHBOOlSG-000015-20121 006HBOOlSG-000015-20121 006HBOOlSG-000015-20121 006HBOOlSG-000015-20121 006HBOOlSG-000015-20121 006HBOOlSG-000015-20121 006HBOOlSG-000015-20121 006HBOOlSG-000015-20121 006HBOOlSG-000015-20121 006HBOOlSG-000015-20121 006HBOOlSG-000015-20121 006HBOOlSG-000015-20121 006HBOOlSG-000015-20121 006HBOOlSG-000015-20121 006HBOOlSG-000015-20121 006HBOOlSG-000015-20121 006HB001SG-000015-20121 006HB001SG-000015-20121 006HB002SG-000015-20121 006HB002SG-000015-20121 006HB002SG-000015-20121 006HB002SG-000015-20121 006HB002SG-000015-20121 006HB002SG-000015-20121 006HB002SG-000015-20121 006HB002SG-000015-20121 006HB002SG-0000 15-20121006HB002SG-0000 15-20121006HB002SG-000015-20121 006HB002SG-000015-20121 006HB002SG-000015-20121006HB002SG-000015-20121 006HB002SG-000015-20121 006HB002SG-000015-20121 006HB002SG-000015-20121 006HB002SG-000015-20121 006HB003SG-000015-20121 006HB003SG-000015-20121 006HB003SG-000015-20121 006HB003SG-000015-20121 006HB003SG-000015-20121 006HB003SG-000015-20121 006HB003SG-000015-20121 006HB003SG-000015-20121 006HB003SG-000015-20121 006HB003SG-000015-20121 006HB003SG-000015-20121 006HB003SG-000015-20121 006HB003SG-000015-20121 006HB003SG-000015-20121 006HB003SG-000015-20121 006HB003SG-0000 15-20121006HB003SG-000015-20121 006HB003SG-000015-20121 006HB004SG-000015-20121 006
Serial_No:11051209:46
Page 270 of 279
SAMPLE_CUSTO
LAB_QC COC_'D DIANNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 Ib
TURN_A CONTAINROUND_ TAT_UNI ER_COUTIME T NT30 DAYS 030 DAYS 130 DAYS 145 DAYS 045 DAYS 130 DAYS 030 DAYS 030 DAYS 037 DAYS 130 DAYS 030 DAYS 030 DAYS 030 DAYS 130 DAYS 030 DAYS 130 DAYS 030 DAYS 1-1 DAYS 130 DAYS 030 DAYS 130 DAYS 145 DAYS 045 DAYS 130 DAYS 030 DAYS 030 DAYS 037 DAYS 130 DAYS 030 DAYS 030 DAYS 030 DAYS 130 DAYS 030 DAYS 130 DAYS 030 DAYS 1-1 DAYS 130 DAYS 030 DAYS 130 DAYS 145 DAYS 045 DAYS 130 DAYS 030 DAYS 030 DAYS 037 DAYS 130 DAYS 030 DAYS 030 DAYS 030 DAYS 130 DAYS 030 DAYS 130 DAYS 030 DAYS 1-1 DAYS 130 DAYS 0
METHODASTM D7263ASTM D422EPA 6010B/6020EPA 8015 modified, AlphaEPA 8270-SIM mod, Alpha SEPA 9045DSM4500NH3-BHEPA 9010BEPA 1631MSM4500N03-FGustafsson, e1aI., 1997SM4500P-ESM4500Norg-CEPA 9060EPA 9030BEPA 160.3EPA 8260BNAASTM D7263ASTM D422EPA 6010B/6020EPA 8015 modified, AlphaEPA 8270-SIM mod, Alpha SEPA 9045DSM4500NH3-BHEPA 9010BEPA 1631MSM4500N03-FGustafsson, et aI., 1997SM4500P-ESM4500Norg-CEPA 9060EPA 9030BEPA 160.3EPA 8260BNAASTM D7263ASTM D422EPA 601OB/6020EPA 8015 modified, AlphaEPA 8270-SIM mod, Alpha SEPA 9045DSM4500NH3-BHEPA 9010BEPA 1631MSM4500N03-FGus1afsson, et aI., 1997SM4500P-ESM4500Norg-CEPA 9060EPA 9030BEPA 160.3EPA 8260BNAASTM D7263
Page 2 of 5
SAMPLE_ SAMPLEMATRIX DATE _TIME TEST_REQUEST
SE 10/6/2012 13:27 DensitySE 10/6/2012 13:27 GrainsizeSE 10/6/2012 13:27 Metals, totalSE 10/6/2012 13:27 n-alkanes & isoprenoids (inc. DRO & TPH)SE 10/6/2012 13:27 PAHs & alkyl PAHsSE 10/6/2012 13:27 pHSE 10/6/2012 13:27 Sediment AmmoniaSE 10/6/2012 13:27 Sediment Cyanide, TotalSE 10/6/2012 13:27 Sediment MercurySE 10/6/2012 13:27 Sediment Nitrate/NitriteSE 10/6/2012 13:27 Soot CarbonSE 10/6/2012 13:27 Sediment Phosphorus, TotalSE 10/6/2012 13:27 SedimentTKNSE 10/6/2012 13:27 SedimentTOCSE 10/6/2012 13:27 SulfideSE 10/6/2012 13:27 Total SolidsSE 10/6/2012 13:27 VOCsSE 10/6/2012 12:19 ArchiveSE 10/6/2012 12:19 DensitySE 10/6/2012 