certificate of analysis - us epa · 2015-09-02 · eastern research group 601 keystone park drive...
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Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
November 10 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas Oty KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontalns the analytical results for the sample(s) received under chaln(s) of custody by Eastern Research Group on 080811 0853 through 092911 1057
The test results In this report are in compliance with NaAC accreditation requirements for the certified parameters All analyses were performed as desaibed in the US EPA-approved QAPP under the oontract for NMOC UATMP PAMS CSATAM and NATIS support (US EPA Contract No EPD-Q9-048) This rover page is an integral part of this report and any exceptions or romments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sinrrely ~rolcUAAU_ 1tJA-t q u4middotzL Laura Van Enwyc Project Manager lauravanenwyckergcom
The infotmation contained lD this repwt and itamp attaclunent(s) are mtcnded only for the use of he individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If thereader of this mesage is not rhe intcndtd recipient you ace hereby notified that any dissenunation disUibution or copying of hibull nport iJ strictly prohibited It you have received tbi~ report in error please notify lawmiddot vanm1wgtl (liltcgcrm and delete the report without ret4ining any copits
Page 1 ~f 16
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMITTED 0810811 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LjibNymber Matrix Sampled Received
Ash ampForest Intersection 1080801-01 Air 080511 0000 0808111 0853
Ash ampForest Intersection 1080909-01 Air 0810611 0000 0810911 11 20
Ash ampForest Intersection 1082901-01 Air 082611 0000 082911 0948
4th and Santa Fe 1090818-01 Air 090711 0000 0908111247
150 west of Hwys 169 and 39 1091501-01 Air 091411 0000 0915i111042
75 north of Oak St on 1092909-01 Air 092811 0000 092911 1057
Eastern Research Group 111~ rtsulti tn bullIus report apply oniy to IM ramples cUJalyted u1 accordance wtlt the Lhllin of ruvrudy d(Jcument This mJalyricul rtpltl~i nuw be llproduced 1111tl tmtirery
Page 2 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII ALE 027800001030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMITTED 08081i to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE 913) 551-5042 FAX (913) 55HOOO SITE CODE OECAwork
Desaiption Ash amp Forest Intersection Lab ID i080801-01 Sampled 080511 0000
Pressure Receipt 7 Hg Canister 607 Received 080811 0853
Comments Background sample Analyzed 0809111226
Air Toxics by EPA Compendium Method T0-15 Results HQb
Analvte Jmbx YIlm fl5l ~ Acetylene 611 amp52 0016 Propylene 533 119 0039 Dlchlorodltluoromethane 0571 283 0011 Olaromethane 0678 140 0012 DlchlorotetraftiiOroethilne 0019 01 OCJDI
Vinyl dlloride ND ND u 0008
13-BUIIIdlene 121 268 opo7 Bromomethane 0014 005 0-009 Chloroethane NO NO middotu 0009
Apoundetonitrlle 0403 068 0024
Trlchlorofluoromethane OZ84 160 0010 Aaylonltnle NO NO u 1)012
11-Didtloroethene ND ND u 0 009
Dlchlaromethane 0081 0 31 0010
Carbon DISUlfide oozo 006 u Oil33 Trlchlorotrlfluoroethllne 0106 081 0011 tJans-12-0tchloroetllylene ND ND u 1108 11-0iehloroethane NO NO u 0008 Methyl tert-Butyl Ether NO NO u 0008
Methyl Ethyl KetOne 0599 1 77 0157 Oloroprene NO NO u 0 008
ds-12-Dkhloroethylene NO NO u 0009
Bromochloromethane NO NO u 0008
01foroform ND NO u 0)09
EtltyiiPrt-Butyl Ether NO ND u 0008
12-0ichforoethane NO NO u 0)09 111-Trichforoethlne 0012 0 07 u 0022
Benzene 2amp7 855 0029 carbon Tetrachloride D106 067 0024
tert-Amyl Methyl Ether NO ND u 0016
12-Didlforopmpme ND NO ll 0023
Ethyl ACrylate NO ND u 0020
Bromochchloromethane NO NO u 0025
Trichloroethylene NO NO u 0025
Methyl Methaayfate NO ND u 0022
ds-13-DichiOIOprOpene ND NO u 0022
Methyl Isobutyl KeliOne 0061 025 0022
trans-13-Dkhloropropene ND ND u 0025
112-Tnchloroethane ND NO u 0025
Toluene 358 1350 0016
Dlbromochloromelhane ND NO u ooa
Eastern Research Group The results in this report apply only to the samp~s cmalyr~d in acordrJIce with rh~ oIUiin of CIIStodY documtml 1111v amrytrtal repobull t musr be reproduced 111 tis entirety
Page 3 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F DaVIS
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001 030
REPORTED 111011 0903
SUBMITTED 080811 to 092911
AQS SITE CODE
SITE CODE OECAwork
Description Ash amp Forest Intersection Lab ID 1080801-01 sampled 080511 ooOO
Pressure Receipt 7 Hg canister 607 Received 080B11 0853
Comments Background Sample Analyzed 0809111226
Air Taxies by EPA Compendium Method T0-15 ampwdb MDL
Analvte DRin Yllm Elm ~ 12-Dlbromoethane NO NO u 0-018
n-Octane 0251 118 0015 Tetrachloroethylene NO NO u Ollld
Chlornbenzene NO NO u 0021
Etllylbenzene 0661 z88 0017
mp-xylene 202 879 0034
Bromoform NO NO u 0025
Styrene 0314 138 oou 1122-Tetrachloroethane NO NO u 0024
o-Xylene 0884 385 0018
135-Trlmethylbenzene 02Z8 111 0016
124-Trimethylbenzene 0873 430 0018
m-DichlorobenzenP NO NO u 0034
Chlllromethylbenzene NO NO u 0039
p-Dkhlorobenzene ND ND u 0035
o-OichlorobtnzEne NO NO u 0037
124-Trichlorobenzene ND NO u 0036
Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The bullbulljults in this rtpqrt appty onlgt to the Sltanpl~ m1alyzod 111 accordQIICe with the chain of cuSI(Jdy docunumt 11ti~ dllQytical report nuISI be rf)roduted i11 its entirety
Page 4 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 111011 09middot03
Kansas City KS 66101 SUBMITTED 0810811 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Description Ash amp Forest Intersection Lab ID 1080909-01 Sampled 080611 0000
Pressure 0 Receipt 65 Hg Canister 401 Received 080911 1120
Comments Background Sample Analyzed 0809112309
Air Toxics by EPA Compendium Method T0-15 Results MJU
AnaMe ~ liILm flu ~ Acetylene 0421 045 0016 lropylene 03151 055 00351
Dlchlorodlfluoromethane 0753 373 oou Chloromethane 0752 156 0012 Dldllorotetrafluoraethane 0023 016 00051 Vinyl chloride NO NO u ooos 13-Butadlene 0034 008 0007
Bromametune 0011 007 0~9
Ollarollhane NO NO u 0009
Aaltllnitrile 0270 045 0024
Trlchlorafluorometllane 0313 L76 0010
Auvlonitrile NO NO u 0012
11-0ichloiIEllllene NO NO u 01)09 Dlchlorormithane 0123 OA3 0010
Carbon DISulfide OOS9 028 0033 TriChlorotrlfiUDroethene 0122 094 0011
trans-12-0ichloroethylene NO NO u OOOB U-Dichloroethane NO NO u 00()8 Methyl tert-Butyl Ether NO NO u OOOB Methyl Ethyl Ketone 06051 180 0157 Olloroprene NO NO u OOOB ci5-1Hlichloroethylene NO NO u 0009
Bromochloromethane NO NO u OOOB
Chloroform 0027 013 0009
Eth-(1 tert-Butyl Ether NO NO u OOOB
12-0ichlorothane ND NO u ooog 111-Trichloroethane 00~3 007 u 0022
Benzene 0210 067 0029
~rbon Tetrbullchloride 0132 083 0024 tert-Amyf Melt1yl Ether NO NO u 0016
12-0lChloroptcpane NO NO u 0023
Ethyl Aaylate NO NO u 0020
Bromodichloromethane NO NO u 0025
Trlchloroetbylene NO NO u 0025
Methyl Methacrylate NO NO u 0022
cis-1J-Oichloropropene ND NO u 0022
Methyl Isobutyl Ketone 0040 016 0022
trans-13-Dichloropropene NO NO u 0025
112-Tnchloroethane NO NO u 0025
TDIUIHie 0334 126 0016
Olbromochloromethane NO NO u 0021
Eastern Research Group Th~ r~sults in tins report apoly only ro the sanrptes fDiaylted in accordance With the chain of Cltstody doc11ment 111is mwlylicalnport muft be reproduced in Its enttrtty
Page 5 of 16
RG CERTIFICATE OF ANALYSIS
EPA Reg1on VII FILE 027800001030
300 Minnesota Avenue REPORTED 1111011 0903
Kansas City KS 66101 SUBMITTED 0808111 to 092911
ATTN Michael F DaviS AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption Ash amp Forest Intersection Lab ID 1080909-01 Sampled 080611 0000
Pressure Receipt 65 Hg Canister 401 Received 0809111120
Comments Background Sample Analyzed 080911 2309
Air Toxics by EPA Compendium Method T0-15 Results lmL
Analvte JmiDt Y9Lm flu Jmbx 12-Dibromoethane ND ND u 0018
n-Ociane 0039 018 0015
Tetrachloroethylene ND NO 0018u
Oilorobenzene ND NO u 0021
Ethyl benzene 0074 032 0017
mp-Xylene ()140 061 0034
Bromoform NO NO u 0025
Styrene 0034 015 0022
1122-Tetrachloroethane NO NO u 0024
o-Xylene 0067 029 0018
135-Trimethylbenane 0031 015 0026
124-Trimethylbenzene 0078 038 0028
m-Dichlorobanzene NO NO 0031u Ollcromethylbenzene ND ND u 0039
p-Dichlorobenzene NO NO 0-035u o-Dichlorobemenl ND ND u 0037
12+Trichlorobenzene NO NO 0036u Hexachlnro-13-butadiene ND NO 0037u
Eastern Research Group lhtJ resutu in thrs r~~porl apply tmly io tht ronrpler onaly~d in accordanc6 wrth the chain of curtoay dOIumelll This analytical report mllSt ~ reprfJduccd rn its lntirety
Page 6 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN~ Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001 030
REPORTEDmiddot 111011 0903
SUBMITIED 080811 tci 092911
AQS SITE CODE
SITE CODE OECAwork
Description Ash amp Forest Intersection Lab ID 1082901-01 Sampled 082611 oomiddotoo Pressure Receipt 8 Hg canister 020 Received 082911 0948
COmments Background Sample Analyzed 083011 0036
Air Taxies by EPA Compendium Method T0-15 Results MnL
Analvte mmx Y9lm fml ~ Acetylene 0A94 053 0016 Propylena OA34 o7s 0039 Dlchlorocllrluoromllthane 0553 274 0011 chloR)IIIIIthane 0604 125 0012 Dldlorollltniftuoroethane 0024 017 0009 VInyl dlorlde 0008 002 opoa 13-Butadlene 0028 0 06 op01 Bromomethane 0016 006 0009
Olloroethane NO NO u 0009 Aatonitrila 0217 037 0024 Tr1dtlorofluorometllane 0211 164 0010
Aaylonltrile NO NO u 0012
11-Didlloroethene NO NO u 0009
Dlchloromethane 0404 141 0010 carbon Disulfide 0161 0 50 0033 Trldlorotrlfluoroethane 0117 otO 0011 trans-12-0khloroeth~ene NO NO u ooos 11-0ichloroethane NO NO u 0008
Methyl tPrt-sutvt Ether NO NO u 0008
Methyl Ethyl Ketone 111 328 0157
Chloroprene ND NO u 0008 ds-12-Dichloroethvlent NO NO u 0009
Bromochloromethane NO NO u 0008
Chlororgtnn 0043 021 0001
Ethyl tert-iutyl Ether NO ND u 0008 12middotDichloroethene 0030 012 0001 111middot TriChloroethane 0018 010 u op22
Benzene 0225 072 OOZ9
Carbon Tetrachloride 0098 0amp2 Op24
tert-Amyl Methyl Ether ND NO u 0016
12-0ichloropropane NO NO u 0023
Ethyl Acrylate ND NO u 0020
Bromod1chloromethane 0011 007 u 0025
Trichloroethylene 0 015 008 U 0025
Methyl Methaaylate NO NO u 0022
ds-13-0idlloropropene NO NO u 0022
Methyl Isobutyl Ketone 0052 021 0022
trans-13-0ichloropropene ND NO u 0025
112middot Tnrhloroethane ND NO u 0025
Toluene 514 1940 0016
Olbromochloromethane 0008 007 u 0021
Eastern Research Group lh~ results in this report apply only to the sample 011alyud in accordance with tht rhain of cusrody documtmr This OJialytlcal nport musliM -Produced in its mirery
