appendix h scaqmd rule 1166 monitoring forms submission · pes environmental, inc. appendix h...
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PES Environmental, Inc.
APPENDIX H
SCAQMD RULE 1166 MONITORING FORMS SUBMISSION
PES Environmental, Inc.
APPENDIX I
LABORATORY ANALYTICAL REPORTS
9765 Eton Avenue
California 91311Tel: (818) 998-5547
Fax: (818) 998-7258
Chatsworth
December 19, 2005
Novato, CA 94947
Enclosed is an analytical report for the above-referenced project. The samples included in this report were received on 12/05/05 14:57 and analyzed in accordance with the attached chain-of-custody.
Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Assurance Program Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety.
If you have any questions regarding this report or require additional information please call me at American Analytics.
Sincerely,
Francois BushPES Environmental, Inc.1682 Novato Blvd. Ste., 100
Eydie Schwartz
Project Manager
Re : KCOP / 241.060.02.014
A60609 / 5L05007
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6060912/05/0512/19/05
Page 2 of 6
Sample ID Laboratory ID Matrix TAT Date Sampled Date Received8260B/5035 Soil Full List
SN-A 5L05007-01 Soil 0 12/05/05 13:10 12/05/05 14:57
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6060912/05/0512/19/05
Page 3 of 6
MethodAnalyzedPreparedDilutionUnitsMRLResultAnalyte
ANALYTICAL DATA SUMMARY
Sample Name
Purgeable Volatile Organic Compounds by GC/MSEPA
8260B/503526 12/05/05 ug/kg 1Tetrachloroethylene (PCE) 5.0 12/05/05 SN-A
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6060912/05/0512/19/05
Page 4 of 6
Units: Method:Sample Matrix:
Purgeable Volatile Organic Compounds by GC/MSSoil ug/kg
Date Sampled: 12/05/05Date Prepared: 12/05/05
12/05/05Date Analyzed:AA ID No: 5L05007-01Client ID No: SN-A
1Dilution Factor: MRL
8260B/5035 Soil Full List (EPA 8260B/5035)
cis-1,2-Dichloroethylene <5.0 5.0Tetrachloroethylene (PCE) 26 5.0Trichloroethylene (TCE) <5.0 5.0Vinyl chloride <5.0 5.0
Surrogates %REC Limits4-Bromofluorobenzene 112% 80-120Dibromofluoromethane 93.6% 80-120Toluene-d8 108% 80-120
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6060912/05/0512/19/05
Page 5 of 6
RPD%RECSourceSpikeMRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResult
Purgeable Volatile Organic Compounds by GC/MS - Quality ControlBatch B5L0610 - EPA 5035
Prepared & Analyzed: 12/05/05 Blank (B5L0610-BLK1)cis-1,2-Dichloroethylene ug/kg5.0<5.0Tetrachloroethylene (PCE) ug/kg5.0<5.0Trichloroethylene (TCE) ug/kg5.0<5.0Vinyl chloride ug/kg5.0<5.0
ug/kg 100 80-120Surrogate: 4-Bromofluorobenzene 102102ug/kg 100 80-120Surrogate: Dibromofluoromethane 94.094.0ug/kg 100 80-120Surrogate: Toluene-d8 103103
Prepared & Analyzed: 12/05/05 LCS (B5L0610-BS1)cis-1,2-Dichloroethylene ug/kg44.2 5.0 40.0 75-125110Tetrachloroethylene (PCE) ug/kg42.4 5.0 40.0 75-125106Trichloroethylene (TCE) ug/kg43.8 5.0 40.0 75-125110Vinyl chloride ug/kg40.0 5.0 40.0 75-125100
ug/kg 100 80-120Surrogate: 4-Bromofluorobenzene 103103ug/kg 100 80-120Surrogate: Dibromofluoromethane 100100ug/kg 100 80-120Surrogate: Toluene-d8 100100
Prepared & Analyzed: 12/05/05 LCS Dup (B5L0610-BSD1)cis-1,2-Dichloroethylene ug/kg43.6 5.0 40.0 4075-125109 1.37Tetrachloroethylene (PCE) ug/kg40.4 5.0 40.0 4075-125101 4.83Trichloroethylene (TCE) ug/kg43.4 5.0 40.0 4075-125108 0.917Vinyl chloride ug/kg39.6 5.0 40.0 4075-12599.0 1.01
ug/kg 100 80-120Surrogate: 4-Bromofluorobenzene 106106ug/kg 100 80-120Surrogate: Dibromofluoromethane 102102ug/kg 100 80-120Surrogate: Toluene-d8 102102
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6060912/05/0512/19/05
Page 6 of 6
Special Notes
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
9765 Eton Avenue
California 91311Tel: (818) 998-5547
Fax: (818) 998-7258
Chatsworth
December 19, 2005
Novato, CA 94947
Enclosed is an analytical report for the above-referenced project. The samples included in this report were received on 12/06/05 16:16 and analyzed in accordance with the attached chain-of-custody.
Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Assurance Program Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety.
If you have any questions regarding this report or require additional information please call me at American Analytics.
Sincerely,
Kyle FloryPES Environmental, Inc.1682 Novato Blvd. Ste., 100
Eydie Schwartz
Project Manager
Re : KCOP / 241.060.02.014
A60611 / 5L07002
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061112/06/0512/19/05
Page 2 of 6
Sample ID Laboratory ID Matrix TAT Date Sampled Date Received8260B/5035 Soil Full List
SS-A-4 ft 5L07002-01 Soil 5 12/06/05 13:30 12/06/05 16:16
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061112/06/0512/19/05
Page 3 of 6
MethodAnalyzedPreparedDilutionUnitsMRLResultAnalyte
ANALYTICAL DATA SUMMARY
Sample Name
Purgeable Volatile Organic Compounds by GC/MSEPA
8260B/5035110 12/09/05 ug/kg 1Tetrachloroethylene (PCE) 5.0 12/09/05 SS-A-4 ft
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061112/06/0512/19/05
Page 4 of 6
Units: Method:Sample Matrix:
Purgeable Volatile Organic Compounds by GC/MSSoil ug/kg
Date Sampled: 12/06/05Date Prepared: 12/09/05
12/09/05Date Analyzed:AA ID No: 5L07002-01Client ID No: SS-A-4 ft
1Dilution Factor: MRL
8260B/5035 Soil Full List (EPA 8260B/5035)
cis-1,2-Dichloroethylene <5.0 5.0Tetrachloroethylene (PCE) 110 5.0Trichloroethylene (TCE) <5.0 5.0Vinyl chloride <5.0 5.0
Surrogates %REC Limits4-Bromofluorobenzene 102% 80-120Dibromofluoromethane 90.0% 80-120Toluene-d8 104% 80-120
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061112/06/0512/19/05
Page 5 of 6
RPD%RECSourceSpikeMRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResult
Purgeable Volatile Organic Compounds by GC/MS - Quality ControlBatch B5L1217 - EPA 5035
Prepared & Analyzed: 12/09/05 Blank (B5L1217-BLK1)cis-1,2-Dichloroethylene ug/kg5.0<5.0Tetrachloroethylene (PCE) ug/kg5.0<5.0Trichloroethylene (TCE) ug/kg5.0<5.0Vinyl chloride ug/kg5.0<5.0
ug/kg 100 80-120Surrogate: 4-Bromofluorobenzene 99.699.6ug/kg 100 80-120Surrogate: Dibromofluoromethane 86.686.6ug/kg 100 80-120Surrogate: Toluene-d8 104104
Prepared & Analyzed: 12/09/05 LCS (B5L1217-BS1)cis-1,2-Dichloroethylene ug/kg44.6 5.0 40.0 75-125112Tetrachloroethylene (PCE) ug/kg44.0 5.0 40.0 75-125110Trichloroethylene (TCE) ug/kg46.2 5.0 40.0 75-125116Vinyl chloride ug/kg42.2 5.0 40.0 75-125106
ug/kg 100 80-120Surrogate: 4-Bromofluorobenzene 97.497.4ug/kg 100 80-120Surrogate: Dibromofluoromethane 96.096.0ug/kg 100 80-120Surrogate: Toluene-d8 96.696.6
Prepared & Analyzed: 12/09/05 LCS Dup (B5L1217-BSD1)cis-1,2-Dichloroethylene ug/kg42.8 5.0 40.0 4075-125107 4.12Tetrachloroethylene (PCE) ug/kg45.4 5.0 40.0 4075-125114 3.13Trichloroethylene (TCE) ug/kg47.8 5.0 40.0 4075-125120 3.40Vinyl chloride ug/kg38.0 5.0 40.0 4075-12595.0 10.5
ug/kg 100 80-120Surrogate: 4-Bromofluorobenzene 99.499.4ug/kg 100 80-120Surrogate: Dibromofluoromethane 95.895.8ug/kg 100 80-120Surrogate: Toluene-d8 98.298.2
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061112/06/0512/19/05
Page 6 of 6
Special Notes
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
9765 Eton Avenue
California 91311Tel: (818) 998-5547
Fax: (818) 998-7258
Chatsworth
December 19, 2005
Novato, CA 94947
Enclosed is an analytical report for the above-referenced project. The samples included in this report were received on 12/07/05 13:36 and analyzed in accordance with the attached chain-of-custody.
Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Assurance Program Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety.
If you have any questions regarding this report or require additional information please call me at American Analytics.