12:19 GrainsizeSE 10/6/2012 12:19 Metals, t01alSE 10/6/2012 12:19 n-alkanes & isoprenoids (inc. DRO & TPH)SE 10/6/2012 12:19 PAHs & alkyl PAHsSE 10/6/2012 12:19 pHSE 10/6/2012 12:19 Sediment AmmoniaSE 10/6/2012 12:19 Sediment Cyanide, T01alSE 10/6/2012 12:19 Sediment MercurySE 10/6/2012 12:19 Sediment Nitrate/NitriteSE 10/6/2012 12:19 Soot CarbonSE 10/6/2012 12:19 Sediment Phosphorus, TotalSE 10/6/2012 12:19 Sediment TKNSE 10/6/2012 12:19 Sediment TOCSE 10/6/2012 12:19 SulfideSE 10/6/2012 12:19 Total SolidsSE 10/6/2012 12:19 VOCsSE 10/6/2012 11:30 ArchiveSE 10/6/2012 11:30 DensitySE 10/6/2012 11:30 GrainsizeSE 10/6/2012 11:30 Metals, totalSE 10/6/2012 11:30 n-alkanes & isoprenoids (inc. DRO & TPH)SE 10/6/2012 11:30 PAHs & alkyl PAHsSE 10/6/2012 11:30 pHSE 10/6/2012 11:30 Sediment AmmoniaSE 10/6/2012 11:30 Sediment Cyanide, TotalSE 10/6/2012 11:30 Sediment MercurySE 10/6/2012 11:30 Sediment Nitrate/NitriteSE 10/6/2012 11:30 Soot CarbonSE 10/6/2012 11:30 Sediment Phosphorus, TotalSE 10/6/2012 11:30 Sediment TKNSE 10/6/2012 11:30 Sediment TOCSE 10/6/2012 11:30 SulfideSE 10/6/201211:30 TotalSolidsSE 10/6/2012 11:30 VOCsSE 10/6/2012 10:45 ArchiveSE 10/6/2012 10:45 Density
FIELD_SAMPLE_IDHB004SG-000015-20121 006HB004SG-000015-20121006HB004SG-000015-20121006HB004SG-000015-20121 006HB004SG-000015-20121 006HB004SG-0000 15-20121006HB004SG-000015-20121 006HB004SG-000015-20121 006HB004SG-000015-20121 006HB004SG-000015-20121 006HB004SG-000015-20121 006HB004SG-000015-20121 006HB004SG-000015-20121 006HB004SG-000015-20121006HB004SG-000015-20121006HB004SG-000015-20121006HB004SG-000015-20121006HB005SG-000015-20121006HB005SG-000015-20121 006HB005SG-000015-20121 006HB005SG-000015-20121006HB005SG-000015-20121 006HB005SG-000015-20121 006HB005SG-000015-20121006HB005SG-0000 15-20121006HB005SG-000015-20121 006HB005SG-000015-20121006HB005SG-000015-20121006HB005SG-000015-20121 006HB005SG-0000 15-20121006HB005SG-000015-20121 006HB005SG-000015-20121 006HB005SG-000015-20121 006HB005SG-000015-20121 006HB005SG-000015-20121 006HB006SG-000015-20121 006HB006SG-000015-20121 006HB006SG-000015-20121006HB006SG-000015-20121 006HB006SG-000015-20121 006HB006SG-000015-20121 006HB006SG-000015-20121 006HB006SG-000015-20121006HB006SG-000015-20121006HB006SG-000015-20121006HB006SG-000015-20121006HB006SG-000015-20121 006HB006SG-000015-20121006HB006SG-000015-20121 006HB006SG-000015-20121 006HB006SG-000015-20121 006HB006SG-000015-20121006HB006SG-000015-20121006HB007SG-000015-20121006HB007SG-000015-20121 006
Serial_No:11051209:46
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FIELD_SAMPLE_IDHB007SG-000015-20121 006HB007SG-000015-20121 006HB007SG-000015-20121 006HB007SG-000015-20121 006HB007SG-0000 15-20121006HB007SG-000015-20121 006HB007SG-000015-20121 006HB007SG-000015-20121 006HB007SG-000015-20121 006HB007SG-000015-20121 006HB007SG-000015-20121 006HB007SG-000015-20121 006HB007SG-000015-20121 006HB007SG-000015-20121 006HB007SG-000015-20121 006HB007SG-000015-20121 006HB008SG-000015-20121 006HB008SG-000015-20121 006HB008SG-000015-20121 006HB008SG-000015-20121006HB008SG-000015-20121 006HB008SG-000015-20121 006HB008SG-000015-20121006HB008SG-000015-20121006HB008SG-000015-20121006HB008SG-000015-20121 006HB008SG-000015-20121 006HB008SG-000015-20121 006HB008SG-000015-20121 006HB008SG-000015-20121 006HB008SG-000015-20121 