Page 7 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN~ Michael F DaviS
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001 030
REPORTED 111 Oi11 0903
SUBMITTED 08108111 to 092911
AQS SITE CODE
SITE CODE OECAwork
Description Ash amp Fcorest Intersection Lab ID 1082901-01 Sampled 082611 0000
Pressure I Receipt 8 Hg Canister 020 Received 082911 09~48
Comments Background Sample Analyzed 083011 0036
Air Toxics by EPA Compendium Method T0-15 Results MW
Anayte DDIn Y9lm Eiim IU2bll 12-Dibromoethane NO ND u 0018
n-Ocblne 0074 035 0015
Ttrachloroethylene 0026 018 0018
Chlorobenzene ND ND u 0021
Ethylbenzene 0218 0-95 0017
mp-Xylene 0551 2AO 0034
Bromoform ND ND u (105
Styrene 0089 038 0022
1122-Tetrachloroethane 0010 0 07 u 0024
a-Xylene 0189 082 0018
135-Trlmethylbenzene 0062 031 0026
124-Trimethylbenzene 0150 074 0028
m-Dichlorobenzene 0006 004 u 0034
Chloromethylbenzene NO ND u 0039
p-Dichlorobenzene 0032 019 u 0348
o-Ochlorobenzene 0006 004 u 0037
124-Trlchlorobenzene 1110 NO u 0036
Hexachloro-13-bullldlene 0008 009 u 0037
Eastern Research Group Tlze bullesuJs m this repon apply on)middot to the sanrpfamp nnalyud ill acordance wh lht chain of custody Joumumt Thi~ OIIOI)middottical report musbull be teptoJduced In its elltiJtty
Page 8 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMilTED 0808111 to 0929111
ATTN Michael F Davts AQS SITE CODE
PHONE 913) 551-5042 FAX (913) 551middot5000 SITE CODE OECAwork
Description 4th and Santa Fe Lab ID 1090818-01 Sampled 090711 0000
Pressure 0 Receipt 6 5 Hg Canister EROOB Received 0908111247
Comments Analyzed 090911 0137
AirToxics by EPA Compendium Method T0-15 BciYlb MQI
Analyte lUlblpound usLm fOOl ~ Acetylene 0175 029 0016 Propylene 0333 057 op39 Dichlorodifluoromethane 0521 258 0011 Chloromethane 0507 LOS oou Okhlorotetrafluoroeihane NO NO u 0009
Vinyl chloride NO NO u OOilll 13-Butadlene NO NO u 0007
Bromomethane NO NO u 0009 Chloroethane NO NO u 0009 AletDnibile 0122 021 0024
Tr1dlloroftuoromethane 0252 142 0010 Acrylonlbile NO NO u 0012 11-0ldlloroethPne NO NO u 0009 Dldlloromethane 0159 055 0010
Carbon Disulfide 0063 020 0033 Trlchlorotrlfluoroethane 0094 072 OJ11
trans-12-Dichloroethylene NO NO u 0008
11-0lchloroethane NO NO u ouoa Methyl tert-BlJtyl Ether NO NO u o~
Ne~IEthyiKetone 0472 139 0157 Chloroprene NO NO u 0008
ds-12-Dichloroethylene NO NO u 0109
Bromochloromethane NO NO u oooa Chlorofomi NO NO u 0009 Ethyl ~Butyl Ether NO NO u 0008
12-Didlloroethane NO NO u 0009
111middot Trtdlloroethane NO NO u 0022
Benzene 0168 054 0029 Carbon Telrldllorlde 0095 oeo 0024
tertmiddotAmyl Methyl Ether NO NO u 0016
12-0Chlolgtpropane NO ND u 0023
ethyl Acrtlate NO NO u 0020
Bromodichloromethane NO NO u OOlS Trichloroethylene ND NO u 0025
MettwiMethacrylate NO NO u oc22 cis-13-0ichloropropene NO NO u 0022
~yiiiObutyiKetone 0035 014 0022
trans-13-0ichloropropene NO NO u oo2S 112middot Trichloroethane NO NO u 0025
Toluene 0373 141 0016
OibromQchloromethane NO NO u 0071
Eastern Research Group The nsults in this nport apply only to the saltlples D11alyzed in acordance with the chain Df cuampmiddottody docWMnt This analytical rttport must be repriJduced in its elllirety
Page 9 of 16
RG CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMIITED 080811 to 09291 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 4th and Santa Fe Lab ID 1090818-01 Sampled 090711 0000
Pressure Receipt 65 Hg canister ER008 Received 09081112~47
Comments Analyzed 090911 0137
Air Toxics by EPA Compendium Method T0-15 Results tmL
Analvte IUllm ll9lm flil Jmbll 12-0ibromoethane NO NO u 0018
n-Octane 0038 018 0015
Tetradiloroethylene ND NO u 0018 Chlomhenllne NO NO u 002
Ethyl benzene 0064 028 0017
mp-Xylene 0148 064 0034
Bromoform NO NO u 0025
Styrene NO NO u 0022
1122-TlliiChloroetllane NO NO u 0021
omiddotXylene 0070 031 0018
135middotTrimethylbenzene ND NO u 0026
124-Trimethylbenzene 0078 038 0028
m-Oiehlorobenzene NO NO u 0034
Chloromethylbenzene NO NO u 0019
p-Orchlorobenzene ND NO u 0348
o-Oidllorobenzene ND NO u 0037
124-Trichlorobenzene NO NO u 0036
Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The results rn Jhis teport apply cmJy 10 the samples (Uraly~ed in ac~ordant-e wilh the chain of CIISiody docunum This atwlytiral report 11111s1 be reprculuced i11 ils e11tirrty
Page 10 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN MIChael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001 030
REPORTED~ 1110111 0903
SUBMmED 0810811 to 092911
AQS SITE CODE
SITE CODE OECAwork
Description 150 west of Hwys 169 and 39 Lab ID 1091501-01 sampled 091411 oooo Pressure 0 ReClelpt 13 Hg canister 709 Received 091511 10~42
Comments Analyzed 0915111926
Air Taxies by EPA Compendium Method T0-15 BHIIIm MDI
Analyte JUlbll li9Lm fJJg JlRinl AcBtylene 0234 025 0-016 Propylene 0258 045 0-0~11
Dlchlorodlfluoromettmne 0544 270 oo11 Chloromethane 0526 109 0 012
DichlorolelrifAJoroethane NO NO u Otgt09 Vinyl chloride NO NO u 0008 13-Butildlene NO NO u 0007 Bromomettlane NO NO u 0009 Chloroethane NO NO u 0009
Acetonitrile 0130 022 0024
Trlchlorcrfluoromethane 0263 lAB 0010 Aaylonltrile NO NP u 0012 11-DIChloroethene NO NO u 0009
Dldloromelhane NO NO u (IOlD
carbon Disulfide 0032 010 u 0033 T~hlo~fluonHdhane 0107 082 0011 tr~ns-12-0ichloroethyler~ NO NO u 0008 11-Dichloroethane ljO NO u 0008 Methl tert-Butyl Ether NO NO u 0008 Methyl Ethyl Ketone 0382 113 0157
Chloroprene NO NO u 0008 ciamp-12-0ichloroethylene NO NO u 0009 Bromochloromethane NO NO u 0008 011oroform NO NO u 0009 Ethyl tert-Butyl Ether NO NO u 0008 JI-Dichloroethilne NO NO u 0009 111-Trichloroethane NO NO u (l022
Benzene ozos 067 0029
Carbon Tetrachloride 0101 064 0024 tert-Amyl Methyl Ether NO NO u 1)016 12-DJChiOropropane NO NO u 0023 Ethyl Acrylate NO NO u (1 020
Bromodichloromethane NO NO u 0025 Trichloroethylene NO NO u 0025
Methyl Methacrylilte NO NO u 0022 cis-13-Dichloropropene NO NO u 0022 Methyl Isobutyl llteDM NCI NO u 0022 trans-13-0ichloropropene NO NO u 0025 112-Trldlloroetflane NO NO u 0025 Toluene 0095 036 0016 Olbromodloromelhane NO NO u 0021
Eastern Research Group The results 111 Jhis r~port apply only to the samplts waalylui in accordance with tht chain of custody document This cuuzlytical report must in reprod~~eed in its entirety
Page 11 of 16
CERTIFICATE OF ANALYSISRG EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 111 011 0903
Kansas City KS 66101 SUBMirrED OBiOB11 to 092911
ATTN~ M1chael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE ~ OECAw(irk
Description 150 west of Hwys 169 and 39 Lab ID 1091501-01 Sampled 091411 00 00
Pressure Receipt 13 Hg canister 709 Received 0915111042
Comments Analyzed 0915111926
Air Toxlcs by EPA Compendium Method T0-15 ~ MW
Analvte wmx uqm fli1g RRint 12-Dibromoethane ND IID u 0()18
n-Oddne ND ND u 0015
Tetrachloroethylene ND ND u 0018
Ollorobenzene ND ND u 0021
Ethylbenzene 0035 015 Q017
mpmiddotXylene 0041 018 0034
Bromoform ND NO 11 0025
Styrene NO ND u 002
11-22-Tetradlloroelhane ND ND u 0024
o-Xylene ND NO u 0018
135-Trimethylbenzene NO NO u 0026
124middotTrlrnathylbenzene 0-042 021 0028
m-Dichlorohenzene ND ND u 0034
Chloromethylbenzene ND ND u 0039
p-OIChlorobenzene NO NO u 0348
o-Dichlorobenzere NO NO u 0037
12+Trlchlorobenzene NO ND u 0036
Hexachloro-13-butadlene ND ND u 0037
Eastern Research Group The result in thrs reoort applgt ltmly to the samplts mral1zed m accordanc11 ~ith thilhain of custodgt document This am1lytical report m11st be rbullpmJuced ill it~ entirety
Page 12 of 16
CERTIFrCATE OF ANALYSIS
EPA Region VII FILE tl 027800001030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMITTED 080811 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Description 73 north of Oak St on Plummer Lab ID 1092909-01 Sampled 0928110000
Pressure 0 Receipt 65 Hg canister 140 Received 0929111057
Comments Analyzed 093011 20 34
Analyte
Acetylene middotPropylene
Dldllorodifluoromethane Chlolomettlane
Dlchlorotetrafluoroethllne VInyl chloride 13-Butadlene Bromometl1dne
Chloroethane
Acetunitrile Trldllorotluoromethane
Acrylonitrile
11-0ithloroethene Dichloromethane Carbon DisulfJde
Trlchlorotrlfkloroetftane lranr1 2-0khloroethylene
11-Dithloroelhane
Methyl tert-Butyl Ether Methyl Ethyl Ketone Chloroprene ds-1HllchloiJethylene Bromochloromethane Chlorofvnn
Ethyl tert-Butyl Ether 12-Dichloroethane 111middotTriChloroethane
Benzene carbon Tetrachloride tert-Amyl Methyl Ether 12-Didlonopropane Ethyl Acrylate Bromodlchlorornelhane Trichloroethylene
Methyl MetllacrylaJ
ds-13-Dithloropropene Methyl Isobutyl KetDne trans-13-0khlorapropene 112-Trichloroethane
Toluene Olbromochloromethane
Air Toxics by EPA Compendium Method T0-15 Results mL
ORb YIiID Eiilg I1IZD 223 238 016 123 212 0039
0564 280 0~11
0525 109 0012 0018 013 ooot
NO NO u 0008 0181 040 0~07
NO NO u o009 NO NO u 0009
0157 028 0024 ozgo 163 0010
NO NO u 0(112 NO NO u 0009
0154 054 0010 0045 0 14 0033 0092 071 0011
NO NO u 0008 NO NO u 0008 NO NO u 0~08
0624 184 0157 NO NO u 0008 NO NO u 0009 NO NO u 0008
0035 017 0009 NO NO u 0008 NO NO u 0009
0012 007 u 0022 L49 477 0029
0088 o56 0024 NO NO u 0016 ND NO u 0023 NO NO u 0020 NO ND u 0025
0178 096 0025
NO NO u 0022 NO NO u 0022
0094 039 0022 NO NO u 0025 NO NO u 0025
276 10400 D 0040 r~O NO u 0021
Eastern Research Group The results m this repon apply only to the samples cmolylld in accordance wilh the chain of cUStOdy docWMnt This arwlytlcal rJort mu~middott be reproduced in its entirety
Page 13 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMITTED 0808111 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECA wa1lt
Description 75 north of Oak St on Plummer Lab ID 1092909-01 Sampled 092811 0000
Pressure Receipt 65 Hg canister 140 Received 0929111057
Comments Analyzed 0930112034
Air Toxics by EPA Compendium Method T0-15 Results lmb
Analyte mmx ugm3 flil on 12-Dibromoethane NO NO u 0018
n-Octane 0193 090 0015 Tetrachloroethylene 0019 013 0018
Chlorobenzene NO NO u 0021
Ethyl benzene 0356 155 p017 mp-Xylene 1oamp 461 OOl4
Bromoform NO NO u 6025
Sty~Wte 0060 026 0022 lll2-Tetrachloroethane NO NO u 0-024
o-Xylene P422 184 01118 135-TrlmethylbenEene 0094 046 0026 1124-Trlmethylbenzene 0340 167 0028
m-Dichlorobenzene 0043 016 0034 Chloromethylbenzene NO NO u 0039
p-Dichlorobenzene 0019 011 u 0035
rDichlorobenzellE NO NO u 0037 121-Trochlorobenzene NO NO u 0-036
Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The ll$Ults in rhis repon appl) NIhbull to the samples analyted in accordance with the cham of custody document Thta analybullical rrporl must he reproduced in in entirety
