analytical report 6 · because the samples have not had a 21-day ingrowth, the activity for...

ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica St. Louis13715 Rider Trail NorthEarth City, MO 63045Tel: (314)298-8566

TestAmerica Job ID: 160-10497-1Client Project/Site: HDP

For:Perma-Fix Environmental Services Inc.2800 Solway RoadKnoxville, Tennessee 37931

Attn: Brian Miller

Authorized for release by:2/24/2015 4:27:14 PMIvan Vania, Project Manager II(314)[email protected]

This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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https://secure.testamericainc.com/TotalAccess/login.aspx

http://www.testamericainc.com/AskTheExpert/Expert_index.htm

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mailto:[email protected]

Table of ContentsClient: Perma-Fix Environmental Services Inc.Project/Site: HDP

TestAmerica Job ID: 160-10497-1

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Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24Tracer Carrier Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27

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Case NarrativeClient: Perma-Fix Environmental Services Inc. TestAmerica Job ID: 160-10497-1

Project/Site: HDP

Job ID: 160-10497-1

Laboratory: TestAmerica St. Louis

Narrative

CASE NARRATIVE

Client: Perma-Fix Environmental Services Inc.

Project: HDP

Report Number: 160-10497-1

With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no

problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control

limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of

the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,

the reporting limits are adjusted relative to the dilution required.

TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses

performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the

application methods. TestAmerica’s operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data

have been found to be compliant with laboratory protocols unless otherwise noted below.

The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions

to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written

approval of the laboratory.

Calculations are performed before rounding to avoid round-off errors in calculated results.

All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the

individual sections below.

All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %

solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and

disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the

client.”

This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.

RECEIPT

The samples were received on 02/13/2015; the samples arrived in good condition, properly preserved and, where required, on ice. The

temperature of the coolers at receipt was 18.0 C.

TECHNETIUM-99 (ICPMS)

Samples L10-12-01-B-E-S-00 (160-10497-1), L10-12-02-B-E-S-00 (160-10497-2), L10-12-03-B-E-S-00 (160-10497-3),

L10-12-04-B-E-S-00 (160-10497-4), L10-12-05-B-R-S-00 (160-10497-5), L10-12-06-B-E-S-00 (160-10497-6), L10-12-07-B-E-S-00

(160-10497-7), L10-12-08-B-R-S-00 (160-10497-8), L10-12-09-B-E-S-00 (160-10497-9), L10-12-10-B-R-S-00 (160-10497-10),

L10-12-11-B-E-S-00 (160-10497-11), L10-12-12-B-E-S-00 (160-10497-12) and L10-12-07-B-E-Q-00 (160-10497-13) were analyzed for

Technetium-99 (ICPMS) in accordance with EPA SW-846 Method 6020A. The samples were prepared and analyzed on 02/23/2015.

No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

PERCENT SOLIDS


TestAmerica St. Louis of 27

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101112

Case NarrativeClient: Perma-Fix Environmental Services Inc. TestAmerica Job ID: 160-10497-1

Project/Site: HDP

Job ID: 160-10497-1 (Continued)

Laboratory: TestAmerica St. Louis (Continued)


(160-10497-7), L10-12-08-B-R-S-00 (160-10497-8), L10-12-09-B-E-S-00 (160-10497-9), L10-12-10-B-R-S-00 (160-10497-10),


percent solids in accordance with EPA Method 160.3 MOD. The samples were analyzed on 02/17/2015.

No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

CESIUM-137 & OTHER GAMMA EMITTERS (GS)



(160-10497-7), L10-12-08-B-R-S-00 (160-10497-8), L10-12-09-B-E-S-00 (160-10497-9), L10-12-10-B-R-S-00 (160-10497-10),


Cesium-137 & Other Gamma Emitters (GS) in accordance with DOE GA-01-R. The samples were leached on 02/13/2015, and prepared

and analyzed on 02/18/2015.

Preparation Batch 174634:

Radium-226 is reported in these samples at the client’s request. Radium-226 is reported from the 609.31 keV line of bismuth-214.

Because the samples have not had a 21-day ingrowth, the activity for radium-226 is an estimated value and may be biased low. This bias

is caused by the disruption of secular equilibrium between radium-226 and bismuth-214 by the loss of radon-222 during sample

preparation. (160-10497-1 DU), (LCS 160-174634/2-A), (MB 160-174634/1-A), L10-12-01-B-E-S-00 (160-10497-1), L10-12-02-B-E-S-00

(160-10497-2), L10-12-03-B-E-S-00 (160-10497-3), L10-12-04-B-E-S-00 (160-10497-4), L10-12-05-B-R-S-00 (160-10497-5),

L10-12-06-B-E-S-00 (160-10497-6), L10-12-07-B-E-Q-00 (160-10497-13), L10-12-07-B-E-S-00 (160-10497-7), L10-12-08-B-R-S-00

(160-10497-8), L10-12-09-B-E-S-00 (160-10497-9), L10-12-10-B-R-S-00 (160-10497-10), L10-12-11-B-E-S-00 (160-10497-11),

L10-12-12-B-E-S-00 (160-10497-12)

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.


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.• TestAmerica St Louis I Chain of Custody Record 13715 Rider Trail North

160-10497 Chain of Custody Earth City, MO 63045 phone 314.298.8566 fax -~~ 0 DW O NPDES D RCRA 0 Other:

Client Contact Project Manager: Brian Miller Site .Contact: Ellen Jakub Pemia-Fix Environmental Services Tel/Fax: (314) 810-3333 Lab Contact: Ivan Vanya 2800 Solway Road Analysis Turnaround Time Knoxville, TN 37931 0 CALENDAR DAYS O WORJ<ING DAYS _{_~65) 690-0501 Phone TAT if different from Below ___ _ z (865) 539,-9868 FAX 1 1 D , _ r~ 0 l week > 6 -en O 2d~ s ~ ~

D i ;":m"P" t 1! ~ Project Name: Hematite Decommissiol'ling Project Site: Westinghouse Hematite, MO P0#832953

~ e :9 _, a. C :c ..

<> .. .. = Q. 0

U) = .. "' Sample Identification

Sample I Sample Date Time

L 10-12-01-8-E-S-00 2/1 1/15 1042

L 10-12-02-8-E-S-OO 2/11/15 J 1048

L 10-12--03-B-E-S-OO 2111115 I 1055

L 10-12-04-B-E-S-OO 2111115 I 1059

L 10-12-05-B-R-S-OO 2111115 I. 1622

L10-12-06-B-E-S-OO 211 1115 I 1627

L 10-12~07-B-E-S-OO 2111115 I 1651

L 10-12--08-B-R-S-OO 2111115 I 1111

L 10-12-09-B-E-S-OO 2111115 I 1130

L 10-12"10-B-R-S-OO 211 1115 I 1638

L 10-12°11-B-E-S-OO 2111115 I 1644

Type (C=Comp, I I # of G=Grab) Matrix Cont.

Q) "-.' ;s ~ = Qt

1 .... CL.