006HB008SG-000015-20121 006HB008SG-000015-20121 006HB008SG-000015-20121 006HB1005SG-000015-20121 006HBI 005SG-000015-20121 006HB1005SG-000015-20121 006HB1005SG-000015-20121 006HB1005SG-000015-20121 006HB1005SG-000015-20121 006HB1005SG-000015-20121006HB1005SG-000015-20121 006HB1005SG-000015-20121 006HB1005SG-000015-20121 006HB1005SG-000015-20121 006HB1005SG-000015-20121006HBI 005SG-000015-20121 006HB1005SG-000015-20121006HBI 005SG-000015-20121 006HB1005SG-0000 15-20121006HBI 005SG-000015-20121 006SG-RB-20121 006SG-RB-20121 006SG-RB-20121006SG-RB-20121 006
SAMPLE_ SAMPLEMATRIX DATE _TIME TEST_REQUEST
SE 10/6/2012 10:45 GrainsizeSE 10/6/2012 10:45 Metals, totalSE 10/6/2012 10:45 n-alkanes & isoprenoids (inc. ORO & TPH)SE 10/6/2012 10:45 PAHs & alkyl PAHsSE 10/6/2012 10:45 pHSE 10/6/2012 10:45 Sediment AmmoniaSE 10/6/2012 10:45 Sediment Cyanide, TotalSE 10/6/2012 10:45 Sediment MercurySE 10/6/2012 10:45 Sediment Nitrate/NitriteSE 10/6/2012 10:45 Soot CarbonSE 10/6/2012 10:45 Sediment Phosphorus, TotalSE 10/6/2012 10:45 Sediment TKNSE 10/6/2012 10:45 Sediment TOCSE 10/6/2012 10:45 SulfideSE 10/6/2012 10:45 Total SolidsSE 10/6/2012 10:45 VOCsSE 10/6/2012 9:55 ArchiveSE 10/6/2012 9:55 DensitySE 10/6/2012 9:55 GrainsizeSE 10/6/2012 9:55 Metals, totalSE 10/6/2012 9:55 n-alkanes & isoprenoids (inc. ORO & TPH)SE 10/6/2012 9:55 PAHs & alkyl PAHsSE 10/6/2012 9:55 pHSE 10/6/2012 9:55 Sediment AmmoniaSE 10/6/2012 9:55 Sediment Cyanide, TotalSE 10/6/2012 9:55 Sediment MercurySE 10/6/2012 9:55 Sediment Nitrate/NitriteSE 10/6/2012 9:55 Soot CarbonSE 10/6/2012 9:55 Sediment Phosphorus, TotalSE 10/6/2012 9:55 SedimentTKNSE 10/6/2012 9:55 Sediment TOCSE 10/6/2012 9:55 SulfideSE 10/6/2012 9:55 Total SolidsSE 10/6/2012 9:55 VOCsSE 10/6/2012 12:19 DensitySE 10/6/2012 12:19 GrainsizeSE 10/6/2012 12:19 Metals, totalSE 10/6/2012 12:19 n-alkanes & isoprenoids (inc. ORO & TPH)SE 10/6/2012 12:19 PAHs & alkyl PAHsSE 10/6/2012 12:19 pHSE 10/6/2012 12:19 Sediment AmmoniaSE 10/6/2012 12:19 Sediment Cyanide, TotalSE 10/6/2012 12:19 Sediment MercurySE 10/6/2012 12:19 Sediment Nitrate/NitriteSE 10/6/2012 12:19 Soot CarbonSE 10/6/2012 12:19 Sediment Phosphorus, TotalSE 10/6/2012 12:19 Sediment TKNSE 10/6/2012 12:19 Sediment TOCSE 10/6/2012 12:19 SulfideSE 10/6/2012 12:19 Total SolidsSE 10/6/2012 12:19 VOCsWQ 10/6/2012 9:05 Metals, totalWQ 10/6/2012 9:05 n-alkanes & isoprenoids (inc. ORO & TPH)WQ 10/6/2012 9:05 PAHs & alkyl PAHsWQ 10/6/2012 9:05 Sediment Mercury
METHODASTM 0422EPA 6010B/6020EPA 8015 modified, AlphaEPA 8270-SIM mod, Alpha SEPA 90450SM4500NH3-BHEPA 9010BEPA 1631MSM4500N03-FGustafsson, et aI., 1997SM4500P-ESM4500Norg-CEPA 9060EPA 9030BEPA 160.3EPA 8260BNAASTM 07263ASTM 0422EPA 6010B/6020EPA 8015 modified, AlphaEPA 8270-SIM mod, Alpha SEPA 90450SM4500NH3-BHEPA 9010BEPA 1631MSM4500N03-FGustafsson, et aI., 1997SM4500P-ESM4500Norg-CEPA 9060EPA 9030BEPA 160.3EPA 8260BASTM 07263ASTM 0422EPA 6010B/6020EPA 8015 modified, AlphaEPA 8270-SIM mod, Alpha SEPA 90450SM4500NH3-BHEPA 9010BEPA 1631MSM4500N03-FGustafsson, et aI., 1997SM4500P-ESM4500Norg-CEPA 9060EPA 9030BEPA 160.3EPA 8260BEPA 6010B/6020EPA 8015 modified, AlphaEPA 8270-SIM mod, Alpha SEPA 1631M