Page 14 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII FILE tl 027800001 030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS66101 SUBMmED 080811 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX~ (913) 551-5000 SITE CODE OECAwork
IAnalyte Result Units SOurce Result RPD
RPD Umit Note
Eastern Research Group ~ resulu in this reprJrt apply oraly to the samples analyed 111 accordance with the chain of crutody docunumt 1his anulmcal report must be reprodu~ed In its enrlnty
Page 15 of 16
CERTIFICATE OF ANALYSISRG EPA Region VII FILEmiddot 027800001 030
300 Minnesota Avenue REPORTED 1110 11 09middot03
Kansas City KS 66101 SUBMITTED 08101311 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX~ (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
u Under Detection Umlt
o Th1s result obtained by dilution
ND Analyte NOT DETECTED at or above the Method Detecbon Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group T1r results in thH report apply on() w the sample tmayzed il occordancltt with the cham of bullur1ody dotumnt This anayllcai report must be prwiuced in its entirety
Page 16 of 16
~RG Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
December 05 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 111511 1121
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the amtract for NMOC UATMP PAMS CSATAM and NATTS support (US EPA Contract No EPD-09-D48) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please oontact me at 919-468-7930
Sincerely
Laura Van Enwyck Project Manager lauravanenwyckergcom
The information contained in this report and its attachment(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauraJnenwyckergcom and delete the report without retairring any copies
Page 1 of6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 120511 1059
Kansas City KS 66101 SUBMITTED 111511
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Lincoln amp 39 Highway 1111501-01 Air 111411 0000 111511 1121 (111 W Lincoln)
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wfth the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001030
REPORTED 120511 1059
SUBMITTED 111511
AQS SITE CODE
SITE CODE OECAwork
DesaiptionUncoln amp 39 Highway (111 W Uncoln) Lab ID 1111501-01 Sampled 111411 0000
Pressure Receipt 8 Hg canister 636 Received 1115111121
Comments Analyzed 111611 0932
Air Toxics by EPA Compendium Method T0-15 blulb lmL
Analvte Jmbx Yllm fiG JlRbl Acetylene 0171 018 A-Ql 0016 Propylene 0272 OA7 A-Ql 0039 Dlchlorodlfluoromethane 0503 2A9 A-Ql 0011 Chloromethane OA74 098 A-Ql 0011 Dichlorobtraftuoroethane 0016 011 A-Ql 0009 Vinyl chloride ND ND A-Ql U 0008 13-Buladlene 0020 004 A-Ql 0007 Bromomethane 0011 004 AmiddotOl 0009 Chloroethane ND ND A-Ql U 0009 Acetonitrile 0138 023 A-Ql 0024 Trichloroftuoromethane D304 L71 A-Ql 0010 Acrylonitrile ND ND A-Q1 U 0012
11-Dichloroethene ND ND A-Q1 U 0009 Dichloromethane 0266 093 A-Ql 0010 Carbon Disulfide 0129 040 A-Ql 0033 Trichlorotrifluoroethane 0079 061 A-Ql 0011 trans-12-0ichloroethylene ND ND A-Ql U 0008 11-Dichloroethane ND ND A-Ql U 0008 Methyl tert-Butyl Ether ND NO A-Q1 U 0008 Methyl Ethyl Ketone 0760 us AmiddotOl 0157 Chloroprene ND NO A-Ql U 0008
cis-12-Dichloroethylene NO NO A-Ql U 0009 Bromochloromethane NO NO A-Ql U 0008 Chloroform NO NO A-Ql U 0009
Ethyl tert-Butyl Ether NO NO Amiddot01 U 0008 12-Dichloroethane 0026 011 A-Ql 0009 111-Trichloroethane 0006 003 A-Q1 U 0022 Benzene 113 362 A-Q1 0029 Carbon Tetrachloride 0069 OA4 A-Q1 0024 tert-Amyl Methyl Ether ND ND A-Ql U 0016 12-Dichloropropane ND NO A-Ql U 0023
Ethyl Acrylate NO NO A-Ql U 0020
Bromodlchloromethane ND NO A-o1 u 0025 Trichloroethylene NO ND A-01 U 0025
Methyl Methacrylate ND NO A-Q1 U 0022 cis-13-Dichloropropene NO NO A-Ql U 0022 Methyl Isobutyl Ketone 0047 019 A-Ql 0022 trans-13-Dichloropropene NO ND A-Q1 U 0025 112-Trichloroethane NO NO A-Q1 U 0025
Toluene 0661 250 A-01 0016 Dibromochloromethane NO ND A-Q1 U 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repoTt must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1210511 1059
Kansas City KS 66101 SUBMITTED 1115 11
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption Uncoln amp 39 Highway (111 W Lincoln) Lab ID 1111501-01 Sampled 111411 0000
Pressure Receipt 8 Hg canister 636 Received 1115111121
Comments Analyzed 111611 0932
Air Toxics by EPA Compendium Method T0-15 RuJID mL
AnaMe IU1bll ~ BiSl IU1bll 12-Dlbromoethane NO NO A-Ql U 0018
n-Oct3ne 0025 012 A-Ql 0015
Tetrachloroethylene 0016 011 A-Ql U 0018
Ollorobenzene NO NO A-Ql U 0021
Ethylbenzene 0068 030 A-Ql 0017
mp-Xylene 0144 063 A-Ql 0034
Bromoform NO NO A-Ql U 0025
Styrene 0058 025 A-Ql 0022
1122-Tetrachloroethane NO NO A-Ql U 0024
o-Xylene 0058 025 A-ol 0018
135-Trlmetflylbenzene 0050 025 A-01 0026
124-Trimetflylbenzene 0130 064 A-Ql 0028
m-Dichlorobenzene NO NO A-Ql U 0034
Chloromelhylbenzene NO NO A-ol U 0039
p-Oichlorobenzene 0027 016 A-Ql U 0035
o-Oichlorobenzene NO NO A-Ql U 0037
124-Trichlorobenzene NO NO A-ol U 0036
Hexachloro-13-butadiene NO NO A-ol U 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 120511 1059
Kansas City KS 66101 SUBMITTED 111511
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance witlz tlze chain of custody documellt This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1205111 1 059
Kansas City KS 66101 SUBMITTED 11151 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
A-ol Estimated value due to possible canister leak
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical re-port must be reproduced in its entirety
Page 6 of 6
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
December 15 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 1206111229
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for NMOC UATMP PAMS CSATAM and NATTS support (US EPA Contract No EPD-09-048) This rover page is an integral part of this report and any exceptions or oomments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Project Manager lauravanenwyckergcom
The information contained in this report and its attachment(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify laura vanenwyck ergcom and delete the report without retaining any copies
Page 1 of 6
RG CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111 1041
Kansas City KS 66101 SUBMITTED 1206 11
ATTN Michael F Davis AQS SITE CODE
PHONE 913) 551-5042 FAX 913) 551-5000 SITE CODE OECAwork
ANALYTlCAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Ash amp Forest SE Corner 1120611-01 Air 120411 0000 120611 1229
middotI I
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytirol repon must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
ALE 027800001030
REPORTED 1215111041
SUBMmED 1210611
AQS SITE CODE
SITE CODE OECAwork
Desaiptlon Ash amp Forest SE Comer Lab ID 1120611-01 sampled 120411 oooo Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 BuYltl MQL
AnaMe IUlllll lWm Bag IUlllll Acetylene OA36 OA7 0016 Propylene 0304 052 0039 Dichlorodiftuoromethane 0567 281 0011 Chloromethane 0566 117 0012 Dlchlorotetnlftuoroethane 0019 013 0009 Vinyl chloride NO NO u 0008 13-Butadiene NO NO u 0007 Bromomethane 0012 005 0009 Chloroethane NO NO u 0009 Acetonitrile 0111 019 0024 Trichlorofluoromethane 0284 160 0010 Aaylonitrile ND NO u 0012 11-Dichloroethene ND ND u 0009 Dichloromethane 0083 029 0010 Carbon Disulfide 0019 006 u 0033
Trlchlorotrlftuoroethane 0099 076 0011 trans-12-Dichloroethylene ND ND u 0008 11-Dichloroethane ND NO u 0008 Methyl tert-Butyl Ether NO NO u 0008 Methyl Ethyl Ketone 0536 158 0157 Chloroprene NO NO u 0008 cis-12-Dichloroethylene NO ND u 0009 Bromochloromethane NO NO u 0008 Chloroform 0022 011 0009 Ethyl tert-Butyl Ether NO NO u 0008 12-Dichloroethane 0025 010 0009 111-Trichloroethane 0011 006 u 0022 Benzene 0188 060 0029 carbon Tetrachloride 0106 067 0024 tert-Amyl Methyl Ether NO NO u 0016 12-Dichloropropane NO NO u 0023 Ethyl Acrylate ND NO u 0020
Bromodichloromethane NO NO u 0025 Trichloroethylene NO NO u 0025 Methyl Methacrylate NO NO u 0022 cis-13-Dichloropropene NO NO u 0022
Methyl Isobutyl Ketone 0042 017 0022 trans-13-Dichloropropene ND NO u 0025 112-Trichloroethane NO NO u 0025
Toluene 0149 056 0016 Oibromochloromethane 0003 003 u 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproducedin its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 121511 1041
Kansas City KS 66101 SUBMmED 1210611
ATTN Michael F Davis AQS SITE CODE
PHONE (913 551-5042 FAX (913 551-5000 SITE CODE OECAwork
Description Ash amp Forest SE Comer Lab ID 1120611-01 Sampled 120411 0000
Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 llWdtl MID
Analyte ubll IUllm Bag ubll 12-0ibromoethane NO NO u 0018 nmiddotOctane 0044 021 0015 Tetrachloroethylene 0006 004 u 0018
Chlorobenzene NO NO u 0021 Ethylbenzene 0047 021 0017 mp-Xylene 0070 031 0034 Bromoform NO NO u 0025 Styrene 0034 015 0022 1122-Tetrachloroethane NO NO u 0024 o-Xylene 0036 016 0018 135-Trlmethylbenzene 0025 012 u 0026 124-Trlmetllylbenzene 0047 023 0028 m-Oichlorobenzene NO NO u 0034
Chloromethylbenzene NO NO u 0039 p-Dichlorcbenzene 0005 003 u 0348 a-Dichlorobenzene NO NO u 0037
124-Trlchlorobenzene NO NO u 0036 Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repon must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS~RG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 66101 SUBMITTED 12061 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPDIAnalyte Result Units Result RPD um1t Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 661 01 SUBMITTED 120611
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its enJirety
Page 6 of 6
i
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
March 12 2012
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 030512 0916
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for UATMP NATTS CSATAM PAMS and NMOC support (US EPA Contract No 68-D-Q9-048) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Program Manager lauravanenwyckergcom
The information contained in this report and its attachmcnt(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauravanenwyckergcom and delete the report dthout retaining any copies
Page 1 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 0312112 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
6th St between Central amp 2030501-01 Air 030212 0000 030512 0916 Malcom
Eastern Research Group The results in this report apply only to the samples anal zed in accordance With the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Aven ue REPORTED 031212 1 051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 ~ tml