Sincerely,
Kyle FloryPES Environmental, Inc.1682 Novato Blvd. Ste., 100
Eydie Schwartz
Project Manager
Re : KCOP / 241.060.02.014
A60612 / 5L07005
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061212/07/0512/19/05
Page 2 of 7
Sample ID Laboratory ID Matrix TAT Date Sampled Date Received8260B/5035 Soil Full List
SSW-4 5L07005-01 Soil 5 12/06/05 15:05 12/07/05 13:36
SSE-4 5L07005-02 Soil 5 12/07/05 10:30 12/07/05 13:36
BS-8 5L07005-03 Soil 0 12/07/05 12:35 12/07/05 13:36
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061212/07/0512/19/05
Page 3 of 7
MethodAnalyzedPreparedDilutionUnitsMRLResultAnalyte
ANALYTICAL DATA SUMMARY
Sample Name
Purgeable Volatile Organic Compounds by GC/MSEPA
8260B/5035140 12/09/05 ug/kg 1Tetrachloroethylene (PCE) 5.0 12/09/05 SSW-4
EPA 8260B/5035
14 12/07/05 ug/kg 1Tetrachloroethylene (PCE) 5.0 12/07/05 BS-8
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061212/07/0512/19/05
Page 4 of 7
Units: Method:Sample Matrix:
Purgeable Volatile Organic Compounds by GC/MSSoil ug/kg
Date Sampled: 12/06/05 12/07/05 12/07/05Date Prepared: 12/09/05 12/09/05 12/07/05
12/09/05 12/09/05 12/07/05Date Analyzed:AA ID No: 5L07005-01 5L07005-02 5L07005-03Client ID No: SSW-4 SSE-4 BS-8
111Dilution Factor: MRL
8260B/5035 Soil Full List (EPA 8260B/5035)
cis-1,2-Dichloroethylene <5.0<5.0<5.0 5.0Tetrachloroethylene (PCE) 14<5.0140 5.0Trichloroethylene (TCE) <5.0<5.0<5.0 5.0Vinyl chloride <5.0<5.0<5.0 5.0
Surrogates %REC Limits4-Bromofluorobenzene 108% 106% 110% 80-120Dibromofluoromethane 88.0% 84.0% 90.0% 80-120Toluene-d8 108% 108% 108% 80-120
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061212/07/0512/19/05
Page 5 of 7
RPD%RECSourceSpikeMRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResult
Purgeable Volatile Organic Compounds by GC/MS - Quality ControlBatch B5L0807 - EPA 5035
Prepared & Analyzed: 12/07/05 Blank (B5L0807-BLK1)cis-1,2-Dichloroethylene ug/kg5.0<5.0Tetrachloroethylene (PCE) ug/kg5.0<5.0Trichloroethylene (TCE) ug/kg5.0<5.0Vinyl chloride ug/kg5.0<5.0
ug/kg 100 80-120Surrogate: 4-Bromofluorobenzene 106106ug/kg 100 80-120Surrogate: Dibromofluoromethane 97.097.0ug/kg 100 80-120Surrogate: Toluene-d8 103103
Prepared & Analyzed: 12/07/05 LCS (B5L0807-BS1)cis-1,2-Dichloroethylene ug/kg39.8 5.0 40.0 75-12599.5Tetrachloroethylene (PCE) ug/kg40.6 5.0 40.0 75-125102Trichloroethylene (TCE) ug/kg41.8 5.0 40.0 75-125104Vinyl chloride ug/kg39.2 5.0 40.0 75-12598.0
ug/kg 100 80-120Surrogate: 4-Bromofluorobenzene 105105ug/kg 100 80-120Surrogate: Dibromofluoromethane 95.095.0ug/kg 100 80-120Surrogate: Toluene-d8 101101
Prepared & Analyzed: 12/07/05 LCS Dup (B5L0807-BSD1)cis-1,2-Dichloroethylene ug/kg39.2 5.0 40.0 4075-12598.0 1.52Tetrachloroethylene (PCE) ug/kg41.4 5.0 40.0 4075-125104 1.95Trichloroethylene (TCE) ug/kg41.4 5.0 40.0 4075-125104 0.962Vinyl chloride ug/kg41.0 5.0 40.0 4075-125102 4.49
ug/kg 100 80-120Surrogate: 4-Bromofluorobenzene 100100ug/kg 100 80-120Surrogate: Dibromofluoromethane 91.491.4ug/kg 100 80-120Surrogate: Toluene-d8 99.899.8
Batch B5L1217 - EPA 5035Prepared & Analyzed: 12/09/05 Blank (B5L1217-BLK1)
cis-1,2-Dichloroethylene ug/kg5.0<5.0Tetrachloroethylene (PCE) ug/kg5.0<5.0Trichloroethylene (TCE) ug/kg5.0<5.0Vinyl chloride ug/kg5.0<5.0
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061212/07/0512/19/05
Page 6 of 7
RPD%RECSourceSpikeMRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResult
Purgeable Volatile Organic Compounds by GC/MS - Quality ControlBatch B5L1217 - EPA 5035
Prepared & Analyzed: 12/09/05 Blank (B5L1217-BLK1) Continuedug/kg 100 80-120Surrogate: 4-Bromofluorobenzene 99.699.6ug/kg 100 80-120Surrogate: Dibromofluoromethane 86.686.6ug/kg 100 80-120Surrogate: Toluene-d8 104104
Prepared & Analyzed: 12/09/05 LCS (B5L1217-BS1)cis-1,2-Dichloroethylene ug/kg44.6 5.0 40.0 75-125112Tetrachloroethylene (PCE) ug/kg44.0 5.0 40.0 75-125110Trichloroethylene (TCE) ug/kg46.2 5.0 40.0 75-125116Vinyl chloride ug/kg42.2 5.0 40.0 75-125106
ug/kg 100 80-120Surrogate: 4-Bromofluorobenzene 97.497.4ug/kg 100 80-120Surrogate: Dibromofluoromethane 96.096.0ug/kg 100 80-120Surrogate: Toluene-d8 96.696.6
Prepared & Analyzed: 12/09/05 LCS Dup (B5L1217-BSD1)cis-1,2-Dichloroethylene ug/kg42.8 5.0 40.0 4075-125107 4.12Tetrachloroethylene (PCE) ug/kg45.4 5.0 40.0 4075-125114 3.13Trichloroethylene (TCE) ug/kg47.8 5.0 40.0 4075-125120 3.40Vinyl chloride ug/kg38.0 5.0 40.0 4075-12595.0 10.5
ug/kg 100 80-120Surrogate: 4-Bromofluorobenzene 99.499.4ug/kg 100 80-120Surrogate: Dibromofluoromethane 95.895.8ug/kg 100 80-120Surrogate: Toluene-d8 98.298.2
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061212/07/0512/19/05
Page 7 of 7
Special Notes
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
9765 Eton Avenue
California 91311Tel: (818) 998-5547
Fax: (818) 998-7258
Chatsworth
December 19, 2005
Novato, CA 94947
Enclosed is an analytical report for the above-referenced project. The samples included in this report were received on 12/13/05 13:11 and analyzed in accordance with the attached chain-of-custody.
Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Assurance Program Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety.
If you have any questions regarding this report or require additional information please call me at American Analytics.
Sincerely,
Kyle FloryPES Environmental, Inc.1682 Novato Blvd. Ste., 100
Eydie Schwartz
Project Manager
Re : KCOP / 241.060.02.014
A60614 / 5L13008
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061412/13/0512/19/05
Page 2 of 7
Sample ID Laboratory ID Matrix TAT Date Sampled Date Received8260B/5035 Soil Full List
BS-13.5 5L13008-01 Soil 0 12/13/05 00:00 12/13/05 13:11
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061412/13/0512/19/05
Page 3 of 7
MethodAnalyzedPreparedDilutionUnitsMRLResultAnalyte
ANALYTICAL DATA SUMMARY
Sample Name
Purgeable Volatile Organic Compounds by GC/MSEPA
8260B/503520 12/13/05 ug/kg 1Tetrachloroethylene (PCE) 5.0 12/13/05 BS-13.5
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061412/13/0512/19/05
Page 4 of 7
Units: Method:Sample Matrix:
Purgeable Volatile Organic Compounds by GC/MSSoil ug/kg
Date Sampled: 12/13/05Date Prepared: 12/13/05
12/13/05Date Analyzed:AA ID No: 5L13008-01Client ID No: BS-13.5
1Dilution Factor: MRL
8260B/5035 Soil Full List (EPA 8260B/5035)
cis-1,2-Dichloroethylene <5.0 5.0Tetrachloroethylene (PCE) 20 5.0Trichloroethylene (TCE) <5.0 5.0Vinyl chloride <5.0 5.0
Surrogates %REC Limits4-Bromofluorobenzene 106% 80-120Dibromofluoromethane 86.0% 80-120Toluene-d8 106% 80-120
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061412/13/0512/19/05
Page 5 of 7
RPD%RECSourceSpikeMRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResult
Purgeable Volatile Organic Compounds by GC/MS - Quality ControlBatch B5L1401 - EPA 5035
Prepared & Analyzed: 12/13/05 Blank (B5L1401-BLK1)cis-1,2-Dichloroethylene ug/kg5.0<5.0Tetrachloroethylene (PCE) ug/kg5.0<5.0Trichloroethylene (TCE) ug/kg5.0<5.0Vinyl chloride ug/kg5.0<5.0
ug/kg 100 80-120Surrogate: 4-Bromofluorobenzene 87.887.8ug/kg 100 80-120Surrogate: Dibromofluoromethane 99.099.0ug/kg 100 80-120Surrogate: Toluene-d8 94.694.6
Prepared & Analyzed: 12/13/05 LCS (B5L1401-BS1)cis-1,2-Dichloroethylene ug/kg43.4 5.0 40.0 75-125108Tetrachloroethylene (PCE) ug/kg39.0 5.0 40.0 75-12597.5Trichloroethylene (TCE) ug/kg41.0 5.0 40.0 75-125102Vinyl chloride ug/kg40.2 5.0 40.0 75-125100
ug/kg 100 80-120Surrogate: 4-Bromofluorobenzene 98.698.6ug/kg 100 80-120Surrogate: Dibromofluoromethane 100100ug/kg 100 80-120Surrogate: Toluene-d8 94.094.0
Prepared & Analyzed: 12/13/05 Matrix Spike (B5L1401-MS1) Source: 5L13006-05cis-1,2-Dichloroethylene ug/kg42.6 5.0 40.0 70-130106<5.0Tetrachloroethylene (PCE) ug/kg37.2 5.0 40.0 70-13093.0<5.0Trichloroethylene (TCE) ug/kg40.8 5.0 40.0 70-130102<5.0Vinyl chloride ug/kg35.2 5.0 40.0 70-13088.0<5.0
ug/kg 100 80-120Surrogate: 4-Bromofluorobenzene 100100ug/kg 100 80-120Surrogate: Dibromofluoromethane 104104ug/kg 100 80-120Surrogate: Toluene-d8 93.493.4
Prepared & Analyzed: 12/13/05 Matrix Spike Dup (B5L1401-MSD1) Source: 5L13006-05cis-1,2-Dichloroethylene ug/kg39.4 5.0 40.0 4070-13098.5 7.80<5.0Tetrachloroethylene (PCE) ug/kg43.2 5.0 40.0 4070-130108 14.9<5.0Trichloroethylene (TCE) ug/kg40.2 5.0 40.0 4070-130100 1.48<5.0Vinyl chloride ug/kg36.6 5.0 40.0 4070-13091.5 3.90<5.0
ug/kg 100 80-120Surrogate: 4-Bromofluorobenzene 102102
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061412/13/0512/19/05
Page 6 of 7
RPD%RECSourceSpikeMRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResult
Purgeable Volatile Organic Compounds by GC/MS - Quality ControlBatch B5L1401 - EPA 5035
Prepared & Analyzed: 12/13/05 Matrix Spike Dup (B5L1401-MSD1) Continued
Source: 5L13006-05
ug/kg 100 80-120Surrogate: Dibromofluoromethane 94.094.0ug/kg 100 80-120Surrogate: Toluene-d8 107107
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061412/13/0512/19/05
Page 7 of 7
Special Notes
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
9765 Eton Avenue
California 91311Tel: (818) 998-5547
Fax: (818) 998-7258
Chatsworth
December 23, 2005
Novato, CA 94947
Enclosed is an analytical report for the above-referenced project. The samples included in this report were received on 12/12/05 19:05 and analyzed in accordance with the attached chain-of-custody.
Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Assurance Program Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety.
If you have any questions regarding this report or require additional information please call me at American Analytics.
Sincerely,
Kyle FloryPES Environmental, Inc.1682 Novato Blvd. Ste., 100
Eydie Schwartz
Project Manager
Re : KCOP / 241.060.02.014
A60615 / 5L14010
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061512/12/0512/23/05
Page 2 of 6
Sample ID Laboratory ID Matrix TAT Date Sampled Date Received8260B/5035 Soil Full List
MSW-4 5L14010-01 Soil 5 12/12/05 10:20 12/12/05 19:05
MSE-4 5L14010-02 Soil 5 12/12/05 12:10 12/12/05 19:05
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061512/12/0512/23/05
Page 3 of 6
MethodAnalyzedPreparedDilutionUnitsMRLResultAnalyte
ANALYTICAL DATA SUMMARY
Sample Name
Purgeable Volatile Organic Compounds by GC/MSEPA
8260B/5035100 12/20/05 ug/kg 1Tetrachloroethylene (PCE) 5.0 12/20/05 MSW-4
EPA 8260B/5035
38 12/20/05 ug/kg 1Tetrachloroethylene (PCE) 5.0 12/20/05 MSE-4
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061512/12/0512/23/05
Page 4 of 6
Units: Method:Sample Matrix:
Purgeable Volatile Organic Compounds by GC/MSSoil ug/kg
Date Sampled: 12/12/05 12/12/05Date Prepared: 12/20/05 12/20/05
12/20/05 12/20/05Date Analyzed:AA ID No: 5L14010-01 5L14010-02Client ID No: MSW-4 MSE-4
11Dilution Factor: MRL
8260B/5035 Soil Full List (EPA 8260B/5035)
cis-1,2-Dichloroethylene <5.0<5.0 5.0Tetrachloroethylene (PCE) 38100 5.0Trichloroethylene (TCE) <5.0<5.0 5.0Vinyl chloride <5.0<5.0 5.0
Surrogates %REC Limits4-Bromofluorobenzene 112% 110% 80-120Dibromofluoromethane 91.7% 92.4% 80-120Toluene-d8 107% 106% 80-120
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061512/12/0512/23/05
Page 5 of 6
RPD%RECSourceSpikeMRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResult
Purgeable Volatile Organic Compounds by GC/MS - Quality ControlBatch B5L2014 - EPA 5035
Prepared & Analyzed: 12/20/05 Blank (B5L2014-BLK1)cis-1,2-Dichloroethylene ug/kg5.0<5.0Tetrachloroethylene (PCE) ug/kg5.0<5.0Trichloroethylene (TCE) ug/kg5.0<5.0Vinyl chloride ug/kg5.0<5.0
ug/kg 100 80-120Surrogate: 4-Bromofluorobenzene 101101ug/kg 100 80-120Surrogate: Dibromofluoromethane 86.686.6ug/kg 100 80-120Surrogate: Toluene-d8 102102
Prepared & Analyzed: 12/20/05 LCS (B5L2014-BS1)cis-1,2-Dichloroethylene ug/kg39.4 5.0 40.0 75-12598.5Tetrachloroethylene (PCE) ug/kg42.0 5.0 40.0 75-125105Trichloroethylene (TCE) ug/kg41.6 5.0 40.0 75-125104Vinyl chloride ug/kg40.4 5.0 40.0 75-125101
ug/kg 100 80-120Surrogate: 4-Bromofluorobenzene 99.099.0ug/kg 100 80-120Surrogate: Dibromofluoromethane 93.293.2ug/kg 100 80-120Surrogate: Toluene-d8 98.498.4
Prepared & Analyzed: 12/20/05 LCS Dup (B5L2014-BSD1)cis-1,2-Dichloroethylene ug/kg41.4 5.0 40.0 4075-125104 4.95Tetrachloroethylene (PCE) ug/kg39.6 5.0 40.0 4075-12599.0 5.88Trichloroethylene (TCE) ug/kg42.6 5.0 40.0 4075-125106 2.38Vinyl chloride ug/kg38.0 5.0 40.0 4075-12595.0 6.12
ug/kg 100 80-120Surrogate: 4-Bromofluorobenzene 103103ug/kg 100 80-120Surrogate: Dibromofluoromethane 102102ug/kg 100 80-120Surrogate: Toluene-d8 99.299.2
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061512/12/0512/23/05
Page 6 of 6
Special Notes
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
9765 Eton Avenue
California 91311Tel: (818) 998-5547
Fax: (818) 998-7258
Chatsworth
December 30, 2005
Novato, CA 94947
Enclosed is an analytical report for the above-referenced project. The samples included in this report were received on 12/19/05 13:10 and analyzed in accordance with the attached chain-of-custody.
Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Assurance Program Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety.
If you have any questions regarding this report or require additional information please call me at American Analytics.
Sincerely,
Kyle FloryPES Environmental, Inc.1682 Novato Blvd. Ste., 100
Eydie Schwartz
Project Manager
Re : KCOP / 241.060.02.014
A60618 / 5L19007
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061812/19/0512/30/05
Page 2 of 16
Sample ID Laboratory ID Matrix TAT Date Sampled Date Received8081A OCPs
SNE-4 5L19007-01 Soil 5 12/19/05 11:00 12/19/05 13:01
8260B/5035 Soil Full ListSNE-4 5L19007-01 Soil 1 12/19/05 11:00 12/19/05 13:01
SNN-4 5L19007-02 Soil 1 12/19/05 11:05 12/19/05 13:01
SNW-4 5L19007-03 Soil 1 12/19/05 11:10 12/19/05 13:01
8270CSNE-4 5L19007-01 Soil 5 12/19/05 11:00 12/19/05 13:01
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061812/19/0512/30/05
Page 3 of 16
MethodAnalyzedPreparedDilutionUnitsMRLResultAnalyte
ANALYTICAL DATA SUMMARY
Sample Name
Extractable Semivolatile Organic Compounds by GC
Extractable Semivolatile Organic Compounds by GC/MS
Purgeable Volatile Organic Compounds by GC/MSEPA
8260B/503537 12/20/05 ug/kg 1Tetrachloroethylene (PCE) 5.0 12/20/05 SNE-4
EPA 8260B/5035
8.2 12/20/05 ug/kg 1Trichloroethylene (TCE) 5.0 12/20/05 SNE-4
EPA 8260B/5035
24 12/20/05 ug/kg 1Tetrachloroethylene (PCE) 5.0 12/20/05 SNN-4
EPA 8260B/5035
380 12/20/05 ug/kg 1Tetrachloroethylene (PCE) 5.0 12/20/05 SNW-4
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061812/19/0512/30/05
Page 4 of 16
Units: Method:Sample Matrix:
Extractable Semivolatile Organic Compounds by GCSoil ug/kg
Date Sampled: 12/19/05Date Prepared: 12/19/05
12/20/05Date Analyzed:AA ID No: 5L19007-01Client ID No: SNE-4
1Dilution Factor: MRL
8081A OCPs (EPA 8081A)
4,4´-DDD <4.0 4.04,4´-DDE <4.0 4.04,4´-DDT <4.0 4.0Aldrin <2.0 2.0beta-BHC <2.0 2.0delta-BHC <2.0 2.0alpha-BHC <2.0 2.0gamma-BHC (Lindane) <4.0 4.0gamma-Chlordane <4.0 4.0alpha-Chlordane <4.0 4.0Chlordane <20 20Dieldrin <4.0 4.0Endosulfan I <2.0 2.0Endosulfan II <4.0 4.0Endosulfan sulfate <4.0 4.0Endrin <4.0 4.0Endrin aldehyde <4.0 4.0Endrin ketone <4.0 4.0Heptachlor <2.0 2.0Heptachlor epoxide <2.0 2.0Methoxychlor <20 20Toxaphene <100 100
Surrogates %REC LimitsTetrachloro-meta-xylene 87.2% 50-150
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061812/19/0512/30/05
Page 5 of 16
Units: Method:Sample Matrix:
Extractable Semivolatile Organic Compounds by GC/MSSoil mg/kg
Date Sampled: 12/19/05Date Prepared: 12/19/05
12/20/05Date Analyzed:AA ID No: 5L19007-01Client ID No: SNE-4
1Dilution Factor: MRL
8270C (EPA 8270C)
3,3´-Dichlorobenzidine <0.40 0.40Acenaphthene <0.10 0.10Acenaphthylene <0.10 0.10Aniline <0.20 0.20Anthracene <0.10 0.10Azobenzene <0.10 0.10Benzidine <0.40 0.40Benzo(a)anthracene <0.10 0.10Benzo(a)pyrene <0.10 0.10Benzo(b)fluoranthene <0.10 0.10Benzo(g,h,i)perylene <0.10 0.10Benzoic acid <1.0 1.0Benzo(k)fluoranthene <0.10 0.10Benzyl alcohol <0.10 0.104-Bromophenyl phenyl ether <0.10 0.10Butyl benzyl phthalate <0.50 0.504-Chloro-3-methylphenol <0.20 0.204-Chloroaniline <0.40 0.40Bis(2-chloroethoxy)methane <0.10 0.10Bis(2-chloroethyl)ether <0.10 0.10Bis(2-chloroisopropyl)ether <0.10 0.102-Chloronaphthalene <0.10 0.102-Chlorophenol <0.10 0.104-Chlorophenyl phenyl ether <0.10 0.10Chrysene <0.10 0.10Dibenzo(a,h)anthracene <0.10 0.10Dibenzofuran <0.10 0.10
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061812/19/0512/30/05
Page 6 of 16
Units: Method:Sample Matrix:
Extractable Semivolatile Organic Compounds by GC/MSSoil mg/kg
Date Sampled: 12/19/05Date Prepared: 12/19/05
12/20/05Date Analyzed:AA ID No: 5L19007-01Client ID No: SNE-4
1Dilution Factor: MRL
8270C (EPA 8270C) (continued)Di-n-butyl phthalate <2.0 2.01,2-Dichlorobenzene <0.10 0.101,3-Dichlorobenzene <0.10 0.101,4-Dichlorobenzene <0.10 0.102,4-Dichlorophenol <0.10 0.10Diethyl phthalate <0.80 0.802,4-Dimethylphenol <0.10 0.10Dimethyl phthalate <0.20 0.204,6-Dinitro-2-methylphenol <0.20 0.202,4-Dinitrophenol <0.40 0.402,6-Dinitrotoluene <0.10 0.102,4-Dinitrotoluene <0.10 0.10Di-n-octyl phthalate <0.10 0.101,2-Diphenylhydrazine <0.10 0.10Bis(2-ethylhexyl)phthalate <0.20 0.20Fluoranthene <0.10 0.10Fluorene <0.10 0.10Hexachlorobenzene <0.10 0.10Hexachlorobutadiene <0.10 0.10Hexachlorocyclopentadiene <0.10 0.10Hexachloroethane <0.10 0.10Indeno (1,2,3-cd) pyrene <0.40 0.40Isophorone <0.10 0.102-Methylnaphthalene <0.10 0.102-Methylphenol <0.20 0.203-Methylphenol <0.20 0.204-Methylphenol <0.20 0.20
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061812/19/0512/30/05
Page 7 of 16
Units: Method:Sample Matrix:
Extractable Semivolatile Organic Compounds by GC/MSSoil mg/kg
Date Sampled: 12/19/05Date Prepared: 12/19/05
12/20/05Date Analyzed:AA ID No: 5L19007-01Client ID No: SNE-4
1Dilution Factor: MRL
8270C (EPA 8270C) (continued)Naphthalene <0.10 0.104-Nitroaniline <0.50 0.503-Nitroaniline <0.40 0.402-Nitroaniline <0.10 0.10Nitrobenzene <0.10 0.102-Nitrophenol <0.20 0.204-Nitrophenol <0.20 0.20N-Nitrosodimethylamine <0.10 0.10N-Nitrosodiphenylamine <0.10 0.10N-Nitrosodi-n-propylamine <0.10 0.10Pentachlorophenol <0.10 0.10Phenanthrene <0.10 0.10Phenol <0.10 0.10Pyrene <0.10 0.101,2,4-Trichlorobenzene <0.10 0.102,4,5-Trichlorophenol <0.20 0.202,4,6-Trichlorophenol <0.20 0.20
Surrogates %REC Limits2-Fluorobiphenyl 50.1% 43-1162-Fluorophenol 44.9% 21-100Nitrobenzene-d5 44.6% 35-134Phenol-d6 45.2% 10-94Terphenyl-dl4 65.8% 33-1412,4,6-Tribromophenol 32.6% 10-123
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061812/19/0512/30/05
Page 8 of 16
Units: Method:Sample Matrix:
Purgeable Volatile Organic Compounds by GC/MSSoil ug/kg
Date Sampled: 12/19/05 12/19/05 12/19/05Date Prepared: 12/20/05 12/20/05 12/20/05
12/20/05 12/20/05 12/20/05Date Analyzed:AA ID No: 5L19007-01 5L19007-02 5L19007-03Client ID No: SNE-4 SNN-4 SNW-4
111Dilution Factor: MRL
8260B/5035 Soil Full List (EPA 8260B/5035)
cis-1,2-Dichloroethylene <5.0<5.0<5.0 5.0Tetrachloroethylene (PCE) 3802437 5.0Trichloroethylene (TCE) <5.0<5.08.2 5.0Vinyl chloride <5.0<5.0<5.0 5.0
Surrogates %REC Limits4-Bromofluorobenzene 110% 104% 114% 80-120Dibromofluoromethane 86.0% 89.7% 90.1% 80-120Toluene-d8 106% 102% 110% 80-120
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061812/19/0512/30/05
Page 9 of 16
RPD%RECSourceSpikeMRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResult
Extractable Semivolatile Organic Compounds by GC/MS - Quality ControlBatch B5L2916 - EPA 3550B
Prepared: 12/19/05 Analyzed: 12/20/05 Blank (B5L2916-BLK1)3,3´-Dichlorobenzidine mg/kg0.40<0.40Acenaphthene mg/kg0.10<0.10Acenaphthylene mg/kg0.10<0.10Aniline mg/kg0.20<0.20Anthracene mg/kg0.10<0.10Azobenzene mg/kg0.10<0.10Benzidine mg/kg0.40<0.40Benzo(a)anthracene mg/kg0.10<0.10Benzo(a)pyrene mg/kg0.10<0.10Benzo(b)fluoranthene mg/kg0.10<0.10Benzo(g,h,i)perylene mg/kg0.10<0.10Benzoic acid mg/kg1.0<1.0Benzo(k)fluoranthene mg/kg0.10<0.10Benzyl alcohol mg/kg0.10<0.104-Bromophenyl phenyl ether mg/kg0.10<0.10Butyl benzyl phthalate mg/kg0.50<0.504-Chloro-3-methylphenol mg/kg0.20<0.204-Chloroaniline mg/kg0.40<0.40Bis(2-chloroethoxy)methane mg/kg0.10<0.10Bis(2-chloroethyl)ether mg/kg0.10<0.10Bis(2-chloroisopropyl)ether mg/kg0.10<0.102-Chloronaphthalene mg/kg0.10<0.102-Chlorophenol mg/kg0.10<0.104-Chlorophenyl phenyl ether mg/kg0.10<0.10Chrysene mg/kg0.10<0.10Dibenzo(a,h)anthracene mg/kg0.10<0.10Dibenzofuran mg/kg0.10<0.10Di-n-butyl phthalate mg/kg2.0<2.01,2-Dichlorobenzene mg/kg0.10<0.10
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061812/19/0512/30/05
Page 10 of 16
RPD%RECSourceSpikeMRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResult
Extractable Semivolatile Organic Compounds by GC/MS - Quality ControlBatch B5L2916 - EPA 3550B
Prepared: 12/19/05 Analyzed: 12/20/05 Blank (B5L2916-BLK1) Continued1,3-Dichlorobenzene mg/kg0.10<0.101,4-Dichlorobenzene mg/kg0.10<0.102,4-Dichlorophenol mg/kg0.10<0.10Diethyl phthalate mg/kg0.80<0.802,4-Dimethylphenol mg/kg0.10<0.10Dimethyl phthalate mg/kg0.20<0.204,6-Dinitro-2-methylphenol mg/kg0.20<0.202,4-Dinitrophenol mg/kg0.40<0.402,6-Dinitrotoluene mg/kg0.10<0.102,4-Dinitrotoluene mg/kg0.10<0.10Di-n-octyl phthalate mg/kg0.10<0.101,2-Diphenylhydrazine mg/kg0.10<0.10Bis(2-ethylhexyl)phthalate mg/kg0.20<0.20Fluoranthene mg/kg0.10<0.10Fluorene mg/kg0.10<0.10Hexachlorobenzene mg/kg0.10<0.10Hexachlorobutadiene mg/kg0.10<0.10Hexachlorocyclopentadiene mg/kg0.10<0.10Hexachloroethane mg/kg0.10<0.10Indeno (1,2,3-cd) pyrene mg/kg0.40<0.40Isophorone mg/kg0.10<0.102-Methylnaphthalene mg/kg0.10<0.102-Methylphenol mg/kg0.20<0.203-Methylphenol mg/kg0.20<0.204-Methylphenol mg/kg0.20<0.20Naphthalene mg/kg0.10<0.104-Nitroaniline mg/kg0.50<0.503-Nitroaniline mg/kg0.40<0.402-Nitroaniline mg/kg0.10<0.10
