certificate of analysis - chill gels · certificate of analysis iso/iec 17025:2017 accreditation...

This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.

Jorge SegredoLab Director

State License # CMTL-0002ISO Accreditation # 97164 ___________________

Signature

09/01/2020

___________________Signed On

4131 SW 47th AVENUE SUITE 1408DAVIE, FL, 33314, USA

Kaycha LabsCHILL GELS

N/AMatrix: Edible

Certificateof Analysis

Sample:DA00825008-001Harvest/Lot ID: 81519

Seed to Sale #N/ABatch Date :N/A

Batch#: 81519Sample Size Received: 1500 mgRetail Product Size: 0.538 gram

Ordered : 08/19/20Sampled : 08/19/20

Completed: 09/01/20 Expires: 09/01/21Sampling Method: SOP Client Method

Sep 01, 2020 | CHILL GELS2424 North Federal Highway, Suite 401Boca Raton, FL, 33431

PASSED of 4

PRODUCT IMAGE SAFETY RESULTS MISC.

PesticidesPASSED

Heavy MetalsPASSED

MicrobialsPASSED

MycotoxinsPASSED

ResidualsSolventsPASSED

FilthPASSED

Water ActivityNOT TESTED

MoistureNOT TESTED

TerpenesNOT TESTED

CANNABINOID RESULTS

Total THC

0.173%THC/Capsule :0.934 mg

Total CBD

4.742%CBD/Capsule :25.513 mg

Total Cannabinoids

5.361%Total Cannabinoids/Capsule:28.842 mg

CBC CBD CBDA CBDV CBG CBGA CBN D8-THC D9-THC THCA THCV

0.165% 3.053% 1.926% ND 0.018% ND 0.023% ND 0.156% 0.020% ND

1.650mg/g

30.530mg/g

19.260mg/g ND

0.180mg/g ND

0.230mg/g ND

1.560mg/g

0.200mg/g ND

LOD 0.001 0.0001 0.001 0.001 0.001 0.001 0.001 0.001 0.0001 0.001 0.001

% % % % % % % % % % %

Cannabinoid Profile TestAnalyzed by Weight Extraction date : Extracted By :450 1.6167g 08/25/20 02:08:45 574

Analysis Method -SOP.T.40.020, SOP.T.30.050 Reviewed On - 08/27/20 15:39:30Analytical Batch -DA015063POT Instrument Used : DA-LC-003 Batch Date : 08/25/20 10:23:24

Reagent Dilution Consums. ID

032320.28 400 280678841082420.R31 918C4-918J082420.R30 914C4-914AK

929C6-929HFull spectrum cannabinoid analysis utilizing High Performance Liquid Chromatography with UV detection (HPLC-UV). (Method: SOP.T.30.050 forsample prep and Shimadzu High Sensitivity Method SOP.T.40.020 for analysis. LOQ for all cannabinoids is 1 mg/L).

Filth PASSED

Analyzed By Weight Extraction date LOD(ppm) Extracted By457 1g NA NA

Analysis Method -SOP.T.40.013 Batch Date : 08/25/20 11:35:39Analytical Batch -DA015069FIL Reviewed On - 08/25/20 13:35:17Instrument Used :

This includes but is not limited to hair, insects, feces, packaging contaminants, and manufacturing wasteand by-products. An SH-2B/T Stereo Microscope is use for inspection.




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09/01/2020

___________________Signed On



N/AMatrix : Edible

Certificate of Analysis PASSEDCHILL GELS

2424 North Federal Highway, Suite 401Boca Raton, FL, 33431Telephone: 1-877-267-4625Email: [email protected]

Sample : DA00825008-001Harvest/LOT ID: 81519Batch# : 81519Sampled : 08/19/20Ordered : 08/19/20

Sample Size Received : 1500 mgCompleted : 09/01/20Expires: 09/01/21Sample Method : SOP Client Method