Analvte RRbll Y9lD1 flu RRbll Acetylene 0627 067 0072 Propylene 0484 084 0033
Dichlorodllluoromethane 0500 248 0023 Chloromethane 0557 115 0033
Dichlorotetrafluoroethane 0015 011 0012 Vinyl chloride NO NO u 0011
13-Butadlene 0036 oo8 0011
Bromomethane 0012 005 0012 Chloroethane NO NO u 0017
Acetonitrile 0073 012 0073
Trichlorofluoromethane 0258 145 0015 Acrylonitrile NO NO u 0020
11-0ichloroethene NO NO u 0014
Dichloromethane 0185 064 0023
Carbon Disulfide 0037 012 0014 Trichlorobitluoroethane 0119 091 0017
trans-12-0ichloroethylene NO NO u 0012
11-0ichloroethane NO NO u 0015
Methyl tert-Butyl Ether NO NO u 0011
Chloroprene NO NO u 0012
ds-12-0ich loroethylene NO NO u OD18
Bromochloromethane NO NO u 0014
Chloroform NO ND u 0014
Ethyl tert-Butyl Ether NO NO u 0011
12-Dichloroethane 0019 008 0016
111-Trichloroethane 0012 007 u 0020
Benzene 0344 L10 0061 Carbon Tetrachloride 0088 056 0024
tert-Amyl Methyl Ether NO NO u 0016
12-0ichloropropane ND NO u 0019
Ethyl Acrylate ND NO u 0014
Bromodichloromethane ND NO u 0021
Trichloroethylene NO ND u 0022
Methyl Methacrylate ND NO u 0025
ds-13-0ichloropropene NO NO u 0015
Methyl Isobutyl Ketone 0015 oo6 0015
trans-13-0ichloropropene NO ND u 0016
112-Trichloroethane NO NO u 0021
Toluene 0416 157 0045
Oibromochloromethane ND NO u 0018
12-0ibromoethane ND NO u 0017
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551 -5000
FILE 027800001030
REPORTED 0312 12 1051
SUBMITTED 030512
AQS SITE CODE
SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 Bwdtl MJlL
Analvte Jmbll Y9Lm Big Jmbx nmiddotOclane 0039 018 0020 Tetrachloroethylene 0005 003 u 0020
Chlorobenzene ND ND u 0025
Ethylbenzene 0045 020 0023 mp-Xylene 0112 OA9 0037 Bromoform ND ND u 0020
Styrene 0030 013 0024 1122-Tetrachloroethane ND ND u 0018
o-Xylene 0050 022 0020
135-Trimethylbenzene 0019 009 u 0022
124-Trimethylbenzene 0047 023 0025 m-Dichlorobenzene ND ND u 0024
p-Dichlorobenzene 0004 002 u 0019
a-Dichlorobenzene NO ND u 0021
124-Trichlorobenzene ND ND u 0022
Hexachloro-13-butadiene ND ND u 0022
Eastern Research Group The results in this report apply only 1o the samples analyzed in accordance with the chain of custody document This analytical rep ort must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 031212 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wilh the chain of custody document This analytical report must be reproduced in its enrirety
Page 5 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 03121121051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report nutst be reproduced in its entirety
Page 6 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMITTED 0810811 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LjibNymber Matrix Sampled Received
Ash ampForest Intersection 1080801-01 Air 080511 0000 0808111 0853
Ash ampForest Intersection 1080909-01 Air 0810611 0000 0810911 11 20
Ash ampForest Intersection 1082901-01 Air 082611 0000 082911 0948
4th and Santa Fe 1090818-01 Air 090711 0000 0908111247
150 west of Hwys 169 and 39 1091501-01 Air 091411 0000 0915i111042
75 north of Oak St on 1092909-01 Air 092811 0000 092911 1057
Eastern Research Group 111~ rtsulti tn bullIus report apply oniy to IM ramples cUJalyted u1 accordance wtlt the Lhllin of ruvrudy d(Jcument This mJalyricul rtpltl~i nuw be llproduced 1111tl tmtirery
Page 2 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII ALE 027800001030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMITTED 08081i to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE 913) 551-5042 FAX (913) 55HOOO SITE CODE OECAwork
Desaiption Ash amp Forest Intersection Lab ID i080801-01 Sampled 080511 0000
Pressure Receipt 7 Hg Canister 607 Received 080811 0853
Comments Background sample Analyzed 0809111226
Air Toxics by EPA Compendium Method T0-15 Results HQb
Analvte Jmbx YIlm fl5l ~ Acetylene 611 amp52 0016 Propylene 533 119 0039 Dlchlorodltluoromethane 0571 283 0011 Olaromethane 0678 140 0012 DlchlorotetraftiiOroethilne 0019 01 OCJDI
Vinyl dlloride ND ND u 0008
13-BUIIIdlene 121 268 opo7 Bromomethane 0014 005 0-009 Chloroethane NO NO middotu 0009
Apoundetonitrlle 0403 068 0024
Trlchlorofluoromethane OZ84 160 0010 Aaylonltnle NO NO u 1)012
11-Didtloroethene ND ND u 0 009
Dlchlaromethane 0081 0 31 0010
Carbon DISUlfide oozo 006 u Oil33 Trlchlorotrlfluoroethllne 0106 081 0011 tJans-12-0tchloroetllylene ND ND u 1108 11-0iehloroethane NO NO u 0008 Methyl tert-Butyl Ether NO NO u 0008
Methyl Ethyl KetOne 0599 1 77 0157 Oloroprene NO NO u 0 008
ds-12-Dkhloroethylene NO NO u 0009
Bromochloromethane NO NO u 0008
01foroform ND NO u 0)09
EtltyiiPrt-Butyl Ether NO ND u 0008
12-0ichforoethane NO NO u 0)09 111-Trichforoethlne 0012 0 07 u 0022
Benzene 2amp7 855 0029 carbon Tetrachloride D106 067 0024
tert-Amyl Methyl Ether NO ND u 0016
12-Didlforopmpme ND NO ll 0023
Ethyl ACrylate NO ND u 0020
Bromochchloromethane NO NO u 0025
Trichloroethylene NO NO u 0025
Methyl Methaayfate NO ND u 0022
ds-13-DichiOIOprOpene ND NO u 0022
Methyl Isobutyl KeliOne 0061 025 0022
trans-13-Dkhloropropene ND ND u 0025
112-Tnchloroethane ND NO u 0025
Toluene 358 1350 0016
Dlbromochloromelhane ND NO u ooa
Eastern Research Group The results in this report apply only to the samp~s cmalyr~d in acordrJIce with rh~ oIUiin of CIIStodY documtml 1111v amrytrtal repobull t musr be reproduced 111 tis entirety
Page 3 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F DaVIS
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001 030
REPORTED 111011 0903
SUBMITTED 080811 to 092911
AQS SITE CODE
SITE CODE OECAwork
Description Ash amp Forest Intersection Lab ID 1080801-01 sampled 080511 ooOO
Pressure Receipt 7 Hg canister 607 Received 080B11 0853
Comments Background Sample Analyzed 0809111226
Air Taxies by EPA Compendium Method T0-15 ampwdb MDL
Analvte DRin Yllm Elm ~ 12-Dlbromoethane NO NO u 0-018
n-Octane 0251 118 0015 Tetrachloroethylene NO NO u Ollld
Chlornbenzene NO NO u 0021
Etllylbenzene 0661 z88 0017
mp-xylene 202 879 0034
Bromoform NO NO u 0025
Styrene 0314 138 oou 1122-Tetrachloroethane NO NO u 0024
o-Xylene 0884 385 0018
135-Trlmethylbenzene 02Z8 111 0016
124-Trimethylbenzene 0873 430 0018
m-DichlorobenzenP NO NO u 0034
Chlllromethylbenzene NO NO u 0039
p-Dkhlorobenzene ND ND u 0035
o-OichlorobtnzEne NO NO u 0037
124-Trichlorobenzene ND NO u 0036
Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The bullbulljults in this rtpqrt appty onlgt to the Sltanpl~ m1alyzod 111 accordQIICe with the chain of cuSI(Jdy docunumt 11ti~ dllQytical report nuISI be rf)roduted i11 its entirety
Page 4 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 111011 09middot03
Kansas City KS 66101 SUBMITTED 0810811 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Description Ash amp Forest Intersection Lab ID 1080909-01 Sampled 080611 0000
Pressure 0 Receipt 65 Hg Canister 401 Received 080911 1120
Comments Background Sample Analyzed 0809112309
Air Toxics by EPA Compendium Method T0-15 Results MJU
AnaMe ~ liILm flu ~ Acetylene 0421 045 0016 lropylene 03151 055 00351
Dlchlorodlfluoromethane 0753 373 oou Chloromethane 0752 156 0012 Dldllorotetrafluoraethane 0023 016 00051 Vinyl chloride NO NO u ooos 13-Butadlene 0034 008 0007
Bromametune 0011 007 0~9
Ollarollhane NO NO u 0009
Aaltllnitrile 0270 045 0024
Trlchlorafluorometllane 0313 L76 0010
Auvlonitrile NO NO u 0012
11-0ichloiIEllllene NO NO u 01)09 Dlchlorormithane 0123 OA3 0010
Carbon DISulfide OOS9 028 0033 TriChlorotrlfiUDroethene 0122 094 0011
trans-12-0ichloroethylene NO NO u OOOB U-Dichloroethane NO NO u 00()8 Methyl tert-Butyl Ether NO NO u OOOB Methyl Ethyl Ketone 06051 180 0157 Olloroprene NO NO u OOOB ci5-1Hlichloroethylene NO NO u 0009
Bromochloromethane NO NO u OOOB
Chloroform 0027 013 0009
Eth-(1 tert-Butyl Ether NO NO u OOOB
12-0ichlorothane ND NO u ooog 111-Trichloroethane 00~3 007 u 0022
Benzene 0210 067 0029
~rbon Tetrbullchloride 0132 083 0024 tert-Amyf Melt1yl Ether NO NO u 0016
12-0lChloroptcpane NO NO u 0023
Ethyl Aaylate NO NO u 0020
Bromodichloromethane NO NO u 0025
Trlchloroetbylene NO NO u 0025
Methyl Methacrylate NO NO u 0022
cis-1J-Oichloropropene ND NO u 0022
Methyl Isobutyl Ketone 0040 016 0022
trans-13-Dichloropropene NO NO u 0025
112-Tnchloroethane NO NO u 0025
TDIUIHie 0334 126 0016
Olbromochloromethane NO NO u 0021
Eastern Research Group Th~ r~sults in tins report apoly only ro the sanrptes fDiaylted in accordance With the chain of Cltstody doc11ment 111is mwlylicalnport muft be reproduced in Its enttrtty
Page 5 of 16
RG CERTIFICATE OF ANALYSIS
EPA Reg1on VII FILE 027800001030
300 Minnesota Avenue REPORTED 1111011 0903
Kansas City KS 66101 SUBMITTED 0808111 to 092911
ATTN Michael F DaviS AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption Ash amp Forest Intersection Lab ID 1080909-01 Sampled 080611 0000
Pressure Receipt 65 Hg Canister 401 Received 0809111120
Comments Background Sample Analyzed 080911 2309
Air Toxics by EPA Compendium Method T0-15 Results lmL
Analvte JmiDt Y9Lm flu Jmbx 12-Dibromoethane ND ND u 0018
n-Ociane 0039 018 0015
Tetrachloroethylene ND NO 0018u
Oilorobenzene ND NO u 0021
Ethyl benzene 0074 032 0017
mp-Xylene ()140 061 0034
Bromoform NO NO u 0025
Styrene 0034 015 0022
1122-Tetrachloroethane NO NO u 0024
o-Xylene 0067 029 0018
135-Trimethylbenane 0031 015 0026
124-Trimethylbenzene 0078 038 0028
m-Dichlorobanzene NO NO 0031u Ollcromethylbenzene ND ND u 0039
p-Dichlorobenzene NO NO 0-035u o-Dichlorobemenl ND ND u 0037
12+Trichlorobenzene NO NO 0036u Hexachlnro-13-butadiene ND NO 0037u
Eastern Research Group lhtJ resutu in thrs r~~porl apply tmly io tht ronrpler onaly~d in accordanc6 wrth the chain of curtoay dOIumelll This analytical report mllSt ~ reprfJduccd rn its lntirety
Page 6 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN~ Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001 030
REPORTEDmiddot 111011 0903
SUBMITIED 080811 tci 092911
AQS SITE CODE
SITE CODE OECAwork
Description Ash amp Forest Intersection Lab ID 1082901-01 Sampled 082611 oomiddotoo Pressure Receipt 8 Hg canister 020 Received 082911 0948
COmments Background Sample Analyzed 083011 0036
Air Taxies by EPA Compendium Method T0-15 Results MnL
Analvte mmx Y9lm fml ~ Acetylene 0A94 053 0016 Propylena OA34 o7s 0039 Dlchlorocllrluoromllthane 0553 274 0011 chloR)IIIIIthane 0604 125 0012 Dldlorollltniftuoroethane 0024 017 0009 VInyl dlorlde 0008 002 opoa 13-Butadlene 0028 0 06 op01 Bromomethane 0016 006 0009
Olloroethane NO NO u 0009 Aatonitrila 0217 037 0024 Tr1dtlorofluorometllane 0211 164 0010
Aaylonltrile NO NO u 0012
