catalytic reforming-design and operation of nht strippers
TRANSCRIPT
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8/10/2019 Catalytic Reforming-Design and Operation of Nht Strippers
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Refinery Process Stream Purification Refinery Process Catalysts Troubleshooting Refinery Process Catalyst Start-Up / ShutdownActivation Reduction In-situ Ex-situ Sulfiding Specializing in Refinery Process Catalyst Performance Evaluation Heat & MassBalance Analysis Catalyst Remaining Life Determination Catalyst Deactivation Assessment Catalyst PerformanceCharacterization Refining & Gas Processing & Petrochemical Industries Catalysts / Process Technology - Hydrogen Catalysts /Process Technology Ammonia Catalyst Process Technology - Methanol Catalysts / process Technology PetrochemicalsSpecializing in the Development & Commercialization of New Technologyin the Refining & Petrochemical Industries
Web Site: www.GBHEnterprises.com
GBHE Technical Bulletin CTB #55
Catalytic Reforming
Design and Operation of NHT StrippersTo Protect Catalytic Reformers
Information contained in this publication or as otherwise supplied to Users is believed tobe accurate and correct at time of going to press, and is given in good faith, but it i s forthe User to satisfy itself of the suitability of the information for its own particular purpose.GBHE gives no warranty as to the fitness of this information for any particular purposeand any impl ied warranty or condit ion (statutory or otherwise) is excluded except to theextent that exclusion is p revented by law. GBHE accepts no liabilit y resulting from relianceon this i nformation. Freedom under Patent, Copyright and Designs cannot be assumed.
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8/10/2019 Catalytic Reforming-Design and Operation of Nht Strippers
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Refinery Process Stream Purification Refinery Process Catalysts Troubleshooting Refinery Process Catalyst Start-Up / ShutdownActivation Reduction In-situ Ex-situ Sulfiding Specializing in Refinery Process Catalyst Performance Evaluation Heat & MassBalance Analysis Catalyst Remaining Life Determination Catalyst Deactivation Assessment Catalyst PerformanceCharacterization Refining & Gas Processing & Petrochemical Industries Catalysts / Process Technology - Hydrogen Catalysts /Process Technology Ammonia Catalyst Process Technology - Methanol Catalysts / process Technology PetrochemicalsSpecializing in the Development & Commercialization of New Technologyin the Refining & Petrochemical Industries
Web Site: www.GBHEnterprises.com
Table of Contents
Common Reformer Problems
Purpose of NHT Stripper
Typical Design
Instrumentation of NHT Stripper
Other Design Issues
Indications of Problems in the NHT
Response to Reformer Upsets
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8/10/2019 Catalytic Reforming-Design and Operation of Nht Strippers
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Refinery Process Stream Purification Refinery Process Catalysts Troubleshooting Refinery Process Catalyst Start-Up / ShutdownActivation Reduction In-situ Ex-situ Sulfiding Specializing in Refinery Process Catalyst Performance Evaluation Heat & MassBalance Analysis Catalyst Remaining Life Determination Catalyst Deactivation Assessment Catalyst PerformanceCharacterization Refining & Gas Processing & Petrochemical Industries Catalysts / Process Technology - Hydrogen Catalysts /Process Technology Ammonia Catalyst Process Technology - Methanol Catalysts / process Technology PetrochemicalsSpecializing in the Development & Commercialization of New Technologyin the Refining & Petrochemical Industries
Web Site: www.GBHEnterprises.com
Common Reformer Problems
H2S in feed to reformer
Water in feed to reformer
Bad H2O:HCl control
Feed quality (High EP, low N+A)
Low H2:Oil
Organic Sulfur Compounds in feed to reformer
Purpose of NHT Stripper
Remove the following to protect Reformer: H2S Light Ends Water
Typical Design
Number of Trays
20-35 Trays
Reflux to Feed Ratio
0.25 0.35 More Reflux = More Reliability
Feed Tray Location
5-10 trays from top of tower
More Rectifying Trays can be added if needed
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Refinery Process Stream Purification Refinery Process Catalysts Troubleshooting Refinery Process Catalyst Start-Up / ShutdownActivation Reduction In-situ Ex-situ Sulfiding Specializing in Refinery Process Catalyst Performance Evaluation Heat & MassBalance Analysis Catalyst Remaining Life Determination Catalyst Deactivation Assessment Catalyst PerformanceCharacterization Refining & Gas Processing & Petrochemical Industries Catalysts / Process Technology - Hydrogen Catalysts /Process Technology Ammonia Catalyst Process Technology - Methanol Catalysts / process Technology PetrochemicalsSpecializing in the Development & Commercialization of New Technologyin the Refining & Petrochemical Industries
Web Site: www.GBHEnterprises.com
Instrumentation of NHT Stripper
Other Design Issues
Fired Reboiler vs. Heat Exchanger Reboiler
Better heat input control with Fired Reboiler
Overhead Pressure
Set by the vapor pressure of the liquid in the overhead receiver
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Refinery Process Stream Purification Refinery Process Catalysts Troubleshooting Refinery Process Catalyst Start-Up / ShutdownActivation Reduction In-situ Ex-situ Sulfiding Specializing in Refinery Process Catalyst Performance Evaluation Heat & MassBalance Analysis Catalyst Remaining Life Determination Catalyst Deactivation Assessment Catalyst PerformanceCharacterization Refining & Gas Processing & Petrochemical Industries Catalysts / Process Technology - Hydrogen Catalysts /Process Technology Ammonia Catalyst Process Technology - Methanol Catalysts / process Technology PetrochemicalsSpecializing in the Development & Commercialization of New Technologyin the Refining & Petrochemical Industries
Web Site: www.GBHEnterprises.com
Other Indicators in Reformer
Yield decreases Recycle gas purity decreases LPG make increases Coke make increases
Response to Reformer Upsets
Cut Temperature on Reformer
~900F Hold until H2S is back down
Increase Chloride Injection
Double or Triple normal rates Hold until H2S is back down
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Refinery Process Stream Purification Refinery Process Catalysts Troubleshooting Refinery Process Catalyst Start-Up / ShutdownActivation Reduction In-situ Ex-situ Sulfiding Specializing in Refinery Process Catalyst Performance Evaluation Heat & MassBalance Analysis Catalyst Remaining Life Determination Catalyst Deactivation Assessment Catalyst PerformanceCharacterization Refining & Gas Processing & Petrochemical Industries Catalysts / Process Technology - Hydrogen Catalysts /Process Technology Ammonia Catalyst Process Technology - Methanol Catalysts / process Technology PetrochemicalsSpecializing in the Development & Commercialization of New Technologyin the Refining & Petrochemical Industries
Web Site: www.GBHEnterprises.com
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