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Calibration of Industry-Standard LNG Flow Meters Under Ambientand Cryogenic Test Conditions
Menne Schakel (VSL) & Asaad Kenbar (NEL)
LNGIII training, 29 May 2020
Two papers available
16-6-2020 LNGIII training 2
VSL website:
https://www.vsl.nl/sites/default/files/rtf/Liquid%20nitroge
n%20calibrations%20of%20industry-
standard%20LNG%20flow%20meters%20used%20in%
20LNG%20custody%20transfer_public.pdf
NEL website:
LNG metrology website:
https://lngmetrology.info/2020/01/Kenbar & Schakel, draft journal publication, 2020
Schakel, 2019, VSL website
Assessment of LNG flow meter measurement uncertainty
16-6-2020 LNGIII training 3
▪ Investigate the onsite flow measurement uncertainty for small and mid-
scale LNG applications. Is LNG flow measurement uncertainty of 0.50%
(k = 2) met in practice?
▪ Effect of typical upstream flow disturbances on LNG flow measurement
uncertainty
▪ Effect of meter insulation on LNG flow measurement uncertainty
▪ Assess transferability of meter calibrations with water at ambient
conditions to cryogenic conditions
Test protocol - first step: water calibrations
16-6-2020 LNGIII training 4
Not displayed
Double bends
NEL’s Water Flow Measurement Facility
From Kenbar & Schakel, draft journal publication, 2020
Test protocol: typical flow disturbances
16-6-2020 LNGIII training 5
Moderate
From Kenbar & Schakel, draft journal publication, 2020
Severe
Test protocol: typical flow disturbances
16-6-2020 LNGIII training 6
From Kenbar & Schakel, draft journal publication, 2020
Test protocol
16-6-2020 LNGIII training 7
▪ I. Ideal setup: no flow disturbance, no insulation
▪ II. As setup I, but with partially blocking plate
▪ III. As setup I, but with double-bend disturbance
From Kenbar & Schakel, draft journal publication, 2020
Test protocol
16-6-2020 LNGIII training 8
▪ 2” and 4”
▪ A total of 6 meters LNG flow calibrated and tested
▪ 3 flow geometries tested
▪ Ambient and cryogenic flow conditions
▪ With and without meter insulation
• Panametrics a
Baker Hughes
company
• Emerson
• Endress + Hauser
• KROHNE
• Yokogawa
Test protocol - second step: cryogenic calibrations
16-6-2020 LNGIII training 9
VSL Cryogenic Research and Calibration Facility
2” metering line with double bends (1) installed and
rockwool (2)
From Schakel, 2019, VSL website
From Kenbar & Schakel, draft journal publication, 2020
Exactly the same metering lines
in cryogenic calibrations as
used in the water calibrations
Systematic assessment of LNG flow meter uncertainty
16-6-2020 LNGIII training 10
▪ I. Ideal setup: no flow disturbance and all meters are insulated
▪ II. As setup I, but with partially blocking plate
▪ III. As setup I, but with double-bend disturbance
▪ IV. As setup I, but with flow meter insulation removed
From Kenbar & Schakel, draft journal publication, 2020
Water and cryogenic calibration results
16-6-2020 LNGIII training 11
-1.0
-0.8
-0.6
-0.4
-0.2
0.0
0.2
0.4
0.6
0.8
1.0
0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0
Err
or
[%]
Mass Flow Rate [kg/s]
Water Flow TestsMeter 1
Ideal, 20 deg. C
Ideal, 36 deg. C
Partial blockage, 20 deg. C
Double-bend, 20 deg. C
-3.0
-2.5
-2.0
-1.5
-1.0
-0.5
0.0
0.5
1.0
1.5
2.0
2.5
3.0
0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0
Err
or
[%]
Mass Flow Rate [kg/s]
Liquid Nitrogen Flow TestsMeter 1
Ideal
Ideal-repeat
Partial blockage
Double-bend
Un-insulated
Nominal
Rate
(kg/s) Ideal, 20 °C
1 -0.018
2 -0.010
3 0.048
4 0.044
5 0.017
6 0.004
7 -0.013
8.5 -0.018
Nominal
Rate
(kg/s) Ideal
2 -0.19
4 -0.10
6 -0.07
8 0.00
10 -0.04
From Kenbar & Schakel, draft journal publication, 2020 From Schakel (2019) & Kenbar and Schakel, draft journal publication (2020)
Water and cryogenic calibration results