11-Didlloroethene NO NO u 0009
Dlchloromethane 0404 141 0010 carbon Disulfide 0161 0 50 0033 Trldlorotrlfluoroethane 0117 otO 0011 trans-12-0khloroeth~ene NO NO u ooos 11-0ichloroethane NO NO u 0008
Methyl tPrt-sutvt Ether NO NO u 0008
Methyl Ethyl Ketone 111 328 0157
Chloroprene ND NO u 0008 ds-12-Dichloroethvlent NO NO u 0009
Bromochloromethane NO NO u 0008
Chlororgtnn 0043 021 0001
Ethyl tert-iutyl Ether NO ND u 0008 12middotDichloroethene 0030 012 0001 111middot TriChloroethane 0018 010 u op22
Benzene 0225 072 OOZ9
Carbon Tetrachloride 0098 0amp2 Op24
tert-Amyl Methyl Ether ND NO u 0016
12-0ichloropropane NO NO u 0023
Ethyl Acrylate ND NO u 0020
Bromod1chloromethane 0011 007 u 0025
Trichloroethylene 0 015 008 U 0025
Methyl Methaaylate NO NO u 0022
ds-13-0idlloropropene NO NO u 0022
Methyl Isobutyl Ketone 0052 021 0022
trans-13-0ichloropropene ND NO u 0025
112middot Tnrhloroethane ND NO u 0025
Toluene 514 1940 0016
Olbromochloromethane 0008 007 u 0021
Eastern Research Group lh~ results in this report apply only to the sample 011alyud in accordance with tht rhain of cusrody documtmr This OJialytlcal nport musliM -Produced in its mirery
Page 7 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN~ Michael F DaviS
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001 030
REPORTED 111 Oi11 0903
SUBMITTED 08108111 to 092911
AQS SITE CODE
SITE CODE OECAwork
Description Ash amp Fcorest Intersection Lab ID 1082901-01 Sampled 082611 0000
Pressure I Receipt 8 Hg Canister 020 Received 082911 09~48
Comments Background Sample Analyzed 083011 0036
Air Toxics by EPA Compendium Method T0-15 Results MW
Anayte DDIn Y9lm Eiim IU2bll 12-Dibromoethane NO ND u 0018
n-Ocblne 0074 035 0015
Ttrachloroethylene 0026 018 0018
Chlorobenzene ND ND u 0021
Ethylbenzene 0218 0-95 0017
mp-Xylene 0551 2AO 0034
Bromoform ND ND u (105
Styrene 0089 038 0022
1122-Tetrachloroethane 0010 0 07 u 0024
a-Xylene 0189 082 0018
135-Trlmethylbenzene 0062 031 0026
124-Trimethylbenzene 0150 074 0028
m-Dichlorobenzene 0006 004 u 0034
Chloromethylbenzene NO ND u 0039
p-Dichlorobenzene 0032 019 u 0348
o-Ochlorobenzene 0006 004 u 0037
124-Trlchlorobenzene 1110 NO u 0036
Hexachloro-13-bullldlene 0008 009 u 0037
Eastern Research Group Tlze bullesuJs m this repon apply on)middot to the sanrpfamp nnalyud ill acordance wh lht chain of custody Joumumt Thi~ OIIOI)middottical report musbull be teptoJduced In its elltiJtty
Page 8 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMilTED 0808111 to 0929111
ATTN Michael F Davts AQS SITE CODE
PHONE 913) 551-5042 FAX (913) 551middot5000 SITE CODE OECAwork
Description 4th and Santa Fe Lab ID 1090818-01 Sampled 090711 0000
Pressure 0 Receipt 6 5 Hg Canister EROOB Received 0908111247
Comments Analyzed 090911 0137
AirToxics by EPA Compendium Method T0-15 BciYlb MQI
Analyte lUlblpound usLm fOOl ~ Acetylene 0175 029 0016 Propylene 0333 057 op39 Dichlorodifluoromethane 0521 258 0011 Chloromethane 0507 LOS oou Okhlorotetrafluoroeihane NO NO u 0009
Vinyl chloride NO NO u OOilll 13-Butadlene NO NO u 0007
Bromomethane NO NO u 0009 Chloroethane NO NO u 0009 AletDnibile 0122 021 0024
Tr1dlloroftuoromethane 0252 142 0010 Acrylonlbile NO NO u 0012 11-0ldlloroethPne NO NO u 0009 Dldlloromethane 0159 055 0010
Carbon Disulfide 0063 020 0033 Trlchlorotrlfluoroethane 0094 072 OJ11
trans-12-Dichloroethylene NO NO u 0008
11-0lchloroethane NO NO u ouoa Methyl tert-BlJtyl Ether NO NO u o~
Ne~IEthyiKetone 0472 139 0157 Chloroprene NO NO u 0008
ds-12-Dichloroethylene NO NO u 0109
Bromochloromethane NO NO u oooa Chlorofomi NO NO u 0009 Ethyl ~Butyl Ether NO NO u 0008
12-Didlloroethane NO NO u 0009
111middot Trtdlloroethane NO NO u 0022
Benzene 0168 054 0029 Carbon Telrldllorlde 0095 oeo 0024
tertmiddotAmyl Methyl Ether NO NO u 0016
12-0Chlolgtpropane NO ND u 0023
ethyl Acrtlate NO NO u 0020
Bromodichloromethane NO NO u OOlS Trichloroethylene ND NO u 0025
MettwiMethacrylate NO NO u oc22 cis-13-0ichloropropene NO NO u 0022
~yiiiObutyiKetone 0035 014 0022
trans-13-0ichloropropene NO NO u oo2S 112middot Trichloroethane NO NO u 0025
Toluene 0373 141 0016
OibromQchloromethane NO NO u 0071
Eastern Research Group The nsults in this nport apply only to the saltlples D11alyzed in acordance with the chain Df cuampmiddottody docWMnt This analytical rttport must be repriJduced in its elllirety
Page 9 of 16
RG CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMIITED 080811 to 09291 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 4th and Santa Fe Lab ID 1090818-01 Sampled 090711 0000
Pressure Receipt 65 Hg canister ER008 Received 09081112~47
Comments Analyzed 090911 0137
Air Toxics by EPA Compendium Method T0-15 Results tmL
Analvte IUllm ll9lm flil Jmbll 12-0ibromoethane NO NO u 0018
n-Octane 0038 018 0015
Tetradiloroethylene ND NO u 0018 Chlomhenllne NO NO u 002
Ethyl benzene 0064 028 0017
mp-Xylene 0148 064 0034
Bromoform NO NO u 0025
Styrene NO NO u 0022
1122-TlliiChloroetllane NO NO u 0021
omiddotXylene 0070 031 0018
135middotTrimethylbenzene ND NO u 0026
124-Trimethylbenzene 0078 038 0028
m-Oiehlorobenzene NO NO u 0034
Chloromethylbenzene NO NO u 0019
p-Orchlorobenzene ND NO u 0348
o-Oidllorobenzene ND NO u 0037
124-Trichlorobenzene NO NO u 0036
Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The results rn Jhis teport apply cmJy 10 the samples (Uraly~ed in ac~ordant-e wilh the chain of CIISiody docunum This atwlytiral report 11111s1 be reprculuced i11 ils e11tirrty
Page 10 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN MIChael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001 030
REPORTED~ 1110111 0903
SUBMmED 0810811 to 092911
AQS SITE CODE
SITE CODE OECAwork
Description 150 west of Hwys 169 and 39 Lab ID 1091501-01 sampled 091411 oooo Pressure 0 ReClelpt 13 Hg canister 709 Received 091511 10~42
Comments Analyzed 0915111926
Air Taxies by EPA Compendium Method T0-15 BHIIIm MDI
Analyte JUlbll li9Lm fJJg JlRinl AcBtylene 0234 025 0-016 Propylene 0258 045 0-0~11
Dlchlorodlfluoromettmne 0544 270 oo11 Chloromethane 0526 109 0 012
DichlorolelrifAJoroethane NO NO u Otgt09 Vinyl chloride NO NO u 0008 13-Butildlene NO NO u 0007 Bromomettlane NO NO u 0009 Chloroethane NO NO u 0009
Acetonitrile 0130 022 0024
Trlchlorcrfluoromethane 0263 lAB 0010 Aaylonltrile NO NP u 0012 11-DIChloroethene NO NO u 0009
Dldloromelhane NO NO u (IOlD
carbon Disulfide 0032 010 u 0033 T~hlo~fluonHdhane 0107 082 0011 tr~ns-12-0ichloroethyler~ NO NO u 0008 11-Dichloroethane ljO NO u 0008 Methl tert-Butyl Ether NO NO u 0008 Methyl Ethyl Ketone 0382 113 0157
Chloroprene NO NO u 0008 ciamp-12-0ichloroethylene NO NO u 0009 Bromochloromethane NO NO u 0008 011oroform NO NO u 0009 Ethyl tert-Butyl Ether NO NO u 0008 JI-Dichloroethilne NO NO u 0009 111-Trichloroethane NO NO u (l022
Benzene ozos 067 0029
Carbon Tetrachloride 0101 064 0024 tert-Amyl Methyl Ether NO NO u 1)016 12-DJChiOropropane NO NO u 0023 Ethyl Acrylate NO NO u (1 020
Bromodichloromethane NO NO u 0025 Trichloroethylene NO NO u 0025
Methyl Methacrylilte NO NO u 0022 cis-13-Dichloropropene NO NO u 0022 Methyl Isobutyl llteDM NCI NO u 0022 trans-13-0ichloropropene NO NO u 0025 112-Trldlloroetflane NO NO u 0025 Toluene 0095 036 0016 Olbromodloromelhane NO NO u 0021
Eastern Research Group The results 111 Jhis r~port apply only to the samplts waalylui in accordance with tht chain of custody document This cuuzlytical report must in reprod~~eed in its entirety
Page 11 of 16
CERTIFICATE OF ANALYSISRG EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 111 011 0903
Kansas City KS 66101 SUBMirrED OBiOB11 to 092911
ATTN~ M1chael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE ~ OECAw(irk
Description 150 west of Hwys 169 and 39 Lab ID 1091501-01 Sampled 091411 00 00
Pressure Receipt 13 Hg canister 709 Received 0915111042
Comments Analyzed 0915111926
Air Toxlcs by EPA Compendium Method T0-15 ~ MW
Analvte wmx uqm fli1g RRint 12-Dibromoethane ND IID u 0()18
n-Oddne ND ND u 0015
Tetrachloroethylene ND ND u 0018
Ollorobenzene ND ND u 0021
Ethylbenzene 0035 015 Q017
mpmiddotXylene 0041 018 0034
Bromoform ND NO 11 0025
Styrene NO ND u 002
11-22-Tetradlloroelhane ND ND u 0024
o-Xylene ND NO u 0018
135-Trimethylbenzene NO NO u 0026
124middotTrlrnathylbenzene 0-042 021 0028
m-Dichlorohenzene ND ND u 0034
Chloromethylbenzene ND ND u 0039
p-OIChlorobenzene NO NO u 0348
o-Dichlorobenzere NO NO u 0037
12+Trlchlorobenzene NO ND u 0036
Hexachloro-13-butadlene ND ND u 0037
Eastern Research Group The result in thrs reoort applgt ltmly to the samplts mral1zed m accordanc11 ~ith thilhain of custodgt document This am1lytical report m11st be rbullpmJuced ill it~ entirety
Page 12 of 16
CERTIFrCATE OF ANALYSIS
EPA Region VII FILE tl 027800001030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMITTED 080811 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Description 73 north of Oak St on Plummer Lab ID 1092909-01 Sampled 0928110000
Pressure 0 Receipt 65 Hg canister 140 Received 0929111057
Comments Analyzed 093011 20 34
Analyte
Acetylene middotPropylene
Dldllorodifluoromethane Chlolomettlane
Dlchlorotetrafluoroethllne VInyl chloride 13-Butadlene Bromometl1dne
Chloroethane
Acetunitrile Trldllorotluoromethane
Acrylonitrile
11-0ithloroethene Dichloromethane Carbon DisulfJde
Trlchlorotrlfkloroetftane lranr1 2-0khloroethylene
11-Dithloroelhane
Methyl tert-Butyl Ether Methyl Ethyl Ketone Chloroprene ds-1HllchloiJethylene Bromochloromethane Chlorofvnn
Ethyl tert-Butyl Ether 12-Dichloroethane 111middotTriChloroethane
Benzene carbon Tetrachloride tert-Amyl Methyl Ether 12-Didlonopropane Ethyl Acrylate Bromodlchlorornelhane Trichloroethylene
Methyl MetllacrylaJ
ds-13-Dithloropropene Methyl Isobutyl KetDne trans-13-0khlorapropene 112-Trichloroethane
Toluene Olbromochloromethane
Air Toxics by EPA Compendium Method T0-15 Results mL
ORb YIiID Eiilg I1IZD 223 238 016 123 212 0039
0564 280 0~11
0525 109 0012 0018 013 ooot
NO NO u 0008 0181 040 0~07
NO NO u o009 NO NO u 0009
0157 028 0024 ozgo 163 0010
NO NO u 0(112 NO NO u 0009
0154 054 0010 0045 0 14 0033 0092 071 0011
NO NO u 0008 NO NO u 0008 NO NO u 0~08
0624 184 0157 NO NO u 0008 NO NO u 0009 NO NO u 0008
0035 017 0009 NO NO u 0008 NO NO u 0009
0012 007 u 0022 L49 477 0029
0088 o56 0024 NO NO u 0016 ND NO u 0023 NO NO u 0020 NO ND u 0025
0178 096 0025
NO NO u 0022 NO NO u 0022
0094 039 0022 NO NO u 0025 NO NO u 0025
276 10400 D 0040 r~O NO u 0021
Eastern Research Group The results m this repon apply only to the samples cmolylld in accordance wilh the chain of cUStOdy docWMnt This arwlytlcal rJort mu~middott be reproduced in its entirety
