appendix g results of analyses soil and ground-water

TECHNICAL MEMORANDUM NO. 3AFOR

REMEDIAL INVESTIGATION/FEASIBILITY STUDYCITY DISPOSAL CORPORATION LANDFILL

(DUNN LANDFILL)

(PELA Reference No. 495207)

Appendix G

Results of AnalysesSoil and Ground-Water Samples

Volume 4 of 16

Summary Package

SAMPLES: CA5568, CA5584, CA5588-CA5593, CA5597,

CA5599, CA5805-CA5806, CA5571-CA5572,

CA5575-CA5583, CA5585-CA5587,

CA5594-CA5596, CA5602-CA5603,

CA4381, CA6020, CA6022, CA6023

April 1991

80

REUMoreaux&Associates

OHM Corporation

Lw| V"* Environmenlal TestingM-J M. \-A and Certification Corp.

Summary Package

for

CITY DISPOSAL CORPORATION LANDFILL

3*mt>l»P*>lnt DM Tim*

Richard P., Qtntra/

TM» Technical topert it «f> irCITE Mrvie* evwr«t*d by LOOESTOT* 0«t« Soltwcr*.

.284 Raritan Center Parkwav CN7808 Edison, New Jersey 08818-7808 201-225-5600.

ETCSDG NARRATIVE

This technical report submitted by ETC Corporation contains theanalytical results and required deliverables for WASTE MANAGEMENT,INC. Site 405 samples as identified below:

ETC IDCA5568CA5584CA5588CA5589CA5590CA5591

CLIENT ID3GWPZ63GWPZ83GWPZ11I3GWPZ53GWFB3GWPZ11D

ETC IDCA5592CA5593CA5597CA5599CA5805CA5806

CLIENT ID3GWPZ11S3GWFB3GWPZ11IDU3GWPZ5DUP02TB02TB

During the preparation and analysis of these samples, the followingwas observed:

VOLATILES:fOV7Q4431: Surrogate recoveries for samples CA5591, CA5599 andCA5805-CA5806 outside of QC control limits may be attributed to thesample matrix which has been confirmed by the results of areplicate analysis.

fOV7QA451: Surrogate recoveries for samples CA5568, CA5592 andCA5597 outside QC control limits may be attributed to sample matrixinterference which was confirmed by the results of the replicateanalysis.

Vinyl Chloride and 1,2-Dichloroethylene in sample CA5597 exceededthe calibration range in the original analysis. These compoundswere not detected in the dilution analysis due to the level of therequired dilution. The spectra from the original analysis has beenincluded in this report.

Release of the data contained in this hardcopy data package hasbeen authorized by the following signature.

MorrisonLaboratory Manager

Date

ru* * ooo«*

YQLHT1LE URliftNlCS HNHLYbISrt Sr»t1HLt NU

SHtET

Lab Name: ETC Corp.

Lab Code: Case No.:

M a t r i x : t. so i 1 - 'water ) Urt i tR

Sample w t / v o i : .3 lg/mLJ

Level: i low/med) LULJ

\ M o i s t u r e : no t dec .

Co 1 umn : " pack --'cap )

Lont rac t :

No . :

CHS NO. LUHRiJUND

Sub No . :

LaD barnpie 1U: LM-; vo

Lad F i l e lu: 'L-ol '?

Uate Keceived: l/7/Ol

Da te r tna lyzed: O l - ' l - i -

L11 1 u t i o n F a c t o r :

CUNLtNTKW I" 1UN U N I T S :<.ug/L or u g . - i - g ) Ub/L

74-87-3 —— ——74-a3-9 —————75-01-4 ----- -75-00-3 -----75-09-2 ------67-64-1 ------75-15-0 —— ——75-35-4 —————75-34-3 —————540-59-0 -----67-66-3 - — — -107-06-2 —— —78-93-3 -- — —71-55-6 —————56-23-5 -----108-05-4 — ——75-27-4 —— ——78-67-5 —————10061-01-5 ——79-01-6 —————124-48-1 ————79-00-5 —————71-43-2 —— ——10061-02-6 ——75-25-2 - —— —108-10-1 ————591-78-6 - ———127-18-4 ————79-34-5 —————108-88-3 ————108-90-7 ————100-41-4 ————100-42-5 -----1330-20-7 — —

---Chloro me thane---Brn mo me thane---Oinul Ch lor ide---Ch loroa thane---HethulBne Chloride---Acetone— -Carbon Diauifide---1,1-Dichloroethene- - - 1 .1-Dichloroethane- — 1,2-Dichlorethene (total)---Ch lorof orm---Ir2-Dichlorne thane---'2-Bu tanone---1 .1 .1-Tr ichloroethane---Carbon Tetrachloride— -Uinyl Hcetate---Bro mo dichlorome thane---1 .2-DichlopopropanB- — cim-1 .3-Gichlorooropene---Tp ich loroathene---Dihromochioro me thane—— 1 rl .2-Tr ich lor oa than*---Benzene---t r an »- 1,3-0 ich loropropene __---Bro mo form---4-nath'ul-2-Pentanone---2-Hexanone „, „., .,---Tetrachloroathene---1 , 1 ,2 ,2-Tet rach 1 or oe thane __---Toluene---Chlorobenzene---Ethylbenzene---St yrene---Xyl«na 1 tot a 1 J

2UUi' u 02UU•JUO31U7'*;uu1UUiuO1UU440louIUO14UUU1UU1UU^UOluuIUO100IUOIUOIuO1001UUIUO2>0'JOUiuO10Ui/uu100luu100iuO

1IU1 UIU1 U1IEIU1 UIU1IU1 UItIUtu1 UIUIUtuIUIUIUIUIUIU1IUIUIUIEIUIUIU1 U1

FUKtl I

VOIATXII OMAJVXC* ANALYSIS DATA SVZXT NO.

to* HAM:Uto Codo:

greCAM Me.:

Matrix: (ioil/v«t«r) J*J£T§£

wt/vo:: Q ^ fq/«L)

(lov/mtd) 0I Moiiturtt not doc.Column: (p«ck/c*p)

Saapio to-

Otto ftocoivod:Otto Antlyitd:'dilution r«etor:

CONCZMTXA7IOM CHITS ;or uo/Koi ^AC/t

Totrahydrofuran

fern x VOA I/I? K«v

IEVOLATILE ORGANICS ANALYSIS DATA SHEET

TENTATIVELY IDENTIFIED COMPOUNDS

Lab Name: ETC Corp. (.Laboratory

Lab Code: Case No.:

Matrix: I soil/water) WATER

Sample wt/vo1: .3 (g/mLJ ML

Level : t low/med) LGLJ

S Moisture: not dec.

Column: (.pack/cap) PACK

Number TICs found: 4

Cont ract :

SAS No.:

ERA SAMPLE NO.IIA5568I ____

SD£ No. :

Lab Sample ID:

Lab File ID: >02615

Date Received:

Date Analyzed:

Di l u t i o n Factor: 2 0. u

CONCENTRATION UNITS:Cug/L or ug/Kg) UG/L

CAS NUMBER

01. 107-87-902. 78-92-203. 67-63-004.

COMPOUND NAME

2-Pentanone2-Butanol2-PropanolUnknown

-

RT

19.4015.2110.2120.41

ES 1 . CUNC

39069037069

1

Q

JJJJ

FURM I VOA-T1C 1/87 Kev.

IttURGMN1CS HNttLrblb UHm bMttT

NU

Lab Name: ETC Corp.

Lab Code: Case No.:

flat r ix : '.soil -'water ) Wtt I t-R

Samp 1e wt -''vo 1 : . uf t g --'mL ,' HL

Leva 1 : ' low/'med ) LUU

*4 Moisture: not dec.

Co 1umn: ' pack/cap J

CflS NU.

Con t rac t :

S*b No . : bL'b No . :

Lab 'sample lU: L,iH':-'';-c,9v.

Lab F i l e ID: >L a2.:'

ua t e Keceived:

Date rtnalysed: Ul 'i'r

L ' l lu t ion h a c t 0 r

CUNLtNTRHI I UN UNi Ib :t, ug^'L or ug •"> g ) Ub--'L

I74-87-3-- — -----Ch lorome thane______________ I 1UUU74-83-9 — —— — --Bromome thane_______________I 1UOO7b-01-4----- — --Uinyl Chlor ide_____________I 1UUO75-00-3- — — - — -Ch lo roe thane_______________I luuu75-09-2- — -- — --Plethyiene Chlor ide_________I 14UU67-64-1-- ——— ---rtcetone____________________ I frÛU75-15-0 — -- — ---Carbon OiauU ide___________lûO75-35-4——- — -— 1,1-Oich loroethene_________i!?oQ75-34-3 —— — ----1,1-0 ichloroe thane_________ibuD540-59-0-—————1,2-Dichlorethene ttotal)__I4iO67-66-3-- —— ----Ch loroform_________________I5UO1Q7-06-2-- —— ---1,2-0 ichloroe thane_________iboO78-93-3--- —— ---2-But anone_________________ I96UU71-55-6 — ——— -—1,1,1-Trich lo roe thane______I 'JOO56-23-5-- — --- — Carbon Tetrachloride ____f?uu108-05-4— ——— --Uinyl Hcetate_________m____I 1UUO75-27-4---------Bromodich lorome thane_______I 5UO78-87-5 ——————— -1,2-Oichloropropane________1-?UO10061-01-5--——-cis-1,3-0ichloropropene____I5UO79-01-6 ——— - — — Tr ich loroethene____________IÛU124-48-1 ——————— Dibromoch lorome thane_______ I b O U79-00-5————————1,1,2-Tr ichloroe thane______ITOO71-43-2 ———— —— -Benzene____________________150010061-02-6————-trans-1,3-Dichloropropene__iÛU75-25-2- —— -- — -Bromoform__________________I5UO108-10-1 ——— —— -4-nethyl-2-Pentanone_______iîU59l-7tt-6----- —— 2-Hex anone_________________I 1UUU127-18-4— —— ——fetrach loroethene__________I t-uO79-34-5 — - — -——1,1,2 ,2-Tctrachloroethane__ I'POO108-88-3 ——— - — -To luene____________________I 1SOO108-90-7---- — --Ch lorobenzene______________1500100-41-4- —— — --Ethylbenzene_______________I t>uO100-42-5- — - —— -Styrene____________________I 5001330-20-7—— ——— Xylene t total )____________IÛU

1 UIU1 U

1 IJ1 UIU1 J1 U1 U1IUIUIUIU1 UIU1 UIUIUIUIUIUUIUIUIU1IUtuIU

1U .

FUKM I '"5

IAVOLATILE OMAffXCS ANALYSIS DATA ffttZT no.

•"•«Code: Case Ko.:

Matrix: (soil/water) tdATce.Sample vt/vol: o.o* fg/mliLevel: (lov/aed) *OtaI Moisture: not dee.Column: (peek/cap)

CAS NO.

Tetrahydrofuran

COMMUHO

dilution factor:COMCCmUTXON ONXTS

or uc/Kci

oo

row x VOA I/I? X«v

1ftVOLATILE ORGANICS ANALYSIS DATA SHEET

EPA SAMPLE NO

A5584Lab Name: ETC Copp.

Lab Code: Case No.:

Matrix: tsoi 1/water) UIATER

Sample wt/vol: 5.0 (g/mLJ ML

Leve 1: (. low/med ) LOW

S Moistupe: not dec.

Column: ipack/cap) PACK

Cont ract

SAS No. SDG No . :

Lab Sample ID:

Lab Fi la ID: > 0^6 00

Date Received:

Date Analyzed: 01/14/91

Di lut ion Factor :

CAS NO. COMPOUNDCONCENTRATION UNITS:Cug/L OP ug/Kgj Uli/L LJ

74-87-3 —————74-83-9 —————75-01-4 ————75-00-3 —————75-09-2 ————67-64-1 —————75-15-0 ————75.35-4 —————75-34-3 ————540-59-0 ————67-66-3 —————107-06-2 ————78-93-3 —————71-55-6 —————56-23-5 —————108-05-4 ————75-27-4 —————78-B7-5 —————10061-01-5 ——79-01-6 —————124-48-1 ————79-00-5 —————71-43-2 —————10061-02-6 ——75-25-2 ————108-10-1 ————591-78-6 ————127-18-4 ————79-34-5 —————108-88-3 ————108-90-7 ————100-41-4 ————100-42-5 ————1330-20-7 ———

---Ch lo pome thane---Bpomome thane---Umyl Chlopide— -Ch lopoathana---Methytan* Chloride—— Acatona ,—— Capbon Diaulfide---1 r 1-Dieh lopaathana— -1 . 1-Dieh larn«th*n«—— 1,2-Dichlopethene I total ) __---Chlopof opm...,,—— 1 r2-Diehlopa*th*n«—— 2-Butanona---l.lrl-Tp ichlopoathana—— Capbon Tat raeh lor \dm- — Uinyl Acetate. — Bpomodichl aroma than*—— 1 .2-Dieh lornnronan*— -c ie-1 ,3-Dich lopoppopene ____—— TP i eh lopae thane...Dibromochlopomathan*— --1 .1 -2-Trichloro«th«n«

--- t r ana- 1, 3-D i chlo rop popene __— -Bromof opm_.-4-M«thyl-2-P«nt«nan«- — 2-Haxanona— -T«t raeh lnro«th«n« ni ma—— 1 , 1,2, 2-Tetpachlo poe thane _ _—— Toluene—— Chlopobanzana . ,---Ethy Ibanzana---Styrana——— Xyl.n. (total )

11101 101101 1013151515151515151101515110151515151515151515110110151515151515151

1 :IU iIUIU 1IU iIJ 1IJ iIU 1IU <IU 1IUIU 1IU iIU 1IU :IU IIU •IU IIU iIU 1IU 1IU tIU !IU 1IUIU 1IUIU 1IU itu iIU iIU 1IU :IU 1IU1 1

FURM I "JOA

XAVOLATILE OMANICS ANALYSIS DATA StttT

ere

SAK9U NO.

Ufe Codoj CAM MO.:Matrix: (»oil/vtttr) jJ*r§g.54apl« wt/voi: S (q/ali

(lov/»«d) O i

% Moisture: not doc.column: (poek/eapj

CU NO. COKMUKO

Totranydrofuran

'.Dilution Factor:COHCCmUTIOM UNITS;(uoyt or ut/Koi MC/L

1/17 »«v.

8

itOOLftTlLE GRGHNlCS MNttLrblS DrtTH ShhET

IDtNTIFIED COMPOUNDS

NU

Lab Name : ETC Corp. I Laboratory

Lab Code: Case No.:

Hatrix: t so i 1 -'water ) WB'I tR

Sample uit/vol: £ . 0

Level: Uow/med) LUld

S Mo i s tu re : not dec.

Column: (pack /cap 3

Number liCs t-ound:

C g / m L J ML

Lontract: i____

bHb No . : Suia No .

Lab bamp ie *iJ: LH

Lab F i l e ID: '• U

L'a t e Kece i ved :

Date nnalyzed: 0 i

D i l u t i o n hactor:

CUNCtNTRHlION UNITS:tug/L or ug/Kg) UbVL

'6UU

1 4

J..

CHb NUMBtR LUHPUUND NHME Ebi .

F UKM I UGA-TIC

UrtliHNiCSIrtHNHLYbIS

SHHKLL NUUtt I rt SMttT

Lab Names ETC Corp. Lontract: i___

Lab Code: Lase No.: Snb No.: Sub No.:

Ma t r i x : ', so i t--"wa t e r ) wm tR

Samp le wt 'vo i : . UO'

Leê 1 : '. low/med ) LULO

S Hoiature: not dec.

Co lumn : '. oack ''cap )

ig/mLJ ML

CHS NO. UUMPUUND

Lab bample iu: LMT-?:

Lab F i le ID: >i_ Jfe2;

Uate Kece r.'ed :

Date nn a i y z e a : u i ' i'? - y i

D i l u t i o n h a c t o r : ™ u

CUNCLNIHHIION UNiIS:'-ug--'L or u g / i g J Ub--'L

74-87-3-— ---- — Ch lorome thane74-a?-9 ————— ---Bromome thane_______________15UUUU75-01-4—- —— - — YinyJ Chlor ide____________IÛUOU75-U 0-3- —— —— --Chlo roe thane_____________I5UUOO75-09-2----- —— -Hethylene Chlor ide_________I2*UOO67-64-1 —— ——— --Acetone____________________I9"?uuu75-15-0 — —— — — Carbon Qisulf ide__________I29UOU75-35-4- ———— — -1,1-01 chlo roe thene_________I25UOU75-34-3- —— -- — - 1,1-01 chlo roe thane_________I2TOOO540-59-0 — — - — -1,2-Dichl ore thene (.total )__l2t>UUO67-66-3- —— — ---Chloroform_________________I25UOO107-06-2 —— ———— 1,2-Dich loroethane________I 2TUUU78-93-3- ————— — 2-Butanone_________________1500UOO71-55-6-- ——— -—1,1,1-Tr i chlo roe thane______I25UUU56-23-5------—-Carbon Tetrachloride • I2»UUU108-05-4—- ———— umyl Hcetate________„____I5UUUO75-27-4———— — -Bromodich lorome thane______ l2bUUO78-87-5 — ——————1,2-Oich loropropane________1250UU10U61-01-5 — ——— c is-1,3-Dichloropropene____I25UUO79-01-6-————————Tr ich loroe thene124-48-1 — ——— — Dibromoch lorome thane79-00-5 ——————— 1,1,2-Tr i chlo roe thane______I2*uuu71-43-2 ——— - —— -Benzene__________________12500010061-02-6--———trens-1,3-Uichioropropene__I2ÛUO75-25-2 —————— --Bromoform__________________I2'?UOO108-10-1- —————— 4-nethyl-2-Pentanone_______I5UUUO591-78-6--- — - — 2-Hexanone_________________I'ruouO127-18-4-- —— - — Tet rach loroe thene__________I25UUU79-34-5 ———— •——1,1,2,2-Tet rach loroe thane__I2-?OOU108-d8-3——————Toluene__________________I34UUQ108-90-7———- —— Chlorobenzene_____________12^000100-41-4——— —— -Ethyl benzene_______________I25UUO10 0-42-5-- — -- — Styrene__________________I2r?u001330-20-7———- — Xylene t total )____________I25UUQ

UuuuuuLJuuuu

uuuuuuuuuuuuuuuuuuuIUI

fUKPI I

VOXATXLZ OMAJIXCS MUX.YIIJ »* HO.

Matrix: (aoil/vatori OlfrrafcSaapla wt/vol: o-coiUval; (lev/sod) O^LII Koisturoi not doc.Coiuan: (pack/cap)

CAJ MO.

UJ> Saaplo ID:UA filo 10:

Data Jtoeoivod:-—-

Data Analysad: / / r? /ni^^^^«p^«BiMB

'^Dilution factor:

Tatrahydrofuran

VOW X VQfc 1/17 ft«v

11

ItYQLHI1LE URCHNlCS HNMLYbIS UttCtt

TENTATIVELY IDENTIFIED COMKOUNQb

NU.

Lab Name:ETC Corp. I Laboratory

Lab Code: Case No.:

Ma t r ix : '.sol 1/water ) Ufi • t.R

Sample wt/vol: .0 ig/mLJ ML

Level: ', low/medJ LUW

S H o i s t u r e : not dec.

Co t umn: 'pack/cap J

Number ! iCs t-ound:

Lontract:

No . : Si- b No . :

Lab iamp i e l L1 : LR';-

Lab F i l e ID: -uJ

Uate

Date Hnalyzed: Ui 'i? -* l

D i l u t i o n i- a c r c- r : : . j U .

wi i ON urulS:'.ug/L or ug-'Kg ) uG/u

CHS CUriKOUND NHHt R l tb 1 . CUNL

-1 1C

12

•JQUHflLE UR&HNICS HNftLtbiS Urt I'ft iHLt f

Lab Name: ETC Corp.

E.KH NO

Lab Code: Case No.:

M a t r i x : k so i [.-'water J LJM i tR

Sample wt/'volJ S.U tg--'mLJ ML

Level: '. low/medJ LUU)

\ rioisture: not dec.

Column: ipack/cap)

Loot rac t:

No. : No. :

Lab F i l e ID: >L:-6Qi

Da t e Kece i ved:

Date Hnalyzed: Ql'14. •*!

D i l u t i o n f- a c t G r :

WttI1UH UNlTS:Cttb NO. LUMPUUND or

74-87-3 —————74-83-9 —————75-01-4 ------75-00-3 —————

67-64-1-- — —

75-35-4 —————75-34-3 —————540-59-0 -----67-66-3 ------107-U6-2 ————78-93-3 — — —71-55-6 —————56-23-5 ----- -108-05-4 -----75-27-4 ------78-87-5 —————10U61-01-5 ——79-01-6 —————124-48-1 -----79-00-5 —————71-43-2 —————10061-02-6 ——75-25-2 ------108-10-1 -----591-78-6--- —127-18-4 -----79-34-5 ------l08-«8-3 ———lOb-90-7- — —100-41-4 ————100-42-5- —— -1330-20-7 - ——

---Ch loro me thane---Sromome thane---U i n«j 1 Chloride---Chloroethane , _ ,---Plethulene Chloride---fteetone---Carbon Oiaulfide—— 1 1 1-Dich loroe thene---1 .1-0 ich loroe thane—— 1,2-Dichloretnene (.total ) __---Chloroform „---1 . 2 -Uich loroe thane---2-8u t an one „„- - - 1 .1 .1-Trichloroethane---Carbon Tetrachloride—— Uinol Hcatata---Bromod ich loro me thane---Ir2-Uichloropropane---ci»-l,3-0ich ioropropene ____---Tr ich loroe thene ,. ..- — Dibromoch lorome thane- — 1 .Ir2-Triehloroe thane—— Benzene---trans-l,3-Dich Ioropropene __---Bromof orm---4-f1eth»jl-2-li'entanone---2-H«xanone- — Tat raeh loroe thene---1 , 1 ,2 ,2-Te t rach loroe thane __---Toluene M---Chlorobenzene---Ethvlbenzena---St yrene—— Xyiene C total )

10IU10IU145553

510

10

5

5

5

10103

5

5

5

1IU iIUIU 1IUIJ 11 JIU 1

IU 1i JIU 1IUIU 1IU1 U 1IUIU !IUIU 1IIU I1 UIU 11 UIU 11 UIU 11 JIU iIUIU IIUIU 1IU1 !

rUKfl I <v-Uft

vou.ni* oxalic* AKALYSU DATA «trr

Co**» ____ caa« MO.:Matrix: (aoii/vatar) frMTEg.

vt/vol:

I Moiiturti not doe.Column: (pack/cap)

CU NO.

Data ftacaiva*: ifefaOata Anal/xad:

''Dilution raetor:

i Tatrahydrofuran

I/I?

14

ItUR&HH1CS HNftLYSlS UWltt

TtNft t l IYELY IDtNTIFItD CUnHQUNUb

NU .

Lab Name: ETC Corp. I Labora tory L o n t r a c t : I

Lab Code: Case No . : Sttb No . : SL'b N o . :

Ha t r i x : ' so i 1 --'wa t e r ) WH I £R Lab Sarnp 1 e i L1 -' Cro

Samp 1 e wt --'vo 1 : S

Level: UoWmed) LOW

\ noisture: not dec.

Column: ipack/capJ

Number TiCs found:

(gXmLJ ML Lab File ID:

Ua t e Kecei • -ad:

Da t e rtna Jvzsa:

D i l u t i o n Hac t oi

CUNCtN f'RnnUN UNITS:lug/L or ug-'kgj U&XL

-'L'J6UA

Ui

1 . ,

CrtS Nunetft

01. 1066-AU-6

CUriHGUND NHHE

Silanol, trimethyl-

R)

16. IS

Eb ( . CUNL

6

Q i

J

i

i

i

i

i

i

I

I

t

i

i

i

i

i

i

Fukn I yQ«-nc

15

1AVOLATILE ORGANICS ANALYSIS DATA SHEET

EPA SAHPLE NO.

IA55*0ILab Name: ETC Corp. Contract: ___

Lab Code: Case No.: SAS No.: SDii No.:

M a t r i x : (soil/water) WATER Lab Sample ID:

Sample wt/vol: 5.0 Cg/mD ML

Leve1: 11 ow/med) LOW

% Moisture: not dec.

Column: ^pack/cap) PACK

CAS NO. COMPOUND

Lab File ID:

Date Received:

Date Analyzed: 01/14/y.L

D i l u t i o n Factor: i

CONCENTRATION UNITS:(ug/L or ug/Kg) Ut»/L u

74-87-3 ———————Chlopome thane_____________11074-83-9 —— ——•—Bromome thane______;_______11075-01-4———————Vinyl Chloride____________11075-00-3 — - ————— Chlo roe thane_____________11075-09-2 ——————— Hethylene Chloride________11667-64-1——— ———— Acetone__________________(775-15-0———————Carbon Oisulf ide__________1575-35-4———————1,1-Oichloroethene________1575-34-3- —————— 1,1-Di chlo roe thane________15540-59-0——————1,2-Dichlopethene (total)__1567-66-3 ——————— Chlopofopm_______________15107-06-2 —————— 1,2-0 ichlopoe thane________1578-93-3———————2-Butanone_______________I 1071-55-6———————1,1,1-TpichloPoe thane______1556-23-5———————Carbon Tet rachlopide 15108-05-4——————Vinyl Acetate_____________I 1075-27-4————-——Bromod i eh lopome thane " 1578-87-5———————1,2-01 chlo pop ropana_______1510061-01-5—————ci»~l,3~Dichlopopropene____1579-01-6-.—————Tpichlopoethene___________15124-48-1———————Dibpomoeh iopomg thana I 579-00-5 ——————— 1,1,2-TpichloPoe thane______1571-43-2———————Benzene__________________1510061-02-6————t p«n»-l, 3-D i chlo pop popene__1575-25-2———————Bpomofopm________________(5108-10-1——————4-nethyl-2-Pentanone______110591-78-6——————2-Hexenone_______________110127-18-4——————Tetpachlopoethene_________1579-34-5 ——————— 1,1,2,2-Tetpachloroethane__15108-88-3——————Toluene__________________15108-90-7——————Chlopobenzene_____________15100-41-4——————Ethylbenzene______________I 5100-42-5——————Stypene__________________151330-20-7—————Xylene (total)___________I 5______________________________________I__

IUIUtuIUIIJIUIUIUIUIUIUIUIUIUIUIUtuIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIU

FURfl I 1/fl/L Rev.

AKAIYSXSere

Matrix:J4.pl, vt/vol: (avail ML

£0^

I Moi»tur«: not doe.Coluam: (paek/eap)

CU NO.

Saapla 10:filo 10:

Data Xocoivod: l A o / O fData AAalysod:

'•Dilution Factor:uwntiflTRATIOM UNITS:(uayt or uo/K«) MC/t

Totrahydrofuran

I/I? ft«v

17


TENTATIVELY IDENTIFIED COflPOUNDS


Lab Code: Case No.:

flat r ix: isoi 1/water) WATER

Sample wt/wol: 5.0 (g/mLJ ML

Level: ( low/med) LOW

S Hoisture: not dec.



Cont ract:

SAS No.:

EPA SAflPLE NO.

IA559QI_____

SOU No.:

Lab Sample ID:

Lab Fiie ID:

Date Rece ived : \l\O\o\\

Date Analyzed: 0

Dilution Factor:

CONCENTRATION UNITS:tug/L or ug/Kg) UG/L

CAS NUriBER

01. 1066-40-6

COrtPOUND NAtlE

Si lano 1 , t r i me thy 1-

RT

16.21

EST. CUNC

9

Q

J

FORM I UOA-TIC 1/87

18

* : ETCNJ

i_ab Cod* :

M a t : - . - : '.*•;: i ''w

Sample wt-'-.-ol:

VOLATILE ORGAN ICS ANALYSIS DAT* SHEET

Cent racr :

EPA SAMPLE NO.

H5591

La« e rio . :

JATEP

' q -''mL J '".L

L e v,' el: ' 1 o u / m e o L C Ui

fti Mo ; i tur e : not dec .

Co luprir . ' pack. 'c as .'• PA

Lab Samoli ID: ^AfS^lUI

Lab -:le : D: C21^1

Da*, e Pec* i vet: 0 1 • |O ^ i

Da t e una1yz e 2: j i i 2 ? .

D i l u t i o n Factor: 25

COMPOUN;CONCENTRATION UNITS:Cug/L or ug-'Kg . UG-''L 0

1 74-87-3--- —— ---Chloreme thane_____________! 74-83-9 — - — — — Bromomethane______________! 75-01-4————————iJinyl Chloride____________i 75-00-3-—------Chloroethane_____________I 75-09-2 ———————— Methylene Chloride________! 67-64-1----- — -.-Acetone___________________I 75-15-0 — ---- — -Carbon Disulf ide_________1 75-75.4———————1,1-Dichloroethene_______I 75-34-3———--——1,1-Dichloroethane_______I 540-59-0- — — —— 1,2-Dichlorethene (total)_I 67-66-?--————--Chloroform________________I 107-06-2 —————— 1,2-Dichloroe thane_______I 78-93-3- — — - —— 2-Butanone_____________'! 71-55-6-- ——— - — 1,1,1-Tr ieh1oroethanei 56-23-5—-————Carbon Tetrachloride______i 108-Q5-4--————IJinyl Acetate____________! 75-27-4———————Bromodich loromethane______I 78-87-5 ———————— 1,2-Dichloropropane_______I 10061-01-5——-—ci»-l,3-Dichloropropene___: 79-01-6————-—Tr ichloroiethene_________1 124-48-1-!---- — --Dibromoch lorome thane______! 79-00-5 ——————— 1,1,2-Trichloroe thane_____I 71-43-2 ——————— Benzene_________________t 10061-02-6————tr«ns-l,3-Dichloropropene_75-25-2- — ———— rflrompform_________________108-10-1 ——————— 4-Methyl-2-Pentenone______591-78-6 —————— 2-Hexenone______________127-18-4——---—Tetrachloroethene_________79-34-5 ——— - ——— 1,1,2,2-Tetrachl oroe thane__t108-88-3 —————— Toluene__________________I108-90-7—-—---Chlorobenzene____________100-41-4——- — — Ethyl benzene_____________100-42-5——-—--Styrene_________________1330-20-7—————Xylene (total )__________

250250250250130160013013013011001301301000013013025013013013060130130130130130250250130130260130130130130

IUIUIUIU!UIIUIU;u!UIUIEIUIUIU!UIUIUIJ!UIUIUIUIUIUIUIUIUIIUIUIUIU

1-9-FORM I UOA 1--87 Re-

VOXATZU OMMIZCS AWU.Y8ZS DATA

ContractiMO.:

Matrix: doa/vator) Q&TBLSaaplo vt/vol;Uvtl: (low/mod)* Moiaturot not doc.Column: (pacx/cap)

CU NO.

Saapio zoito:

Otto Roeoivod:

dilution Factor:

Totrahydrofuran

I/I? R«v,

20

IEVOLATILE ORGAN IC5 ANALYSIS DHTH SHEET


EPA BAMPLE MO.

_ab Name:ETCNJ

Lab Cede: Case No.:

Ma *.:•:-: ( so i 1 'wa t e r • WATER

Sample w t - ' v o l ; .2 g -'mL

Leve 1 : • io^'mec ; LOW

"• Mo i s t ure : not dec .

Co lumr : '. pack--'cap ) PACK

Number TICs. found: 1

Can tract :

Lab Sample ID: CA?5* I'.'C

Lab - i 1 e ID: III1?:

Dat* Pecei^ed: 01 |0 91

Date Anal y z e d : 0 1 ••' i 3 • 9 1

Dilution Factor: 2"?.Q

CONCENTRATION UNITS:(ug^L or ug/Kg) UG/L

11 CAS NUMBER

1 01. 14899-79-411Iii!1Ij1i!1!1!

!1!1I1111I1111

COMPOUND NAME

2-Butano 1 , (R)-

.

.

RT

14.74

'k

1EST. CONC 1 Q

730 Ui!

1•

I!1!111!1

I:1iiI1!ii111!1

FORM I UOA-TIC 1/8

UQLATILE ORGAN IC3

-st Mar-* : ETClO

'_ sb Cede : Caie No . :

- SHFE'

E'arnp 1 » w f •• jo 1 : . i

L* .'e ; • . : .M -'me ; LQ..-1

3s Mo i i t U r e ; r j t dec .

Co lu i r - . ' ? a c ' - 'cs^ ' PACi-

g --'mL ' "1L -_ab

COMPOUND ug>'L. UG 'L

[0

; 74-37-7------- — Chlcrorne thane ______________ !500 i U7^-87-9---- —— --Sromome thane _______________ ! 500 I U

. -l5_i}i-4_-.---_._i.jlr,yi Ch l o r i d e _____________ ! 5 Q 0 ! U75-00-?---------Chloroethans _______________ 150 j !U

I 75-Q9-2---------Methylene Chlor ide _________ i 2?Q 'J67-64- i---------Ace t one ____________________ I 9 10

i 75-15-0 ——— ———— Carbon Disulf ide ___________ :25075-35-4 ———————— 1,1-Dichloroethene _________ 1250 ' ' J

i 75-34-7---------l,l-Dichloroethane _________ i 2 5 0 " J: ^40-59-0 ——— - —— 1,2-Dichlorethene ' total ) __ I 1100I 67-66-?---- — - — Chloroform _________________ 1250 if107-Oo-2 —— ———— 1,2-Dich lor oe thane ______ .— .'2?C : 'J

i 73-9?-?------- — 2-Butanone _______________ I -4400"1-55-6 ———————— 1,1,1-Tr ichloroethane " 1250 IU

I 56-2?-5 ———————— Carbon Te t rach lor ide _______ ;250 ! 'J108-05-4 —— ———— iJinyl Acetate _____________ 1500 IU

! 75-27-4------ —— Bromodichlcrome thane _______ ! 250 : UI 73-87-5-- — ———— 1,2-Dichloropropan* ________ 1250 IUI 10061-01-5 ————— ci*-l,3-Dichloroprapene ____ 1250 IU79-01-6 ——————— Trichloroethene ___________ ISO I 3

! 124-48-1 —————— D ibromochl or ome thane ______ : 250 : L1rg-00-5 ——————— 1 , 1 ,2-Tr ich lor oe thane ______ 1250 !U

I 71-43-2 ——————— Benzene __________________ !250 ;UI 10 Co 1-02-6 — -- — t rans-l,3-Dichloropropene __ 1250 I 'JI 75-25-2 ———————— Bromoform __________________ I 250 Ui 108- 10-1- — — - — 4-Methyl-2-Pentanone _______ 1500 IUi 591-78-6 ———— ---2-Hexanone _________________ : 500 :U127-18-4 ——————— Tetrachloroethene __________ 1250 IU

i 79-34-5- ——————— 1 ,1,2,2-Tetrachliroe thane __ 1250 I -Ji 108-88-3 —————— Toluene __________________ I 110 :-I 108-90-7 ——————— Chlorobenzene ______________ 1250 IUI 100-41-4 —————— Ethyl benzene _____________ .1250 IUI 100-42-5 ——————— Styrene ____________________ 1250 !UI 133C-20-7 —————— Xylene Uotal ) ____________ 1250 IU

FOPM I UQn '8'

muffles MUU.YSXS DATA ram

*** **»•* arg oo*» Contract:Caao HO.:

Matrix: (aoil/vatari Oi rce.

Sup It vt/vel: Q-i fg/mli mz.

% Moiaturot not doe.

Coluan: (paeX/eap)

Data ftaeoivod:Data Analysod:

dilution^Factor

Totrahydrofuran

1/17

23


EPA SAMPLE NO,

IH5592I_____Leb Name: ETC Corp. Contract: ________

Lab Code: Case No.: SAS No.: SD£ No.:

Matrix: (soil/water) UlttTER Lab Sample ID: CA5592U2

Sample wt/vo1 : .1 Cg/mLJ ML

Level: (low/med) LOW


Column: tpack/capJ PrtCK

CAS NO. COMPOUND

Lab F i l e ID: >D26l6

Date Received: l/gjt?J

Dete Analyzed: 01/14/91

Dilution Factor: 5 u

CONCENTRATION UNITS:(ug/L or ug/Kg) Ub/L u

74-87-3 ———— ——— Chlorome thane_____________150074-83-9 —————— -Bromo me thane_____________I5UO75-01-4————————Uinyl Chloride_____________150075-00-3 ——————— Chloroe thane_____________150075-09-2———————Methylene Chloride________177067-64-1 ———————— Acetone____________________1740075-15-0 ——————— Carbon Dieulf ide__________125075-35-4———————1,1-Dichloroethene________125075-34-3 ——————— 1,1-Dichloroethane________1250540-59-0——————1,2-Dichlorethene (total )__125067-66-3 ———— —— Chloroform_______________1250107-06-2——————1,2-Dichloroethane________I 25078-93-3 ——————— 2-Butenone_______________1700071-55-6———————1,1,1-Trichloroethane______125056-23-5 ——————— Carbon Tet rach lor ide_______1250108-05-4——————Umyl Acetate_________ 150075-27-4————————Bromodiehloromathana 125078-87-5———————1,2-Dichloropropane_______125010061-01-5—————ci»-l,3-Dichloropropene____125079-01-6 ——————— Trichloroethene___________1250124-48-1 —————— Dibromochlorome thane_______125079-00-5———————1,1,2-Tri chloroe thane______125071-43-2———————Benzene__________________125010061-02-6————tran»-l,3-Dichloropropene__125075-25-2———————Bromoform________________1250108-10-1——————4-Methyl-2-Pentanone_______1400591-78-6——————2-Hexanone_______________1500127-18-4——————Tet rach loroethene_________125079-34-5———————1,1,2,2-Tet rach loroe thane__1250108-88-3 —————— Toluene__________________13200108-90-7——————Chlorobenzene_____________1250100-41-4——————Ethylbenzene_____________1160100-42-5——————Styrene__________________12501330-20-7—————Xylene C total )___________1300______________________________________I___

IUIUIUIU

IUIUIU1UIUIUIZIUIUIUIUIUIUIUIUIUIUIUIUuIUIUIUIEIUIJIU

FURP1 I «JOA 1/87 Kev24

MO.

Matrix: f«oa/v»ttr.)vt/vol:

« Moisturo: not doc.Column: (pacJi/cap)

CAI NO. COMPOUND

dilution factorCOHOTTTRAT10H UNITS:(ug/t or ug/xgj

so

TttraAydrofurtn

25

IEUOLATILE ORGAN ICS ANALYSIS DATA SHEET


Lab Name:£TC Corp. I Laboratory

Lab Code: Case No.:

Matrix: (3011/water) WATER

Samp 1 e uit /vo 1 '• .1 (g/mL) ML

Level: Uow/med) LOU


Column: (pack/cap) PACK

Number TICa found: 4

Cont ract :

SAS No. :

EPA SAMPLE NO.

IIA5592I__

SOG No.:

Lab Sample ID: CA5592U2

Lab Ftle ID: >D2616

Date Received; I/f/41


Dilution Factor: 50. 0


CAS NUMBER

01. 67-63-002. 78-92-203.04. 963-80-4

COMPOUND NAME

2-Propanol2-ButanolUnknown2 -But anone , 3- me thy 1-

RT

10.2215.2222.7419.40

.

EST. CONC

560510220160

Q

J0JJ

FORM I UOA-TIC 1/8

1AORGANICS ANALYSIS DATA SHEET

ERA SAMPLE NO,

Lab Name: ETC Corp.

Lab Code: Case No.:

Matrix* csoil/water) WATER

Sample wt/vol: .0) Cg/mLJ ML

Level: Uow/med) LOW

\ Moisture: not dec.

Column: tpack/cap) PACK

CAS NO. COMPOUND

Contract: I___

SAS No.: SOU No.:

Lab Sample ID:

Lab File ID:

Date fceceived:


Dilution Factor: 5GU

CONCENTRATION UNITS:tug/L or ug/Kg) UG/L u

74-87-3———————Chloromethane__________74-83-9——————-Sromome thane___________75-01-4———————Uinyl Chloride_________75-00-3———————Chloroethan*___________75-09-2———————Methyl ana Chloride______67-64-1 ——————— Acetone_______________75-15-0———————Carbon Disulf ida________75-35-4———————1,1-Dichloroethane______75-34-3 — ————— 1,1-Dichloroe thane______540-59-0——————1,2-Dich lore thane ( t o t a l ).67-66-3———————Chloroform_____________107-06-2 —————— 1,2-Dich loroethana______78-93-3 —— ———— 2-Butanone_____________71-55-6———————1,1,1-Trichloro* thane___56-23-5———————Carbon Tat rach lor ide___u108-05-4——————Uinyl Acetate__________75-27-4——————-Br omodi ch loroma thane____78-87-5--—-—--1,2-Dichloropropane_____10061-01-5————-ci»-l,3-Dichloropropen«_79-01-6————-Trieh 1 o r o « t h a n e _ _ _ _ _ _124-48-1----—-—Dibromochloromethene_.___79-00-5———————1,1,2-Trichloroe thane___71-43-2———————Benzene_______________10061-02-6————~trane-l,3-Dichloropropene.75-25-2———————Bromoform_____________108-10-1——————4-f1athyl-2-Pentanone____591-78-6——————2-Hexanona_____________127-18-4——————Tat rach lore* thene_______79-34-5 ——————— 1,1,2,2-Tet rach loro*thane.108-88-3——————Tolu*na_______________108-90-7——————Chlorobenzene__________100-41-4——————Ethylbanzen*___________100-42-5——————Styrane_______________1330-20-7—————Xylena (total)_________

I___________

I.15000.I50UQ.15000.15000.16400.1 140UO.12500.12500.12500.1250012500.12500.19500.12500.1250015000.12500.12500.1250012500.12500.12500.12500,12500.12500.I5QUO,15000I25UO.12500.I36UO.12500.12500.12500,12500.1____

IIUIUtuIUIIIUIUIUIUIUtuIIUIUIUIUIUtuIUIUIUIUIUIUtuIUIUIUIIUIUIUIU

FORM I UOA

IAOMMXCI AKXLY.I, DATA

•~ fiTg

*»«*•« -____ C... He.:Matrix: (aoii/vator)JJ£T^S«apl« vt/vol:

I Meisturtt not docColumn: (paeX/c«p)

CXJ KO. COMPOUND

Totrahydrofuran,

Saaplo ID:mo ID:

i Xocoivod: t/BfaiAnalyxod: i/iv/^/

/ ~~r^dilution Factor: _JO?

COKCCmUTlOM OMITS(ug/t or u«/Kgj -

mm z VOA I/I? Rev

28

VOLATILE ORGANICS ANALYSIS DATA SHEETEPA SAMPLE

Lab Namai ETC Corp.

Lab Coda: Case No.:

Matrix: (»oiI/water) UA.TER

Sample wt/vol: 5.0 Cg/mLJ ML

Level: i low/mod) LCltJ



Cont pact

SHS No.

IA5593I________

SDb No.:

Lab Sample ID: Crt-?59?c

Lab File ID: >D2602

Date Keceived:

CAS NO. LQMPOUND


Di 1 ut ion Factor:

CONCENTRATION UNITS:tug/L or ug/Kg) Ub/L U

74-87-3---------Chloromethane__________74-83-9---------Bromomethane___________75-01-4————————Vinyl ChloPide__________75-00-3———————Chlopoe thane___________75-09-2 ——————— tlethylene Chlopide______67-64-1 —————— -Acetone_______________75-15-0 ——————— Capbon Disulf ide_______75-35-4———————l,l-0ichlopoethene______75-34-3 ——————— 1,1-01chloroe thane______540-59-0——————1,2-Dichlorethene t total).67-66-3————————Chlopofopm______________107-06-2——————1,2-DichloPoe thane______78-93-3 ——————— 2-Sutanone_____________71-55-6———————1,1,1-TpichloPoe thane___56-23-5———————Carbon Tat pach IOP ide____108-05-4——————Vinyl Acetate__________75-27-4----—----Bromodichloromethane____78-87-5———————1,2-0ich lopoppopane____'_10061-01-5—————ci»-l,3-DiehlopopPopene^_79-01-6—-———'-Tpichlopoethene^.._______124-48-1——--——Dibromochloromethane^.___79-00-5———————1,1,2-Tp ich lopoethane___71-43-2———————Benzene_______________10061-02-6—-——tP«n»-l,3-DichlopopPop«ne.75-25-2———————Bpomofopm______________108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-H«xanone_____________127-18-4——-———Tetpachlopoethene_______79-34-5 ——————— 1,1,2,2-TetPechlOPoethane.108-88-3 —————— Toluene_______________108-90-7——————Chlopobenzene__________100-41-4——————Ethylbenzene___________100-42-5———————Stypene_________________1330-20-7—————Xylene (total)________

I.1 10.110.110.110.14.18.15.15.15.15.15.15.110.151511015.15.1515.15,151515,1511011015151515151515I__

IUIUIUIUIJIJIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU

FORM I UDA 1/87

29

Ma**:,Coda:

VOIATZIX OMAMZCS

ereDATA SHXZT NO.

caa« MO.:Matrix: (aoil/vatar) adfrrafcSaapla vt/vol: S (q/aLi ^Uval: (lov/iad) LQL±* Moiaturat not doc.column: (pacX/cap)

CXJ HO. COMPOUND

Contract;

IAS M O . J _____ 100 M«.:

Ua Supla ID:

Ub fU« 10:

Data Kaeaivod:Data AAalysod:

dilution Factor:COMCtzmUTXOM ONZTS;

or ua/Kai AAC/t

Tatrahydrofuran

1/17

30

ItE UftliftMlCS wNWLrSIS UHfft bHc.£TViYELY lUtNTIFlEU COMPGUNUb

NU

Lab Name:£TC Corp, I Laboratory

Lab Code: Case No.:

Mat r i x : ', so i 1''water .1 UH , £R

Samp le wt -j'vo l : b . U '. g -'mL-1 ML

Le'-<e 1 : ". low/med J LJW


Co 1 umn : ". pack •- -;ap J

Number lICs found: 1

Lon tract :

SHb No.: SL-IJ No .