TURN_A CONTAINROUND_ TAT_UNI ER_COUTIME T NT30 DAYS 130 DAYS 145 DAYS 045 DAYS 130 DAYS 030 DAYS 030 DAYS 037 DAYS 130 DAYS 030 DAYS 030 DAYS 030 DAYS 130 DAYS 030 DAYS 130 DAYS 030 DAYS 1-1 DAYS 130 DAYS 030 DAYS 130 DAYS 145 DAYS 045 DAYS 130 DAYS 030 DAYS 030 DAYS 037 DAYS 130 DAYS 030 DAYS 030 DAYS 030 DAYS 130 DAYS 030 DAYS 130 DAYS 030 DAYS 130 DAYS 030 DAYS 130 DAYS 145 DAYS 045 DAYS 130 DAYS 030 DAYS 030 DAYS 037 DAYS 130 DAYS 030 DAYS 030 DAYS 030 DAYS 130 DAYS 030 DAYS 130 DAYS 030 DAYS 130 DAYS 145 DAYS 245 DAYS 237 DAYS 1
SAMPLE_CUSTO
LAB_QC COC_ID DIANNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20t21006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 Ib
Page 3 of 5
Serial_No:11051209:46
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SAMPLE_CUSTO
LAB_QC COC_ID DIANNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 lbNO AAL-20121006-164742 lbNO AAL-20121006-164742 lbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 lbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 lbNO AAL-20121006-164742 lbNO AAL-20121006-164742 lbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 lbNO AAL-20121006-164742 lbNO AAL-20121006-164742 lbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 lbNO AAL-20121006-164742 IbNO AAL-20121006-164742 lbNO AAL-20121006-164742 lbNO AAL-20121006-164742 lbNO AAL-20121006-164742 lbNO AAL-20121006-164742 lbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 Ib
TURN_A CONTAINROUND_ TAT_UNI ER_COUTIME T NT30 DAYS 345 DAYS 2-1 DAYS 130 DAYS 030 DAYS 130 DAYS 145 DAYS 045 DAYS 130 DAYS 030 DAYS 030 DAYS 037 DAYS 130 DAYS 030 DAYS 030 DAYS 030 DAYS 130 DAYS 030 DAYS 130 DAYS 030 DAYS 1-1 DAYS 130 DAYS 030 DAYS 130 DAYS 145 DAYS 045 DAYS 130 DAYS 030 DAYS 030 DAYS 037 DAYS 130 DAYS 030 DAYS 030 DAYS 030 DAYS 130 DAYS 030 DAYS 130 DAYS 030 DAYS 1-1 DAYS 130 DAYS 030 DAYS 130 DAYS 145 DAYS 045 DAYS 130 DAYS 030 DAYS 030 DAYS 037 DAYS 130 DAYS 030 DAYS 030 DAYS 030 DAYS 130 DAYS 030 DAYS 130 DAYS 0
METHODEPA 8260BEPA 8260BNAASTM D7263ASTM D422EPA 6010B/6020EPA 8015 modified, AlphaEPA 8270-SIM mod, Alpha SEPA 9045DSM4500NH3-BHEPA 9010BEPA 1631MSM4500N03-FGustafsson, et aI., 1997SM4500P-ESM4500Norg-CEPA 9060EPA 9030BEPA 160.3EPA 8260BNAASTM D7263ASTM D422EPA 6010B/6020EPA 8015 modified, AlphaEPA 8270-SIM mod, Alpha SEPA 9045DSM4500NH3-BHEPA 9010BEPA 1631MSM4500N03-FGustafsson, et aI., 1997SM4500P-ESM4500Norg-CEPA 9060EPA 9030BEPA 160.3EPA 8260BNAASTM D7263ASTM D422EPA 6010B/6020EPA 8015 modified, AlphaEPA 8270-SIM mod, Alpha SEPA 9045DSM4500NH3-BHEPA 9010BEPA 1631MSM4500N03-FGustafsson, et aI., 1997SM4500P-ESM4500Norg-CEPA 9060EPA 9030BEPA 160.3
Page 4 of 5
SAMPLE_ SAMPLEMATRIX DATE _TIME TEST_REQUESTWQ 10/6/2012 9:05 VOCsWQ 10/6/2012 16:23 VOCsSE 10/5/2012 10:41 ArchiveSE 10/5/2012 10:41 DensitySE 10/5/2012 10:41 GrainsizeSE 10/5/2012 10:41 Metals, totalSE 10/5/2012 10:41 n-alkanes & isoprenoids (inc. DRO & TPH)SE 10/5/2012 10:41 PAHs & alkyl PAHsSE 10/5/2012 10:41 pHSE 10/5/2012 10:41 Sediment AmmoniaSE 10/5/2012 10:41 Sediment Cyanide, TotalSE 10/5/2012 10:41 Sediment MercurySE 10/5/2012 10:41 Sediment Nitrate/NitriteSE 10/5/2012 10:41 Soot CarbonSE 10/5/2012 10:41 Sediment Phosphorus, TotalSE 10/5/2012 10:41 Sediment TKNSE 10/5/2012 10:41 SedimentTOCSE 10/5/2012 10:41 SulfideSE 10/5/2012 10:41 Total SolidsSE 10/5/2012 10:41 VOCsSE 10/5/2012 11:24 ArchiveSE 10/5/2012 11:24 DensitySE 10/5/2012 11:24 GrainsizeSE 10/5/2012 11:24 Metals, totalSE 10/5/2012 11:24 n-alkanes & isoprenoids (inc. DRO & TPH)SE 