Page 13 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMITTED 0808111 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECA wa1lt
Description 75 north of Oak St on Plummer Lab ID 1092909-01 Sampled 092811 0000
Pressure Receipt 65 Hg canister 140 Received 0929111057
Comments Analyzed 0930112034
Air Toxics by EPA Compendium Method T0-15 Results lmb
Analyte mmx ugm3 flil on 12-Dibromoethane NO NO u 0018
n-Octane 0193 090 0015 Tetrachloroethylene 0019 013 0018
Chlorobenzene NO NO u 0021
Ethyl benzene 0356 155 p017 mp-Xylene 1oamp 461 OOl4
Bromoform NO NO u 6025
Sty~Wte 0060 026 0022 lll2-Tetrachloroethane NO NO u 0-024
o-Xylene P422 184 01118 135-TrlmethylbenEene 0094 046 0026 1124-Trlmethylbenzene 0340 167 0028
m-Dichlorobenzene 0043 016 0034 Chloromethylbenzene NO NO u 0039
p-Dichlorobenzene 0019 011 u 0035
rDichlorobenzellE NO NO u 0037 121-Trochlorobenzene NO NO u 0-036
Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The ll$Ults in rhis repon appl) NIhbull to the samples analyted in accordance with the cham of custody document Thta analybullical rrporl must he reproduced in in entirety
Page 14 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII FILE tl 027800001 030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS66101 SUBMmED 080811 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX~ (913) 551-5000 SITE CODE OECAwork
IAnalyte Result Units SOurce Result RPD
RPD Umit Note
Eastern Research Group ~ resulu in this reprJrt apply oraly to the samples analyed 111 accordance with the chain of crutody docunumt 1his anulmcal report must be reprodu~ed In its enrlnty
Page 15 of 16
CERTIFICATE OF ANALYSISRG EPA Region VII FILEmiddot 027800001 030
300 Minnesota Avenue REPORTED 1110 11 09middot03
Kansas City KS 66101 SUBMITTED 08101311 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX~ (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
u Under Detection Umlt
o Th1s result obtained by dilution
ND Analyte NOT DETECTED at or above the Method Detecbon Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group T1r results in thH report apply on() w the sample tmayzed il occordancltt with the cham of bullur1ody dotumnt This anayllcai report must be prwiuced in its entirety
Page 16 of 16
~RG Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
December 05 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 111511 1121
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the amtract for NMOC UATMP PAMS CSATAM and NATTS support (US EPA Contract No EPD-09-D48) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please oontact me at 919-468-7930
Sincerely
Laura Van Enwyck Project Manager lauravanenwyckergcom
The information contained in this report and its attachment(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauraJnenwyckergcom and delete the report without retairring any copies
Page 1 of6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 120511 1059
Kansas City KS 66101 SUBMITTED 111511
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Lincoln amp 39 Highway 1111501-01 Air 111411 0000 111511 1121 (111 W Lincoln)
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wfth the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001030
REPORTED 120511 1059
SUBMITTED 111511
AQS SITE CODE
SITE CODE OECAwork
DesaiptionUncoln amp 39 Highway (111 W Uncoln) Lab ID 1111501-01 Sampled 111411 0000
Pressure Receipt 8 Hg canister 636 Received 1115111121
Comments Analyzed 111611 0932
Air Toxics by EPA Compendium Method T0-15 blulb lmL
Analvte Jmbx Yllm fiG JlRbl Acetylene 0171 018 A-Ql 0016 Propylene 0272 OA7 A-Ql 0039 Dlchlorodlfluoromethane 0503 2A9 A-Ql 0011 Chloromethane OA74 098 A-Ql 0011 Dichlorobtraftuoroethane 0016 011 A-Ql 0009 Vinyl chloride ND ND A-Ql U 0008 13-Buladlene 0020 004 A-Ql 0007 Bromomethane 0011 004 AmiddotOl 0009 Chloroethane ND ND A-Ql U 0009 Acetonitrile 0138 023 A-Ql 0024 Trichloroftuoromethane D304 L71 A-Ql 0010 Acrylonitrile ND ND A-Q1 U 0012
11-Dichloroethene ND ND A-Q1 U 0009 Dichloromethane 0266 093 A-Ql 0010 Carbon Disulfide 0129 040 A-Ql 0033 Trichlorotrifluoroethane 0079 061 A-Ql 0011 trans-12-0ichloroethylene ND ND A-Ql U 0008 11-Dichloroethane ND ND A-Ql U 0008 Methyl tert-Butyl Ether ND NO A-Q1 U 0008 Methyl Ethyl Ketone 0760 us AmiddotOl 0157 Chloroprene ND NO A-Ql U 0008
cis-12-Dichloroethylene NO NO A-Ql U 0009 Bromochloromethane NO NO A-Ql U 0008 Chloroform NO NO A-Ql U 0009
Ethyl tert-Butyl Ether NO NO Amiddot01 U 0008 12-Dichloroethane 0026 011 A-Ql 0009 111-Trichloroethane 0006 003 A-Q1 U 0022 Benzene 113 362 A-Q1 0029 Carbon Tetrachloride 0069 OA4 A-Q1 0024 tert-Amyl Methyl Ether ND ND A-Ql U 0016 12-Dichloropropane ND NO A-Ql U 0023
Ethyl Acrylate NO NO A-Ql U 0020
Bromodlchloromethane ND NO A-o1 u 0025 Trichloroethylene NO ND A-01 U 0025
Methyl Methacrylate ND NO A-Q1 U 0022 cis-13-Dichloropropene NO NO A-Ql U 0022 Methyl Isobutyl Ketone 0047 019 A-Ql 0022 trans-13-Dichloropropene NO ND A-Q1 U 0025 112-Trichloroethane NO NO A-Q1 U 0025
Toluene 0661 250 A-01 0016 Dibromochloromethane NO ND A-Q1 U 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repoTt must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1210511 1059
Kansas City KS 66101 SUBMITTED 1115 11
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption Uncoln amp 39 Highway (111 W Lincoln) Lab ID 1111501-01 Sampled 111411 0000
Pressure Receipt 8 Hg canister 636 Received 1115111121
Comments Analyzed 111611 0932
Air Toxics by EPA Compendium Method T0-15 RuJID mL
AnaMe IU1bll ~ BiSl IU1bll 12-Dlbromoethane NO NO A-Ql U 0018
n-Oct3ne 0025 012 A-Ql 0015
Tetrachloroethylene 0016 011 A-Ql U 0018
Ollorobenzene NO NO A-Ql U 0021
Ethylbenzene 0068 030 A-Ql 0017
mp-Xylene 0144 063 A-Ql 0034
Bromoform NO NO A-Ql U 0025
Styrene 0058 025 A-Ql 0022
1122-Tetrachloroethane NO NO A-Ql U 0024
o-Xylene 0058 025 A-ol 0018
135-Trlmetflylbenzene 0050 025 A-01 0026
124-Trimetflylbenzene 0130 064 A-Ql 0028
m-Dichlorobenzene NO NO A-Ql U 0034
Chloromelhylbenzene NO NO A-ol U 0039
p-Oichlorobenzene 0027 016 A-Ql U 0035
o-Oichlorobenzene NO NO A-Ql U 0037
124-Trichlorobenzene NO NO A-ol U 0036
Hexachloro-13-butadiene NO NO A-ol U 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 120511 1059
Kansas City KS 66101 SUBMITTED 111511
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance witlz tlze chain of custody documellt This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1205111 1 059
Kansas City KS 66101 SUBMITTED 11151 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
A-ol Estimated value due to possible canister leak
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical re-port must be reproduced in its entirety
Page 6 of 6
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
December 15 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 1206111229
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for NMOC UATMP PAMS CSATAM and NATTS support (US EPA Contract No EPD-09-048) This rover page is an integral part of this report and any exceptions or oomments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Project Manager lauravanenwyckergcom
The information contained in this report and its attachment(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify laura vanenwyck ergcom and delete the report without retaining any copies
Page 1 of 6
RG CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111 1041
Kansas City KS 66101 SUBMITTED 1206 11
ATTN Michael F Davis AQS SITE CODE
PHONE 913) 551-5042 FAX 913) 551-5000 SITE CODE OECAwork
ANALYTlCAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Ash amp Forest SE Corner 1120611-01 Air 120411 0000 120611 1229
middotI I
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytirol repon must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
ALE 027800001030
REPORTED 1215111041
SUBMmED 1210611
AQS SITE CODE
SITE CODE OECAwork
Desaiptlon Ash amp Forest SE Comer Lab ID 1120611-01 sampled 120411 oooo Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 BuYltl MQL
AnaMe IUlllll lWm Bag IUlllll Acetylene OA36 OA7 0016 Propylene 0304 052 0039 Dichlorodiftuoromethane 0567 281 0011 Chloromethane 0566 117 0012 Dlchlorotetnlftuoroethane 0019 013 0009 Vinyl chloride NO NO u 0008 13-Butadiene NO NO u 0007 Bromomethane 0012 005 0009 Chloroethane NO NO u 0009 Acetonitrile 0111 019 0024 Trichlorofluoromethane 0284 160 0010 Aaylonitrile ND NO u 0012 11-Dichloroethene ND ND u 0009 Dichloromethane 0083 029 0010 Carbon Disulfide 0019 006 u 0033
Trlchlorotrlftuoroethane 0099 076 0011 trans-12-Dichloroethylene ND ND u 0008 11-Dichloroethane ND NO u 0008 Methyl tert-Butyl Ether NO NO u 0008 Methyl Ethyl Ketone 0536 158 0157 Chloroprene NO NO u 0008 cis-12-Dichloroethylene NO ND u 0009 Bromochloromethane NO NO u 0008 Chloroform 0022 011 0009 Ethyl tert-Butyl Ether NO NO u 0008 12-Dichloroethane 0025 010 0009 111-Trichloroethane 0011 006 u 0022 Benzene 0188 060 0029 carbon Tetrachloride 0106 067 0024 tert-Amyl Methyl Ether NO NO u 0016 12-Dichloropropane NO NO u 0023 Ethyl Acrylate ND NO u 0020
Bromodichloromethane NO NO u 0025 Trichloroethylene NO NO u 0025 Methyl Methacrylate NO NO u 0022 cis-13-Dichloropropene NO NO u 0022
Methyl Isobutyl Ketone 0042 017 0022 trans-13-Dichloropropene ND NO u 0025 112-Trichloroethane NO NO u 0025
Toluene 0149 056 0016 Oibromochloromethane 0003 003 u 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproducedin its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 121511 1041
Kansas City KS 66101 SUBMmED 1210611
ATTN Michael F Davis AQS SITE CODE
PHONE (913 551-5042 FAX (913 551-5000 SITE CODE OECAwork
Description Ash amp Forest SE Comer Lab ID 1120611-01 Sampled 120411 0000
Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 llWdtl MID
Analyte ubll IUllm Bag ubll 12-0ibromoethane NO NO u 0018 nmiddotOctane 0044 021 0015 Tetrachloroethylene 0006 004 u 0018
Chlorobenzene NO NO u 0021 Ethylbenzene 0047 021 0017 mp-Xylene 0070 031 0034 Bromoform NO NO u 0025 Styrene 0034 015 0022 1122-Tetrachloroethane NO NO u 0024 o-Xylene 0036 016 0018 135-Trlmethylbenzene 0025 012 u 0026 124-Trlmetllylbenzene 0047 023 0028 m-Oichlorobenzene NO NO u 0034
Chloromethylbenzene NO NO u 0039 p-Dichlorcbenzene 0005 003 u 0348 a-Dichlorobenzene NO NO u 0037
124-Trlchlorobenzene NO NO u 0036 Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repon must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS~RG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 66101 SUBMITTED 12061 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPDIAnalyte Result Units Result RPD um1t Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 661 01 SUBMITTED 120611