Lab 'samp 1 e ;-j: C>-"•

Lab F i i e ID: - L'

ua te Kec

Date Hnaiyzed: Ul

U i l u t i o n i- a c t o f :

LUNLtN rfctt i IUH Ur^, ltug/L or ug-'KgJ u

CttSs NUMBtft

01. 1U66-4U-6

COMPGUNU NMML

bilanoi, trimethyl-

.

R l

16 . 2*

1Eb ' . CUML t U 1

2 / U ili i1t lii li1 !11 1I1 111 111 111 11i 111 1t1 1I1 111 [11 1

r LWfl I '.'Gft- I IC

31


Lab Name: ETC Corp.

EPA SAMPLE NO.

A5597Contract: i___

Lab Code: Case No.: SAS No.: SU£ No.:

Matrix: (.soil/water) WATER Lab Sample ID:

Sample wt/vol: 5.0 Cg/mL) ML Lab File ID:

Lave 1: c. low/mad) LGU1 Date Received:


Column: ipeck/cap) PACK

Date Analyzed: 01/15x91

Di lut ion Factor: i

CAS NO. COMPOUNDCONCENTRATION UNITS:lug/L or ug/Kg) U6/L

74-87-3 ——————— Chlorome thane_____________11074-83-9 ——————— Bromomethane____________ 11075-01-4———————Vinyl Chloride____________1130075-00-3———————Chloroe thane______________11075-09-2———————Methylene Chloride________1567-64-1 ——————— Acetone__________________15400075-15-0———————Carbon Dieulf ide__________1575-35-4———————1,1-Dichloroethene________1575-34-3 ——————— 1,1-Dichlo roe thane________15540-59-0——————1,2-Dichlorethene (total)__1110067-66-3———————Chloroform_______________15107-06-2——————1,2-Dichloroe thane________1578-93-3———————2-Butanone_______________11700071-55-6———————1,1,1-Tnchlo roe thane______1556-23-5———————Carbon Tetrachlor ide______15108-05-4——————Uinyl Acetate_________ 11075-27-4--——----Bromodich lorome thane_____ 1578-87-5———————1,2-Dichloropropane_______1210061-01-5—————ci»-l,3-Dichloropropene____1579-01-6———————Tri chloroe thane___________12124-48-1————--Dibromochloromethane_^____l579-00-5———————1,1,2-Tr i chloroe thane_____1571-43-2———————Benzene__________________1510061-02-6—————trane-l,3-Dichloropropene__!575-25-2——------Bromoform_________m_______15108-10-1——————4-n«thyl-2-Pentanone_______I 39 00591-78-6——————2-Hexanone______________110127-18-4——————Tetrachloroethene_________1279-34-5———————1,1,2,2-Tetrachloroethane__15108-88-3——————Toluene__________________13300108-90-7——————Chlorobenzene_____________15100-41-4——————Ethylbenzene______________1770100-42-5——————Styrene__________________151330-20-7—————Xylene (total)___________11600..______________________________________I____

U

IIUIUIEIUIUIEIUIUIUIEIUIUIEIUIUIUIUuIUIJIUIUIUIUIUIEIUIJIUIEIUIIUIE

FORM I VGA I/.

1AVOXATXIX OXOAXXes ANAlYStS DATA 08ZZT SAKm KG.

Uto Naaot grigU» Coda i Caao No.:Matrix; fooil/vatori aJfrrae.Samplo vt/voi:Uvol: (low/mod)I Moisturo: not doe.Column: (paeJc/cap)

CAJ NO.

fq/mli mt

COMPOUND

'•Dilution raetor:coNccmurioN CNXTS

or uo/Koi

Totraiiydrofuran

row x 1/17 R«v.

33

IEVOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS


Lab Code: Caee No.t

Matrix: (soil/water) UtATER

Samp la wt/vol: 9.0 Cg/mL) ML

Level: (low/mad) LOLJ

* Moistura: not dac.


Numbar TICm found: 10

EPA SAMPLE NO.

IIA9997

Contract:

SAS No.: SDG No.:

Lab Samp la ID: CA5597V3

Lab Fila ID: >D2630

Data Received:

Data Analyzed:

Di lut ion Factor: 1.0

CONCENTRATION UNITS:(ug/L or ug/Kg> UG/L

CAS

01.02.03.04.09.06.07.08.09.10.

NUMBER

78-92-267-65-0107-87-979-01-46032-29-7626-93-779-43-4

963-80-4

COMPOUND NAME

2-Butanol2-Propanol2-PantanonaEthane, chloro-2-Pantanol2-HexanolMethane, dichlorof luoro-Unknown2-Butanona, 3-mathyl-Unknown

...

...

RT

19.6610.6419.424.2020.3923.697.1916.9417.792.90

EST. CONC

910026001002901912404110

Q

3JJJJJJJJJ

FORM I UOA-TIC 1/87 Raw.

34

1AVOLATILE ORGAN ICS ANALYSIS DATA SHEET

EPA SAMPLE NO

LaD Name: ETCNJ

Lab Code: Case No.:

Cont ract

SAS No.

Matri (soil /water) WATER

Sample wt/vol: . (W

Le^e 1 : ( low/med > LOW



CAS NO. COMPOUND

g/mL) ML

SDG Mo.:

Lab Sample ID: CA5597V2j»f

Lab File ID: C2139

Date Received: 01/2 '91

Date Analyzed: 01 ••' 13••"51

Di lut ion Factor

CONCENTRATION UNITS:Cug/L or ug/Kgj UG/L

1000

1 I74-87-3 ——————— Chloromethane_____________I 10000 ID74-83-9 — — - ——— Bromome thane_____________I 10000 IU75-01-4———————Uinyl Chloride____________110000 IU75-00-3 ——————— Chlo roe thane_____________I 10 000 IU75-09-2———————Methylene Chloride________15000 !U67-64-1 ——————— Acetone__________________1 110000 I75-15-0———————Carbon Disulfide__________15000 IU75-35-4———————1,1-Di chlo roe thene________15000 IU75-34-3———————1,1-Dichloroe thane________15000 IU540-59-0 —————— 1,2-Dichlorethene (total)__15000 IU67-66-3 ——————— Chloroform_____________r_l5000 IU107-06-2——————1,2-Dichloroethane________15000 IU78-93-3————————2-Butanone______________ I74QQQQ IE71-55-6———————1,1,1-Tri chlo roe thane______15000 IU56-23-5———————Carbon Tet rach lor ide______15000 IU108-05-4——————Vinyl Acetate_____________I 10000 IU75-27-4————————Bromodich loromethane_______15000 I U78-87-5———————1,2-Oichloropropana_______15000 IU10061-01-5—— —— ci*-l,3-Dichloropropene____15000 IU79-01-6 ——————— Trichloroethene___________15000 IU124-48-1——————Dibromochlorome thane______15000 IU79-00-5———————1,1,2-Tr ichloroethane______15000 IU71-43-2———————Benzene__________________15000 IU10061-02-6————tran»-l,3-Dichloropropene__15000 IU75-25-2 ——————— Bromoform________________15000 IU108-10-1 —————— 4-Methyl-2-Pentanone______13400 U591-78-6——————2-Hexanone_______________110000 IU127-18-4——————Te t rach lo roe then*_________15000 IU79-34-5———————1,1,2,2-Tetrachloroethane__15000 IU108-88-3 —————— Toluene__________________118000 I108-90-7——————Chlorobenzene____________15000 IU100-41-4——————Ethyl benzene_____________15000 IU100-42-5 ——————— Styrene____________________15000 IU1330-20-7——————Xylene (total )____________15000 IU______________________ ___ _____________I____ ___ ___t

FORM T

SAKVU NO

caaa NO.:Matrix: (•oil/vatar) W*r&LSample vt/voi: GOT fq/mliUvai: (lev/Bad) tonI Moisturot not dac.column: (pack/cap)

CXJ NO. COMWUKO

£Ab rila 10:

0*ta Raeaivad:Data Anaiyiad: _tMht

dilution factor: (ccoCONCXXTMTXON CHITS'"-" or ug/Kgj -

Tatranydrofuran

VOW Z VOA 1/17 X«v,

36

UQLATILE ORGAN ICS

_3t Nan-.* : ETCNJ

_sb Code : Case NO. :

Mat r . • : ',st i . • uat«- LJATE=

5amp le wt ••''.•&1 i 5.0 • q-'ml

IHANALYSI5 DfcT* SHEET

EPrt SAMPLE

L o n *. r a c • :

Moiiture: rot aec .

Columr : r. pack 'ca

CAS NO. COMPOUND

5AS No . : BDG ' -.o . '

Lac S amp 1 e ID: Cn55 ilJ'

J *1L Lab F: le ID: C21SS

Date Rece ii-.'*c : 01 •? 9

Date analyzed: 31-"13"'

D i l u t i o n Factor:

CONCENTRATION UNITS:(ug'L or ug/Kg, UG.-'L Q

! 74-87-7---- — ---Chloromethane______________ 101 74-33-9----- — --Bromomethane_______________ 10! 75-01-4- ——————— U i n y l Chloride_____________ 1075-00-7- — — - —— Chlo roe thane_______________ 10

! 75-09-2-- ————— tlethylene Chloride________ 5! 67-64-1 —— ------Acetone____________________ 7I 75-15-0 ——————— Carbon Disulfide__________ 5! 75_35-4_.._ — —— 1,1-Dich loroethen*________ 5I 75-34-3 —— ———— 1,1-Dichloroethane________ 5I 540-59-0———————1,2-Dichlorethene (total)__ 31 67-66-3--- —— - — Chloroform______________,__ 5! 107-06-2———————1,2-D ich lo roe thane_________ 5! 78-93-3 ———————— 2-Butanone_____________" 10t 71-55-0- —— ———— 1,1,1-Tr ich loroethane______ 5i 56-23-5 — - ———— Carbon Tet rach lor ide______ 5! 108-05-4———————Uinyl Acetate______________ 10I 75-27-4--- — ----Bromod ich loromethane_______ 5: 78-87-5 —— - ———— 1,2-Dich loropropane_______ 51 10061-01-5—————ci»-l,3-0ichlopopropene____ 5! 79-01-6———————Trichioroethene___________ 89I 124-48-1-- — ----Dibromoch loromethane_______ 5: 79-00-5- ———————1,1,2-Tr ich loroethane______ 5I 71-43-2 ——————— Benzene__________________ 5! 10061-02-6—-——tran»-l,3-Dichloropropene__ 5I 75-25-2 —— --- — -!-8romo.form__________________ 5i 108-10-1- —— - —— 4-Methyl-2-Pentanone______ 10I 591-78-6 —————— 2-Hex»none_______________ 10i 127-18-4 — ------Tetrachloroethene_________ 2I 79-34-5 ———— ——— 1,1,2,2-Tetrachloroethane__ 5! 108-88-3 —————— Toluene__________________ 5I 103-90-7---- ——— Chlorobenzene______________ 5I 100-41-4—--- —— Ethylbenzene_____________ 5I 100-42-5 —————— Styrene__________________ 5i 1330-20-7—————Xylene (total)___________ 5

ItuIUIUIUIUIJtuIUIU10IUIUIUtuIU1UIUIUIUIIUIUIUIU!UIUIU13IUIU;uIUtuIU

-57FORM I UOA 1/87

1AvoutrxLt OMANZCS ANALYSIS DATA raterU* flftt

U» Cotfos

Matrix: (aou/watar) Q&TBLvt/v°l' _S__(f/Bt)m

(lev/mod) iGLi% Moiaturai not doe.Coluan: (pack/cap)

"* K0' COMPOUND

*08 NO.:Saapia zoi«!• ID:

Otta Kaeaivad: ,7 ,*ta Anaiytad: _^,»iiution raetor:

I Tatrahydrofuran

I/I? Xov,

38

IEVOLATILE ORGAN ICS ANALYSIS DftTn SHEET


E 'iO.

Lit NameiETCNJ

_sb '!•:• de : laie No .

M a t - . . - : ', 5'-;. 'wats.-1 HATER

r-ampl* wt--'''ol: ?.0 ':

Leve 1 - ' lo-.j-''mec .• LQi!

** Me i a-1 UP* : not aec .

Co 1'jnv-. : '.pack '-'cac ) PACi-'


Contract :

Lab 'Sample IL '• Cn'rf'3'

Lab Fi le it"- C::*'

Date Receiver: 01

Date Hna 1 y=ed : C 1 •'! 3


CONCENTRATION UNITS:Cug/L or ug/Kg 1 UG/'L

1,0

CAS NUMBER COMPOUND NAME ! RT 1ST. CONC

FORM I "JOA-TIC 1-'

1AVOLATILE ORGANICS ANALYSIS OATH SHEET

EPA SAMPLE NO.

A53Q5LaD Name: ETCNJ

Lab Code: Case No.:

Matrix: ', so i 1 /water ) WATER

Sample uit/vol: 5.0 (g/mLJ ML

Level: f. low/med; LOW

'•i Moisture: not dec.


Cont ract:

5AS No.:

CAS NO. COMPOUND

SDG Mo . :

Lab Sample ID: Crt5805U2

Lab F i l e ID: C2187

Date Received: Ql-'fcx91

Date Analyzed: Ql'18'91

Di lu t ion Factor : 1

CONCENTRATION UNITS:CugxL or ug/Kg) UG/L

74-87-3 — - ——— — Chlorome thane_____________I 1074-83-9--- ———— Bromome thane_____________11075-01-4———————Vinyl Chloride____________HO75-00-3 ——————— Chloroa thane_____________11075-09-2 ————— --Methylene Chloride________1567-64-1———————Acetone__________________11075-15-0———————Carbon Disulf ide__________1575-35-4———————1,1-Dichloroethene________1575-34-3 — ————— 1,1-Dichloroethane________15540-59-0 —————— 1,2-Dichlorethane (total )__1567-66-3———————Chloroform_____________ 15107-06-2 —————— 1,2-Dichloroe thane________1578-93-3———————2-Butanone_______________11071-55-6 ——————— 1,1,1-Tri chloroa thane______1556-23-5———————Carbon Tetrach lor ida_______15108-05-4——————Uinyl Acetate_____________11075-27-4——-———-Bromodich loromethane_____ 1578-87-5 ——————— 1,2-Dichloropropana_______1510061-01-5—————ci»-l,3-Dichloropropene____1579-01-6———————Trichloroe thane___________15124-48-1——-———Dibromochlorome thane______1579-00-5 ——————— 1,1,2-Trich loroethane______1571-43-2———————Benzene__________________1510061-02-6 ——— --tran»-l,3-Dichloropropene__(575-25-2- — -————Bromoform________________15108-10-1——————4-Methyl-2-Pent«none______110591-78-6——————2-Hexanone_______________110127-18-4——————Tetrachloroethen*_________1579-34-5———————1,1,2,2-Tatrachloroethane__15108-88-3 —————— Toluene__________________15108-90-7——————Chlorobenzene_____________15100-41-4——————Ethylbenzene_____________!5100-42-5——————Styrene__________________151330-20-7—————Xylene (total)___________15

IIUIUIUIUIUIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUtuIUIU

IEVOLATILE ORGAN ICS ANALYSIS DATr, SHEET


Lai 'iirr*:

Lab Code : _ase No . '•

Lcr. t r ac r :

SAS No.:

le vit --'vo 1 : 5.0

Leva 1 : • low/med LOW

'b tlo is t ur e : not dec .

Column.: < pack /'c a^ .' PACK

Number T ICs found: 0

Lab Samp 1* 1C: d-^SO'

g---'mL.' r'lL Lab ~: le ID: 121?'

Dat* Pacaived: 0 1 -- g

Date Ana lyied : 01 -"'13

D i l u t i o n Fac tor:

CONCENTRATION UNITS:lug/L or ug^Kg,' UG/L

•3 1

1 CAS NUMBER

1ti1111i!i

!1I11t»

i1ii

I;I1111111

COMPOUND liAMEI 1

RT 1 EST. CONC 1 J........ i............. )»....

1 !!11t i1 11 i1 Ii ;

U ! !! 11 1i i1 1i 11 I1 1t 111 11 !

1 1

1 !1 11 >1 I1 !

1 1

1 !t '1 !

FORM I UQA-TIC -42.

iri EP« SAMPLE '0VOLATILE ORGAN1CS ANALYSIS D*'H SHEET _____________

I

;*: ETCNJ • Cop-tracr:

Lab Cede : Cai* :-»c . : EAS ? :<. :

h a t r ; . : '. so i 1 /wat* - ' UHTEF Lab Samp:* 1C: CA^SO*1.'?

Samp 1* wt /vo 1 i 5.0 '" g 'mL.1 1L -ab F: le ID: C2i°0

Level 'Isw/mei LOU Dai- Receiver: Hi |0 •?:

% Hoistups: not dec. Date nna 1 yz*d : 1-1-'I3 '3.'

Column. tpack'cac PACK D i l u t i o n Factor:

CONCENTRATION .HITS:CAS NC. COMPOUND (ug -'L OP ug/Kg UG/L Q

11 74-87-3 ———— -i 74-83-9 ———— -t 75-01-4 ———— -• 75-00-3 ———— •! 75-09-2 ———— -i 67-64-1 ———— -1 75-15-0- ——— -; 75-35-4 ———— -1 75-34-3 ———— -1 540-59-Q ——— -1 67-66-3 ———— -' 107-06-2 ——— -! 78-93-3 ———— -: 71-55-0 ———— -1 56-23-5 ———— -1 108-05-4 ——— -i 75-27-4 ———— -1 78-87-5 ———— -1 10061-01-5 ——! 79-01-6 ———— -1 124-48-1 ——— -! 79-00-5 ———— -i 71-43-2 ———— -

1•---Chloromftthan* 1•---Bromome thane 1. —— Vinul Chloride !- —— Chlopo* thane 1. — -Methvlene Chloride 1

. —— Capbon Disulfide „ „ :- —— 1.1-Oiehloroethenft 1• —— 1.1-Dichloroethane !- — -1,2-Dichlorethene '.total .1 __ 1•---Ch lorof opm , 1•- — 1.2-Dichlaroethane, - 1. — -2-Butanon« 1. —— 1.1.1-Tp ichlape«than« 1.- — Capbon Tet rach lar ide 1. —— Uinyl Acetate ,.., n . .. ., 1

.»..! ,2-Oieh Inraprapan* _IM _. 1— — ci»-l,3-DichlopopPOpene____f.---Tp iehloro«th«n«_ 1. — -Dihromaeh larom»th«n« 1• -• — 1 rlr2-Tp ieh larce thane t

1 10061-02-6 ———— trans-l,3-DichloPopPOpene __ 1! 75-25-2- ————— --Bromoform _ 1! 108-10-1 ——— -1 591-78-6 ——— -! 127-18-4 ——— -I 79-34-5 ———— -I 108-88-3 ——— -1 108-90-7 ——— -1 100-41-4 ——— -1 100-42-5 ——— -1 1330-20-7 —— -i

. —— A-M«thvl-2-P«ntanan* , , ,. 1• — -2-H«x«non« IM , mii 1

• —— 1>1>2 ,2-Tetrechloroe thane __ 1. — .Talu»n« m m M I• —— Chlareb*nz*n« , , 1— --Cthy Ibenzena., .... 1• —— Styp«n« mi ma 1- —— Xylene (total) ,, . 1

1

10101010

3

5551055105555

55551010

6555R

1IUtuIUIU: JI JIUtuIUIU

IUiUIUtuIUIUIUIUIUIUIUIUIUIUIUIUIU!U1IUIU!UIU) . _

FORM I VOA 1/87 Re-

Uval: (lov/Md)I Maiaturai net dee*Coluan: (paeX/ctpj

Taerafey4rofuran

Jt«v

44

IEVOLATILE ORGAN1CS ANALYSIS DAT* SHEETTENTATIVELY IDENTIFIED COMPOUNDS

Lab NamaiETCNJ

Lab Code:

Ma *: c i . : i sc i 1 'us t e

Samp le wt^vo 1 :

Lev* 1 : '. iou/'mrsc '

*4 Moisture: not dec.

Column: i pack 'car:) PACK.


EPA SAMPLE . iO.

IA53QoCon t; rac t :

Case 'la. :

UiATEP

? . Q -.g/mL J ML

LOU

3&G -.0. :

LSD Sample ID: CM?39oU2

Lab F i l e ID: C21* 3

Dat* Received: Ol'p-'9l

Date Analyzed: 01/18 '91

D i l u t i o n Factor: 1.0

CONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

i1 CAS NUMBER

Il11I!!1i1ii

!iii1iiItIti11!1i11

COMPOUND NAME RT

.fc_

1EST. CONC 1 Q

!1II11!1

1111t

1i;iIiiilil!1111

FORM I UOA-TIC

Lab Nama: ETCNJ

Lab Cod*:

2AUATER VOLATILE SURROGATE RECOVERY

Contract:

Casa No.: 5A8 No.: SOG No

1 EPAI SAMPLE NO.

Oil UBLK01021 A996303 t A9974041 A9999091 A998006 t A9981071 A998208 t A9603091 A9994101 A9999111 UBLK02121 A980913 1 A9999141 A9806,191 A999116 1 A98Q9JB171 A9606A*181 A9991AB19 1 UBLK03201 A9999MS211 A9999MSO221231241291261271281291 -301

SICTOL)*

100989899102979696981071077876847977787898109128 *

.

S2CBFB)*

999799100999796989910610778768479767678110117144

S3CDCE)*

979897101979999100979893929394919092919696 •94

OTHER

—————

TOTOUT

000000000002222222012

paga 1 of

51 CTOL) - Toluin«-d852 CBFB) « Bromofluorobanzana53 CDCE) • l,2-Dichloro«than«-d4

* Column to ba usad to flag* Valuas outsid* QC limits0 Surrogates dilutad out

QC LIMITS(98-110-)(86-119)(76-114)

raeovary values

FORM II UOA -1

2AWATER VOLATILE SURROGATE R£LO<Jfc*Y

L*b N*m»: ETC Corp. I Laboratory Contract:

Ljb Code: Cas« No.: SrtS No.: SOU No

paoa 1 of

1 EPA1 bftrlPLE NO.

Oil UBLK01021 W577U3i A**85041 ft^-586051 H-J^Q?061 A5596071 A5571081 A*583U9I A'?$84101 AS989111 A5S9312 1 UBLK0213 1 A5578141 At-579151 A$*9Q161 A5$68171 «5*92lai UfaLKO>191 A55772UI A^572211 A957^nS221 A5572MSO231 A*>*68Mr241 A5588251 A5*92«fr261 A5597271281291301

SItroutV61001U197979697979796V6989898ya969898979710010099989745 •

S2(BFBJ*

iUQ99y9100101999999V998ys999998V8999810010198V997va9896106

S3(DCEJ*

9086919291909111311291109100105102113128 •125 »100114101112128 .*120 *99"123 *3 *

01 HEW TonOUTi

0 :0 I00 10 i00a0000000110000 :1 11 i0 11 12 I

!11t

UC LlPlITbSI (TOLJ • Tolu«ne-dS C88-110JS2 (8H8) - Bromof luorobanz«n« C86-11TJS3 (UCEJ - 1 ,2-Oichloro«th«n»-d4 (76-114)

t Column to b« u»ad to flaa* U*lu«» outside QC lim i t s0 Surpoa«t«» diluted out

FORM II UOA -1 1X87 Re-

47

Lab N«me: ETCNJ

Lab Code:

2AWATER VOLATILE SURROGATE RECOVERY

Con t. rac t :

Case No.: 3AS ho. : EDG

t EPA1 SAMPLE NO.

01 UBLKQV*021 4?99:«4ft.|fa|03134105 10*1071081.091101111121131141151161171191191201211221231241251261271291291301

SIC TOL ) *

107» 76 *

32(BFBj*

10777 *

S3IDCE)*

9333

•

1

OTHER TOTOUT

0i

page 1 of

51 tTOL,' « Toluene-d952 CBFB) * Bromofluorobenzene3? CDCE) • l,2-Dichloroeth«ne-d«i

QC LIMITSC88-11Q)'.86-115.'C76-114)

* Column to be used to flag* Values outside QC l i m i t sD Surrogates diluted out

recovery va lues

FORM II UOA -1

3AWATER VOLATILE HA I SIX SHIKE/MA1RIX SPIKE OUPLICHIE RfcuQOtKY

Lab Name: ETC Corp. I Laboratory Contract:

Lab Coda: Case No.: SHb No.: Sub No.:

Matrix Spika - biPA Sample No.:

COMPOUND

1 rl-Dieh loroathene _Trichloroathane,BanzanaTo luanaChlorabanzena . — .,

SPIKE«UL>eUtug/L)

90. UUQ90. OOU90. UUO90. OOU50. UUO

SftHh-LELUNCENTRrtTION

tug/LJ

o.uoo0.0009.^08o.oooo. uoo

nsCUNLtNfftMl 1UN

tug/LJ

49. 6>4<.6ly47.j»294^ . 45«4A.dl9

MbH

Ktt #

*185/889yQ

XLini I'bi.--c. •

61-145 i7i-liu i>^6-i27i76- 121? I/"?-iJOi

I

COMPOUND

1 rl-Dichloro«th«n« __.Tr ich laroathana _ — ,.„ ^BmnxmnmTolu«n«Ch larofa«nz«n«

SHIKEADUEDtug/LJ

90.00090.00090.00090.00090.000

MbDCONCENT RATION

(ug/LJ

42 . 74238.81044.06b .40.UJ941.696

MbOS

RhL *

897fl72 •8083

*RHU *

6y967

UC LRPU

141411i313

IMl i SKtL. 1

61-14T' t/1-T20 i76-12/1/6-J.25 i7T-13u t

•

4 Column to ba u»ad to flag raeovary and RPO valuaa with an a»t«n»K

* Ualuaa outsida of l i m i t s

RHO: 0 out of 9 outaida l i m i t sSpike Recovery: 1 out of 10 outside l i m i t s

Comments:

FORM III UOA -1 1/87 Re'

49

WATER VOLATILE MATRIX SPIKE-'MATRIX SPIKE DUPLICATE RECOVERY

Lab Name: ETCNJ Contract:

Lab Code: Case Mo.: SAS Mo.: SDG Mo,:

Matrix Spike - EPrt Sample No.: A5599

!! COMPOUND

1 1,1-Oichloroe thane1 Trichloroethene^,,1 Benzene1 To lu«naim _ .,1 Ch lorobenzana1

1 SPIKE! ADDEDI (ug/L)

1 50.0001 50.0001 50.0001 50.0001 50.0001

! SAMPLE1 CONCENTRATIQM1 Cug/L)1 ..............1 0.000I 39.0671 0.0001 0.0001 0.0001

MSCONCENTRATION

Cug/Lj.............

49 . 764101.27245.55956.9339.432

MSNREC

100249111419

L;:-:TS# 1 REC . I

161-145 1*i7i-i:o i176-1271176-125 1

*I75-1?OI1 I

COMPOUND

1 , 1-Dich loroetheneTr ich loroatheneBenzeneTo luene nCh lorobenzena,

I SPIKE/ I ADDED

1 Cug/L)

1 50.0001 50.0001 50.0001 50.0001 50.0001

MSDCONCENTRATION

(ug/L)

45.41799.75745.41965.130 149.348

MSD\REC *

9121 *91130 •99

SRPD *

<9

13013136 *

!QC LIMITS IRPD ; PEC. '

14 61-U5I14 171-120111 I76-12TI13 176-125113 :75-17Q:

I i

t Column to be used to flag recovery and RPD values uith an asterisk

* Values outa id* of limits

RPD: 1 out of 5 outside limitsSpike Recovery: 4 out of 10 outside limits

lommen t 9 '•

FORFl III VOA -1 'l/87 Pev.

50

VOLATILE METHOD BLANK SUMMARY

Lab Name: ETCMJ

_ab Code: _ase Mo.

^ab F i l e ID: . C213o

Oats Analyzed 01--'13/9i

flat r ix : < so i 1 '-'water > WATER

Instrument ID: GC/MS C

Contract:

5AS tlo . '• 5DG no. :

Lab Samp la 10: • SLKO

Time Analyzac: 1237

Lsve 1 '. '. low-'med ! _GU

THIS P1ETHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, '13 AND M

Comment 3:

! ERAI SAMPLE NO.

01 A58Q5021 M959903: A5806041 H559105 i A5805)t&061 A?8Q6*£07. A5591nfr08109 t10111112 t13114115116117118119150121122123 t241251261 ^^27128129 1301

LABSAMPLE ID

CA58Q5U2CA5599U2CA5806U2CA5591Y2CA5805IJ2CA5806U2CA5591W2

• ••

LABFILE ID

>C2187•'C2188>C2190>C2191VC2192>C2196>C2197

"

TIME 1ANALYZED t

1336 I1424 11558 11646 11747 t2058 !2146 1

1t111I!I1I1I11111tIf111

page 1 of \FORM IU "JOA 1/87 Re-

51

uIk

*D

I tO33

o;o

aD

Vjl

OIJ^

I-JCO

IJ•sj

IOCK

I-JvJl

10**

10•v*

I-Jto

IOI-1

KtO

t->•o

r-CO

t—M

e-O

i—•Jl

»-**v

•

1—»j4

I—IO

1—I-*

t—O

Cl•ft

oOD

oNJ

C=>^

Osfl

t_«*

c-*J* 0 0

10 »-"

01-I I>*J» ^sn -Q pi•*• r 11^j m xR so

nI> U*l*J» I>•n n•c ur•-j r y>c ma?IO

o

no r fu m i>•- CD(D•« o

»- i•J1 zH- D -^»- r —

an mRO

HT

Lll

URHXOO

CDri-T;X-•DT)rMRUJ

•HO

HJ.m-norroEZffi

inl»at>rm01

II01

I*-T

6"2ulO

33 ftO .-»••» TT .-C ;-.3a3rt- w

O•— < >-O• •

£ftrr9~t

CJn E3>

3 Hin mDn

r9<•^• •^^_D^

39a.

i "LJ

riar*•

I-3ft

v:Maa

1=1i--XI-*GO\•*)i-»

-1«-•39

!••3ft

\IIna.••»- -i j'•!

J

r»IT

'i..—n^_n

••'OI >»— •U-'lO

ru*aU"lft3T)

ik,„i '•••.-cnr-7;i=.

. **

rikcr

noao

n»IP•zo•"

ui1>tA

O

"

u>O(H..O-••

1"i*IT

Zft3»

mHnzCi

nDjr»TwUft—

COri>H

rm3mHIOO

OJr5xUlC33J>Tl.<

Case No. : DG : o. :

Ls: Samp.-

-H

VOLATILE METHOD BLuNt1 3JMr*AP'f

LaD Mam*: ETCNJ

:_ab Cod*:

L a'. r i i * ! I C 211.

Date -inalvzad 01'1 '?- '91

r1a « : • • : . • . : '. so : 1 -'^a t * r WATER

Inst r ..merit: [ 0: SCAT'S C

THl'E METHOD SLAr;-, APPLIES TO THE FOLLOWING SAMPLES, r'S AMD MSC

! ERA i LAB• SAMPLE NO. . SAMPLE ID

LAB~ILE ID

Commcr. t 5 :

page i of 1 _FORM IV UOA

TIME 1ANALYZED !

Oil H«599MS

03 104105 106 1071oai09 !10 1111121I? 114115 116 117113 119 120121122 1231241251261-<-fi ^^23129 I301

CA5599US 1 C2215CA559°UR i >C2216

1111t1I111111111

* 111iI11|I111

2024 12112 1

11t1I!11

1'1it11i1i111iiI-1^1!

1-'S7

53

4HMEfHUO

Lab Name: £TC Corp.

Lab Code: Case No.:

Lab Fi le ID: >Di99Q

Date Analyzed 01/13/91

Matrix: tsoi 1/water) Uft I tR

Instrument ID: &L/HS 0

THIS ntlMQO bLHNK HPPLttS TO i ME FULLUUlNS •*(•

Con tract:

Srtb No.: iub No.:

Lab iamp le iu:

T i me Hna 1 yzed : I*?"?6

Leve 1 : t t ow/med LUI-.

fib WNU

Comment s;

page 1 of _J_FQRH 10

1 t fl1 5HMPLE NO.

Oil A9S7702 1 «9585031 A9586041 H^98705 1 ft9'596061 H5571071 «9'7a3oa i A9<?84o* i Hf'jSy101 fl599311112113 11411* t16117 1iaily i'20 12il22 123 124125 1261

291'2* 13GI

^ £^aa *j K \ i^M7 f 0 y Vl""~ £^ bh C £* 1 1^ W7 V O O V

CW5596ULH5571U

l" £ b* C O U 1 1^M7 f O f vl" £A^% C* W 4 L 1

Lr-,bFILE ID

> 0*591

> 02594> 0*9*5> 02 5 96> 0*59 7>U*599> 02 6 0 0>D2601> 026 02

•

Ti trtNHLYZbU 1

221623 U> 1

00>7 1

0*97 IU344

t

111I

111i1i1

1,II11

54

VOLATILE MtmQu BLANK

Lab Name: ETC Corp. Contract:

Lab Code: Case No.;

Lab F!le 10: >D*6U6


Matrix: tsoi 1/water) UA I tR

Instrument ID: GL/MS D

No.: 5Ub No.:

Lab bample iij: k-^LK.iJ

Time ttna lyzcd: l*;u/

Leve 1 ; i low'''mea ( LUI

S METHOD BLANK >

1 tr'A1 SAMPLE NO.

Oil A5578U2I A5579031 A5590U4i A556S05 1 A559206 I07108109110111!121131141151161171iaiiy i20 1211221231241251^6 1271281

301

^PPLltS TO (ME

Lriti

SAMPLE ID

LA557VU2CA559U*J2CA5563V2

:ULLQW1NG iHMHL

LHflFILE ID

>LJ26l5> 0^6 16

iS . rib «NU r

Tl i£ i

1*^6 11911 I

i1,1j1I1j

1

1I1

1

1

1i1i1i

Commen ts '•

page 1 ofFQRn IW ft*

55

VOLATILE PlfclHOU BLHNK

Lab Name: ETC Corp.

Lab Coda: Case No.:

Lab Fi le ID: >02621

Date Analyzed Oi/15/91

Matrix: '. so i l/wa ter ) wrt t tR

Instrument ID: GL/nb D

TMlS ME I MOD BLHNK riPPLltS TO I ME t-ULLQwlNG bttPIPLtS, HS nNU MSO =

Contract:

Srtb No.: SUb No.:

Lab Sample 10:

T;me rtnalyzed: IT 14

I: t I owxmed ) Lui.

1 LH«1 SttHPLE NO.

Oil H5577U2I Hl?57203) A5572HS

U61 A5788

U8 109110111112113114115 116117118119 120121122123124125126127128129 t301

LH&SHHPLE ID

CM5592Y3

LrtbFILE ID

>D2624

>D2627>D2628> 02 6 2V

Tl 'E

16U9 11 749 ilti>6 11922 i20U7 I205121J*7 t

l

ii1,

1i1i1i1;l,l,l;ti

Common t s:

page 1 ofFUKH UQtt

56

1AYOLATILE ORGANICS ANALYSIS DATA SHEET

ERA SAMPLE NO.

Lab Name: ETCNJ

Lab Coda: Case No.:

Matrix: (soil/water) LJATER


Level: (low/med) LOU

S Moisture: not dac.


Contract:

SAS No.: SDG No.:

Lab Sample ID: QC7Q443U2

Lab File ID: >C2186

Date Received: 01/1? /91


Dilut ion Factor: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L OP ug/Kg) UG/L Q

74-87-3 ————74-83-9 ————75-01-4 —————75-00-3 —————75-09-2 ————67-64-1 ————75-15-0 ————75-35-4 —————75-34-3 —————540-59-0 ————67-66-3 —————107-06-2 ————78-93-3 —————71-55-6 —————56-23-5 —————108-05-4 ————75-27-4 —————78-87-5 —————10061-01-5 ——79-01-6 —————124-48-1 ————79-00-5 —————71-43-2 —————10061-02-6 ——75-25-2 —————108-10-1 ————591-78-6 ————127-19-4 ————79-34-5 —————108-88-3 ————108-90-7 ————100-41-4 ————100-42-5 ————1330-20-7 ———

1— -Chl aroma thane _ 1--.-Bramamathane I- — Uinyl Chloride , 1—— Chloroethane M I | 1 i— -Methylene Chloride 1—— Acetone , 1—— Carbon Di*ulfide_ 1—— 1 rl-Diehloraethena 1—— 1 r 1-Di eh loroe thane I—— 1,2-Dichlorethene (total ) __ 1— -Chloroform 1—— 1 r2-Diehloroethene ...,_ , 1—— 2-Butanone 1—— 1.1 . 1-Tr ichlo roe thane 1- — Carbon Tet rech lor ide . 1—— Uinyl Acetate 1—— Bromadiehlorome thane 1— -1 r2-Diehlorapraoene 1---ci»-l ,3-Dich loropropene ____ _l---Tr iehlaraathena I---Oihramaehloromathane _, _ n 1—— 1 rlr2-Trieh loroe thane 1- — Benzene 1—— trans-1 ,3-Dich loropropene __ 1---Bromof orm „_. „ 1—— .4-Methyl-2-Pentanona .„ 1, — ~2-Haxanona . , . , , , 1—— Tat raehloroathana , _ . 1—— 1 , 1,2 ,2-Tet rech loroethene __ 1—— Toluene _ 1—— Chlorobenzene , ., '—— Ethulbanzene 1- — Sturene 1——— Xylena (total) 1

1

101010105455555510551055555555510105555555

11UIUIUIUIUIJIUIUIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1

FORM I UQA 1/82 ib /

IAOMAffZC* AJUUYStJ DATA SAT.9U NC

are Contract:

Matrix: (ttil/vatar) coatee.Saaplo vt/vol: s /«/«i.iUvti; (lev/Md)

% Moiaturti not doe.caluan: (pacX/cap) dilution r«ctsr:

TttraAydrofuran

I/I? fttv.

58


ERA SAMPLE NO.

Lab Name:ETCNJ

Lab Coda : Case No.:

Matrix: (soil/water) WATER

Sample wt/vol: 9.0 Cg/mL) ML

Level: (low/mad) LOW



Number TIC» found: 0

Contract:

SAS No.: SDG No.:


Lab File ID: >C2186

Date Received: Q1/|S /91


Di lut ion Factor; 1.0


CAS NUMBER COMPOUND NAME

FORM I UOA-TIC

RT

k

EST. CONC

1/87

5

Q

Rev.

9

1AUOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: ETCNJ

Lab Code: Case No.:



Level: Mow/mad-' LOW



Cont ract:

SAS No.:

ERA SAMPLE NO

1IUBLKQ3I_____________

SDG No.:

Lab Sample ID: QC70443v3

Lab File ID: >C22U

Date Received: Ol/H -'91


Di lut ion Factor: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:Cug/L OP ug/Kg) UG/L

•Ch lopome thane.•Bromomethane_

74-87-3—————74-83-9————75-01-4———————Uinyl Chloride___75-00-3 ——— —— --Chlopoe thane_____75-09-2 ——————— Methylene Chloride.67-64-1——————-'-Acetone_________75-15-0————— •Carbon Diaulf ide.

______(10______110______110______110______15______110______15______15.______15

540-59-0 —————— 1,2-Dichlorethene (total)__1567-66-3———————Chloroform_______________15

15_________ IIP

71-55-6 ——————— 1,1,1-Trichloroe thane______1556.-23-5 ——————— Carbon Tet rach lor ide108-05-4————75-27-4—————78-87-5—————10061-01-5——

75-35-4- ———— —— 1,1-Dichloroethene,75-34-3 ——————— 1,1-Dichlopoe thane.

107-06-2——-———1,2-Dichloroethane.78-93-3———————2-Butanone_______

•Uinyl Acet«t«______•Bromodichloromethane.1,2-Dichloropropane,

——cis-1,3-Dichloropropene,79-01-6- —————— Trichloroethene_______124-48-1——---—Dibromochlorometh«n«_79-00-5 ——————— 1,1,2-Trichloroethane.71-43-2- —————— Benzene____________10061-02-6——-—trana-1,3-Dichloropropene.75-25-2 — - ——— --Bromo'form_____________1Q8-10-1--——---4-Methyl-2-Pentenone.591-78-6 —————— 2-Hexanone________127-18-4-———-Tetrachloroethene_______79-34-5———————1,1,2,2-Tet rach lo roe thane.108-88-3 — ———— Toluene_______________108-90-7---——--Chlorobenzene_100-41-4--———Ethylbenzene__100-42-5-———--Styrene_______1330-20-7—————Xylene (total)

1511015151515151515151511011015151515151515

IUIUIUIUIUIUIUIUIUtuIUIUIUIU!UIUIUIUfUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU

1AVOLA7ZU OMAffZCS AMAX.YSZS DATA 9MXX7

Uft *a««j_firt2

CTA SAXPU HO

Lato Coda: . _^ Caa« *«.:Matrix: (aoil/vatar)JSJJ2B-

vt/voi: 5Lavai: (lev/Bad) *anI Meiaturat not dac.Column: (pack/cap)

CU NO. COMPOUND

Tatrahydrofuran

'.Dilution factor:

(at/I ar

U

I/I? R«v,

61

IEVOLATILE ORGANICS ANALYSIS OATH SHEETTENTATIUELY IDENTIFIED COMPOUNDS

ERA SAMPLE NO.

UBLKQ?Lab Name:ETCNJ

Lab Code : Case no . '•

Matri.. : '. so i 1 ••'water ) WATER

Samp le wt -Vo 1 : 5.0 tg.-'mL) riL

Leva 1 : ' low/med :• LOW



Number TIC* found: 0

Con t r a c t :

3AS Mo.: 3DG rlo. :

Lab Sample ID: QC^04

Lab P i l e ID: •C2211

Date Recewed: Ql-'/fl '* i

Date Analyzed: 01--;9.-9i

Dilution Factor: 1.0


CAS NUMBER

.*f\

COMPOUND NAME

.

• v; -

^

r<

.

RT

..

EST. CONC P Q

FORM I UOA-TIC

VOLATILE ORCAN1CS ANALYSIS OATA SHEET

Lab Name: ETC Corp. Contract: I___

Lab Code: Case No.: S«S No.: Sub No.:

M a t r i x : (soil/water) WAI£R Lab Sample ID: QC~

Sample wt/voi: 5.0 Ig/'mLJ ML Lab File ID: >0*59o

Level: ilow/mad) LUU Uate



CAS NO. LUnPOUNO

NO

Date Analyzed: D

Ui lu t ion t-ac t or :

ION UNITS:tug/L or ug/Kg) Ub-'L

74-87-3 — - ———— Chloromethane_____________11U74-83-9 —— - ——— -Sromomethane_______________I iO75-01-4————————Umyl Chloride_____________I 1075-00-3———— —— Chloroe thane_____________ I J.U75-09-2————————Methyiene Chloride_________I 167-64-1 ——————— Acetone__________________i 1075-15-0 ——————— Carbon Oisulf ide__________1575-35-4———————1,1-Dicnloroethene________1575-34-3 ——— ———— 1,1-0 ichlopoe thane________15540-59-0- ————— 1,2-Dichiorethene t total J__1567-66-3————————Chloroform_________________15107-06-2——————1,2-DichloPoethane________I 978-93-3- —————— 2-Butenone_______________I 1071-55-6 ——————— 1,1,1-Trichlo roe thane______ (956-23-5 ——————— Capbon Tet paeh lor ide ' 19108-05-4——————Vinyl Acetate________ I 1075-27-4-————--Bromod ich loromethane_______1578-87-9 ————-—1,2-0 ichloroppopane_______1510061-01-5—————c »»-1,3-D i chlo pop popene____ I 579-01-6-- ———— -Tpichlopoethene___________15124-48-1———--Di bromochlorome thane______1579-00-5———————1,1,2-Tpichloroethane______ I 571-43-2 ——————— Benzene__________________1510061-02-6 ———— tran»-l,3-0ichlopopropene__I 575-25-2———————Bpomofopm________________15108-10-1 —————— 4-riethyl-2-Pentenone______I 10591-78-6 —————— 2-Hexenone_______________110127-18-4——————Tetrachlopoethene_________1579-34-5 ——————— 1,1,2,2-TetPachlopoelhane__15108-88-3——————Toluene__________________15106-90-7——————Chlopobenzene____________15100-41-4——————Ethyl benzene_____________15100-42-5——————Styrene__________________151330-20-7—————Xylene t total >___________(5______________________________________I__

IUIUIUIUIJIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU

1 UQA

VOZATXU OKOAJrXCS ANALYSIS DATA SXCZTt»A

Uft IUMI gfg

u* c°*«' ——Matrix:

Caso NO*:

Saaplo vt/vol: S (9/mL\Uvol: (lov/aod) 03^I Moisturot not doc.Caluan: (pack/cap)

CXJ KO. COMPOUND

Totrahydrofuran

Dilution factor:CHITS:

or uo/Ktf) MC/L

JSL

HO.

u

I/I? ftcv,

64

It"JOLHTILE ORGftNlCS HNHLYbIS UrtTH SHEET


Si-iMPLE NU.