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061812/19/0512/30/05
Page 11 of 16
RPD%RECSourceSpikeMRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResult
Extractable Semivolatile Organic Compounds by GC/MS - Quality ControlBatch B5L2916 - EPA 3550B
Prepared: 12/19/05 Analyzed: 12/20/05 Blank (B5L2916-BLK1) ContinuedNitrobenzene mg/kg0.10<0.102-Nitrophenol mg/kg0.20<0.204-Nitrophenol mg/kg0.20<0.20N-Nitrosodimethylamine mg/kg0.10<0.10N-Nitrosodiphenylamine mg/kg0.10<0.10N-Nitrosodi-n-propylamine mg/kg0.10<0.10Pentachlorophenol mg/kg0.10<0.10Phenanthrene mg/kg0.10<0.10Phenol mg/kg0.10<0.10Pyrene mg/kg0.10<0.101,2,4-Trichlorobenzene mg/kg0.10<0.102,4,5-Trichlorophenol mg/kg0.20<0.202,4,6-Trichlorophenol mg/kg0.20<0.20
mg/kg 1.00 43-116Surrogate: 2-Fluorobiphenyl 49.80.498mg/kg 2.00 21-100Surrogate: 2-Fluorophenol 47.00.940mg/kg 1.00 35-134Surrogate: Nitrobenzene-d5 47.40.474mg/kg 2.00 10-94Surrogate: Phenol-d6 48.20.964mg/kg 1.00 33-141Surrogate: Terphenyl-dl4 76.00.760mg/kg 2.00 10-123Surrogate: 2,4,6-Tribromophenol 35.60.712
Prepared: 12/19/05 Analyzed: 12/20/05 LCS (B5L2916-BS1)Acenaphthene mg/kg0.524 0.10 1.00 50-12152.4Anthracene mg/kg0.630 0.10 1.00 41-12163.0Benzo(a)pyrene mg/kg0.608 0.10 1.00 17-16360.8Benzo(b)fluoranthene mg/kg0.524 0.10 1.00 33-13752.4Butyl benzyl phthalate mg/kg0.712 0.50 1.00 19-13971.24-Chloro-3-methylphenol mg/kg0.968 0.20 1.00 22-14796.8Bis(2-chloroethyl)ether mg/kg0.540 0.10 1.00 26-12254.02-Chloronaphthalene mg/kg0.626 0.10 1.00 60-11862.64-Chlorophenyl phenyl ether mg/kg0.482 0.10 1.00 41-12848.21,4-Dichlorobenzene mg/kg0.532 0.10 1.00 26-10553.2
Eydie SchwartzProject Manager
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Date Received:
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KCOP241.060.02.014
A6061812/19/0512/30/05
Page 12 of 16
RPD%RECSourceSpikeMRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResult
Extractable Semivolatile Organic Compounds by GC/MS - Quality ControlBatch B5L2916 - EPA 3550B
Prepared: 12/19/05 Analyzed: 12/20/05 LCS (B5L2916-BS1) Continued2,4-Dichlorophenol mg/kg0.482 0.10 1.00 39-13548.2Di-n-octyl phthalate mg/kg0.528 0.10 1.00 4-14652.8Fluoranthene mg/kg0.408 0.10 1.00 SP147-12540.8Fluorene mg/kg0.522 0.10 1.00 SP160-12052.2Hexachlorobenzene mg/kg0.634 0.10 1.00 2-15263.4Hexachlorobutadiene mg/kg0.480 0.10 1.00 24-11648.0Hexachloroethane mg/kg0.480 0.10 1.00 40-11348.0Isophorone mg/kg0.524 0.10 1.00 21-19652.4Naphthalene mg/kg0.578 0.10 1.00 25-12157.8Nitrobenzene mg/kg0.560 0.10 1.00 38-13356.02-Nitrophenol mg/kg0.360 0.20 1.00 2-16336.0N-Nitrosodi-n-propylamine mg/kg0.584 0.10 1.00 2-23058.4Pentachlorophenol mg/kg0.290 0.10 1.00 14-17629.0Phenol mg/kg0.584 0.10 1.00 5-11258.4Pyrene mg/kg0.690 0.10 1.00 52-11569.01,2,4-Trichlorobenzene mg/kg0.480 0.10 1.00 44-14248.02,4,6-Trichlorophenol mg/kg0.600 0.20 1.00 37-14460.0
mg/kg 0.250 43-116Surrogate: 2-Fluorobiphenyl 60.80.152mg/kg 0.500 21-100Surrogate: 2-Fluorophenol 56.60.283mg/kg 0.250 35-134Surrogate: Nitrobenzene-d5 48.00.120mg/kg 2.00 10-94Surrogate: Phenol-d6 58.51.17mg/kg 0.250 33-141Surrogate: Terphenyl-dl4 77.60.194mg/kg 0.500 10-123Surrogate: 2,4,6-Tribromophenol 48.60.243
Extractable Semivolatile Organic Compounds by GC - Quality ControlBatch B5L2017 - EPA 3550B
Prepared: 12/19/05 Analyzed: 12/20/05 Blank (B5L2017-BLK1)4,4´-DDD ug/kg4.0<4.04,4´-DDE ug/kg4.0<4.04,4´-DDT ug/kg4.0<4.0Aldrin ug/kg2.0<2.0
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
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Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061812/19/0512/30/05
Page 13 of 16
RPD%RECSourceSpikeMRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResult
Extractable Semivolatile Organic Compounds by GC - Quality ControlBatch B5L2017 - EPA 3550B
Prepared: 12/19/05 Analyzed: 12/20/05 Blank (B5L2017-BLK1) Continuedbeta-BHC ug/kg2.0<2.0delta-BHC ug/kg2.0<2.0alpha-BHC ug/kg2.0<2.0gamma-BHC (Lindane) ug/kg4.0<4.0gamma-Chlordane ug/kg4.0<4.0alpha-Chlordane ug/kg4.0<4.0Chlordane ug/kg20<20Dieldrin ug/kg4.0<4.0Endosulfan I ug/kg2.0<2.0Endosulfan II ug/kg4.0<4.0Endosulfan sulfate ug/kg4.0<4.0Endrin ug/kg4.0<4.0Endrin aldehyde ug/kg4.0<4.0Endrin ketone ug/kg4.0<4.0Heptachlor ug/kg2.0<2.0Heptachlor epoxide ug/kg2.0<2.0Methoxychlor ug/kg20<20Toxaphene ug/kg100<100
ug/kg 5.00 50-150Surrogate: Tetrachloro-meta-xylene 1105.49Prepared: 12/19/05 Analyzed: 12/20/05 LCS (B5L2017-BS1)
4,4´-DDD ug/kg4.16 4.0 5.00 60-14083.24,4´-DDE ug/kg5.66 4.0 5.00 60-1401134,4´-DDT ug/kg5.99 4.0 5.00 60-140120Aldrin ug/kg4.05 2.0 5.00 60-14081.0beta-BHC ug/kg4.65 2.0 5.00 60-14093.0delta-BHC ug/kg5.72 2.0 5.00 60-140114alpha-BHC ug/kg5.23 2.0 5.00 60-140105gamma-BHC (Lindane) ug/kg5.26 4.0 5.00 60-140105gamma-Chlordane ug/kg3.98 4.0 5.00 60-14079.6
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Date Received:
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AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061812/19/0512/30/05
Page 14 of 16
RPD%RECSourceSpikeMRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResult
Extractable Semivolatile Organic Compounds by GC - Quality ControlBatch B5L2017 - EPA 3550B
Prepared: 12/19/05 Analyzed: 12/20/05 LCS (B5L2017-BS1) Continuedalpha-Chlordane ug/kg3.87 4.0 5.00 60-14077.4Dieldrin ug/kg4.83 4.0 5.00 60-14096.6Endosulfan I ug/kg5.09 2.0 5.00 60-140102Endosulfan II ug/kg4.16 4.0 5.00 60-14083.2Endosulfan sulfate ug/kg5.87 4.0 5.00 60-140117Endrin ug/kg6.13 4.0 5.00 60-140123Endrin aldehyde ug/kg5.11 4.0 5.00 60-140102Endrin ketone ug/kg4.76 4.0 5.00 60-14095.2Heptachlor ug/kg4.46 2.0 5.00 60-14089.2Heptachlor epoxide ug/kg4.13 2.0 5.00 60-14082.6Methoxychlor ug/kg4.59 20 5.00 60-14091.8
ug/kg 5.00 50-150Surrogate: Tetrachloro-meta-xylene 1417.06Prepared: 12/19/05 Analyzed: 12/20/05 LCS Dup (B5L2017-BSD1)
4,4´-DDD ug/kg4.57 4.0 5.00 4060-14091.4 9.394,4´-DDE ug/kg6.92 4.0 5.00 4060-140138 20.04,4´-DDT ug/kg6.37 4.0 5.00 4060-140127 6.15Aldrin ug/kg4.27 2.0 5.00 4060-14085.4 5.29beta-BHC ug/kg5.96 2.0 5.00 4060-140119 24.7delta-BHC ug/kg5.63 2.0 5.00 4060-140113 1.59alpha-BHC ug/kg5.30 2.0 5.00 4060-140106 1.33gamma-BHC (Lindane) ug/kg5.31 4.0 5.00 4060-140106 0.946gamma-Chlordane ug/kg4.14 4.0 5.00 4060-14082.8 3.94alpha-Chlordane ug/kg4.02 4.0 5.00 4060-14080.4 3.80Dieldrin ug/kg4.30 4.0 5.00 4060-14086.0 11.6Endosulfan I ug/kg5.26 2.0 5.00 4060-140105 3.29Endosulfan II ug/kg4.57 4.0 5.00 4060-14091.4 9.39Endosulfan sulfate ug/kg6.74 4.0 5.00 4060-140135 13.8Endrin ug/kg6.08 4.0 5.00 4060-140122 0.819Endrin aldehyde ug/kg5.13 4.0 5.00 4060-140103 0.391Endrin ketone ug/kg5.01 4.0 5.00 4060-140100 5.12Heptachlor ug/kg4.63 2.0 5.00 4060-14092.6 3.74
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
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Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061812/19/0512/30/05
Page 15 of 16
RPD%RECSourceSpikeMRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResult
Extractable Semivolatile Organic Compounds by GC - Quality ControlBatch B5L2017 - EPA 3550B
Prepared: 12/19/05 Analyzed: 12/20/05 LCS Dup (B5L2017-BSD1) ContinuedHeptachlor epoxide ug/kg4.09 2.0 5.00 4060-14081.8 0.973Methoxychlor ug/kg5.09 20 5.00 4060-140102 10.3
ug/kg 5.00 50-150Surrogate: Tetrachloro-meta-xylene 1266.30Purgeable Volatile Organic Compounds by GC/MS - Quality ControlBatch B5L2014 - EPA 5035
Prepared & Analyzed: 12/20/05 Blank (B5L2014-BLK1)cis-1,2-Dichloroethylene ug/kg5.0<5.0Tetrachloroethylene (PCE) ug/kg5.0<5.0Trichloroethylene (TCE) ug/kg5.0<5.0Vinyl chloride ug/kg5.0<5.0
ug/kg 100 80-120Surrogate: 4-Bromofluorobenzene 101101ug/kg 100 80-120Surrogate: Dibromofluoromethane 86.686.6ug/kg 100 80-120Surrogate: Toluene-d8 102102
Prepared & Analyzed: 12/20/05 LCS (B5L2014-BS1)cis-1,2-Dichloroethylene ug/kg39.4 5.0 40.0 75-12598.5Tetrachloroethylene (PCE) ug/kg42.0 5.0 40.0 75-125105Trichloroethylene (TCE) ug/kg41.6 5.0 40.0 75-125104Vinyl chloride ug/kg40.4 5.0 40.0 75-125101
ug/kg 100 80-120Surrogate: 4-Bromofluorobenzene 99.099.0ug/kg 100 80-120Surrogate: Dibromofluoromethane 93.293.2ug/kg 100 80-120Surrogate: Toluene-d8 98.498.4
Prepared & Analyzed: 12/20/05 LCS Dup (B5L2014-BSD1)cis-1,2-Dichloroethylene ug/kg41.4 5.0 40.0 4075-125104 4.95Tetrachloroethylene (PCE) ug/kg39.6 5.0 40.0 4075-12599.0 5.88Trichloroethylene (TCE) ug/kg42.6 5.0 40.0 4075-125106 2.38Vinyl chloride ug/kg38.0 5.0 40.0 4075-12595.0 6.12
ug/kg 100 80-120Surrogate: 4-Bromofluorobenzene 103103ug/kg 100 80-120Surrogate: Dibromofluoromethane 102102ug/kg 100 80-120Surrogate: Toluene-d8 99.299.2
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
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Date Received:
LABORATORY ANALYSIS RESULTS
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PES Environmental, Inc.