E :§ E "' ~~

-G Soil NI I X

G Soil 1 INI I X G Soil 1 INI I X

G Soil 1 INI I X

C Soil 1 INI I X

G Soil 1 INI I X

G Soil 1 INI I X

C Soil 1 INI I X

G Sb.ii 1 INI I X C Soil 1 INI I X

G Soil 1 I NI .I X

L 10-12-12-B-E-S-OO G Soil 1 /i~?~®k~~i~:~~~~$,~Mll'.~Jr!J\l,~C·"~ ,'..2 '.l1iir~!im1'g;r~: :'.'.""'"~ Ji;}!l':\:.tt~N&lfIB/ilf,f ~;i;l.;,,tJ~

I ·o s, .5

°'ii "' ,.... . "' t=. .·~ - .. U) 0 ::;; . Q.

- = a.. ~ 2 ~

XI X

XIX

XI X

XIX

XIX

XIX

XIX

XIX

XIX

XI X

XIX

Date: 02/13/2015 Carrier: Courier

Test America THE LEADER IN ENVIRONMENTAL TESTING

TestAmerica Laboratories, Inc. COC No: 021315-FSS1 Page 1 of2 Sampler: For Lab Use Oilly: 'Walk-in Client: I I Lab Sampling:

Job I SDG No.:

Sample Specific Notes:

Matt Cushman

Matt Cushman

Matt Cushman

Matt Cushman

Jahmai Williams

Matt Cushman

Jahmai Williams

Matt Cushman

Matt Cushman

Jahmai Williams

Jahmaf Williams

Possible Hazard Identification: Sample Disposal (.A lee may be assessed if samples are retained longer than 1 month) Are any samples from a listed EPA Hazardous Waste? Please List any EPA Waste Codes for the sample in the Comments Section if the lab is to dlspose of the sample.

0 Non-Ha:rard D Flammable D· Skin rmtant D Prnson B D Unknown J 0 Return to Gient D DispoSal by Lab D Archive fur Months :special Instructions/QC Requirements & Comments: Potential for Radiological Contamination

Custody Seals Intact: 0 Yes D No

Relinqu&:.... y: ~

\ l p/b.f-~Cl4'9 R~.inn9 . L uished by:

-~ ~ --.A& 1

Relinquish¢'d b~ V

Custody Seal No.:

•<AimPany: h'-r (../~ .-- '/. company: 6d;STo~s Company:

Cooler Temp. (°C): Obs'd: Corr'd: Therm ID No.: ·--- - -- ----

Date/Time: IR~Tved in Laboratory by: !Company: !Date/Time:

'!,( ~ :..,,

)/2.0

I Hem~e Decommronigg Project I Permafuc (fur W~stingi\l'wse) Non-Proprietary Class 3 { Procedm.-e:HDP-PR-QA--006, Chair. cf Custoo.y -1 Rewsio.-r 3 ! ; ;·e----

of 27

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TestAmerica St. Louis 13715 Rider Trail North

Earth City, MO 63045 phone 314.298.8566 fax

Client Contact PeF!Tla-Fix Environmental Services 2800 Solway Road Knoxville., TN 37931 {865) 690-0501 Phone (865) 539-9868 FAX Project Name: Hematite Decommissioning Project Site: Westinghouse Hematite, MO P 0#832953

Sample Identification

L 10-12-07-8-E-Q-OO

I'-------------

Chain of Custody Record TestAmerica THE LEADER IN ENVIRONMENT AL TESTlNG

Regulatory Program: D DW D NP.DES D RCRA 0 Other: TestAmerica Laboratories, Inc. Project Manager: Brian Miller Site Contact: Ellen Jakub Date: 02'13/2015 COC No: 021315-FSS1 TeUFax: (314) 810-3333 Lab Contact: Ivan Vanya Carrier: ·courier Page2of2

Analysis Turna~ound Time Sampler:

- ~ :: z l!! 3 -·-· .Cl z >' ::::; e - - a. "' ~lg C .!:

:r: >,

i~ .. .. .., ., 0, , -,:, E en .. :,

() ~ P• /g ::;; C. 0 t. (/) J: ... ,~ C. -c E .. "' (/) ! 0 E~ (/) e a ...

~ t; .s 'f:: E "' J: .... _g. = Cb; (!)~ :§. LL. a..: ~ (.)

0 CALENDAR DAYS O WORKING DAYS TAT if different from Below ___ _

For Lab Use Only: Walk-in Client I I Lab Sampling: D 2 weeks

0 1 week

D 2days

D lday I t satnpre

Type Sample l Sample I tC=Comp, I #of Date Time G=Grab} Matrix Cont.

Job/ SDG No.:

Sample Specific Notes:

2111115 I 1651 I G Soil I 1 ' N X X X J.ahmai Williams---~,

------I ~~1 I- I I I 111111 llllll±tt~ 1, -----i._ l--+-r r---_ L----r

N I A ~

•••·+ - ., _ _ ,a.,-~ , ,w,. ····••.; • "'',,/,• ..... ~ ·,·•~-··•-•

-----r-+-L -----r- rt-t---1-: ------ r----_ ~ ·~~1~;~/1@J(~f.~&"ii~~~iftt~~~'lI~n1i,~•e.ifJ~ ~m~wt$tt'!&l@,1~;~11~frJW~ i1~I~J~ Possible Hazard Identification: Sample Disposal. (A fee may be assessed if samples are retained longer thaR 1 month) Are any samples from a listed EPA Hazardous Waste? Please List any EPA Waste Codes for the sample in the Comments Section if the lab is to dispose of the sample.

0 Non-Hazard O Flammable O Skin I rrttant O Poison B O Unknown 0 Return to Client 0 Disposal by Lab 0 Archive for Months Special Instructions/QC Requirements & Comments: Potential for Radiological Contamination

Custody Seals Intact 0 Yes

RelinquishedL~

Rel~9uished by: ;: q<y; <; ~/A,.;, Jtk,,~

Relinquisl/ed tzy:

O No CustodySeal No.: 9'(mpany: r:. 1<.,.....,,. - t-, ')C Company: (J"c;/;}.l'b,:;.~

,,company:

Cooler Temp. ("Cj:"Oos'd:

; r_1 1 1 ,<J Date/Time: I Received by: . "l:'i. 4 2-1]-I> {jq,1fj) -?J1_k-'y...,._,'.•k.,,/i_..,,,;G,.,.. ~;;;:~t:·:~r~y:b_ar~ Date/Time: 1Re<%lved in Laboratory by:

Corr'd: Company: Cr~ ·,<;,,..:, ,,.j. 5'

Company:

-n:i SP---Company:

Therm fD No.:

Date/Tirrie: /-;d I_?, { F,. _" Date/Time: :2-,B-io

Date/Time:

~ c.) _,

/,.<? ,~ i ""-C/_

I Hew.ame De€ommiooiny Project I Permafil:{ ·{fm Wesung.'rottse) Noo..Proprietmy CJass 3 r ~ ~edun,:HDP-PR--0Ml06, Chain ~f Custod_v I Reiisfon: 3 !

I I I I I ·1---------

Login Sample Receipt Checklist

Client: Perma-Fix Environmental Services Inc. Job Number: 160-10497-1

Login Number: 10497

Question Answer Comment

Creator: Clarke, Jill C

List Source: TestAmerica St. Louis

List Number: 1

TrueRadioactivity wasn't checked or is </= background as measured by a survey

meter.

TrueThe cooler's custody seal, if present, is intact.

N/ASample custody seals, if present, are intact.

TrueThe cooler or samples do not appear to have been compromised or

tampered with.

N/ASamples were received on ice.

TrueCooler Temperature is acceptable.

