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Addendum to Supplemental Source Area Investigation, Former Anaconda Wire & Cable Facility, Low-Level Analysis of 1,4-DIoxane in Soil, 220-296 North Cypress Street, Orange, California May 8, 2013

Anaconda_SSA_Addendum.FINAL.docx i

TABLE OF CONTENTS LIST OF FIGURES ................................................................................................................................. i LIST OF APPENDICES ......................................................................................................................... i

1.0 ADDENDUM REPORT ..................................................................................................................... 1 2.0 REFERENCES ................................................................................................................................. 2 3.0 STATEMENT OF LIMITATIONS ...................................................................................................... 3

FIGURES

1. Site Location Map 2. Site Plan

APPENDIX

A. Laboratory Report


Anaconda_SSA_Addendum.FINAL.docx 1

1.0 ADDENDUM REPORT The Source Group, Inc. (SGI), is pleased to provide this Addendum to Supplemental Source Area Investigation for the former Anaconda Wire & Cable facility located at 220-296 North Cypress Street in Orange, California (Figures 1 and 2). The investigation was conducted in accordance with the Work Plan for Supplemental Source Area Investigation, Former Anaconda Wire & Cable Facility, Orange, California (Geosyntec, 2013), dated February 15, 2013, and comments provided by the Regional Water Quality Control Board (RWQCB) in a letter dated March 11, 2013. The Supplemental Source Area Investigation report, dated April 25, 2013 (SGI, 2013), summarized field procedures and presented analytical results for soil and groundwater. Because 1,4-dioxane was reported in groundwater, but was not detected in soil at or above the 0.20-milligram per kilogram (mg/kg) laboratory reporting limit, the RWQCB requested that the soil samples be analyzed for low-level 1,4-dioxane. California-certified Calscience Laboratory was contacted and the soil samples were reanalyzed for 1,4-dioxane. The original samples, collected March 21, 2013, had been retained by Calscience and were analyzed within prescribed holding times. The samples were collected at 5, 10, and 15 feet below ground surface from soil borings B-101 through B-104 on March 21, 2013. Based upon the results for the low-level analysis, 1,4-dioxane was not detected at or above the lower reporting limit of 0.025 mg/kg in any of the soil samples. The laboratory report is provided as Appendix A.



2.0 REFERENCES

Geosyntec Consultants, 2013, Work Plan for Supplemental Source Area Investigation, Former

Anaconda Wire & Cable Facility, Orange, California. February 15.

The Source Group, Inc., 2013, Supplemental Source Area Investigation, Former Anaconda Wire &

Cable Facility, 220-296 North Cypress Street, Orange, California. April 25.



3.0 STATEMENT OF LIMITATIONS

This report has been prepared for the exclusive use of Chapman University, their representatives, and authorized agents as it pertains to the Former Anaconda Wire & Cable Facility in Orange, California. The findings and conclusions presented in this report are based primarily on the chemical analysis of soil and groundwater samples obtained during the current and historical investigations and a review of geologic literature available for the project area. All work has been performed in a manner consistent with that level of care and skill normally exercised by members of the environmental science profession currently practicing under similar conditions in the area. No other warranty, either expressed or implied, is made.

FIGURES

SITE

)

SOURCE:ESRI 7.5 MINUTE TOPOGRAPHIC MAP.http://resources.esri.com/arcgisonlineservices

SITE LOCATION MAP

4/8/2013 AC DS

1

0 1,500 3,000750Feet ¯

250 NORTH CYPRESS STREETORANGE, CALIFORNIA 92866

04-ANA-002

FORMER ANACONDA FACILITY

SCALE= 1:24,000

FIGURE

APP.BY:DR.BY:DATE:PROJECT NO.:

1962 FREEMAN AVE.SIGNAL HILL, CA 90755

Administrator

Text Box

220-296 NORTH CYPRESS STREET

APPENDIX A

LABORATORY REPORT

Analytical Report ForClient: The Source Group, Inc.