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its enJirety
Page 6 of 6
i
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
March 12 2012
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 030512 0916
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for UATMP NATTS CSATAM PAMS and NMOC support (US EPA Contract No 68-D-Q9-048) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Program Manager lauravanenwyckergcom
The information contained in this report and its attachmcnt(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauravanenwyckergcom and delete the report dthout retaining any copies
Page 1 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 0312112 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
6th St between Central amp 2030501-01 Air 030212 0000 030512 0916 Malcom
Eastern Research Group The results in this report apply only to the samples anal zed in accordance With the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Aven ue REPORTED 031212 1 051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 ~ tml
Analvte RRbll Y9lD1 flu RRbll Acetylene 0627 067 0072 Propylene 0484 084 0033
Dichlorodllluoromethane 0500 248 0023 Chloromethane 0557 115 0033
Dichlorotetrafluoroethane 0015 011 0012 Vinyl chloride NO NO u 0011
13-Butadlene 0036 oo8 0011
Bromomethane 0012 005 0012 Chloroethane NO NO u 0017
Acetonitrile 0073 012 0073
Trichlorofluoromethane 0258 145 0015 Acrylonitrile NO NO u 0020
11-0ichloroethene NO NO u 0014
Dichloromethane 0185 064 0023
Carbon Disulfide 0037 012 0014 Trichlorobitluoroethane 0119 091 0017
trans-12-0ichloroethylene NO NO u 0012
11-0ichloroethane NO NO u 0015
Methyl tert-Butyl Ether NO NO u 0011
Chloroprene NO NO u 0012
ds-12-0ich loroethylene NO NO u OD18
Bromochloromethane NO NO u 0014
Chloroform NO ND u 0014
Ethyl tert-Butyl Ether NO NO u 0011
12-Dichloroethane 0019 008 0016
111-Trichloroethane 0012 007 u 0020
Benzene 0344 L10 0061 Carbon Tetrachloride 0088 056 0024
tert-Amyl Methyl Ether NO NO u 0016
12-0ichloropropane ND NO u 0019
Ethyl Acrylate ND NO u 0014
Bromodichloromethane ND NO u 0021
Trichloroethylene NO ND u 0022
Methyl Methacrylate ND NO u 0025
ds-13-0ichloropropene NO NO u 0015
Methyl Isobutyl Ketone 0015 oo6 0015
trans-13-0ichloropropene NO ND u 0016
112-Trichloroethane NO NO u 0021
Toluene 0416 157 0045
Oibromochloromethane ND NO u 0018
12-0ibromoethane ND NO u 0017
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551 -5000
FILE 027800001030
REPORTED 0312 12 1051
SUBMITTED 030512
AQS SITE CODE
SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 Bwdtl MJlL
Analvte Jmbll Y9Lm Big Jmbx nmiddotOclane 0039 018 0020 Tetrachloroethylene 0005 003 u 0020
Chlorobenzene ND ND u 0025
Ethylbenzene 0045 020 0023 mp-Xylene 0112 OA9 0037 Bromoform ND ND u 0020
Styrene 0030 013 0024 1122-Tetrachloroethane ND ND u 0018
o-Xylene 0050 022 0020
135-Trimethylbenzene 0019 009 u 0022
124-Trimethylbenzene 0047 023 0025 m-Dichlorobenzene ND ND u 0024
p-Dichlorobenzene 0004 002 u 0019
a-Dichlorobenzene NO ND u 0021
124-Trichlorobenzene ND ND u 0022
Hexachloro-13-butadiene ND ND u 0022
Eastern Research Group The results in this report apply only 1o the samples analyzed in accordance with the chain of custody document This analytical rep ort must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 031212 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wilh the chain of custody document This analytical report must be reproduced in its enrirety
Page 5 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 03121121051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report nutst be reproduced in its entirety
Page 6 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII ALE 027800001030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMITTED 08081i to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE 913) 551-5042 FAX (913) 55HOOO SITE CODE OECAwork
Desaiption Ash amp Forest Intersection Lab ID i080801-01 Sampled 080511 0000
Pressure Receipt 7 Hg Canister 607 Received 080811 0853
Comments Background sample Analyzed 0809111226
Air Toxics by EPA Compendium Method T0-15 Results HQb
Analvte Jmbx YIlm fl5l ~ Acetylene 611 amp52 0016 Propylene 533 119 0039 Dlchlorodltluoromethane 0571 283 0011 Olaromethane 0678 140 0012 DlchlorotetraftiiOroethilne 0019 01 OCJDI
Vinyl dlloride ND ND u 0008
13-BUIIIdlene 121 268 opo7 Bromomethane 0014 005 0-009 Chloroethane NO NO middotu 0009
Apoundetonitrlle 0403 068 0024
Trlchlorofluoromethane OZ84 160 0010 Aaylonltnle NO NO u 1)012
11-Didtloroethene ND ND u 0 009
Dlchlaromethane 0081 0 31 0010
Carbon DISUlfide oozo 006 u Oil33 Trlchlorotrlfluoroethllne 0106 081 0011 tJans-12-0tchloroetllylene ND ND u 1108 11-0iehloroethane NO NO u 0008 Methyl tert-Butyl Ether NO NO u 0008
Methyl Ethyl KetOne 0599 1 77 0157 Oloroprene NO NO u 0 008
ds-12-Dkhloroethylene NO NO u 0009
Bromochloromethane NO NO u 0008
01foroform ND NO u 0)09
EtltyiiPrt-Butyl Ether NO ND u 0008
12-0ichforoethane NO NO u 0)09 111-Trichforoethlne 0012 0 07 u 0022
Benzene 2amp7 855 0029 carbon Tetrachloride D106 067 0024
tert-Amyl Methyl Ether NO ND u 0016
12-Didlforopmpme ND NO ll 0023
Ethyl ACrylate NO ND u 0020
Bromochchloromethane NO NO u 0025
Trichloroethylene NO NO u 0025
Methyl Methaayfate NO ND u 0022
ds-13-DichiOIOprOpene ND NO u 0022
Methyl Isobutyl KeliOne 0061 025 0022
trans-13-Dkhloropropene ND ND u 0025
112-Tnchloroethane ND NO u 0025
Toluene 358 1350 0016
Dlbromochloromelhane ND NO u ooa
Eastern Research Group The results in this report apply only to the samp~s cmalyr~d in acordrJIce with rh~ oIUiin of CIIStodY documtml 1111v amrytrtal repobull t musr be reproduced 111 tis entirety
Page 3 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F DaVIS
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001 030
REPORTED 111011 0903
SUBMITTED 080811 to 092911
AQS SITE CODE
SITE CODE OECAwork
Description Ash amp Forest Intersection Lab ID 1080801-01 sampled 080511 ooOO
Pressure Receipt 7 Hg canister 607 Received 080B11 0853
Comments Background Sample Analyzed 0809111226
Air Taxies by EPA Compendium Method T0-15 ampwdb MDL
Analvte DRin Yllm Elm ~ 12-Dlbromoethane NO NO u 0-018
n-Octane 0251 118 0015 Tetrachloroethylene NO NO u Ollld
Chlornbenzene NO NO u 0021
Etllylbenzene 0661 z88 0017
mp-xylene 202 879 0034
Bromoform NO NO u 0025
Styrene 0314 138 oou 1122-Tetrachloroethane NO NO u 0024
o-Xylene 0884 385 0018
135-Trlmethylbenzene 02Z8 111 0016
124-Trimethylbenzene 0873 430 0018
m-DichlorobenzenP NO NO u 0034
Chlllromethylbenzene NO NO u 0039
p-Dkhlorobenzene ND ND u 0035
o-OichlorobtnzEne NO NO u 0037
124-Trichlorobenzene ND NO u 0036
Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The bullbulljults in this rtpqrt appty onlgt to the Sltanpl~ m1alyzod 111 accordQIICe with the chain of cuSI(Jdy docunumt 11ti~ dllQytical report nuISI be rf)roduted i11 its entirety
Page 4 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 111011 09middot03
Kansas City KS 66101 SUBMITTED 0810811 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Description Ash amp Forest Intersection Lab ID 1080909-01 Sampled 080611 0000
Pressure 0 Receipt 65 Hg Canister 401 Received 080911 1120
Comments Background Sample Analyzed 0809112309
Air Toxics by EPA Compendium Method T0-15 Results MJU
AnaMe ~ liILm flu ~ Acetylene 0421 045 0016 lropylene 03151 055 00351
Dlchlorodlfluoromethane 0753 373 oou Chloromethane 0752 156 0012 Dldllorotetrafluoraethane 0023 016 00051 Vinyl chloride NO NO u ooos 13-Butadlene 0034 008 0007
Bromametune 0011 007 0~9
Ollarollhane NO NO u 0009
Aaltllnitrile 0270 045 0024
Trlchlorafluorometllane 0313 L76 0010
Auvlonitrile NO NO u 0012
11-0ichloiIEllllene NO NO u 01)09 Dlchlorormithane 0123 OA3 0010
Carbon DISulfide OOS9 028 0033 TriChlorotrlfiUDroethene 0122 094 0011
trans-12-0ichloroethylene NO NO u OOOB U-Dichloroethane NO NO u 00()8 Methyl tert-Butyl Ether NO NO u OOOB Methyl Ethyl Ketone 06051 180 0157 Olloroprene NO NO u OOOB ci5-1Hlichloroethylene NO NO u 0009
Bromochloromethane NO NO u OOOB
Chloroform 0027 013 0009
Eth-(1 tert-Butyl Ether NO NO u OOOB
12-0ichlorothane ND NO u ooog 111-Trichloroethane 00~3 007 u 0022
Benzene 0210 067 0029
~rbon Tetrbullchloride 0132 083 0024 tert-Amyf Melt1yl Ether NO NO u 0016
12-0lChloroptcpane NO NO u 0023
Ethyl Aaylate NO NO u 0020
Bromodichloromethane NO NO u 0025
Trlchloroetbylene NO NO u 0025
Methyl Methacrylate NO NO u 0022
cis-1J-Oichloropropene ND NO u 0022
Methyl Isobutyl Ketone 0040 016 0022
trans-13-Dichloropropene NO NO u 0025
112-Tnchloroethane NO NO u 0025
TDIUIHie 0334 126 0016
Olbromochloromethane NO NO u 0021
Eastern Research Group Th~ r~sults in tins report apoly only ro the sanrptes fDiaylted in accordance With the chain of Cltstody doc11ment 111is mwlylicalnport muft be reproduced in Its enttrtty
Page 5 of 16
RG CERTIFICATE OF ANALYSIS
EPA Reg1on VII FILE 027800001030
300 Minnesota Avenue REPORTED 1111011 0903
Kansas City KS 66101 SUBMITTED 0808111 to 092911
ATTN Michael F DaviS AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption Ash amp Forest Intersection Lab ID 1080909-01 Sampled 080611 0000
Pressure Receipt 65 Hg Canister 401 Received 0809111120
Comments Background Sample Analyzed 080911 2309
Air Toxics by EPA Compendium Method T0-15 Results lmL
Analvte JmiDt Y9Lm flu Jmbx 12-Dibromoethane ND ND u 0018
n-Ociane 0039 018 0015
Tetrachloroethylene ND NO 0018u
Oilorobenzene ND NO u 0021
Ethyl benzene 0074 032 0017
mp-Xylene ()140 061 0034
Bromoform NO NO u 0025
Styrene 0034 015 0022
1122-Tetrachloroethane NO NO u 0024
o-Xylene 0067 029 0018
135-Trimethylbenane 0031 015 0026
124-Trimethylbenzene 0078 038 0028
m-Dichlorobanzene NO NO 0031u Ollcromethylbenzene ND ND u 0039
p-Dichlorobenzene NO NO 0-035u o-Dichlorobemenl ND ND u 0037
12+Trichlorobenzene NO NO 0036u Hexachlnro-13-butadiene ND NO 0037u
Eastern Research Group lhtJ resutu in thrs r~~porl apply tmly io tht ronrpler onaly~d in accordanc6 wrth the chain of curtoay dOIumelll This analytical report mllSt ~ reprfJduccd rn its lntirety
Page 6 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN~ Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001 030
REPORTEDmiddot 111011 0903
SUBMITIED 080811 tci 092911
AQS SITE CODE
SITE CODE OECAwork
Description Ash amp Forest Intersection Lab ID 1082901-01 Sampled 082611 oomiddotoo Pressure Receipt 8 Hg canister 020 Received 082911 0948
COmments Background Sample Analyzed 083011 0036
Air Taxies by EPA Compendium Method T0-15 Results MnL
