bear. mr - epawebapp.epa.ie

Bear. Mr Wallace,

Please find enclosed rnnn thl y air rnunitoring results for the month of October 21118. All paramtltcrs am within the license limits.

If you havc any cpries in relation to the information cuntaii-ted within these ruports yIca~c do not hesitate tu contact me 01.1 061 707403.

Yc-turs sincerely,

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EPA Export 31-12-2018:03:43:52

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EPA Export 31-12-2018:03:43:52

Document No.: ENSHft1091018 / 2018605 Visit No: 10 Year: 2018 Office: Trim

EPA licence No.: WlOO41-01 Licence Holder: Enva Shannon, X2

Facility location; Smithstown Facility Rev.No: 1.

Stack Testing Team Report Date

Repm Type

- ..,.., , , ,

'Test Report Compliance Monitoring

Page 1, of 30

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EPA Export 31-12-2018:03:43:52

Document No . . ENSHT11091UlX / 2018605 Visit No: 10 Year: 2018 Office: Trim

EPA Licence No . . WLOO4.1-01 Llcen~e Holder; Enva Shannon. X2

Facility Location: %IithstOWR Facility Rev.No: x

Cosit1tepeb 1 . Executive Summary ............................................................................................................................

Overall Aim of the monitoring Campaign ....................................................................................... 5pecial Requirements ........................................................................................................................ Tarpt Parameters .............................................................................................................................. Emission Limit Values ........................................................................................................................ Reference Conditions ........................................................................................................................ Overall Results .................................................................................................................................... Accrditation detail5 .......................................................................................................................... Monitoring Dates & Times ................................................................................................................

Sampling Deviations ........................................................................................................................... Reference Documents ........................................................................................................................ Suitability of sampling location ......................................................................................................... Process details ..................................................................................................................................... Stack diagram ......................................................................................................................................

2. APPENDiCEZ ......................................................................................................................................... Appendix i - Monitoring Personnel & Equipment

Stack Emissions Monitoring Personnel ............................................................................................ Appendix II - Stack Details &flow characteristics ........................................................................

Preliminary stack survey calculations .............................................................................................. Appendix Ill - individual parameter sampling details and results .............................................

H yd rogc n Chloride 4a rnpling Det a i I5 8 Resu It5 ..............................................................................

...................................................................................................................... I . Monitoring Objectives

Monitoring, Equipment & Analytical Methods ...............................................................................

........................................................................ tl .

111 .

IV.

Hydrogen C hlarfde Quality Assurance ............................................................................................. Hydrogen Chloride Results & Measurement Uncertainty ............................................................

Ammonia Sampling Details & Results ........................................................................................... Arnmania Quatity Assurance ..........................................................................................................

T A I.uft Orgstllcs ................................................................................................................................

Ammonia Results & Measurement Uncertainty .........................................................................

3 3 3 3 3 4 4 5 6 7 8 9 11 11 12 IS 14 14 14 15 15 23 23 24 25 26 28 29 30

Page 2 of 30

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EPA Export 31-12-2018:03:43:52

Document NO.: EN5HTL1091018 / 2018605 Visit: No: 10 Year: 2028 Office; Trim

EPA ticcnce NO.; WLOO41-01 licance Molder: Enva Shannon, X2

Facility Location: Srnixhstown Facltity Rev.No: 1

Overall Aim of the monitoring Campaign The aim of the rnnbnltbrlm campaign was to demonstrate compliance wtlh a set of emlssim limit values as specified in ihe site licance.

Spaclal Raquimments Thew were no special requirements.

Target Parameters

T A Luft Organics

Page 3 of 30

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EPA Export 31-12-2018:03:43:52

hcurnent No.: ENSHTL1091028 / 2018605 Visit No; 10 Year: 2018 Office: Trim

Emission Limit Values

EPA Licence No.: WLU041-0l. Licence klotder: Enva Shannon, XZ

Facility Lacation: 5rnith5town Facility Rev.No: 1

Stack Gas Temperature

Volume Irn3.tt-')

Rofermcrt Conrlitlons

Oxygen Reloronco % No Oxygen Ref

Total Pressura kPa 101.3

Page 4 of 30

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EPA Export 31-12-2018:03:43:52

Accredltatlon dgtBll$ ----- Air Scicnlllc Limilad

Paee 5 of 30

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EPA Export 31-12-2018:03:43:52