Client Project Name: Anaconda / 04-ANA-001Attention: Angela Czuba

1962 Freeman AveSignal Hill, CA 90755-1241

WORK ORDER NUMBER: 13-03-1555

Virendra PatelProject Manager

05/7/2013

Supplemental Report 1

Additional requested analyses are reported as a stand-alone report.

Page 1 of 16

mailto:[email protected]

https://www.calscience.com/clientwebaccess/login.aspx

ContentsClient Project Name: Anaconda / 04-ANA-001

Work Order Number: 13-03-1555

1 Work Order Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

2 Client Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 42.1 EPA 8270C (M) Isotope Dilution 1,4-Dioxane (Solid) . . . . . . . . . . . . . 4

3 Quality Control Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 83.1 MS/MSD and/or Duplicate . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 83.2 LCS/LCSD . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9

4 Sample Analysis Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10

5 Glossary of Terms and Qualifiers . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12

6 Chain of Custody/Sample Receipt Form . . . . . . . . . . . . . . . . . . . . . . . . . 13

Page 2 of 16

Work Order Narrative

Condition Upon Receipt:

Samples were received under Chain of Custody (COC) on 03/21/2013. They were assigned toWork Order 13-03-1555.

Unless otherwise noted on the Sample Receiving forms all samples were received in goodcondition and within the recommended EPA temperature criteria for the methods noted on theCOC. The COC and Sample Receiving Documents are integral elements of the analyticalreport and are presented at the back of the report.

Holding Times:

All samples were analyzed within prescribed holding times (HT) and/or in accordance with theCalscience Sample Acceptance Policy unless otherwise noted in the analytical report and/orcomprehensive case narrative, if required.

Any parameter identified in 40CFR Part 136.3 Table II that is designated as "analyzeimmediately" with an immediate holding time (HT </= 15 minutes --40CFR-136.3 Table IIfootnote 4), is considered a "field" test and reported samples results are not flagged unless theanalysis is performed beyond 24 hours of the time of collection.

Quality Control:

All quality control parameters (QC) were within established control limits except where noted inthe QC summary forms or described further within this report.

Additional Comments:

Solid - Unless otherwise indicated, solid sample data is reported on a wet weight basis, notcorrected for % moisture. All QC results are always reported on a wet weight basis.

Subcontract Information:

Unless otherwise noted below (or on the subcontract form), no samples were subcontracted.

7440 Lincoln Way, Garden Grove, CA 92841-1427 TEL:(714) 895-5494 FAX: (714) 894-7501.....NELAP ID: 03220CA CSDLAC ID: 10109 SCAQMD ID: 93LA0830DoD-ELAP ID: L10-41

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Analytical Report

The Source Group, Inc. 03/21/13Date Received:1962 Freeman Ave 13-03-1555Work Order No:Signal Hill, CA 90755-1241 EPA 3545Preparation:

EPA 8270C(M) IsotopeDilution

Method:

Project: Anaconda / 04-ANA-001 Page 1 of 4

Lab SampleNumber

Date/TimeCollected QC Batch IDClient Sample Number Matrix

DatePrepared

Date/TimeAnalyzedInstrument

03/21/13 04/01/13 05/06/13Solid 130401L03B-103-5' 13-03-1555-1-A GC/MS DDD15:3310:35

-Results were evaluated to the MDL (DL), concentrations >= to the MDL (DL) but < RL (LOQ), if found, are qualified with a "J" flag.Comment(s):Parameter Result RL DFMDL Qual Units

mg/kg1,4-Dioxane 0.025 1ND 0.0035

Surrogates: REC (%) Control Limits Qual

Nitrobenzene-d5 118 28-139



mg/kg1,4-Dioxane 0.025 1ND 0.0035





mg/kg1,4-Dioxane 0.025 1ND 0.0035





mg/kg1,4-Dioxane 0.025 1ND 0.0035



7440 Lincoln Way, Garden Grove, CA 92841-1427 TEL:(714) 895-5494 FAX: (714) 894-7501..

RL - Reporting Limit , DF - Dilution Factor , Qual - Qualifiers

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Analytical Report



Method:


Lab SampleNumber


DatePrepared




mg/kg1,4-Dioxane 0.025 1ND 0.0035





mg/kg1,4-Dioxane 0.025 1ND 0.0035





mg/kg1,4-Dioxane 0.025 1ND 0.0035





mg/kg1,4-Dioxane 0.025 1ND 0.0035





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Analytical Report



Method:


Lab SampleNumber


DatePrepared




mg/kg1,4-Dioxane 0.025 1ND 0.0035





mg/kg1,4-Dioxane 0.025 1ND 0.0035





mg/kg1,4-Dioxane 0.025 1ND 0.0035





mg/kg1,4-Dioxane 0.025 1ND 0.0035





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Analytical Report



Method:


Lab SampleNumber


DatePrepared


04/01/13N/A 05/04/13Solid 130401L03Method Blank 099-09-011-109 GC/MS DDD05:30


mg/kg1,4-Dioxane 0.025 1ND 0.0035





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Quality Control - Spike/Spike Duplicate

Work Order No: 13-03-1555

Method: EPA 8270C(M) Isotope Dilution

1962 Freeman AveSignal Hill, CA 90755-1241

The Source Group, Inc.

Anaconda / 04-ANA-001Project

EPA 3545Preparation:

03/21/13Date Received:

Quality Control Sample ID

B-102-10'

MS/MSD BatchNumber

130401S03

Matrix

Solid

DateAnalyzed

04/01/13

DatePrepared

04/01/13

Instrument

GC/MS DDD

MS%REC

MSD%REC

%REC CL QualifiersRPD CLRPDSPIKEADDED

Parameter SAMPLECONC

MSCONC

MSDCONC

0-201,4-Dioxane 396 50-1309920.00 19.13 19.73ND

7440 Lincoln Way, Garden Grove, CA 92841-1427 TEL:(714) 895-5494 FAX: (714) 894-7501. .

RPD - Relative Percent Difference , CL - Control Limit

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Quality Control - Laboratory Control Sample

EPA 3545Preparation:EPA 8270C(M) Isotope DilutionMethod:

The Source Group, Inc.1962 Freeman AveSignal Hill, CA 90755-1241

Anaconda / 04-ANA-001

13-03-1555Date Received:Work Order No:

Project:

N/A

Quality Control Sample ID

099-09-011-109

Matrix

Solid

LCS Batch Number

130401L03

Lab File ID

03MAY060.rr

Instrument

GC/MS DDD

Date Analyzed

05/04/13

Parameter QualifiersConc Added LCS %Rec %Rec CLConc Recovered

50-1301001,4-Dioxane 5.000 5.003


RPD - Relative Percent Difference , CL - Control Limit

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Sample Analysis Summary Report

