august 9, 1988 - us environmental protection agency · hercules hercules incorporated hercules...
TRANSCRIPT
HERCULES Hercules IncorporatedHercules PlazaWilmington, Delaware 19894(302) '594-5000Telex: 83-5479
August 9, 1988
Kate Arthur (6H-EE)U . S . Environmental Protection AgencyRegion 61445 Ross AvenueDallas, Texas 75202-2733
RE: Vertac Off-site Areas - Fine Grid Sampling PlanJacksonville, Arkansas
Dear Kate:
Transmitted with this letter are copies of the "TCDD Final Data Report Sheet"and the "GC/MS/MS Worksheet Report Form" from final reports received to datefrom TMS Analytical Services for analyses for total TCDD . These data werepreviously sent to you after we received the data by FAX. These copies areprobably, in most cases, clearer and more easily read than some of copies ofthe FAX transmittals previously sent to you.
Sincerely,
Florence K. Kinoshita, P h . D .Senior Toxicologist
80764
TCDD FM. SA'P. F.EWT S»;ET
FILE RECH'/ES DATE;FiLE RECEIVES UK;
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. AKALY5DATE T
07/0&/BE07/06/8807/0&/BB07/(6/8B07/06/8B07/05/BB07/06/B807/C6/8807/06/8807/06/8807/06/8S07/06/8B07/06/8807/07/8807/07/BB07/07/BB07/07/8B07/07/8B07/07/8807/07/B8
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0.13*O.OS*1.121 . 1 00.iS<1.99l.:31.131.101.0E1.161 .141.091.030.94»I.OS1.04•14B»0.72t0.42«
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101.^1101,759E.B799.59
102.40103.0B
TOD m^ VALI3CD'tt. COCE CODE
0.300 •J •0.309 U0.84?0.6300.3CO L1
1.2521.67B1.4171.0771.162S.0241.4191.0090.963C.300-U0.7351.2660.300 U0.3CO U •0.300 U
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07/04/8807/04/8807/06/B607/04/BB07/(>4/8B07/04/B307/(l4/e807/04/ea07/06/ea07/04/8807/04/B907/Ot/BB07/oi/ea07/07/88&7/07/BB07/07/BB07/07/8807/07/BB()7/07/BB07/07/88
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ST I M E
1»231935194719592010202020312"432054210521152126213t104B105911111150120012191229
83
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5.005.005.005.005,025.074.975,114.984.924.935.014.904.935.285.105.065.114.924,84
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E ION 257T
i54329
S511329t494
491310841799828
1042i49946i7258387076
- 37B47127567794091481534958430t5
14826551193
: 1.0'"? TCt FACTOR;
!QII 259
5120IB91
134432B7405
721799887876379198990t?8672357525333218
11725576790178513339341409
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1.2:30.019
1CN 263
1413511426052512921450&611964010365373965"4650
!143"2B051S
10725632592
15S42215336512954789347637496274B
121237144516
SITE: HERCF"; 070'!DflTE: C7/09
ION 268 RIST10257/259
521065 0.13506751 0.05780961511247422138 0.68382198261523316390411493 .102842453''2712116593573479381051305548 0.942C.9661 1.05153621 1.04151212 148284092 0.72336440 (1.42
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65,1067,5476.7267.6167.9917.496i.9070.9466.0967.3268,4666.2565.7096.05