Lab Name:£TC Corp. I Laboratory

Lao Code: Case No.:

M a t r i x : t s o i 1-'water ) WRIER

Sample ut/Vol: 5.U Cg/mLJ HL

Lev* 1 : ', low/Tisd ) LUU


Co lumn : '.pack/cap ) rHCK

Number llCs found: 0

uont rac t:

Srtb NO.: Sub No,:

Lab Sample iu: 'JL- J-4

Lab F i l e iu: : L-^59

Uate Keceiv-a: |

Date Analyzed: u* 13 -.

D i l u t i o n i-actor:

UNITS:or ug^Kgj UG/'L

CHS NUHBEh; CUnPQUNO NftME

PU«M I yOH-TlC

Rl ES i . CUNL i u

111i1

i

11111111111111111;1)11111

i a 7 " * .- .

65

UOLHMUE UftGrtNlCSIttWNHLfSIS

tflW SHt£T

Lab Name: ETC Corp. Contract: i _

Lab Code: Case No.: Sttb No.: Sub No

datr ix : tsoiI/water) UttitR

Sample wt/yo1: 5 . U

Le^-e I: '. low'med ) LUU


Column: '. pack''cap) KM

CHS NO.

tg/mLJ ML

Lab Sample lO: .

Lab F i l e ID: >L

ua t e Kece i --ed : I

Date rtna lyzed : IJ

D i l u t i o n (-actor:

'RHI'IUN UN i PS:'. ug/L or ug/K.g) bb--'L

74-87-3 — -- —— --Ch ioromethane______________i 1074-83-9 — -- — ---Bromomethane_______________I ID75-01-4- ———— ---umyi Chloride_____________1 1U75-UO-3-- — --- — Ch loroe thane_____________I 1075-09-2 —— - ——— -Methylene Chloride_________1467-64-1 — --- — --ttcetone____________________I 1075-15-0 — —— -- — Carbon Disulf ide__________1575-35-4———— —— -1,1-Oichloroethene_________1575-34-3 — -- —— — 1,1-Dichloroethane________I 5540-59-0- ——— - — 1,2-Uichlorethene t tote I )__i567-66-3 — --- —— -Ch lo reform_________________15107-06-2 —— - ——— 1,2-Dichloroethane________ I 578-93-3 ————— —— 2-Butanone_________________I lu71-55-6 —— — ———1,1,1-Trich loroethane______1556-23-5 — --- — --Carbon Tet rachior ide_______15108-U5-4——————"Jinyl Acetate_______^_____I 1075-27-4———— ——— Bromod ich Iorome thane_______1579-87-5————————1,2-Dichloropropane____ 1510061-01-5——— — ci»-l,3-Dichloropropene____(579-01-6 ———————— Tr ich loroe thene____________15124-48-1---————Oibromoch Iorome thane______l 579-00-5 ———————1,1,2-Tr ich loroethane______i571-43-2 ——————— Benzene__________________1510061-02-6--————t ran*-1,3-0ich loropropene__1575-25-2 ———————— Bromoform__________________I 5108-10-1 ———— - — 4-Methyl-2-Pentenone_______I 10591-78-6 — -- ——— 2-Mexanone_______________I 10127-18-4- ———— -- fetrachloroethene_________I 579-34-5-----——-1,1,2,2-Tetrachloroethane__i5108-88-3 —————— Toluene__________________(510b-90-7————--Ch lorobenzene_____________15100-41-4——————Ethylbenzene_____________I 510U-42-5 ———— - — Styrene__________________ I 51330-20-7—————Xylene t tote I)___________I 5

FUKM I VUH

L9

VOA X

•a»p aou :»in%fTQH I

IE.E ORGAN ICS HNALYSIS DATA SritET

TENTATIVELY lOtNTIFIEU COMPOUNDS

EKH S* NU

Lab Name:£TC Corp. . I Laboratory

Lab Code : Case No . :

Matrix: (. so i 1 /water ) UJA I tR

Sample wt/vol: 5.0

Level: '. low-'med) LUU


Column: f.pack/capj

Number flCs found:

Cont ract :

SttS No . :

ML

No.:

Lab sample iQ: uC.7iJ-t*i5|j_

Lab F i l e ID: >Ui'6U6

Uate Keceived: (/ m/f/

Date Analyzed: Oi--'14. * i

D i l u t i o n hactor: l..

ON UNITS:or ug/KgJ

1CMS HUnBER COMPOUND NflME

•

FURM I UQA-TIC

RF ES I . CUNC

i 37

68

Q

i

i

i

i

t

i

rev.

UftGANICS HNftLYblS DttTH SMtETEt-tt SHMPLt Nl

Lab Name: ETC Corp.

Lab Code: Case No.:

Matrix: (soil/water) UHTER

Sample wt/voi: 5,U tg/mLJ ML

Level: ', low/mad) LOW

H Moisture: not dec.

Column: tpack/cap) P«CK

Contract:

No.: Sub No.:

Lab Sample iD: UC70-*45u.

Lab Fiie ID: >0*62l

Date

Date Hna lyred : 01 •'15'"

D i 1 u t ion hac tor:

C«S NO. LunPQUNDCUNCfcNTRpriON UNITS:tug/L or ug/Kgj uu^

74-87-3 — —— ——— Chloromethane_____________I iO74-8^-9———— —— -Bromomethana ___________| iQ75-01-4———————Uinyl Chloride,^__________11U75-00-3———————Chloro*thane_____________I iO79-09-2 ——————— nathylena Chloride________I 567-64-1———————rtcetone__________________11075-15-0———————Carbon Oi»ulf id*_________1575-35-4———————1,1-OichJo roe than*________I 575-34-3———————1,1-Dichloroethan*________15540-59-0——————1,2-01 ch lore then* (total)__1567-66-3———————Chloroform_______________15107-06-2 —————— 1,2-0 ichloro* than*________1578-93-3 ——————— 2-Sutanon*_______________I 1071-55-6———————1,1,1-Tr ichloro* thane______I 556-23-5———————Carbon Tetrachloride^_____15108-05-4——————Yinyl Hcatata_______;_____r 1075-27-4————---8romodichlorom*than«_______1578-87-5—————---1.2-Dichloropropan* ____1510061-01-5————CJ»-l,3-Oiehloropropen*____1579-01-6———————Tr ichloro* then*___________15124-48-1———"--DibromQCh lQrofn«th«n« 1579-00-5———————1,1,2-Tr ichloro* than*______1571-43-2———————B*nz*n*__________________151U 061-02-6————tran*-l,3-0ichioroprop*n*__t575-25-2———————Bromoform________________15108-10-1——————4-n*tnyl-2-P«nt*none_______I 10591-78-6——————2-M*x«non*_______________110127-18-4——————T*tr*chloro*th*n*_________ I 579-34-5 ——————— l,l,2,2-r*tr*chloro*than*__15108-88-3 —————— Toluene__________________11106-9U-7——————Ch I ore-benzene_____________I 5100-41-4——————Ethylbenzene_____________15100-42-5——————Styrene__________________I .8001330-20-7—————Xyiene Uot*l)___________15. ___________________________________I___

iUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIJIUIUuIUI_

FURfl 1 r-;e v.

VQ&ATZLX ANJU.YSI4 DATA flXIT »* SAK9U HC.

Uft KAMIU» cadai

Matrix: (aail/vatan fcUAray.Saapla wt/vei;Laval:

% Moitturat not daeColumn: (paeJe/eapj

fUa 10;

Oata ftacaivad:

dilution Faetar:COXCZHTXATZON OHITS;(«»/t Or Uf/K€] Mfl/L

i Tatrahydrofuran

row z VGA 1/17 JUv

70

ItE GRGftNlCS HNftLYSIS DttTft SMtET

TENTATIVELY lOtNTIFIEO COMPOUNDS

NO


Lab Code: Case No.:

Matrix: '.soil/water) UHTER

Sample wt/vol: 5.0 tg/mLJ ML

Level: (. low/med) LOW


Column: '.pack/cap) PRLK

Number TICs found: Q

Cont ract:

No.: SUb NO.:

Lab bamp le ID: :4C7u-»45u;

Lab Fi le Iu: >U^62l

Uate Keceived: i / iffl/

Date Hna lyzed: Oi-'15' v i

Dilution ractor: l.

CUNCtNTRHriON UNITS:tug/L or ug'-'Kgj UG/L

CMS NUMBER CUHPOUNO NHHE

.

FUKfl I'UQA-TIC

Rl ESI. CUNC

1 87

71

Q

- a v .

8AVOLATILE INTERNAL STANDARD AREA SUMMARY

Lab Name: ETCNJ - Contract:

Lab Code: Case No.: SAS Ho.: 3DG No,:

Lab File ID (Standard): >C2184 Data Analyzed: 01x18/91

Instrument ID: GC/MS C Time Analyzed: 1043

Mat r ix : '. so i 1/water ; WATER Level : ( low/mod ) LOW Co lumn: (pack/cap ) a*</

0102030405060708091.0111213141516171819202122

12 HOUR STD

UPPER LIMIT

LOWER LIMIT

EPA SAMPLENO.

"JBLK02A5805A5599A5806A5591A5805A5806A5591

IS1CBCM)AREA #

61891

123782

30946

4745356629572005349753475516315565156077

ST

10.38

10.4710.4910.3910.4110.3910.4310.4010.38

IS2CDFB)AREA #

270337

540674

135168

208802246388247875231118224989229838239082237252

RT

21.09

21.1321.1521.1221.1121.0921.0921.0621.08

IS3CCBZ?rtREA ft

163017

326034

81508

121129198269204889173798191521188846196316191053

tRT '

25.971

1

1

11

25.98126.01125.97125.95 125.97125.94125.94125.931

11tIt1111i1111

151 CBCtlJ - Bromochloromethane152 (DFB> - 1,4-Oifluorobenzene153 CCB2) - Chlorobenzene-d5

UPPER LIMIT - * 10QSof internal standard areaLOWER LIMIT - - 5QHof internal standard area

# Column used to flag internal standard area values with an asterisk

of

FORM UIII UOA l/97'2Rc1-'

3-UOLATILE INTERNAL STANDARD -*E* SUMMARY

_sb Name: ETCNJ Contract:

_ab Cad«s Case Mo.: SAS 'io.: 30G 'o

Lab F i l e [0 'Srandard: -C21S4 Oa * a Analyze-:

Instrument ID: GC-'MS C Time .-nal;, zed:

["•5 : r i x : ' sc : l-xwat ar ; LJATEP Lave 1 ; ' lowXmed ' LOW Co lumn : > pack

.04?

01020304050607030910111213141516171319:o2122

12 HOUR STD

UPPER LIMIT

LQUER LIMIT

EPA SAMPLENO.

i s i < scr- .<

ol391

123732

30946

4745753493

-r10.33

10.4710.45

IS2'.DFB- ! !S7fCBI- i

?4067-U 7260741

1751631 ' 31508!

! i: . i

208802 1 21.13 121129 1 25.93228455 i 21.. 01 134272 ! 26. -:1?

1 1I i1 I i! 11 11 i ;I i ii i! 1 1

"1 !1 1 !1 !1 i !! ! i1 ! .1 1I ii ; ii ii i

JS1 fBCM i • Bromochlorome thaneIS2 'DFB) • 1 ,4-Di f luorobenzer.eIS7 tCBZ'J • Ch lorobenzene-d?

UPPER LIMIT - - 10OSof i n t e r n a l standard ar-saLOWER LIMIT » - 5OSof i n t e r n a l standard ar*a

# Column used *. o flag internal standard area -.'a lues w i t h an

page __ of __

FORM U I I I VOA


Lab Name: ETCNJ • Contract:

Lab Code: Case No.: SAS No.: 3DG No.:

Lab File ID (Standard): >C2199 Data Analyzed: 01/19-91


Matrix:(so i I/water) LJATER Le-^e 1 : C low/med ) LDU Co lumn : (pack-'cap j £>/+

01020304050607080910111213141516171919202122

12 HOUR STD

UPPER LIMIT

LOUER LIMIT

EPA SAMPLENO.

VBLK03A5599MSA5599MSD

IS1CBCM)AREA ^

54089

108178

27044

425655013152788

'

RT

10.45

10.4310.4710.42

1 32 C DFB )AREA ft

222969

445938

111484

182628218075220332

RT

21.08

21.0921.1521.11

IS3CCB2)AREA ft

173290

346580

86645

133122148069122464

ST

25 . 92

25.9326.0025.96

131 CBD1) • Bromochloromethane152 (DFB) • 1,4-Difluorobenzene153 CCBZ) - Chlorobenzene-d5

UPPER LIMIT - + 100Sof interne 1 standard area.LOUIER LIMIT - - 50*of internal standard area.

ft Column used to flag internal standard area values with an asterisk,

page 1 of \

FORM W i l l YOA 1/8? £e

E lNlb.RN«l_ S

Lab N«meI ETC Corp. Contract:

Lab Coda: Case No.: Sttb No.: SUu No.:

Lab File 10 ^Standard): >D2*b7 uata Hneiyzaa: 01-;

Instrument 10: GC/P1S 0 Time Analyzed: 171?/

Hat r ix: 110 i 1 /water ) WH i tR Leva 1: I low/med > LUU) Column: tpack/cap J

11

1 12 HQUH STO

1 UPHER LiniT

1 LOWER LIMIT

I £KH SAMPLE1 NO.

01 IU6LKU102lf t957703 IW(?'?8504t f t558605 IW958706i«5'?9607IH557108 IA558309 IA558410I«558911IH559312113114115116117 Tia i1912 0 12112*1

iSltBLPIJMKtH *

56050

112100

28U25

7535373*267>4947426372B1775*43706025V277596477117159874

Rl

11.40

11. >811.4011. ^911.7611. J911.3911.3011.3011.3111.3011.39

i 'a'i I Uh 6 JAKtrt *

3^170'^

6A3404

16Uti^i

32'-* 3 73*729>314^673^33663UB333^d05t>3027973136913127243iiaey316452

•

RT

2-.10

22.1^2^. 1022. US'2-J.0222. U922.0922. U422 . 0422. ui22.0022.05

lS3tLb^JftRcrt f

263014

5^602a

I^i5u/

27U>682**l4y'^666662e'y?41*J 6 4^/22/6961?25580726792V2695^126*808273343

I

Ri I

2/. uu i

i

i

1

_ / . U 2 .2 , ' . Q 1 'J6.992 6 . 9 2 1*6 .992 / . 0 3 i^6 . ya2o . 9<n-;o . v8 •2 6 . 9 4 1*6.95 .

I

1

IiI

1

i

LSI (.bCM) - Bromoch toromathane UPr-tR LiniT - * iuuH152 (DrB) • 114-0ifluorobenzena of internal standard area.153 tLSZ? - Chlorobanzane-d5 LOWER LiniT - - 5uH

of internal standard area.

* Column used to flag internal standard area values with an asterisk,

page i_ of

FQR(1 I I 1/87 Re-

75

8ALE INTERNAL STHNDHRD ftfttA SUPlflftKY


Lab Cod*: Case No.: SHb No.: SUb No.:

Lab File ID ^Standard;: >D26U4 L'ata Analyzed: 01-i4/y.

Instrument ID: GC/MS 0 Time Analyzed: lU^l

Mat r ix: t so i l/w«ttfr ) WM I tR Level:I low/med ) LUW Co lumn: '.pack/.rap ; PACK-

11

1 12 HUUK STiJ

1 UP^ER LIMIT

1 LOWER LIMIT

1 EPft SrtMPLE1 NO.

01 IIJBLKU202m$5?803IH557904m5590Q5I«556806m5592071Qdl09 t1011111211311411511611711811912GI211221

ISltSCMJAKtR *

78U44

l56l)bU

39022

789617487477870610814938163078

R[

11.41

11.3611.3411.3611. 4011.4111.42

I S2 t Uh 8 HKtrt *

33731:,:

6/4624

16U696

348767333550343684341741256192341147

a

R;

22.11

22. 1U22.0422. 1022.1022.1122. Q8

I =3 '. LB^ JflKirt #

2 '"7 4^0

^-y'janu

13/71U

29401823699*2*61/12*J86B226U352*3282

R

* • . U 1

2 / . 0 0 i26.982/. UO i2/.00J / . 0 I2,'. 01

IiI,

i1iI

i

151 ttiCM) « Bromochloromethane152 lOr'B) - 1,4-Dif luorobenzene133 lUUZ) - ChLorob*nzene-d5

UPPER LIMIT " * 1UUXof internal standard area.LOWER LIMIT - - <?UHof internal standard area.

# Column used to flag internal standard area values with an asterisk.

page _\_ of _i_

FORM UII I YQft 1^67 *e

76

aftYOLftTlLE INTERNAL ST«ND«RO ARtrt SUPIM«ftY


Lab Coda: Case No.: SttS No.: Suii No.:

Lab File [0 (Standard): >D2620 Uata Analyzed: 'Jl-:5/y.

Instrumant ID: GC/MS 0 Time ttnalyzed: 14<;3

Hat r ix : tso i I/water ) Wtt I b!R Leva I : '. low/mad ) LOW Column: tpaek/cap J

111 12 HOUR STD

1 UPPER LI HIT

( LOWER LIMIT

1 EPfl SrtMPLE1 NO.

01 IUBLKU302IW557703IHS57204IH5572MS05lW5572nSOQ6lft5568«e07m^'?aaQ8lA9<792Ae09 t101111121131141151161171181191201211221

isuacmAKtft *

5yi^6118312

2**?e

8U5565960157>Q5669447U226674558296765526

R1

11.39

11.35ii.3811. >a11. 4U11.3911.3911.3711.39

IS210K8JAKtW *

331306

662612

16'?653

347-919341715309*85376441414303767446370337359706

"

Rl

22.02

22. US22.0422. U 522.0722. U522.0522.072*. 09

lS3CLbiJHKC.H *

2 /a ll1?

5-7623U

139057

3021512*27082 789 2 U3i407tt344U883109233186JO316706

R 1

2o . >"? i

1

1

1i

26 . 98 126.941^6.94i27.001*6 . 98 I26 . 98 i

It 6. 96 i2 0 - 9 9 i

1

Ii1iI,1;1i1

151 igCtt) " Bromochlorom«thana152 (Dr'8) « 1,4-Dif luorobanzena153 tC82) • Chlorobenzene-d5

UPPER LIMIT - + 1UUHof internal standard area.LOWER LIMIT - - 5u*of internal standard area.


page i_ of _|_

FORM "JIM UOft 1/87 Re

77

ETC

TABULATED RESULTS

PARAMETERS

78

M^f M. \s —FEB 5. 1991

TABLE 1: QUANTITATIVE RESULTS and QUALITY ASSURANCE DATA

NPDESNumber

ChlorideFluoride

»»jvO

Conventional Analysis Data (QR1O)

Chain of Custody Oat* Required for ETC Data Management Summary Reports

CA5568 WASTE MANAGEMENT, INC. 405 W3GWPZ6 910108 1120 0Elap*«d

ETC Sample No. Company Facility SJ*PJ* Point Out Tim* Hours

Retultt

SampleConcen.

«g/i139.9

.2

HDLmg/1

1 .0.10

•

ETCJAN 30. 1991

TABLE 1: MISCELLANEOUS DATA (QR64)

:IHMHMfilfe: mtm•a/ISulfate as S04Total Dissolved SolidsBicarbonate as CaC03Carbonate as CaC03

(TDS13

960651

2101010

OOO

———— _L>.f ^ ———————————————————— ——— ———— " —— — ———————————————————————————————————————— —


Field Parameters (QR16)

Chain of Custody Data Required for ETC Data Management Summary Reports

CA5568 WASTE MANAGEMENT, INC. 405 W3QWPZ6 9101081120 0EJip.-d

CTC 8«Mplt No, Company Facility Sampl* Point 0*(* HIM Hour*

Parameter

pH (Field) stdpH iField stdpH i Field stdpH Field stdSpecific Conductance Field urn/ cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmTemperature Deg. CRedox Potential mvRedox Potential mvRedox Potential mvRedox Potential mv

oo

Results

SampleMeasure

7.397.337.327.34

1282129812871291

10.9- 74- 79- 83- 82

i

HDL

-

JAN 15, 1991

•

——— i^ J Vx ————————————————————————————————————————————————————— — ————————————————————




CA5584 WASTE HftfttGEMECT. INC. 405 W3GUPZ8 910108 1251 0ETC Sample No, Company Facility S«pl« Point Dat* Tint Hours

NPDESNumber

ChlorideFluoride

i

CONJ

Remit*

Conceit,

11.8

MOL

1.0.10

FEB 5. 1991

1

r— ETCJAN 30. 1W1

TABLE 1: MISCELLANEOUS DATA (OR64)

Clwrn "of Cwtooy D»ti «•«*«) for ETC D*u M*n*own«m Summary Repof t*

t INC. 40S W3QUPZ8 > »IOIO» 1251 0CA5S84 WASTE

Sulfate as S04Total Dissolved Solids (TDSBicarbonate as CaC03Carbonate as CaC03

CD

28410340

2101010

ETCJAN IS. 1991




CAS584 WASTE MANAGEMENT. INC. 405 W3QWPZ8 910108 125 1 0EJap»*d

CTC Sample No, Company Facility Samplt Point Oat* lima Hour*

Parameter

pH (Field) stdpH 1 Field stdpH i Field stdpH I Field stdSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmTemperature Deg. CRedox Potential mvRedox Potential mvRedox Potential mvRedox Potential mv

00

Results

SampleHeaiure

7.497.397.417.37

717727727678

9.8+ 50* 43+ 32+ 36

M>L

-

•

ETCTABLE 1: QUANTITATIVE RESULTS and QUALITY ASSURANCE DATA

Conventional Analysis Data (QR10)

FEB 5. 1991

Chain of Custody D*t» Required for ETC Data Management Summary Report*

CA5588 WASTE MWWQEMENT. INC. 405 W3GWPZ11I 9101070929 0CTC S«npl« No. Compioy Facilily S«tpl* Point 0»lm Tim Aour*

NPOESNumber

ChlorideFluoride

COen

Remit*

SampleConceit,

•0/1

135.8.2

HPL•9/1

1.0.10

•

___ M^± Vx —————————


• • ' • . x::. :.ChaM>tf.<piiiJft p*tof!l ^ -• ^ " ••wBsi! ^^ '/v:y:; •' W3QUPZHI - 91010? OSM • o

'••••^^^••••••••^"''•-.'..-•••^•.-••••••^ " • " • • • • • : • : / . • : • • • • • • • : : • • • • • • . / • . . • • • • , . • . . , . • . . . " . : • . • , , . . • . . . - ; . ..-•- ' ' - • • ' • " : /•':•": • . ej*p«*<iETC Swplc ^^^•{/•••''•/•,.-^-tSmfuiif/:\ '•": '•••'::..'"'^ :.•.•:.'•• '. Facility::;.' -^ imp)* t*i*\ _ D*t« ..-. . .!•*»•:. *Hir*

• • ' ' • • . Compound .•.•^•••^^^m-^

Sulfate as S04Total Dissolved Solids (IDSBicarbonate as CaC03Carbonate as CaC03

COON

^k^ lltlllli1: /..:"1'

S«*pl«• pg l ;

101260802<10

i

.a '-MPt -------: :*»mr2

101010

JAN 30. 1991

'• "•"• -- r 'J :"" '" '. i ': i ' i:: ::- i : ::'7:':'".^ -v: ;:;•:/:•



Chain of Custody Data Required for ETC Data Man*9ement Summary Reports

CA5588 WASTE MANAGEMENT, INC. 405 W3GWPZ11I 910107 0929 0ETC S«mpl« No. Compifty Fjciiity S«npl« Point D*tt TIM Hours

Parameter

pH (FieldpH i FieldpH I Field ipH I Field!Specific Conduct anSpecific ConductanSpecific ConductanSpecific ConductanTemperatureRedox PotentialRedox PotentialRedox PotentialRedox Potential

oo

stdstdstdstd

ce Field urn/cmce Field urn/cmce Field urn/cmce Field urn/cm

Deg. Cmvmvmvmv

Results

SampleMeasure

7.227.287.277.26

1536150714121398

5.8- 73- 73- 82- 89

•

~

-

JAN 15. 1991

•

———— A>^ V^ ——————————FEB 5, 1991



Chain of Custody Data Required for ETC Data Manajement Summary Reports

CA5589 WASTE WWAGEMEMT, INC, 405 W3QWPZ5 9101080911 0EJ •{**«<)

ETC 3*npJ« Me, Comptny facility Samplt Point fiat* Timt Hour*

NPDESNumbtr

ChlorideFluoride

COCO

Result*

SaopleConetn,

8 9

MDL•9/1

1.0.10

•

•


•-•-;:•;• -^ •-••: ^-^GtoiR «f Cuttotfy Dim BayiradfoV ETC Data Managtmtrrt 5um«ary n»pof t» ^:.x/ %j? v••:-' 58«^>tt(ife«»li(6^^

:-;:ftIMl v: :;; -i

'W^^H:9X^^S^^^S^^^^^^SulfaU ai S04Total Dissolved Solids (TDSBicarbonata as CaC03Carbonate as CaC03

CONO

^uiay P

23420330

Illllllsw^101010

SSsffiSsS^si-

:S SlS5ssi:

SSSiS^^SfflS; 'Zjj§j£$gl§^- Wi&iM

«*,.--PI •.;/••

JAN 30. 1991

WSiiiiiiii.mmmmm

^sffi

—— i>-I \^ ——————————————————————————————————————————————————JAN IS. 1991


Field Parameters (OR 16)

Chain of Custody Data Required for ETC Data Management Summary Report*

CA5S89 WASTE MANAGEMENT. INC. 405 W3GWPZ5 910108 0911 0El«f>**d

ETC SMipli Ho. C«w«>y facility S*nple Point 0*t* Ti*» Hour*

Parameter

pH Field stdpH i Field stdpH 'Field stdpH 'Field stdSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmTemperature Deg CRedox Potential mv

O

ftatulu

SampleHeasure

7.437.337.297.30

934925928917

8.5* 264

HDL

-

•

———— M^/M. V/ ———————————————————— " ————— ———————————————————————————————————————————————————————— "' ———————————————— - —— -FEB 5. 1991



Chain of Cu»tody Data Required for ETC Data Management Summary Reports

CA5590 WASTE MWW3EMENT. INC. 405 X3GWFB 9101080952 0CJ«p*«4

CTC S«nplt ND, Compiny Facility S«iplt Point 0*t« Tim Hours

NPDESNumber

ChlorideFluoride

VO

fUtaltl

Conctn,•tf/1

<.10

i

Sh1.0

.10

•

'

JAN 30. 1991TABLE 1: MISCELLANEOUS DATA (QR64)

Chittn of CMKotfy D»tt f!Kiqu>r«<l for CTC CHU MannMiiMiH •Minim y; Baporti

^

CompoundIKmm

Sulfata as S04Total Dissolved Solids (TDSBicarbonate as CaC03Carbonate as CaC03

to

<221 10

1010

——— 4^^ V —————————FEB 5. 1991




CA559V WASTE MANAGEMENT, INC. 405 W3GUPZ11D 9101081037 0ETC 3«Mp)t No. CMp«ny F»cility S«*pl« Point D*t* Ti*t Hours

NPDESNunbar

ChlorideFluoride

ft«<iUU

S&mpl*Coflctn,

6.2.1

MDl

1.0.10

•

JAN 30. 1991TABLE 1: MISCELLANEOUS DATA (QR64)

•.•:;.•;: '"-v ".•:•::•''•'•'• "''-•-•-•.:-.- ~:- - -'•':-•-::. --.-. -^tmiaM •tmaawtowt :.:.--:"D«u.: •. >vTu*:;::**KSr:

Concfh.

Sulfata as S04Total Dissolved Solids (IDSBicarbonate as CaC03Carbonate as CaC03

20196130

2101010

A ^ ———————————————————————————— . ——————————————————————



Chain of Cuttody Data Required for ETC Data Management Summary Report*

CA5591 WASTE MANAGEMENT. INC. 405 W3QWPZHD 910108 1037 0CTC SMDli Mo, CMMpmx Facility S«npl« Point 0*t« Time Hours

Parameter

pH Field stdpH Field stdpH Field stdpH Field stdSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmTemperature Deg. CRedox Potential mv

cn

RfttulU

Sawpl*Measure

11.4011.4111.3911.41

623629597578

4.5+ 66

MDL

•

JAN 16. 1991

M^fJ. \-sFEB 5. 1991




CA5592 WASTE HMWGEMENT, INC. 405 W3GUPZUS 9101080850 0ETC Sample No, (tawny Facility Swiple Point 0*le Time Hours

NPDESNumber

ChlorideFluoride

voON

Retulit

SampleConcen,

47 8.1

rC-Lnfl/1

1 .0.10

—— 4>Jt *^ ——————

Compoun


Chain of CufttwfX Data n«q

tie tMipi«.N»v;: l :|,i;;iSiitX::^

u*red for ETC D«i« Manaflemwrt Summa

>•'•• L' "-•-. .•" 40S ••' ••'••'••:':-:-:;.^,-M3aiPZIlS

/,f«m« ;0^ ;i*.|ri¥ i

ry Report* ;

910109 0850 0nt &•!• TlM Hour ft

d -,V..A..^:^;

Sulfate as S04Total Dissolved Solids (IDSBicarbonate as CaCOSCarbonate as CaC03

:;^: •:::;;. * |f::; /'::

•$sj**"*to

738516

i

SS^%;: fff/i v^;

2101010

JAN 30, 1991

" . ' " . . . . ' . ' • • • * " • • ' -y- •''•••' >..•' ' - -

—— M_ff A ^ —————————————————————————————————————— __ ———————————————————————————JAN 15. 1991




CA5592 WASTE MANAGEMENT. INC. 405 W3GWPZHS 910108 0850 0Eltpsed

ETC 8«npl« No. Company Facility S*npl« Point Date Time Hours

Parameter

pH Field stdpH Field stdpH Field stdpH Field stdSpecif ic Conductance Field urn/cmSpecif ic Conductance Field urn/cmSpeci f ic Conductance Field urn/ cmSpecif ic Conductance Field urn/ cmTemperature Deg . CRedox Potential mv

CO

Resul ts

SampleMeasure

7 026 976 956 94

1042106110621061

6 8- 28

MDL

-

M*/ A \-^ • ' • ' ' - -




CA5593 WASTE MANAGEMENT. INC. 405 X3GHFB 910108 0930 0'ETC Sample No. Company Facility S«npl« Point Date Time Hours

NPDESNumbs r

Chloride iFluoride

i

\oVO

lUtultt

SanpleCoiicen,

«9/l<1.0

< .10

;

W>LB0/1

1.0.10

•

— ,

FEB 5. 1991

•

——— M*tA Vx —————————


Chain of Custody D*t* Required for ETC Data Management Summary Report*

CA5593 WASTE MANAGEMENT, INC. 405 X3OWFB 9101080930 0

ETC Sample HP. Company : Facility Xjvpla Point D*l« Tim» Hours

Compound


OO

RfltUlU

SampleCoflctn,

•0/1

<220

^2

101010

JAN 30. 1991

1 '". ' . -• • .

——— j^ j V ————————————————————————————————————————————————————————————————————————— ' ' "




CA5597 WASTE MANAGEMENT. INC. 405 W3GWPZ It IDU 910107 0929 0€TC 3«nplc No. Company Facility Sample Point Date Tim; Hour*

NPOESNumber

ChlorideFluoride

CD

fUtults

SampleConcen,

ng/1

134 5.2

MDLmfl/1

1 .0.10

FEB 5. 1991

•

Coppoun


•• • Chain of Cwrtody D«t» B«p*W *w ETC

CA559* w^ WMttflBiBff;; lie .; ;-;;-;Pat*'M*fM9i

**** •.>-;;.;.;;;;;;:•'

ment Summary Report* • - v- ' • ; - . ' • •

waawpzniETC t-l^^^^^^VB^^r; •"••;' - ^;^^:^vv-fKilI^:^^^fN»?»-*tt

DU 910107 0929 0

At fiit* T1*B *>urs

1- Y;:?:: ^


O

::i **£

101420805

2101010

JAN 30. 1991

- -:,:::, '

i-/ M. \~s —————JAN 15, 1991




CA5597 WASTE MANAGEMENT. INC. 40S W3GWPZ11IDU 910107 0929 0Elap»«d

ETC Sample No. Company Facility Sample Point Dale Time Hoiirs

Parameter

pH FieldpH FieldpH FieldpH FieldSpecific ConductanSpecific ConductanSpecific ConductanSpecif ic ConductanTemperatureRedox PotentialRedox PotentialRedox PotentialRedox Potential

CDOJ

stdstdstdstd

ce Field urn/cmce Field urn/cmce Field urn/cmce Field urn/cm

Deg Cmvmvmvmv

Reiultt

SampleMeasure

7 227 287 277.26

1536150714121398

5 8- 73- 73- 82- 89

MPL

-

———— J_> M. \^ ——————————FEB S. 1991




CA5599 WASTE MANAGEMENT. INC. 405 W3GWPZ50UP 910108091! 0El •pica

CTC Sample No. Compjny Facility 8«npl« Point D»i» HIM Hours

NPDESNumber

ChlorideFluoride

CD

Rciultt

SampleConctn,

•9/1

9.5.1

MDL

1.0.10

J-> J Vs


Cnatn of Custojfity Data Ftequire4 for ETC Data Management Summary Reports

CA5599 WASTE NMM3B4EMT; INC. ^tTC Swpla H»i>-~ -•.-.".,-.-.•:•: :•' . • • • • • " • - . . /.•.Caapiay---::-:-:------ . .•.. . • • - • - • • ::.. . ' '

(05 W3GWPZ5DUP 910108 0911 D

: '.-; :;: "i Compound : --'..- :V


Otn

•^•y. ::Jt«ttltlv:--: -

CPOCflU,•fl/123

429336

^*Sh2

101010

JAN 30. 1991

• - •'• ;:: ' '.-:''•' -

flM

—— 1_>M. *^ ———————————————————————————————————————————————————————————————————————————



Chain of Custody Data Required tor CTC Data Management Summary Reports

CA5599 WASTE MANAGEMENT. INC. 405 W3GWPZ5DUP 910108 0911 0

ETC Sample Ho. Company Facility S*npl« Point Ddle Time Hours

Parameter

pH <Field stdpH Field stdpH Field stdpH Field stdSpecific Conductance Field urn/cmSpecif ic Conductance Field urn/ cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmTemperature Deg. CRedox Potential mv

CDO\

Result s

SampleMeasure

7.437.337.297.30

934925928917

8.5+ 264

MDl

-

JAN IS. 1991

OHM Corporation

Environmental Testingand Certification Corp.

Summary Package

for


Ch*in of Cuttoay D»t* A»quir»<f for ETC Data Management Summary ftvporft

WASTE MANAGEMENT, INC. 405

FacWty

CAS571-CA5572.CA5575-CA55B3,CA5585-CAS58 7,CA5S94-CA5596

Company f/aptedSamp/* Point Oaf* Tim9 Hours

Richard P. AlbertVice Prts/tftnf, Genera/ Mantg«r

Thu TtChnie*! Report is «n IN5ITE Mrvic* g«rwrat«d bx LOOESTRR tou n«n»9im«nt Softwar*.

-284 RariUn Center Parkway CN7808 Edison, New Jersey 08818-7808 201-225.5600.

ETCSDG NARRATIVE

This technical report submitted by ETC Corporation contains theanalytical results and required deliverables for WASTE MANAGEMENT,INC. Site 405 samples as identified below:

CA5571CA5572CA5575CA5576CA5577CA5578CA5579CA5580CA5581CA5582

CLIENT ID3GWB18RR3GWB7RR3GWP1A3GW616RR3GWP5A3GWP8A3GWB7RR3GWP1B3GWPZ153GWPZ14

EC£_ID_CA5583CA5585CA5586CA5587CA5594CA5595CA5596CA5602CA5603

CLIENT ID3GWFB3GWPZ183GWPZ21S3GWPZ103GWPZ18DUP3GWPZ103GWPZ902TB02TB


fOV7Q442. OV7Q443 and OV70445^I

Problems were not observed during the analysis of these samples.


-;/-<?/Gregofc^G. MorrisonLaboratory Manager

Date

Fll* * OOO452

1AVOLATILE ORGAN ICS ANALYSIS DATA SM£ET

Lab Name: ETC Corp.

Lab Code: Case No.:


Sample wt/voi: 1.0 Ig/mD ML

Level: Uow/med) LUtJ

S flo isture: not dec.


Cont ract

SAS No.

EPA SAMPLE NO

IA5571I

! SDb No.:

Lab Sample ID:

Lab File ID: >D2597

Date Received:

CAS NO. COMPOUND


Di 1 u t ion Fac tor:

CONCENTRATION UNITS:Cug/L or ug/Kg) UG/L ui

74-87-3 —— ———— -Ch lorome thane_____________15074-83-9————————Bromome thane_______________15075-01-4————————Oinyl Chloride_____________I 1275-00-3———————Ch I o roe thane______________l 5075-09-2 ———————— Methyl one Chloride_________12567-64-1 ——————— Acetone__________________t 1275-15-0 ———————— Carbon Disulf ide___________12575-35-4————— —— 1,1-Dich loroethene_________12575-34-3 ————— — -1,1-Dichloroe thane________I 8540-59-0 ———— — -1,2-Dichlorethene t total )__I 1167-66-3 ——————— Chloroform_______________125107-06-2 —————— 1,2-Dichloroe thane________I 2578-93-3 —— - ——— -2-Butanone_________________15071-55-6————————1,1,1-Tr ich I o roe thane______12556-23-5 — - —— —— Carbon Te t rach lor ide_______125108-05-4———————Oinyl Acetate______________15075-27-4---------Bromod ich lorome thane_______I 2578-87-5————————1,2-Dich loropropane________12510061-01-5 ————— cis-l,3-Dichloropropene____12579-01-6 —— ————— Tr ich loroethene____________I 25124-48-1 — ————— Dibromoch lorome thane_______12579-00-5————————1,1,2-Tnch lo roe thane______12571-43-2 ———————— Benzene____________________12510061-02-6—————tran»-l,3-Dich loropropene__I 2575-25-2- ——————— Bromoform__________________125108-10-1 ——————— 4-Methyl-2-Pentanone_______IVO591-78-6- — -- — -2-Hexanone_________________150127-18-4--- — — -Tet rach loroethene__________12579-34-5 — -------1,1,2,2-Tetrachloroe thane__1251 OB-88-3 ——————— Toluene____________________196108-90-7———————Chlorobenzene______________125100-41-4———————Ethyl benzene_______________12UO100-42-5 ——————— Styrene____________________1251330-20-7——————Xylene t total )____________Ii50

IIUIUIJIUIUIJIUIUIJIJIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIIU

FURM I 1/87

IAVOXATZIX OMAIKCS AJCAtYflXJ DATA IttTT X9A SAKVIX NO.

tab Naao:Ub Codos Caao Mo.:Matrix: ftoil/vator) 6J»TEe.Stvplt vt/vol: I fg/mLl m^

l«v«l: (lov/B«d) 03u

t Moisturo: not doe.Coluan: (p»ck/eip)

Contract:SAS NO.:

AST? i

CAS NO. COMPOUND

Totrahydrofuran

tDO NO.:

faapla ID:Ub mo 10:Dato Jtoeaivod:Data Analysed:'.Dilution Factor:

coNcomurzoN UNITS(ug/t or uo/Koi

lloo

s/q

raoi i VOA 1/17 Mv,


TENTATIUELY IDENTIFIED COMPOUNDS

EPtt SAMPLE NO.

1A5571Lab Name:ETC Corp. I Laboratory

Lab Code: Case No.:

Matrix: laoi1/water) WATER

Sample wt/vol: 1.0 Ig/mLJ ML

Level : ( low/mod) LULd




Cont rac t:

SAS No,: SD£ No.:

Lab Sample 10:

Lab File ID: >D2597

Date Received: I/S/4I

Date Analyzed: Ol'l4/9l

Di l u t i o n Factor: 5 .

CONCENTRATION UNITS:tug/L or ug''Kg) UG/L

CAS NUMBER COMPOUND NAME RT EST. CONC

FORM I OQA-TIC 1/87

VOLATILE ORGANICS ANALYSIS DATA SHEETERA SAMPLE NO

IIA5572

Lab Name: ETC Corp. Contract: I___


Matrix: tsoiI/water) WATER Lab Sample ID:

Sample wt/vol: 5.0 tg/mLJ ML Lab File ID: >D^624

Level: Uow/med) LOU Date Ke-ceived: \kfa\


Column: '.pack/cap) PACK

CAS NO. COMPOUND

Date Analyzed: O


CONCENTRATION UNITS:tug/L or ug/Kg) Ub-'L

74-87-3 —— — - — -Ch lorome thane______________I 1074-83-9 — — — - — Bromome thane______________11075-01-4————————Winyl Chloride_____________) 1075-00-3 ———————— Chloroethane_______________I 1475-09-2- — — —— -Methylene Chlor ide_________I 1667-64-1 — - — — --Acetone____________________I 1075-15-0 —— — — --Carbon Disulf ide__________1575-35-4-- — — ——1,1-D i chio roe thene_________1575-34-3 ———— — —1,1-Dich 1 oroethane_________I 7540-59-0 —— —— —1,2-Dichlorethene (total )__1567-66-3 — — --- — Chloroform_________________15107-06-2 —— — —— 1,2-Dichloroe thane_________1578-93-3 — ———— — 2-Butanone_________________I 1071-55-6- ———— — -1,1,1-Tr ichloroethane______1556-23-5 — —— ——— Carbon Tetrachlor ide_______15108-05-4——————"Jmyl Acetate_____________I 1075-27-4---------Bromodich lorome thane_______I 578-87-5———————1,2-Dichloropropane_______*510U61-01-5 —— —— cis-l,3-Dich loropropene____I 579-01-6————————Trich lo roe thane____________15124-48-1——— ——— Olbromoch lorome thane_______1579-00-5 ———— — —1,1,2-Tr ichloroe thane______I 571-43-2 ———————— Benzene____________________'61U061-02-6- —— —trans-l,3-Dichloropropene__I 575-25-2 ——— -- —— Bromoform__________________I"?108-10-1 ——— - — -4-Methyl-2-Pentanone_______i 1059l-78-6--------2-Mexanone_________________1 lu127-18-4- — — ---Tetrach loroethene__________'579-34-5---------l,l,2,2-Tetrachloroethane__I 5108-86-3 ——— — — Toluene____________________I 5108-90-7-- — — — Ch lorobenzene______________15100-41-4--------Ethyl benzene_______________1 210 0-42-5-- — ----Styrene____________________ I 5133Q-20-7——————Xylene (.total J____________15__ _________ ________ _______I

U0U

1U101010IU101010IU10IU10IOIIUIOIUIUIOIUIOIOUIUIU

FOkM I 1/87

VQ& Z ttO*

C

t**/»n 20 I/An) QNAOtfKOO *ON

TO? (pom/not)

•ON nrors YiW tlCXTYICV S9ZMVMO TILIVIOAVt




Lab Code: Case No.:

Matrix: Vsoil/water) WATER

Sample wt/vol: 5.0 Cg/mLJ ML

Level: I low/mad) LQLJ


Column: tpack/cap) PACK


Cont ract :

S«S No.:

EPA SAMPLE NO.

A5572

SD£ No.:

Lab Sample ID: CA'7572'J*

Lab File ID: >D2624

Date Received:

Date Analyzed: Oi/15'91

Dilution Factor: 1.u

CONCENTRATION UNtTS:t-ug/L or ug/Kg) UG/L

CAS NUMBER

01.02. 60-29-703. 75-43-4

COMPOUND NAME

UnknownEthyl ether C8CI )Methane, dichlorofluoro-

RT

2.5113.527.08

ESP. CUNC432015

Q

JJJ

FuRM I UOA-T1C 1-'S7

11=1VOLATILE ORGAN ICS ANALYSIS DATA SHEET

ERA SAMPLE NO.

A5575Lab Name: ETC Corp. Contract: I________

Lab Code: Case No.: SAS No.: SDG No.:

Matr ix: tsoi1/water) WHTER Lab Sample ID: CA5575kM

Sample wt/vol: 5.0 Cg/mL) ML Lab F i l e ID: >D2585

Level: (low/med) LQU1 Date Received:



CAS NO. COMPOUND


Di lut ion Fac tor : J.