KCOP241.060.02.014
A6061812/19/0512/30/05
Page 16 of 16
Special Notes: The recovery for this analyte is slightly below acceptance criteria.SP1
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
9765 Eton Avenue
California 91311Tel: (818) 998-5547
Fax: (818) 998-7258
Chatsworth
December 30, 2005
Novato, CA 94947
Enclosed is an analytical report for the above-referenced project. The samples included in this report were received on 12/21/05 11:27 and analyzed in accordance with the attached chain-of-custody.
Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Assurance Program Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety.
If you have any questions regarding this report or require additional information please call me at American Analytics.
Sincerely,
Kyle FloryPES Environmental, Inc.1682 Novato Blvd. Ste., 100
Eydie Schwartz
Project Manager
Re : KCOP / 241.060.02.014
A60619 / 5L21005
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061912/21/0512/30/05
Page 2 of 17
Sample ID Laboratory ID Matrix TAT Date Sampled Date Received8081A OCPs
BN-13 5L21005-01 Soil 5 12/21/05 10:35 12/21/05 11:27
8260B/5035 Soil Full ListBN-13 5L21005-01 Soil 0 12/21/05 10:35 12/21/05 11:27
8270CBN-13 5L21005-01 Soil 5 12/21/05 10:35 12/21/05 11:27
Eydie SchwartzProject Manager
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Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061912/21/0512/30/05
Page 3 of 17
MethodAnalyzedPreparedDilutionUnitsMRLResultAnalyte
ANALYTICAL DATA SUMMARY
Sample Name
Extractable Semivolatile Organic Compounds by GC
Extractable Semivolatile Organic Compounds by GC/MS
Purgeable Volatile Organic Compounds by GC/MSEPA
8260B/50357.4 12/21/05 ug/kg 1Tetrachloroethylene (PCE) 5.0 12/21/05 BN-13
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LABORATORY ANALYSIS RESULTS
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PES Environmental, Inc.
KCOP241.060.02.014
A6061912/21/0512/30/05
Page 4 of 17
Units: Method:Sample Matrix:
Extractable Semivolatile Organic Compounds by GCSoil ug/kg
Date Sampled: 12/21/05Date Prepared: 12/22/05
12/27/05Date Analyzed:AA ID No: 5L21005-01Client ID No: BN-13
5Dilution Factor: MRL
8081A OCPs (EPA 8081A)
4,4´-DDD <20 4.04,4´-DDE <20 4.04,4´-DDT <20 4.0Aldrin <10 2.0beta-BHC <10 2.0delta-BHC <10 2.0alpha-BHC <10 2.0gamma-BHC (Lindane) <20 4.0gamma-Chlordane <20 4.0alpha-Chlordane <20 4.0Chlordane <100 20Dieldrin <20 4.0Endosulfan I <10 2.0Endosulfan II <20 4.0Endosulfan sulfate <20 4.0Endrin <20 4.0Endrin aldehyde <20 4.0Endrin ketone <20 4.0Heptachlor <10 2.0Heptachlor epoxide <10 2.0Methoxychlor <100 20Toxaphene <500 100
Surrogates %REC LimitsTetrachloro-meta-xylene 92.0% 50-150
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
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Date Received:
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PES Environmental, Inc.
KCOP241.060.02.014
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Page 5 of 17
Units: Method:Sample Matrix:
Extractable Semivolatile Organic Compounds by GC/MSSoil mg/kg
Date Sampled: 12/21/05Date Prepared: 12/22/05
12/29/05Date Analyzed:AA ID No: 5L21005-01Client ID No: BN-13
1Dilution Factor: MRL
8270C (EPA 8270C)
3,3´-Dichlorobenzidine <0.40 0.40Acenaphthene <0.10 0.10Acenaphthylene <0.10 0.10Aniline <0.20 0.20Anthracene <0.10 0.10Azobenzene <0.10 0.10Benzidine <0.40 0.40Benzo(a)anthracene <0.10 0.10Benzo(a)pyrene <0.10 0.10Benzo(b)fluoranthene <0.10 0.10Benzo(g,h,i)perylene <0.10 0.10Benzoic acid <1.0 1.0Benzo(k)fluoranthene <0.10 0.10Benzyl alcohol <0.10 0.104-Bromophenyl phenyl ether <0.10 0.10Butyl benzyl phthalate <0.50 0.504-Chloro-3-methylphenol <0.20 0.204-Chloroaniline <0.40 0.40Bis(2-chloroethoxy)methane <0.10 0.10Bis(2-chloroethyl)ether <0.10 0.10Bis(2-chloroisopropyl)ether <0.10 0.102-Chloronaphthalene <0.10 0.102-Chlorophenol <0.10 0.104-Chlorophenyl phenyl ether <0.10 0.10Chrysene <0.10 0.10Dibenzo(a,h)anthracene <0.10 0.10Dibenzofuran <0.10 0.10
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
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Date Received:
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PES Environmental, Inc.
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Page 6 of 17
Units: Method:Sample Matrix:
Extractable Semivolatile Organic Compounds by GC/MSSoil mg/kg
Date Sampled: 12/21/05Date Prepared: 12/22/05
12/29/05Date Analyzed:AA ID No: 5L21005-01Client ID No: BN-13
1Dilution Factor: MRL
8270C (EPA 8270C) (continued)Di-n-butyl phthalate <2.0 2.01,2-Dichlorobenzene <0.10 0.101,3-Dichlorobenzene <0.10 0.101,4-Dichlorobenzene <0.10 0.102,4-Dichlorophenol <0.10 0.10Diethyl phthalate <0.80 0.802,4-Dimethylphenol <0.10 0.10Dimethyl phthalate <0.20 0.204,6-Dinitro-2-methylphenol <0.20 0.202,4-Dinitrophenol <0.40 0.402,6-Dinitrotoluene <0.10 0.102,4-Dinitrotoluene <0.10 0.10Di-n-octyl phthalate <0.10 0.101,2-Diphenylhydrazine <0.10 0.10Bis(2-ethylhexyl)phthalate <0.20 0.20Fluoranthene <0.10 0.10Fluorene <0.10 0.10Hexachlorobenzene <0.10 0.10Hexachlorobutadiene <0.10 0.10Hexachlorocyclopentadiene <0.10 0.10Hexachloroethane <0.10 0.10Indeno (1,2,3-cd) pyrene <0.40 0.40Isophorone <0.10 0.102-Methylnaphthalene <0.10 0.102-Methylphenol <0.20 0.203-Methylphenol <0.20 0.204-Methylphenol <0.20 0.20
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
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Date Received:
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Page 7 of 17
Units: Method:Sample Matrix:
Extractable Semivolatile Organic Compounds by GC/MSSoil mg/kg
Date Sampled: 12/21/05Date Prepared: 12/22/05
12/29/05Date Analyzed:AA ID No: 5L21005-01Client ID No: BN-13
1Dilution Factor: MRL
8270C (EPA 8270C) (continued)Naphthalene <0.10 0.104-Nitroaniline <0.50 0.503-Nitroaniline <0.40 0.402-Nitroaniline <0.10 0.10Nitrobenzene <0.10 0.102-Nitrophenol <0.20 0.204-Nitrophenol <0.20 0.20N-Nitrosodimethylamine <0.10 0.10N-Nitrosodiphenylamine <0.10 0.10N-Nitrosodi-n-propylamine <0.10 0.10Pentachlorophenol <0.10 0.10Phenanthrene <0.10 0.10Phenol <0.10 0.10Pyrene <0.10 0.101,2,4-Trichlorobenzene <0.10 0.102,4,5-Trichlorophenol <0.20 0.202,4,6-Trichlorophenol <0.20 0.20
Surrogates %REC Limits2-Fluorobiphenyl 0.00 43-1162-Fluorophenol 0.00 21-100Nitrobenzene-d5 0.00 35-134Phenol-d6 0.00 10-94Terphenyl-dl4 0.00 33-1412,4,6-Tribromophenol 0.00 10-123
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
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KCOP241.060.02.014
A6061912/21/0512/30/05
Page 8 of 17
Units: Method:Sample Matrix:
Purgeable Volatile Organic Compounds by GC/MSSoil ug/kg
Date Sampled: 12/21/05Date Prepared: 12/21/05
12/21/05Date Analyzed:AA ID No: 5L21005-01Client ID No: BN-13
1Dilution Factor: MRL
8260B/5035 Soil Full List (EPA 8260B/5035)
cis-1,2-Dichloroethylene <5.0 5.0Tetrachloroethylene (PCE) 7.4 5.0Trichloroethylene (TCE) <5.0 5.0Vinyl chloride <5.0 5.0
Surrogates %REC Limits4-Bromofluorobenzene 104% 80-120Dibromofluoromethane 90.1% 80-120Toluene-d8 104% 80-120
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
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Date Received:
LABORATORY ANALYSIS RESULTS
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Page 9 of 17
RPD%RECSourceSpikeMRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResult
Extractable Semivolatile Organic Compounds by GC/MS - Quality ControlBatch B5L2217 - EPA 3550B
Prepared: 12/22/05 Analyzed: 12/20/05 Blank (B5L2217-BLK1)3,3´-Dichlorobenzidine mg/kg0.40<0.40Acenaphthene mg/kg0.10<0.10Acenaphthylene mg/kg0.10<0.10Aniline mg/kg0.20<0.20Anthracene mg/kg0.10<0.10Azobenzene mg/kg0.10<0.10Benzidine mg/kg0.40<0.40Benzo(a)anthracene mg/kg0.10<0.10Benzo(a)pyrene mg/kg0.10<0.10Benzo(b)fluoranthene mg/kg0.10<0.10Benzo(g,h,i)perylene mg/kg0.10<0.10Benzoic acid mg/kg1.0<1.0Benzo(k)fluoranthene mg/kg0.10<0.10Benzyl alcohol mg/kg0.10<0.104-Bromophenyl phenyl ether mg/kg0.10<0.10Butyl benzyl phthalate mg/kg0.50<0.504-Chloro-3-methylphenol mg/kg0.20<0.204-Chloroaniline mg/kg0.40<0.40Bis(2-chloroethoxy)methane mg/kg0.10<0.10Bis(2-chloroethyl)ether mg/kg0.10<0.10Bis(2-chloroisopropyl)ether mg/kg0.10<0.102-Chloronaphthalene mg/kg0.10<0.102-Chlorophenol mg/kg0.10<0.104-Chlorophenyl phenyl ether mg/kg0.10<0.10Chrysene mg/kg0.10<0.10Dibenzo(a,h)anthracene mg/kg0.10<0.10Dibenzofuran mg/kg0.10<0.10Di-n-butyl phthalate mg/kg2.0<2.01,2-Dichlorobenzene mg/kg0.10<0.10
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061912/21/0512/30/05
Page 10 of 17
RPD%RECSourceSpikeMRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResult
Extractable Semivolatile Organic Compounds by GC/MS - Quality ControlBatch B5L2217 - EPA 3550B
Prepared: 12/22/05 Analyzed: 12/20/05 Blank (B5L2217-BLK1) Continued1,3-Dichlorobenzene mg/kg0.10<0.101,4-Dichlorobenzene mg/kg0.10<0.102,4-Dichlorophenol mg/kg0.10<0.10Diethyl phthalate mg/kg0.80<0.802,4-Dimethylphenol mg/kg0.10<0.10Dimethyl phthalate mg/kg0.20<0.204,6-Dinitro-2-methylphenol mg/kg0.20<0.202,4-Dinitrophenol mg/kg0.40<0.402,6-Dinitrotoluene mg/kg0.10<0.102,4-Dinitrotoluene mg/kg0.10<0.10Di-n-octyl phthalate mg/kg0.10<0.101,2-Diphenylhydrazine mg/kg0.10<0.10Bis(2-ethylhexyl)phthalate mg/kg0.20<0.20Fluoranthene mg/kg0.10<0.10Fluorene mg/kg0.10<0.10Hexachlorobenzene mg/kg0.10<0.10Hexachlorobutadiene mg/kg0.10<0.10Hexachlorocyclopentadiene mg/kg0.10<0.10Hexachloroethane mg/kg0.10<0.10Indeno (1,2,3-cd) pyrene mg/kg0.40<0.40Isophorone mg/kg0.10<0.102-Methylnaphthalene mg/kg0.10<0.102-Methylphenol mg/kg0.20<0.203-Methylphenol mg/kg0.20<0.204-Methylphenol mg/kg0.20<0.20Naphthalene mg/kg0.10<0.104-Nitroaniline mg/kg0.50<0.503-Nitroaniline mg/kg0.40<0.402-Nitroaniline mg/kg0.10<0.10