101.41101,7598.8799.59
102.40103.08
PAH U N I T SVftl'-IE
0.003 fiS/6110.011 N6.'6M0.845 f;6/BN0.830 N 6 / G B0.045 KS/8K1.252 N 6 / G H ,1.678 NS/SH^1.417 N5,'6K1.077 K8/6H1.162 >16'6M1.024 H5/M1.419 NS/Sl*'1.009 N6/6H0.°&.3 N6/6H0.233 »i5/6!1
0.735 N3/S11.266 liS'SH
-0.0:0 li5.'5fl0.031 %!W0.006 WIW
TCCB FINN. DATA RE?31iT SHEET
f!LE RECEIVE!) DATE:FILE RECEIVED 11HE:
SITE; HERCflSE; 0706DATE; 07/14/89
?P£fi 1
•ETHB-.ANK•aiLBLAm;QILSPire.3IL PE(014044054104114 i 2414<15«641342142442543043!436437443444
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HETHBLHKOCL9334OCL35723PE-B140114041405-1410141114121414H151416I41B14211424142514301431143t143714431444
ANALyS]DATE Tl
07/07/Bfl07/01/6807/07/B807/07/B807/07/6307/07/Ba07/07/8807/07/8807/07/8807/07/B807/07/8807/07/8607/07/8807/07/8807/07/5807/07/8807/07/8807/07/8807/07/8807/07/8807/07/8807/07/8807/07/88
IS NIBE
1451150|151215Z1153415451557li()71118!i2916401651170217131737174817581BCB181;18301842185319!)4
ATMiftTIO
0.3H1.00»1.0*1.020.50*1.27*0.72«1.0<1.02!.070.85*1.07
747»0.5'i»1.00*1.061.051.051.011.111.051.051.04
SUItROSfiTEftCC
102.6191.74
111.54104.M100.23?B.t3
102.8399.4999.14
100.03101.24101.3599.96
102.1691.00
100.8496.7089,7399.2699,8395.8093.0996.53
TCDD RESUNCONC. CODE
0.300 U0.300 U0.7834,0480.300 U0.300 U0.300 U0.300 U0.5690.4890.300 U0.3870.300 U0.300 U0.300 U0.300 U0,300 U0.8720.4750.300 U0.6320.6820.3:!5
W.IC UK1TSC38E
Nt/E"N5/6.1w/saN6/61N6/S1NG/9N
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}l.iaLIF[CBTION FLftBS:
» 257/259 RATI(] GUKISE nF WtEFTBBLE PSflBEn SURRC6<TE OUTSIDE Of BCCEFTfSBLE SSUBEm H!SH DETECTION LIMIT
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HE^BLNKOC1.34334OCL35723PE-B1401 -14C41405141814111412 -14141415l41iH1B142114241425143014311436143714431*»
RF IWTIVERF SURSOES
ftNALYSMTE
07/07/SB07/Ot/BB07/07/8807/07/8807/07/BS07/07/B?07/07/S807/07/8807/07/8807/07/6807/07/8B07/07/8B07/07/B807/07/8807/07/8807/07/8807/07/5807/07/B807/07/B807/07/8807/07/8307/07/8807/07/88
2.!0'TE 2.01
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.14511702171317371748175918C8181'?183(11S42IS^l'?"4
?33
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5.005.005,005,004.825.115.335.034.934,964.9'?5,254.8<?4.975.015.044.944.994.874.854,825,124.8')
IOX RATHCORRECT!
IDN 257
sasi
23441184358
3098303522017801
35715131359816
22440747
248232004531
12720759843444222213527003908437940
B: 1.0W 71ON FacToa;
ION 259
28421
22411183323
4145238230737517
3514112299114042(i954
1417032024240
12140721403t;3919924485343704335485
] 1.2330.010
ION 243
11707850337432919592489098
13023410508014527812144449441
1057B510154042598473534534B
144440 '200054147833147733144444152084
-. 975412009??
srCfl!ca"
IOH 24S
273807131482135433215299213244-314814245207350240293535118757250527
J39874150272158137172307391747496149393222354229352024'379584250452498731
tE: HERiE; 0794FE: 07/1.