CONCENTRATION UNITS:Cug/L or ug/Kg) UG/L Q

I74-87-3- —— ——— -Chlorome thane______________I 1074-83-9-- —— - — -Bromome thane_______________I 1075-01-4————————Vinyl Chloride_____________I 1075-00-3- ————— --Chlo roe thane_______________I 1075-09-2————————Methylene Chloride_________1567-64-1 — --- — --Acetone____________________I 1075-15-0 ——————— Carbon Disulfide__________1575-35-4——- —— --1,1-Dich loroethene_________1575-34-3————————1,1-Dichloroe thane_________15540-59-0—--———1,2-Dichlorethene ttotalJ__13567-66-3 ———————— Chloroform_________________15107-06-2 — — ----1,2-Dichloroethane_________I 578-93-3 ———————— 2-Butanone_________________11071-55-6 —————— —1,1 ,1-Tri chlo roe thane______1556-23-5 — - ————— Carbon Tetrachlor ide_______15108-05-4——————Vinyl Acetate_____________I 1075-27-4---------Bromod ich lorome thane_______I 578-87-5 ———— — — 1,2-Dichloropropane________1510061-01-5 ————— cis-l,3-Dich loropropene____1579-01-6-- — — — -Tr ich loroethene____________I 18124-48-l--------Dibromochloromet hane_______ I 579-00-5 —— — ———1,1,2-Trich loroe thane______I 571-43-2 — — — ---Benzene____________________1510061-02-6- — — -trans-l,3-Dichloropropene__I 575-25-2--- —— — -Bromof orm__________________15108-10-l--------4-riethy 1-2-Pen t anone_______ I 10591-78-6---- — --2-Hexanone_________________I 10127-18-4----- — -Tet rach loroethene__________1579-34-5 — -----—1,1,2,2-Tetrachloroethane__15108-88-3 ——————— Toluene____________________15108-90-7------ — Ch lorobenzene______________15100-41-4— — — --Ethyl benzene_______________15100-42-5 ——————— Styrene____________________151330-20-7——————Xylene C total )____________15

____ ___I__

IUIDIUIUIUIUIUIUIUIIUIUIUIUIUIUIUIUtuIIUIUIUIUIUIUIUIUIUIUIUIUIUIU

8FORM I UGft 1/87 Re-

Lab Naaa:Lab Coda:

IAVOLATZLC OKOAWZCS AHALYSZS DATA fHtTT

ere

t»A SAK7U NO.

Caaa No.:Matrix: uoil/vatar) OJATBg.Saapla wt/vol: s fq/mLl O^LLaval: (lev/Bad) £c^I Moiaturo: not dac.coluan: (pacK/ctp)

CAS NO.

Dilution Factor:CONCUmUTION ONZTS(ug/L or uq/yqi

Tatrahydrofuran, u

Z VGA I/I? »«v

IEVOLATILE ORGANICS ANALYSIS DATA


ERA SAMPLE NO.

A5575Lab Name:ETC Corp. 1 Laboratory

Lab Code: Case No.:

M a t r i x : Isoil/water) WATER

Samp 1e wt/voI: 5.0 Cg/mL) ML

Level: tlow/med) LOW


Column: (pack/capJ PACK


Cont rac t :

SAS No.: SDG No.:

Lab Sample ID:

Lab File ID: >D25B5

Date Received: 1/5/91




CAS NUMBER

01. 75-43-4

COMPOUND NAME

Me thane, dichlorofluoro-

RT

7.10

EST. CONC

16

Q

J

FORM I UQA-TIC 1/87 Rev.

10

IttuQLftTlLE ORGttNlCS HNHLYblS UH1« bHbtT

Lab Name: ETC Corp.

Lab Code: Case No.

Mat r tx : ' so i 1 •'wa ter ) Uft ! tR

Samp I e wt ''o 1 : 5.0 <

L«i--e 1 : <• low/med ) LULJ

S M o i s t u r e : not dec.

Co 1 umn : f. oack -'cap J

Crtb HO. LUMPUUND

Cont rac t : I

Srtb No . : Sutsi No . :

Lab Sample IU: CMrr.'6u:

ML Lab F i le lu= >Ui;1?.-:'

Uate kece i^-ed :

Date Hnalvzed: 0 i 'li--'^I

d i l u t i o n hactor:

CUNLLNIKrtTIQN UNITS:f, uq/L or uQ'-'KqJ Ub-''L

7a-a"'-3---------Ch lorome thane !iU74-«3-9-----——-Bromomethane 11U7^-01^4—-------umvl Chlor ide I 1U75-UU-3-----—--Chloroethane I1U7^-09-2-- -—--- -Methvlene Ch lor ide 1^67-64-1---- — ---rtcetone I 107^-15-0---------Carbon DisuIf ide 1575->(?-4--- — --—1,1-Oichloroethene l^7"?-34-3----- — --1,1-Oichloroethane I4?•?40-?>9-0----- — -1.2-Dichlorethene f. t o t a l ) I1?6/ ' -66-3- - - - - - - - -Chlorotorm I1?1Q7-U6-2---- — —1,2-Dichloroethane i1?7S-93-?---------2-Butanone I1U71-t'?-6---- — — -1 ,1 ,1-Tnchlo roe thane I1?5fr-23-5---------Carbon Te t rach lo r i de 151U8-U5-4-—-----Yinvl Hcetate IiU75-2.-?-4---------Bromod ich lorome thane I •?••'8-8.--5- — — — —1,2-Dichlorooropane 151UU6I-U1-5---—-cis-l,3-Dichloropropene 1579-U1-6--———-Trichloroethene '5124-4b-l--------Dibromochloromethane 1579_UU_5_____——-1,1,2-Trichloroethane '571-43-2---------Benzene I1?lu061-02-6- ——— -trans-1.3-OichlorooroDfcne i 57^-25-2---------Bromoform 15lu6-lu-l--------4-Methvl-2-f:'eni: anone '1U5Wi-7a-6--------2-Hexanone i 10l27-ia-4--------Tetrachloroeth*ne *579-3*+-5---------l,l,2.2-Tetrachloroethane I1?10y-d8-3--------Toluene 15lUb-9u-7--------Chlorobenzene 15lUU-4l-4--------Ethvlbenzene 1310L'-42-5--------Stvrene 15133u-20-7-------Xvlene (. t o t a l ) 14

I

I UIU

l LI L 1

IUIUI L-I U

IUI '.IUI L

I L

IU

I L'

F UKM I UUft

11


EPA SAK?LE NC.

Lab

Lab Code:

Bit C6AP.

Caaa NO.:

Contract:SAS No.: SDC No.:

Matrix: faoil/vatar)Sanpla vt/vol:L«val : (low/m«d)% Moistura: not d«c.ccluicn: (pack/cap)

CAS NO.

fg/mL) POLLab Sanpla ID:Lab Fila ID:Data Racaivad:Data Analyzad:

COMPOUND

Dilution Factor:

CONCENTRATION UNITS:(u /L or uq/Kq) U&!L

Tetrahydrofuran

PORM I VGA

1.0

1/8? Ftv

12

V /

1Lm 1LE urt&HNlCS HNHLTbIS UrtTH bHtET

TtNTtt i lytLY lutNTihitu

NU.

'6Lab Name J ETC Corp. I Laborat ory

Lab Lode: Case No.:

ria t r i x : ' s o i l - 'wa ten. ' WH ' tR

b-amD Iff wt -'vo 1 : •? . U '- Q-''mL .' ML

Lc'-e 1 : '. low. /;n»d J LUU

\ r io is tu re : not dec.

Co 1 -jrnn : ! oack cap ) KMLK

Number i ' lCs hound: 2

Lont rac t :

bMb No . : SL'ij Nc . :

Lab 'sample LU: LH1?1: --'cu:

Lab I- i le lu: 'U'J^;11

Uate Kecciijed:

Uate Hnalvzed: Ol-'ll '•'I

U i l u t i o n l-actor: I.

fr.ttl I UN UNITS:'ua - 'L or u a ' K q ) UG/L

LMb

I Ul.i U2.

LUHHUUNU NhHt.

UnknownUnknown

Ri 1

iu.63v 1. 1Q

I. LUNL I U Immmmmmmmm \ «*=...

IJ I

I I

- i 1 C

13

VOLATILE ORGAN ICS ANALYSIS DATA SHEETEPA SAMPLE NO.

A5577Lab Name: ETC Corp. Contract: I___

Lab Code: Case No.: SAS No.: SUU No.:

Matrix: I soi1/waterJ UATER Lab Sample ID:

Sample wt/vol: 5.0 tg/mLJ ML Lab File ID: >D_591

Level: Uou/mcd) LOU Date Received:


Column: tpack/cap) PWCK

Date analyzed: 01-'13'9i

Di lut ion Factor:

CAS NO. COMPOUNDCONCENTRATION UNITS:lug/L or ug/Kg) Ub/L U

74-87-3 —— ——74-83-9 —— ——75-01-4 —— ——75_00_3 _ _ _ _ _ _75-09-2 ------67-64-1 —————75-15-0 ------75-35-4 —————75-34-3 —— ——540-59-0 ————67-66-3 ------107-06-2 ————78-93-3 —————71-55-6 —————56-23-5 —————108-05-4 ————75-27-4 —————78-87-5 —————1Q061-01-5 ——79-01-6 ------124-48-1 -----79-00-5 —— — -71-43-2 —— ——1U061-02-6 ——75-25-2 —————108-10-1 ————591-78-6 -----127-18-4-- ---79-34-5 —————108-88-3 ————10b-90-7- — --100-41-4 -----100-42-5-----1330-20-7 ———

t---Chloro me thane 1---Bromome thane 1— -Uinyl Chloride 1---Ch loroethane , 1---Methulene Chloride t---ttce tone , . . 1---CarbonDiaulfide 1— -lrl-Dichloroethene 1— -1 . 1-Dichloroe thane 1— -1,2-Dichlorethene t total ) __ 1---Ch lore form 1---1 .2-Dich lo roe thane 1---2-Butanone . 1- — 1.1.1-Trichloroethane 1-^-Carbon Te t rach lor ide 1---Uinyl Acetate 1---Brornod ich loromethana I---1.2-Diehloroprooane 1-*-eis-l, 3-Dich ioropropene ____ 1--_Tp ich loroathene „,..._. _. . 1---Dihpomoeh lorome thane 1---1.1.2-Triehlnraethane 1---Benzene 1— -trans-l,3-Dich Ioropropene __ I---Bromof arm , 1_ — A-M«thyl--2-PBntanone 1---2-Haxanone n ., __ a \---T«traehlnpo«th«ne I---1,1,2 ,2-Tetrachloroe thane __ 1---To luene 1---Chlorohenzane.---Eth-ulbenzene---Styrene „„„„_,.„,---Xy lene t tota 1 )

FUKP1 I UOrt

101010559705540105533005510535855955H97.duo513054512

i1UIUIUIJtoIE10IOIIIUIUIEIUIUIUIUIJIUIIUIUIIUIUII JIJIU1IU1 JIU11

1^87 wev.14

1AVOXATZU OMAffZCS AJfALYflXS nATA ffXXZT t>A SAKTU NO

ere*••* Cod*s ___—— Caaa Ko.:Matrix: (aoil/vatar) toJfrray.saapla vt/vol: ^ fa/«Li MLLaval: (low/mad) Lot*I Moiaturat not doc.column: (pack/cap)

CAI NO. COKPOUKO

100 M.:

Saapla ID:UB filo 10:

Data Xacaivad:Data Analyzad:

'•Dilution Factor:COHCtKTlUTIOH CMZTS:(ug/L or u€/Kg] MC/L

Totrahydrofuran HQ6

re» z VOA 1/17

15

IEVOLATILE URGANlCS ANALYSIS DATA SHEET


EHA SAMPLE NO.

A5577Lab Name:ETC Corp. I Laboratory

Lab Code: Case No.:

Matrix: tsoil/water) WATER

Sample ut/vol: 5.0 Cg/mLJ ML

Level; l low/med) LUU1


Column: (.pack/cap) PALK


Cont ract:

SAS No.: SDli No.:

Lab bample ID: C,A'?577v

Lab File ID: >U2591

Date Received:

Date Analyzed: 01/13/9i

D i l u t i o n Factor: l.u

CONCENTRATION UNITS:tug/L or ug--'Kg) UG/L

CAS NUMBER

01. 78-92-202. 75-43-403. 67-63-004. 75-71-805. 75-45-606.07. 6U-29-708.09.10. 624-64-611.

COMPOUND NAME

2-ButanolMethane-, d ich lorof luoro-2-Propano 1Methane , d ich lorodif luoro-Me thane, chlorodifluoro-UnknownEthyl ether C8COUnknownUnknown2-8utene, lE)-Unknown

R l

15.287.U9

1U.314. 182.48

16.2113.5329. >423.6516. ya3.21

ESI. CUNC

230*a6b4929272310446

Q

JJJJJjJ<_>JJJ

FUKM I OOA-T1C

16

UOLATILE ORGAN ICS ANALYSIS DATA SHEETERA SAMPLE NO

IA5577.DI-Lab Name: ETC Corp.

Lab Code: Case No.:

Matrix: tsoi 1/water) WATER

Sample wt/vol: .1 Ig/mLJ ML

Level: tlow/med) LOU



SOU No . :

CAS NO. COMPOUND

Cont ract:

SAS No.:

Lab Sample ID:

Lab Fi le ID: >D*622

Date Received:


Dilution Factor: 5U

CONCENTRATION UNITS:tug/L or ug/Kg) UG/L U

I74-87-3———— ——— Ch lorome thane______________150074-83-9 — ————— Bromomethane______________I 5 0075-01-4———————v"inyl Chloride____________150075-00-3 ———————— Chlo roe thane_______________150075-09-2 —— ———— -Methylene Chloride_________174067-64-1 —— ————— Acetone__________________116UO75-15-0———-- — -Carbon Disulf ide__________125075-35-4————————1,1-Di chlo roe thane_________125075-34-3 ——————— 1,1-Di chlo roe thane________1250540-59-0———————1,2-Dichlorethene t total )__125067-66-3- — — - —— Chloroform_________________1250107-06-2 ——— ——— 1,2-Di chlo roe thane_________1*5078-93-3 —— ——— — 2-Butanone_________________1290071-55-6 — ———— — 1,1,1-Tr ich loroethane______125056-23-5 —— —— —— Carbon Tetrach lor ide_______1250108-05-4———————v-inyl Acetate______________I5UO75-27-4——-- ——— Bromodich lorome thane_______125078-87-5 —— ————— 1,2-Dichloropropane_______125010U61-01-5 ————— ci»-l,3-Dich loropropene____125079-01-6 — —————— Tr ich loroethene____________I2b0124-48-1 ————— — Dibromoch lorome thane_______125079-00-5-- ————— -1,1,2-Tr ich loroe thane______l2*?071-43-2 — —— ——— Benzene____________________I25U10061-02-6-- —— -trans-l,3-Dich loropropene__I 2*»075-25-2-- —— — — Bromoform__________________I25U108-10-1---- —— -4-Methyl-2-Pentanone_______I5UO591-78-6--------2-Hexanone_________________I5UU127-18-4— — ----Tetrach loroe thene__________1 25079-34-5--- — --—1,1,2,2-Tetrachloroethane__1250108-88-3 ——————— Toluene________________ 178108-90-7--- — —— Chlorobenzene______________I2b0100-41-4— ————— Ethyl benzene_______________ I 250100-42-5--- — ---Styrene____________________12501330-20-7- — —— -Xylene (total )____________1250 I

FORM I OOA 1X87 Rev

17

1AVOXATXXX OMANXCS AKAX.YSX1 DATA StttT SAK9U NO.

Lab Namo:,Lab Coda:

areCaM No.:

Matrix: (aoil/vator) fcUfrTEg.Saapla wt/voi: 0-^ fg/mLi mi.Laval: (low/mad)

% Moiaturat not dae.Column: (pack/cap)

Contract:SAS HO.i

CAS NO. COMPOUND

SM No.:Saapla IDi

Ub Pilo ID:

Data ftoeoivod:Data Analyiod: i/f^l

dilution Factor:coNccmurxoN ONZTS(u»/t or uf/Kf)

Totrahydrofuran.

z VOA I/I? R«v

18

VOLATILE ORGftNlCS HNftLVSIS DftTft SHEETSRHPLE NO.

«55?8Lab Name: ETC Corp. Contract: I

Lab Code: Case No.: SAS No.: SUU No.:

matrix: Isoil/water) WATER Lab Sample 10:

Sample wt/vol: 5.0 (g/mLJ ML Lab F i l e ID:

Level: Uow/med) LOUI Date Received:


Column: t-oack/cap) PACK

CAS NQ. CuriPGUND

Date Analyzed: 01/14x^1

Dilution Factor:

CONCENTRATION UNITS:tug/L or ug/KgJ UL./L U

74-87-3 —————74-83-9 —————75-01-4 —————75-00-3 —————75-09-2 —————67-64-1 —————75-15-0 —————75-35-4 —————75-34-3 —————540-59-0 ————67-66-3 —————107-06-2 ————78-93-3 —————71-55-6 —————56-23-5 —————108-U5-4 ————75_97- A------78-87-5 —————10061-01-5 ——79-01-6 —————124-48-1 ————79-00-5 —————71-43-2 —————1U061-02-6 ——75-25-2 —————108-10-1 ————591-78-6 ————127-18-4 ————79-34-5 —————108-68-3 ————10b-90-7 ————100-41-4 ————10U-42-5-- — -1330-20-7 ———

---Ch lorome thane---Bromo me thane- — Umyl Chloride---Chloroethane,.---Mettrjlene Ch lor ide---Acetone---Carbon Disu 1 f ide---1 ,1-Dichloroethene---1 .1-Dichloroethane—— 1 ,2-D ich lore thene t t o t a l ) __---Ch lorof arm---1 . 2-D ich lor oe thane---2-But anone_---1 .1 .1-Tr ich loroe thane---Carbon Tetrachloride---Uinyl Acetate---Bromod ich lorome thane---1 ,2-Dich lore-propane, ,._ IM _---c is-1 , 3-D ich lorop rooene— -Trichloroethene „,..._---Dibromoch lorome than*---1.1.2-Tr ich loroe tnan«---Benzene---trans-1 , 3-D ich loropropene __---Bra mo form---4-Meth-ul-2-Pentanonft---2-Hexanone---Tetrach loroe thene---1 ,1 ,2/2-Tetrach loroe thane __---To luene---Chlorohenzene---Ethylbenzene---Sturene---Xylene ttotal) _,

11101 1012131515151514716615151 101515liO15151511715i5121515l 101 IU1491515151515121

1 i10 1IU :U I1 J1 i1 J !IU 1IU1 11IU 1IUIU 1IUIU 1IUIU 1IUIU 11IU 11 UU i1 UIU 1IUIU 11IU 11 UIU 1IUIU 1u1 1

FUrtM I

19

IAVOZATXU OHOAJttCJ ANALYSIS DATA SMXTT SAKPU NO.

Ufe NAMS

U0 COdOJ

ensCaoo NO.:

Matrix: (soU/vatar)JjJ rgg.

Contract:SA* NO.t

AV57?

Saaplo vt/vol:Lovol:

fa/mLi mi

*00 NO.j

Ub Saaplo ID:Filo ID:

s (low/mod) ^^ Data Meoivod: i/cAt•turot not doc. Data Analv««d: j/laMin: (paelc/eap) ffW^ dilution Factor: _j

CONCZNTKATXON UNITS:CAS NO. COMPOUND (UC/L or UC/KO) MC/t

Totrahydrofuran

•

10

•• ^^^B

Q

U

FOJW X VOA 1/17

20

IEVOLATILE ORGAN ICS ANALYSIS DATA SHEET

TENTATIVELY IDENTIFIED CQnPQUNDS

EPA SAHPLE NO.

Lab Name:ETC Corp. 1 Laboratory

Lab Code: Case No.:

flatrix: tsoil/water) WATER

Sample wt/vol: 5.0 Ig/mL)

Leve1: U ow/med) LOU

S Hoisture: not dec.

Co lumn: '.pack/cap) PACK


Contract:

SAS No.: SDG No.;

Lab Sample ID:

Lab File ID: >U2610

Date Received:

Date Ana lyzed: Ol''l4/"*l

D i l u t i o n Factor: 1. ;.


CAS NUHBER

01. 75-43-402.

COnPOUND NAHE

Methane, dichlorofluoro-Unknown

RT

7.082 . 42

EST . CONC

18a

Q

JJ

FuRfl I UOA-TIC l-'ti?

21


EHA SAHPLE NO

IIA5579

Lab Name: ETC Corp.

Lab Code: Case No.:

Matrix: Isoil/water) UAf£R

Sample wt/vol: 2.5 ig/mLJ flL

Level: Clou/med) LQUi


Column: (.pack/cap J PACK

Cont ract

SAS No.

CAS NO. COMPOUND

: SUb No.:

Lab Sample ID: CA(?'?79U1

Lab File ID: >D*612

Date Received:

Date Analyzed:

Di l u t i o n Factor

CONCENTRATION ONITS:lug/L or ug/Kg) Ub/L

i74-87-3 ——— - ——— Chlorome thane______________12074-83-9 —— - ——— -Bromo me thane_______________I 2075-01-4—— — ——— Yinyl Chloride_____________12U75-00-3 ——————— -Chlo roe thane_______________I 1275-09-2-- — — — -Methylene Chloride_________I 1067-64-1 — -- — —— Acetone____________________139075-15-0- ——— — — Carbon Disulf ide___________I IU75-35-4————— — -1,1-Dichloroethene________I 1075-34-3———————1,1-Dichloroethane________ 1170540-59-0-————1,2-Dichlorethene ttotal)__1867-66-3- ——— — — Chloroform_________________t IU107-06-2 ———— ——1,2-Dichloroethane_________1 1078-93-3 ——————— 2-Butanone_______________I 21071-55-6—— — ———1,1,1-Trichloroe thane______I 1056-23-5 ———————— Carbon Tetrachlor ide_______I 10108-05-4- — - ——— Yinyl Acetate______________12075-27-4---------Bromod ich loromethane_______I IU78-87-5- ——— ——— 1,2-Dich loropropane________I 310061-01-5 — — — cis-l,3-Dichloropropene_____I 1079-01-6 — ————— Tnchloroethene___________I 19124-48-1 ——— — — Dibromoch lorome thane_______i 1079-00-5 — ——— ——1,1,2-Tr i chloroe thane______I 1071-43-2- — — —— -Benzene___________ IB10061-02-6—————trans-1, 3-D ich loropropene__I 1075-25-2 — — -- — -Bromoform__________________I IU108-10-1 ——— ——— 4-nethyl-2-Pentanone_______ I 4459 l-78-6--------2-Mexanone_____ ______ I 2U127-18-4— — — — Tet rachloroethene__________I 279-34-5———— ——— 1,1 ,2,,2-Tetrachloroethane__I 10108-88-3 — ——— --Toluene____________________,1 14108-90-7— ——— --Chlorobenzene______________I 10100-41-4- — — — -Ethylbenzene_______________I 10100-42-5--------Styrene_____________________I 101330-20-7— — — -Xylene (.total J____________13

___ I

1010101 J10110IO1tj10IU1101010IOUtu110IUUIO101IU1 JIU1IUIUIU1 J

FORM I 1/87 Rev

22

1AVOLATILE OftOANZCS ANALYSIS DATA StttT SAK9U NO.

*** Codgl - Caao NO.:Matrix: faoil/vatori tolfrTEfcSaaplo vt/vol:Lavol: (lov/aod)I Noisturot not doe.Coluan: (paeX/eap)

CAS NO. COMPOUND

*00 No.:

Ufe Saaplo ZD:Lab Fllo 10:Data Xoeoivod:Data Analysod:

'.Dilution Factor:CONCZNTXATXON UNITS:(u»/L or uq/Kgi Mfl/L

Totrahydrofuran ,270

Z VOA

IEVOLATILE ORGAN1CS ANALYSIS DATA SHEET

TENTATIVELY IDtNTIFIED COMPOUNDS

Lab Name:ETC Corp, I Laboratory

Lab Code: Case No.•

Hatrix: Isoi1/uater) UA1ER

Sample wt/vol: 2.5 Ig/mL) ML





Cont ract:

SAS No.:

EPA SAMPLE NO.

Ii A55;-1*I_

SDb No

Lab Sample ID: C

Lab File ID:

Date Received:

Date Analyzed:

D i l u t i o n Factor

CONCENTRATION UNITS:(.ug/L or ug/Kg) UG/L

2 .»

CAS NUMBER

01. 75-43-402. 75-71-803. 75-45-604. 60-29-705.

COMPOUND NAME -

Methane, dichlorofluoro-Me thane, dichlorodifluoro-Me thane, chlorodifluoro-Ethyl ether IBCI )Unknown

RT

7.054. 152 .4413.5310.31

Esr. CUNC9U29252210

Q

JJJJJ

FuRM I iJOA-TIC

24


ERA SAMPLE NO

A558QLab Name: ETCNJ

Lab Code:

Cont ract:

Case No.:

Matrix: (soil/water) UATER





CAS NO. COMPOUND

SAS No.: SDG Mo.:

Lab Sample ID: CA558QV

Lab File ID: ->C2133



Dilut ion Factor : 1

CONCENTRATION UNITS:Cug/L or ug/Kg> UG/L Q

74-87-3---------Chloromethane__________74-83-9---------Bromomethane____________75-01-4———————Vinyl Chloride_________75-00-3—-———Chloroethane___________75-09-2 ————— -r-Methylene Chloride______67-64-1 — — - ——— Acetone_________________75-15-0——---—Carbon Disulfide________75-35-4--—————1,1-Dichloroethene______75-34-3 — — - — — 1,1-Dichloroe thane______540-59-0--————1,2-Dichlorethene (total).67-66-3-~-------Chlorofor m______________107-06-2—-———1,2-Dichloroethane______78-93-3---———2-Butanone__________7X-55-6--—-———1,1,1-Trichloroethane____56-23-5-————Carbon Tetrachloride____108-Q5-4--————Vinyl Acetate___________75-27-4---------Bromodichloromethane____78-87-5-- — - — —1,2-Dichloropropane______10061-01-5--——cis-1,3-Dichloropropene__79-01-6-- — - — --Tr ichloroethene_________124-48-l--------Dibromochloromethane_____79-00-5---———-1,1,2-Trichloroethane____71-43-2- ——— ——— Benzene_________________10061-02-6----—trans-l,3-Dichloropropene.75-25-2---------Bromoform_______________108-10-1---——-4-Methyl-2-Pentanone_____591-78-6——————2-Hexanone______________127-18-4----- — -Tetrach loroethene_______79-34-5-—---—-1,1,2,2-Tetrachloroethane.108-88-3--------Toluene________________108-90-7————Chlorobenzene___________100-41-4--———-Ethylbenzene____________100-42-5--—-—-Styrene_________________

1 1330-20-7——————Xylene (total)_________I________________________________________

,110110110

.12515

.1101515,139.1815.1511011615,11015,1215112015,1514.151511011017015.15.15.15.1513

IIU1UIUIIUIUIUIU

IUIUIU1IUIUIUIJIU1IUIUuIUIUIUIUIIUIUIUIUIUIJ

1A

LAD NAM:,Codo:

are

VOIATILI OMANXCS ANALYSIS OATA SVXXT

contract! jAtyy?

*** »«•« ____ fM No. iLas Saaplo 10:Lab mo 10:

SAKPU HO

CM* No.:

Matrix: (soil/vatorl 6Jfrrae.Sa»plo vt/voi; S fg/«LlLovol: (lov/aod) Ux*% Moisturot not doc.Co1umn: (pack/cap)

Oat* Meoivod:Data AMlyiod: Unfa

dilution ftctor :

cu HO. COMPOUNDBKKS

(Uf/L or ua/Kal

TotraAydrofuran

1/17 Mv

26



EPA SAMPLE NO.

A'rSSGLab NamssETCNJ

Lab Code: Case No.:

Mat r i - : '.so; 1 -'water • WATER

Sample w t / v o l : 5.0 (g/mL> ML

Leve 1 : < low/mad.' LOW


C o l u m n : (pack/cap) PACK


Contract:

5AS No.: SDG Mo.:

Lab Sample ID: CA55SOU

Lab Fi le ID: 'C2133

Date Received: 01/9 •'91


Di l u t i o n Factor: 1.0

CONCENTRATION UNITS:Cug/L or ug/KgJ UG/L

1CAS NUMBER 1 COMPOUND NAME

01. 75-43-4 IMcthane, dichlorofluoro-1111111111111111

- I1111111!11111

RT

6.00

EST. CONC

37

tQ i

J lIi11111i1t11111!

'

|

1

1

i

!

111i

FORM I "JOA-TIC 1/87 Rev. 2 7


ERA SAMPLE NO.

A5581Lab Name: ETCNJ

Lab Code: Case No.:

Ma t r i x: (soil/wa t e r) WATER

Sample wt/vol: 5.0 (g/mL) ML




Con t rac t :

SAS No.: SDG No.:

Lab Sample ID: CA5581U

Lab Fi le ID: '-C2134

Date Received: Ol/S/91


Dilution Factor: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

74-87-3 — — - — --Ch lorome thane____________*l 1074-83-9 — -- — — -Bromome thane_______________I 1075-01-4————————Uinyl Chloride_____________t 1075-00-3 ———————— Chloroe thane_______________11075-09-2 —————— --Methylene Chloride_________1567-64-1 ———————— Acetone____________________1 1075-15-0 ———————— Carbon Disulf ide___________1575-35-4—-- —— --1,1-D i chio roe thene_________1575-34-3————————1,1-Dichloroe thane_________15540-59-0 ———————1,2-0 ich lore thene (total )__1567-66-3 ———————— Chloroform_________________15107-06-2 — -- — —1,2-Dichloroe thane_________1578-93-3 ——————— 2-Butanone_______________I 1071-55-6———————1,1,1-Trichloroethane______1556-23-5 — — — —— Carbon Te t rach lor ide_______15108-05-4———————Uinyl Acetate______________I 1075-27-4---------Bromod ich lorome thane_______1 578-87-5---- ———— 1,2-Dichloropropane________1510061-01-5----—cis-l,3-Dichloropropene____1579-01-6---- — - — Tr ich loroet hene____________15124-48-1- — — — -Dibromoch lorome thane_______I 579-00-5------——1,1,2-Tr ich lo roe thane______1571-43-2 ———— ——— Benzene__________________1510061-02-6——--trans-l,3-Dichloropropene__157?-25-2---------Bromof orm__________________15108-10-1 ——————— 4-Methyl-2-Pentanone_______I 10591-78-6 ——————— 2-Hexanone_________________1 10127-18-4-- — ----Tetrach loroet hene__________1579-34-5---------l,l,2,2-Tet rachloroe thane__15108-88-3 ——————— Toluene____________________15108-90-7--------Ch lorobenzene______________15100-41-4———————Ethyl benzene_______________15100-42-5 ——————— Styrene____________________151330-20-7—————Xylene (total)___________15

I

ID1UIUIUIU131UIUIUIUIU1UIUIUIUIUIU1UIUIUIUIUIUIUIUIUIUIUIUIUIUtutuIU

28

1AVOtATXU OMANXCS ANA1.YSXJ DATA fMEtT SAKPU NO.

I

UB Coda: ^__— Caoo No.Matrix: («oii/vatorl olfrTBESamplo vt/vol: S fq/mLlUv«l; (lev/mod) ten% Moisturoi not doe.Column: (pacX/cap)

Contract:SAS No.s

CAJ NO COMPOUND

Totrohydrofuran.

IWUB Samplo 101UB Pilo 10:Data KoeoivodiOtto AMlysod:

dilution Factor:COHCCmUTXON UWCS:(ug/t or ug/Kaa MCS/L

row z 1/17 ftcv

29



EPA SAMPLE NO.

Lab Name:ETCNJ

Lab Code: Case No.:

M a t r i ^ : 'so*1'water J WATER

Sample wt/vol: 6.0 'g/mD ML

Leve 1 : '. 1 ow/med .' LOW

"B Moisture: not dec.


Cont ract:

SAS Mo.: SDG Mo.:

Lab Sample ID: CA5S81U

Lab F i l e ID: /C213A

Date Recewec:: Ol-'S '91

Date Analyzed: Gl-'ll'-'91

Dilut ion Factor: 1.0

Number TIC* found: 0CONCENTRATION UNITS:Cug/L or ug/KgJ UG/L

I iI CAS NUMBER COMPOUND NAME RT EST. CONC

FORM I UOA-TIC 1/87 Rev30


ERA SAMPLE NO.


Lab Code: Case No.:

Mat r i x : C s o i l / w a t e r J UATER

Sample wt/vol: 5.0 tg/mL) ML

Level: (low/med-1 LQU



Contract:

SAS No. :

I ________

SDG Ho . :


CAS NO. COMPOUND

Date Received: 01-'S/91

Date Analyzed: Ql/11'91

Dilut ion Factor: 1

CONCENTRATION UNITS:Cug/L or ug/Kgj UG/L Q

I 74-87-3-- — - — — Ch lorome thane______________ I 10I 74-83-9------ — -Bromome thane_______________I 10I 75-01-4-———————Uinyl Chloride_____________110I 75-00-3 ——— ———— Chlo roe thane______________I 10I 75-09-2 —————— --Methylene Chloride_________15I 67-64-1 ———————— Acetone____________________I 10I 75-15-0 ——————— Carbon Disulfide__________15I 75-35-4————————1 ,1-Dich loroethene_________15I 75.34-3————————1,1-Di chlo roe thane_________15I 540-59-0———————1,2-Dichlorethene (total)__15I 67-66-3--- — -- — Chloroform_________________15I 107-06-2———————1,2-0 i chlo roe thane_________15I 78-93-3 ———————— 2-Butanone_________________1 10! 71-55-6 ———————— 1,1,1-Tr ich loroethane______151 56-23-5---- — — -Carbon Tet rach lor ide_______15I 108-05-4———————Uinyl Acetate______________110I 75-27-4----- — --Bromod ich lorome thane_______I 5I 73-87-5- — - —— — 1,2-Dichloropropane________15I 10061-01-5------cis-l,3-Dichloropropene____15i 79-01-6-- — -----Tr ich loroethene____________15I 124-48-1-- — —— -Dibromoch lorome thane_______15: 79-QO-5————————1,1,2-Tr ich loroe thane______15I 71-43-2 ———————— Benzene____________________15I 10061-02-6----—trana-1,3-Dichloropropene__15I 75-25-2-- ————— -Bromoform__________________15I 108-10-1- — — ---4-Methyl-2-Pentanone_______I 10I 591-78-6-——————2-Hexanone_________________110I 127-18-4--------Tet rach loroethene__________15I 79.34-5————————1,1,2,2-Tet rach loroe thane__15I 108-88-3 ——————— Toluene____________________151 108-90-7— — - — -Chlorobenzene______________15I 100-41-4—- —— — Ethyl benzene_______________15I 100-42-5 ——————— Styrene____________________15I 1330-20-7——————Xylene (total )____________15

IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUHJI 31

1AVOLATILE OMAMXCS ANALYSIS DATA NBXT

«*» *"•' are A*»________ Contracti___

CVA SAX.7U NO,

U* codoi CAM MO.IMatrix: (soil/vator) fcO»rgfcSaaelo vt/vol: 9 fg/mll mL

Lovol: (lev/mod) LOL*% Moisturo: not doe.Column: (paek/eap)

CAS MO.

Ho.:

SAaplO ID:

Ub riZo ID:Oato ftoeoivod:Oato AMlysod:

'•Dilution Factor:

COMPOUND (ug/t or

TotraAydrofuran, lo u

1/17 K«v

32

IEVOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIUELY IDENTIFIED COMPOUNDS

ERA 5AMPLE MO.

Lab Name:ETCNJ

Lab Code: Case No.:

M a t r i * : <-so i 1/water ^ WATER


Level: 'low/mad.' LQUJ

S Moisture.: not dec.



Cont ract:

SAS Ho.': SDG Ho.:


Lab Fi le ID: -C2131?

Date Received: 01/5x91

Date Analyzed: 01/11'91

D i l u t ion Factor: 1


CAS NUMBER COMPOUND NAME RT EST. CONC Q !

FORM I UOA-TIC 1/87 Rev.33

IttVOLATILE ORGANiCS ANALYSIS DATA SHEET

Lab Name: ETC Corp.

Lab Code: Case No.:

Matrix: isoi I/water) UIA'IER


Level: Clou/mad) LUUI

X Moisture: not dec.

Co lumn: (.pack/cap ) PACK

Con t ract

SAS No.

EPA SAMPLE NO

IA55b3I__

CAS NQ. COMPOUND

SDb No.:

Lab Sample ID: CA-?583^:

Lab Fi le ID: >D'<!599

Date Received: lhjat


Dilution Factor:

CONCENTRATION UNITS:tug/L or ug/Kg) Ub/L U

74-87-3— ———— — Ch loromethane___________74-83-9-————————Bromo me thane____________75-01-4—— ————— Umyl Chloride__________75-00-3-— ———— -Chloroe thane____________75-09-2--—————Methylene Chloride_______67-64-1 ———— — — Acetone_________________75-15-0 —— ————— Carbon Disulf ide________75-35-4-————-1,1-Dichloroethene_______75-34-3—————---1,1-Dichloroethane______540-59-0———————1,2-Dichlorethene I total).67-66-3---------Chloreform______________107-06-2———— —— 1,2-Dichloroe thane_______78-93-3 ———— — — 2-Butanone______________71-55-6-----—--1,1,1-Trichloroethane____56-23-5---------Carbon Tetrachloride____108-05-4- —————— "Jinyl Acetate___________75-27-4---------Bromodichloromethane78-87-5---------l,2-Dichloropropane______10061-01-5————ci»-l,3-Dichloropropene__79-01-6———————Tr ich loroethene_________124-48-1 ——— ——— Dibromoch lorome thane____79-00-5 ——— ————1,1,2-Trich loroe thane____71-43-2- — - ——— -Benzene_______________1U061-02-6—————t rans-1,3-Dichloropropene.75-25-2---------Bromofor m_______________108-10-1————-4-Methyl-2-Pentanone_____591-78-6-----—-2-Hexanone______________127-18-4--------Tetrachloroethene________79-34-5-—-__—-1f1,2,2-Tetrachloroethane.108-68-3--------Toluene_________________10ti-90-7————-Chlorobenzene___________100-41-A---——-Ethylbenzene____________100-42-5--——--Styrene_________________1330-20-7—— —— -Xylene t t o t a l )__________

I.110.110.110.1 1013.1515.15.15.15.15.15.110.15.15.1 1015,15,1515,15.151515.15,1 10i 10151515,15,1515.15

I

IIUIUIUIUIJUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUI UIUI UIUIUIUI UIUIUIUIUIUIUI

FUKM i 1/87 Rev.34

La* Namo*

1AVOZATIIX OMAMXCS ANALYSIS DATA SKXT

ere

WA SAKTU NO.

ta* Codoj _____ caa* NO.:Matrix: (soil/vator) 6J*rgg.Sampla vt/voi:Uval: (lev/mod)% Moisturat not doc.Column: (pack/cap)

CJkJ HO. COMMUKO

Totrahydrofuran,

•00 tfo.:

Samplo toiUb Filo 10:Otto ftocoivod:Otto Antlysod:

'•Dilution Factor:COWCtJmUTIOM CHITS:(U»/L or W/Kgj M&/L

POtH Z VOA 1/17 R«v

35



Lab Name:ETC Corp. I Laboratory Contract: I_____

Lab Code: Case No.: SAS No.: SDb No.:

Matrix: tsoiI/water> WATER Lab Sample ID:

EPA SAMPLE NO.

Sample wt/vol: 5.0

Level: Uow/med) LOIO

X Moisture: not dec.

Column: Ipack/cap) PHCK


Cg/mLJ ML Lab File ID:

Date Received: \J~JJ6\\

Date Hnalyzed: 01/14/91

Dilution Factor: l.u

CGNCENTRftTION UNITS:(.ug/L or ug/Kg) UG/L

CAS NUMBER

01. 1066-40-6

1

COMPOUND NAME

Silanol, trimethyl-

RT

16.15

ES ( . CONC

5

Q

J

FURM I 1/B7

36

1AVOLATILE ORGAN1CS ANALYSIS DATA SHEET

Lab Name: ETC Corp.

EHA SAMPLE NO.

A5585Cont rac t: I ___

Lab Code: Case No.: SttS No.: SUU No.:

Matrix: i-soi 1/water) WAVER Lab Sample 10:

Sample wt/vol: 5.0 tg/mL) ML Lab File ID: >D^593

Level: llow/med) LOW Date Received:


Column: '.pack/cap) PHCK

CAS NO. COMPOUND


Dilution Factor: i

CONCENTRATION UNITS:lug/L or ug/Kg) U&/L Li

74-87-3 ------74-83-9 —————75-01-4 -----75-00-3 —————75-09-2 — ———67-64-1 —————75-15-0 —————75-35-4 —————75-34-3 ----- -540-59-0 -----67-66-3 ------107-06-2 -----7B-93-3 ------71-55-6 ——— —56-23-5 — — —108-05-4 ————75-27-4 ------78-87-5 — — —10U61-01-5 ——79-01-6 —————124-48-1 ————79-00-5 ------71-43-2 ——— —10061-02-6 ——75-25-2 —— ——108-10-1 -----591-78-6 -----127-18-4 -----79-34-5 ------108-88-3 — ——108-90-7 ————100-41-4 — - —1UU-42-5--- —1330-20-7 ———

---Ch lorome thane---Bro mo me thane- — Vin«jl Chloride---Chloroe thane---Methylene Chloride---Acetone---Carbon Diaulfide ,.,.,„- — lrl-Dichloroethene---1 ,1-Dich lor oe thane—— 1,2-Dichlorethene t total ) __---Chloroform ,._- — 1 r2-Dich lor oa thane---2-Butanone---1 .1 .1-Trichloroe thane---Carbon Tetrachloride---"Jinyl Acetate---Bra mod ich lorome thane---1 .2-Dichloroorooane---cis-l,3-Dich loropropene ____---Tr ich loroethene . ,_---Dihromnch lorome thane---1.1.2-Trichloroetnane---Benzene , ..,.„---trana-1 .3-Dichloroorooene---Bro mo form---4-Methyl-2-Pentanone---2-Hexanone ,---Tetraeh loroethene- — 1,1,2 ,2-Tet rachloroethane __---Toluene ,„,..---Ch lorabenzene---Ethyl benzene---Styrene---Xy lene C tota 1 )

11 10110110I 10111361515151515151101515110151515121515151515HOI 10121515151515151

1 iIU 1IU IIU 1IU 1IJ 11 iIU 1IUIU 1IU :IU 1IU <IU 1IU iIU 1IU iIU 1IU iIU 1U iIU 1IU iIU 1IUIU 1IUIU 1IJ 1IU 1IU 1IU 1IU iIU IIU I1 I

FURM I "JOA 1/87

37

VOtATZLX OMAHZCS AXALYSIS DATA SKtXT WA SAK7LI NQ.

Lab KAMILib C0d«3 Case He.:Matrix: (»oil/wAt«r) j^rgg.

wt/vol: X fq/mLl me(lev/mtd) £OLi

I Moisturti not dae.Column: (pack/cap)

CAS NO. COMPOUND

SOO V«.:

LA* laapio ID:Ut riia ZO:Date Me«iv«d:Data Analysad: _i

'•Dilution raetor:COKCIOmUTIOH UHITS(ug/L or ut/xai

TotraAydrofuran fo

ran x VOA 1/17 JUv

38

EHtt SttHPLE NO.

I

IEOOLftTILE ORGBNICS ANALYSIS DftTR SHEET

TENTATIVELY IDtNTIFIED COMPOUNDS

Lab Name:ETC Corp. I Laboratory Cont rac t : I_____

Lab Code: Case No.: SRS No.: SDb No.:

M a t r i x : tso i I /water ) UtA (ER Lab Sample 1LJ:

Sample w t / w o l : 5.0 Cg/mLJ ML Lab Fi le ID:

Level: ( . low/mod) LOtJ Date Kecei^ed: 1/7/11

% Ho i s t u r e : n o t d e c . Da te Hna lyzed : LJ

Column: (.pack/cap) PHCK Dilution fac tor :

Number TICs found:CQNCENTRHTION UNITS:tug/L or ug/Kg) UG/L

CMS NUHBE.R

01.

11111

COMPOUND NHHE

Unknown

Furttl I YOft-UC

RT

21.05

ES»i . CUNC

4

1--87

Q I

J l

i

i

i

i

i

i

i

I

i

i

i

i

i

i

i

Kev .