WORK ORDER #: 13-03-1555

InstrumentClient Sample

IDDate/TimeAnalyzedMethod Extraction

ChemistID

Lab Sample Number

AnalyticalLocation

B-103-5' SM 2510 B (M) N/A 03/25/2013 16:491-A SC 5688 1B-103-5' EPA 8260B EPA 5035 03/23/2013 12:451-C GC/MS OO486 2B-103-5' EPA 8270C(M) Iso EPA 3545 04/1/2013 18:341-A GC/MS DD449 1B-103-5' EPA 8270C(M) Iso EPA 3545 05/6/2013 15:331-A GC/MS DD449 1B-103-10' SM 2510 B (M) N/A 03/25/2013 16:492-A SC 5688 1B-103-10' EPA 8260B EPA 5035 03/23/2013 13:112-C GC/MS OO486 2B-103-10' EPA 8270C(M) Iso EPA 3545 04/2/2013 11:272-A GC/MS DD449 1B-103-10' EPA 8270C(M) Iso EPA 3545 05/4/2013 6:282-A GC/MS DD449 1B-103-15' SM 2510 B (M) N/A 03/25/2013 16:493-A SC 5688 1B-103-15' EPA 8260B EPA 5035 03/23/2013 13:383-C GC/MS OO486 2B-103-15' EPA 8270C(M) Iso EPA 3545 04/1/2013 19:143-A GC/MS DD449 1B-103-15' EPA 8270C(M) Iso EPA 3545 05/4/2013 6:483-A GC/MS DD449 1B-104-5' SM 2510 B (M) N/A 03/25/2013 16:494-A SC 5688 1B-104-5' EPA 8260B EPA 5035 03/23/2013 14:044-C GC/MS OO486 2B-104-5' EPA 8270C(M) Iso EPA 3545 04/1/2013 19:324-A GC/MS DD449 1B-104-5' EPA 8270C(M) Iso EPA 3545 05/4/2013 7:074-A GC/MS DD449 1B-104-10' SM 2510 B (M) N/A 03/25/2013 16:495-A SC 5688 1B-104-10' EPA 8260B EPA 5035 03/23/2013 14:315-C GC/MS OO486 2B-104-10' EPA 8270C(M) Iso EPA 3545 04/1/2013 19:535-A GC/MS DD449 1B-104-10' EPA 8270C(M) Iso EPA 3545 05/4/2013 7:275-A GC/MS DD449 1B-104-15' SM 2510 B (M) N/A 03/25/2013 16:496-A SC 5688 1B-104-15' EPA 8260B EPA 5035 03/23/2013 14:576-C GC/MS OO486 2B-104-15' EPA 8270C(M) Iso EPA 3545 04/1/2013 20:116-A GC/MS DD449 1B-104-15' EPA 8270C(M) Iso EPA 3545 05/4/2013 7:466-A GC/MS DD449 1B-102-5' SM 2510 B (M) N/A 03/25/2013 16:497-A SC 5688 1B-102-5' EPA 8260B EPA 5035 03/23/2013 15:247-C GC/MS OO486 2B-102-5' EPA 8270C(M) Iso EPA 3545 04/1/2013 20:327-A GC/MS DD449 1B-102-5' EPA 8270C(M) Iso EPA 3545 05/4/2013 8:057-A GC/MS DD449 1B-102-10' SM 2510 B (M) N/A 03/25/2013 16:498-A SC 5688 1B-102-10' EPA 8260B EPA 5035 03/23/2013 15:508-C GC/MS OO486 2B-102-10' EPA 8270C(M) Iso EPA 3545 04/1/2013 20:508-A GC/MS DD449 1B-102-10' EPA 8270C(M) Iso EPA 3545 05/4/2013 8:268-A GC/MS DD449 1B-102-15' SM 2510 B (M) N/A 03/25/2013 16:499-A SC 5688 1B-102-15' EPA 8260B EPA 5035 03/23/2013 16:179-C GC/MS OO486 2B-102-15' EPA 8270C(M) Iso EPA 3545 04/1/2013 21:099-A GC/MS DD449 1B-102-15' EPA 8270C(M) Iso EPA 3545 05/6/2013 12:249-A GC/MS DD449 1TB-032113 EPA 8260B EPA 5030C 03/24/2013 0:1410-A GC/MS OO486 2B-101-5' SM 2510 B (M) N/A 03/25/2013 16:4911-A SC 5688 1B-101-5' EPA 8260B EPA 5035 03/23/2013 16:4311-C GC/MS OO486 2B-101-5' EPA 8270C(M) Iso EPA 3545 04/1/2013 21:2911-A GC/MS DD449 1B-101-5' EPA 8270C(M) Iso EPA 3545 05/6/2013 12:4411-A GC/MS DD449 1B-101-10' SM 2510 B (M) N/A 03/25/2013 16:4912-A SC 5688 1

DescriptionLocation

1 7440 Lincoln Way, Garden Grove, CA 92841

2 7445 Lampson Avenue, Garden Grove, CA 92841

05/07/13 1

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Sample Analysis Summary Report