TrueCooler Temperature is recorded.

TrueCOC is present.

TrueCOC is filled out in ink and legible.

TrueCOC is filled out with all pertinent information.

FalseIs the Field Sampler's name present on COC?

TrueThere are no discrepancies between the containers received and the COC.

TrueSamples are received within Holding Time.

TrueSample containers have legible labels.

TrueContainers are not broken or leaking.

TrueSample collection date/times are provided.

TrueAppropriate sample containers are used.

TrueSample bottles are completely filled.

TrueSample Preservation Verified.

TrueThere is sufficient vol. for all requested analyses, incl. any requested

MS/MSDs

N/AContainers requiring zero headspace have no headspace or bubble is

<6mm (1/4").

TrueMultiphasic samples are not present.

TrueSamples do not require splitting or compositing.

N/AResidual Chlorine Checked.


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Definitions/GlossaryTestAmerica Job ID: 160-10497-1Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP

Qualifiers

Rad

Qualifier Description

U Result is less than the sample detection limit.

Qualifier

Glossary

These commonly used abbreviations may or may not be present in this report.

¤ Listed under the "D" column to designate that the result is reported on a dry weight basis

Abbreviation

%R Percent Recovery

CFL Contains Free Liquid

CNF Contains no Free Liquid

DER Duplicate error ratio (normalized absolute difference)

Dil Fac Dilution Factor

DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample

DLC Decision level concentration

MDA Minimum detectable activity

EDL Estimated Detection Limit

MDC Minimum detectable concentration

MDL Method Detection Limit

ML Minimum Level (Dioxin)

NC Not Calculated

ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit

QC Quality Control

RER Relative error ratio

RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points

TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

TestAmerica St. Louis

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Method SummaryTestAmerica Job ID: 160-10497-1Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP

Method Method Description LaboratoryProtocol

SW8466020A Metals (ICP/MS), Tc-99 TAL SL

EPAMoisture Percent Moisture TAL SL

SW8466020A Metals (ICP/MS), Tc-99 in Activity TAL SL

DOEGA-01-R Cesium-137 & Other Gamma Emitters (GS) TAL SL

Protocol References:

DOE = U.S. Department of Energy

EPA = US Environmental Protection Agency

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

Laboratory References:

TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566


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Sample SummaryTestAmerica Job ID: 160-10497-1Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP

Lab Sample ID Client Sample ID ReceivedCollectedMatrix

160-10497-1 L10-12-01-B-E-S-00 Solid 02/11/15 10:42 02/13/15 12:10

160-10497-2 L10-12-02-B-E-S-00 Solid 02/11/15 10:48 02/13/15 12:10

160-10497-3 L10-12-03-B-E-S-00 Solid 02/11/15 10:55 02/13/15 12:10

160-10497-4 L10-12-04-B-E-S-00 Solid 02/11/15 10:59 02/13/15 12:10

160-10497-5 L10-12-05-B-R-S-00 Solid 02/11/15 16:22 02/13/15 12:10

160-10497-6 L10-12-06-B-E-S-00 Solid 02/11/15 16:27 02/13/15 12:10

160-10497-7 L10-12-07-B-E-S-00 Solid 02/11/15 16:51 02/13/15 12:10

160-10497-8 L10-12-08-B-R-S-00 Solid 02/11/15 11:11 02/13/15 12:10

160-10497-9 L10-12-09-B-E-S-00 Solid 02/11/15 11:30 02/13/15 12:10

160-10497-10 L10-12-10-B-R-S-00 Solid 02/11/15 16:38 02/13/15 12:10

160-10497-11 L10-12-11-B-E-S-00 Solid 02/11/15 16:44 02/13/15 12:10

160-10497-12 L10-12-12-B-E-S-00 Solid 02/11/15 11:03 02/13/15 12:10

160-10497-13 L10-12-07-B-E-Q-00 Solid 02/11/15 16:51 02/13/15 12:10


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Client Sample ResultsTestAmerica Job ID: 160-10497-1Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP

Lab Sample ID: 160-10497-1Client Sample ID: L10-12-01-B-E-S-00Matrix: SolidDate Collected: 02/11/15 10:42

Percent Solids: 80.5Date Received: 02/13/15 12:10

Method: 6020A - Metals (ICP/MS), Tc-99RL MDL

Technetium 99 0.00025 0.000067 0.000020 mg/Kg ☼ 02/23/15 08:45 02/23/15 17:11 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

Method: 6020A - Metals (ICP/MS), Tc-99 in Activity

Analyte

Technetium 99 4.20

(2σ+/-)

0.527

(2σ+/-)

102/23/15 17:1102/23/15 08:45pCi/g0.2311.35

RL MDC

0.358

Dil FacAnalyzedPreparedUnitResult Qualifier

Count Total

Uncert. Uncert.

Re 30 - 110

Carrier

02/23/15 08:45 02/23/15 17:11 1

Dil FacAnalyzedPreparedQualifier Limits%Yield

92

Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS)

Analyte

Actinium 228 1.07

(2σ+/-)

0.176

(2σ+/-)

102/18/15 17:2402/18/15 09:00pCi/g0.107

RL MDC

0.139


Count Total

Uncert. Uncert.

pCi/g 02/18/15 09:00 02/18/15 17:24 10.1110.06670.0666U-0.0281Americium 241

pCi/g 02/18/15 09:00 02/18/15 17:24 10.4580.5310.5091.46Bismuth 212

pCi/g 02/18/15 09:00 02/18/15 17:24 10.05820.1180.09060.730Bismuth 214

pCi/g 02/18/15 09:00 02/18/15 17:24 10.05470.1530.07541.03Lead 212

pCi/g 02/18/15 09:00 02/18/15 17:24 10.07320.1290.08690.913Lead 214

pCi/g 02/18/15 09:00 02/18/15 17:24 10.2542.291.2818.6Potassium 40

pCi/g 02/18/15 09:00 02/18/15 17:24 15.873.543.53U2.47Protactinium 234m

pCi/g 02/18/15 09:00 02/18/15 17:24 11.240.2850.280U0.461Protactinium 231

pCi/g 02/18/15 09:00 02/18/15 17:24 10.05820.1180.09060.730Radium 226

pCi/g 02/18/15 09:00 02/18/15 17:24 10.8430.5420.5301.06Thorium 234

pCi/g 02/18/15 09:00 02/18/15 17:24 10.1790.1370.136U0.147Uranium 235

pCi/g 02/18/15 09:00 02/18/15 17:24 10.1070.1760.1391.07Thorium 232

Tl-208 0.329 0.0503 0.0607 0.0374 pCi/g 02/18/15 09:00 02/18/15 17:24 1

(2σ+/-) (2σ+/-) MDCRL Dil FacAnalyzedPreparedUnitResult Qualifier

Count Total

Other Detected

Radionuclides

Uncert. Uncert.




Technetium 99 0.0011 0.000064 0.000019 mg/Kg ☼ 02/23/15 08:45 02/23/15 17:23 1



Analyte

Technetium 99 19.1

(2σ+/-)

1.84

(2σ+/-)

102/23/15 17:2302/23/15 08:45pCi/g0.2181.28

RL MDC

0.549


Count Total

Uncert. Uncert.