39

IflUOLHTILE ORGftNlCS HNflLYSIS DHTtt SHEET

EPft SrtHPLt NO.

l«5586Lab Name: ETC Corp. Contract: I___

Lab Code: Case No.: SRS No.: SDG No.:

Matrix: (.so i 1/water ) UttTER Lab Sample ID:

Sample wt/vol: 5.0 tg/mLJ ML Lab File ID: >D^594

Level: tlow/med) LOUt Date Received:


Column: ^pack/cap) PHCK

CAS NO. COMPOUND

Date ttnalyzed: Ol/13/yi

D i l u t i o n hactor:

CUNCENTRRTION UNITS:lug/L or ug/Kg) UG/L L

I74-87-3- — — — — Chlorome thane______________I 1074-83-9 — ——————Bromome thane_______________I 1075-01-4————————Uinyl Chloride_____________I 1075-00-3 ———————— Ch Ioroe thane_______________I 1075-09-2 ———————— Methyl one Chloride_________I 167-64-1 —————— -ftcetone__________________15475-15-0 — —— -- — Carbon Disulf ide___________1575-35-4——— ——— -1,1-Dich loroethene_________1 575-34-3 — ———— --1,1-Dichloroe thane_________I 2540-59-0- — ————1,2-Dichlorethene I total )__1567-66-3 ——— -* —— Chloroform_________________15107-06-2- ————— -1 ,2-Dichloroethane_________I 578-93-3- ——— — — 2-8utanone_________________I 1071-55-6 — ————— -1,1,1-Tr ichloroe thane______I .9uO56-23-5-- ——— —— Carbon Tetrachlor ide_______I 5108-05-4——— — — iJinyl Hcetate______________I 1075-27-4---------Bromodich loromethane_______I 578-87-5 ———— ———1,2-Oich loropropane________1510U61-01-5 —— —— cis-l,3-Dichloropropene____1579-01-6 —— — ——— Trich loroethene____________I 7124-48-1 ——————— Dibromoch lorome thane_______I 579-00-5 ———— — —1,1,2-Tr ichloroe thane______1571-43-2-- —— — — Benzene____________________1510061-02-6 ———— -trans-l,3-Dich loropropene__I 575-25-2 —— — — — Bromoform__________________ I 5108-10-1- — — — -4-Me t hy 1-2-Pent ana ne_______i 10591-78-6- ——— ---2-Hexanone_________________I 1U127-18-4- ——— ---Tetrach loroethene__________i 579-34-5-- — -- — -1,1,2,2-Tetrachloroe thane__15108-88-3 — — - — -To luene____________________ I 51U8-90-7— — ——— Ch lorobenzene______________15100-41-4- — — ---Ethylbenzene_______________I 5100-42-5--------Styrene____________________151330-20-7— — —— Xylene t total J____________15____________ ______ I

IU1UIUIUIJIIU'IUu1 UIUIUIUIJIUIUIUIUIUIIU

IUIUIUIUuIU1 UIUIUIUI U

FURM I

40

1AVOLATILE OMANICS ANALYSIS DATA SVXTT WA SAKPU NO.

tab NAMS,u* codot

ereCaao No.:

Matrix: UoU/vator) frlAree.Saaplo wt/vol: ^ fq/«Li r?LI*vol: (low/mod) LQL*I Moisturo: not doc.Coloan: (pocX/etp)

CAS NO. COMPOUND

fM No.:UA Saaplo 10:Lab rilo 10:Data Aocoivod:Data Analyiod:'•Dilution factor:

CONCZKT1UTION CHITS(ug/L or uo/Kai

Totrahydrofuran

rom i VOA 1/17 Rtv

41



ERA SAMPLE NO.

IIA55B6


Lab Code: Case No.:

Matrix: (.soi I/water ) WATER

Sample ut/vol: 5.0 (g/mL) ML

LeveI: Clow/med) LQU




Cont ract :

SAS No.: SDU No.:

Lab Sample ID:

Lab File ID:

Date Received:


Di lut ion Factor: 1. u


CAS NUMBER

01.02. 1066-40-6

COMPOUND NAME

UnknownSilanol, trimethyl-

RT

20.9716.24

ESF. OJNC45

Q

Jj

FORM I

42

1AVOLATILE ORGMNICS ANALYSIS DATA SH£ET

EHA SAHPLE NO.

A5587Lab Name: ETC Corp.

Lab Code: Case No.: SUii No . :

Matrix: I so ; 1 /water ) UIAIER

Sample wt/vol: 5.0

Leva 1 : i low/med ) LQUt

S floisture: not dec.


CAS NO.

Cont ract:

SAS No.:

Lab Sample ID:

tg/mLJ HL Lab F i l e ID: >D^595

Date Deceived: 1/7/11

Date Analyzed: 01-'13/yl

Di lut ion Factor:

CONCENTRATION UNITS:LOP1POUND tug/L or ug/Kg J Ub/L u

I74-87-3 — ———— — Ch lorome thane_____________110•74-83-9———————-Bromome thane_______________I 1075-01-4————————Vinyl Chlor ide_____________I 1075-00-3 ———————— Chloroe thane_______________I 1075-09-2- — ————— he thy I one Chloride_________1567-64-1 — - — ——— Acetone.___________________1 1375-15-0- —— — —— Carbon Disulfide___________I 575-35-4- — - — — -1,1-Dich loroethene_________1575-34-3 — — ————1,1-Dichloroe thane_________15540-59-0—— ——— -1,2-Dichlorethene t total )__I 567-66-3 ——— - — — Chloroform_________________I 5107-06-2 ————— — 1,2-Dichloroe thane________1578-93-3 ———————— 2-Butanone_________________I 1071-55-6———————1,1,1-Trichloroe thane______1556-23-5---------Carbon Tetrachlor ide_______ I 5108-05-4— — —— -Vinyl Acetate______________I 1075-27-4---------Bromod ich lorome thane_______t 578-87-5 ——— — ——1,2-Dichloropropane________t510061-01-5 — — — cis-l,3-Dichloropropene____1579-01-6 ———————— Trich loroethene____________I 1124-48- l--------Dibromoch lorome thane_______I 579-00-5- —— — ——1,1,2-Tr ichloroe thane______I 571-43-2 ———— — — Benzene______________ 151UQ61-02-6 —— ——trans-l,3-Dichloropropene__I 575-25-2- ——— — --Bromoform__________________ I 5108-10-1 —————— -4-nethyl-2-Pentanone_______I 10591-78-6——————-2-Hexanone_________________I 10127-18-4- — - — --Tetrach loroethene.__________I 579-34-5-------—1,1,2,2-Tetrachloroethane__15108-88-3----- —— Toluene____________________'5106-90-7——- — --Chlorobenzene,______________15100-41-4- — — ---Etl-mlbenzene ___________I 5100-42-5- — -----Styrene_________________ I 51330-20-7-------Xy lene (total )____________15

FUKPI I

43

IAVOtATXXX OMAJIXCS AKAX.YSX4 DATA 0XXXT SAK9U NO.

Ub HaaaiLab Codo: _ caao No.:Matrix: (•oil/vatarl QJfrTEq.Sa»ple vt/vol: ^ (a/mL)Loval: (lov/mod) ton% Moisturoi net doe.Coluan: (paek/cap)

CAJ NO.

Totrahydrofuran

COXMUXD

Dilution Faetor:COWCtHTTUTION CHITS(uoyi or ug/Kai

(0

ram z VOA 1/17 »«v

44

ERA SAMPLE NO.IEVOLATILE ORGANICS ANALYSIS DATA SHEET


Lab Name:ETC Corp. I Laboratory Contract: 1_____

Lab Code: Case No.: SAS No.: SUb No.:

Mat r ix: isoi I/water ) WATER Lab Samp le lu:

Sample wt/vol: 5.0 Cg/mLJ ML Lab File ID: >D2595

Level: '.low/med) LOU)


Column: tpack/c«p) PACK


Date Received:

Date Analyzed: 01>-'13''91

D i l u t i o n Factor: 1.u

CONCENTRATION UNITS:lug/L or ug/KgJ UG/L


FURM I YQA-TIC

RT ES 1 . CUNC

1- 87

1

Q 1

iiIii

Iiiil

i

I,i

i,i

i

i

i;1,1

h <S •-.' ,

45


ERA SAMPLE NO.


Lab Code: Case No.:





Column: Cpack/cap) PACK

Cont pact:

SAS No.: SOG No.:


Lab File ID: >C2137

Date Received: 01/8 /91


Dilution Factop: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/KgJ UG/L

74-87-3-- —— - —— Ch lorome thane______________I 1074-83-9 ————— - — Bpomome thane_______________I 1075-01-4————————Uinyl Chloride_____________11075-00-3 — ————— Chlopoe thane______________11075-09-2 —————— --Methylene Chloride_________1567-64-1 ————— --Acetone__________________11075-15-0 ——————— Carbon Disulf ide__________1575-35-4———————I,l-Dichlopoethene________1575-34-3———————1,1-Dichloroethane________15540-59-0 —————— 1,2-Dichlopethene (total)__1567-66-3 ———————— Chloroform_________________15107-06-2 —————— 1,2-Dichloroe thane________1578-93-3 ———— — — 2-Butanone_______________11071-55-6 — -------1,1,1-Trich loroethane______1556-23-5- — — ——— Capbon Tet rach IOP ide_______15108-05-4——————"Jinyl Acetate_____________11075-27-4------- — Bpomod ich lo pome thane_______1578-87-5 — — ———— 1,2-Dichloropropane________1510061-01-5—— — -cis-l,3-Dich lopoppopene____1579-01-6-- ————— Tpichlopoethene___________1212 4-46-1-- — ----Dibpomoch lorome thane_______! 579-00-5————————1,1,2-Tr ich loroe thane______1571-43-2- — - ———— Benzene____________________1510061-02-6- — — -t rens-1,3-Dichlopoppopene__1575-25-2------- — BromoFopm__________________15108-10-1 — —— - — 4-Methyl-2-Pentanone_______I 10591-78-6 ——————— 2-Hexanone_________________I 10127-18-4—--- — -Tet pach IOPOC thene_________1279-34-5-- — — — -1,1,2,2-TetrachloPoethane__15108-88-3 ——————— Toluene____________________15108-90-7— — - — -Chiopobenzene_____________15100-41-4——————Ethylbenzene______________15100-42-5 ——————— Stypene____________________151330-20-7—————Xylene (total)___________15____ ____ ____ ________I__

IDIUIIIIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUuIUIUIUIUIUiUIU13IUIUIUIUIUIU

46

NaBOS.

Uto codas

LAVOlATItX OMANXCS ANALYSIS DATA

Contract:SAI He.i

CTA

CAM Mo.:Matrix: («oil/vator) Wrree.Saaplo vt/vol: S fg/mLi HTL

Uvol: (lev/mod)% Moisturoi not doe.Column: (pack/cap)

•08 Wo.I

Ud Saapla ID: GASCTU.mo 10:

CAS NO.

Totrahydrofuran,

COXPOUNOCONCOmUTION(ug/t or uq/Kai

NO.

Data Xocaivod: _i/»;<n^^^T*^"^^^™^^Data Analysod: i /n / t i

dilution Factor:

k>

rom x VOA 1/17 X«v

47

IEVOLATILE ORGAN ICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

ERA SAMPLE: NO.

Lab Name:ETCNJ

Lab Code : Case No.:

Matr i • : (soi1/water ? WATER

Samp le uit 'Vo 1 : 5.0 (. g/mL -1 ML

Leve1: <low/mod• LOW

^ Moisture: not dec.

Column: (pack.'cap) PACK


Con t rac t:

SAS Ho.: SDG :io. :

Lab Sample ID: CA5?Q4y

Lab File ID: .C2I77

Date Received: 01 % '91

Date Analyzed: U 1 ••'i 1-'9 1


CONCENTRATION UNITS:tug/L or ug/Kg? UG/L


FORH I UOA-TIC ^ Re-


Lab Name: ETCNJ

Lab Code: Case No.:

Matrix: Csoil/water) WATER





Cont ract:

SAS No.:

EPA SAMPLE NO.

I "IA5595I______________

'SDG Ho . :


Lab File ID: >C2138




CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

74-87-3- —— — — -Ch lorome thane______________I 1074-83-9- ——— — — Bromome thane_______________I 1075-01-4————————Uinyl Chloride_____________I 1075-00-3 — - — -- — Ch loroe thane_______________I 1075-09-2 —————— --Methylene Chloride_________1567-64-1- ——— — --Acetone__________________1475-15-0 ———————— Carbon Disulf ide___________1575-35-4————————1,1-Dich loroethene_________1575-34-3————————1,1-D ich loroe thane_________16540-59-0———————1,2-Dichlorethene (total )__18467-66-3 ———————— Chloroform_________________15107-06-2———————1,2-Dich loroethene_________1578-93-3 ———————— 2-Butenone_________________I 1071-55-6- ————— —1,1,1-Tr ich loroe thane______1356-23-5 ———— — — Carbon Tet rach lor ide_______15108-05-4———————Vinyl Acetate______________I 1075-27-4---- — ---Bromod ich lorome thane_______I 578-87-5----- — — 1,2-Dichloropropane________1510061-01-5- — — -cia-l,3-Dich loropropene____I 579-01-6---—— — — Tr ich loroethene____________174124-48-l--------Dibromoch lorome thane_______ I 579-00-5——— ———— 1,1,2-Tr ich loroe thane______1571-43-2- — — ----Benzene____________________1510061-02-6- — ---tran»-l,3-Dichloropropene__1575-25-2---------Bromo form__________________15108-10-1 ——————— 4-Methyl-2-Pentanone_______I 10591-78-6 ——————— 2-Hexanone_________________I 10127-18-4--------Tet rach loroethene__________1879-34-5- ——————— 1 ,1 ,2,2-Tet rach loroe thane__15108-88-3 ———— —— Toluene____________________15108-90-7— — — --Chlorobenzene______________15100-41-4———————Ethyl benzene_______________15100-42-5 ——————— Styrene____________________151330-20-7——————Xylene (total )____________15

IUIUIUIUIUIJIUIUIIIUIUIUUIUIUIUIUIUIIUIUIUIUIUIUIUIIUIUIUIUIU!UI 49

1AVOLATZtt OMAITZCS AXALYSZJ DATA IttTT t»A SAKPU NO.

sreeodot

Matrix:Saapla vt/vol:Uvol: (lev/sod)% Moisturo: not doe.Coluan: (pacX/eap)

CAS HO.

,(9/«t»

COMPOUND

ID:

rilo ID:

Data Koeoivodt ifvfutData Analyiad: tlnki

dilution Factor: ICOHCtHTKATION(U»/t or ut/K<l

Totrahydrofuran

1/17

50

IEVOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIUELY IDENTIFIED COMPOUNDS

EPA SAMPLE

Lab Name:ETCN3

Lab Code: Case No. :

M a t r - . - ' : (30 : I - ' w a t e r ) LJATER

S a m p l e w t - ' v o l : ? . 0 ' g - 'mD M L

Lev* 1 : !. 1 ow/med LOW


Columr: Cpack^cap) PACK

Num&er TICs found: 0

Cont rac t:

SAS No.: 3DG ho.:

Lab Sample ID: CA5S95Y

Lab Fi le ID: <C2138

Date Received: 01 8 '91

Date Analyzed: 0 l--'i2 --'9 1

D i l u t i o n Factor: 1

CONCENTRATION UNITS:Cug/L or ug/Kg< UG/'L

1 !! CAS NUMBER 1 COMPOUND NAMEi................ |............................

1 1: 1: 1: 1! |

1' 1

11I111I11I1111

1 11

! 1I 1i 11 11 11 11 11 1

FORM I UQA-TIC

i iRT i EST. CONC i 0

........ i-. ........... {.....1 !1 I1 !1 !1 11 11 I1 1i ;i i! 1i i1 !1 1i !1 11 i! 1I !1 1i |! 1i I1 I1 1I I1 11 1i :I i! t

1X37 Rev.51

UOLWTILE ORGANICS ANALYSIS DATA SHEETEHA SHMPLE NO

Lab Name: ETC Corp.

Lab Code: Case No.:

riatnx: Csoil/water) WA'IER

Sample wt/vol: 2.5 tg/mLJ ML

Level: ( low/med) LOW


Column: (.pack/cap) HACK

Cont ract:

SAS No.:

1A5596I________

SL'li No . :

Lab Sample 10: CH-?596V

Lab Fi le ID: >D'J596

Date Received:

Date Analyzed: 0


CAS NO. COMPOUNDCONCENTRATION ONUS:tug/L or ug/Kg) U&/L

74-87-3 ------74-83-9 ------75-01-4 —— ——75-00-3 —— ——75-09-2 —— ——67-64-1 —————75-15-0 ------75-35-4 —————75-34-3 —————540-59-0 -----67-66-3 -----107-06-2 ————78-93-3 —— ——71-55-6 —— ——56-23-5 —————108-05-4 —— —75-27-4 —— ——78-87-5 —————10061-01-5 ——79-01-6 -----124-48-1 — — -79-00-5 ----- -71-43-2 ------10061-02-6---75-25-2 -----108-10-1 -----591-78-6 -----127-18-4 —— —79-34-5 ——— --108-88-3 -----108-90-7--- —

100-42-5- ----1330-20-7 ———

---Chloro me thane---Bromome thane---V-Unvl Chloride---Chloroethana---Me thvlene Ch lor ide---Acetone- — Carbon Diaulfide---1 .1-0 ich loroethene---1 .1-Dich loroe thane- — 1,2-Dichlorethene t total J __---Ch lorof orm---1 ,2-D ich loroe thane---2-But anone---1 .1 .1-Trichloroethane---Carbon Tetrachlnride— -vinyl Acetate---Bra mod ich loro me thane---1 .2-Dichlnronronane---c is-1 , 3-D ich 1 oropropene-- -Trichloroethene---Dibromoeh loromethane---1 . 1 .2-Tr ichloroetnane---Benzene ,---trans-1 , 3-D ich I oropropene---Bromoform___4-nathvl-2-PBntanane---2-Hexanone---Tatrachloroatnene---1 , 1 , 2, 2-Tetrach loroe thane---To luene---Chlorobenzene---Ethvl benzene---St vrene——— Xylene t tota 1 J

2020202010111010108101020101U20101010

1010101U1UJO2041U1010101U10

uouuoJO 1oU 1JU 1uO 10o ioO 1oO 1

U 1U :U 1uuuU IJU IU iu tuU 1u

1

FORM I VOA 1/8

52

NaBOl

Lab Codoi

1AVOXATZXX onoANzes AXAX.YSZS DATA svzrr

ere

NO.

caao NO.:Matrix: (aoil/vator) jujgg,Staple vt/vol: AS fq/MLl nr

Uval: (lov/aod) 6Qta% Meisturot not doe.Column: (pack/cap)

CAS KO. COMMUNO

'•Dilution Factor: _ACOHCOmUTIOK UWITS;(uff/t or uf/Kgj

Totrmhydrofuran O

Fom x VOA 1/17 ft«v,

53

IE EHA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET ______________

TENTATIVELY IDENTIFIED COMPOUNDS I

Lab Name:ETC Corp. I Laboratory Contract: I __________


Matrix: I so i 1 /wa t er ) WATER

Sample wt/vol: 2.5

Level : I low/rned) LGUI

N Moisture: not dec.

Column: (.pack/cap) PHCK


Lab Samp le ID: CM'7596V

Cg/mLJ ML Lab File ID:

Date ftecewed:

Date Analyzed:

D i l u t i o n r a c t o r

CUNCENTRRTIQN UNITS:tug/L or ug/Kg) UG/L

CRS NUMBER COMPOUND NftME

FURM I UOA-T1C

RT ES 1 . CUNC

f

1--37

iQ 1

iii

1

1

1

1

j

1

!

1I1i1!

1

1

I,

1;1i

Ii

1

Kev.

54

1AUOLATILE ORGAN ICS ANALYSIS DATA SHEET

EPA SAMPLE NO.

IIA5602

Lab Name: ETC Corp.

Lab Code: Case No.:

Mat r ix : (soi 1/water) WATER

Sample wt/Vol: 5.0 (g/mL) ML

Level: Uow/med) LOW



Con t rac t

SAS No. SDG No.:

Lab Sample ID: CA56Q2U4

Lab File ID: >D2584

Date Received:

CrtS NO. COMPOUND


Di 1 u t ion Fac tor: 1

CONCENTRATION UNITS:<ug/L or ug/Kg) UG/L Q

74-87-3 ------74-83-9 — - ——75-01-4 -- — —75-00-3 — — —75-09-2 ------67-64-1 ------7?-15-0 —— ——75-35-4 —————75-34-3 —— ——540-59-0 — ---67-66-3 ------107-06-2 -----78-93-3 ------71-55-6 —————56-23-5 ----- -108-05-4 -----75-27-4 —————78-87-5 ------10061-01-5 ——79-01-6 —— ——124-48-1 ————79 cio-5 -----••1-43-2 -----10061-02-6 ——75-25-2 —— ——108-10-1- ———591-78-6-----127-18-4 ——— -79-34-5 ———— -108-88-3 -----108-90-7 —— --100-41-4 -----100-42-5 -----1330-20-7- ——

1---Chloro me thane 1---Bromome thane 1---YinulChloride !---Ch loroe thane 1---Methylene Chloride 1---Acetone , , , 1—— Carbon Disulfide 1— -1.1-Dichloroethene 1— -1,1-DichloroethanB 1—— 1,2-Dichlorethene Ctotal ) __ 1---Chloroform . 1— -1.2-Dichloroethane 1---2-Butanone t---1.1.1-Trichloroethane 1---Carbon Tetrachlaride 1- — Uinul Acetate 1---Bromod ichloro me thane 1— -1.2-DichloroDraoane 1---cis-l,3-Dich loropropene ____ 1---Tr ich loroe thene , , .._ 1---Dihrnmnehloro me thane 1---1,1.2-Triehloroathane 1---Benzene . iirai<i 1---trans-1 ,3-Dich loropropene __ I---Bromo form 1___4-Methyl-2-PcntanQnc .„ ,„.,.!---2-Hexanone , „., 1---Tat rach loroe thane , 1---1,1,2,2-Tet rach loroe thane __ 1---Toluene i i i i n i _ I---Chlorobenzene 1---Et hylbenzene 1---St yrane 1---Xvjlene ( tota 1 ) 1

1

FORM I UOA

1010101041055555510551055555555510105555555

1IUIUIUIUIJIUIUIUIUIUIUIUIUIUIUIUIUIUIUiUIUIUIUIUIUIUi.uIUIUIUIUIUIUIU1

551/87 Rev.

1AVOLATZU OK6AJIZCS ANALYSIS DATA «ttTT CVA SAK9U NO.

Na»o:_ era dot*Lab Codo: Caao No.:Matrix: (•oil/vatariSaaplo vt/vel: S fa/mil ffu.Lavol: (lov/aod) ion% Moisturo: not doc.Column: (pack/ cap)

CAS NO. COMPOUND

Totrahydrofuran.

'•Dilution Factor:CONCZMTRATZON OHZTS

or

10

rem z VOA 1/17

56

IEOOLATILE ORGAN ICS ANALYSIS DATA SHEET



Lab Code: Case No.:

M a t r i x : ^soil/water) WATER

Sample wt/vol: 5.0 Ig/mL) ML

Level: clow/med) LQU




Con t rac t:

SAS No.:

EPA SAMPLE NO.

IA5602I

SDG No.:

Lab Sample ID:

Lab File ID: >D2584

Date Received: i/ujO'

Date Analyzed: 01/l?'9l

D i l u t i o n Factor: 1. Cl


CAS NUMBER

01 . 1066-40-6

COMPOUND NAME

Silanol, trimethyl-

RT

16.24

EST. CONC

17

Q

J

FORM I UOA-TIC 1---87 Rev.

57

1AUOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: ETCNJ

Lab Code: Case No.:

M a t r i x : (soil/water) WATER

Sample wt/vol: 5.0 (gXmL) ML

Leve1: (1ow/med > LQU



Cont rac t:

SAS No.:

ERA SAMPLE NO.

IIA56Q3I______________

SDG No.:

Lab Sample ID: CA56Q3U

Lab File ID: ,C2136

Date Renewed: QlxSx91

Date Analyzed: 01x11x91

Dilution Factor: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:CugXL or ugXKg) UGxL

I 74-87-?---- —— --Chlorome thane______________I 10I 74-83-9- — — — --Bromome thane_______________I 10I 75-01-4————————Uinyl Chloride_____________1101 75-00-3 ———————— Chlo roe thane_______________I 10I 75-09-2 —————— --Methylene Chloride_________15I 67-64-1 — -- — ---Acetone____________________15I 75-15-Q---------Carbon Disulf ide___________15I 75-35-4--- — — —1 ,1-Dich loroethene_________15I 75-34-3————————1 ,1-Dich loroethane_________151 540-59-0---——--1,2-Dichlorethene (total)__15I 67-66-3--- — - — -Chloroform_________________15i 107-06-2- ——— —— 1,2-Oich I o roe thane________15I 78-93-3-- — --- — 2-Butanone_________________1 101 71-55-6- — - ——— -1 ,1,1-Trichlo roe thane______151 56-23-5------- — Carbon Tet rach lor ide_______15i 108-05-4———————Uinyl Acetate______________110i 75-27-4-- —— ——— Bromodichlorome thane_______151 ^8-87-5----—— --1,2-Dich loropropane________15i 10061-01-5-- —— -cis-1,3-Dichloropropene____15; ^9_Qi-6---------Trich loroe thene____________I 5i 12^-48-1--—— ---Dibromochlorome thane_______1579-00-5--- —— -—1 ,1,2-Tr ich 1 o roe thane______15

i 71-A3-2---------Benzene____________________15! 1006l-02-6------trans-l,3-Dichloropropene__I 5I 7q.25-2---------Bromof orm__________________151 108-10-l--------4-Methyl-2-Pentanone_______I 10I 591-78-6- —————— 2-Hexanone_________________1 10I 127-18-4----- — -Tetrach loroe thene__________15I 79-34-5---------1.1,2,2-Tetrach loroethane__15I 109-88-3 —— ———— Toluene____________________15I 108-90-7—--- — -Ch lorobenzene______________15I 100-41-4———————Ethyl benzene_______________15I 100-42-5 ——————— Styrene____________________15I 1330-20-7——————Xylene (total )____________15I ___. ... ___________.______________________!__

IU1UIUIUIUIJIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUI 58

*•••

1AVOLATZXX OMANZCS AMA1.YSZS DATA flBXT

Contract:

CTA tAKfL£ NO.

Cotei CM* NO.:Matrix: (aoU/vatorl 60ATBESasplo vt/vol:Lovtl: (low/Bad) ten% Moiaturot not doc.,Column: (pack/cap)

CU NO. COMPOUND

Totrahydrofuran

1AJ NO.: _

Saaplo ZO:rilo ZO:

Data Itocoivod:Data Analysed: _ilnkt^«.

SOllutlon Factor: iCONCZNTXATZON CHWJ:(U»/t or ug/Mi Mfl/L

rom z VOA 1/17 K«v

59



ERA SAMPLE NO.

A56Q?Lab Name:ETCNJ

Lab Code: Case No.:

Matrix: Isoil/water) WATER

Sample wt/vol: 5.0 (.g-'mL) ML

Leve 1 : C low/med) LOU1


Co lumn : I pack /cap ') PACK


Cont ract :

3AS No.: SDG No.:


Lab Tile ID: -C2176

Date Received: Ol/S/91



CONCENTRATION UNITS:Cug/L or ug/Kg; UG/L

I! CAS NUMBER .

01. 1066-40-6

i

COMPOUND NAME

Silanol, trimethyl-

RT

15.60

.

EST. CONC

13

tQ I

J ]1iI!

1

,

1

!11Ii1;i

iii;1|1!I

Ii

1

FORM I UOA-TIC 1/87 Re-.-.60



Lab Code: Case No.: SAS No.: SDG No

1 EPA1 SAMPLE NO.

O i l UBLK01021 A555403 I A5554MS041 A5554MSD051 A5556061 A5547071 A5548061 A5549091 A5550101 A5553111 A5555121 A5557131 A5558141 UBLK02151 A5562161 A5564171 A5569181 A556Q19 1 A5561 ^201 UBLKOY'.taW211 A5562 **221 A5570231 A5573241 A560225 1 A557526 t vfcucoa271 ATT7t2 B I2913 Q I

SIiTOLi*

9898999898991011009998100100999910099

10010099

i 100100102100101101«/?*

S2IBFB)*

9898959594958990898989889098969697979799979997989511*b

S3IDCE)*

1041049810499106927776 X95/ffM98949098939797971128886991029688100101

OTHER

*/*'

TOTOUT

00000000*o0000000000000000oo

page 1 of

51 (TOD - Toiuen«-d852 CBFS) • Bromofluorobenzene53 CDCE) • l,2-Dichloroethane-d4

QC LIMITS(88-110)(86-115)(76-114)

t Column to be used to flag* Values outsida QC l i m i t sD Surrogates diluted out

FORM I I

recovery values

- 161

1x87 Rev.

Lab Name: ETCNJ

Lab Code:

2AUATER VOLATILE SURROGATE RECOVERY

Contract:

Case No.: SAS No.: SDG No

t EPA1 SAMPLE NO.

Oil UBLK01021 A996303 1 A9974041 A9999091 A998Q061 A9981071 A998208 1 A96Q309 1 A9994101 A9999111 UBLK02121 A980913 1 A999914 t A980*191 A9991161 A9B09W171 A9806AElet A999m19 1 UBLK0320) A9999MS211 A9999MSD2212312412912612712BI29 t301

SI(TOD*

100989899102979696981071077876847977787898109128 •

..

52CBFB1*

999799100999796989910610778768479767678110117144

S3COCE)*

97989710197989910097989392939491909291969694

OTHER TOTOUT

000000000002222222012

page 1 of

51 CTOL) - Tolu«na-d852 CBFB) • Bromofluorobanzena53 COCE) • l,2-Dichloroathana-d4

t Column to ba u»ad to flag* Ualuas outmida QC limit*D Surrogataa diluted out

QC LIMITS(88-110)(86-119)(76-114)

recovery value*

FORM II UOA -1 1X87 Rev.62

2AWATER VOLATILE SURROGATE RELOYERY


Lab Code: Case No.: Snb No.: SUb No

01QvU30405060708U910il121314151617la192o212223242526272B293U

EPAbAHPLE NO.

U6LK01Ab577rtt't-a?586

Al;>*87A5596A5571A5583A-i^SAA^>589A5*93UBLKQ2A5S78Ac.-579A^-?90A^^SAc'792UBLKO.''A5577A^572A5572I-1SA'? 72nSDM(T'1?63(t£rA5588A5'?92I£-Ac'797

Si( TGL J #

V61001U197V79fc97979796969b9898989o98989797

1UO1009996974b *

S2t8FB.i*

iuo99991001019999999998989999999 fl9998

IUO1019899979898*6106

S3tDCEJ*

9036919291909111311291109100105102113128 •125 *100114101112128 »120 •99123 *3 *

or HE* TOT iGUTi

0 :

0 10 >0 10 i0 I0 i0 io .0 t0 i0 i0 i0 101 11 10 10 i0 10 i1 11 .0 11 I2 1

!

1i1

a o. e 1 of

SI (TGD • Toluene-d8Si (8KB) « BromotluorobenzeneS3 ' L'LE J - 1.2-Dichloroetnane-d4

# Column to be used to flaa recovery» Ualues outside QC l i m i t sD Surroaates d i l u t e d out

FOHfl I 1 UOA -1

UC L * n I T •='. a a - 110 .'< B 6 -11 TO1.76-114 •

l-'«7 Re'.-.

63


Lab Name: ETCNJ

Lab Code:

Con tract :

Case No.:

1 ERA1 SAMPLE NO.

01- yBLKQ\||02! -i?59-16yipito07 13 4 105 10 6 10710 8 109 1101ill12 11? 11411? 116117113119 12 0 121122 I2? !2412? 126127 128!09 |

7 0 1

SI . 32 37 OTHER < ~QT !( TQL , # ! '- BFB > # 1 I DCE ) * ! i OUT i»»*»».!».. = .. \mmmmmm\mmmmmm\mmm\

107 ! 1 n 7 i 93 ! i 0 i» 7b * 1 77 * | 33 . 12;

i ! i 1 1! i : ii i i 1 11 1 ' ! !i i ; ! i1 ! ! 1 11 ! 1 i 11 ! ! i 11 1 ! ; 11 i ' : i! 1 1 i 1i 1 ! ! :1 1 ! ! !i I , i :1 1 1 i I1 ' 1 i ;1 1 i : !! ! ! i1 1 ! I t1 1 ! i1 1 1 : !! ! i . ii ! 1 i 11 ! : i! 1 !! ! ! '•1 1 i !

! : :

page 1 c*

El '. TQ_ - Toluene-dE32 '.BFB,1 * Bromo f 1 UQ robenzane'EJ 'DCE '- - 1,2-Dichloroethane-d-.

Ht Column to be used t •-• Mag -eco* Va1ues outside QC 1 i m i t iD Surrogates d i l u t e d out

FORh :I VGA -.

35-11036-11?76-114

a 1 ue =

64

3AWATER UOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOUERY


Lab Code: Case No.: SAS No.: SOb No.:

Matrix Soike - EPA Samole No.: A5554

COMPOUND

1 .1-Dichlo roe thaneTr ich loroetheneBenzene.,To 1 ueneCh lo robenzene

SPIKEADDED(ug/L)

50.00090.00090.00090.00090.000

SAMPLECONCENTRATION

tug/Li

0.0000.0000.0000.0001.044

MSCONCENTRATION

Cuo/L).............

41.68744.71743.74143.21244.847

MS%PEC

9?89878688

1 QC1 LIMITS

* i REG .

161-14?171-120176-127176-129175-1301

COMPOUND

I .1-D ich loroetheneTr ieh loroetheneBenzeneTO lueneCh lorobenzene

SPIKEADDED(ug/L)

90.00050.00090.00090.00050.000

MSDCONCENTRATION

Cug/L)

38.27944.83244.35643.83845.137

MSD\

REC *

7790898888

SRPD #

90111

QC LRPD

1414111313

iIMITS 1

REC. •

61-1*45 ;

71-120 i76-127176-125 i75-170 i

i

Column to be used to flag recovery and RPD values with an asterisk

'.'a lues outside of l i m i t s!D: 0 out of 5 outside limits;;ke Recovery: 0 out of 10 outside l i m i t s

FORM I I I UOA -1 1x87 Re--.

65

3ftUHfER DGLftTILE HA IK IX SPlKE/flfti RlX SPIKE DUPLICATE

Lab Name• ETC Corp. I Laboratory Contract:

Lab Code: Case No.: SAb No.: Sui= No.:

Hatrix Spike - EPA Sample No.: A5572

LQMPGUND

1.1-DichloroetheneTrichloroetheneBenzene „.„.„,.„To lueneCh lorobenzene

SPIKEADDEDtug/L)

50. UUO5U. OOU50. UUU5U.OOU50. UUU

SttHPLELUNCENTKAflUN

Cug/L)

U. UUOG. UUU8.^080. UUU0. UUO

nsCUNCENVftHl ION

tug/LJ

45.-J6342.61V47.JJ-J54^i.45b44. b!5

ns%

KEL #

9185/885yfl

JCL i n l T b i

r-iC . i

61-145 •71- 12 u I/6-12776-121? l-"?-l3U i

i

CGHPOUND

1 fl-DichlorcietheneTr ich loroe thaneBenzeneTo luene , ,Ch lorobenzene

SPIKEADDEDtug/LJ

5U. OOU50. UUU5U. OOU50. OUU5U.OOU

MbDCQNCENTRAl I UN

Cug/LJ

42.74238.tilU44. 06740. U3941.696

HbD 1

RtL *1 RPD *

85 1 6>'6 1 V72 * t 9au i 683 1 7

UC LRPU

1414111313

n, ShtL.

6.-14'• 1 - 1 2 UTc-li.1

/ft- :2*7"- -l?u

Co 1 umn to be used to flag recovery and RPD values with an asterisk

Da lues outside of l i m i t s

0 out of 5 outside l i m i t sRecovery: 1 out of 1U outside l i m i t s

Lommen t s:

11 I DGR -1

66

3AWATER VOLATILE MATRIX SPIKE'MATSIX SPIKE DUPLICATE RECOVERY


Lab Code: Case Ho.: SAS No.: SDG Mo.:

M a t r i x Spike - EPrt Sample No.: A5599

COMPOUND

I tl-Dicr.laroeth«neTriehloroetheneBenzeneTo luaneCh lorobenzane

SPIKEADDEDlug/L>

50.00090.00090.00050.00050.000

1 SAMPLE(CONCENTRATION1 (ug/L)

1 O.QOQ1 39.0671 0.000I 0.0001 0.0001

MS 1CONCENTRATION I

tug/L) I

49 . 764 I101.272 145.558 I56.973 19.432 1

t

MS\REC

100249111419

QC: LIMITS

Ml REC.

161-145'171-120176-127126-125

•175-1301

COMPOUND

1 .1-DichloroetheneTr ich loroe theneBenzeneT^ lueneCh lopnbenzftne „ imm

SPIKEADDED(ug/L)

50.00050.00050.00050.00050.000

1 MSD1 CONCENTRAT I ON1 (ug/L)

1 45.4171 99.7571 45.419I 65.1?01 49.348I

MSD 1% 1

REC #1

91 121 •!91 ;

130 -I99 !

%RPD ft

9130

13136 »

1QC LIMITS 1=>PD : REC. '

14 .61-145114 171-120111 176-127113 176-125113 '.75-1301

1 1

Column to be used to flag recovery and.RPD values with an asterisk

Values outside of limits

°0: 1 out of 5 outside limits2ii-» Recovery: 4 out of 10 outside l i m i t s

ommen t s:

FORM III VOA -1 1/87 Rev

67

4AVOLATILE METHOD BLANK SUMMARY

Lab Nam*: ETCNJ

Lab Code: Case No.

Lat rile ID1 »C2124


Matri,-,: ( so i I -'wa t er .' WATER

instrument ID: GC/MS C

Con t rac t:

SAS Mo.: SDG Mo.:

Lab Sample 10: U8LX01

Time Analyzed: 1704

Leve1:tlow/med) LOW

THIS METHOD BLANK APPLIES TO THE FOLLOUING SAMPLES, MS AND MSD:

Zommen t s:

Dage 1 of

0102030405060708091011121?141516171819202122232425269-7282930

EPASAMPLE NO.

A5563A5574A5559A5580A5581A5582A5603 ..A5594rt5595

—

LABSAMPLE ID

CA5563VCA5574IJCA5559IJCA5580yCA55810CA5582UCA5603UCA5594WCA5595U

LABFILE ID

>C2125>C2126>C2127>C2133>C2134>C2135>C2136>C2137>C2138

TIMEANALYZED

141015001549201221002149223723250014

FORM I'J 1/87 Pev.

68


Lab Name: ETCNJ

Lab Code: Case No.:

Lab File ID: -C2136


M a t r i x : '. *o i 1 /ua t e r ) U1ATER

Instrument ID: GC-'MS C

THIS METHOD BLANK APPLIES TO THE FOLLOUIING SAMPLES, MS AND MSD:

Cont ract:

SAS Mo. : SDG rto . :

Lab Sample ID: VBLKQ2

Time Analyzed: 1237

Leve I : '. low/mod ,' LOW

_omments'

aage

1 ERA1 SAMPLE NO.

01 A5805021 H559903 i A5806041 H559105 i A58Q5K6061 A5806*t07: A5591H&-.08109110111112113114115 116117118119120121122123124125 !26 1 —271281291301

LABSAMPLE ID

CA58051J2CA5599U2CA5806U2CA5591Y2CA5805U2CA5806U2CA559HJ2

-

LABFILE ID

>C2197•'C2188>C2190>C2191>C2192>C2196>C2197

TIMEANALYZED

1336142415581646174720582146

,.

FORM iJOA 1./87 Re'.-.69

4A'JOLATILE METHOD BLANK

L-sb Mam*: ETCNJ Cent r a r t :

_ab Code : Case No. : 3AS :.o . :

Lat ~i > 1C: >C21Sb

jat* Analyzed 01/I3V91

Ma • r i -. : '. s o i 1 -'wa t « r WATEF

I ns t r umen t ID: 3C/T1S C

'HIS METHOD ELANf- APPLIES TO T-<E FOLLOWING SAMPLES, MS AND

Lab Samp!* 11 : '.'BLKOX/I

T i m e nnaiyzed: 1277

Leve 1 : t low 'med ,- LOU

EPh LuB IME !i SAMPLE NO.

01 1 5597802:07 !0- 1D5 106!a •? i08 i09 110 !I l l12 l17 !i •i1? 1i o lI"7 1ie i19 120!21 122 1:? i24 I25 1

SAMPLE : 0 : ~ I LE 1 D i M.' iAL': ZED............. ........... .... !.«......,.CA5597U2 i C218« 1 l?li

1 1t !! 1i :! I1 I! !1 1i 11 !1i ii ;1! 1; ;1 '1 1i i! !

1 !

1

-ORM :

70

u'•'•ad iB.- won

M

3UI1

91

c: 31 1 01 3'duys ON

3H1 01 S

at

£3

13Oc6TBT

9T

"III016330iO90aO

£0

TO

:QI

HD~ .' PSUJ/-.OI j : ; s^*n

93? * : parr', 5 u^ *'jj i

10 i~afi -"I s

T6.-6T--TC

: 'OH

it QOH13U 3"iiWf

UOLATILE METHOD BLANK SUMMARY

Lab Nam«: ETC Corp.

Lab Code: Case No.:

Lab File ID: >D2534

Date rtnaIvzed 01x09x91

M a t r i x : '. so i 1 --'wa ter ) LJwTER

Instrument ID: GCxMS D

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES. MS AND MSO:

Cont rac t :

SAS No . : SDG No, :

Lab Sample ID: UBLKQ1

Time nnalvzed: 1716

Leve 1 : t lowXmed 't LQLJ

t s:

111

O i l02103104105106 107108109110111112113114115116117118119120121122127124125126 I27128 129 170!

ERASAMPLE NO.

A5554A5554MSA5554MSOA5556A5547A5548A5549H5550A5553A5555A5557A5559

LABSAMPLE ID

CA5554UCA5554USCA5554URCA5556UCA5547UCA5548UCA5549UCA5550UCA5553UCA5555UCA5557UCA5558U

LABFILE ID

>D2536>D2537>D2538>02539> 02 5 40>D2541>D2542>D2543>D2544>D2545>D2546>D2547

TIMEANALYSED

182519101953203721202203224723310015005701410225

FORM IU UOA 1x8

72


Lab Name: ETC Corp.

Lab Code: Case No.:

Lab F i l e ID: >D2550


Matri x : Csoil/uater) WATER

Instrument ID: GC/MS D

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD:

Cont ract:

SAS No.: SDG No.:

Lab Sample ID: UBLK02

Time Analyzed: 1054

1 : ( lou/med ) LQUJ

Comment s:

01020304050607080910111213141516171819202122232425?f>2728293G

EPASAMPLE NO.

A5562A5564A5569A5560A5561

LHBSAMPLE ID

CA5562V2CA5564U2CA5569U2CA5560U2CA556102

LABFILE ID

>D2553>D2556>D2557>D2562>D2563

TIMEANALYZED

13551614171921142202

page 1 of _(_FORM IJOA 1/87 Re"73

4AVOLATILE METHOD BL«NK SUMMARY

Lab Name: ETC Corp.

Lab Code: Case No.:

Lab F t l e ID: >D2571





Cont ract :

SAS No.: SDG No.:

Lab Sample ID: UBLKQ3

Time Analyzed: 1803

Leva 1 : ( low/med ) LGUi

01020304050607OB09101112131415161716192021??2324252627282930

EPASAMPLE NO.

A5576

LABSAMPLE ID

CA5576Y3

LABFILE ID

>D2577

TIMEANALYZED

2248

Commen t s:

page 1 ofFORM IU UOA 1/97 Rev

74


Lab Name: ETC Corp.

Lab Code: Case No.:





THIS METHOD BLANK APPLIES TO THE FOLLOW ING SAMPLES, MS AND MSD:

Con t rac t:

SAS No.: SDG No.:

Lab Sample ID: U8LKOXt*

Time Analyzed: 1302

Leva 1: t1ow/med) LOW

1 EPA1 SAMPLE NO.

Oil A5562021 A5570031 A5573041 A5602051 A5575Q6 \071L)9I09110111 112113114115116 117119!19120121122123124125126 127128 1291301

LABSAMPLE ID

CA556204CA5570W4CA5573U4CA5602U4CA5575U4

LABFILE ID

>D2581>D2582>D2583>D2584>D2585

TIMEANALYZED

13591446153316201706

Comment s:

page 1 of [FORM UOA 1/87 Rev

YOLftTlLE METHOD BLANK SUnMHRY

Lab Name: ETC Corp,

Lab Code: Case No.:

Lab File ID: >02590


Matr ix: Isoi 1/water) UAIER

Instrument ID: GL/Mb D

THIS nElHOD BLANK APPLIES TO I HE FULLOW1N£ b

Cont ract:

SAS No.: SUb No.:

Lab Sample ID;

Time Analyzed:

Leve 1 : t 1 ow/med J

fib AND

Commen t s:

page 1 ofFORH

010203U405U607USOv101112114I1?16l/>18ly202i22232421?262/Jd2v30

t-KttSHHPLE NO.