WORK ORDER #: 13-03-1555

InstrumentClient Sample

IDDate/TimeAnalyzedMethod Extraction

ChemistID

Lab Sample Number

AnalyticalLocation

B-101-10' EPA 8260B EPA 5035 03/23/2013 17:1012-C GC/MS OO486 2B-101-10' EPA 8270C(M) Iso EPA 3545 04/1/2013 21:4812-A GC/MS DD449 1B-101-10' EPA 8270C(M) Iso EPA 3545 05/6/2013 13:0312-A GC/MS DD449 1B-101-15' SM 2510 B (M) N/A 03/25/2013 16:4913-A SC 5688 1B-101-15' EPA 8260B EPA 5035 03/23/2013 17:3613-C GC/MS OO486 2B-101-15' EPA 8270C(M) Iso EPA 3545 04/1/2013 22:0713-A GC/MS DD449 1B-101-15' EPA 8270C(M) Iso EPA 3545 05/6/2013 13:2213-A GC/MS DD449 1EB-032113 EPA 8260B EPA 5030C 03/24/2013 0:4114-A GC/MS OO486 2

DescriptionLocation

1 7440 Lincoln Way, Garden Grove, CA 92841

2 7445 Lampson Avenue, Garden Grove, CA 92841

05/07/13 2

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Glossary of Terms and Qualifiers

Work Order Number:

Qualifier Definition

13-03-1555

See applicable analysis comment.*Less than the indicated value.<Greater than the indicated value.>Surrogate compound recovery was out of control due to a required sample dilution. Therefore, the sampledata was reported without further clarification.

1

Surrogate compound recovery was out of control due to matrix interference. The associated method blanksurrogate spike compound was in control and, therefore, the sample data was reported without furtherclarification.

2

Recovery of the Matrix Spike (MS) or Matrix Spike Duplicate (MSD) compound was out of control due tomatrix interference. The associated LCS and/or LCSD was in control and, therefore, the sample data wasreported without further clarification.

3

The MS/MSD RPD was out of control due to matrix interference. The LCS/LCSD RPD was in control and,therefore, the sample data was reported without further clarification.

4

The PDS/PDSD or PES/PESD associated with this batch of samples was out of control due to a matrixinterference effect. The associated batch LCS/LCSD was in control and, hence, the associated sampledata was reported without further clarification.

5

Surrogate recovery below the acceptance limit.6Surrogate recovery above the acceptance limit.7Analyte was present in the associated method blank.BSample analyzed after holding time expired.BUSample received after holding time expired.BVConcentration exceeds the calibration range.ESample was extracted past end of recommended max. holding time.ETThe chromatographic pattern was inconsistent with the profile of the reference fuel standard.HDThe sample chromatographic pattern for TPH matches the chromatographic pattern of the specifiedstandard but heavier hydrocarbons were also present (or detected).

HDH

The sample chromatographic pattern for TPH matches the chromatographic pattern of the specifiedstandard but lighter hydrocarbons were also present (or detected).

HDL

Analyte was detected at a concentration below the reporting limit and above the laboratory methoddetection limit. Reported value is estimated.

J

LCS/LCSD Recovery Percentage is within Marginal Exceedance (ME) Control Limit range.MEParameter not detected at the indicated reporting limit.NDSpike recovery and RPD control limits do not apply resulting from the parameter concentration in thesample exceeding the spike concentration by a factor of four or greater.

Q

The sample extract was subjected to Silica Gel treatment prior to analysis.SG% Recovery and/or RPD out-of-range.XAnalyte presence was not confirmed by second column or GC/MS analysis.Z

Solid - Unless otherwise indicated, solid sample data is reported on a wet weight basis, not corrected for% moisture. All QC results are reported on a wet weight basis.

For any analysis identified as a "field" test with a holding time (HT) </= 15 minutes where the sample isreceived outside of HT, Calscience will adhere to its internal HT of 24 hours. In cases where sampleanalysis does not meet Calscience's internal HT, results will be appropriately qualified.

7440 Lincoln Way, Garden Grove, CA 92841-1427 TEL:(714) 895-5494 FAX: (714) 894-7501. .

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