10/5/2012 11:24 PAHs & alkyl PAHsSE 10/5/2012 11:24 pHSE 10/5/2012 11:24 Sediment AmmoniaSE 10/5/2012 11:24 Sediment Cyanide, TotalSE 10/5/2012 11:24 Sediment MercurySE 10/5/2012 11:24 Sediment Nitrate/NitriteSE 10/5/2012 11:24 Soot CarbonSE 10/5/2012 11:24 Sediment Phosphorus, TotalSE 10/5/2012 11:24 Sediment TKNSE 10/5/2012 11:24 Sediment TOCSE 10/5/2012 11:24 SulfideSE 10/5/2012 11:24 Total SolidsSE 10/5/2012 11:24 VOCsSE 10/5/2012 11:46 ArchiveSE 10/5/2012 11:46 DensitySE 10/5/2012 11:46 GrainsizeSE 10/5/2012 11:46 Metals, totalSE 10/5/2012 11:46 n-alkanes & isoprenoids (inc. DRO & TPH)SE 10/5/2012 11:46 PAHs & alkyl PAHsSE 10/5/2012 11:46 pHSE 10/5/2012 11:46 Sediment AmmoniaSE 10/5/2012 11:46 Sediment Cyanide, TotalSE 10/5/2012 11:46 Sediment MercurySE 10/5/2012 11:46 Sediment Nitrate/NitriteSE 10/5/2012 11:46 Soot CarbonSE 10/5/2012 11:46 Sediment Phosphorus, TotalSE 10/5/2012 11:46 SedimentTKNSE 10/5/2012 11:46 Sediment TOCSE 10/5/2012 11:46 SulfideSE 10/5/2012 11:46 Total Solids
FIELD_SAMPLE_IDSG-RB-20121 006SG-TB-20121 006TN002SG-000011-20121005TN002SG-000011-20121005TN002SG-000011-20121005TN002SG-000011-20 121005TN002SG-000011-20121005TN002SG-000011-20121005TN002SG-000011-20121005TN002SG-000011-20121005TN002SG-000011-20121005TN002SG-000011-20121005TN002SG-000011-20121005TN002SG-000011-20121005TN002SG-000011-20121005TN002SG-000011-20121005TN002SG-000011-20121005TN002SG-000011-20121005TN002SG-000011-20121005TN002SG-000011-20121005TN003SG-000015-20121 005TN003SG-000015-20121 005TN003SG-000015-20121 005TN003SG-000015-20121 005TN003SG-000015-20121005TN003SG-000015-20121005TN003SG-000015-20121005TN003SG-000015-20121005TN003SG-000015-20121005TN003SG-0000 15-20121005TN003SG-000015-20121005TN003SG-000015-20 121005TN003SG-0000 15-20121005TN003SG-000015-20 121005TN003SG-000015-20121005TN003SG-000015-20 121005TN003SG-000015-20 121005TN003SG-000015-20 121005TN004SG-000015-20121005TN004SG-000015-20121 005TN004SG-000015-20121 005TN004SG-000015-20121 005TN004SG-000015-20121 005TN004SG-000015-20121 005TN004SG-000015-20121 005TN004SG-000015-20121 005TN004SG-000015-20121 005TN004SG-000015-20121005TN004SG-000015-20121 005TN004SG-000015-20121 005TN004SG-000015-20121 005TN004SG-000015-20121 005TN004SG-000015-20121 005TN004SG-000015-20121005TN004SG-000015-20121 005
Serial_No:11051209:46
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FIELD_SAMPLE_'DTN004SG-000015-20121005TN005SG-000014-20 121005TN005SG-000014-20121 005TN005SG-000014-20121 005TN005SG-000014-20121 005TN005SG-000014-20121 005TN005SG-000014-20121 005TN005SG-000014-20121 005TN005SG-000014-20121 005TN005SG-000014-20121 005TN005SG-000014-20121 005TN005SG-000014-20121005TN005SG-000014-20 121005TN005SG-000014-20121005TN005SG-000014-20121 005TN005SG-000014-20121 005TN005SG-000014-20121 005TN005SG-000014-20121 005TN005SG-0000 14-20121005TN006SG-000015-20121 005TN006SG-000015-20121 005TN006SG-000015-20121 005TN006SG-000015-20121 005TN006SG-000015-20121 005TN006SG-000015-20121 005TN006SG-000015-20121 005TN006SG-000015-20121 005TN006SG-000015-20121005TN006SG-000015-20121 005TN006SG-000015-20121 005TN006SG-0000 15-20121005TN006SG-000015-20121005TN006SG-000015-20121005TN006SG-000015-20121005TN006SG-000015-20 121005TN006SG-000015-20 121005TN006SG-0000 15-20121005
SAMPLE_ SAMPLEMATRIX DATE _TIME TEST_REQUEST