A1?1???A^585Ab586rt^^>87W^?596«5571Ht"?83ft1?1?^Ht>t»8VH-7^93

LHBSAMPLE ID

CH55770Cft5585"JCH-p^SbiJCA5(?b7UCA5596ULH557iyCH'?583'JC«55b4^Ctt"?589iJLW55V3U

LHBFILE ID

>D'^591> 025*3> 0*594>D2-?y5>D'^596>D2^97>D'^599>026UO>D*601>D26U2

TT:£ ittNHLYZEU 1

2042 1*216 i23U3 1234^ iOU>7 10123 iO*1?.? 1U344 i04>1 1051? i

I,ti1i

1!

1;IiI

I

li

1t

;/ Rev.

76

4AVOLATILE HE!HOD BLANK SOMHAKY

Lab Name: ETC Corp.

Lab Code: Case No.:

Lab File ID: >D2606


Hatrix: tsoil/water) WH I ER


THIS rtElHOD BLANK APPLIES TO I HE FULLQUING bAflKLES, tlb AND HSD:

Con t ract:

SAb No.: SUb No.:

Lab bample ID:

Time Analyzed: 12U/

Leve1:(low/med'

Commen t s:

01U203UAO1?U6a/08091011121>141*161^181920212223242TJ6•7??fl7930

tKASAHPLE NO.

A1?1? 78A)?(?79A-?^90Ac'368A-7592

LHtiSAHHLt ID

CA'?^7b'J2LA55/9V2Cft!?59UV2Cft556UV2CA-?992V2

LM6FILE ID

>D2610> 02 6 12>D2614>U26i5>D2616

Tl:-i£ IANALYSED 1

15^6 116^^ 11U26 11911 11956 1

\\,\\

\I1\1(

111;

I

1

11111\

page 1 of _\_FURH IV VOA Rev.

77

UQLHTILE HETHOU BLHNK

Lab Name: ETC Corp.

Lab Code: Case No.:

Lab Fi Le 10: >D^621

Date Analyzed 01x15/91

Matrix: Isoi 1/water) WttIER

Instrument ID: GL/tlb D

THIS HE I HOD BLttNK rtPPLltS TO I HE t-ULLOWlNG bUHPLtS, rib HNU HSD

Contract :

S«b No . : Sub No . :

Lab Samp le iD: '

Time ttnalyzed:

Leve 1: (. low/med )

Common t 5:

page 1 of

01U20304Q^>u607080910111213141*161?18IV2021222?24252627282yJU

tHASflHPLE ND.

r S77tt-9572A5'?72nS«5572nbDA^566REft^^SSA«?592RE-

LMBSHHPLE ID

CH5577W3L«5572"J3Cfl5572USLfl557^"JRCH'?56ay3Ltt55tiaiJ3CH5592U3

LrtBFILE ID

>D2622>D2624>D2625>D2626>D2627>D2628>D262V

Tl -E iHNHLYZtU 1

16U9 1174V ilb>6 11922 120U7 120512137 1

I\

1;

1;111

1|

1

1

1i1

1i

FUKM I"J OOW

78


EPA SAMPLE NO

UBLKQ1Lab Name: ETC Corp.

Lab Code : Case No.:

M a t r i x : <soi1/water) WATER


Leve1: tlow/med) LOW



Cont rac t

SAS No.

CrtS NO. COMPOUND

SDG No.:

Lab Sample 10: QC7Q442U

Lab File ID: >D2534

Date Received: 91104/41




I74-97-3- —— —— — Chl or ome thane_____________11074-83-9- ———— — Bromome thane______________I 1075-01-4———————Uinyl Chloride____________11075-00-3- —— ——— -Chloroe thane_______________I 1075-09-2 ———————— Methylene Chloride_________1367-64-1- —— —— --Acetone____________________I 1075-15-0 ——————— Carbon Disulfide__________1575-35-4— — —— --1,1-Dichloroethene________1575-34-3 ———————— 1,1-01 chloroe thane_________15540-59-0 —————— 1,2-Dichlorethene (total )__1567-66-3 ———————— Chloroform_________________15107-06-2- — —— —1,2-Dichloroethane_________1578-93-3 ——————— 2-Butanone_______________11071-55-6 ———————— 1,1,1-Tn chloroe thane______I 556-23-5 ——— — —— Carbon Tetrachlor ide_______15108-05-4——————Uinyl Acetate_____________11075-27-4---------Bromod ich lorome thane_______1578-87-5- —————— -1,2-Dich loropropane________1510061-01-5 ———— -cim-1,3-Dich1oropropene____15^9-01-6 ——————— Trichloroethene___________15124-48-1--- — — -Dibromoch lorome thane_______I 579-00-5 ——————— 1,1,2-Trich loroethane______1571-43-2 ——————— Benzene__________________1510061-02-6—————t rans-1, 3-Dich loropropene__1575-25-2- ——— - — -Bromof orm__________________15i OB-10-1- — - — --4-Methyl-2-Pentanone_______ I 10591-78-6 ——————— 2-Hexanone_________________I 10127-18-4--- — — -Tetrachloroethene__________1579-34-5- — - — ——1,1,2,2-Tetrachloroethane__15108-88-3 ——————— Toluene____________________15108-90-7- —— —— -Chlorobenzene______________15100-41-4——————Ethyl benzene_____________ '5100-42-5 ——————— Styrene____________________151330-20-7—————Xylene (total )___________15

IUIUIUIUIJIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUI

FORM I iJOA 1/87 Rev.

79

1AVOLATILE ORGANIC* ANALYSIS DATA SHEET

E?A SAMPLE NO.

Lab Nana: gTCLab Coda: ___ Case He.:

Contract:SAS No.: SDC No.:

Matrix: faoil/vatar)Sample vt/vol: fq/BLl JTL

Lovol: (low/B«d) LOta

% Moisturo: not dae.

Column: (pack/cap)

CAS NO.

Tatrahvdrofuran

COMPOUND

Lab Sample ID:Lab Filo ID:

Data Xaeaivod: £>\Data Analyzad:dilution Factor:

CONCENT1UTION UNITS(ug/L or ug/Kal

JO U

FORM I VGA 1/17 R«v

80



EPA SAMPLE NO.


Lab Code: Case No.:


Samp 1e wt/vo1: 5.0 C g/mL) ML



Column: 'pack/cap) PACK


Cont ract:

SAS No.: SDG No.:

Lab Sample ID: QC70A42U


Date Received:


D i l u t i o n Factor: l.Q

CONCENTRATION UNITS:lug/L or ug/Kg) UG/L


,

FORM I UOA-TIC

RT EST. CONC

1/87

0

Rev.81

1ftVOLATILE ORGAN ICS ANALYSIS DATA SHEET

EPA SAMPLE NO

U8LK02Lab Name: ETC Corp.

Lab Code: Case No.:

Cont ract

SAS No.

Ma t r i x : tsoil/water) UATER

Sample wt/vo 1: 5.0

Level: Uow/med) LOLJ


Co lumn: (pack/cap) PACK

(g/mL) ML

CAS NO. COMPOUND

SDG No.:

Lab Sample ID: QC7Q442'J2

Lab File ID: >D255Q

Date Received: p\ //eft/

Date Analysed: 01/10/91

D i lut ion Factor: 1

CONCENTRATION UNITS:(ug/L OP ug/Kg) UG/L Q

74-87-3 —————74-83-9 —————75-01-4 —————75-00-3 —————75-09-2 —————67-64-1 —————75-15-0 —————75-35-4 —————75-34-3 —————540-59-0 ————67-66-3 —————107-06-2 ————78-93-3 —————71-55-6 —————56-23-5 —————108-05-4 ————75-27-4------78-87-5 —————10061-01-5 ——79-01-6 —————

79-00-5 —————71-43-2 —————10061-02-6 ——75-25-2-- ———108-10-1 ————591-78-6 ————127-18-4 ————79-34-5 —————108-88-3 —— --108-90-7 ————100-41-4 ————100-42-5 ————1330-20-7 ———

1---Chloromethan* 1---Bromomethane I- — Oin»jl Chlor ide 1---Ch loroe thane 1—— Meth-jlene Chloride 1---Acetone 1—— Carbon Diaulfide. __ 1---1.1-Diehlaroethene (---1.1-Dichlopoathana 1— - 1, 2-0 i ch lore then* (total ) __ I---Chloroform 1- — 1.2-Diehloroethane 1— -2-Butanone I---1.1.1-Trichloroe thane 1---Carbon Tet raeh lor ide 1— -Uinyl Acetate _ 1---BramoH ich lorome thane 1—— 1,2-Diehloropropane 1---cis-l,3-Dich loropropene ____ 1---Tr ich Inroe thene _ ,. 1---Dihromneh lorome thane 1— -1 , 1 ,2-Tr ich Inroethane mi . 1---Benzene ._ 1---trans-l,3-Dich loropropene __ I---Bromofnrm . ,. 1— -A-Methy 1-2 -Pant anone 1---2-Haxannne ,. im „ 1---Tetraehloroethene 1- — 1,1,2,2-Tetrach loroe thane __ 1---Toluene , 1---ChlorQhenzene_ 1---Ethylbanzene _, 1---Styrene n 1——— Xylena ( t o t a l ) 1

1

1010101061055555510551055555555510105555555

1IUIUIUIU1IUIUIUIU>uIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1 82

1AVOIATZIX OWANZCS ANAW.J, WTA ^^ W* SAKPU MO,

fq/ml) PILLCLI

* Moifturt: not dtcColumn: (pacX/cap)

CAS NO. COMPOUND•

Totrahydrofuran

'•Dilution Factor:CONCZNTRATZON CNZTS;(ug/L or ug/Kq) MC/L

FOKM X VOA 1/17

83



ERA SAMPLE NO.

"VIBLK02Lab Name:ETC Corp. I Laboratory

Lab Code: Case No.:

M a t r i x : taoil/water) WATER


Level: tloui/med) LOUI


Co lumn: (pack/cap) PACK

Number TI Cs found: 0

Cont ract:

SAS No.: SDG No.:

Lab Sample 10: QC7Q442«2

Lab File ID: >D255G

Date Received:

Date Analyzed: Ql/lCl-'91



CAS NUMBER COMPOUND NAME RT EST. CONCI

Q l

iiiiiiiiIi!11!1111111,

11111111t

FORM I UOA-TIC 1/87 Rev.

84

1ftURGrtNlCS

Lab Name: ETC Lorp.

Lab Code: Case No.:

Ha t r i x : '.soil-' wa t * r ) WM i tR

Sample wt 'vo1: 5.0

Level: Uow'med) LOW

\ rioisture: not dec.

Column: 'pack-'cap) PttCK

ft SHHPLL NODftfft SHEET

Lont ract

SftS No.

ML

CftS NO. LunPuuND

SUli No. :

Lab 'sample 10: JC,~'U*+42l.!

Lab Fi le 10: >U'J57l

Da te Received:

Date Analyzed: Ol-'ll-'yj.


CONCENTRATION UNITS:lua/L or UQ/KQJ Ub/L

I 74-87-3 — - — — --Chloromethane I 10I 74-83-9-————--Bromomethane 110I 75-01-4———— — — Vinvl Chloride I 10I 75-OQ-3--————Chloroethane 110I 75-09-2 ———————— Hethvlene Chloride 15I 67-64-1--— —— --ftcetone I 101 75-15-0-————Carbon Disulfide 15I 75-35-4———— ——— 1.1-Dich loroethene I 5I 75-34-3--- — — —1,1-DiChloroethane 15I 540-59-0- — — — -1 ,2-Dichlorethene t t o t a l ) I 51 67-66-3 ———— — — Chloroform 15I 107-U6-2- —— —— -1.2-DichIoroethane I 5I 76-93-3 ——————— -2-Butanone I 10I 71-55-6———————1.1,1-Tr i Chloroethane 15I 56-23-5—--——-Carbon Tetrachloride 151 108-05-4———————Yinyl Acetate HOi 75-27-4-————-Bromodichloromethane 15I 78-87-5————————1 ,2-Dich loropropane I 5I 10061-01-5—————ci»-l,3-Dichloropropene 15I 79-01-6- —————— Trichloroethene 15I 124-48-1-—————-Dibromochloromethane 15I 79-OU-5—————1.1.2-Trichloroethane 15I 71-43-2 ——————— Benzene 15I 1U061-02-6————tran»-l,3-Dichloroprooene 151 75-25-2-————-Bromoform 15l 108-10-1—-———-4-Methvl-2-Pentanone 110I 591-78-6- — - — --2-Hexanone I 10I 127-18-4—-———-Tetrachloroethene 15I 79-34-5——-----1,1,2,2-Tetrachloroethane 15I 108-88-3 —————— Toluene 15I 108-90-7- — ———— Chlorobeniene 15I iQQ-41-4- ———— — Ethvlbenzene I 51 100-42-5 ——————— Stvrene 15I 1330-20-7——————Xvlene (total) 15I I

IUIUIUIUIIUIUI UIUIUIUIUIUI UIUIUIU1 UIUIUIU1 UIUIUIUIUIUIUIUIUIUIUIUIUI

85FORM I UOft 1/87

1AVOLATZU OftOANZCS ANALYSIS DATA tHZTT

IfA SAKFLI NO.

Lab Naaa:

Lab Coda: Caaa No.:Contract:SAS No.:

Matrix: (aoU/vatar)Staple wt/vol: S fo/aLl mt.

(lov/B«d} O a

* Meistura: not dac.Column: (pack/cap)

CAS NO. COMPOUND

Tatrahydrofuran

SOG No.:

Lafc Saapla ZD:Lab Fila ZD: 7&JgS7i

Data Kaeaivad: __^_Data Analyxad:

dilution Factor:CONCENTTUTION UNITS(ug/L or ua/Kg)

JO

row z VOA

u

1/17 Mv

86



EPA SAMPLE NO.

VBLK03Lab Name:ETC Corp. I Laboratory Contract: 1___________


Matrix: (soil/water) WATER Lab Sample ID: QC7Q4«2v3

Sample wt/vol: 5.0 (g/mL) ML Lab F i l e ID: >D2571

Level: (low/med) LOUI Date Received: |/||






CONCENTRATION UNITS:CugxL or ug/Kg) UG/L

CAS NUMBER

01.

COMPOUND NAME

Unknown

RT

21.07

EST. CONC

7

Q

J

i

FORM I UOA-TIC 1/87 Rev87

1AUOLATILE ORGAN ICS rtNALYSIS DATA SHEET

Lao Name: ETC Corp. Contract: I___

t.ab Code: Case No.: SAS No.: SDG No.:

M a t r i x : r. so i U'water) WATER Lab Sample ID: QC.~

tg'mLJ ML Lab F i l e ID: >D2580

Date Received: £///:

Date Analyzed: Ql'13

EPA SAMPLE NO

Sample wt/^ol: 5.0

Leve I : c lout/med J LOW


Column: Cpack^cap ) PACK

NO. COMPOUND

D i lut ion Fac tor:


74-87-3 —— ——74-83-9 —————75-01-4 ----- -75-00-3 ------75-09-2 —————67-64-1 — — —75-15-0 ------75-35-4 ——— --75-34-3-- - ——540-59-0 -----67-66-3 ------107-06-2 —— --78-93-3 ------71-55-6 ------56-23-5 —— ——108-05-4 — ——75-27-4 ----- -78-87-5 —————10061-01-5 ---79-01-6 ----- -124-48-1 —————79-00-5 ----- -71-43-2 —— ——10061-02-6 - —75-25-2-- ———108-10-1 -----591-78-6 -----127-18-4 — ——79-34-5 ------108-88-3 -----108-90-7 — ---100-41-4 -----100-42-5 -----1330-20-7 —— -

---Ch lorome thane---Bro mo me thane---Uinvl Chloride---Chloroethane---Methulene Chloride---Acetone---Carbon Diaulfide---1 rl-Dichloroethene---1 .1-Dichloroethane—— 1 ,2-Dichlorethene (total t __---Ch lorof orm---1 .2-Dich lor oe thane— -2-Butanone---1 .1 .1-Trichloroethane—— Carbon Tet rach lor ide—— Omul Acetate---Bromod ich lorome thane— -1 . 2-Dich lorooroo an e---c 13-1, 3-D ich loropropene ____---Trichloroethene , iiimii _ n _MI_---Dibromoch lorome thane— -1.1 .2-Trichloroethane---Benzene---trans-1 , 3-D ich loropropene __---Bromof orm---4-Methyl-2-P«ntanone---2-Hexanone---Tatrachloroe thane—— 1,1,2,2-Tetrach loroe thane __---To luene---Chlorobenzene---Ethyl benzene---St yrene---Xylena (total) _ ..,„„

11 101 101 1011015110151515151515t i o15151 101515151515i51515151 101 1015151515151515i

1 iIU 1IU iIU 1IU iIU iIU IIU IIU 11U 1IU iIU 1IU 1IU IIU iIU iIU iIU iIU iiu iIUIU IIU •IU IIUIU 1IU IIU 1IUIUIUIU 1IU iIU IIU I1 1

1AVOLATILE OMAWXCS AXALYSXJ DATA «tt!T CVA SAK9LC HO

LAB MAOQ! ergLAB codo: CAM NO.:

Matrix: faoil/vatori QJArgg.Staple vt/voi: .^ fa/ml) rot,Lovol: (low/mod} 0

I Moisturt: not doe.Column: (pocit/ ctp)

Contract:SAS Mo.:

CAS HO. COMPOUND

Totrahydrofuran,

100 NO

LAB SAaplo 10:U* FUo XO:OAto ftocoivod:OAtO AAAlyiOd:

dilution Factor:CONCXNTIUTXON ONXTS:(ug/L or uo/Koi MC./L

X VOA

89



Lab Name:ETC Corp. I Laboratory Contract: I_____


ERA SAMPLE NO.

t*'/IP

flat r ix : ( s o i l / w a t e r ) WATER

Sample wt/vo1: 5.0 Ig/mL) ML

Le"e 1 : '. lowmed ) LOU


Column: < pack/cap) PACK


Lab Sample ID: QC70442V\

Lab Fi le ID: >D258Ci

Date Received:

Date Analyzed: 01'13'91



11 CAS NUMBER

11Ii1I1Ii!111i1*

*

i

1,

111i

11111

COMPOUND NAME

FORM I UOA-TIC

RT EST. CONC

1'87

IU 1

1,

i1!111111I

11(IIi1

11

111I1i111

Rev.

90


ERA SAMPLE NO.

UBLKQ1Lab Name: ETCNJ

Lab Code: Case No.:

M a t r i x : ', so i 1 ' 'water i UIATER

Sample w t / v o l t 5.0 (g/mD ML

Leva 1 : '. lou/med > LOUI


Column: Ipack/cap) PACK

Con t ract:

SAS No.: SDG No.:

Lab Sample ID: QC70443U

Lab File ID: 'C2124

Date Received: Ql-'*»/91

Date Analyzed: 01/11,'91

Dilut ion Factor: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:Cug/L or ug/Kg) UG/L

74-87-3- — — — --Ch lorome thane_____________11074-83-9 — --- —— -Bromome thane______________11075-01-4———————vinyl Chloride____________11075-00-3- —— - ——— Chloroe thane______________11075-09-2 ————— --Methylene Chloride________1567-64-1 — —— — --Acetone__________________11075-15-0 ——————— Carbon Diaulfide__________1575-35-4———————1,1-Dichloroethene________1575-34-3———————1,1-Dichloroethane________15540-59-0 — - —— — 1,2-Dichlorethene (total)__1567-66-3 ——————— Chloroform_______________15107-06-2 —————— 1,2-Di chloroe thane________1578-93-3 ——————— 2-Butanone_______________11071-55-6 ——————— 1,1,1-Tnchloroe thane______1556-23-5———————Carbon Tet rach lor ide_______15108-05-4——————Uinyl ftcetate_;__________11075-27-4------ — -Bromodichloromethane_______1578-87-5 ——————— 1,2-Diehloropropane_______1510061-01-5—————cia-1,3-D;ch loropropene____1579-01-6 — ————— Tr ichloroethene___________15124-48-l--------Dibromoch lorome thane_______1579-00-5 ——————— 1,1,2-Tn chloroe thane______1571-43-2 ——————— Benzene__________________1510 061-02-6 — -.jia^trans-ljS-Dich loropropene__1575-25-2--- — -- — BromoTorm________________15108-10-1 ——————— 4-Methyl-2-P*ntanone_______HO591-78-6 —————— 2-Hexanone_______________110127-18-4— — ——— Tet rach loroethene,_________1579-34-5 ——————— 1,1,2,2-Tet rach loroe thane__15108-88-3 —————— Toluene__________________15108-90-7—— — —— Chlorobenzene_____________15100-41-4——————Ethylbenzene______________15100-42-5 —————— Styrene__________________151330-20-7—————Xylene (total)___________15_______________ _______________________I_

IUIUIUIUIUIUIUtuIUIUIUIUIUIUIUIUIUIUtuIUIUIUIUIUtuIUIUIUIUIUIUIUIUIU

91

vozarzu OMAJIZCS AXAX.YSXJ DATA snxr

Naaai are

»A SAKVU NO.

Codoi .._ caao NO.:Matrix; (aoil/vatari 60*TBe.Saapla vt/vol: ?Lavol: (lev/Bod) /fl% Moiaturo: not doe.Co1umn: (pack/cap)

Contract:SAS No.:

CXS NO. COMPOUND

Totrahydrofuran,

•00 NO.:

laapla ID:ma XO:

Data ftocaivod:Data Analysad:

dilution factor:

(ug/t or

u

I/I? R«v

92

IEUOLATILE ORGANICS ANALYSIS D*T* SHEET


EPft SAMPLE -10.

M.'BLKOlLab MameiETC-O

Lab lode: Case Mo.

ria 11- . • : ( « o : 1 --'wa t e r > UIATER

3arr.pl e w t - ' v o l : ?.0 (

Leve1: ; l a w ^ m e d ; LOW

'• M o i s t u r e : not dec.

C a l u m r : '. pack/capJ PACK

Number TICa found: 0

Con t r a c t :

3AS Mo.: SDG io. :

Lab Sample ID: OC7Q*-*?U

Lab F: le ID: -C:i2**

Date Received: 01 - U 91

Date Ana lyzed: :il 'Il-"?i

D i l u t ion Factor: 1.0

CONCENTRATION UNITS:fug/L or ug/Kgj UG/L

CHS NUMBER COMPOUND NAME RT EST. CONC

FORM I i/er Re,. 93

1AVOLATILE ORGAN ICS ANALYSIS DAT* SHEET

uab Name: ETCNJ

Lab Code: Case No.:

Mat r :/.: '. sci 1 --'water > WATER

Sample wt'vol: 5.0 rg-TnL) ML

Leve 1 : (. low/'mec . LOW


Column: t, pack/capJ PACK

uontract:

SAS Mo.:

ERA SAMPLE r-C.

I1UBLKQ2I.______________

SDG Mo.:

Lab Sample ID: QC7Q44?iJt

Lab ci le ID: C2136

Date Received: 01 8 '91

Date Analyzed: 01'19/91


CAS NO. COMPOUNDCONCENTRATION UNITS:fug/L or ug/Kg; UG/L

I 74-87-3-- — - — --Chlorome thane_____________ 10I 74-33-9---------Bromomethane_______________ 10l 75-01-4————————Uinyl Chloride_____________ 10i 75-00-3 — —— -- — Chloroethane______________ 10I 75-09-2 ————— --Methylene Chloride________ 5I 67-64-1- ——— - — -Acetone____________________ 4l 75-15-0———————Carbon Disulfide__________ 5l 75-35-4———————1,1-Dichloroethene________ 51 75-34-3————————1,1-Dichloroethane_________ 5I 540-59-0 —————— 1,2-Dichlorethene (total)__ 5I 67-66-3---------Chloroform_________________ 5i 107-06-2----- — -1,2-0ich loroe thane________ 5i 78-93-3--- — - —— 2-Butanone_______________ 1071-55-6-- — -- —— 1,1,1-Tr ich loroethane______ 5

i 56-23-5 ——————— Carbon Tet rach lor ide_______ 5! 108-05-4— — —— -Vinyl Acetate_I____________ 10i 75-27-4— — - — — Bromodlchlorome thane_______ 5i 79-87-5 — — — ——1,2-0ich loropropane_______ 5l 10061-01-5- — —— cis-1,3-Dichloropropene____ 5: 79-01-6 ——— - ——— Tr ich loroe thene____________ 5i I2**-48-l--------Dibromochloromethane ____ 5' ^9-00-5-- — —— --1,1,2-Tr ich loroethane______ 5i 71-43-2---------Benzene__________________ 5I 10Q6l-02-6---^^tt rans-l ,3-Dich loropropene__ 5I 75-25-2---------Bromoform__________________ 5I 108-10-1 ————— -4-t1ethyl-2-Pentenone_______ 10I 591-78-6 ——————— 2-Hexanone_________________ 10I 127-18-4---- —— -Tet rach loroe thene_________ 5I 79-34-5 — - — - — -1,1 ,2,2-Tet rach loroe thane__ 5l 108-83-3 —————— Toluene__________________ 5l 108-90-7—— —— --Chlorobenzene_____________ 5I 100-41-4——— ——— Ethylbenzene______________ 51 100-42-5 ——————— Styrene____________________ 5I 1330-20-7——————Xylene (total)____________ 5

Q

IUIDIUIUIUUiuIUiuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU'.UIUIUIUIUIU!UIUIUHU

94

1AVOtATXZX OMANXCS AKAZ.YSZS DATA fttZT

**» Naao: greNO.:

Matrix: (aoil/wator) j*J*Tg,Saaplo vt/vol:Lovol: (lov/aod)I Moiftturoi not doe.Caluan: (pack/cap)

„.y°' CWOUNO

Totrahydrofuran

SAS NO.:

faaplo ID:Ub filo ID:Otto ftoeoivod:

Oato Analysod: t / / 8 /g t^^^ •••••• • ™dilution Factor:

100 No.i

FQM X VOA I/I? R«v

95

96' ** -B--T on -won i uaoj

ONOI 'IS! Ic 3WWH QUnOdWOO dSauf

~ 1.- 5 ft ' 6 v-i .-• 6" .10 - / 6 n}

7 : j o * D e j u o i 4 n ] i Q

T i. t T -• T J : P * - ' •

•D SI T^ :--•• '-

'MD d -JJT, c

3i Jli33HS "i

31

IAVOLATILE ORGANICS ANALYSIS DATA SHEET

ERA SAMPLE MO

UBLKQ3Lab Name: ETCNJ

Lab Code:

Con t rac t :

Case No. : SAS No. : SDG

Matri...: <soi1/uater) UATER

Sample wt-'vcl: 5.0 rgXmL) ML

Level: ', low/med-1 LOU1


Column: tpackxcap) PACK


Lab Fi le ID: C2211

Date Received: 01 fl -'91

Date Analyzed: U--19.-'91

Di lut ion Factor :

CAS NO. COMPOUNDCONCENTRATION UNITS:Cug/L or ug/Kg; UG/L Q i

I 74-87-3 — --- — — Chloromethane_____________I 10I 74-83-9 — - — - —— Bromome thane_______________I 10I 75-01-4————————Uinyl Chloride_____________110: 75-00-3 ———————— Chlo roe thane_______________t 10I 75-09-2 ————— -.-Methylene Chloride________151 67-64-1 ———— -——Acetone____________________I 10I 75-15-0 ——————— Carbon Disulfide__________15I 75-35-4———————1,1-0 ichloroe thane________15I 75-34-3———————1,1-Dichloroe thane________15I 540-59-0 —————— 1,2-Dichlorethene (total)__15I 67-66-3 — - ———— -Chloroform_________________15I 107-06-2 —————— 1,2-Dichloroe thane________151 78-93-3———————2-Butanone_______________I 1071-55-6---- — -— 1,1,1-Trich lo roe thane______ I 5

i 56-23-5- ———— —— Carbon Tet rach lor ide_______15I 108-05-4——————Yinyl Ac«tate_J__________110I 75-27-4------ — -Bromodich lorome thane_______I 51 78-87-5- ——————— 1,2-Dichloropropane________15! 10061-01-5 ——— — c is-l,3-Dichloropropene____15i 79-01-6-- ——— —— Tr ichloroethene___________15i 124-48-1——————Dibromoch lorome thane_______15, 79-00-5-- — ————1,1,2-Tr ichloroe thane______15! 71-43-2--- — — --Benzene__________________15I 10061-02-6 — - .t_rana.= l ,3-Bich loropropene__15I 75-25-2-- — -----Bromoform__________________15I 108-10-1 ———— - — 4-Methyl-2-Pentanone_______1 10I 591-78-6 —————— 2-Hexanone_______________I 10I 127-18-4- — ——— -Tetrachloroethene__________15I 79-34-5————————1,1,2,2-Tet rach lo roe thane__15l 108-88-3 —————— Toluene__________________15I 108-90-7———— — -Chlorobenzene_____________15! 1QO-41-4——— ——— Ethyl benzene_______________151 100-42-5——————-Styrene____________________15I 1330-20-7——————Xylana (total )____________15

1U1U1UIUiUIU1UIUIUIUIUIUHJIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU

97

1AVOtATXIX OJWAHICt ANALYSIS DATA MOXT CTA SAKfU NO.

Uft NAMS

U» COtfOS CftM No.:

Matrix: (•oil/wtt«r)JjjgB-$4»pl« wt/vol: 5 fa/»ll WLUvtl: (lev/ltd)

I Moi»tur«i not doecolumn: (paek/e«p)

CAI HO. COHMUNO

Dilution factor:COHCCCTIUTIOK CWMS

or

Totraiiydrofuran JO u

1/17

98

IEVOLATILE ORGAN ICS ANALYSIS OAT* SHEET


ERA IAMPLE :;0.

I vBLK 01Lab NamesETCNJ

Lab Code : Ca se Mo . :

Ma-.'i-: '.so: 1 -'water > WATER

Sample wt--'i.-ol: 5.0 fg/mLJ

Level: 'iow/mea LOW


Column: (pack 'cap) PACK

Cont ract:

3AS Mo -: 3DG : !o . :

Lab Sample ID: QC""Q4*+?U7

Lab r i l e ID: C2211

Date Received: G 1 • fl -'91

Date analyzed: 0 1 ••' 1'3-""J 1


Numbs r T I Cs found JCONCENTRATION UNITS:Cug/L or ug'Kg; UG/L

11 CAS NUMBER

11tI1

tI!(

i1

iii

I

11!I111

COMPOUND NAME

•.

• —

1 1RT 1 EST . -ONC 1 3

11 t1 '1 !1 i

1 11 11 1!1 t1 !! 1! 11 t1 11 11 !1 11 '1 11 I1 .. 11 11 11 !1 t1 11 11 11 11 I

FORM I "JOA-TIC 1-'S7 Pe-.-.99

IttOhtGftNlCS HNflLYSIS DttTA SHEET

S*nPL£ NO.

Lab Name: ETC Corp.

Lab Code: Case No.:

Matrix: tsoil/water) WH I l£R

Lont ract :

SHS No.:

Sample w t / vo l : 5 .0

Level : '. low/mod) LCIU

\ Mo is tu re : not dec.

Column: ' .pack/cap)

CflS NO.

Cg/mLJ tIL

I YBLKU1I________

SDG No.:

Lab Sample 10: QC7U445V

Lab Fi le 10: >£j^59u

uate Keceived:

Date Analyzed: 01-'13''yl

D i l u t i o n r~actor:

CUflPOUNDCONCENTRATION UNITS:tug/L or ug/Kg) Ub/L

74-87-3 —— ——74-d3-9 —————75-01-4 —————75-UO-3 ------75-09-2 —————67-64-1-- — --75-15-0 —— ——75.35.4 ......75-34-3 — — —540-59-0--- —67-66-3------107-06-2 -----78-93-3 ------71-55-6 —————56-23-5 —————1U8-05-4 — ---75-27-4 —— ——76-87-5 ------1U061-01-5 ——79-01-6 ------124-48-1 -----79-UU-5-- -- —71-43-2 -----10061-02-6- --75-25-2 —————106-10-1 -----

127-18-4 ————79-34-5-- ----108-68-3 -----10b-90-7 -----100-41-4 — ---100-42-5-----1330-20-7 ———

---Chloro me thane---Bromo me thane---"Jinyl Chloride---Ch loroe thane---Methvlene Chloride---ftcet one---Carbon Disulfide---1 .1-Dichloroethene---1 .1-0 ich lor oe thane--- 1.2-0 ich lore th en e (.total;---Ch lorof arm---1 .2-0 ich loroe thane---2-Bu tanone---1 .1 .1-Tr ich loroethane---Carbon Tetrachloride---Winyl Acetate---Bromo d ich loro me thane---1 .2-Diehloroprooane---cis-l,3-Dich loropropene ____---Tr ich loroe thene---Dibromoch lorome thane---1 .1 . 2 - T r ichlnroethane---Benzene---trans-1 , 3-D ich loropropene __---Bromotorm

---2-Mexanone---Tetrach loroethene---1, 1,2, 2- Tetrach loroe thane---To luene ,„. „„.---Ch lorobenzene---Eth^lbenzene---Styrene,, MII— -Xy iene I tota 1 )

11101 101101 101 1l 101515151515151 1015151 101515151515151515151 10I 10t51515151515151

1

U 1U 1U 1U iJ 1U :U iuU 1U 1U 1uU 1uU 1uU 1U :U 1uU 1uU 1uU 'uU iuU 1U iU 1uU 1u

1

FUKfl I "JOA

100

Lab tfua:Ub coda i

1AVOLATILE OftOANZCS ANALYSIS DATA SVZZT

ere

CVA SAK9U NO.

CaM No.:

Matrix; (aoii/vatar) toJfrrge.Sampla wt/vel: S (a/*L\Laval: (lov/aad) ttn% Moistura: not dac.

Column: (paeX/cap)

CAS NO.

Tatrahydrofuran,

COMPOUND

*00

Ub Saapla ID:Lab Pilo 10:Data Raeaivad:Data Analyxad:

Dilution Factor:coNcnmuTioH UKITS:(uoyt or uq/Kq] j*G/L

"7"J£^ u

POM Z VOA 1/17 X«v

101

ItVOLATILE GRGANlCS ANALYSIS DATA SHEET


£PA SAriPLE NO.

UBLKUlLab Name:ETC Corp. 1 Laboratory Contract: I______

Lab Code: Case No.: SAS No.: SUb No.:

Matrix: (soil/water) UIAl£R Lab Sample ID: QO

Sample wt/vol: 5.0 Cg/mLJ ML Lab File ID:

Level: Uow/med) LOW




Date Received: I//.?/?/

Date Analyzed: O.U'13/91

Ui lut ion Kactor : 1. i.

CONCENTRATION UNITS:lug/L or ug/Kg) UG/L

11 CHS NUMBER

lilltili1illltlttiitiiiliiiiill

COMPOUND- NAME

rU*M I VOW-TIC

RT ESI. CUNC

i-'d?

t

Q

r •* v .

102

1AVOLATILE QRGAN1CS ANALYSIS DATA SHEET

Lab Name: ETC Corp. Contract: i

Lab Code: Case No.: SAS No.: Sub No.:

Mat Pix: I so;1/water) WATER Lab Sample 10: uC7

Sample wt/vol: 5.0 tg/mLJ ML Lab F i l e ID:

Level: Uow/med) LOW Date Keceived:



CAS NQ.

EKA SAMPLE NQ

Date Analyzed: Ol'l4,9i

D i l u t i o n I- actor:

CONCENTRATION UNITS:tug/L or ug/Kg) Ub/L LJ

74-87-3 —————74-83-9 —————75-01-4 —————75-UO-3 —————75-09-2 —————67-64-1 —————75-15-0 —————75-35-4 —————75-34-3 —————540-59-0 ————67-66-3 — ———107-U6-2 ————78-93-3 —————71-55-6 —————56-23-5 —————108-05-4 ————75-27-4 —————78-87-5 —————1UU61-U1-5 — -79-U1-6 — — --124-48-1 ————79-00-5 —————71-43-2 —————1UU61-02-6---75-25-2 —————108-10-1 ————5V1-78-6-----127-18-4-- ——79-34-5 ——— __108-88-3 ————lUb-90-7-----100-41-4 ————10U-42-5 ——— -1330-20-7 ———

---Ch loro me thane---Bromome thane—— Uin«ul Chlor ide---Ch loroa thane---Meth*jlena Ch lor ide---Acetone---Carbon Diau 1 f ide--- 1 .l-Dichloroethene---1 .1-Dich loroe thane— -1,2-Dichlorethene (. total ) __---Ch loro form---1 .2-Dich loroe thane___2-6utanone---1.1.1-Trichloroethane---Carbon Tetrachloride---Uinyl Acetate---Bra mod ich lora me thane---1 .2-Dichloroorooane---cis- 1,3-0 ich loropropene ____---Trich loroe thene---Dibromoch loro me thane---1 . 1 . 2 - T r ich loroathane---Benzene---trans-1 ,3-Dichloropropene __---Bromo form---4-M«thul-2-PentanonB---2-Hexanone---Tat raeh loroethene---1 ,1 ,2 , 2-Tetrachloroethane---To luene---Ch lorobenzene---Ethylbenzane---St urene---Xulene t tota 1 )

11 10I 101 101 101 41 10151515

15151 IU1515l 101515

151515

i5t •?i 101 IU151515151515151

iU 1U 1U tUJ 1U •U 1UU iUU 1U :U 1U !U 1UU 1UU 1UU 1UU iUU 1U •U lUU 1UU 1U :U 1U

1

FUKH I l-'ti/ Kev.103

1AVOZATZU OMANZCS ANAX.YSZS DATA flZZT

fifC

*PA SAKVU MO.

Codo* —___ caao NO.:Matrix: (aoil/vatar) WTBJ.Saaplo vt/voi: c to/mL\Uval: (lov/aod) <U^% Moiaturai not doc.Column: (pack/cap)

CAS NO. COMPOUND

Totrahydrofuran.

'.Dilution Factor:CONCUmUTXON UNZTS:(ug/L or «g/Kg)jg*C^L_ g

u

row z VOA 1/17 K*v.

104

IEUQLHTtLE ORGANICS ANALYSIS DATA SHtET


SHMPLE NO.


Lab Code: Case No.:

Matrix: tsoi 1 /water) UIA I ER

Sample wt/vol: 5.0 Ig/mLJ ML

Level: t low/med) LOW


Column: '.pack /cap) PACK

Number TlCs found: 0

IW8LKU2Cont ract :

SAS No.: SDb No.:

Lab Sample ID:

Lab Fi le ID: >U260&

Date Deceived: (/

Date Analyzed: t


CONCENTRATION UNITS:lug/L or ug/Kg) U6/L

l.u

CftS NUMBER COMPOUND NAME

FUKM I VOW-TIC

RI ESI. CUNC

1 'S7

Q I

I

iii•i,

i.I,i

i,i:1

l

1

1

1

1

1

rev .

105

1RVOLATILE URGANICS ANALYSIS OAT A SrltET

EHA NO.

OBLKU3Lab Name: ETC Corp. Contract: I________

Lab Code: Case No.: SAS No.: Sub No.:

Matrix: Isoil/water) WATER Lab Sample 10: O.C7U4450.

Sample wt/vol: 5.0 tg/mLJ ML Lab File 10:

Level: Uow/med) LGUJ Date Received:


Column: '.pack/cap) PACK

CAS NO. CUMPGUND

Oate Analyzed: 01/15/yi


CONCENTRATION UNITS:tug/L or ug/Kg) OL./L U

I74-87-3- — - — — -Ch lorome thane______________1 1074-83-9-- ———— — Bromome thane______________I 1075-01-4————————umyl Chloride.^____________I 1075-00-3 — —— — — Ch I o roe thane_______________1 1075-09-2 ———— — — Dethylene Chloride_________I 567-64-1--—— — — Acetone____________________I 1075-15-0 — - — ----Carbon Disulf ide___________1575-35-4—--- — —1 ,1-0 ich loroe thene_________I 575-34-3------ — -1,1-0ichloroethane________I 5540-59-0 — —————1,2-0ich lore thane t total J__1567-66-3------ — -Ch lo reform_________________15107-06-2- —— — —1,2-0ichloroe thane_________1578-93-3 — -- — —— 2-Butanone_________________I 1071-55-6 —— — — — 1,1,1-Tr ichloroe thane______1556-23-5- — —— ---Carbon Tetrach lor ide_______15108-05-4— — — --Vinyl Hcetate______________I 1075-27-4---------Bromod ich lorome thane_______I 578-87-5- — — — —1,2-0ichloropropane________I 510061-01-5- — —— cis-l,3-Dichloropropene____I 579-01-6—— ————— Tr ich loroe thene____________I 5124-48-l--------Dibromoch lorome thane_______1579-00-5 — ——— -—1,1,2-Tnch loroe thane______I 571-43-2---------Benzene____________________151U061-CI2-6- — ---trans-l,3-Dich loropropene__1575-25-2-- — - — — Bromof orm__________________15108-10-1- — -----4-riethyl-2-Pentanone_______I 10591-78-6--------2-Mexanone_________________I 10127-l8-4--------Tetrach loroe thene__________1579-34-5---------l;l,2,2-Tetrachloroethane__15108-88-3-- — ----Toluene____________________I 11UB-9U-7—------Ch lorobenzene______________15100-41-4- — -----Ethyl benzene_______________15100-42-5------ — Styrene____________________I .8UU1330-20-7----- — Xylene t tot a 1 )____________I 5

\

IUIDIUtoIOIOIOIO10IOIOIO10IOIOIOIO10IOIO10IO101 OIOIOto10IUuIOIUIJto

FORM I 1/87 Kev.106

IAVOIATXE* OX0AJIXCS AJCAI.YSX* DATA 0KXXT SAX9U NQ.

tftfe HAMS,

Uto cotft*fines

CAM He.:Matrix: f»oil/v«t»ri 6J»TBg.Staple vt/vel: S fq/mLl

Uv«l: (low/»«d) O^Li

% Moi«tur«: net d«c.Column: (ptcX/ctp)

100 *••!

UD S«apl« ID:

CU HO. COMMUHO

Data ftacaivad:

Data Analysad:dilution Factor:

COKCXHTRATIOH OHXTS(ug/L or ug/Kg)

Totrahydrofurtn JO

roni x VOA !/•? ffcv.

107

IEVOLATILE QRSflNiCS HNALYSIS DrtTA SHtET

TENTATIVELY IDENTIFIED COnPOUNDS

EPft SHHPLE NO.

IYBLKU3Lab Name:ETC Corp. I Laboratory

Lab Code: Case No.:

Matrix: tsoiI/water) UttTER

Sample wt/vol: 5.0 (g/mLJ ML

Level: C low/mad) LQLJ

\ Ploisture: not dec.

Column: tpack/cap) PHCK


Cont ract:

SHS No.: SUb No.:

Lab Sample ID: LjC7u445"v';

Lab Fi le ID: >U2621

uate Received: I ( /S'/^/

Date ttnaiyzed: Oixl5/Vi

Dilution Factor: l.u

CONCENTRHTION UNITS:tug/L or ug/Kg) UG/L

CHS NUMBER CUHPOUND Esr. CUNC

1 "87 r-v.

1C8

FORM i.'I I iJQA 1--87 Rev.

3AUOLATILE INTERNAL STANDARD AREA SUMMARY


Lab Code: Case No.: SAS No.: SDG Mo.:

Lab File ID '.Standard): -C2123 Data Analyzed: "J i •''!! ••


*1a t r i... : t so i 1--'water ) WATER Leve 1 : i, low/med ) LQLJ Co lumn : ' pack,-cap ,'

01020?04050607080910111217

131«2021

12 HOUR STD

UPPER LIMIT

LOUER LIMIT

EPA SAMPLENO.

UBLK01A5563A5574A5559A5580A5581A5582A5603A5594A5595

I SI (BCM)AREA #

41336

92672

20668

41744.. 412994067439598395384035639095386323973139223

—

RT

10.40

10.3910.4110.4710.4410.3810.4210.4010.3710.3710.38

-

IS2(DFB)AREA #

192366

384732

96183

185350191339178678179668176663179986175116170000171199169671

RT

21.10

21.0821.1121.1621.0921.0721.1121.1321.1021.1021.11

I S3 ( CBZ )AREA f

148946

297992

74473

146141153000142834141080136324144135143586138427136955125034

RT

25.99

~

25. "626.0026.0526. 0125.9526.0026.0225.9326.0025.99

;I SI '.BCM) • Bromoch lorome thaneIS2 i.DFB) - 1,4-Di f luorobenzeneIS? (CBZ) - Chlorobenzene-d5

UPPER LIMIT - * 100Sof internal standard areaLOWER LIMIT - - 50*of internal standard area

* Column used to flag internal standard area values with an asterisk.109

FORM UII I UOA 1/87 Rev.