Re 30 - 110

Carrier

02/23/15 08:45 02/23/15 17:23 1


97


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101112


Project/Site: HDP


Date Received: 02/13/15 12:10


Analyte

Actinium 228 0.875

(2σ+/-)

0.136

(2σ+/-)

102/18/15 17:2602/18/15 09:00pCi/g0.0903

RL MDC

0.102


Count Total

Uncert. Uncert.

pCi/g 02/18/15 09:00 02/18/15 17:26 10.09690.05780.0578U0.0154Americium 241

pCi/g 02/18/15 09:00 02/18/15 17:26 10.3340.3710.3551.05Bismuth 212

pCi/g 02/18/15 09:00 02/18/15 17:26 10.05510.1130.08220.753Bismuth 214

pCi/g 02/18/15 09:00 02/18/15 17:26 10.05470.1440.06740.982Lead 212

pCi/g 02/18/15 09:00 02/18/15 17:26 10.06300.1180.07360.886Lead 214

pCi/g 02/18/15 09:00 02/18/15 17:26 10.2841.981.0416.5Potassium 40



pCi/g 02/18/15 09:00 02/18/15 17:26 10.05510.1130.08220.753Radium 226

pCi/g 02/18/15 09:00 02/18/15 17:26 10.7950.2880.2740.852Thorium 234

pCi/g 02/18/15 09:00 02/18/15 17:26 10.1710.1250.125U0.136Uranium 235

pCi/g 02/18/15 09:00 02/18/15 17:26 10.09030.1360.1020.875Thorium 232

Tl-208 0.369 0.0416 0.0565 0.0232 pCi/g 02/18/15 09:00 02/18/15 17:26 1


Count Total

Other Detected

Radionuclides

Uncert. Uncert.




Technetium 99 ND 0.000064 0.000019 mg/Kg ☼ 02/23/15 08:45 02/23/15 17:27 1



Analyte

Technetium 99 0.267

(2σ+/-)

0.160

(2σ+/-)

102/23/15 17:2702/23/15 08:45pCi/g0.2201.29

RL MDC

0.158


Count Total

Uncert. Uncert.

Re 30 - 110

Carrier

02/23/15 08:45 02/23/15 17:27 1


94


Analyte

Actinium 228 1.30

(2σ+/-)

0.217

(2σ+/-)

102/18/15 17:2702/18/15 09:00pCi/g0.176

RL MDC

0.172


Count Total

Uncert. Uncert.

pCi/g 02/18/15 09:00 02/18/15 17:27 10.1360.07990.0799U-0.00562Americium 241

pCi/g 02/18/15 09:00 02/18/15 17:27 10.5820.6590.6411.47Bismuth 212

pCi/g 02/18/15 09:00 02/18/15 17:27 10.1170.2000.1681.06Bismuth 214

pCi/g 02/18/15 09:00 02/18/15 17:27 10.1300.2010.1401.11Lead 212

pCi/g 02/18/15 09:00 02/18/15 17:27 10.1210.1900.1541.07Lead 214

pCi/g 02/18/15 09:00 02/18/15 17:27 10.3862.511.6318.7Potassium 40




of 27

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101112


Project/Site: HDP



Method: GA-01-R - Cesium-137 & Other Gamma Emitters (GS) (Continued)

Analyte

Radium 226 1.06

(2σ+/-)

0.200

(2σ+/-)

102/18/15 17:2702/18/15 09:00pCi/g0.117

RL MDC

0.168


Count Total

Uncert. Uncert.

pCi/g 02/18/15 09:00 02/18/15 17:27 11.370.5040.496U0.854Thorium 234

pCi/g 02/18/15 09:00 02/18/15 17:27 10.2600.1430.143U0.120Uranium 235

pCi/g 02/18/15 09:00 02/18/15 17:27 10.1760.2170.1721.30Thorium 232

Tl-208 0.492 0.0776 0.0929 0.0520 pCi/g 02/18/15 09:00 02/18/15 17:27 1


Count Total

Other Detected

Radionuclides

Uncert. Uncert.




Technetium 99 0.00026 0.000064 0.000019 mg/Kg ☼ 02/23/15 08:45 02/23/15 17:31 1



Analyte

Technetium 99 4.42

(2σ+/-)

0.507

(2σ+/-)

102/23/15 17:3102/23/15 08:45pCi/g0.2211.29

RL MDC

0.303


Count Total

Uncert. Uncert.

Re 30 - 110

Carrier

02/23/15 08:45 02/23/15 17:31 1


96


Analyte

Actinium 228 1.21

(2σ+/-)

0.190

(2σ+/-)

102/18/15 17:5702/18/15 09:00pCi/g0.126

RL MDC

0.145


Count Total

Uncert. Uncert.

pCi/g 02/18/15 09:00 02/18/15 17:57 10.1170.06970.0696U0.0266Americium 241

pCi/g 02/18/15 09:00 02/18/15 17:57 10.5000.5830.5621.48Bismuth 212

pCi/g 02/18/15 09:00 02/18/15 17:57 10.09420.1530.1240.874Bismuth 214

pCi/g 02/18/15 09:00 02/18/15 17:57 10.06610.1710.08851.13Lead 212

pCi/g 02/18/15 09:00 02/18/15 17:57 10.08720.1480.1041.01Lead 214

pCi/g 02/18/15 09:00 02/18/15 17:57 10.3172.451.4519.3Potassium 40



pCi/g 02/18/15 09:00 02/18/15 17:57 10.09420.1530.1240.874Radium 226

pCi/g 02/18/15 09:00 02/18/15 17:57 10.8550.5850.5621.56Thorium 234

pCi/g 02/18/15 09:00 02/18/15 17:57 10.2680.1430.142U0.114Uranium 235

pCi/g 02/18/15 09:00 02/18/15 17:57 10.1260.1900.1451.21Thorium 232

Pb-210 1.06 0.694 0.705 0.922 pCi/g 02/18/15 09:00 02/18/15 17:57 1


Count Total

Other Detected

Radionuclides

Uncert. Uncert.

Tl-208 0.375 0.0557 0.0680 0.0375 pCi/g 02/18/15 09:00 02/18/15 17:57 1


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Project/Site: HDP

Lab Sample ID: 160-10497-5Client Sample ID: L10-12-05-B-R-S-00Matrix: SolidDate Collected: 02/11/15 16:22



Technetium 99 0.00014 0.000066 0.000020 mg/Kg ☼ 02/23/15 08:45 02/23/15 17:34 1



Analyte

Technetium 99 2.42

(2σ+/-)

0.405

(2σ+/-)

102/23/15 17:3402/23/15 08:45pCi/g0.2251.31

RL MDC

0.339


Count Total

Uncert. Uncert.