Document No.: EN5HTll09101& / 2018605 Visit No: 10 Year: 2018 OHicc: Trim

Eracuttue Summary

Monitoring Data$ & Tlmes

EPA ticenct; No.: WLOO41-01 Licence Holder: Enva Shannon, X2

Facility Location: Smithstown Facility Rev.No: 1

09/2012018 13:20:00 Stack EA$ Tamperalure

- , , , ,, ,, , , , , ,

I

Page 6 of 30

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EPA Export 31-12-2018:03:43:52

of 30

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EPA Export 31-12-2018:03:43:52

Document No.; ENSHTLlO9ZOl& / 2028605 Wit No: 1.0 Year: 2018 Qfflcc: Trim

Sampling Deviations

EPA LiccnCC No.: WLO(341-01 Licence Holder: Enva Shannon, X2

Facility Location: Smithstown facility Rav.No: 1

Page 9 of 30

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EPA Export 31-12-2018:03:43:52

Document No.: ENSHTL1091018 / 2018605 Visit No: 10 Year: 2018 Office: Trim

€FA Licence No.: WlC)041-01 Licence Molder: Envzl Shannon, X2


Safe Access Avaltabto

Process dotails

Parameter . , . . . , . , , , , , , . . , , , , ,

proOceI;1 Statu$ Normal - . . . . . . . , , , , , . . . . . . , , , . , U

Caprrctry (psrlhour] (If applkablo) NIA - . . , . , . , . . . , . . , , . ',,,,--

Continuous or Batch Process Continuous Process Air

Abatement System Ye9

Abatement Syrtems Runtrlng Status Normal -- , , , , . , .. , , , .. ,, , - NIA

None

Page 10 of 313

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EPA Export 31-12-2018:03:43:52

Document No.: ENSHTt1091018 / 2013605 Vtsit No: 10 Year: 2018 Office: Trim

EPA licence No.: WLDO4l-t)l Licence Holder: Enva Shannon, X2


Page 11 of 30

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EPA Export 31-12-2018:03:43:52

Documant No.; ENSHTL1091018 I’ 2018605 Visit No: 10 Year: 21318 Office: Trim

Exocutlvo Summary

Stack diagram

EPA Licence Nu.: WLDO41-03. Licence Holder; Enva Shannon, X2


Page 12 of 30

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EPA Export 31-12-2018:03:43:52

Docurnent No.: ENSHTL1091018 / 20186fJ5 Visit No: 10 Year: 2018 Office: Trim

EPA Licence No.: WLI3041-01 licence Holder: Enva Shannon, X2

Facility Location: Smithstown Facility Rev,Na: 1

2. APPENDICES

Stack Emissions Monitoring Personnel

Page 13 of 30

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EPA Export 31-12-2018:03:43:52

Document No.: ENSMTL1091018 / 2018605 Visit No: 10 Year: 2018 Office: Trim

EPA Licence No.: WLOO414X Licence Holder: Enva Shannon, XZ

Facility location: Smithstown Facility Rev,No: Z

Page 14 of 30

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EPA Export 31-12-2018:03:43:52

€PA LiCerltl No.; WLOO41-01 I.Icenr;e tialder: Ei'lre Shannon. %2

Facility Locatlon: Smithstown Fdcility ileu.No: 1

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EPA Export 31-12-2018:03:43:52

.""" -1-

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EPA Export 31-12-2018:03:43:52

EPA k.ictnc.I: NO.: w~0041-UZ I.ic;ence Holder: Enva Shannon, X2

Facility Location; Smithatown Facility Rov.NO: 1

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EPA Export 31-12-2018:03:43:52

Document No,; EN5HTL1091018 / 201&605 Visit No: 10 Year: 2018 Office: Trim

-. . . . . . . . . Imphger 3 ID X 2 HCL 3 142 -

Timo an 1405

Time off 1435 _I__ pp

I

Leak Cheek Results _______I_ ...........____._.______,. . . . . . ~ . . . . . . . . . .

Prior to le$!: . . . . . . . . 0.01 I/mtn -. . . . . . . . . . . . . . . . . . . . . ~ -.. -

EPA L~XIIO? NO.: WL(3041-01 l icence Holder: Enva Shannon, X2

Facility Lncatlon: Smithstown Facility Rev.No: 1

~~

Actual Sample Valumc: 0.054 ma NarmaIl$ed Gas Volume. 0.054 Nm3

-__________.I

Page TI of 30

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EPA Export 31-12-2018:03:43:52

Document; No.: ENSWTFl091018 / 2018605 Visit MO: 10 Year; 2018 Office: Trim

EPA Licencc NO.: WLOO41-03. Licence Holder: Enva Shannon, X2

Facility Location; S r n k R ~ t ~ w n Facility Rev.No: 1

Hydrogen Chloride Quality Assurance

- Le& test nrcrlte Units Run -I Run 2 Run 3 - .,, . . . . ' " " ' " ' " ~ ~ ~ ~ . , , . . , , , . . ~ ~ . ' " ~ ~ ~ ~ " ~ ~ ' ~