SE 10/5/2012 11:46 VOCsSE 10/5/2012 9:32 ArchiveSE 10/5/2012 9:32 DensitySE 10/5/2012 9:32 GrainsizeSE 10/5/2012 9:32 Metals, totalSE 10/5/2012 9:32 n-alkanes & isoprenoids (inc. DRO & TPH)SE 10/5/2012 9:32 PAHs & alkyl PAHsSE 10/5/2012 9:32 pHSE 10/5/2012 9:32 Sediment AmmoniaSE 10/5/2012 9:32 Sediment Cyanide, TotalSE 10/5/2012 9:32 Sediment MercurySE 10/5/2012 9:32 Sediment Nitrate/NitriteSE 10/5/2012 9:32 Soot CarbonSE 10/5/2012 9:32 Sediment Phosphorus, TotalSE 10/5/2012 9:32 Sediment TKNSE 10/5/2012 9:32 Sediment TOCSE 10/5/2012 9:32 SulfideSE 10/5/2012 9:32 Total SolidsSE 10/5/2012 9:32 VOCsSE 10/5/2012 13:16 ArchiveSE 10/5/2012 13:16 DensitySE 10/5/2012 13:16 GrainsizeSE 10/5/2012 13:16 Metals, totalSE 10/5/2012 13:16 n-alkanes & isoprenoids (inc. DRO & TPH)SE 10/5/2012 13:16 PAHs & alkyl PAHsSE 10/5/2012 13:16 pHSE 10/5/2012 13:16 Sediment AmmoniaSE 10/5/2012 13:16 Sediment Cyanide, TotalSE 10/5/2012 13:16 Sediment MercurySE 10/5/2012 13:16 Sediment Nitrate/NitriteSE 10/5/2012 13:16 Soot CarbonSE 10/5/2012 13:16 Sediment Phosphorus, TotalSE 10/5/2012 13:16 Sediment TKNSE 10/5/2012 13:16 Sediment TOCSE 10/5/2012 13:16 SulfideSE 10/5/2012 13:16 Total SolidsSE 10/5/2012 13:16 VOCs
METHODEPA 8260BNAASTM D7263ASTM D422EPA 6010B/6020EPA 8015 modified, AlphaEPA 8270-SIM mod, Alpha SEPA 9045DSM4500NH3-BHEPA 9010BEPA 1631MSM4500N03-FGustafsson, et aI., 1997SM4500P-ESM4500Norg-CEPA 9060EPA 9030BEPA.160.3EPA 8260BNAASTM D7263ASTM D422EPA 6010B/6020EPA 8015 modified, AlphaEPA 8270-SIM mod, Alpha SEPA 9045DSM4500NH3-BHEPA 9010BEPA 1631MSM4500N03-FGustafsson, et aI., 1997SM4500P-ESM4500Norg-CEPA 9060EPA 9030BEPA 160.3EPA 8260B
TURN_A CONTAINROUND_ TAT_UN I ER_COUTIME T NT30 DAYS 1-1 DAYS 130 DAYS 030 DAYS 130 DAYS 145 DAYS 045 DAYS 130 DAYS 030 DAYS 030 DAYS 037 DAYS 130 DAYS 030 DAYS 030 DAYS 030 DAYS 130 DAYS 030 DAYS 130 DAYS 030 DAYS 1-1 DAYS 130 DAYS 030 DAYS 130 DAYS 145 DAYS 045 DAYS 130 DAYS 030 DAYS 030 DAYS 037 DAYS 130 DAYS 030 DAYS 030 DAYS 030 DAYS 130 DAYS 030 DAYS 130 DAYS 030 DAYS 1
SAMPLE_CUSTO
LAB_QC COC_ID DIANNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 IbNO AAL-20121006-164742 Ib
Page 5 of 5
Serial_No:11051209:46
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CHAIN OF CUSTODY-. PAGE 1 OF 1
nA. ... • • ~ ~:X · .. ~ ~~;L. .. . ~ sa:e as~Iien; inf: PO #:NALYTlCAL
Westborough, MA Mansfield, MA Project Name: Newtown CreekTEL: 508-898;9220 TEL: 508-822-9300
o ADEx o Add'i Deliverables
FAX: 508-898C9193 FAX: 508-822-3288 .- . . . .- . . - ....- • . • Project Location: StatelFed Proaram
t
Criteria
Client: Aloha Amtlvtical Proiect#: ~-...Address: 320 Forbes Blvd Proiect Manaoer: Chris Anderson DYes o No Are MCP Analvtical Methods Reauired?
Mansfield. MA 02048 ALPHA Quote #: DYes 10 No Are CT RCP (Reasonable Confidence Protocols) Reauired?
Phone: 508-8¥-4' 22. • • - ANALYSIS •
Fax: 508-822-3288 181 Standard o Rush (ONLY IF PRE-AP,PROVED)
SAMPLE HANDLING
:Filtr.atlon
.Email: canderson@alphalab.com
o Done
o These samples have been Previously analyzed by Alpha Due Date: Time:
o Not Needed
o Lab to do :
Otl:ler Project Specific Requirements/Comments/Detection Limits:N
Preservation •N
l"l -=t -0 Lab to do
<0 0
Please provide ANCHOR EQUIS EDD and reference Newtown CreekN ~
(Please specify•....~ I-
beloW)
enI- ~en~ wN
?,~t;~~~W~~;:":;:I.'.1 Sample 10 ollection Sample I Sampler's ~ CiiCii z .