Re 30 - 110

Carrier

02/23/15 08:45 02/23/15 17:34 1


94


Analyte

Actinium 228 1.11

(2σ+/-)

0.212

(2σ+/-)

102/18/15 17:5802/18/15 09:00pCi/g0.0841

RL MDC

0.179


Count Total

Uncert. Uncert.

pCi/g 02/18/15 09:00 02/18/15 17:58 10.1220.07220.0722U0.0163Americium 241

pCi/g 02/18/15 09:00 02/18/15 17:58 10.4290.5590.5341.59Bismuth 212

pCi/g 02/18/15 09:00 02/18/15 17:58 10.1060.1570.1320.807Bismuth 214

pCi/g 02/18/15 09:00 02/18/15 17:58 10.08510.1560.08920.992Lead 212

pCi/g 02/18/15 09:00 02/18/15 17:58 10.08870.1450.1100.915Lead 214

pCi/g 02/18/15 09:00 02/18/15 17:58 10.5922.361.4917.9Potassium 40



pCi/g 02/18/15 09:00 02/18/15 17:58 10.1060.1570.1320.807Radium 226

pCi/g 02/18/15 09:00 02/18/15 17:58 11.010.3980.3821.07Thorium 234

pCi/g 02/18/15 09:00 02/18/15 17:58 10.2650.2320.2290.416Uranium 235

pCi/g 02/18/15 09:00 02/18/15 17:58 10.08410.2120.1791.11Thorium 232

Pb-210 1.27 0.813 0.826 1.03 pCi/g 02/18/15 09:00 02/18/15 17:58 1


Count Total

Other Detected

Radionuclides

Uncert. Uncert.

Tl-208 0.352 0.0558 0.0667 0.0411 pCi/g 02/18/15 09:00 02/18/15 17:58 1




Technetium 99 0.000090 0.000065 0.000020 mg/Kg ☼ 02/23/15 08:45 02/23/15 17:38 1



Analyte

Technetium 99 1.53

(2σ+/-)

0.324

(2σ+/-)

102/23/15 17:3802/23/15 08:45pCi/g0.2231.30

RL MDC

0.291


Count Total

Uncert. Uncert.

Re 30 - 110

Carrier

02/23/15 08:45 02/23/15 17:38 1


95


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101112


Project/Site: HDP




Analyte

Actinium 228 1.15

(2σ+/-)

0.168

(2σ+/-)

102/18/15 17:5902/18/15 09:00pCi/g0.0873

RL MDC

0.120


Count Total

Uncert. Uncert.

pCi/g 02/18/15 09:00 02/18/15 17:59 10.09990.06000.0599U-0.0269Americium 241

pCi/g 02/18/15 09:00 02/18/15 17:59 10.3750.4560.4331.36Bismuth 212

pCi/g 02/18/15 09:00 02/18/15 17:59 10.06910.1220.09470.741Bismuth 214

pCi/g 02/18/15 09:00 02/18/15 17:59 10.05490.1550.07141.07Lead 212

pCi/g 02/18/15 09:00 02/18/15 17:59 10.06580.1210.07850.891Lead 214

pCi/g 02/18/15 09:00 02/18/15 17:59 10.2922.171.1218.1Potassium 40


pCi/g 02/18/15 09:00 02/18/15 17:59 11.150.7050.701U-0.642Protactinium 231

pCi/g 02/18/15 09:00 02/18/15 17:59 10.06910.1220.09470.741Radium 226

pCi/g 02/18/15 09:00 02/18/15 17:59 10.8040.6270.6091.44Thorium 234

pCi/g 02/18/15 09:00 02/18/15 17:59 10.2210.1470.146U0.0947Uranium 235

pCi/g 02/18/15 09:00 02/18/15 17:59 10.08730.1680.1201.15Thorium 232

Tl-208 0.328 0.0436 0.0553 0.0317 pCi/g 02/18/15 09:00 02/18/15 17:59 1


Count Total

Other Detected

Radionuclides

Uncert. Uncert.







Analyte

Technetium 99 0.0661 U

(2σ+/-)

0.0782

(2σ+/-)

102/23/15 17:5002/23/15 08:45pCi/g0.2131.24

RL MDC

0.0780


Count Total

Uncert. Uncert.

Re 30 - 110

Carrier

02/23/15 08:45 02/23/15 17:50 1


95


Analyte

Actinium 228 1.25

(2σ+/-)

0.228

(2σ+/-)

102/18/15 17:5902/18/15 09:00pCi/g0.174

RL MDC

0.189


Count Total

Uncert. Uncert.

pCi/g 02/18/15 09:00 02/18/15 17:59 10.1210.07190.0719U-0.00817Americium 241

pCi/g 02/18/15 09:00 02/18/15 17:59 10.3520.5090.4711.87Bismuth 212

pCi/g 02/18/15 09:00 02/18/15 17:59 10.08340.1740.1341.06Bismuth 214

pCi/g 02/18/15 09:00 02/18/15 17:59 10.1070.1640.09641.02Lead 212

pCi/g 02/18/15 09:00 02/18/15 17:59 10.1050.1710.1231.15Lead 214

pCi/g 02/18/15 09:00 02/18/15 17:59 10.2902.281.3817.8Potassium 40




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Project/Site: HDP




Analyte

Radium 226 1.06

(2σ+/-)

0.174

(2σ+/-)

102/18/15 17:5902/18/15 09:00pCi/g0.0834

RL MDC

0.134


Count Total

Uncert. Uncert.

pCi/g 02/18/15 09:00 02/18/15 17:59 10.9940.7570.7441.29Thorium 234

pCi/g 02/18/15 09:00 02/18/15 17:59 10.2600.1630.162U0.132Uranium 235

pCi/g 02/18/15 09:00 02/18/15 17:59 10.1740.2280.1891.25Thorium 232

Tl-208 0.419 0.0644 0.0777 0.0453 pCi/g 02/18/15 09:00 02/18/15 17:59 1


Count Total

Other Detected

Radionuclides

Uncert. Uncert.







Analyte


(2σ+/-)

0.0206

(2σ+/-)

102/23/15 17:5402/23/15 08:45pCi/g0.2631.54

RL MDC

0.0203


Count Total

Uncert. Uncert.

Re 30 - 110

Carrier

02/23/15 08:45 02/23/15 17:54 1


92


Analyte

Actinium 228 1.28

(2σ+/-)

0.185

(2σ+/-)

102/18/15 18:3402/18/15 09:00pCi/g0.100

RL MDC

0.131


Count Total

Uncert. Uncert.

pCi/g 02/18/15 09:00 02/18/15 18:34 10.09550.05650.0565U-0.00146Americium 241

pCi/g 02/18/15 09:00 02/18/15 18:34 10.3890.4510.4191.60Bismuth 212

pCi/g 02/18/15 09:00 02/18/15 18:34 10.06750.1370.09580.948Bismuth 214

pCi/g 02/18/15 09:00 02/18/15 18:34 10.07180.1880.08051.31Lead 212

pCi/g 02/18/15 09:00 02/18/15 18:34 10.06890.1400.09251.01Lead 214

pCi/g 02/18/15 09:00 02/18/15 18:34 10.3852.221.1218.7Potassium 40


pCi/g 02/18/15 09:00 02/18/15 18:34 11.200.7340.730U-0.613Protactinium 231

pCi/g 02/18/15 09:00 02/18/15 18:34 10.06750.1370.09580.948Radium 226

pCi/g 02/18/15 09:00 02/18/15 18:34 11.010.6430.6291.29Thorium 234

pCi/g 02/18/15 09:00 02/18/15 18:34 10.2520.1510.151U0.0753Uranium 235

pCi/g 02/18/15 09:00 02/18/15 18:34 10.1000.1850.1311.28Thorium 232

Tl-208 0.432 0.0523 0.0689 0.0388 pCi/g 02/18/15 09:00 02/18/15 18:34 1


Count Total

Other Detected

Radionuclides

Uncert. Uncert.