RflTIO257/259
0.311,001.04l.(120.501.270.721.041.021.070.85I-".-747
0.591.001.041.051.051.011.111.091.051,06
4/B8
SURRACC
102.6191,74
111.54104.49100.2398.43
102.8399.4999.14
11)0.03101.24101.3599.94
102.!B91.00
100.8494.7089.7399.2499.8395.8093.0994.53
RAH UN!1VM.UE
0.009 KS/SH-0.023 M3/6H0.783 N6/6114.048 NS'SH0.083JtE.'6H0.017 X5/6110.024 11E/H1O.ftSO N6/6II0.549 N8/6X0.469 NS/6110.180 liB/SIl0.387 N6/6B
-t.Oii KS/SH•0.077 VSim0.045 US/SB0.030 118/5B0.097 XG/GH0,672 N5/5H0.47; K6/8H0.249 WW0.432 X6/8H0.482 N6'H»0.335 mw
TCDO FISP.L OfiTB REPORT SHEET
FILE RECEF I L E RECE
AREA »
<ETHELBSKSa iLBiaNKi O I L S P I f E3011. PE;41i1448i4521453>154!l55H5TH6014611462
NED IlfilE;!VEO r iKE;
C L I E N TSfllFLE »
NETHSLNr.')CL7433400.35590PE-A1446144S14521453145414551459144014&11462
ANALYS:BfiTE T
07/08/86e?/oB/6a07/08/B807,'08/Ba07/OB/Ba07/OB/B8-07/OB/B807/08/8807/OB/8807/08/88
•-07/08/3807/08/8807/08/8807/OB/88
!S IIRE
17081719173017441755180518151826183718481859191019201932
K f t T I V E SRfl7l0
0.')StO.OOl1,111.14C.OOto.omi.or -1.091.04i . i i0.00(0.57iO.i5t2.i0*
SIJFRDfiiSTEflCC
83.7071.2396.4883.2982.8982.7183.7379.1386.3484.6383.2387.0584.3982.24
TCDDCOM:.
0,300l).300H.8330,9110.3000.3000.3000.3000.3000.3000.3000.3000.3000.300
RESUN VfiLIBCODE CODE
Utj
UU^UUUUUUU
SITE; HERCSSE; 0708CflTE; 07/1?/S8
U N I T S
SG/5?1SS/5!1t<S ,'6'!siG/snNG/G"BB/SI!NG/GKOS/eftKB/GHNG'GHNB/EHN6/GHH5/6HKB-Ell
UXITS GF N5 PER SAHPLE
Ufl'.TS OF N6 FEP SanPLE .
aUf iLIFIMTIOfl FLBES;
» 257/259 BSTIO ODTSISE OF BCCEPTfiBLE RfiSEE»» suRF'aeaTE OUTSIDE DF accEF'iflaLE RANSE<»* H I G H CETECT10N LIB1T
RERUN CCDES;(i fiUTDIATiC RESUNS REQUESTED RESUN
MERCULeSINCORPO?,^rsu
RECEIVED
JUL 25 1988
MEDICAL DEPARTMENT
6C/,1S/"S HCKSHEET FEPORT FORM
;URPOSfiTE:NTEB!lftl
.AS^."FLE »
;UL0838.'ULOB39)liL084i)UJL0841;ijL0842;UL0843iUi-08441UL0845iUI.08443UL0847JULD843JULOB493UL0850JUL085!
tOUC 0.0ST!1 CONC 1
fiPEfl 1
KETHSLAaKSOllELAUKSO'LSPIKESOIL PE1444144B1452145314541455145? •144014S1 -1442
0
.05
CLIENTBAflFLE t
KETH8LNK00.34334OCL35590PE-fl144S144B1452145314541455145914401441IW
RF H A T I V E 2,10'RF SUSROEftTE 2.01
AtiflLYSISDA7E T I N E
07/08/38 170807/OB/S3 171907/08/83 173007/08/88 174407/08/83 175507/08/89 160507/08/88 1B1507/08/88 1B2407/08/88 183707/08/S3 1B4807/08/38 185907/08/BB 191007/08/B3 192007/OB/B8 1932
1B3
SA-WLE(SilOUNT
5.005.005.1505.005.04I . C O5,045.035.045,035.095.055.021.00
IGN Rf tTIO:COSSECTISH
ION 257
21541
45332IC'7299
1!