16-6-2020 LNGIII training 12
-1.0
-0.8
-0.6
-0.4
-0.2
0.0
0.2
0.4
0.6
0.8
1.0
0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0
Err
or
[%]
Mass Flow Rate [kg/s]
Water Flow TestsMeter 6
Ideal, 20 deg. C
Ideal, 36 deg. C
Partial blockage, 20 deg. C
Double-bend, 20 deg. C
Nominal
Rate
(kg/s) Ideal, 20 °C
1 -0.026
2 -0.020
3 0.036
4 0.036
5 0.016
6 0.007
7 -0.006
8.5 -0.010
Nominal
Rate
(kg/s) Ideal
2 0.26
4 0.44
6 0.52
8 0.60
10 0.59
From Kenbar & Schakel, draft journal publication, 2020
From Schakel (2019) & Kenbar and Schakel, draft journal publication (2020)
Water and cryogenic calibration results
16-6-2020 LNGIII training 13
-1.0
-0.8
-0.6
-0.4
-0.2
0.0
0.2
0.4
0.6
0.8
1.0
0.0 5.0 10.0 15.0 20.0 25.0 30.0
Err
or
[%]
Mass Flow Rate [kg/s]
Water Flow Tests
Meter 0
Ideal, 20 deg. C
Ideal, 36 deg. C
Partial blockage, 20 deg. C
Double-bend, 20 deg. C
-3.0
-2.5
-2.0
-1.5
-1.0
-0.5
0.0
0.5
1.0
1.5
2.0
2.5
3.0
0 5 10 15 20
Err
or
[%]
Mass Flow Rate [kg/s]
Liquid Nitrogen Flow TestsMeter 0
Ideal
Ideal-repeat
Partial blockage
Double-bend
Un-insulated
Nominal
Rate
(kg/s) Ideal, 20 °C
7 -0.041
16 -0.017
25 -0.018
35 -0.012
Nominal
Rate
(kg/s) Ideal
4 -0.07
8 0.02
12
16 0.13
20 0.10
From Kenbar & Schakel, draft journal publication, 2020 From Schakel (2019) & Kenbar and Schakel, draft journal publication (2020)
Water and cryogenic calibration results
16-6-2020 LNGIII training 14
-1.0
-0.8
-0.6
-0.4
-0.2
0.0
0.2
0.4
0.6
0.8
1.0
0.0 5.0 10.0 15.0 20.0 25.0 30.0
Err
or
[%]
Mass Flow Rate [kg/s]
Water Flow Tests
Meter 3
Ideal, 20 deg. C
Ideal, 36 deg. C
Partial blockage, 20 deg. C
Double-bend, 20 deg. C
-3.0
-2.5
-2.0
-1.5
-1.0
-0.5
0.0
0.5
1.0
1.5
2.0
2.5
3.0
0 5 10 15 20
Err
or
[%]
Mass Flow Rate [kg/s]
Liquid Nitrogen Flow TestsMeter 3
Ideal
Ideal-repeat
Partial blockage
Double-bend
Un-insulated
Nominal
Rate
(kg/s)
Ideal,
20 °C
7 -0.107
12 -0.115
17 -0.123
22 -0.145
28 -0.137
Nominal
Rate
(kg/s) Ideal
4 -0.21
8 -0.20
12 -0.12
16 -0.12
20
From Kenbar & Schakel, draft journal publication, 2020 From Schakel (2019) & Kenbar and Schakel, draft journal publication (2020)
Water and cryogenic calibration results
16-6-2020 LNGIII training 15
-1.0
-0.8
-0.6
-0.4
-0.2
0.0
0.2
0.4
0.6
0.8
1.0
0.0 5.0 10.0 15.0 20.0 25.0 30.0
Err
or
[%]
Mass Flow Rate [kg/s]
Water Flow Tests
Meter 4
Ideal, 20 deg. C
Ideal, 36 deg. C
Partial blockage, 20 deg. C
Double-bend, 20 deg. C
-3.0
-2.5
-2.0
-1.5
-1.0
-0.5
0.0
0.5
1.0
1.5
2.0
2.5
3.0
0 5 10 15 20
Err
or
[%]
Mass Flow Rate [kg/s]
Liquid Nitrogen Flow TestsMeter 4
Ideal
Ideal-repeat
Partial blockage
Double-bend
Un-insulated
Nominal
Rate
(kg/s)
Ideal,
20 °C
7 -0.155
12 -0.148
17 -0.118
22 -0.111
28 -0.135
Nominal
Rate
(kg/s) Ideal
4 0.67
8 0.43
12 0.38
16 0.27
20
From Kenbar & Schakel, draft journal publication, 2020 From Schakel (2019) & Kenbar and Schakel, draft journal publication (2020)
Water and cryogenic calibration results
16-6-2020 LNGIII training 16
-1.0
-0.8
-0.6
-0.4
-0.2
0.0
0.2
0.4
0.6
0.8
1.0
0.0 5.0 10.0 15.0 20.0 25.0 30.0
Err
or
[%]
Mass Flow Rate [kg/s]
Water Flow Tests
Meter 8
Ideal, 36 deg. C
Partial blockage, 20 deg. C
Double-bend, 20 deg. C
-3.0
-2.5
-2.0
-1.5
-1.0
-0.5
0.0
0.5
1.0
1.5
2.0
2.5
3.0
0 5 10 15 20
Err
or
[%]
Mass Flow Rate [kg/s]
Liquid Nitrogen Flow TestsMeter 8
Ideal
Partial blockage
Double-bend
Un-insulated
Nominal
Rate
(kg/s)
Ideal,
36 °C
7 0.204
16 0.021
25 -0.035
Nominal
Rate
(kg/s) Ideal
4 0.29
8 -0.25
12
16 -0.22
20 -0.22
From Kenbar & Schakel, draft journal publication, 2020From Schakel (2019) & Kenbar and Schakel, draft journal publication (2020)
Cryogenic flow stability
16-6-2020 LNGIII training 17
▪ Target per batch:
− 0.2 bar/minute
− 0.2 °C/minute
− Flow rate variability: 1% - 2%