of 4

Pesticides PASSEDPesticides LOD Units Action Level ResultABAMECTIN B1A 0.01 ppm 0.3 NDACEPHATE 0.01 ppm 3 NDACEQUINOCYL 0.01 ppm 2 NDACETAMIPRID 0.01 ppm 3 NDALDICARB 0.01 ppm 0.1 NDAZOXYSTROBIN 0.01 ppm 3 NDBIFENAZATE 0.01 ppm 3 NDBIFENTHRIN 0.01 ppm 0.5 NDBOSCALID 0.01 PPM 3 NDCARBARYL 0.05 ppm 0.5 NDCARBOFURAN 0.01 ppm 0.1 NDCHLORANTRANILIPROLE 0.1 ppm 3 NDCHLORMEQUAT CHLORIDE 0.1 ppm 3 NDCHLORPYRIFOS 0.01 ppm 0.1 NDCLOFENTEZINE 0.02 ppm 0.5 NDCOUMAPHOS 0.01 ppm 0.1 NDDAMINOZIDE 0.01 ppm 0.1 NDDIAZANON 0.01 ppm 0.2 NDDICHLORVOS 0.01 ppm 0.1 NDDIMETHOATE 0.01 ppm 0.1 NDDIMETHOMORPH 0.02 ppm 3 NDETHOPROPHOS 0.01 ppm 0.1 NDETOFENPROX 0.01 ppm 0.1 NDETOXAZOLE 0.01 ppm 1.5 NDFENHEXAMID 0.01 ppm 3 NDFENOXYCARB 0.01 ppm 0.1 NDFENPYROXIMATE 0.01 ppm 2 NDFIPRONIL 0.01 ppm 0.1 NDFLONICAMID 0.01 ppm 2 NDFLUDIOXONIL 0.01 ppm 3 NDHEXYTHIAZOX 0.01 ppm 2 NDIMAZALIL 0.01 ppm 0.1 NDIMIDACLOPRID 0.04 ppm 3 NDKRESOXIM-METHYL 0.01 ppm 1 NDMALATHION 0.02 ppm 2 NDMETALAXYL 0.01 ppm 3 NDMETHIOCARB 0.01 ppm 0.1 NDMETHOMYL 0.01 ppm 0.1 NDMEVINPHOS 0.01 ppm 0.1 NDMYCLOBUTANIL 0.01 ppm 3 NDNALED 0.025 ppm 0.5 NDOXAMYL 0.05 ppm 0.5 NDPACLOBUTRAZOL 0.01 ppm 0.1 NDPHOSMET 0.01 ppm 0.2 NDPIPERONYL BUTOXIDE 0.1 ppm 3 NDPRALLETHRIN 0.01 ppm 0.4 ND

Pesticides LOD Units Action Level ResultPROPICONAZOLE 0.01 ppm 1 NDPROPOXUR 0.01 ppm 0.1 NDPYRETHRIN I 0.01 ppm 1 NDPYRETHRIN II 0.01 ppm 1 NDPYRETHRINS 0.05 ppm 1 NDPYRIDABEN 0.02 ppm 3 NDSPINETORAM 0.02 PPM 3 NDSPINOSAD (SPINOSYN A) 0.01 ppm 3 NDSPINOSAD (SPINOSYN D) 0.01 ppm 3 NDSPIROMESIFEN 0.01 ppm 3 NDSPIROTETRAMAT 0.01 ppm 3 NDSPIROXAMINE 0.01 ppm 0.1 NDTEBUCONAZOLE 0.01 ppm 1 NDTHIACLOPRID 0.01 ppm 0.1 NDTHIAMETHOXAM 0.05 ppm 1 NDTOTAL CONTAMINANT LOAD(PESTICIDES)

0 PPM 20 ND

TOTAL PERMETHRIN 0.01 ppm 1 NDTOTAL SPINOSAD 0.01 ppm 3 NDTRIFLOXYSTROBIN 0.01 ppm 3 ND

Pesticides PASSED

Analyzed by Weight Extraction date Extracted By585 0.9396g 08/25/20 01:08:48 1082

Analysis Method - SOP.T.30.065, SOP.T.40.065 ,SOP.T.30.065, SOP.T40.070Analytical Batch - DA014974PES Reviewed On- 08/25/20 13:35:17Instrument Used : DA-LCMS-002_DER (PES)Batch Date : 08/21/20 11:01:17

Reagent Dilution Consums. ID080320.02 10 280678841070620.02 76262-590

Pesticide screen is performed using LC-MS which can screen down to below single digit ppb concentrationsfor regulated Pesticides. Currently we analyze for 67 Pesticides. (Method: SOP.T.30.060 Sample Preparationfor Pesticides Analysis via LCMSMS and SOP.T40.065 Procedure for Pesticide Quantification Using LCMS). *Volatile Pesticide screening is performed using GC-MS which can screen down to below single digit ppbconcentrations for regulated Pesticides. Analytes marked with an asterisk were tested using GC-MS.




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09/01/2020

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Residual Solvents PASSED

Solvent LOD Units ActionLevel(PPM)

Pass/Fail Result

1,1-DICHLOROETHENE 0.8 ppm 8 PASS ND

1,2-DICHLOROETHANE 0.2 ppm 5 PASS ND

2-PROPANOL 50 ppm 500 PASS ND

ACETONE 75 ppm 5000 PASS ND

ACETONITRILE 6 ppm 410 PASS ND

BENZENE 0.1 ppm 2 PASS ND

BUTANES (N-BUTANE) 500 ppm 2000 PASS ND

CHLOROFORM 0.2 ppm 60 PASS ND

DICHLOROMETHANE 12.5 ppm 600 PASS ND

ETHANOL 500 ppm 5000 PASS ND

ETHYL ACETATE 40 ppm 5000 PASS ND

ETHYL ETHER 50 ppm 5000 PASS ND

ETHYLENE OXIDE 0.5 ppm 5 PASS ND

HEPTANE 500 ppm 5000 PASS ND

METHANOL 25 ppm 3000 PASS ND

N-HEXANE 25 ppm 290 PASS ND

PENTANES (N-PENTANE) 75 ppm 5000 PASS ND

PROPANE 500 ppm 2100 PASS ND

TOLUENE 15 ppm 890 PASS ND

TOTAL XYLENES 15 ppm 150 PASS ND

TRICHLOROETHYLENE 2.5 ppm 80 PASS ND

XYLENES-M (1,3-DIMETHYLBENZENE)