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Project/Site: HDP







Analyte


(2σ+/-)

0.157

(2σ+/-)

102/23/15 17:5802/23/15 08:45pCi/g0.2481.45

RL MDC

0.156


Count Total

Uncert. Uncert.

Re 30 - 110

Carrier

02/23/15 08:45 02/23/15 17:58 1


93


Analyte

Actinium 228 1.38

(2σ+/-)

0.209

(2σ+/-)

102/18/15 18:3402/18/15 09:00pCi/g0.107

RL MDC

0.155


Count Total

Uncert. Uncert.

pCi/g 02/18/15 09:00 02/18/15 18:34 10.1040.06280.0627U0.0334Americium 241

pCi/g 02/18/15 09:00 02/18/15 18:34 10.4230.4980.4731.48Bismuth 212

pCi/g 02/18/15 09:00 02/18/15 18:34 10.08060.1600.1201.02Bismuth 214

pCi/g 02/18/15 09:00 02/18/15 18:34 10.07160.1810.08691.22Lead 212

pCi/g 02/18/15 09:00 02/18/15 18:34 10.08210.1650.1151.13Lead 214

pCi/g 02/18/15 09:00 02/18/15 18:34 10.2662.211.2717.7Potassium 40



pCi/g 02/18/15 09:00 02/18/15 18:34 10.08060.1600.1201.02Radium 226

pCi/g 02/18/15 09:00 02/18/15 18:34 10.7990.3330.3111.15Thorium 234

pCi/g 02/18/15 09:00 02/18/15 18:34 10.2670.1700.169U0.174Uranium 235

pCi/g 02/18/15 09:00 02/18/15 18:34 10.1070.2090.1551.38Thorium 232

Pb-210 1.29 0.605 0.623 0.822 pCi/g 02/18/15 09:00 02/18/15 18:34 1


Count Total

Other Detected

Radionuclides

Uncert. Uncert.

Tl-208 0.414 0.0570 0.0714 0.0394 pCi/g 02/18/15 09:00 02/18/15 18:34 1







Analyte


(2σ+/-)

0.0528

(2σ+/-)

102/23/15 18:0202/23/15 08:45pCi/g0.2251.32

RL MDC

0.0489


Count Total

Uncert. Uncert.

Re 30 - 110

Carrier

02/23/15 08:45 02/23/15 18:02 1


92


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101112


Project/Site: HDP




Analyte

Actinium 228 1.15

(2σ+/-)

0.200

(2σ+/-)

102/18/15 18:3502/18/15 09:00pCi/g0.176

RL MDC

0.161


Count Total

Uncert. Uncert.

pCi/g 02/18/15 09:00 02/18/15 18:35 10.1270.07580.0758U0.0208Americium 241

pCi/g 02/18/15 09:00 02/18/15 18:35 10.4750.5260.5091.29Bismuth 212

pCi/g 02/18/15 09:00 02/18/15 18:35 10.08860.1730.1341.05Bismuth 214

pCi/g 02/18/15 09:00 02/18/15 18:35 10.09690.1810.09901.17Lead 212

pCi/g 02/18/15 09:00 02/18/15 18:35 10.09150.1600.1111.11Lead 214

pCi/g 02/18/15 09:00 02/18/15 18:35 10.5062.191.4116.3Potassium 40



pCi/g 02/18/15 09:00 02/18/15 18:35 10.08860.1730.1341.05Radium 226

pCi/g 02/18/15 09:00 02/18/15 18:35 10.9980.6360.6241.17Thorium 234

pCi/g 02/18/15 09:00 02/18/15 18:35 10.3070.1790.178U0.159Uranium 235

pCi/g 02/18/15 09:00 02/18/15 18:35 10.1760.2000.1611.15Thorium 232

Pb-210 1.48 0.811 0.830 0.994 pCi/g 02/18/15 09:00 02/18/15 18:35 1


Count Total

Other Detected

Radionuclides

Uncert. Uncert.

Tl-208 0.491 0.0648 0.0824 0.0393 pCi/g 02/18/15 09:00 02/18/15 18:35 1







Analyte


(2σ+/-)

0.0961

(2σ+/-)

102/23/15 18:0502/23/15 08:45pCi/g0.2351.37

RL MDC

0.0960


Count Total

Uncert. Uncert.

Re 30 - 110

Carrier

02/23/15 08:45 02/23/15 18:05 1


93


Analyte

Actinium 228 1.12

(2σ+/-)

0.174

(2σ+/-)

102/18/15 18:3602/18/15 09:00pCi/g0.111

RL MDC

0.131


Count Total

Uncert. Uncert.

pCi/g 02/18/15 09:00 02/18/15 18:36 10.1040.06230.0623U-0.0215Americium 241

pCi/g 02/18/15 09:00 02/18/15 18:36 10.4090.3620.3371.28Bismuth 212

pCi/g 02/18/15 09:00 02/18/15 18:36 10.06030.1420.09750.994Bismuth 214

pCi/g 02/18/15 09:00 02/18/15 18:36 10.05480.1860.07531.31Lead 212

pCi/g 02/18/15 09:00 02/18/15 18:36 10.06570.1450.09161.08Lead 214

pCi/g 02/18/15 09:00 02/18/15 18:36 10.2901.981.0316.5Potassium 40

pCi/g 02/18/15 09:00 02/18/15 18:36 14.762.382.335.12Protactinium 234m


of 27

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Project/Site: HDP




Analyte

Protactinium 231 -0.550 U

(2σ+/-)

0.702

(2σ+/-)

102/18/15 18:3602/18/15 09:00pCi/g1.15

RL MDC

0.699


Count Total

Uncert. Uncert.

pCi/g 02/18/15 09:00 02/18/15 18:36 10.06030.1420.09750.994Radium 226

pCi/g 02/18/15 09:00 02/18/15 18:36 10.8140.5400.5191.42Thorium 234

pCi/g 02/18/15 09:00 02/18/15 18:36 10.2390.1440.144U0.142Uranium 235

pCi/g 02/18/15 09:00 02/18/15 18:36 10.1110.1740.1311.12Thorium 232

Pb-210 1.43 0.515 0.542 0.695 pCi/g 02/18/15 09:00 02/18/15 18:36 1


Count Total

Other Detected

Radionuclides

Uncert. Uncert.

Tl-208 0.378 0.0457 0.0603 0.0343 pCi/g 02/18/15 09:00 02/18/15 18:36 1







Analyte


(2σ+/-)

0.164

(2σ+/-)

102/23/15 18:0902/23/15 08:45pCi/g0.2231.30

RL MDC

0.164


Count Total

Uncert. Uncert.