▪ Achieved:
− Pressure_std < 0.03 bar for 120
s – 130 s batch
− Temperature_std < 0.10 °C for
120 s – 130 s batch
− Flow rate: ±1.5% for 2” line
− Flow rate: ±0.5% for 4” line
Conclusions
16-6-2020 LNGIII training 18
▪ Investigate the onsite flow measurement uncertainty for small and mid-
scale LNG applications. Is LNG flow measurement uncertainty of 0.50%
(k = 2) met in practice?
− Provisional LIN calibration uncertainty at 0.30% in mass flow rate:
Schakel, 2019
Conclusions
16-6-2020 LNGIII training 19
▪ Investigate the onsite flow measurement uncertainty for small and mid-
scale LNG applications. Is LNG flow measurement uncertainty of 0.50%
(k = 2) met in practice?
− For 85% of the LIN calibrations, total measurement uncertainty was < 0.50%:
“Taking into consideration the maximum combined measurement uncertainty of the cryogenic
facility of 0.30% (k = 2) the target measurement uncertainty of 0.50% (k= 2) can be achieved
provided that the standard error of the mean value, computed from the individual calibration
points per set flow rate, is smaller than 0.40%”
From Kenbar & Schakel, draft journal publication, 2020
Conclusions
16-6-2020 LNGIII training 20
▪ Effect of typical upstream flow disturbances on LNG flow measurement
uncertainty
− Effect of 20D upstream flow disturbances investigated generally smaller than
±0.50% meter error
“…it can be said that meter errors within ±0.50% can be achieved for the cryogenic testing
with LIN at approximately -180 °C, even with the presence of the disturbances tested in this
work and no additional flow conditioning devices installed, in particular, for ultrasonic meters.
This also means that the influence of these flow disturbances on meter error is limited (i.e.,
contribution to meter error below ±0.50%), however it should be remembered that these
disturbances are followed by straight piping equivalent to 20 pipe diameters.”From Kenbar & Schakel, draft journal publication, 2020
Conclusions
16-6-2020 LNGIII training 21
▪ Effect of meter insulation on LNG flow measurement uncertainty
− Effect of insulation on measurement accuracy can be significant i.e. error >
±0.50%
− “The results show that the effect of removing the meter insulation on measurement accuracy
can be significant (i.e. error > |±0.50%|). The difference in the meter error between the
insulated and un-insulated cases varied between a minimum value of -0.01% and a maximum
value of 1.04%. Therefore, meter insulation is recommended when used in cryogenic service.”
From Kenbar & Schakel, draft journal publication, 2020
Conclusions
16-6-2020 LNGIII training 22
▪ Assess transferability of meter calibrations with water at ambient
conditions to cryogenic conditions
− “The results indicate that the corrections used to transfer the water
calibration to LIN conditions resulted in meter errors, for the ideal case,
within ±0.50% for about 85% of the results.”From Kenbar & Schakel, draft journal publication, 2020
Conclusions – important note
16-6-2020 LNGIII training 23
“The results presented in this paper cannot be extrapolated, with meaningfully low uncertainty, to flow
meters of different type, size, model and make (manufacturer) than those tested..”
From Kenbar & Schakel, draft journal publication, 2020
Conclusions – last remarks
16-6-2020 LNGIII training 24
▪ Other effects planned to investigate:
− Thermal insulation
− Multi-phase flow
− Meter inclination
− Coriolis meter response time
▪ More meters were included than originally planned
Acknowledgment
28/5/2020 LNGIII workshop 25
The participation and support received from the LNG flow meter
manufacturers is highly appreciated!
Thanks to:
▪Panametrics a Baker Hughes company,
▪Emerson,
▪Endress + Hauser,
▪KROHNE, and
▪Yokogawa