SHUOLATILE INTERNAL STANDARD AREA SUMMARY


Lab Code: Case No.: 3AS Mo.: SDG Ho.:

Lab F i l e 10 '.Si andard ) '. C2134 Data Analyzed: Ol/lS'91

Instrument ID: GC.-'MS C Time nna1y=ed: 1043

Mar - IA : '.so i I/water i WATER Leve1:Clow/mod) LQU Column:(pack/cap) /»*</

\

01020304090607080910111215141516

18;Q202 1 1—i n i

12 HOUR 3TD

UPPER LIMIT

LOWER LIMIT

EPA SAMPLENQ.

OBLK02A5805A5599A5806A5591A5805A5806A5591

ISltBCMJAREA it

61391

123782

30946

4745356629

. 572005349753475516315565156077

^^. ____ .

PT

10.33

10.4710.4910.3910.4110.3910.4310.4010.38

i*

IS2CDFB.'AREA ft

27Q337

540674

135168

208802246388247875231118224989229838239082237252

"

?T

21.09

21.1321.1521.1221.1121.0921.0921.0621.08

IS3CCBZ)nREA ft

163017

326034

31503

121129198269204889173798191521188846196316191053

I=T

25.971

1

i

Ii

25 .93 126.01 i25.«7I25 . '?5 '25.97125.9-. 125.96125 . ?3 1

I1llI;1

•i

liI

^ '

I£l CBCM.1 • Bromoch loromethaneIS2 <DFB) - 1,4-DifluorobenzeneIS? CCBZ.i • Chlorobenzene-d5

UPPER LIMIT - * 100Sof internal standard area.LOWER LIMIT - - 5OHof internal standard area.

ft Column used to flag internal standard area values with-an asterisk.

°f J_ 110FORM UIII "JOA l-'87 Rev.

SHVOLATILE INTERNAL STANDARD AREA SUMMARY


Lab Code: . Case No.: SAS Mo.: SDG No.:

Lab F i l e ID (Standard): >C2184 Data Analyzed: 01/18 '91


Mat r ix: (»c i 1/water ) UIATER Leva 1 : ' low/med ) LOW Co lumn: C pack /cap J ____

010203040?0607090910

13

1

1 12 HOUR STD

1 UPPER LIMIT

1 LOWER LIMIT

1 ERA SAMPLE! NO.

1 A5597 ^ •P'f*I1I111i1ii1IiI,!'1

!I

I31CBCM)nREA *

61891

123732

30946

4745353493

= T

10.33

10.4710.45

I S2 t DFB JnREA -f

270337

540674

135163

'

208802228455

?T

21.09

21.1321.10

ISJCCBZ' iHREA --M ^^

Io3017l 25.?^

3260341

315081

11

121129 1 25.98134232 ! :6.C>?

1t1ti1iiii;1i111*

11

! S 1 ^ BCM ? - Bromochloromethane152 <DFB) - 1,4-Difluorobenzene1ST iCBI) • Chlorobenzene-d5

UPPER LIMIT - * 10QSof internal standard area.LOWER LIMIT - - 5 OSof internal Etandard area.


page __ of __

FORM UII I UOA1 1 1

1-37 Rev.

Lab

SAVOLATILE INTERNAL STANDARD *REA SUMMARY

-: ETCNJ Contract:

Lab lode: Case No.:

Lar Fi 1« ID '.Standard •: -C2199

Instrument ID: £CXMS C

SAS 3DG :io.:

Data Analyzed: 01 -'19- -91

Time Analyzed: 1434

Mar r ix : '. s D i 1 'water .• UATEF Leve 1 : '. law'med ) LOW Co lumn : (pack- 'cap :

1 i ! S 1 C BCM )1 I AREA 9

\ 12 HOUR STDI 54089

! UPPER LIMITI 108178

1 LOWER LIMITI 27044

1 ERA SAMPLE 1I NO . !

01 IUBLK07 1 42565021 A5599MS I 5013107IA5599MSD 1 - 52788041 105 1 106 1 Ion iOBI 1QQ i 1101 111' 1121 117 1 1141 I15 I 116! I:^' i191 11* ' 1:o i i111 i22 i 1 *^- •

=>T

10.45

10.4710.4710.42

IS2CDFB)rtREA *

222969

445978

111484

182623218075220372

1 1 S3 C CBZ J3T nREA *

21.08 1 173290

! 346580

! 86645

iI

21.091 13712221. 151 14806921.111 122464

1111!11111111111111

ST

25 . 92

25.9326.0025.96

fc

131 '• BCM.' • Bromochloro me thane152 iDFB) - 1,4-DifluorobenzeneIS? CCBZ.' " Chlorobenzene-d5

UPPER LIMIT - * 100Sof internal standard area.LOUER LIMIT - - 5OXof internal standard area.

# Column used to flag internal standard area values with an asterisk,

page I of \

FORM UI I I1 12

1/87 Re--'.



Lab Code: Case No.: SAS No.: SDG No

Lab File ID ^Standard): >D2532


Matr ix : Iso i 1 /water ) WATER Leve 1 : ( low/med ) LOW

Data Analyzed: 01/09/91

Time Analyzed: 1442

Co lumn : Ipack/cap ) PAftf.

111 12 HOUR STD

1 UPPER LIMIT

1 LOLJER LIMIT

1 EPA SAMPLE1 NO.

01 IUBLK0102IA555403 IA5554MS04IA5554MSD05 IA5556061 A554707IA554808 1 A5549Q9IA555010IA555311 IA555512IA555713 1A5558141151161171isi19 1201211221

IS1CBCM)AREA *

42809

85618

21404

42349398654153241650448164174955750728117486854199585215635757558

RT

11.39

11.3611.3911.4211.4311.4311.4111.4311.4211.3911.4211.3511.3511.40

IS2<DFB)AREA *

189142

378284

94571

189592177115174947187660186987188626317976319359323105305460319662320405311684

RT

22.06

22.0622.0922.0822.0922.0922.1122.0922.0822.0922.0822.0922.0922.10

IS31CBZ)AREA *

153083

306166

76541

158732150780145860157641156045156718254554256191257310248605257481257227249274

RT

27.00

26.9527.0027.0127. 0227.0227.0027.0327.0227. 0326.9826.9826.9927,00

151 CBCM) - Bromochloromethane152 (DFB) • 1,4-Difluorobenzene153 (CBZ) • Chlorobenzene-d5

UPPER LIMIT - * 10OSof internal standard areaLOWER LIMIT - - 5OSof internal standard area

t Column used to flag internal standard area values with an asterisk.

p«g« | of I_ 115FORM U I I I UOA 1/97 Rev.



Lab Code: Case No.: SAS No.: SOS No.:

Lab File ID (Standard): >D2549 Data Analyzed: 01/10/91

Instrument ID: GC/MS D Time Analyzed: 1010

flat r jx : (so i 1/ua t er ) WATER Leve1:(low/med) LOW Co lumn : (.pack/cap j

0102030405060706091011121314151617161«202122

12 HOUR STD

UPPER LIMIT

LOWER LIMIT

EPA SAMPLENO.

USLK02A5562A5564A5569A5560A5561

ISHBCM)AREA *

65743

131486

32871

779027906275231794778004960639

RT

11.43

11.4311.3811.3711.3511.4011.40

IS2CDFB)AREA *

291832

583664

145916

345269343911317553338559335739326117

RT

22.16

22.1722.0622.0722.0522.0622.10

153CCB2)AREA *

231908

463616

115954

272037270619253627270169272362270393

RT

27.08

27.0626.9926.9626.9927.0027.00

151 (BCM) • Bromochloromethane152 (DFB) - 1,4-Difluorobenzene153 CCBZ) • Chlorobenzene-d5

UPPER LIMIT - * 10OSof internal standard areaLOWER LIMIT - - 90Sof internal standard area

* Column used to flag internal standard area values with an asterisk.

P«9* _(_ of J—— 1 1 4

FORM UI I I UOA 1/87 Rev.

SAVOLATILE INTERNAL STANDARD ARE« SUMMARY


Lab Code: Case No.: SAS No.: SOG No.:

Lab File ID (Standard;: >D2567 Data Analyzed: 01/11/91


hat P ix : Cso i 1/water ) LJATER Level: t low/med) LOW Co lumn : l pack /cap ) ___

01020304050607080910111213141516171819202122

12 HOUR STD

UPPER LIMIT

LOWER LIMIT

EPA SAMPLENO.

YBLKQ3A5576

ISKBCM)AREA *

75970

151940

37985

7207875017

RT

11.35

11.4111.44

IS2CDFB)AREA *

340304

680608

170152

316969333782

RT

22.06

22.0722.14

IS31CBZ)AREA *

270911

541822

135455

264164277048

RT

26,96

27.0127.08

151 IBCM) * Bromochloromethane152 (DFB) * 1,4-Difluorobenzene153 CCB2) - Chlorobenzene-d5

UPPER LIMIT - * 10OSof internal standard areaLOWER LIMIT - - 5OSof internal standard area

page

* Column used to flag internal standard area values with an asterisk.

_=f_ 115FORM gi I I IJOA 1/87 Rev.




Lab F i l e ID tStandard): >D2579 Data Analyzed: Gl''13/91

Instrument ID: GC/MS D Time Analyzed: 12J.4

Hatrix:(soiI/water) WATER LeveI:(low/med) LOW Co lumn : ipack/cap ) Mt/<-

0102030405060708091011121314151617IS19202122

12 HOUR STD

UPPER LIMIT

LOWER LIMIT

EPA SAMPLENO.

UBLKO*t*#*A5562 ***» nA5570A5573A5602A5575

ISKBCMJAREA *

54151

108302

27076

734097378059-621554315743173485

RT

11.78

11.3811.3511.3911.3911.4411.40

IS21QFB)AREA *

297333

594666

148666

310825313103310497301444290573320409

RT

22.53

22.0822.0522.0922.0922.1022.10

IS31CBZ)AREA *

240614

481228

120307

263396263546258788252467243058274869

RT

27.54

26.9826.9926.9927.0327.0327.00

I SI (BCM) • Bromochloromethane152 (DFB) " 1,4-Difluorobenzene153 tCBZ) • ChIorobenzene-d5

UPPER LIMIT - * 100Sof internal standard areaLOWER LIMIT - - 5OSof internal standard area

* Column used to flag internal standard area values with an asterisk

P«ge —|- of J——

FORM UI II "JOA

1161/87 Rev.

8AOOLATILE iNIERNftL STANDARD ARtA SUMMARY


Lab Code: Case No.: SAS No.: SDb No.:



Mat r ix: (so i I/water ) UAItR Leve1:(low/mod) LUU Co lumn : tpack/cap ) p/i«

11t 12 HOUR STD

1 UPPER LIMIT

1 LGUER LIMIT

1 EPA SAMPLE1 NO,

01 IUBLKU102IA557703IA5585041 A5586051 A558706 IA<?'?9607IH5571OU l R558309 1 A55S410lH5(?8911 IH559312113114115116117118119120121122 1

ISHBD1)AREA *

56U50

112100

28025

7535373226734947426372bl7759437U60259277596477117159874

RT

11.40

11. >811.4011.3911.3611.3911.3911.3011.3011.3111.3011.39

1S2 lUFBJARtA *

321702

643404

160851

322537327295314V67323366313333328055302797313691312724311889316452

Rl

22.10

22 . 1222.1022 . U922.0222. U922.0922. U422. 0422. Ul22.0022. U5

iS3^Lbi:)AfctR t

263014

526028

13150^

270368265149•J666662695412642/22/696*2558472 6 /92v•J655M26f8ua273343

iRl 1

27.001

1

t

1

•z/,02 ;2 / . 0 1 1-6.99 -26.921-'6 .99 .2 / . 0 3 i*;6 . 9b2o. 94 i^6 .96 i26.941<:6.95 .

li

1

i

1t

1I

1

• i

1

151 tbCM) • Bromochloromethane152 (Df-B) • 1 ,4-Di f luorobenzene153 ILBZ) - ChIorobenzene-d5

LiniT • * luusof internal standard areaLUWER Lini T - - 'ruSot internal standard area

# Column used to Mag internal standard area values with an asterisk,

page j o f _|_

FORM (Jl I I UOA 1/b/ Rev

117

8AUQLftTILE INTERNAL STANDARD ARtA SUMMARY



Lab File ID (Standard): >D26tl4 Data Analyzed: 01/14/91


natr ix : tsoi I/water ) UIA ! ER Leve1:l Vow/med) LOUI Co lumn: t pack /cap ) QAC!^

0102030405060708091011121314151617lb192U211221

12 HOUR STD

UPPER LIMIT

LOWER LIMIT

ERA SAMPLENO.

YBLK02A5578A5579A5590A5568A5592

ISltBCM)AREA *

78044

156088

39022

789617487477870610814938163078

Rl

11.41

11.3611.3411.3611.4011.4111.42

IS21DFBJARtft *

337312

674624

168656

348767333550343684341741256192341147

R:

22.11

22. 1022.0422. 1022. 1022.1122.08

lS3tCBZ)AKtiA *

275420

55U84U

13771U

2940182B69992961712V286b226U352^328^

IRl 1

27.011

I

I

1

27.00126.98 I27.00127.00 I'J7.0H2/.01 l

l;1i1i1i1111

I11

151 tbCtl) « Bromoch loromethane152 iDr'B) • 1,4-Difluorobenzene153 IL6Z) - ChIorobenzene-d5

UPPER LIMIT » * 1UUXot internal standard areaLOWER LIMIT - - 5UHof internal standard area

# Column used to flag internal standard area values w i t h an asterisk,

page i of

FORM UII I 1X87 Re-.-

118





Instrument ID: GC/MS 0 Time Analyzed: 1423

Matrix: Isoi I/water ) WATER Leve 1 : (. low/med ) LQU Co lumn : Ipack/cap )

111 12 HOUR STD

1 UPPER LIMIT

1 LOUER LIMIT

1 EPA SAMPLE1 NO.

01 1 YBLK03021 A557703IH557204IA5572MS05 IA5572MSD06 1A55680E071 A558808lA5592ft609 1101111121131141151161171181191201211221

ISltBCM)AREA *

59156

118312

29578

805565980157385669447U226674558296765526

RT

11.39

.

11.3511.3811.3811.4011.3911.3911.3711.39

IS2CDFB)AfctA »

331306

662612

165653

347519341715309*85376441414303367446370337359706

Rl

22.02

22.0522 . 0422 . 0522.0722. U522.0522.0722.09

1S31C8ZJARLA *

278115

556230

139057

3021512V2708278920314078344088310923318630316706

IRl 1

26.95 1

1

1

11

26.98 126.94126 .94t27.00126.98 l26.96 i<;6.96 i26 .99 l

11i1i1i1i

I1

1

1

1

151 IBCP1) • Bromoch loromethane152 (DFB) - 1,4-Difluorobenzene153 ^CBZ) • ChIorobenzene-d5

UPPER LIMIT • + 1UUXo* internal standard area.LOUER LIMIT - - 5USot internal standard area.

t Column used to flag internal standard area values with an asterisk,

page I_ of _|_

FORM "J I I I UOA 1/87 Rev

119

ETC

TABUiLATED RESULTS

MOM CLE> PARAMETERS

120

FTCTABLE 1: QUANTITATIVE RESULTS and QUALITY ASSURANCE DATA


Chain of Custody Data Required for ETC Data Mana9«mwit Summary R«port» ;j

CA5571 WASTE MANAGEMENT. INC. 405 W3QU618RR '-.. 910104 0839 0 >/tTC Swigle No, C«Mpmy • - " ' , . " • Ficllity :::.:>-'':'I««iii«.i>«iirt : .';0*t^-:^; Ttoi»-^*W(Wfs^';:

NPDES.Number

ChlorideFluoride

NJ

Retults

SampleConctn,

A9/1

28.4.1

MPI.•9/1

1.0.1

JAN 30. 1991

I^JL V/ •



CA5571 WASTE MANAGEMENT. INC, 405 H3QHB18RR 9)0104 0839 0

ETC Sjmplt No, CompMy : Ficilltj- .; Smpl« p»int ft*t« -;•• •; :TM».:,:: Maufi

Compound

Sulfate as S04Total Dissolved Solids (TDSBicarbonate as CaC03Carbonate a; CaC03

R.iult*

SampleConc«n,

mg/1

20578500

MDL•9/1

2101010

JAN 30. 1991

———— i> A Vx '




CA5571 WASTE MANAGEMENT. INC. 405 W3GWB18RR 910104 0839 0El»f>»4<)

He Sample No. Company Facility Sample Point Date Time Hours

Parameter

pH Field stdpH Field stdpH Field stdpH Field stdSpecif ic Conductance Field urn/cmSpeci f ic Conductance Field urn/cmSpeci f ic Conductance Field urn/cmSpeci f ic Conductance Field urn/cmTemperature Deg (Redox Potent ia l nw

ro

R e s u l t s

SampleMeasure

6 696 656 666.68

999953976897

6 0- 88

MDL

-

JAN 16, 1991

——— MJ A V/ ———————— •



Chain of Custody D»U R*qufr*<t for £TC D**» M*n*9*m*ni Summitry B»port» :

CA5572 WASTE MWWGEMEMT, INC. 405 W3QWB7RR 910104 1046 0. ' . : . " - " . . . ' " .'.. - - • " : • • . . . - , - . . - ' glluiUf . .

ETC S«npla Mo, CMvany Ficllity lanpli taint Dit» Ti«M Aouri

NPDESNumber

ChlorideFluoride

ro-U

Results

SampleConc«n.

*3/l

53.4.2

Wtma/1

1.0.1

JAN 30, 1991

——— i^M. V/ —————————


Chain of Custody Data Rw ifred for ETC Da*» Management Summitry Report* :;

CA5572 WASTE MANAGEMENT, INC. 405 H3QWB7RR 910104 1045 0

ETC 3«nplt No, ComoMy FMcility Snplt feint Dit* tiiiii> ttouri :

Compound

Sulfate as S04Total Dissolved Solids (TDSBicarbonate as CaCOSCarbonate as CaC03

Result*

SampleConcen,

nfl/1

14518442

MDLWfl/1

2101010

JAN 30, 1991

M^ 1 \^ ————————————————————————————————————————————————————————————————————————




CA5572 WASTE MANAGEMENT. INC. 405 W3GUB7RR 910104 1045 0E 1 »p»*<t

E1C 5<*npl? No. Company Facility Sample Point Dtte Time Hours

Parameter

pH Field stdpH Field stdpH Field stdpH Field stdSpecific Conductance Field urn/cmSpecif ic Conductance Field urn/cmSpecif ic Conductance Field urn/cmSpecific Conductance Field urn/cmTemperature Deg CRedox Potential mv

ON

Results

SampleMeasure

7.387 .337 317.36

841884872893

6.3- 127

MDL

-

JAN 16, 1991

PTCTAB

JAN 30. 1991LE 1: QUANTITATIVE RESULTS and QUALITY ASSURANCE DATA


Chain of Custody Data Required for ETC Data Management Summary Report* : ;;,

CA5575 WASTE HANASD€*Tt INC: ;> ;;ITC S*mpl« Mo, CwHpmy ""'• " • ' • " • ' • :

*OS T:?--; -H3QUPlA'-;: ^1»tt«i -^^fmK^.".teflSt*:.; ••:^::,lw*It:f*lirt ltat : ..T^ |«irv:/,:

NPDESNiinbir

ChlorideFluoride

Rasi

SampleConcen.

6.2

Itc

HDL

1.0

—— J^A ^ ——————


Chain of Custody Data Required for ETC Data Man*9«merrt Summary Report*

CA5575 WASTE MANAGEMENT, INC. 405 W3QWP1A 910104 0907 0'• - • : - • . ttiHmlm

(1C 3«nple No. CoMf>»y P»clUty ; Swpl* Pftiiit ,.;0*t* "'.". limit Jteurv

Compound

Sulfate as 504Total Dissolved Solids (IDSBicarbonate as CaC03Carbonate as CaC03

K>OO

Results

SaMpI*Conc«n.

•fl/1

31426407<IO

MPL•fl/1

2101010

JAN 30, 1991

i-/ A V^ '




CA5575 WASTE MANAGEMENT. INC. 405 W3GWP1A 910104 0907 0El»p*«d

E1C S*mpl« No. Cometny Facility S*npl« Point 0*t* Time Hours

Parameter

pH i Field stdpH < Field stdpH 'F ie ld stdpH 'Field stdSpecif ic Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmTemperature Deg. CRedox Potent ial mv

NJ

Result!

SampleMeasure

7 407 .337 337 32

368408685689

7 .4+ 230

HDL

-

JAN 16. 1991

——— l^J V^ ————JAN 30. 1991



Chain of Custody Data Required for ETC Data Management Summary Report* ! i

CA5576 WASTE MANAGEMENT. INC, 405 W3QWB16RR 910104 0945 0ETC 3«npl« No. Company Facility S«npl« Peifif Oat* Ti*w Hours

NPDESNumber

ChlorideFluoride

CD

Results

SampleCone«n.

fflfl/1

167.8.1

fflS/11.0

.1

. —— t> J Vx ——————


Chain of Custody Oat* Required for ETC Data Management Summary Reports

CA5S76 WASTE MANAGEMENT, INC. 405 W3GWB16RR 910104 0945 0€TC S*np]« No. Company : Facility Sanplt Print • Oati : ti*w Hours ::

Compound


OJ

Results

SampleConceit.

•9/1

39703408<IO

MPl»»/l

2101010

JAN 30. 1991

—— J^/i ^ ————————————————————————————————————————————————————————— — ————————— 1JAN 16, 1991




CA5S76 WASTE MANAGEMENT. INC. 405 W3GWB16RR 910104 0945 0ETC S*npl* No. Compcny Facility Senple Point 0«tt Time Hours

Paramet or

pM Field stdpH i Field stdpH i Field stdpH I'Field stdSpecif ic Conductance Field urn/cmSpecif ic Conductance Field urn/cmSpecif ic Conductance Field urn/cmSpecif ic Conductance Field um/cmTemperature Deg. CRedox Potential mv

CMNJ

Result i

SampleMeasure

7 167 187 . 1 27 . 1 4

1419136713421322

8 9+ 236

HDL

-

TAB

NPDESNuiib«r

ChlorideFluoride

CM

LE 1: QUANTITATIVE RESULTS and QUALITY ASSURANCE DATA


Chain of Custody o»1a Required for ETC Data Management Summary Report* :^.:±S^:J;^.

CA5577 WASTE MANAGEMENT, INC. 40S ;;ETC Sample Ho, Company :

Haiti

StMpi*Conctn.IK/1

92.9

Itt ...y. '...

1.0.1

W3QWPSA ; »t 0 V04 tMT ftricillt7 !•*!« Point OiU .. Ita» fio&ri ••

JAN 30, 1991

LJ A Vx


Chain of Cu9<ody Data Required for ETC Data M*n*g*tn*nt SUrtrtwry Hvpwt*; . ;

CA5577 WASTE HANAQEMftfT, IWC. 405 , • • . - . . • . ;vW3QMP5A --:v9lO»i4 .:10'4i';:: /

ETC 3«np)« No. Campmy Facility Swpli Point :/ / 'ftiiti ••^•i "• .iiJ**;'' ttouri

Compound


Ratultt

SampleConcvn.

Bfl/1

141520924

fl/i2

101010

JAN 30. 1991

JL/ j ^ —— .- ——————————— . ————————— - —————————————————————————————————— _ ——— __ ——————— __


Field Parameters (QR16)Chain of Custody Data Required for ETC Data Management Summary Reports

CA5577 WASTE MANAGEMENT. INC. 405 W3GWP5A 910104 1045 0EJ*ps«d

UC 5*np]> '«'. Coflwtny Facility Simple Point D*t« Time Hours

Parameter

pH i Field stdpH 'F ie ld stdpH Field stdpH 'F ie ld stdSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecif ic Conductance 'Field um/cmTemperature Deg CRedox Potential nw

OJ

'

Resul ts

SampleMeasure

7 037 . 0 77 087 09

1742190417161713

8 .1- 81

MDL

-

JAN 16. 1991

JAN 30. 1991TABLE 1: QUANTITATIVE RESULTS and QUALITY ASSURANCE DATA


Chain of Custody Data Required for ETC Data Management Summary Report* \. ;^v^;\

CA5578 WASTE MANAGEMENT, INC. 405 W3GWP8A 910104 1100 6ETC S«npl« No. C*w>*fty : F«cIHty •• S^^ Point Dit*:Tiii»;iS<Miri

NpoesNumber

ChlorideFluoride

CMo

Retultt

SampleCoflcen,

7.5

MDt

1.0

" —— ' Us 4 Vx ' —————————


Chain of Custody Data R*qufr*d for ETC Data MaMgMMfrt SuiiiiiffW:&*fH>fo-^^^^^^^ •'••

CA5578 WASTE MANAGEMENT, INC. 40S ^ETC SfJtpJv ND * •. - . CWB'MIl' "- - - - - ' - ' " '•' '.'-!"''!.. '• .i1 • - • • "

MftflBWW. m -?*1 0 f $4 ]?11 JNi l : • :-;-:x- 'v.. FKUHrG-.: y:'::V;:lppi»;«*l rt-'iv.-Oit* :.-. :;:;:'Tiii ::knrarK -::';::'

Compound


•• K«ttlt* .:;:;,'•-./ ":

SampleConc«ii.

19689702

•9/12

101010

- v .-.-': - ' '-.- '.v. '

JAN 30, 1991

——— U M. V^ -



Chain of Custody Data Requked for ETC Data Management Summary Reports

CA5578 WASTE MANAGEMEOT . INC. 405 W3GWP8A 910104 1100 0Ellp»«0

ETC Sample No. Company Facility Simple Point Date Time Hour*

Parameter

pH Field stdpH Field stdpH Field stdpH Field stdSpecific Conductance i Field urn/cmSpecif ic Conductance i Field urn/cmSpecific Conductance Field urn/cmSpecif ic Conductance i Field urn/cmTemperature Deg CRedox Potential mv

CMoo

Resu l ts

SampleMeasure

6.676 636.626 64

1332131513071268

6 . 1* 133

MDL

-

JAN 16. 1991

M^J. V/ ——— " ————————————————————————— ' ——————————————————————————————————————————————




CASS79 WASTE MANAGEMENT, INC. 405 W3QWB7RR 910104 1045 0

ETC Sample No. Compiny Facility S«q>l« taint Oit« TUM : Hours

NPDESNwmtotr

ChlorideFluoride

01

Results

SampleConcen.

"9/1

69.6.3

MDl.

t . O.1

JAN 30, 1991

*



CA5S79 WASTE MANAGEMENT. INC. 405 W3QWB7RR 910104 104$ 0

ETC Swnple No. C«*piny F»cilitr Imqtlm feint Dal* Ttaw ttwir*

Compound

Sulfate as 504Total Dissolved Solids (TDSBicarbonate as CaC03Carbonate as CaC03

O

RtiulU

SampleConc*n.

•9/1

6SBO418

MDL•0/1

2101010

JAN 30. 1991

ETCJAN 16. 1991


Field Parameters (QR16)Chain of Custody Data Requked for ETC Data Management Summary Reports

CA5579 WASTE MANAGEMENT. INC. 405 W3GWB7RR 910104 1045 0El*(tt*<t

ETC ;*npj. Mo. Compiny Facility Simple Point t>«te Tint Hour*

Parameter

pH (Field stdpH 'Field stdpH ' Field stdpH ' Field stdSpecif ic Conductance (Field um/cmSpecif ic Conductance (Field um/cmSpecif ic Conductance (Field um/cmSpecif ic Conductance (Field um/cmTemperature Deg . CRedox Potent ia l mv

Resul ts

SampleMeasure

7 387 337 . 3 17 36

841884872893

6 3* 188

MDL

---------

——— i> M. Vx —————————


Conventional Analysis Data (QR10)Chita of Custody DM* Required for ETC Out* M»M9emwt Summitry Reports

CA5580 WASTE MANAGEMENT. INC. 405 W3QWP1B 910104FTC Simple No. Cempwiy Ficilit)> Sii il* Hint Oit* :iii» :: ffiufiT ::

NPOESNumbtr

ChlorideFluorlde

ro

ftetalft

Samp ItConcen.

mg/l5.2

.. wi -;.;."• ••fl/l V

1.0.1

JAN 30. 1991

ETCTABLE 1: MISCELLANEOUS DATA (QR64)

JAN 30. 1991

Compound

RttUlU

SawrUCo lie en.•9/1

Sulfate as S04Total Dissolved SolidsBicarbonate as CaC03Carbonate as CaC03

(IDS31

910868< J O

2101010

CM

———— Ls M. \*s m




CA5580 WASTE MANAGEMENT. INC. 405 W3GWP1B 910104 1213 0ETC S*mpl* MQ. Company Facility S*mple Point Oat* Time Hours

Parameter

pH Field stdpH Field stdpH Field stdpH Field stdSpecif ic Conductance Field urn/cmSpeci f ic Conductance Field urn/cmSpecif ic Conductance Field urn/cmSpecific Conductance Field urn/cmTemperature Deg CRedox Potential mv

-C*

Resul ts

SampleMeasure

6.906 916 826 86

1576167616991716

3 5+ 87

MDl

-

JAN 16. 1991



Chain of Custody Data Required for ETC Data M«n*g*mwH Summary .Reports.

CA5S81 WASTE MANAGEMENT , INC. 405 W30UP21S 910104 t3U 0

€TC Sample Mo, Company pjcility Swspli Point D«t« Tl«i» Houri

NPDESNumber

ChlorideFluoride

LP

Remits

SampleConccn,

35.9.1

MPt•9/1

1.0.1

JAN 30. 1991

—— i>-I ^y ——————


Chain of Cu»to«y Oat* n*quk*d for CTC

CA5581 WASTE MANAGEMENT, INC.(1C Sample No . Company . : . . . ' . - . Facility \: ...;• SMJiM :<<ip»i

T HapwW •__•;.; ;. .. •;•" :;;'.":;.;. ''•

4t0104 )314 :.llrti .Bil*' ':: :.f:lit:>:./H«ir*'.-:;:./

Compound


ON

mumSaWlpU

Conctn,

12385235

'•""'•fl/i.'1:1--

2101010

JAN 30. 1991

'.•;:.-?.:•?,.. '.'f. '.•'.;•;::..;;;.: -\\-.-,

ETCJAN 16. 1991



pHpHpHpM

FieldFieldFieldField

Chain of Custody Data Requked for ETC Data Management Summary Reports

CA5581 WASTE MANAGEMENT. INC. 405 W3GWPZI5 910104 1314 0ETC Sample t4o . Company Facility S*npl« Point Djt* Time Hours

Parameter

stdstdstdstd

Specif ic Conductance Field urn/ cmSpecific Conductance Field urn/cmSpecif ic Conductance Field urn/cmSpecific Conductance Field urn/cmTemperature Deg. CRedox Potential mvRedox Potential mvRedox Potential mvRedox Potent ia l mv

Resu l ts

SampleMeasure

7.757.607 .617.59

782788778776

9 8+ 188* 188+ 192* 196

MDL

------------



ch»tn of cu>t Kly Dirt* Requh-w) 'for ETC D*U Mw»8«t»trrt Stimnrtry n*por t»

CA5582 WASTE MANAGEMENT, INfc :^ -I'i: ,; 4 -V :. ^Ml:«y|it|i| i;iJM«tt*:t1^SlS:>-ITC S«nple No. ' - Compmy ...,;-. '.. - - . . : . ; •- •'. >:.:;.. : tttt ::li liJ^

NPDESNunbtr

ChlorideFluoride

-t^oo

ft*C4ilit

SampleCoiicvn.

m«/l

17.7

.HML'••-.»•/ IV:-

1.0

JAN 30. 199T



CA5582 WASTE MANAGEMENT. INC. 405 W3QWPZ14 9101041755 0

ETC 8«npl« No. CoMpwiy ; Facility . ::.;.Ia^i]» f»iiit: || Data tlib ; wuiV

Compound


Recti

Sampl«Concen.

•0/1

21345222

It*

HDL

2101010

JAN 30, 1991

—— 1_>M. \^ ———————JAN 16. 1991




CA5582 WASTE MANAGEMENT. INC. 405 W3GWPZ14 910104 1755 0ETC Sonple No. Company Facility 3*mpl* Point D«t« Tine Hours

Parameter

pH FieldpH Field'pH FieldpH FieldSpecific ConductanSpecif ic ConductanSpecific ConductanSpecific ConductanTemperatureRedox PotentialRedox PotentialRedox PotentialRedox Potential

t

cno

stdstdstdstd

ce Field um/cmce Field um/cmce Field um/cmce Field um/cm

Deg Cmvmvmvmv

Results

SampleMeasure

7.367.367 .327.40

771689694685

8.5224224223223

MDL

-

PTC

TAB

NPDESNumtoir


Conventional Analysis Data (QR10)Chain of Cu»iody Data Required for ETC D*U Man*9am«rrt Summary Reporter ::

CA5S83 WASTE MANAGEMENT. INC. 405 X3QWFB 910(07 0830 0

ETC S*npl« No. CoMp<*>y F»ctlltjr S*npl« taint Dit«:; ttaii •.. (teur»'

ChlorideFluoride

cn

Retultt

SampleConctn, HPl

1.0.1

JAN 30. 1991

——— i> J V> —————————



CA5583 WASTE MANAGEMENT, INC. 405 X3GWFB 91010? 0830 0.• • • " • " " • . • • . • . • . : . . . . . ' . " . . . • • . y.." ' .. ' . • - , . ' - : ' .':'.''•. - tiiwwi '

ETC S*mpl« Ho. C«nf>«iy ' FKillty Irn l* >»l4it Bit* ;•.• .:; •'••1'^^tlHStF^. •

Compound


cnro

Results

SampleConceit.

•9/1

<214

<10<10

MPt•fl/1

2101010

JAN 30. 1991

M^A \~>



Chain of CwtwJy Data Required fgr ETCDa*« Mim9<

CA5585 WASTE MANAGEMENT, INC, 405 ; ;ETC S«npJ« No. Cewpwftr •

fnefif 9uiwiMfy Hiipoi (i :'':" :/: l^-'-^i^:-^'-'-'-' '':':: ~

•• Ficilltjr : •;,•;>:;;•. •it«j(iW;,ffI»f:..xvi, Oil* ;/.;:...;-:?.**. .. .flKi.*...; .

NPDESNiimbtr

ChlorideFluoride

cnt/j

. . Reiultt ...-.;..;., . - ' • • ' '- ' '" ••••••"••" '• '• ' - • - - • • • • • • • • • - - • • • • • • • - -••••••———— —— - ••••••-•••••••.

SampleConc«n,

•0/1«y/ *

16.1

ma/imy/ A

1.0

JAN 30, 1991


Chain of Custody D«t« n*qufr«4 for ETC ° MW*i!*«:f«S*CA558S HASTE H«lWfir«irrI*C;v^^

ETC Sample No. C«i»piny '.\ -•- •.-.;;• . - • • Pw:;liitirVi; ; r:;,.,l-iiii»iii!i/ji*iiit; -:i,iMi4r'::

Compound


en

Retu

Sample

*wn16

452343

m, . . . • . : . . -

2101010

JAN 30, 1991

J->. 1 sm




CA5585 WASTE MANAGEMENT. INC. 405 U3GWP218 9)0167 0900 0Etc Simple No. Cwwiny FiciHty Sanplc Point Oite Time Hours

Parameter

pH 1 Field; stdpH (Field stdpH i Field stdpH i Field! stdSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmTemperature Deg. (Redox Potential mv

cnen

RatulU

SampleMeasure

7.167.257.307.35

657664656675

6.1+ 249

MDL

-

JAN 18. 1991

•• • • • . • -—.- . . .-.. •:•.••:•:•'•' •/• :•:•;•-•• •--

FTCJAN 30. 1991


Conventional Analysis Data (QR10)Chain of Custody Data Required for ETC Data Management Summary Report* :

CA5586 WASTE MANAGEMENT. INC. 405 W3QWPZ21S 910107 0

tTC Simple No, CfMptny Facility \. .. >Mpl« hint: Qati Tfai* . rtaufi

NPDESNumber

ChlorideFluoride

cnON

Results

SampleConcen,••9/1

15.1.4

HDL

1.0.1


Chain of Cu»to<Jy Data Required for ETC Data MaiwgemwH Suroma;

CA5586 WASTE MANAGEMENT, INC. .' ;; ." ... .'405 'f^jj :f iipi*iilj|ETC 3«npl* HP. CoMpifly

•• ::'; &10l0? '''v'1;' ''' fl

-.. . •- : • ; • • • . . . . • . . . . • • : • • : . FKiUt f **:"*^ tmv^i&wiv;:-

Compound

Sulfate as S04Total Dissolved Solids (IDSBicarbonate as CaC03Carbonate a* CaC03

t

en

Sample

mo/187

602449

Sh101010

JAN 30. 1991

<:'•:: -:?--m :^>

—— I_J A ^ ——————————————————————————————————————————— _ ——————————




CA5586 WASTE MANAGEMENT. INC. 405 U3GMP221S 91010? 0E1.MMHU -

ETC Sample No, Conpifiy Facility Soipl* Point 0«t« linw Hours

Parameter

pH i Field' stdpH i Field, stdpH Field stdpH (Field stdSpecific Conductance Field urn/ cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmTemperature Deg. CRedox Potential mv

trtOO

Result*

SampleMeasure

7. S37.637.647.66

1228967972994

3.0+ 227

HDL

-

•

——————

JAN 18. 1991



Chain of Custody Data Required for ETC Data Management Summary lteport»

CA5587 WASTE MANAGEMENT. INC. 405 W3QWPZIO 910107 1525 0. . - . " • - • • ' • / • . • --•EUfeiiiif •

ETC Sample No, Company Ficility Svipl* Point B»t* ttat Hauri

NPDESNuHtotr

ChlorideFluoride

cn

Results

SampleConceit,

mg/112.4

.1

WDt :-;

1.0.1

JAN 30. 1991

——— 1^ A Vx —————————



CA5587 WASTE MANAGEMENT. INC. 405 W3QUPZIO 910107 1525 0

ETC Swiple No. C<M»»y Facility S«ipl« Pflint Oat* ltm» (tours

Compound


O

Retultt

SampleConceit.

22353276

MPL•0/1

2101010

JAN 30. 1991

—— Is .

pMPHPH

i. V/ '

FieldFieldField

pH (Field



Chain of Custody Dili* Required for ETC Data Management Summary Reports

CA5587 WASTE MANAGEMENT. INC. 405 W30WPZIO 910107 I S 2 & 0

ETC Sample No, Company F«clllty SHB)!* taint 0«t« TbM Houra

Parameter

stdstdstdstd

Specific Conductance Field um/cmSpecific Conductance Field um/cmSpecific Conductance Field um/cmSpecif ic Conductance Field um/cmTemperature Deg. CRedox Potential mv

Results

SampleMeasure

7.497 407.407.40

661675666563

6.3+ 239

MDl

_--------

JAN 18, 1991



Chain of Custody D*t« Required for ETC Data Management Summary n«port» :

CA5594 WASTE MANAGEMEffT, IMC. 405 W3QWPZi800P 9t0107 0900 6ETC S«nple No. Compiny Facility Sopli Point B»t« HUM Hours

NPDESNumtotr

ChlorideFluorlde

ro

Rtiulti

SampleConctn.

IB9/1

16.6.1

MDL

t . O

JAN 30. 1991

JUJ Vx


Chain of custody Data Required for ETC Data Management Summary Report*

CA5594 WASTE MANAGEMENT. INC. 405 W3QWPZI8DUP 910107

ETC S«nple No. C««p«y ' . ' : ; .. . . . . . . . -'.. • • . • • " • •.. teiHt7l\:;: .\ii ^^^?^*»ii :':

Compound


ONCM

Rttulti

SampleConctn.

•9/116

468340<10

W>U•fl/l

2101010

WOO 0ri ^SS1HW'*. ; • :

JAN 30, 1991




CA5594 WASTE MANAGEMENT. INC. 405 W3QWr*Zt80UP 910107 0900 0ETC Sample No. Company Facility Sonpl* Point Dat« tint* ttouri .

Parameter

pH i Field stdpH i Field stdpH i Field, stdpH Field stdSpecific Conductance Field urn/ cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmTemperature Deg. CRedox Potential mv

O\-fe.

Result*

SampleMe aj a re

7.167.257.307.35

657664656675

6. t+ 249

MDl

-

JAN 18. 1991

-FTCJAN 30, 1991


NPDESNumber

ChlorideFluoride

O"\

Conventional Analysis Data (QR10)Chain of Custody Data Required for ETC Data Management Summary Reports

CA5595 WASTE MANAGEMENT. INC. 405 W3GWP2IO 910107 0ETC Sample No, Cempmy Ficllitf : 3«*»1« Point 0*1« limit Heufi

Rftittltt

SampleConceit,

fflfl/1

9 1.1

MDL•0/1

1.0.1

——— ' M*fM. \*s —————————


Chain of Custody D»ta Required for ETC Data Management Summary Report*

CA5595 WASTE MANMSEMCtfr. INC. - ... 405 -^'^'^S^ETC Sample No, ; C«npi»y:-.-/ ' • • •O.v .v ' : .• '• .• ' / ; . / • : • .> • .• pvMiii w '''"''' :':":'' :'''"ai ii.::ilK i

'.."' *•;-•• : ::•••,->• •;:•.••"*! . - . . : . - • . - . -"i-1""1 '"' n" i1'1 '"' """"' ' T'* ' '" *«*l''* '-"i-

Compound


ONON

R"°1U

Conceit.

ttn

cn

i—

»O

tls>

«oo

Msx

n

*• ¥ •»/ * :

2101010

JAN 30, 1991

JU -




CA5595 WASTE MANAGEMENT. INC. 405 W3QWPZIO 9)0107 0

EIC Sample No, Company Facility 3«npl« Point 0»t» Ttaw rtours

Parameter

pH I Field; stdpH I Field stdpH i Field < stdpH i Field stdSpecific Conductance Field um/cmSpecific Conductance Field um/cmSpecific Conductance Field um/cmSpecific Conductance Field um/cmTemperature Deg. CRedox Potential mv

ON

Results

SampleHeaiure

7 207 127.147 07

1150113911411142

7 8* 241

HDt

-

JAN 18. 1991

——— IsM. Vx —————————

TAB

NPDESNumber




CA5S96 WASTE MANAGEMENT. INC. 405 W3GMPZ9 910107 1546 0

ETC Sample Ng, Company Facility lo ilt Point Oit* T taw : Hour »

ChlorideFluoride

ONCO

R««ults

SampleConceit .

"9/1

5.6.1

MDL•9/1

1.0.1

JAN 30. 1991

—— i>.f V, ——————

Compoun.


Chain of Custody D«t« Required for ETC DaU Man»»emwrt Summary Bepofts

CA5596 WASTE MAMAQENEtfT, 1NCV:^::V:; ;. MS :;:;5ETC S«npJe Mo, CoMf>»y / ':

ri

Sulfate as SO 4Total Dissolved Solids (TDSBicarbonate as CaCOSCarbonate as CaC03

&\

Rtttu

SAMple •Conc*n,

•fl/128

494396

JU

•'••-:;»i -•-:,:•ff/i2

101010

iiiifi :; Picintj- iMpl* Hifti.:;.;;: Oit* ::>>>:. ftt*":*SSu

JAN 30, 1991

i>.A V/ •


Field Parameters (QR16)Chain o* Custody O»t« Required for ETC D«t« Mwwgemwrt Summary Report*

CA5596 WASTE MANAGEMENT. INC. 405ETC Sample Ho, Compmy P«ellitjr-:r:;

Parameter

pH i Field) stdpH i Field stdpH Field stdpH Field stdSpecific Conductance Field urn/ cmSpecific Conductance Field urn/ cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmTemperature Deg. CRedox Potential mv

^1O

Ret til tt

Sampl*M»«»ur«

7.137.107.117 12

668679680680

7.0+ 167

::S |;f::::'

-

W30WPZ9»« l« Pfli

910107 1545 f :• i • ' '»". ' •>.•.••: •."••.-_ ; .-:-". -:.:ll*jMHW'M ."«•-••:. D«t« .'ii ./Iiwr^vltoufVi.v...

JAN 18. 1991

^ /*"OHM Corporation

Environmental TestingCertification Corp.

Summary Package

for


Ctitin of Cuttoty &•?* Atqufrttf for STC O*t» Alanaf•m«n* Sairmmy fftporf tCA4331,CA6020,CA6022,CA6023 WASTE MANAGEMENT, INC, 405

ETC NO. Company Simp/t Point Dtt* T/m» Hour*

Richard P. Alb«rtV/ct Pntidtnt. Q*n»r»l M»n»g»r

Thu• 284 Raritan Center Parkway

Report if «r> INSITE*" Mrvie* gmcr«t«d by LODESTAR*1 Data Harwmnt ,SoftMfr».iv • CN 7808 • Edison. Ne* Jersey 08818-7808 1^ 201.23-3600

ETCSDG NARRATIVE

This technical report submitted by ETC Corporation contains theanalytical results and required deliverables for HASTE MANAGEMENT,INC. Site 405 samples as identified below:

ETC IDCA4381CA6020

CLIENT ID3GHPZ22D3GWP222S

ETC IDCA6022CA6023

CLIENT ID3GWP3A02TB


Problems were not observed during the analysis of these samples.

f Total Dissolved Solids^:

Holding time for this analysis is 48 hours as per the site QualityAssurance Project Plan. Sample CA4381 (3GWPZ22D) was sampled onFriday February 15, 1991, the shuttle received at DonahueLaboratories on Saturday and was not opened until Monday, February18, 1991. As per telephone conversation between Dan Green of PELAand Robin Goebel of ETC Corp. on February 15, 1991, the analysiswas performed outside of holding tine.