Mean Sampling Rate Vmin 1.a

llmin

7

Max. Fllter Temp

Page 22 of 30

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EPA Export 31-12-2018:03:43:52

Document. No.: EN5HTL1091018 / 20186135 Visit No: 10 Year: 2018 Office: Trim

EPA Licence No.: WLOO41-01 Licence Holder: Enva Shannon, X2


Start time 14;05

Flnlsh Tlme 14:35 -....,.....,,,., ... ,

412 ftll lmpinger final Volume

Factor -.,. . , , . --

I 0.76 Erpantled uncertainty in units of maasurement

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EPA Export 31-12-2018:03:43:52

Document No.: ENSHTL1.09X03.8 / 2018605 Visit No: 10 Year: 2018 Office: Trim

Client; Enva Shannon 1 3 3 5 -,, . . . . . . . . . . . . . .

Log Sheet Complele by: John Casey 14:M Test oats: D9/1 Ol2018

Laboratory Used; UKASl549 .Cwtlflcate Numbors: 776020

--,, , , , , , , , , , ,

___. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . -- - .".... . . . . . . . . . . . . . . . . . -

Tube

PhW Qn pp

Tima off

. . . . . . . . . . . . -

EPA Fi~encfi NO.: WL00414I1 FicIencc Holder; Enva Shannon, X2


. . . . .

Tltlo: Dewrninatian of Speclated Organtc Compounds

- pp

POL[ TQR: 0.001 Vrnh Sample vollrrno Flow Rare: 0.42 llrnin

Standard Requirement: e2 Qh --, . . . . . . . . . . . . . . . . . . . . . . . . . ,,,PP

Test Status

. . . . . . . . . . . . . . . . . . . . . . . Callbration Rate Beforc Test:

Calibration Rate After Test; 0.42 litres per minute

Average sample Valuma: 0.42 litres per mlnuto

Sample Test "rime: 31 minutes

- . . . . . . . . . . . . . . . . . .

-,, ,, , . , . -- ---, . . . . . . . . . . . . . . . ,.,...

-PPI.

Pump Gas Temperature; 14 OC burno Sarnnle ~rassure: I 100.3 7 kPa f I

__I_ pp

0.03 302 I . . . . . . . . . . 0.01226 Normalised Gas VoIuma-

- . , . ,

Page 24 of 30

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EPA Export 31-12-2018:03:43:52

Document No.: ENSHTLlU91018 / 2018605 Visit No: 10 Year: 2018 Office: Trim

EPA Licence No.: WL0041-01 Licence Holder; Enva Shannon, X2

Facilltv Location: Smithstown Facility Rev.No: 1

Stack Flaw Rater

Diameter. 0.26 rn . . . . . . .

Averago V@locliy~ 8 27 m/s . . . . . . . . . . . . .

Averago Prsssere’ 100 3 .................... kP3 ACtubi Flow Rate 1582 m3/Hr

Normalmd Flow Rate Nm31Hr

. . . . . . . . . . . . . . . . . . . . . . . . . . - ”..”............. . . . . . . . . . . . . . . . . ............. ~ -

-, ......- Average Temperature 14 . . . . . . . . . . . . . . . . QC ......- - l_____ -... ~

-. . . . . . . . . . . . . . . . . . . . ~ ~. . . . . . . . . . . . . . . .

-

-

- ..... . . . . . . . . . . . . . . . . Total

% of measured value -,,..,. . . . . . . . . . . . . . . . .

. . . . . . . . . . Exparlded uncedainty in units mg.rn” 0.16 0.33

- Expanded uncertainty as percantage of limit vahe % Of ELV

............,,. . . . . . . . . . . . . . . . . .

Page 25 of 30

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EPA Export 31-12-2018:03:43:52

Document. No.: ENSHTllOSlOlX / 2018605 Visit No: 10 Year: 2018 Office: Trim

€FA Licence No.: WLO041-01 Licence Holder: Enva Shannon, X2

Facility Location: Smithstown Facility Rev.hlo: 1

Page 26 of 30

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EPA Export 31-12-2018:03:43:52

Document No.: ENSMT1109181& / 2018605 Visit No: IO Year: 2018 OfficEt: Trim

Actual Sample Volume; - . , . . , . , , . , , , , , , , , , , , , . . . , , , , . . . , . , , . . . . , . . , . , .