I Date I Time 1Matrix Initials Z ~W
Sample Specific
0 C>Comments
TN005SG-000014-20121 005 10/5/12 0932 sediment !XI !XI D D D D D D D D D D L1218042-02 1
TN002SG-000011-20121005 10/5/12 1041 sediment !XI !XI D D D D D D D D D D L1218042-04 1
TN003SG-000015-20121005 10/5/12 1124 sediment !XI !XI D D D D D D D D D D L1218042-06 1
TN004SG-000015-20121005 10/5/12 1146 sediment !XI !XI- D D D D D D D D D D L1218042-08 1
TN006SG-000015-20121 005 10/5/12 1316 sediment-[gJ !XI D D D D D D D D D D L1218042-10 1
HB008SG-000015-20121 006 10/6/12 0955 sediment !XI !XI D D D D D D D D D D L1218042-14 1
HB007SG-Q00015-20121 006 10/6/12 1045 sediment [gJ !XI D D D D D D D D D D L1218042-16 1
HB006SG-000015-20121006 10!6/12 1130 sediment !XI !XI D D D D D D D D D D L1218042-18 1
HB005SG-000015-20121006 10/6/12 1219 sediment [gJ !XI D D D D D D D D D D L1218042-20 1
HB1005SG-000015-20121006 10/6/12 1219 sediment !XI !XI D D D D D 0 D D 0 0 L1218042-22 1
PLEASE ANSWER QUESTIONS ABOVEl Container Type - - - - - - - - - -
/7 Preservative - - - - - - - - - ,
IS YOUR PROJECT ,ij Re~ished By: qiltemme Received By: Datemme
.I /7 A V9#.( /7~MA MCP or CT RCP?FORM NO: 01..01(1)
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Serial_No:11051209:46
Page 275 of 279
Sample 10 ollection Sample I Sampler's
I Date I Time I Matrix Initials
~> L'i HB004SG-000015-20121 006 10/6/12 1327 sediment.~!
II HB003SG-000015-20121006 10/6/12 1421 sedimentj
HB002SG-000015-20121006 10/6/12 1505 sediment
HB001 SG-000015-20121006 10/6/12 1554 sediment
''../;..'
'.:
PI~ase provide ANCHOR EQUIS EDD and reference Newtown Creek
•SAMPLEHANDLINGFiltration
DOoneo NotNeededo LabtodoPresentationo Labto do(Please specifybeloW)
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0 L1218042-24 1
D L1218042-26 1
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o Add'i Deliverables
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....o FAX
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__ {elltreT••.e
~ Are MCPAnalvtical Methods Reauired?o Yes I 0 No Are CT RCP (Reasonable Confidence Protocols) Reauired?
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,
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Container Type -
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PAGE1 OF 1
Time:
o Rush (ON~Y IFPRE-APPROVED)
. ..
... .•.
Due Date:
ALPHA Quote #:
Project Location:
Proiect#:
Project Manager: Chris Anderson
181 Standard,
. . -Project Name: Newtown Creek
CHAIN OF CUSTODY
Mansfield,MATEL:508-822-9300FAX:508-822-3288
1;;\ANALYT~L
Other Project Specific Requirements/Comments/Detection limits:
. ..Client: Aloha Analytical
Addr~s: 320 Forbes Blvd
Westborough,MATEL:508-898.9220FAX:508-898-9193
PLEASE ANSWER QUESTIONS ABOVEI
Mansfield, MA 02048
Phone: 508-844-4122
Fax: 508-822-3288j , • .,
Email: ..canderson@alphalab.com
o ThesesampleshavebeenPrelliouslyanalyzedbyAlpha
IS YOUR PROJ.ECTMA MCP or CT RCP?FORMNO: 01~1(1)(rw.3G-JUL.(7)
/? Relinquisjled By:
./ /.h. .L/"-/ /?'1/
DatelTime
/2lAV ~ /70--,
Received By: Daternme
Serial_No:11051209:46
Page 276 of 279
SAMPLE HANDLING
Rltratlon,
o Doneo Not Needed
o Labtodo
Preservationo Labtodo
(Please specifybeloW)
" ,
Time:
o Rush (ONLY IF PRE.APPROVI"D)~ Standard
Due Date:
Turn-Around Time
Pro'ect#:
ALPHAQ t #
Project Location:
CHAIN OF CUSTODY1-iA.