13.5 ppm 2170 PASS ND

XYLENES-M&P (1,3&1,4-DIMETHYLBENZENE)

27 ppm 2170 PASS ND

XYLENES-O (1,2-DIMETHYLBENZENE)


XYLENES-P (1,4-DIMETHYLBENZENE)


Residual Solvents PASSED


Analysis Method -SOP.T.40.032Analytical Batch -DA015083SOL Reviewed On - 08/28/20 09:50:19Instrument Used : DA-GCMS-002Batch Date : 08/25/20 18:03:26

Reagent Dilution Consums. ID

1 H2017.07700279984161291-1

Residual solvents screening is performed using GC-MS which can detect belowsingle digit ppm concentrations. Currently we analyze for 21 Residualsolvents.(Method: SOP.T.40.032 Residual Solvents Analysis via GC-MS).




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Microbials PASSED

Analyte ResultASPERGILLUS_FLAVUS not present in 1 gram.ASPERGILLUS_FUMIGATUS not present in 1 gram.ASPERGILLUS_NIGER not present in 1 gram.ASPERGILLUS_TERREUS not present in 1 gram.ESCHERICHIA_COLI_SHIGELLA_SPP not present in 1 gram.SALMONELLA_SPECIFIC_GENE not present in 1 gram.

Analysis Method -SOP.T.40.043 / SOP.T.40.044Analytical Batch -DA015045MIC Batch Date : 08/25/20Instrument Used : PathogenDX PCR_Array Scanner DA-111,PathogenDX PCR_DA-010

Analyzed by Weight Extraction date Extracted By513 .9673g 08/25/20 1082

Reagent Consums. ID Consums. ID Consums. ID Consums. ID071020.08101519.09

181019-274SG298A11989-024CC-024181207119C918C4-918J914C4-914AK

929C6-929H50AX308191942308071728020192803029

280700728090052810014D02928040262808006

2811017001001001001001001A07

Microbiological testing for Fungal and Bacterial Identification via Polymerase Chain Reaction (PCR) methodconsisting of sample DNA amplified via tandem Polymerase Chain Reaction (PCR) as a crude lysate which avoidspurification. (Method SOP.T.40.043) If a pathogenic Escherichia Coli, Salmonella, Aspergillus fumigatus,Aspergillus flavus, Aspergillus niger, or Aspergillus terreus is detected in 1g of a sample, the sample fails themicrobiological-impurity testing.

Mycotoxins PASSED

Analyte LOD Units Result Action Level (PPM)AFLATOXIN G2 0.002 ppm ND 0.02AFLATOXIN G1 0.002 ppm ND 0.02AFLATOXIN B2 0.002 ppm ND 0.02AFLATOXIN B1 0.002 ppm ND 0.02OCHRATOXIN A+ 0.002 ppm ND 0.02

Analysis Method -SOP.T.30.065, SOP.T.40.065Analytical Batch -DA014975MYC | Reviewed On - 09/01/20 15:10:42Instrument Used : DA-LCMS-002_DER (MYC)Batch Date : 08/21/20 11:04:23

Analyzed by Weight Extraction date Extracted By585 1g 08/26/20 12:08:30 585

Aflatoxins B1, B2, G1, G2, and Ochratoxins A testing using LC-MS. (Method: SOP.T.30.065 forSample Preparation and SOP.T40.065 Procedure for Mycotoxins Quantification Using LCMS. LOQ 1.0ppb). Aflatoxin B1, B2, G1, and G2 must individually be <20ug/Kg. Ochratoxins must be <20µg/Kg.

Heavy Metals PASSED

Reagent Reagent Dilution Consums. ID082420.R01082520.R13071320.08082420.R03082420.R17082420.R16

082420.R15082420.R18080420.R01022520.02030420.06080120.01

100 89401-566

Metal LOD Unit Result Action Level (PPM)

ARSENIC 0.02 PPM ND 1.5CADMIUM 0.02 PPM ND 0.5LEAD 0.05 PPM ND 0.5MERCURY 0.02 PPM ND 3


Analysis Method -SOP.T.40.050, SOP.T.30.052Analytical Batch -DA015133HEA | Reviewed On - 08/31/20 11:27:33Instrument Used : DA-GCMS-001Batch Date : 08/26/20 14:17:17

Heavy Metals screening is performed using ICP-MS (Inductively Coupled Plasma – MassSpectrometer) which can screen down to below single digit ppb concentrations for regulated heavymetals using Method SOP.T.30.052 Sample Preparation for Heavy Metals Analysis via ICP-MS andSOP.T.40.050 Heavy Metals Analysis via ICP-MS.

certificate of analysis - chill gels · certificate of analysis iso/iec 17025:2017 accreditation...

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