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061912/21/0512/30/05
Page 11 of 17
RPD%RECSourceSpikeMRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResult
Extractable Semivolatile Organic Compounds by GC/MS - Quality ControlBatch B5L2217 - EPA 3550B
Prepared: 12/22/05 Analyzed: 12/20/05 Blank (B5L2217-BLK1) ContinuedNitrobenzene mg/kg0.10<0.102-Nitrophenol mg/kg0.20<0.204-Nitrophenol mg/kg0.20<0.20N-Nitrosodimethylamine mg/kg0.10<0.10N-Nitrosodiphenylamine mg/kg0.10<0.10N-Nitrosodi-n-propylamine mg/kg0.10<0.10Pentachlorophenol mg/kg0.10<0.10Phenanthrene mg/kg0.10<0.10Phenol mg/kg0.10<0.10Pyrene mg/kg0.10<0.101,2,4-Trichlorobenzene mg/kg0.10<0.102,4,5-Trichlorophenol mg/kg0.20<0.202,4,6-Trichlorophenol mg/kg0.20<0.20
mg/kg 1.00 43-116Surrogate: 2-Fluorobiphenyl 49.80.498mg/kg 2.00 21-100Surrogate: 2-Fluorophenol 47.00.940mg/kg 1.00 35-134Surrogate: Nitrobenzene-d5 47.40.474mg/kg 2.00 10-94Surrogate: Phenol-d6 47.10.942mg/kg 1.00 33-141Surrogate: Terphenyl-dl4 76.00.760mg/kg 2.00 10-123Surrogate: 2,4,6-Tribromophenol 35.60.712
Prepared: 12/22/05 Analyzed: 12/20/05 LCS (B5L2217-BS1)Acenaphthene mg/kg0.524 0.10 1.00 50-12152.4Anthracene mg/kg0.630 0.10 1.00 41-12163.0Benzo(a)pyrene mg/kg0.607 0.10 1.00 17-16360.7Benzo(b)fluoranthene mg/kg0.524 0.10 1.00 33-13752.4Butyl benzyl phthalate mg/kg0.712 0.50 1.00 19-13971.24-Chloro-3-methylphenol mg/kg0.968 0.20 1.00 22-14796.8Bis(2-chloroethyl)ether mg/kg0.540 0.10 1.00 26-12254.02-Chloronaphthalene mg/kg0.626 0.10 1.00 60-11862.64-Chlorophenyl phenyl ether mg/kg0.481 0.10 1.00 41-12848.11,4-Dichlorobenzene mg/kg0.531 0.10 1.00 26-10553.1
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061912/21/0512/30/05
Page 12 of 17
RPD%RECSourceSpikeMRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResult
Extractable Semivolatile Organic Compounds by GC/MS - Quality ControlBatch B5L2217 - EPA 3550B
Prepared: 12/22/05 Analyzed: 12/20/05 LCS (B5L2217-BS1) Continued2,4-Dichlorophenol mg/kg0.482 0.10 1.00 39-13548.2Di-n-octyl phthalate mg/kg0.528 0.10 1.00 4-14652.8Fluoranthene mg/kg0.408 0.10 1.00 47-12540.8Fluorene mg/kg0.521 0.10 1.00 60-12052.1Hexachlorobenzene mg/kg0.634 0.10 1.00 2-15263.4Hexachlorobutadiene mg/kg0.479 0.10 1.00 24-11647.9Hexachloroethane mg/kg0.480 0.10 1.00 40-11348.0Isophorone mg/kg0.524 0.10 1.00 21-19652.4Naphthalene mg/kg0.578 0.10 1.00 25-12157.8Nitrobenzene mg/kg0.560 0.10 1.00 38-13356.02-Nitrophenol mg/kg0.360 0.20 1.00 2-16336.0N-Nitrosodi-n-propylamine mg/kg0.584 0.10 1.00 2-23058.4Pentachlorophenol mg/kg0.290 0.10 1.00 14-17629.0Phenol mg/kg0.584 0.10 1.00 5-11258.4Pyrene mg/kg0.690 0.10 1.00 52-11569.01,2,4-Trichlorobenzene mg/kg0.480 0.10 1.00 44-14248.02,4,6-Trichlorophenol mg/kg0.600 0.20 1.00 37-14460.0
mg/kg 0.250 43-116Surrogate: 2-Fluorobiphenyl 2430.608mg/kg 0.500 21-100Surrogate: 2-Fluorophenol 2261.13mg/kg 0.250 35-134Surrogate: Nitrobenzene-d5 2400.600mg/kg 2.00 10-94Surrogate: Phenol-d6 58.51.17mg/kg 0.250 33-141Surrogate: Terphenyl-dl4 3100.776mg/kg 0.500 10-123Surrogate: 2,4,6-Tribromophenol 1200.598
Prepared: 12/22/05 Analyzed: 12/20/05 LCS Dup (B5L2217-BSD1)Acenaphthene mg/kg0.473 0.10 1.00 4050-12147.3 10.2Anthracene mg/kg0.506 0.10 1.00 4041-12150.6 21.8Benzo(a)pyrene mg/kg0.518 0.10 1.00 4017-16351.8 15.8Benzo(b)fluoranthene mg/kg0.430 0.10 1.00 4033-13743.0 19.7Butyl benzyl phthalate mg/kg0.410 0.50 1.00 4019-13941.0 53.84-Chloro-3-methylphenol mg/kg0.758 0.20 1.00 4022-14775.8 24.3Bis(2-chloroethyl)ether mg/kg0.440 0.10 1.00 4026-12244.0 20.4
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061912/21/0512/30/05
Page 13 of 17
RPD%RECSourceSpikeMRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResult
Extractable Semivolatile Organic Compounds by GC/MS - Quality ControlBatch B5L2217 - EPA 3550B
Prepared: 12/22/05 Analyzed: 12/20/05 LCS Dup (B5L2217-BSD1) Continued2-Chloronaphthalene mg/kg0.374 0.10 1.00 4060-11837.4 50.44-Chlorophenyl phenyl ether mg/kg0.450 0.10 1.00 4041-12845.0 6.661,4-Dichlorobenzene mg/kg0.458 0.10 1.00 4026-10545.8 14.82,4-Dichlorophenol mg/kg0.296 0.10 1.00 4039-13529.6 47.8Di-n-octyl phthalate mg/kg0.422 0.10 1.00 404-14642.2 22.3Fluoranthene mg/kg0.447 0.10 1.00 4047-12544.7 9.12Fluorene mg/kg0.450 0.10 1.00 4060-12045.0 14.6Hexachlorobenzene mg/kg0.522 0.10 1.00 402-15252.2 19.4Hexachlorobutadiene mg/kg0.490 0.10 1.00 4024-11649.0 2.27Hexachloroethane mg/kg0.350 0.10 1.00 4040-11335.0 31.3Isophorone mg/kg0.454 0.10 1.00 4021-19645.4 14.3Naphthalene mg/kg0.500 0.10 1.00 4025-12150.0 14.5Nitrobenzene mg/kg0.384 0.10 1.00 4038-13338.4 37.32-Nitrophenol mg/kg0.165 0.20 1.00 402-16316.5 74.3N-Nitrosodi-n-propylamine mg/kg0.550 0.10 1.00 402-23055.0 6.00Pentachlorophenol mg/kg0.10 1.00 4014-176<0.10Phenol mg/kg0.430 0.10 1.00 405-11243.0 30.4Pyrene mg/kg0.334 0.10 1.00 4052-11533.4 69.51,2,4-Trichlorobenzene mg/kg0.412 0.10 1.00 4044-14241.2 15.22,4,6-Trichlorophenol mg/kg0.374 0.20 1.00 4037-14437.4 46.4
mg/kg 0.250 43-116Surrogate: 2-Fluorobiphenyl 2000.500mg/kg 0.500 21-100Surrogate: 2-Fluorophenol 1790.894mg/kg 0.250 35-134Surrogate: Nitrobenzene-d5 1450.362mg/kg 2.00 10-94Surrogate: Phenol-d6 48.30.966mg/kg 0.250 33-141Surrogate: Terphenyl-dl4 1790.448mg/kg 0.500 10-123Surrogate: 2,4,6-Tribromophenol 1400.702
Extractable Semivolatile Organic Compounds by GC - Quality ControlBatch B5L2224 - EPA 3550B
Prepared: 12/22/05 Analyzed: 12/27/05 Blank (B5L2224-BLK1)4,4´-DDD ug/kg4.0<4.0
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061912/21/0512/30/05
Page 14 of 17
RPD%RECSourceSpikeMRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResult
Extractable Semivolatile Organic Compounds by GC - Quality ControlBatch B5L2224 - EPA 3550B
Prepared: 12/22/05 Analyzed: 12/27/05 Blank (B5L2224-BLK1) Continued4,4´-DDE ug/kg4.0<4.04,4´-DDT ug/kg4.0<4.0Aldrin ug/kg2.0<2.0beta-BHC ug/kg2.0<2.0delta-BHC ug/kg2.0<2.0alpha-BHC ug/kg2.0<2.0gamma-BHC (Lindane) ug/kg4.0<4.0gamma-Chlordane ug/kg4.0<4.0alpha-Chlordane ug/kg4.0<4.0Chlordane ug/kg20<20Dieldrin ug/kg4.0<4.0Endosulfan I ug/kg2.0<2.0Endosulfan II ug/kg4.0<4.0Endosulfan sulfate ug/kg4.0<4.0Endrin ug/kg4.0<4.0Endrin aldehyde ug/kg4.0<4.0Endrin ketone ug/kg4.0<4.0Heptachlor ug/kg2.0<2.0Heptachlor epoxide ug/kg2.0<2.0Methoxychlor ug/kg20<20Toxaphene ug/kg100<100
ug/kg 5.00 50-150Surrogate: Tetrachloro-meta-xylene 77.23.86Prepared: 12/22/05 Analyzed: 12/27/05 LCS (B5L2224-BS1)
4,4´-DDD ug/kg4.42 4.0 5.00 60-14088.44,4´-DDE ug/kg5.72 4.0 5.00 60-1401144,4´-DDT ug/kg5.66 4.0 5.00 60-140113Aldrin ug/kg4.22 2.0 5.00 60-14084.4beta-BHC ug/kg6.19 2.0 5.00 60-140124delta-BHC ug/kg5.62 2.0 5.00 60-140112
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061912/21/0512/30/05
Page 15 of 17
RPD%RECSourceSpikeMRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResult
Extractable Semivolatile Organic Compounds by GC - Quality ControlBatch B5L2224 - EPA 3550B
Prepared: 12/22/05 Analyzed: 12/27/05 LCS (B5L2224-BS1) Continuedalpha-BHC ug/kg5.18 2.0 5.00 60-140104gamma-BHC (Lindane) ug/kg4.99 4.0 5.00 60-14099.8gamma-Chlordane ug/kg3.91 4.0 5.00 60-14078.2alpha-Chlordane ug/kg3.65 4.0 5.00 60-14073.0Dieldrin ug/kg3.82 4.0 5.00 60-14076.4Endosulfan I ug/kg4.65 2.0 5.00 60-14093.0Endosulfan II ug/kg4.42 4.0 5.00 60-14088.4Endosulfan sulfate ug/kg5.23 4.0 5.00 60-140105Endrin ug/kg5.02 4.0 5.00 60-140100Endrin aldehyde ug/kg3.84 4.0 5.00 60-14076.8Endrin ketone ug/kg4.01 4.0 5.00 60-14080.2Heptachlor ug/kg4.24 2.0 5.00 60-14084.8Heptachlor epoxide ug/kg3.95 2.0 5.00 60-14079.0Methoxychlor ug/kg4.89 20 5.00 60-14097.8
ug/kg 5.00 50-150Surrogate: Tetrachloro-meta-xylene 1226.10Purgeable Volatile Organic Compounds by GC/MS - Quality ControlBatch B5L2120 - EPA 5035
Prepared & Analyzed: 12/21/05 Blank (B5L2120-BLK1)cis-1,2-Dichloroethylene ug/kg5.0<5.0Tetrachloroethylene (PCE) ug/kg5.0<5.0Trichloroethylene (TCE) ug/kg5.0<5.0Vinyl chloride ug/kg5.0<5.0
ug/kg 100 80-120Surrogate: 4-Bromofluorobenzene 101101ug/kg 100 80-120Surrogate: Dibromofluoromethane 86.686.6ug/kg 100 80-120Surrogate: Toluene-d8 102102
Prepared & Analyzed: 12/21/05 LCS (B5L2120-BS1)cis-1,2-Dichloroethylene ug/kg39.6 5.0 40.0 75-12599.0Tetrachloroethylene (PCE) ug/kg40.8 5.0 40.0 75-125102Trichloroethylene (TCE) ug/kg41.0 5.0 40.0 75-125102Vinyl chloride ug/kg40.4 5.0 40.0 75-125101
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061912/21/0512/30/05
Page 16 of 17
RPD%RECSourceSpikeMRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResult
Purgeable Volatile Organic Compounds by GC/MS - Quality ControlBatch B5L2120 - EPA 5035
Prepared & Analyzed: 12/21/05 LCS (B5L2120-BS1) Continuedug/kg 100 80-120Surrogate: 4-Bromofluorobenzene 101101ug/kg 100 80-120Surrogate: Dibromofluoromethane 95.095.0ug/kg 100 80-120Surrogate: Toluene-d8 101101