GregorVc. MorrisonLaboratory Manager

Date

rii* * oootic


ERA SAMPLE NO,


Lab Code: Case No.:

Cont ract

SAS No.

Matrix: tsoi1/water) UATER

Sample wt/vo1: 9.0

Level : '. low/med J LOU



CgXmL) ML

CAS NO. COMPOUND

SDG No.:

Lab Sample ID: CR4331U

Lab File ID: >C2524

Date Received: 02/*/91

Date Analyzed: 02>-'21--'91

Di lut ion Factor:

CONCENTRATION UNITS:Cug/L or ug/Kgj UG/L Q

I74-87-3 ——————— Chlorome thane_____________t 1074-83-9 — — — ---Bromome thane______________I 1075-01-4-——————Uinyl Chloride____________I 1075-00-3 ——————— Chlo roe thane______________ 11075-09-2 ——————— Methyl one Chloride________1567-64-1 ——————— Acetone__________________11075-15-0 ——————— Carbon Disulf ide__________1575-35-4——— —— --1,1-0ichloroethene________1575-34-3———————1,1-Dichloroethana________15540-59-0——————1,2-Dichlorethene (total )__15267-66-3 ——————— Chloroform________________15107-06-2 —————— 1,2-Dicnloroethana________1578-93-3 ——————— 2-Butanone________________11071-55-6 ——————— 1,1,1-Trichloroe thane______1556-23-5-- ——— —— Carbon Tetrach lor id*_______15108-05-4——————Uinyl Acetate_____________I 1075-27-4-——————Bromodich loromathane_______1578-87-5 ——————— 1,2-Dichloropropane________1510061-01-5 ————ci»-l,3-Dich loropropene____1579-01-6 ——— --- — Tr ich loroe thene___________13124-48-1 — ————— Dibromochlorome thane_______1579-00-5 ——————— 1,1,2-Trichloroethane______1571-43-2 ——————— Benzane__________________1510061-02-6------trans-l,3-Dichloropropene__1575-25-2---- — —— Bromoform_________________15108-10-1 ————— — 4-Methyl-2-Pentanone_______110591-78-6 —————— 2-Hexanone________________110127-18-4- —— -- — Tetrach loroe thene_________1579-34-5———————1,1,2,2-Tetrach loroe thane__15108-88-3 —————— Toluene__________________!5108-90-7——- —— -Chlorobenzene___________ 15100-41-4——————Ethyl benzene______________15100-42-5 —————— Styrene__________________151330-20-7——————Xylene (total)___________15_______________________________________I__

IIUtuIUIUIUIUIUIUIUIIUIUIUIUtuIUIUIUIUIJIUIUIUIUtuIUIUIUIUIUIUIUIUIU

1A__VOIATJIX OMMXCS ANALYSIS DATA MRTT t?A SAK9U NO.

NA»AI

CAM Jt«.lMatrix: fioil/vattr) 6U»Ttt.Itapl* wt/voi; ^ fg/aii mL

I Noisturti nttColuan:

Uft SABS4A 10:

U* filA XO;

OACADAtA

CM NO. COMPOUND

dilution FtetAr:CQNC&fTXATXOIf ONXTS(itf/L •r uf/Kf j

TAtrAhydrofurAA .1

i/lt ft«v.

IEVOLATILE ORGAN ICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE NO.

IA4381Lab Name:£TCNJ

Lab Code: Case No.:

Matrix: tsoiI/water) WATER

Sample wt/vol: 5.0 <g/mL> ML

Level: (low/mod) LOU


Column: (pack^cap > PACK


Cont ract:

SAS No.: SDG Mo.:

Lab Sample ID: CA4381*,'

Lab File ID: >C2524

Date Received: 02/1* ---91

Date Analyzed: C(2/'21--*91



CAS NUMBER

01. 108-20-3

COMPOUND NAME

Diisopropyl ether (DOT)

RT

19.79

EST. CONC

eQ

J

FORM I VGA-TIC 1/87 Rev


ERA SAMPLE NO.


Lab Code: Case No.:

Cont ract :

SAS No.:

Ma t rix: (soi1/wa t er) WATER

Sample wt/^ol: 5.0

Leve 1 : t low/mad) LOUI


Column: (pack/capJ PACK

Cg/mL) ML

SDG No.:


Lab File ID: >C2525

Date Received: 02--W/91

Date Analyzed: 02--21--91

Di lut ion Fac tor: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:lug/L or ugxKg) UG/L Q

174-87-3 —————74-83-9 ------75-01-4 —————75-00-3 —————75-09-2 —————67-64-1 —————75-15-0 —————75-35-4 —————75-34-3 —————540-59-0 ————67-66-3 —————107-06-2 ————78-93-3 —————71-55-6 —————56-23-5 —————108-05-4 ————75-27-4 —————78-87-5 —————10061-01-5 ——79-01-6 —————124-48-1 ————79-00-5 —————71-43-2 —————10061-02-6 ——75-25-2 —————108-10-1 ————591-78-6 ————127-18-4 ————79-34-5 —————108-88-3 ————108-90-7 ————100-41-4 ————100-42-5 ————1330-20-7 ———

1---Ch lo pome thane 1---Bramoma thane 1—— Uinyl Chloride 1— -Chloroethane t---Methulene Chloride 1— -Acetone I---Carbon Diaulfide_, __... 1—— 1.1-Diehloraethene 1- — 1 rl-Dichlaroethane , t—— 1,2-Dichlorethene (total ) __ 1—— Chloroform 1---1.2-Dieh lor oe thane 1—— 2-Butanone 1— -1 . lrl-Tr ichlo roe thane 1—— -Carbon Tat rachlor ide 1- — Uinyl Acetate 1—— Bromadichlorome thane 1---1 r2-Diehloreprapane 1—— cis-1 ,3-Dichloropropene ____ t— -Trichloroethene. _ 1---Dibromoch lorome thane 1—— 1.1.2-Tr iehlo roe thane 1—— Benzene 1— -trana-l,3-Dich loropropene __ 1---Bromoform 1_--4-Methyl-2-Pentanone 1— -2-Hexenone , 1- — Tet raehlaroethene , , 1— -1,1,2, 2-Tetrach loroe thane __ 1---To luene 1—— Chlorobenzene 1—— Eth-jl benzene 1---Styrene I—— Xylene (total) 1

\

10101010532555215510551055555555510105525555

1 11U t1UIUIUIU1IUIUIU1iUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1UIUIUIUIJIUIU1U ciu b1

1Avolant! oftOAjrxcj AXAI.YSZ* DATA sntt

are Cantrmet:cadat ^___ caaa Na.

Matrix: (aoii/vatar) OJfrTifeSaapla vt/voi:tavali (lov/vad)t Moiaturai net dac.Column: (pack/cap)

CU NO COMPOUND

tooUft S4»plt 10:

Ub rila 10:

Data Kaeaivad: <*M<*\Data Analysad:

dilutionCONCZNTKATION

or

Tatrahydrofuran

1/17

IEUQLATlLE ORGANICS ANALYSIS DATA SHEET


Lab Name:ETCNJ

Lab Code: Case No.:

Matrix: Iso i !.-• water ) LJATER

Sample ut/vol: 5.0 Cg/mL) ML

Leve1: C1ou/med) LOW




Cent ract:

SAS No.:

EPA SAMPLE HO,

IIA6020I_____

SDG No.:


Lab File ID: >C2525

Date Received: 02--'|9--'91

Date Analyzed: 02^21--'9 i

Dilution Factor: i.Q

CONCENTRATION UNITS:CugXL or ug/Kg) UG/L


FORM I UOA-TIC

RT EST. CQNC

1/87r

Q

Rev.

?


EPA SAMPLE NO


Lab Code: Case No.:

Matrix: tsoi1/water) WATER


Le^e 1: ( low/mod .' LOUJ


Co 1 umn : ', pack/cap ) PACK

Cont ract :

SAS No.: SDG No.:

Lab Sample ID: CA6Q22U

Lab File ID: >C2526

Date Received: Q2/J&/91


Di lution Factor: 1

CAS NO. COMPOUNDCONCENTRATION UNITS:Cug/L or ug/Kg) UG/L

74-87-3- ——— -- — Ch loromethane_____________I 1074-83-9-- ——— —— Bromome thane______________11075-01-4———————Uinyl Chloride____________11075-00-3 ——————— Chlo roe thane______________11075-09-2 ——————— Methylene Chloride________1567-64-1———————Acetona__________________12575-15-0 ——————— Carbon Disulf ide__________1575-35-4———————1,1-D i chlo roe thene________1575-34-3———————1,1-Dichloroethane________15540-59-0——————1,2-Dich lor. thane (total)__1567-66-3--——- —— Chloroform_______________15107-06-2 —————— 1,2-Dichloroethane________1578-93-3 ——————— 2-Butanona________________11071-55-6 ——————— 1,1,1-Trichloroe thane______1556-23-5- —————— Carbon Tatraeh lor ide 15108-05-4——————Uinyl Acetate_____________11075-27-4———————Bromodichloromethane_______1578-87-5 ——————— 1,2-Dichloropropane________1510061-01-5--—•—ci*-l,3-Dich loropropene____1579-01-6 ——— ———— Tr ich loroe thene___________15124-48-1————————Dibrnmoeh loromathana 1579-00-5 ——————— 1,1,2-Tr ich loroe thane______1571-43-2 ——————— Benzene__________________1510061-02-6——-—tran»-l,3-Dich loropropene__1575-25-2-- —— -- — Bromof orm _________15108-10-1 —————— 4-Methyl-2-Pentanone_______110591-78-6 —————— 2-Hexanone________________I 10127-18-4——————Tetrach loroe thene_________1579-34-5———————1,1,2,2-Tetrach loroe thane__15108-88-3 —————— Toluene__________________15108-90-7———— —— Chlorobenzene_____________15100-41-4——————Ethyl benzene______________15100-42-5 —————— Styrene__________________151330-20-7—————Xylane (total)___________15_______________________________________I__

Q

IUIIIIUIUIUIIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU

1AVeXATXLX OMAffXCS AMAX.YSXJ DATA NO.

notColuan: (paex/capj

CAS NO.

dilution Factor:CQNCZVTXATXON OWTlij-numjuii-jL »w»^w*«*ff40p yjnTJi

COK'«WO (ttf/t 0» Of/Ml Mg/L

Totrahydrofuran

I/IT JUv

9



EPA SAMPLE NO.

Lab NemesETCNJ

Lab Code: Case No.:

Mat r ix: Cso i1/water) WATER




Co lumn : (pack/cap ) PACK

Number TICs found: X

A6022Contract '•

SAS No.: SDG No.:

Lab Sample ID: CA6022'J

Lab File ID: >C2526

Date Received: 02-'Jo '91

Date Analyzed: 02--21--'*!


CONCENTRATION UNITS:Cug/L or ug/Kg ') UG/L

CAS NUMBER

01. 75-69-4

COMPOUND NAME

Methane, trichlorofluoro-

RT

9.44

EST. CONC

9

Q

J

FORM I UOA-TIC 1/87

10


EPA SAMPLE NO.

Lab Name: ETCNJ

Lab Code: Case No. :

Matrix: (soi 1 /water) WATER

Sample wt/vol! 5.0 Cg/mL) ML

Lave 1 : ( low/med ) LOUt


Co lumn : C pack/cap ) PACK

CAS NO. COMPOUND

IA6023Contract: I_________

SAS No.: SDG No.:

Lab Sample ID: CA6023U2

Lab File ID: >C2535

Date Received: Q2--JO/91


Dilution Factor: 1

CONCENTRATION UNITS:(ug/L or ug/Kg) UG/L Q

74-87-3 ——————— Chlorome thane_____________I 1074-83-9 — —————— Bromomethane______________11075-01-4———————vinyl Chloride____________I 1075-00-3 ——————— Chlo roe thane______________11075-09-2 ——————— Me thy lane Chloride________1567-64-1———————Acetone__________________12575-15-0 ——————— Carbon Disulf ide__________1575-35-4———————1,1-Dichloroethene________1575-34-3———————1,1-Dichloroe thane________15540-59-0 —————— 1,2-Dichlorethene (total)__1567-66-3 ——————— Chloroform________________15107-06-2 —————— 1,2-Dichloroethane________1578-93-3———————2-Butanone_______________11071-55-6 ——————— 1,1,1-Trichloroe thane______1556-23-5———————Carbon Tet rach lor ide______15108-05-4——————Uinyl Acetate_____________11075-27-4-——————• -••Bramodieh 1 aroma thane 1578-87-5 — -« ——— l,2-Dichloropropane__^._____1510061-01-5—————eim-1 .3-DiehloroprQpena 1579-01-6———————Trichloroethene___________15124-48-1————————DibrQmoehlorama thane 1579-00-5 ——————— 1,1,2-Trichlo roe thane______1571-43-2———————Benzene_________________1510061-02-6————tran»-l,3-Dichloropropen«__1575-25-2 ——————— Bromoform_____.___________15108-10-1——————4-Methyl-2-Pentanone_______110591-78-6 —————— 2-Hexanone________________110127-18-4-- ———— -Tetrechloroethene_________1579-34-5 ——————— 1,1,2,2-Tetrach loroethane__15108-88-3 —————— Toluene__________________15108-90-7———- — -Chlorobenzene_____________15100-41-4——————Ethyl benzene______________15100-42-5——————Styrene__________________15

I 1330-20-7——————Xylene (total )___________15I ___________ ._..___________________I_

1UIDtuIUIUiIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUtuIUIUIUIUIUIUIUI

FORM I UOA11

1/87 Rev.

1AVOtATJIX OMAffXCS ANALYSt* DATA SHttT

Cantraeti

«PA aAKPU KO.

Late cotfoi eaM No.iMatrix: (aoil/vatori 6U*TBe.Staple wt/vol: ? fg/mLiLaval: (lov/aod) .I Moisturat not doe.Column: (pack/cap]

CU HO. COMPOUND

SAJ Mo.i

Tatrahydrofuran

Lab s a l a tOiLab FHa 10:Data ftacaivad:Data Analysad:'•Dilution Factor:

coifccmurxoit(uf/t or

JD

1/17 Ktv,

12



Lab NamesETCNJ

Lab Code: Case No.:

Matrix: (soi1/water) WATER


Leve1: I 1ow/med) LQU


Co 1umn: (pack/cap) PACK


EPA SAMPLE NO.

A6023Cont ract '•

SAS No.: SDG No.;

Lab Sample ID: CA6Q2JU2

Lab File ID: >C257?

Date Received: 02/Jo'91

Date Analyzed: 02/22^91



1CAS NUMBER

01. 75-69-4

COMPOUND NAME

Methane , trichlorof luoro-

. .

RT

9.60

1EST. CONC t Q

10 IJ1t1!11111111111

. t

111111t1111!11

FORM I "JOA-TIC

Lab Name: ETCNJ

Lab Code:

2AUIATER UOLATILE SURROGATE RECOUERY

Contract'

Case No.: SAS No.: SOG No

1 ERA1 SAMPLE NO.

Oil UBLK01021 A9766031 A9769041 A4381091 A602006 t A6022071 A975308 1 UBLK02091 A6023101 A9755111 UBLK03121 A9794MS13 1 UBLK04141 A9794MSD19 1 A9794161171181191201211221231241251261271281291301

SI(TOD*

97999896999496101100100100104979999

52CBFB5*

9893979694969610199100991089610196

S3CDCE)*

8990898684868294999896109939388

OTHER TOTOUT

000000000000000

page 1 of

51 CTOL) • Toluene-de52 (BFB) - Bromofluorobenzene53 (DCE) - l,2-Dichloroethene-d4

QC LIMITS(88-110)(86-119)(76-114)

* Column to ba used to flag* Ualues outside QC limitsD Surrogates diluted out

recovery values

FORM II UOA -1

14

1x87 Rev.

3AWATER VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY


Lab Code: Caaa No.: SAS No.: SOG No.:

Matrix Spika - EPA Samp la No.: A5754

COMPOUND

1 ,1-Dichlaroathena mu —iTr ieh loro«th«n* __ (i _ ___Banzene_ ,_ _Tolu«n«ChlnrobanzanB

SPIKEADDEDCug/L)

90.00090.00050.00090.00090.000

SAMPLECONCENTRATION

(ug/L)

0.0000.0000.0000.0000.000

MSCONCENTRATION

Cug/L>

57.11746.09556.47252.08248.997

MS 1 QC* ILIMITS

REC *l REC.

114 161-14592 171-120113 176-127104 176-12598 175-130

1

COMPOUND

1 f 1-Diehloroathena _ „Tr iehloroathena_ „ __. im .BmnzmnmToluanaChlorobanzana

SPIKEADDEDCug/L)

50.00050.00050.00050.00050.000

MSDCONCENTRATION

(ug/L)

52.18944.29250.48547.88048.315

MSDHREC *

104891019697

HRPD *

941161

QC LIMITSRPD 1 REC.

14 161-14514 171-12011 176-12713 176-12513 175-130

1

t Column to ba uaad to flag racovary and RPD value* with an asterisk

* Values outside of limits

RPD: 0 out of 5 outside limitsSpike Recovery: .0 out of 10 outside limits

Comments:

FORM III VOA -1 1x87 Rev,

15


Lab Name: ETCNJ

Lab Code: Caee No.:

Lab File ID: >C2920.

Dete Analyzed 02x21X91

Matrix: Csoi1/water) WATER

Instrument ID: GCxMS C


Contract:

SAS No.t SDG No.:


Tim* Analyzed: 1902

Lave 1: (1 ow/med) LQUI

1 EPA1 SAMPLE NO.

01 t A9766021 A9769031 A4361041 A6020091 A6022061 A5753071OBI091101111121131141151161171Ifil19120121122123124 1291261271281291301

LABSAMPLE ID

CA97660CA9769UCA4381UCA6020UCA6022UCA9793U

LABFILE ID

>C2522>C2523>C2924>C2929>C2926>C2927

.

TIMEANALYZED

164917331820190719592042

Comment*

oege 1 ofFORM IV YOA

T61X87 Rev.

4AUOLATILE METHOD BLANK SUMMARY

Lab Name: ETCNJ

Lab Code: Ca»e No.:

Lab File ID: >C2534

Data Analyzed 02/22x91


Instrument ID: GCxMS C

THIS METHOD BLANK APPLIES TO THE FOLLOUINC SAMPLES, MS AND MSDi

Contract:

SAS No.: SDG No.:

Lab Samp la ID: UBLK02

Time Analyzed: 1157

Level:<lowXmed) LQU

1 EPA1 SAMPLE NO.

Oil A602302 1 A575503104105)06 t071081091101111121131141151161171Ifil191201211221231241251261271281291301

LABSAMPLE ID

CA6023U2CA5755U2

LABFILE ID

>C2535>C2536

TIMEANALYZED

13021350

Comments!

page 1 ofFORM IU UOA

171X87 Rev,


Lab Name: ETCNJ

Lab Cod*: Case No.:

Lab File ID: >C2541

Date Analyzed 02/29x91



THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD:

Contract:

SAS No.: SDG No.:

Lab Sample ID: USLK03

Time Analyzed: 1442

Level:(lou/med) LOW

1 EPA1 SAMPLE NO.

Oil A5754MS021031041051061071081091101111121131141151141171181191201211221231241251261271281291301

LABSAMPLE ID

CA5754US

LABFILE ID

>C2542

X

TIMEANALYZED

1712

Comments:

page 1 ofFORM IU YOA X/87 Rev


Leb Name: ETCNJ

Lab Code: Ceee No.i

Lab File ID: >C2946

Dete Analyzed 02/26X91



THIS METHOD BLANK APPLIES TO THE FOLLOUINC SAMPLES, MS AND MSD:

Contract:

SAS No.: SDG No.:


Time Analyzed: 1029

Level:Clow/med) LOU

Comment»

1 EPA1 SAMPLE NO.

Oil A9794MSD02 1 A5754031041091061071OBI091101111121131141191161171Ifil191201211221231241291261271281291301

LABSAMPLE ID

CA9794URCA9794U4

LABFILE ID

>C2947>C2948

TIMEANALYZED

11241959

JJLpage 1 of J.

FORM IU UOA 1/97 Rev


ERA SAMPLE NO,

Lab Nama: ETCNJ

Lab Coda: Case No.:

Matrix: Isoi1/water) WATER


Level: Clow/mad) LOW



Cent ractIUBLK01l

SAS No.: SDG No.:c.

Lab Sample ID: QN70*i87'J

Lab File ID: >C2520

Date Received: 02/oU/91



CAS NO. COMPOUNDCONCENTRATION UNITS:lug/L or ug/Kg) UG/L Q

74-87-3 —————74-83-9 —————75-01-4 —————75-00-3 —————75-09-2 —————67-64-1 —————75-15-0 —————75-35-4 —————75-74-3 —————540-59-0 ————67-66-3 —————107-06-2 ————78-93-3 —————71-55-6 —————56-23-5 —————108-05-4 ————75-27-4 —————78-87-5 —————10061-01-5 ——79-01-6 —————124-48-1 ————79-00-5 —————71-43-2 —————10061-02-6 ——75-25-2 —————108-10-1 ————591-78-6 ————127-18-4 ————79-34-5 —————108-88-3 ————108-90-7 ————100-41-4 ————100-42-5 ————1330-20-7 ———

—— Ch loromathana—— Bromome thane B f—— Uinyl Chlor ide---Ch lo roe thane—— Me thy lane Chlor ide. _ _—— Acetone ., . , „.— -Carbon Dimulfida , ,. ,—— 1 .1-Dich loroethene , „ . ,—— 1 .1-Dich loroathane , , , ,—— 1,2-Dich lore thane (total ) __—— Chloroform ,. „ , ,- — 1 r2-Di ch lo roe thane _ ,—— 2-Butanone_ ... ,---1.1 .1-Trieh loroathane—— Carbon Tetrach lor ide—— Uinul Acatata _ fi _,— --Bromodich lorome thane— -1 .2-Diehloroprooane— — eia-1 .3-DiehlorQDrQpane---Tr ieh loroethena« —— Dibromoch loroma thane_- — 1.1 .2-Tr ichloroa thane—— Benzana .,—— t rans-1 ,3-Dichloropropane __---Bromoform , ,—— >4-Mathul-2-Pantanone—— 2-Hexanona „ . ,---Tat rach lor oe thane—— 1 ,1,2,2-Tet rach loroathane __—— Toluene---Chlorobanzena— -Ethvlbenzene , .,—— Sturene , , , ,—— Xvlene (total ) . . . . , , „„

1110110110110151101515151515151101515110151515151515151515110110151515151515151

1 IIU tIUtuIUIUIUIUIUIUIUIUIUIUIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU• -L J2TJ

FORM I UOA 1/S~ Rev,

II

4i/T

WU *Mn»tTOH %

:T.Arj

•o* ruifrt m


Lab Name:ETCNJ

Lab Code: Case No.:

Matrix: (soi1/water ) WATER

Sample wt/vo1: 5.0 (g/TnL) ML

Level: llow/med) LQLJ


Column: (pack.-'cap ) PACK


EPA SAMPLE NO.

IlUBLKOi1 __________

SDG No.:.e

Cant ract :

SAS No.:

Lab Sample ID:

Lab File ID: >C2520

Date Received: G2.od^l

Date Analyzed: 02/21''91


CONCENTRATION UNITS:tug/L or ug/KgJ UG/L


FORM I UOA-T-IC 1/87 Pev


ERA SAMPLE NO

UBLK02Lab Name: ETCNJ

Lab Coda:

Cont ract:

Case No.:

Matrix: (so i 1.••'water ) UIATER

Sample wt/vol: 5.0 <gXmL) Mi-

Level: C low/mod) LOW


Co 1 Limn : (pack/cap ) PACK

CAS NO. COMPOUND

SAS No.: SDG No.:

Lab Sample ID: QC70487U2

Lab File ID: >C2534

Date Received: 02/JU/91


Di lut ion Factor : 1

CONCENTRATION UNITS:Cug/L or ug/Kg) UG/L Q

74-87-3 —————74-83-9 —————75-01-4 —————75-00-3 —————75-09-2 —————67-64-1 —————75-15-0 —————75-35-4 —————75-34-3 —————540-59-0 ————67-66-3 —————107-06-2 ————78-93-3 —————71-55-6 —————56-23-5 —————108-05-4 ————75-27-4 —————78-87-5 —————10061-01-5 ——79-01-6 —————124-48-1 ————79-00-5 —————71-43-2 —————10061-02-6 ——75-25-2 —————108-10-1 ————591-78-6 ————127-18-4 ————79-34-5------108-88-3 ————108-90-7 ————100-41-4 ————100-42-5 ————1330-20-7 ———

— -Chlorame thane---BromomB thane, mfmmmM—— Uinyl Chloride—— Ch IQ roe thane—— Mathylene Chloride—— Acetone ,—— Carbon Diaulfide ,.„ , „.- — lrl-Diehloroethene—— 1 r 1-D i eh lo roe thane—— 1,2-Dichlorethene (total ) __—— Chloroform,... ,.„„, _,,-• — 1 r2-Di eh lo roe thane—— 2-Butanone _.,..— --1 rlTl-Tr ichlo roe thane-« — Carbon Tetrachloride—— Ui ny 1 Ae« t a t e _„..,„„, ,„„—— Bromod ichl aroma thane—— 1 ,2-Diehloropropana— *-ci»-l .3-Diehlorooronene- — Tr i eh lo roe thane—— Dibromoch 1 aroma than* „,„ ,— -Irlr2-Tr iehlo roe thane— -Benzene .._, „„,,„ ,,,—— t rans-1 .3-Dich loroorooene—— Bromof orm ,,,— -4-Mathy 1-2-Pen t anone— -2-Hexanona „.,—— T*t rachloroethene ,— -1,1,2,2-Tetrach lo roe thane __—— Toluene,,,,,,,,,.,, .- — Ch lorobenzene- — Ethylbenzene——— Styrane _„„, ,,, ,„ ,—— Xylan. (total)

111011011011015110151515151515110151511015151515151515151511011015151515151515I

1 iIU !IU 1IU 1IU 1IU 1IU 1IU 1IU IIU 1IU IIU iIU IIU 1IU 1IU iIU 1IU iIU 1IU 1IU 1IU iIU iIU iIU iIU !IU iIU iIU iIU iIU iIU iIU iIU iIU iI t

FORM I UQA i/er

la* If MO i

VOtATXtX QMAJIZCS ANALYSIS DATA SWXT

Pg frrt______ eoatraetz

HO.

C«M NO*Matrix: (soil/vator)JUjJg.S4apl« vt/vol:

Uvol: (lov/aod)I Moisturtt not doeColumn: (paeJc/eap)

oa HO.

(«/«t)jX.

coffFotmoiI Totraftydrofuran

10:Data ftocoivod:Data Analxsod:

dilution factor:COHCnfTIATZOIt UWWJ;(uoyt. or uf/Mi M^/L

I/it R«v

24



ERA SAMPLE NO.

VBLK02Lab NameiETCNJ

Lab Code: Case No.:

Ma t P \ x : (soil /wa t e r ) UIATER


Level: Clow/med) LOU


Column: tpack/cap ) PACK


Contract:

SAS No.: SDG No.:

Lab Sample ID: QC7G437U2

Lab File ID: >C25?4

Date Received: 02/j£/91





FORM I VOA-TIC

RT EST. CONC

————— 21/87

i0

i

Rev.

1AUQLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: ETCNJ

Lab Code: Caae No.:



Lava It Clow/mad) LOU

S Moisture: not dac.


Contracti

SAS No.:

ERA SAMPLE NO,

IIUBLK03I_____

CAS NO. COMPOUND

SOC No.:

Lab Samp la ID: QC7Q487U3

Lab Ft la ID: >C2541

Data Received: 02/Jtf/91

Data Analyzed: 02/25/91

Dilution Factor: 1


74-87-3 —————74-83-9 -----75-01-4 — — —75-00-3 —————75-09-2 —————67-64-1 —————75-15-0 —————75-35-4 —— ——75-34-3 —————540-59-0 ————67-66-3 —————107-06-2 ————78-93-3 ————71-55-6 ------56-23-5 ————108-05-4 ————75-27-4 —————78-87-5 —————10061-01-5 ——79-01-6 —————

79-00-5 —————71-43-2 —————10061-02-6 ——75-25-2 ————108-10-1 ————591-78-6 ————127-18-4 ————79-34-5 —————108-88-3 ————108-90-7 ————100-41-4 ————100-42-5 ————1330-20-7 ———

---Ch laromathana _,_ — m— — Bromomathana ._ __ m M---Uiny 1 Ch lor ida _ , . „_ „. „—— Chloroathana,——— Mathylane Chloride.^ „..,„_ ——— Aeatona_ _,_ ._,—— Carbon Dimul f id«_i— , _ — „ _ — ,_---1 rl-Diehloroeth«n« ^ m—— 1 Pl-Diehloroath«n« — — .._.,_ M1-—— 1,2-Dich lor ethane (total )——Chloroform— -1 r2-Diehloroathana ._, , __.—— 2-Butanona ,— -1 .1 . 1-Trichlo roe thane——Carbon Tet rach lor id*---Uinyl Acetate 1-1— _— — — Brained i eh lo rone thane—— 1 .2-Diehlorooraoana— -eia-1 .3-Diehloroorooana— -Trichloroethene_---Dibromoehlopomethana—— 1. 1.2-Tri eh loraa thane—— Benxene— -tranft-l,3-Dichloropropena_ _---Bromoform_ M-—— 4-Methyl-2-Pantanone ._ _ ,__-— 2-Hexenone__—— Tetraehloroethana 1— ._— _„ lll— _ ,..- — 1 .1 .2.2-Tetraehloroethene—— Toluene _. ,_ — , .—— Chlorobenzena _H ,_, _,—— Ethylbenzene — . mt — „.,,. ., ,—— Styrana__ ._—— Xylene (total).., ._,_,_„._.

1110110110110151101515151515151101515110151515151515151515110110151515151515151

1IUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1

FORM I UOA 1/87



EPA SAMPLE NO.

IUBLK03Lab Nama:ETCNJ

Lab Coda: Casa No.:


Samp la wt/vol: 5.0 (g/mD ML

Lavel: Clou/mad) LOU

% Moisture: not dac.


Numbar TICa found: 0

Contract:

SAS No.: SDG No.:

Lab Samp la IDi QC70487V3

Lab Fila ID: >C2541

Data Racaivad: 02/&/91

Data Analyzad: 02/25/91

Dilut ion Factor: 1.Q

CONCENTRATION UNITS:Cug/L or ug/Kg) UC/L


FORM I UOA-TIC 1X87 Rav.

1AUQLATILE ORGANICS ANALYSIS DATA SHEET

tab Nama: ETCNJ Contract:

EPA SAMPLE NO.

UBLK04

Lab Coda: Caaa No.: SAS No.: SDG No.:

Matrix: (aoil/watar) WATER


Laval: Clow/mad) LOUI

K Moistura: not dac.


CAS NO. COMPOUND

Lab Samp la ID: QC70487U4

Lab Fila ID: >C2546

Data Raca is/ad: 02/J&/91

Data Analyzad: 02/26/91

Dilution Factor: 1

CONCENTRATION UNITS:(ug/L or ug/Kg) UC/L Q

74-87-3 —— ——74-83-9 —————75-01-4 —————75-00-3 —————75-09-2 ------67-64-1 —————75-15-0 —— ——75-35-4 —————75-34-3 —————540-59-0 ————67-66-3 —————107-06-2 ————78-93-3 —————71-55-6 —————56-23-5 —————108-05-4 ————75-27-4 —————78-87-5 —————10061-01-5 ——79-01-6 —————124-48-1 ————79-00-5 —————71-43-2 —————10061-02-6 ——75-25-2 —————108-10-1 ————591-78-6 ————127-18-4 ————79-34-5 —————108-88-3 ————108-90-7 ————100-41-4 ————100-42-5 ————1330-20-7 ———

1—— Ch 1 o roffla t hana . ,.„, , _ 1—— Hromomathana, „,,„., , '---Uinyl Chlorida... , 1—— Chloroathana __ .„_,.,. '—— Mathylana Chlarida,. __ 1— -Aeatona , , 1——Carbon Diau 1 f ida_iwi IIBI 1- — 1 f l-0ichloroathan« . ,,l—— 1 rl-DiehlQroath«n« __ipi 1—— 1,2-Oiehlorathana (total ) __ 1— --Chloroform 1—— 1 r2-Diehloro«th*n« _, ,.._,„__,_„_ 1---2-Butanon« .,„„,.. I-«1 .1 .1-Tr iehloroathana 1-—Carbon Tat raeh lor ida 1— -Utnyl Aeatata 1---Bramadiehlaramathana 1—— 1 .2-Diehloroorooana 1—— eia-ir3-PiehlorQBrQpana 1...TriohloroathanaHii. I---rjibramaehlaramathana 1— -1 .1 -2-Tr iehlaraathana 1—— Banzana M 1—— trana- 1,3-0 ichlorop ropana. .!---Bromafarm .,.,.„...., 1- — .4~Mathul-2-Pantanona 1---2-Haxanona 1- - .-Tatrachlaraathana _ _ . 1---1,1,2,2-Tatrachloroathana.^^l—— Toluana 1—— Chlorabanzana ,. wi ,. , 1---Cthylhanzana „__„..,„_,.,.., , 1— — Styrana 1—— Xylana (total) 1

1

1010101051055555510551055555555510105555555

1IUtutututuIUIUtuIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIUIU1

FORM I UOA29

1X87 Rav.

Uft NAMt

1AOMAffXCS ANAX.YSX* DATA SKR

______ Cmtneti

I9A NO.

Matrix: f«oil/v»t«ri bJArae.SAftpla vt/vol:Uvtl: (lov/atd) ^^% Moiaturtt net 4tc.Coluan: (paex/eap)

eu no. COI90UHO

Tttraftydrofuran

dilution factor:COHCtWTKATXOK OVXTSj

. t

1/17 R«v.

IEVOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIUELY IDENTIFIED COMPOUNDSLab NameiETCNJ

Lab Code: Case No.:


Sample ut/vol: 5.0 Cg/mD ML

Level: (low/mad) LOU


Co 1umn: (pack/cap) PACK


EPA SAMPLE NO.

IIU8LK04

Contract:

SAS No.: SDC No.:

Lab Sample ID: QC70487V4

Lab File ID: >C2546

Date Received: 02/jtt/91


Dilution Factor! 1.0

CONCENTRATION UNITS:<ugxL or ug/Kg) UC/L


FORM I UOA-TIC 1/87 Rev.


Lab Nama: ETCNJ Contract:

Lab Coda: Casa No.: SAS No.: SDG No.:

Lab Fila ID (Standard): >C2517 Data Analyzad: 02x21/91

Instrumant IDi GC/MS C Tima Analyzad: 1239

Matrix: (soi 1/watar) WATER Lava1:(low/mad) LOW Column:/(pacto/cap) ___

111 12 HOUR STO

1 UPPER LIMIT

1 LOWER LIMIT

1 EPA SAMPLE1 NO.

01IUBLK0102IA9766031A976504IA438109IA602006IA6022Q71A9793081091101111121131141151161171181191201211221

IS1CBCM)AREA *

29361

98722

14681

30922309633323733698349993430036689

RT

10.64

10.6110.6910.6410.6410.6310.6410.61

IS2CDFB)AREA *

130944

261088

69272

138921144176149299146307148939191329196391

RT

21.29

21.3121.3921.3421.3021.3321.3021.30

IS3CCBZ)AREA ft

109790

219900

94879

117046123779124723129429127687126999131941

RT

26.18

26.1926.1926.1826.1826.1726.1826.19

151 CBCM) -152 CDFB) -153 CCBZ) -

Bromochloromathana1,4-DifluorobanzanaCn Iorobanzana-d9

UPPER LIMIT - + 100*of internal standard araaLOWER LIMIT • - 90*of intarnal standard araa

ft Column ussd to flag intarnal standard araa valuas with an astar isk.

paga I of _[_

FORM UIII UOA32

1/87 Rav




Lab File ID (Standard): >C2533 Data Analyzed: 02/22/91


Matrix: (soil/water) UIATER Level:(low/med) LOW ColumwiCpecKXcap) ___

11t 12 HOUR STD

1 UPPER LIMIT

1 LOWER LIMIT

1 ERA SAMPLE1 NO.

01IUBLK0202IA602303IA5755041091061071081091101111121131141151161171181191201211221

ISKBCM)AREA *

33850

67700

16925

313932830734452

RT

10.68

10.7210.8010.75

IS2CDFB)AREA *

149172

298344

74586

129498128829151846

RT

21.34

21.3721.4121.41

IS3CC8Z)AREA *

128455

256910

64228

109466110019130520

RT

26.23

26.2526.2626.25

151 (8CM) • Bromochloromethane152 CDFB) - 1,4-Difluorobenzene153 (CBZ) - Chlorobenzene-d5

UPPER LIMIT - * 100*of internal standard ereaLOWER LIMIT - - 50*of internal standard area

ft Column used to flag intarnal standard araa velues with an asterisk.

page | of _j_

FORM V I I I UOA33

1x87 Rev,



Lab Coda: Case No.: SAS No.: SDG No.:

Lab File ID (Standard): >C2940 Data Analyzad: 02/29/91

Instrument ID: GC/MS C Tim* Analyzad: 1399x*—>

Matrix:(soiI/water) WATER Level:(low/med) LOU Column:fpack/cap) _____

111 12 HOUR STD

1 UPPER LIMIT

1 LOUER LIMIT

1 EPA SAMPLE1 NO.

01IUBLK0302IA9794MS03104109106107106109110)111121131141191161171Ifll191201211221

ISKBCM)AREA *

42099

84190

21046

4828129911

RT

10.77

10.7610.68

IS2CDFB)AREA *

1B2628

369296

91314

212728119616

RT

21.39

21.3621.37

I S3 C C8Z )AREA *

197700

319400

76690

16466396722

RT

26.23

26.2626.26

151 (BCM) • Bromochloromethane152 (DFB) • 1,4-Difluorobenzene153 CCBZ) • Chiorobenzene-d9

UPPER LIMIT • * 100*of intarnal standard araaLOUER LIMIT - - 90kof intarnal standard area

t Column usad to flag intarnal standard araa values with an asterisk,

page 1 of J_.

FORM UIII UOA34

1/87 Rev



Lab Coda: Casa No.: SAS No.: SDG No.:

Lab Fila ID (Standard): >C2545 Data Analyzad: 02/26/91

Instrument ID: GC/MS C Tima Analyzad: 0942

Matrix: (sol 1/watar) UIATER Laval:(low/mad) LOW Column: (pacU'cap) ^_

111 12 HOUR STD

1 UPPER LIMIT

1 LOUIER LIMIT

1 EPA SAMPLEI NO.

01IVBLK04021A5754MSD03IA5754041091061071aai091101111121131141151161171181191201211221

IS1CBCM)AREA *

30885

61770

1544?

340393196033890

RT

10.68

10.6910.6910.73

IS2CDFB)AREA *

132652

265304

66326

145758131619152480

RT

21.38

21.3621.4221.35

IS3CCBZ)AREA *

110796

221592

55398

123921109563127263

RT

26.22

26.2326.2726.23

151 CBCM) - Bromochloromathans152 (DFB) • 1,4-Oifluorobanzana153 CCBZ) • Chlorobanzana-d5

UPPER LIMIT - * 100*of internal standard araaLOWER LIMIT - - 50*of intarnal standard araa

* Column uaad to flag intarnal standard araa valuas with an astarisk.

_L_ of J_ 35

FORM UIII UOA 1/87 Rav

•ETC

TABUXuATED RESULTS

NON CUP

36

M^M. Vx




CA4381 WASTE MWGEMENT. INC. 405 W3QUPZ220 910215 1622 1Eli****

ETC Sttvle Mo. Co*p*ny Facility S*«pl* Poi«t 0»t« Tim Hours

NPDESNunb*r

ChlorideFluoride

CM

(tttoltt

SaapleConcen,

•fl/1

178.8.4

M>L•0/1

1.0.1

MAR 14. 1991

—— " JL>* ^ ————————


-. : ::;:'•.;-. .-.••;; Chain of Custody O«U Beq* for ETC Data Manaowwnt Swnm»rv Reports - ._:;

CM t*:';: UTE*l«VIM0ieiirjr ll^ ^ 40S H^';7l!3tWfZ22D-".:--*»»2l»' l63Kt; 1ETC lii^-|li '":^:^^P^V.C«4(ii^^.v.y-^ .V "•• ".V:^;.. .;v •:•- F«c illty -:-'••.

• : . • • • . - -1 • - • ' ..:.• -••:•:.•.--.. 5i*p»»« -•>:-> I«>1« taint "-" OiU TiM Anirs -

•••: Compound •. l lKif"


UJCD

: : : KM'ttlf •••V^-->:-,:.

,- s««pl* :,;:.CoflCWi:^»«/r>^

32.2614348<IO

--^•fiot''-^:} »«7i

2.0101010

MR 4. 199)

ETCFEB 26. 1991




CA438I WASTE MANAGEMENT. INC. 405 W3GWPZ22D 910215 1622 1ETC Simple No, Company Facility 3*npl« Point Oat«

El«piedTime Hiun

Parameter

pHpHpHpH

FieldFieldFieldField

stdstdstdstd

Specific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance 'Field urn/cmSpecific Conductance Field urn/ cmTemperature D*g . CRedox Potential mvRedox Potential mvRedox Potential mvRedox Potential mv

Results

SampleMeasure

6 636.676.656.72

9789679949776 1

275277272270

MDL

------------

ETCTABLE 1: QUANTITATIVE RESULTS and QUALITY ASSURANCE DATA


MAR 14. 1991


CA6020 WASTE MANAGEMENT, INC. 405 U3GWPZ22S 910218 1500 1ETC Sample No. Company Facility Sample Point Oat* Time Hour*

NPDESNufflbtr

ChlorideFluoride

O

R*cults

SatjpleConcen.

•9/1

208.7.4

MDl

1 .0.1

——— Arfi V/ —————————

Compouq


Chain of Cwtody Data Required for ETC Data Management Summary Reports

CA6020 WASTE MM«6&tHT, INC, 405 W3QWPZ22S 910218 1500 1

ETC SM?!« Ha. FxLiiity Iwpla P»int 0»t« TbM Hour»

* - ....^M

Sulfate as S04Total Dissolved Solid* (TDSBicarbonate as CaC03Carbonate as CaC03

4*

Rtittlll

SK44.5

824380

ftittiU.-;:\....*^/V' '••:."

2.0101010

MAR 4. 1991

———— i>jl Vx —————————————————————————————————————————————————————————————————————————————



Cnabi of Custody Data Required for ETC Data Management Summary Reports

CA6020 WASTE MANAGEMENT. INC 40S W3GWPZ22S 9102181500 1El'pted

ETC Sample No. Company Facility Sample Poini Dale Time Hours

Parameter

pH i Field' stdpH Field stdpH Field stdpH Field stdSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/ cmTemperature Deg. CRedox Potential mvRedox Potential mvRedox Potential mvRedox Potential mv

NO

Results

SampleMeasure

7.507.357.287.29

1183118811811184

10.0272280277275

MDL

-

FEB 26. 1991

—— i>^ Vx ——————MAR 14. )99I


NPDESNumb* r

ChlorideFluoride



CA6022 WASTE MANAGEMENT. INC. 405 W3GHP3A 910219 1132 1ETC Sanple No. Company Facility Sanple Point Oil* Time Hours

fUcdltt

SampleConcen.

moll<1 0

.1

»f>L«g/l

1 .0.1

—— j^A ^ ——————


Chain of Custody Data fteqwvd for ETC Data Management Summary Reports

CA6022 HASTE MANAGEMENT, INC, 40$ W3QHP3A 910219 1132 1ETC l lt KB* :.:.-: ; ; ' : . . CanwMy- V h ; i"- Ficility S«pl« Point Oat* Tb* Sours

Compound ! C


4*.

Ratultt

Coflctn.

26.8301253

•g/1

2.0101010

MAR 4. 1991

———— Ks. * \^~




CA6022 WASTE MANAGEMEMT. INC. 405 W3GWP3A 910219 1U2 1EK Sample No. C<mp«ny Facility S*nple Point Date Tine Hours

Parameter

pH i Field stdpH iField stdpH Field stdpH i Field stdSpecific Conductance Field urn/cmSpecific Conductance Field urn/cmSpecific Conductance Field urn/ cmSpecific Conductance Field urn/cmTemperature Deg. CRedox Potential mvRedox Potential mvRedox Potential mvRedox Potential mv

tJi

Ret ul tt

SampleMeasure

7.447.387.377.38

498462464464

9.5- 60- 66- 70- 70

H>L

-

FEB 27. 1991

appendix g results of analyses soil and ground-water

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