ANALYTICAL
Other Project Specific Requirements/Comments/Detection Limits:
o These samples have been Pr~viouSlyanalyzed by Alpha
PI(:lase provide ANCHOR EQUIS EDD and reference Newtown Creek
Mansfield, MA 02048
Phone: 508-844-4122
Fax: 508-822-32l;l8,"
Email: canderson@alphalab.com
~:>
AtPi-q:~~~!fq';f'~
Sample ID Sampler'sQ):2
.""(L~~U~.gn)YF.' Initials (;j
~S.mpkl SpecificComments
TN005SG-000014-20121 005 1015/12 0932 sediment [gI 0 0 0 0 0 0 0 0 0 0 0 L1218042-02
TN002SG-000011-20121005 10f5f12 1041 sediment [gI 0 0 0 0 0 0 0 0 0 L1218042-04
TN003SG-000015-20121 005 10f5f12 1124 sediment [gI 0 0 0 0 0 0 0 0 0 0 0 L1218042-06
TN004SG-000015-20121 005 10f5f12 1146 sediment [gI 0 0 0 0 0 0 0 0 0 0 0 L1218042-08
TN006SG-000015-20121 005 10f5f12 1316 sediment [gI 0 0 0 0, 0 0 0 0 0 0 0 L1218042-10
HB008SG-000015-20121006 10/6f12 0955 sediment '[gI 0 0 0 0 D 0 0 0 0 0 0 L1218042-14
HB007SG-000015-20121006 10f6/12 1045 sediment [gI 0 0 0 0 0 0 0 0 0 0 0 L1218042-16
HB006SG-000015-20121006 10f6f12 1130 sediment [gI 0 0 0 0 0 0 0 0 0 0 0 L1218042-18
HB005SG-000015-20121 006 10f6f12 1219 sediment [gI 0 0 0 0 0 0 0 0 0 0 0 L1218042-20
HB 1005SG-000015-20121 006 10f6f12 1219 sediment [gI 0 0 0 0 0 0 0 0 0 L1218042-22
PLEASE ANSWER QUESTIONS ABOVEI Container Type
Preservative
15 YOUR PROJECT By: Datemme
MA MCP or CT RCP?FORM NO: 01-01(1)(rev.3O-JUL.o7)
Serial_No:11051209:46
Page 277 of 279
.'
AJ:iO,CHAIN OF CUSTODY PAGE 1 OF 1
. • . • . • ~_.~:X • .• ~ ~':;L-.. ' . ~ ::':::;i:~PO' .Westborough, MA Mansfield, MA Project Name: Newtown Creek 0TEL: 508~98-9220 TEL: 508~22-9300
\, AOEx o Add'i Deliverables
FAX: 508~98.9193 FAX: 508~22-3288 ... • ... . . ....... • . • Project Location: State/Fed Proaram Criteria
Client: Alpha Analvtical Proiect#:... ~_:l.lIf'.nf.
Addrehs: 320 Forbes Blvd Proiect Manaaer: Chris AndersonI DYes 0 No Are MCP Analvtical Methods Reauired?
Mansfield, MA 02048 ALPHA Quote #: DYes 10 No Are CT RCP (Reasonable Confidence Protocols Reauired?
Phone: 508-844-4122 . • • . ANALYSIS •Fax: 508-822-3288 181 Standard o ~ush (ONLY IF PRE-APPROVED)
SAMPLE HANDLING
": Filtration \
Email: canderson@alphalab.com " o Done
o These samples have been Previously analyzed by Alpha Due Date: Time:o Not Needed
o Lab to do :
Other Project Specific Requirements/Comments/Detection Limits: Preservation •o Labtodo
PI~ase provide ANCHOR EQUIS EDD and reference Newtown Creek(Please specifybeloW)
~::>
. 'ALPPi..i.Jb.ablp'.:'> \:\!:?
Sample 10 ollection Sample I Sampler'sQ)
:;;E"i(~~,bWsel()n~¥2}: " I Date I Time I Matrix Inilials "iii
(5 Sample Specific~ Comments
".'.yy on ..,....../'{:,'\.SiHB004SG-000015-20121 006 10/6/12 1327 sediment ~ 0 0 0 0 0 0 0 0 0 0 0 L1218042-24 1
'.",}' :'~'I,".'. HB003SG-000015-20121 006 ~ 0 0 0 0 0 0 0 0 0 0 0 1
10/6/12 1421 sediment L1218042-26
Ii'" HB002SG-000015-20121006 10/6/12 1505 sediment ~ 0 0 0 0 0 0 0 0 0 0 0 L 1218042-28 1
,::,i HB001 SG-000015-20121006 10/6/12 1554 sediment ~ 0 0 0 0 0 0 0 0 0 0 0 L1218042-30 1
....' ..lrSG-RB-20121006 10/6/12 0905 water ~ 0 0 0 O. 0 0 0 0 0 0 0 L1218042-12 1
~' ,.,1:,/,," '0 0 0 0 0 0 0 0 0 0 0 0,i;,,:' ,;;>:' 0 0 0 0 0 0 0 0 0 0 0 0' .. '.:',. .••.:;<.". 0 0 0 D 0 0 0 0 0 0 0 0,""ii", ";"H; 0 0 0 0 0 0 0 0 0 0 0 0.....f.! " ;", .1' 0 0 0 0 0 D 0 0 0 0 0 0"
PLEASE ANSWER QUESTIONS ABOVEl Container Type - . . . - . - -
Preservative - - . - . . - -
IS YOUR PROJECT 4 Relinquished By: Datemme Received By: Oalemme i,
MA MCP or CT RCP? / ~- A jtJJ a/IL. 0700 ur0\" >'FORM NO: 01-01(1)
,~ I I ~j.(teY.3O-JUL.()1) ';']j? Ii:
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Serial_No:11051209:46
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Serial_No:11051209:46
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