Re 30 - 110

Carrier

02/23/15 08:45 02/23/15 18:09 1


94


Analyte

Actinium 228 1.34

(2σ+/-)

0.290

(2σ+/-)

102/18/15 18:3602/18/15 09:00pCi/g0.178

RL MDC

0.256


Count Total

Uncert. Uncert.

pCi/g 02/18/15 09:00 02/18/15 18:36 10.1230.07280.0728U0.0117Americium 241

pCi/g 02/18/15 09:00 02/18/15 18:36 10.5490.5740.5561.40Bismuth 212

pCi/g 02/18/15 09:00 02/18/15 18:36 10.09550.1750.1391.03Bismuth 214

pCi/g 02/18/15 09:00 02/18/15 18:36 10.1120.1550.09670.941Lead 212

pCi/g 02/18/15 09:00 02/18/15 18:36 10.08940.1620.1171.08Lead 214

pCi/g 02/18/15 09:00 02/18/15 18:36 10.3012.311.4117.9Potassium 40



pCi/g 02/18/15 09:00 02/18/15 18:36 10.09550.1750.1391.03Radium 226

pCi/g 02/18/15 09:00 02/18/15 18:36 11.010.3580.350U0.707Thorium 234

pCi/g 02/18/15 09:00 02/18/15 18:36 10.2220.1070.106U0.0392Uranium 235

pCi/g 02/18/15 09:00 02/18/15 18:36 10.1780.2900.2561.34Thorium 232


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101112


Project/Site: HDP



Tl-208 0.458 0.0669 0.0821 0.0431 pCi/g 02/18/15 09:00 02/18/15 18:36 1


Count Total

Other Detected

Radionuclides

Uncert. Uncert.

Lab Sample ID: 160-10497-13Client Sample ID: L10-12-07-B-E-Q-00Matrix: SolidDate Collected: 02/11/15 16:51






Analyte


(2σ+/-)

0.0776

(2σ+/-)

102/23/15 18:1302/23/15 08:45pCi/g0.2061.20

RL MDC

0.0775


Count Total

Uncert. Uncert.

Re 30 - 110

Carrier

02/23/15 08:45 02/23/15 18:13 1


98


Analyte

Actinium 228 1.19

(2σ+/-)

0.211

(2σ+/-)

102/18/15 19:1902/18/15 09:00pCi/g0.176

RL MDC

0.173


Count Total

Uncert. Uncert.

pCi/g 02/18/15 09:00 02/18/15 19:19 10.1250.07480.0748U0.0270Americium 241

pCi/g 02/18/15 09:00 02/18/15 19:19 10.7300.5010.4930.869Bismuth 212

pCi/g 02/18/15 09:00 02/18/15 19:19 10.09780.1770.1431.01Bismuth 214

pCi/g 02/18/15 09:00 02/18/15 19:19 10.1170.1630.1020.977Lead 212

pCi/g 02/18/15 09:00 02/18/15 19:19 10.08940.1740.1251.16Lead 214

pCi/g 02/18/15 09:00 02/18/15 19:19 10.5212.501.5718.9Potassium 40



pCi/g 02/18/15 09:00 02/18/15 19:19 10.09780.1770.1431.01Radium 226

pCi/g 02/18/15 09:00 02/18/15 19:19 11.290.4280.421U0.727Thorium 234

pCi/g 02/18/15 09:00 02/18/15 19:19 10.3070.1400.140U0.0561Uranium 235

pCi/g 02/18/15 09:00 02/18/15 19:19 10.1760.2110.1731.19Thorium 232

Tl-208 0.475 0.0724 0.0875 0.0471 pCi/g 02/18/15 09:00 02/18/15 19:19 1


Count Total

Other Detected

Radionuclides

Uncert. Uncert.


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QC Sample ResultsTestAmerica Job ID: 160-10497-1Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP

Method: 6020A - Metals (ICP/MS), Tc-99

Client Sample ID: Method BlankLab Sample ID: MB 160-175279/1-A

Matrix: Solid Prep Type: Total/NA

Analysis Batch: 175538 Prep Batch: 175279

RL MDL

Technetium 99 ND 0.000051 0.000015 mg/Kg 02/23/15 08:45 02/23/15 17:04 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-175279/2-A



Technetium 99 0.00123 0.00122 mg/Kg 99 80 - 120

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Client Sample ID: L10-12-01-B-E-S-00Lab Sample ID: 160-10497-1 MS



Technetium 99 0.00025 0.00153 0.00178 mg/Kg 100 75 - 125☼

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Client Sample ID: L10-12-01-B-E-S-00Lab Sample ID: 160-10497-1 MSD



Technetium 99 0.00025 0.00153 0.00188 mg/Kg 107 75 - 125 5 30☼

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD





Technetium 99

Analyte

U 102/23/15 17:0402/23/15 08:45pCi/g0.174

MDC

1.02

RL

0.05140.0514

(2σ+/-) (2σ+/-)

MB

0.01691

MB

Dil FacPrepared AnalyzedUnitResult Qualifier

Uncert.

Count

Uncert.

Total

Carrier

Re 30 - 110 02/23/15 08:45 02/23/15 17:04 1

Dil FacPrepared AnalyzedQualifier Limits%Yield

98

MB MB




Technetium 99

Analyte

120-809920.8521.0 1.93 1.02 0.175

RL MDC(2σ+/-)

LCS LCS

pCi/g

UnitResult Qual %RecAdded

Spike

Limits

%Rec.Uncert.

Total

Re

Carrier

30 - 110

LCS

Qualifier Limits%Yield

98

LCS


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Project/Site: HDP

Method: 6020A - Metals (ICP/MS), Tc-99 in Activity (Continued)

Client Sample ID: L10-12-01-B-E-S-00Lab Sample ID: 160-10497-1 MS



Technetium 99

Analyte

125-7510030.4126.24.20 2.99 1.32 0.226

RL MDC(2σ+/-)

MS MS

pCi/g


Spike

Result

Sample Sample

Qual Limits

%Rec.Uncert.

Total

Re

Carrier

30 - 110

MS


94

MS

Client Sample ID: L10-12-01-B-E-S-00Lab Sample ID: 160-10497-1 MSD



Technetium 99

Analyte

10.28125-7510732.1326.14.20 3.14 1.30 0.223

RL MDC(2σ+/-)

MSD MSD

pCi/g

UnitResult Qual %Rec LimitAdded

Spike

Result

Sample Sample

Qual Limits

%Rec.Uncert.

Total

RER

RER

Re

Carrier

30 - 110

MSD


95

MSD





Actinium 228

Analyte

U 102/18/15 17:2402/18/15 09:00pCi/g0.0600

MDCRL

0.01660.0166

(2σ+/-) (2σ+/-)

MB

0.007662

MB


Uncert.

Count

Uncert.

Total

102/18/15 17:2402/18/15 09:00pCi/g0.02210.01240.0124U-0.002489Americium 241

102/18/15 17:2402/18/15 09:00pCi/g0.1350.06300.0630U-0.002369Bismuth 212

102/18/15 17:2402/18/15 09:00pCi/g0.03890.6080.608U-0.01520Bismuth 214

102/18/15 17:2402/18/15 09:00pCi/g0.01970.01310.0130U0.01444Lead 212

102/18/15 17:2402/18/15 09:00pCi/g0.03120.03270.0327U-0.005118Lead 214

102/18/15 17:2402/18/15 09:00pCi/g0.2290.1690.169U-0.02574Potassium 40

102/18/15 17:2402/18/15 09:00pCi/g2.1310.210.2U-0.2836Protactinium 234m

102/18/15 17:2402/18/15 09:00pCi/g0.2730.05300.0529U0.02900Protactinium 231

102/18/15 17:2402/18/15 09:00pCi/g0.03890.6080.608U-0.01520Radium 226

102/18/15 17:2402/18/15 09:00pCi/g0.2630.09440.0943U0.04264Thorium 234

102/18/15 17:2402/18/15 09:00pCi/g0.05620.03370.0336U0.02296Uranium 235

102/18/15 17:2402/18/15 09:00pCi/g0.06000.01660.0166U0.007662Thorium 232

Other Detected

Radionuclide

None

MB

(2σ+/-) (2σ+/-) MDCRL

pCi/g 02/18/15 09:00 02/18/15 17:24 1

MB


Uncert.