43371537711492'4091
!2278
9801823
1.009 11 Ff lCTCRi
!"!1 259
22011914
5904?94272
924771
41501404412040144BB
104539431504701
0 1,233O.C10
IOH 243
14242194733
1392181999741003.4030705713745483E41
. 87454B74796435B7832874514
234710
S1Cf
ION 248
444233319354344544572914290595890939393734252865
- 24323824751)21912292!5a80211877634B59
[TEi "ER'SE; 07')BSTE; 07/1S
RATIO257/259
0.980.001.111.140.000.001.031.091.041.110.000.570.452.60
/E8
SLIR9fIC!
83.7071.2394.4883.2992.89B2.7183.7379.1334.3484.4383.28B7.0584.3982.24
BflKV5LUE
-0.011-0.0090.833
-O.B11-0.015-0.1040.0520.252&.2150.248
-0.0090,0450.005
-0.075
!i«i!1
SS/B1116/6)1US/SBNS/BHKG/SHS8/EHSSfWwimSB/EHNS/GttXB/GHX6/EXIffi/GKNG/GH
TC5D FINAL OBI'S PEiWT SHEET
F I L E KECEF!LE PECS
fifEU t
KETHBLANtSO!LBIAH!!SOILSPIKESCI'L PE«m4t9tiHUEOKHUiiKH1467NH14':8MHU'i?HH1471KH1474NK1475HK1474KH1480KH1481NK14B2KK14B3KH1490KH1491»H14?2»HH93HH1494»H!<95
!V;t BS-E!!VEC r i R E ;
CLIESTSAKPLE »
BETHBLKK6CL?4373OCL35412PE-BMHK49NH!450NH14iiNH14i7K"!44BNH14t9HH1471KH1474BH1475BHi476MHKBONHI481NH1462N H S 4 B 3mm«H14»1NH149;WH1493XH1494NH1495
A.NHTSDaTE T;BE
07/13/Sa07/13/8807/13/aa07/13/6807/13,'8BC7/13/9BQ7/13/BB07/13/BB07,'13/SB07/13/BB07/13/BB07/13/Be07/13/6907/13/8807/13/8807/13/8807/13/8807/13/8807/13/8807/13'8807/13/8807/13/8807/13/8807/13/88
!S
07500801081:OS2408350848090409190934094810011011102110331043105311041114112412481341130813541328
SfiTH'ERATIO
l.OOtl.OOf1.121.141.051.091.131,161.181,06t.OOf1.111..15(1.52*O.t9*0.17«1.00*1.00*l.OO*l.OOt1.0<Hl.OOtl.OOt0.70t
BURRCSflTEftCC
80,89ii8.4080.4272.4070.B374.0275.1470.1874.7i77.2077.4976.1077.1777.6677.4978.6780.2978.5S77.74B8.3373.8789.9284.4178.11
-
TCDDCONC.