Normalised Gas V O ~ U ~ Q :

EPA licence No.: Wl0041-01 Licence Holder: Enva Shannon, X2

Facility location: Smithstawn Facility Rev.No: 1

0.057 m3 ,,--______

0.057 NIT?

Ammonia Sampling Details L Results

Samalu ID XZ NH3 1+2

Test Reault

Test Status

Pump Number

Calibration Unit

Cslibrztllorl Rate M W f ? 're61

Catibration Raie M e r Tevi Avorage samplo Votuine: 1.9

Sample Test Time; 30 Pump Gas Temperature: 0

101 3

Page 27 of 30

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EPA Export 31-12-2018:03:43:52

Documant No.: ENSHTLIOSlQlX / 2131.86135 Visit No: 10 Year: 2018 Office: Trim

EPA Licence NO.; WEOQ41-OI Licence Holder: Enva Shannon, X2

Facility I.cscation: Smithstown Facility Rev.No: 1

-- Total m p l + ~rnp z + imp 3

Impinger 3 - -

14

Absorption eflicioncv U 79 , , , , , , ,,I$,, , , , , , , , , , , , , , , , , , , , ,, , , , , , , , , , , , ,, , , , , , , , , , ' , , , , , , , , , , , , , , , , ,,, ,,,,,, , , , , , , , , , , ,:,, , , ,,,- - ..,,. , , . . . . , . . , , , . . . , . . , , , , . , , ,- , , . .., ,. ,,. ,. , .. . , ,

I Ellank samala IO 1 I I

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EPA Export 31-12-2018:03:43:52

EPA l icence No.: WLOO41-01 licence Holder: Enva Shannon, X2

Facility location : Sm it hstown Facility Rev.Na; 1

Ammonia R ~ ~ l t s & Maasurrrnant Uncertahty

~7 Stack ID x2

1 Emissions Concentration 1 1.16 I mum'' I I 1 Mass Emissions 0.002

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EPA Export 31-12-2018:03:43:52

Document No.: ENSHTLlO9101i3 / 2018605 Visit No: 10 Year: 2018 Office: Trim

EPA Licence No.: WL0041-01 Licence Holder: Enva Shannon, X2

Facility Lucation: Smithstown Facility Rev.No: 1

Parameter 4 Run 4

Camblnad Uncertajnty mg m.3 1.159 -- 200 18

2 $I8

f 73

Expanded uncertainty 8s percentage of measured value W of rneaaured value

Expanded uncertainty tn units of mg rn-' memurement Expanded uncertainty as percentage of limit

vabe

~ ~~ ~ II

-- _I

9b Of

Expanded uncertainty in units of measurement , , , , , , , .:,. , , , ,,, ,, , , ,,,, ~

n1g.m"

YV ELV

Page 30 of 30

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EPA Export 31-12-2018:03:43:52

concept Life Sciences Certificate of Analysis

Hadfield House Hadfield Street

Cornbrook Mrtncheeler

M1% DFE Tal ! 0161 8'14 24UO

Fax : 0161 874 2404

Report Numfslar: 775020-1

Date of Report: 30-Oct-2018

Customer: Air Scientific Unit 32 Dqjranvilla Court Dublin Road Trim Co. Meath Iruland.

Customer Contact: Project Management

Customer Job Reference: ENSHTLIOSI 01 8

Date Analysis Started: 18-Oct-2018 Date Analysis Completed: 24-Oct-2018

DaG Job R@CaiVod at C ~ n c ~ p t : 16-Oct-2018

The results reported relate to sarnplas received in the laboratory and may not be representative of a whale batch. Opinions and interpretations expressed herein are outside the scopm of UKAS accreditation This report should not be reproduced except in full without the written approval of the faboratoiy Tests covered by this certificate were conducted in accordance with Concept LifB Sciences SOPS AI1 results have been reviewed in accordance with Section 25 of the Concept Life Sciences, Analytical Services Quality Manual

4 549

Report chtxked and authorised by : Rachel Traynier Deputy Laboratory Managar

Issued by : Kathryn Gleaves Customer Service Advisor

PagEJ 1 o f 2

77 5020-1 This documen! has bean printod from a digifslly signed master copy

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EPA Export 31-12-2018:03:43:52

t

index ta symbols used in 7750204

Produced by Concept Life Sciences. Hadfiatd House, Hadfjald Street, Cornbrook. Manchester, M16 9FE

Thls document has been printed from a digitally slgned master copy

Page 2 of 2

775020-2

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EPA Export 31-12-2018:03:43:52