Count

Uncert.

Total

Radionuclides

Other Detected


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Project/Site: HDP





Americium 241

Analyte

116-879595.75101 9.97 0.609

RL MDC(2σ+/-)

LCS LCS

pCi/g


Spike

Limits

%Rec.Uncert.

Total

Cesium 137 35.0 33.40 3.51 0.200 0.207 pCi/g 96 87 - 120

Cobalt 60 36.7 35.28 3.56 0.131 pCi/g 96 87 - 115

Client Sample ID: L10-12-01-B-E-S-00Lab Sample ID: 160-10497-1 DU



Actinium 228

Analyte

10.081.0401.07 0.162 0.102

RL MDC(2σ+/-)

DU DU

pCi/g

UnitResult Qual LimitResult

Sample Sample

Qual

Uncert.

Total

RER

RER

Americium 241 -0.0281 U 0.02341 U 0.0614 0.102 pCi/g 0.40 1

Bismuth 212 1.46 1.587 0.442 0.320 pCi/g 0.13 1

Bismuth 214 0.730 0.7781 0.118 0.0587 pCi/g 0.20 1

Lead 212 1.03 1.062 0.155 0.0627 pCi/g 0.09 1

Lead 214 0.913 0.8791 0.125 0.0730 pCi/g 0.13 1

Potassium 40 18.6 17.63 2.11 0.366 pCi/g 0.22 1

Protactinium

234m

2.47 U 2.249 U 2.79 5.02 pCi/g 0.04 1

Protactinium 231 0.461 U 0.6469 U 0.360 0.941 pCi/g 0.29 1

Radium 226 0.730 0.7781 0.118 0.0587 pCi/g 0.20 1

Thorium 234 1.06 1.271 0.510 0.769 pCi/g 0.20 1

Uranium 235 0.147 U 0.1199 U 0.135 0.231 pCi/g 0.10 1

Thorium 232 1.07 1.040 0.162 0.102 pCi/g 0.08 1

Tl-208 10.230.35750.329 0.0619 0.0368

RL MDC(2σ+/-)

DU DU

pCi/g

UnitResult Qual LimitResult

Sample Sample

Qual

Uncert.

RER

RER

Total

Other Detected

Radionuclides


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QC Association SummaryTestAmerica Job ID: 160-10497-1Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP

Metals

Prep Batch: 175279

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid None160-10497-1 L10-12-01-B-E-S-00 Total/NA

Solid None160-10497-1 MS L10-12-01-B-E-S-00 Total/NA

Solid None160-10497-1 MSD L10-12-01-B-E-S-00 Total/NA




Solid None160-10497-5 L10-12-05-B-R-S-00 Total/NA








Solid None160-10497-13 L10-12-07-B-E-Q-00 Total/NA

Solid NoneLCS 160-175279/2-A Lab Control Sample Total/NA

Solid NoneMB 160-175279/1-A Method Blank Total/NA

Analysis Batch: 175538


Solid 6020A 175279160-10497-1 L10-12-01-B-E-S-00 Total/NA

Solid 6020A 175279160-10497-1 MS L10-12-01-B-E-S-00 Total/NA

Solid 6020A 175279160-10497-1 MSD L10-12-01-B-E-S-00 Total/NA




Solid 6020A 175279160-10497-5 L10-12-05-B-R-S-00 Total/NA








Solid 6020A 175279160-10497-13 L10-12-07-B-E-Q-00 Total/NA

Solid 6020A 175279LCS 160-175279/2-A Lab Control Sample Total/NA

Solid 6020A 175279MB 160-175279/1-A Method Blank Total/NA

General Chemistry

Analysis Batch: 174385


Solid Moisture160-10497-1 L10-12-01-B-E-S-00 Total/NA




Solid Moisture160-10497-5 L10-12-05-B-R-S-00 Total/NA





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Project/Site: HDP

General Chemistry (Continued)

Analysis Batch: 174385 (Continued)






Solid Moisture160-10497-13 L10-12-07-B-E-Q-00 Total/NA

Solid Moisture160-10497-13 DU L10-12-07-B-E-Q-00 Total/NA

Rad

Leach Batch: 173804


Solid Dry and Grind160-10497-1 L10-12-01-B-E-S-00 Total/NA

Solid Dry and Grind160-10497-1 DU L10-12-01-B-E-S-00 Total/NA




Solid Dry and Grind160-10497-5 L10-12-05-B-R-S-00 Total/NA








Solid Dry and Grind160-10497-13 L10-12-07-B-E-Q-00 Total/NA

Prep Batch: 174634


Solid Fill_Geo-0 173804160-10497-1 L10-12-01-B-E-S-00 Total/NA

Solid Fill_Geo-0 173804160-10497-1 DU L10-12-01-B-E-S-00 Total/NA




Solid Fill_Geo-0 173804160-10497-5 L10-12-05-B-R-S-00 Total/NA








Solid Fill_Geo-0 173804160-10497-13 L10-12-07-B-E-Q-00 Total/NA

Solid Fill_Geo-0LCS 160-174634/2-A Lab Control Sample Total/NA

Solid Fill_Geo-0MB 160-174634/1-A Method Blank Total/NA

Prep Batch: 175279



Solid None160-10497-1 MS L10-12-01-B-E-S-00 Total/NA

Solid None160-10497-1 MSD L10-12-01-B-E-S-00 Total/NA


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101112


Project/Site: HDP

Rad (Continued)

Prep Batch: 175279 (Continued)













Solid None160-10497-13 L10-12-07-B-E-Q-00 Total/NA

Solid NoneLCS 160-175279/2-A Lab Control Sample Total/NA

Solid NoneMB 160-175279/1-A Method Blank Total/NA


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Tracer/Carrier SummaryTestAmerica Job ID: 160-10497-1Client: Perma-Fix Environmental Services Inc.

Project/Site: HDP

Method: 6020A - Metals (ICP/MS), Tc-99 in ActivityPrep Type: Total/NAMatrix: Solid

Lab Sample ID Client Sample ID (30-110)

Re

92160-10497-1

Percent Yield (Acceptance Limits)

L10-12-01-B-E-S-00

94160-10497-1 MS L10-12-01-B-E-S-00

95160-10497-1 MSD L10-12-01-B-E-S-00

97160-10497-2 L10-12-02-B-E-S-00

94160-10497-3 L10-12-03-B-E-S-00

96160-10497-4 L10-12-04-B-E-S-00

94160-10497-5 L10-12-05-B-R-S-00

95160-10497-6 L10-12-06-B-E-S-00

95160-10497-7 L10-12-07-B-E-S-00

92160-10497-8 L10-12-08-B-R-S-00

93160-10497-9 L10-12-09-B-E-S-00

92160-10497-10 L10-12-10-B-R-S-00

93160-10497-11 L10-12-11-B-E-S-00

94160-10497-12 L10-12-12-B-E-S-00

98160-10497-13 L10-12-07-B-E-Q-00

98LCS 160-175279/2-A Lab Control Sample

98MB 160-175279/1-A Method Blank

Tracer/Carrier Legend

Re = Re


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101112

analytical report 6 · because the samples have not had a 21-day ingrowth, the activity for...

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