Prepared & Analyzed: 12/21/05 LCS Dup (B5L2120-BSD1)cis-1,2-Dichloroethylene ug/kg40.8 5.0 40.0 4075-125102 2.99Tetrachloroethylene (PCE) ug/kg45.6 5.0 40.0 4075-125114 11.1Trichloroethylene (TCE) ug/kg42.0 5.0 40.0 4075-125105 2.41Vinyl chloride ug/kg35.4 5.0 40.0 4075-12588.5 13.2
ug/kg 100 80-120Surrogate: 4-Bromofluorobenzene 102102ug/kg 100 80-120Surrogate: Dibromofluoromethane 102102ug/kg 100 80-120Surrogate: Toluene-d8 94.094.0
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061912/21/0512/30/05
Page 17 of 17
Special Notes
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
9765 Eton Avenue
California 91311Tel: (818) 998-5547
Fax: (818) 998-7258
Chatsworth
December 29, 2005
Novato, CA 94947
Enclosed is an analytical report for the above-referenced project. The samples included in this report were received on 12/23/05 17:29 and analyzed in accordance with the attached chain-of-custody.
Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Assurance Program Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety.
If you have any questions regarding this report or require additional information please call me at American Analytics.
Sincerely,
Kyle FloryPES Environmental, Inc.1682 Novato Blvd. Ste., 100
Eydie Schwartz
Project Manager
Re : KCOP / 241.060.02.014
A60621 / 5L27001
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6062112/23/0512/29/05
Page 2 of 6
Sample ID Laboratory ID Matrix TAT Date Sampled Date Received8260B/5035 Soil Full List
SNW-4B 5L27001-01 Soil 5 12/23/05 07:30 12/23/05 17:29
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6062112/23/0512/29/05
Page 3 of 6
MethodAnalyzedPreparedDilutionUnitsMRLResultAnalyte
ANALYTICAL DATA SUMMARY
Sample Name
Purgeable Volatile Organic Compounds by GC/MSEPA
8260B/503552 12/27/05 ug/kg 1Tetrachloroethylene (PCE) 5.0 12/27/05 SNW-4B
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6062112/23/0512/29/05
Page 4 of 6
Units: Method:Sample Matrix:
Purgeable Volatile Organic Compounds by GC/MSSoil ug/kg
Date Sampled: 12/23/05Date Prepared: 12/27/05
12/27/05Date Analyzed:AA ID No: 5L27001-01Client ID No: SNW-4B
1Dilution Factor: MRL
8260B/5035 Soil Full List (EPA 8260B/5035)
cis-1,2-Dichloroethylene <5.0 5.0Tetrachloroethylene (PCE) 52 5.0Trichloroethylene (TCE) <5.0 5.0Vinyl chloride <5.0 5.0
Surrogates %REC Limits4-Bromofluorobenzene 100% 80-120Dibromofluoromethane 90.0% 80-120Toluene-d8 110% 80-120
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6062112/23/0512/29/05
Page 5 of 6
RPD%RECSourceSpikeMRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResult
Purgeable Volatile Organic Compounds by GC/MS - Quality ControlBatch B5L2722 - EPA 5035
Prepared & Analyzed: 12/27/05 Blank (B5L2722-BLK1)cis-1,2-Dichloroethylene ug/kg5.0<5.0Tetrachloroethylene (PCE) ug/kg5.0<5.0Trichloroethylene (TCE) ug/kg5.0<5.0Vinyl chloride ug/kg5.0<5.0
ug/kg 100 80-120Surrogate: 4-Bromofluorobenzene 97.297.2ug/kg 100 80-120Surrogate: Dibromofluoromethane 93.693.6ug/kg 100 80-120Surrogate: Toluene-d8 106106
Prepared & Analyzed: 12/27/05 LCS (B5L2722-BS1)cis-1,2-Dichloroethylene ug/kg36.4 5.0 40.0 75-12591.0Tetrachloroethylene (PCE) ug/kg45.0 5.0 40.0 75-125112Trichloroethylene (TCE) ug/kg36.2 5.0 40.0 75-12590.5Vinyl chloride ug/kg43.2 5.0 40.0 75-125108
ug/kg 100 80-120Surrogate: 4-Bromofluorobenzene 99.699.6ug/kg 100 80-120Surrogate: Dibromofluoromethane 101101ug/kg 100 80-120Surrogate: Toluene-d8 102102
Prepared & Analyzed: 12/27/05 LCS Dup (B5L2722-BSD1)cis-1,2-Dichloroethylene ug/kg34.2 5.0 40.0 4075-12585.5 6.23Tetrachloroethylene (PCE) ug/kg44.8 5.0 40.0 4075-125112 0.445Trichloroethylene (TCE) ug/kg36.6 5.0 40.0 4075-12591.5 1.10Vinyl chloride ug/kg39.8 5.0 40.0 4075-12599.5 8.19
ug/kg 100 80-120Surrogate: 4-Bromofluorobenzene 100100ug/kg 100 80-120Surrogate: Dibromofluoromethane 104104ug/kg 100 80-120Surrogate: Toluene-d8 102102
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6062112/23/0512/29/05
Page 6 of 6
Special Notes
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
9765 Eton Avenue
California 91311Tel: (818) 998-5547
Fax: (818) 998-7258
Chatsworth
December 19, 2005
Novato, CA 94947
Enclosed is an analytical report for the above-referenced project. The samples included in this report were received on 12/12/05 19:05 and analyzed in accordance with the attached chain-of-custody.
Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Assurance Program Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety.
If you have any questions regarding this report or require additional information please call me at American Analytics.
Sincerely,
Kyle FloryPES Environmental, Inc.1682 Novato Blvd. Ste., 100
Eydie Schwartz
Project Manager
Re : KCOP / 241.060.02.014
A60613 / 5L13004
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061312/12/0512/19/05
Page 2 of 7
Sample ID Laboratory ID Matrix TAT Date Sampled Date Received8260B/5035 Soil Full List
SP-1 5L13004-01 Soil 1 12/12/05 12:35 12/12/05 19:05
SP-2 5L13004-02 Soil 1 12/12/05 12:40 12/12/05 19:05
ASP-1 5L13004-03 Soil 1 12/12/05 13:20 12/12/05 19:05
ASP-2 5L13004-04 Soil 1 12/12/05 13:22 12/12/05 19:05
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061312/12/0512/19/05
Page 3 of 7
MethodAnalyzedPreparedDilutionUnitsMRLResultAnalyte
ANALYTICAL DATA SUMMARY
Sample Name
Purgeable Volatile Organic Compounds by GC/MSEPA
8260B/503511 12/13/05 ug/kg 1Tetrachloroethylene (PCE) 5.0 12/13/05 SP-1
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061312/12/0512/19/05
Page 4 of 7
Units: Method:Sample Matrix:
Purgeable Volatile Organic Compounds by GC/MSSoil ug/kg
Date Sampled: 12/12/05 12/12/05 12/12/05 12/12/05Date Prepared: 12/13/05 12/13/05 12/13/05 12/13/05
12/13/05 12/13/05 12/13/05 12/13/05Date Analyzed:AA ID No: 5L13004-01 5L13004-02 5L13004-03 5L13004-04Client ID No: SP-1 SP-2 ASP-1 ASP-2
1111Dilution Factor: MRL
8260B/5035 Soil Full List (EPA 8260B/5035)
cis-1,2-Dichloroethylene <5.0<5.0<5.0<5.0 5.0Tetrachloroethylene (PCE) <5.0<5.0<5.011 5.0Trichloroethylene (TCE) <5.0<5.0<5.0<5.0 5.0Vinyl chloride <5.0<5.0<5.0<5.0 5.0
Surrogates %REC Limits4-Bromofluorobenzene 94.0% 96.0% 134% [1] 140% [1] 80-120Dibromofluoromethane 88.0% 92.0% 98.0% 106% 80-120Toluene-d8 102% 100% 120% 124% [1] 80-120
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061312/12/0512/19/05
Page 5 of 7
RPD%RECSourceSpikeMRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResult
Purgeable Volatile Organic Compounds by GC/MS - Quality ControlBatch B5L1401 - EPA 5035
Prepared & Analyzed: 12/13/05 Blank (B5L1401-BLK1)cis-1,2-Dichloroethylene ug/kg5.0<5.0Tetrachloroethylene (PCE) ug/kg5.0<5.0Trichloroethylene (TCE) ug/kg5.0<5.0Vinyl chloride ug/kg5.0<5.0
ug/kg 100 80-120Surrogate: 4-Bromofluorobenzene 87.887.8ug/kg 100 80-120Surrogate: Dibromofluoromethane 99.099.0ug/kg 100 80-120Surrogate: Toluene-d8 94.694.6
Prepared & Analyzed: 12/13/05 LCS (B5L1401-BS1)cis-1,2-Dichloroethylene ug/kg43.4 5.0 40.0 75-125108Tetrachloroethylene (PCE) ug/kg39.0 5.0 40.0 75-12597.5Trichloroethylene (TCE) ug/kg41.0 5.0 40.0 75-125102Vinyl chloride ug/kg40.2 5.0 40.0 75-125100
ug/kg 100 80-120Surrogate: 4-Bromofluorobenzene 98.698.6ug/kg 100 80-120Surrogate: Dibromofluoromethane 100100ug/kg 100 80-120Surrogate: Toluene-d8 94.094.0
Prepared & Analyzed: 12/13/05 Matrix Spike (B5L1401-MS1) Source: 5L13006-05cis-1,2-Dichloroethylene ug/kg42.6 5.0 40.0 70-130106<5.0Tetrachloroethylene (PCE) ug/kg37.2 5.0 40.0 70-13093.0<5.0Trichloroethylene (TCE) ug/kg40.8 5.0 40.0 70-130102<5.0Vinyl chloride ug/kg35.2 5.0 40.0 70-13088.0<5.0
ug/kg 100 80-120Surrogate: 4-Bromofluorobenzene 100100ug/kg 100 80-120Surrogate: Dibromofluoromethane 104104ug/kg 100 80-120Surrogate: Toluene-d8 93.493.4
Prepared & Analyzed: 12/13/05 Matrix Spike Dup (B5L1401-MSD1) Source: 5L13006-05cis-1,2-Dichloroethylene ug/kg39.4 5.0 40.0 4070-13098.5 7.80<5.0Tetrachloroethylene (PCE) ug/kg43.2 5.0 40.0 4070-130108 14.9<5.0Trichloroethylene (TCE) ug/kg40.2 5.0 40.0 4070-130100 1.48<5.0Vinyl chloride ug/kg36.6 5.0 40.0 4070-13091.5 3.90<5.0
ug/kg 100 80-120Surrogate: 4-Bromofluorobenzene 102102
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061312/12/0512/19/05
Page 6 of 7
RPD%RECSourceSpikeMRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResult
Purgeable Volatile Organic Compounds by GC/MS - Quality ControlBatch B5L1401 - EPA 5035
Prepared & Analyzed: 12/13/05 Matrix Spike Dup (B5L1401-MSD1) Continued
Source: 5L13006-05
ug/kg 100 80-120Surrogate: Dibromofluoromethane 94.094.0ug/kg 100 80-120Surrogate: Toluene-d8 107107
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6061312/12/0512/19/05
Page 7 of 7
Special Notes: The surrogate recovery for this sample is outside of established control limits due to a sample
matrix effect.= S-04[1]
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
9765 Eton Avenue
California 91311Tel: (818) 998-5547
Fax: (818) 998-7258
Chatsworth
December 19, 2005
Novato, CA 94947
Enclosed is an analytical report for the above-referenced project. The samples included in this report were received on 12/14/05 14:50 and analyzed in accordance with the attached chain-of-custody.
Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Assurance Program Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety.
If you have any questions regarding this report or require additional information please call me at American Analytics.
Sincerely,
Kyle FloryPES Environmental, Inc.1682 Novato Blvd. Ste., 100
Eydie Schwartz
Project Manager
Re : KCOP / 241.060.02.14
A60616 / 5L14020
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.14
A6061612/14/0512/19/05
Page 2 of 6
Sample ID Laboratory ID Matrix TAT Date Sampled Date Received8260B/5035 Soil Full List
SP-3 5L14020-01 Soil 1 12/14/05 12:40 12/14/05 14:50
SP-4 5L14020-02 Soil 1 12/14/05 12:43 12/14/05 14:50
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.14
A6061612/14/0512/19/05
Page 3 of 6
MethodAnalyzedPreparedDilutionUnitsMRLResultAnalyte
ANALYTICAL DATA SUMMARY
Sample Name
Purgeable Volatile Organic Compounds by GC/MS
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.14
A6061612/14/0512/19/05
Page 4 of 6
Units: Method:Sample Matrix:
Purgeable Volatile Organic Compounds by GC/MSSoil ug/kg
Date Sampled: 12/14/05 12/14/05Date Prepared: 12/15/05 12/15/05
12/15/05 12/15/05Date Analyzed:AA ID No: 5L14020-01 5L14020-02Client ID No: SP-3 SP-4
11Dilution Factor: MRL
8260B/5035 Soil Full List (EPA 8260B/5035)
cis-1,2-Dichloroethylene <5.0<5.0 5.0Tetrachloroethylene (PCE) <5.0<5.0 5.0Trichloroethylene (TCE) <5.0<5.0 5.0Vinyl chloride <5.0<5.0 5.0
Surrogates %REC Limits4-Bromofluorobenzene 100% 102% 80-120Dibromofluoromethane 90.0% 92.0% 80-120Toluene-d8 100% 98.0% 80-120
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.14
A6061612/14/0512/19/05
Page 5 of 6
RPD%RECSourceSpikeMRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResult
Purgeable Volatile Organic Compounds by GC/MS - Quality ControlBatch B5L1520 - EPA 5035
Prepared & Analyzed: 12/15/05 Blank (B5L1520-BLK1)cis-1,2-Dichloroethylene ug/kg5.0<5.0Tetrachloroethylene (PCE) ug/kg5.0<5.0Trichloroethylene (TCE) ug/kg5.0<5.0Vinyl chloride ug/kg5.0<5.0
ug/kg 100 80-120Surrogate: 4-Bromofluorobenzene 94.294.2ug/kg 100 80-120Surrogate: Dibromofluoromethane 96.296.2ug/kg 100 80-120Surrogate: Toluene-d8 95.495.4
Prepared & Analyzed: 12/15/05 LCS (B5L1520-BS1)cis-1,2-Dichloroethylene ug/kg39.4 5.0 40.0 75-12598.5Tetrachloroethylene (PCE) ug/kg39.8 5.0 40.0 75-12599.5Trichloroethylene (TCE) ug/kg42.4 5.0 40.0 75-125106Vinyl chloride ug/kg40.2 5.0 40.0 75-125100
ug/kg 100 80-120Surrogate: 4-Bromofluorobenzene 105105ug/kg 100 80-120Surrogate: Dibromofluoromethane 94.494.4ug/kg 100 80-120Surrogate: Toluene-d8 99.699.6
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.14
A6061612/14/0512/19/05
Page 6 of 6
Special Notes
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
9765 Eton Avenue
California 91311Tel: (818) 998-5547
Fax: (818) 998-7258
Chatsworth
December 29, 2005
Novato, CA 94947
Enclosed is an analytical report for the above-referenced project. The samples included in this report were received on 12/27/05 13:57 and analyzed in accordance with the attached chain-of-custody.
Unless otherwise noted, all analytical testing was accomplished in accordance with the guidelines established in our Quality Assurance Program Manual, applicable standard operating procedures, and other related documentation. The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety.
If you have any questions regarding this report or require additional information please call me at American Analytics.
Sincerely,
Kyle FloryPES Environmental, Inc.1682 Novato Blvd. Ste., 100
Eydie Schwartz
Project Manager
Re : KCOP / 241.060.02.014
A60622 / 5L27002
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6062212/27/0512/29/05
Page 2 of 6
Sample ID Laboratory ID Matrix TAT Date Sampled Date Received8260B/5035 Soil Full List
SP-5 5L27002-01 Soil 1 12/27/05 09:45 12/27/05 13:57
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6062212/27/0512/29/05
Page 3 of 6
MethodAnalyzedPreparedDilutionUnitsMRLResultAnalyte
ANALYTICAL DATA SUMMARY
Sample Name
Purgeable Volatile Organic Compounds by GC/MSEPA
8260B/503523 12/27/05 ug/kg 1Tetrachloroethylene (PCE) 5.0 12/27/05 SP-5
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6062212/27/0512/29/05
Page 4 of 6
Units: Method:Sample Matrix:
Purgeable Volatile Organic Compounds by GC/MSSoil ug/kg
Date Sampled: 12/27/05Date Prepared: 12/27/05
12/27/05Date Analyzed:AA ID No: 5L27002-01Client ID No: SP-5
1Dilution Factor: MRL
8260B/5035 Soil Full List (EPA 8260B/5035)
cis-1,2-Dichloroethylene <5.0 5.0Tetrachloroethylene (PCE) 23 5.0Trichloroethylene (TCE) <5.0 5.0Vinyl chloride <5.0 5.0
Surrogates %REC Limits4-Bromofluorobenzene 112% 80-120Dibromofluoromethane 62.0% [1] 80-120Toluene-d8 108% 80-120
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6062212/27/0512/29/05
Page 5 of 6
RPD%RECSourceSpikeMRL Analyte Notes LimitRPDLimits%RECResultLevelUnitsResult
Purgeable Volatile Organic Compounds by GC/MS - Quality ControlBatch B5L2722 - EPA 5035
Prepared & Analyzed: 12/27/05 Blank (B5L2722-BLK1)cis-1,2-Dichloroethylene ug/kg5.0<5.0Tetrachloroethylene (PCE) ug/kg5.0<5.0Trichloroethylene (TCE) ug/kg5.0<5.0Vinyl chloride ug/kg5.0<5.0
ug/kg 100 80-120Surrogate: 4-Bromofluorobenzene 97.297.2ug/kg 100 80-120Surrogate: Dibromofluoromethane 93.693.6ug/kg 100 80-120Surrogate: Toluene-d8 106106
Prepared & Analyzed: 12/27/05 LCS (B5L2722-BS1)cis-1,2-Dichloroethylene ug/kg36.4 5.0 40.0 75-12591.0Tetrachloroethylene (PCE) ug/kg45.0 5.0 40.0 75-125112Trichloroethylene (TCE) ug/kg36.2 5.0 40.0 75-12590.5Vinyl chloride ug/kg43.2 5.0 40.0 75-125108
ug/kg 100 80-120Surrogate: 4-Bromofluorobenzene 99.699.6ug/kg 100 80-120Surrogate: Dibromofluoromethane 101101ug/kg 100 80-120Surrogate: Toluene-d8 102102
Prepared & Analyzed: 12/27/05 LCS Dup (B5L2722-BSD1)cis-1,2-Dichloroethylene ug/kg34.2 5.0 40.0 4075-12585.5 6.23Tetrachloroethylene (PCE) ug/kg44.8 5.0 40.0 4075-125112 0.445Trichloroethylene (TCE) ug/kg36.6 5.0 40.0 4075-12591.5 1.10Vinyl chloride ug/kg39.8 5.0 40.0 4075-12599.5 8.19
ug/kg 100 80-120Surrogate: 4-Bromofluorobenzene 100100ug/kg 100 80-120Surrogate: Dibromofluoromethane 104104ug/kg 100 80-120Surrogate: Toluene-d8 102102
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
Date Received:
LABORATORY ANALYSIS RESULTS
Project Name:
Client:Project No:
AA Project No:
Date Reported:
PES Environmental, Inc.
KCOP241.060.02.014
A6062212/27/0512/29/05
Page 6 of 6
Special Notes: Surrogate recovery outside of control limits. The data was accepted based on valid recovery of the
remaining surrogate.= S-GC[1]
Eydie SchwartzProject Manager
American Analytics ü 9765 Eton Avenue, Chatsworth, California 91311Tel: (818) 998-5547 ü Fax: (818) 998-7258
ss
PES Environmental, Inc.
APPENDIX J
SOIL AND ASPHALT REMOVAL DOCUMENTATION
PES Environmental, Inc.
APPENDIX K
IMPORTED FILL AND ASPHALT DOCUMENTATION
PES Environmental, Inc.
24106002R007.doc
DISTRIBUTION
CORRECTIVE ACTION COMPLETION REPORT FORMER KCOP PRODUCTION STUDIOS
915 NORTH LA BREA AVENUE LOS ANGELES, CALIFORNIA
FEBRUARY 10, 2006
COPY NO. ____ Copy No. 1 Copy Ms. Thizar Tinut-Williams Los Angeles Regional Water Quality Control Board 1 320 West 4th Street, Suite 200 Los Angeles, California 90013-2343 2 Copies Mr. Ted Snyder La Brea Gateway, LLC 2 - 3 100 Wilshire Boulevard, Suite 1850 Santa Monica, California 90401 2 Copies Mr. Mathew Aleksich Bomel Management 4 - 5
8455 Beverly Boulevard, Suite 308 Los Angeles, California 90048 2 Copies Maria Hoye, Esq. Latham & Watkins 6 - 7 633 West Fifth Street, Suite 4000 Los Angeles, California 90071-2007 1 Copy David D. Cooke, Esq. Allen Matkins Leck Gamble & Mallory, LLC 8 Three Embarcadero Center, 12th Floor San Francisco, California 94111
3 Copies PES Files 9 - 11 1 Copy Unbound Original 12