0.3000.3600.8060,7920.304a.m0.3000.3000.3000.3.000.3003.3090.3000.3000.3000.3000.3000.5000.3000,30f!0.3000.3000.3M0.300
REPUS VaL!DCOCE COGE
U1)
UUUUUU
1Lt)UUUU11UUUUU
UNITS
SB/6KNi /GMNB/EHHB/BHN6/BHNB/BHW/BBK B / E N»iS'B"!<B/BHKS/BMUS/ENN6/6HSS/BHIIS/Sfl1(S/6MNS/SHN6/811N6/6HN6/S11liS/6H»6/6KW/6HN6/SH
SUaLIFlCf lTION FtflfiS;
» ;57/;S9 RfiTID C"TS!tE OF (l[CEPTaSLE RfiNGEtt SURRDS^E OUTSSCE OF HCCEPTKLE RSN6E<" HIGH DETECTIOH l.I>tIT
RERU.*! CGDES;a fiUTD^Tic PERllKf. E^EiTEi) fiERliN
SITE; H£BCfiSE; 0712DBTE! 07'1B,'E8
CONNENTS
UNITS BF NB PER SBHPLE
6C/HS/NS IIIWEHEET REPORT FDRH
SUTOOGATEIKTEPHAL
LA8SAHPLE t
JUL1302JBL1303JUL13C4J"L13(i5JUL1306JUL1350;UL13(l7Ml 308JUL1309JUL1369JUL1310-JUL1311JUL1312JUL1313JUL1314JUL1315JUL1316JU11317JUL1318JUL1319JUL1324Jtii-1321JL"-1325Ji)Ll323
cone o.cSTD CDNC 1
AREA 1
KETHBLBNKSOILBLflNI;SOILSPIKESOIL PEBH1449BH1450WH1466NH1467KH1468KH1469«H1471IIHH74NH1475l(H147iHH1480NH1431UH14e2HH14B3NHH90M H U f lIIHK92.NH1493»H14T41(H1495
6.05
CLIENTSdKPLE 1
BETHBLNKOCL34373OCL35612PE-BNH1449NH1450NH1466NH1467HKi4'i8MH'469tiH1471HH1474NH1475MH1474rH14BONK!481NH1482BH14331(H1491)NH1491KH!4928H!(93HH1494NK1495
RF teTIVEfF EJRfl05B
ANaLYSMTE
07/13/8807/13/8B07/13'8807/13/6B07/13/BB07/!3,-'BB07/13/8807/13/3B07/13/8807/13/8807/13/aa07/13/B807/13./B807/13/BS07/13/SBC7/13/BB07/13/BS07/13/6B07/13/881)7/13/8807/13/8807/!3/3SC'7,'13'3307/!3'38
2.16TE 2.0
IST I K E
675008C1081308240835CB4fl090409! 90534094810011011102110331C431053110411'.4112412431341!3('B!3541328
183
SAMPLEAXOUNT
5.005.005,005.005.145.225.045.035.045,145 .29-5.255.22 .5.01;5.085.081.M5.065.275.185.245.035,155.0i
ION Rf t I IOCDRRECTIO
ION 257
11
548t225993191929877
20170947473148431
1159362
144981458
" 3302552
111111!
4089
! !,009 TO 1.233N FftCTDS; 0,010
ION 259 ION 2S3
1 462401 56923
49039 10014422877 4314318345 781729044 45i2i
17905 91702815(i 63795(il9i 4&1417790 61:51
1 56159143536 6B554
12320 1274642027 695844780 B42493344 6B752
1 219505B6(i 111123
954152724246933593373(983!6327
SICADA
Iffll 268
137196199725297090142146264169147595292211217824147B74190140173939205371395907215007260815209727285217
B32001443381612241136794357962413
342B32
T E i HERSE; 0712TE; 07/
RATIO257/25
1.001.001.121.141.05!.fi91.131.161.181.6B1.001.111.150.520.690.171.001.00I.CO1.001.001.001.00C.70
8/BB
SUffl9 ACC
80.8968.4080.4272.4070.8374,6275.1470.1874.7677.20
J7.4978.1077.1777,6677.4978.6780.2978.5877.7488.3373.8789.9284.4178.11
Rfilt IIKITSVALUE
-0.023 N6/6(1 ,-0.023 N6/6K"0.8S6 N6/El0.792 N5/eP0.304 K6/6H0.269 HS/6M0.2B4 NE/eMO.li-3 HB/S110.192 NS/EM0.175 KB/BH
-0.022 KB/BI3,309 N6;BHO.lii N E / G MO.(i24 NS/EH0.050 !i5/6H0.02'. NE.'SB
-0.114 »i5'6H-0,!);'? WIW-0.022 W]'St-<1.622 N G / B H-0,d22 f(G/6K-?,023 NE/SH-O.C22 N B / E K0.045 WW
TCDO F1SA1. OATH REPORT SHEET
;LE R£C£:LE RECE
^ a »
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