Analvte mmx Y9lm fml ~ Acetylene 0A94 053 0016 Propylena OA34 o7s 0039 Dlchlorocllrluoromllthane 0553 274 0011 chloR)IIIIIthane 0604 125 0012 Dldlorollltniftuoroethane 0024 017 0009 VInyl dlorlde 0008 002 opoa 13-Butadlene 0028 0 06 op01 Bromomethane 0016 006 0009
Olloroethane NO NO u 0009 Aatonitrila 0217 037 0024 Tr1dtlorofluorometllane 0211 164 0010
Aaylonltrile NO NO u 0012
11-Didlloroethene NO NO u 0009
Dlchloromethane 0404 141 0010 carbon Disulfide 0161 0 50 0033 Trldlorotrlfluoroethane 0117 otO 0011 trans-12-0khloroeth~ene NO NO u ooos 11-0ichloroethane NO NO u 0008
Methyl tPrt-sutvt Ether NO NO u 0008
Methyl Ethyl Ketone 111 328 0157
Chloroprene ND NO u 0008 ds-12-Dichloroethvlent NO NO u 0009
Bromochloromethane NO NO u 0008
Chlororgtnn 0043 021 0001
Ethyl tert-iutyl Ether NO ND u 0008 12middotDichloroethene 0030 012 0001 111middot TriChloroethane 0018 010 u op22
Benzene 0225 072 OOZ9
Carbon Tetrachloride 0098 0amp2 Op24
tert-Amyl Methyl Ether ND NO u 0016
12-0ichloropropane NO NO u 0023
Ethyl Acrylate ND NO u 0020
Bromod1chloromethane 0011 007 u 0025
Trichloroethylene 0 015 008 U 0025
Methyl Methaaylate NO NO u 0022
ds-13-0idlloropropene NO NO u 0022
Methyl Isobutyl Ketone 0052 021 0022
trans-13-0ichloropropene ND NO u 0025
112middot Tnrhloroethane ND NO u 0025
Toluene 514 1940 0016
Olbromochloromethane 0008 007 u 0021
Eastern Research Group lh~ results in this report apply only to the sample 011alyud in accordance with tht rhain of cusrody documtmr This OJialytlcal nport musliM -Produced in its mirery
Page 7 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN~ Michael F DaviS
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001 030
REPORTED 111 Oi11 0903
SUBMITTED 08108111 to 092911
AQS SITE CODE
SITE CODE OECAwork
Description Ash amp Fcorest Intersection Lab ID 1082901-01 Sampled 082611 0000
Pressure I Receipt 8 Hg Canister 020 Received 082911 09~48
Comments Background Sample Analyzed 083011 0036
Air Toxics by EPA Compendium Method T0-15 Results MW
Anayte DDIn Y9lm Eiim IU2bll 12-Dibromoethane NO ND u 0018
n-Ocblne 0074 035 0015
Ttrachloroethylene 0026 018 0018
Chlorobenzene ND ND u 0021
Ethylbenzene 0218 0-95 0017
mp-Xylene 0551 2AO 0034
Bromoform ND ND u (105
Styrene 0089 038 0022
1122-Tetrachloroethane 0010 0 07 u 0024
a-Xylene 0189 082 0018
135-Trlmethylbenzene 0062 031 0026
124-Trimethylbenzene 0150 074 0028
m-Dichlorobenzene 0006 004 u 0034
Chloromethylbenzene NO ND u 0039
p-Dichlorobenzene 0032 019 u 0348
o-Ochlorobenzene 0006 004 u 0037
124-Trlchlorobenzene 1110 NO u 0036
Hexachloro-13-bullldlene 0008 009 u 0037
Eastern Research Group Tlze bullesuJs m this repon apply on)middot to the sanrpfamp nnalyud ill acordance wh lht chain of custody Joumumt Thi~ OIIOI)middottical report musbull be teptoJduced In its elltiJtty
Page 8 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMilTED 0808111 to 0929111
ATTN Michael F Davts AQS SITE CODE
PHONE 913) 551-5042 FAX (913) 551middot5000 SITE CODE OECAwork
Description 4th and Santa Fe Lab ID 1090818-01 Sampled 090711 0000
Pressure 0 Receipt 6 5 Hg Canister EROOB Received 0908111247
Comments Analyzed 090911 0137
AirToxics by EPA Compendium Method T0-15 BciYlb MQI
Analyte lUlblpound usLm fOOl ~ Acetylene 0175 029 0016 Propylene 0333 057 op39 Dichlorodifluoromethane 0521 258 0011 Chloromethane 0507 LOS oou Okhlorotetrafluoroeihane NO NO u 0009
Vinyl chloride NO NO u OOilll 13-Butadlene NO NO u 0007
Bromomethane NO NO u 0009 Chloroethane NO NO u 0009 AletDnibile 0122 021 0024
Tr1dlloroftuoromethane 0252 142 0010 Acrylonlbile NO NO u 0012 11-0ldlloroethPne NO NO u 0009 Dldlloromethane 0159 055 0010
Carbon Disulfide 0063 020 0033 Trlchlorotrlfluoroethane 0094 072 OJ11
trans-12-Dichloroethylene NO NO u 0008
11-0lchloroethane NO NO u ouoa Methyl tert-BlJtyl Ether NO NO u o~
Ne~IEthyiKetone 0472 139 0157 Chloroprene NO NO u 0008
ds-12-Dichloroethylene NO NO u 0109
Bromochloromethane NO NO u oooa Chlorofomi NO NO u 0009 Ethyl ~Butyl Ether NO NO u 0008
12-Didlloroethane NO NO u 0009
111middot Trtdlloroethane NO NO u 0022
Benzene 0168 054 0029 Carbon Telrldllorlde 0095 oeo 0024
tertmiddotAmyl Methyl Ether NO NO u 0016
12-0Chlolgtpropane NO ND u 0023
ethyl Acrtlate NO NO u 0020
Bromodichloromethane NO NO u OOlS Trichloroethylene ND NO u 0025
MettwiMethacrylate NO NO u oc22 cis-13-0ichloropropene NO NO u 0022
~yiiiObutyiKetone 0035 014 0022
trans-13-0ichloropropene NO NO u oo2S 112middot Trichloroethane NO NO u 0025
Toluene 0373 141 0016
OibromQchloromethane NO NO u 0071
Eastern Research Group The nsults in this nport apply only to the saltlples D11alyzed in acordance with the chain Df cuampmiddottody docWMnt This analytical rttport must be repriJduced in its elllirety
Page 9 of 16
RG CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMIITED 080811 to 09291 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 4th and Santa Fe Lab ID 1090818-01 Sampled 090711 0000
Pressure Receipt 65 Hg canister ER008 Received 09081112~47
Comments Analyzed 090911 0137
Air Toxics by EPA Compendium Method T0-15 Results tmL
Analvte IUllm ll9lm flil Jmbll 12-0ibromoethane NO NO u 0018
n-Octane 0038 018 0015
Tetradiloroethylene ND NO u 0018 Chlomhenllne NO NO u 002
Ethyl benzene 0064 028 0017
mp-Xylene 0148 064 0034
Bromoform NO NO u 0025
Styrene NO NO u 0022
1122-TlliiChloroetllane NO NO u 0021
omiddotXylene 0070 031 0018
135middotTrimethylbenzene ND NO u 0026
124-Trimethylbenzene 0078 038 0028
m-Oiehlorobenzene NO NO u 0034
Chloromethylbenzene NO NO u 0019
p-Orchlorobenzene ND NO u 0348
o-Oidllorobenzene ND NO u 0037
124-Trichlorobenzene NO NO u 0036
Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The results rn Jhis teport apply cmJy 10 the samples (Uraly~ed in ac~ordant-e wilh the chain of CIISiody docunum This atwlytiral report 11111s1 be reprculuced i11 ils e11tirrty
Page 10 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN MIChael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001 030
REPORTED~ 1110111 0903
SUBMmED 0810811 to 092911
AQS SITE CODE
SITE CODE OECAwork
Description 150 west of Hwys 169 and 39 Lab ID 1091501-01 sampled 091411 oooo Pressure 0 ReClelpt 13 Hg canister 709 Received 091511 10~42
Comments Analyzed 0915111926
Air Taxies by EPA Compendium Method T0-15 BHIIIm MDI
Analyte JUlbll li9Lm fJJg JlRinl AcBtylene 0234 025 0-016 Propylene 0258 045 0-0~11
Dlchlorodlfluoromettmne 0544 270 oo11 Chloromethane 0526 109 0 012
DichlorolelrifAJoroethane NO NO u Otgt09 Vinyl chloride NO NO u 0008 13-Butildlene NO NO u 0007 Bromomettlane NO NO u 0009 Chloroethane NO NO u 0009
Acetonitrile 0130 022 0024
Trlchlorcrfluoromethane 0263 lAB 0010 Aaylonltrile NO NP u 0012 11-DIChloroethene NO NO u 0009
Dldloromelhane NO NO u (IOlD
carbon Disulfide 0032 010 u 0033 T~hlo~fluonHdhane 0107 082 0011 tr~ns-12-0ichloroethyler~ NO NO u 0008 11-Dichloroethane ljO NO u 0008 Methl tert-Butyl Ether NO NO u 0008 Methyl Ethyl Ketone 0382 113 0157
Chloroprene NO NO u 0008 ciamp-12-0ichloroethylene NO NO u 0009 Bromochloromethane NO NO u 0008 011oroform NO NO u 0009 Ethyl tert-Butyl Ether NO NO u 0008 JI-Dichloroethilne NO NO u 0009 111-Trichloroethane NO NO u (l022
Benzene ozos 067 0029
Carbon Tetrachloride 0101 064 0024 tert-Amyl Methyl Ether NO NO u 1)016 12-DJChiOropropane NO NO u 0023 Ethyl Acrylate NO NO u (1 020
Bromodichloromethane NO NO u 0025 Trichloroethylene NO NO u 0025
Methyl Methacrylilte NO NO u 0022 cis-13-Dichloropropene NO NO u 0022 Methyl Isobutyl llteDM NCI NO u 0022 trans-13-0ichloropropene NO NO u 0025 112-Trldlloroetflane NO NO u 0025 Toluene 0095 036 0016 Olbromodloromelhane NO NO u 0021
Eastern Research Group The results 111 Jhis r~port apply only to the samplts waalylui in accordance with tht chain of custody document This cuuzlytical report must in reprod~~eed in its entirety
Page 11 of 16
CERTIFICATE OF ANALYSISRG EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 111 011 0903
Kansas City KS 66101 SUBMirrED OBiOB11 to 092911
ATTN~ M1chael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE ~ OECAw(irk
Description 150 west of Hwys 169 and 39 Lab ID 1091501-01 Sampled 091411 00 00
Pressure Receipt 13 Hg canister 709 Received 0915111042
Comments Analyzed 0915111926
Air Toxlcs by EPA Compendium Method T0-15 ~ MW
Analvte wmx uqm fli1g RRint 12-Dibromoethane ND IID u 0()18
n-Oddne ND ND u 0015
Tetrachloroethylene ND ND u 0018
Ollorobenzene ND ND u 0021
Ethylbenzene 0035 015 Q017
mpmiddotXylene 0041 018 0034
Bromoform ND NO 11 0025
Styrene NO ND u 002
11-22-Tetradlloroelhane ND ND u 0024
o-Xylene ND NO u 0018
135-Trimethylbenzene NO NO u 0026
124middotTrlrnathylbenzene 0-042 021 0028
m-Dichlorohenzene ND ND u 0034
Chloromethylbenzene ND ND u 0039
p-OIChlorobenzene NO NO u 0348
o-Dichlorobenzere NO NO u 0037
12+Trlchlorobenzene NO ND u 0036
Hexachloro-13-butadlene ND ND u 0037
Eastern Research Group The result in thrs reoort applgt ltmly to the samplts mral1zed m accordanc11 ~ith thilhain of custodgt document This am1lytical report m11st be rbullpmJuced ill it~ entirety
Page 12 of 16
CERTIFrCATE OF ANALYSIS
EPA Region VII FILE tl 027800001030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMITTED 080811 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Description 73 north of Oak St on Plummer Lab ID 1092909-01 Sampled 0928110000
Pressure 0 Receipt 65 Hg canister 140 Received 0929111057
Comments Analyzed 093011 20 34
Analyte
Acetylene middotPropylene
Dldllorodifluoromethane Chlolomettlane
Dlchlorotetrafluoroethllne VInyl chloride 13-Butadlene Bromometl1dne
Chloroethane
Acetunitrile Trldllorotluoromethane
Acrylonitrile
11-0ithloroethene Dichloromethane Carbon DisulfJde
Trlchlorotrlfkloroetftane lranr1 2-0khloroethylene
11-Dithloroelhane
Methyl tert-Butyl Ether Methyl Ethyl Ketone Chloroprene ds-1HllchloiJethylene Bromochloromethane Chlorofvnn
Ethyl tert-Butyl Ether 12-Dichloroethane 111middotTriChloroethane
Benzene carbon Tetrachloride tert-Amyl Methyl Ether 12-Didlonopropane Ethyl Acrylate Bromodlchlorornelhane Trichloroethylene
Methyl MetllacrylaJ
ds-13-Dithloropropene Methyl Isobutyl KetDne trans-13-0khlorapropene 112-Trichloroethane
Toluene Olbromochloromethane
Air Toxics by EPA Compendium Method T0-15 Results mL
ORb YIiID Eiilg I1IZD 223 238 016 123 212 0039
0564 280 0~11
0525 109 0012 0018 013 ooot
NO NO u 0008 0181 040 0~07
NO NO u o009 NO NO u 0009
0157 028 0024 ozgo 163 0010
NO NO u 0(112 NO NO u 0009
0154 054 0010 0045 0 14 0033 0092 071 0011
NO NO u 0008 NO NO u 0008 NO NO u 0~08
0624 184 0157 NO NO u 0008 NO NO u 0009 NO NO u 0008
0035 017 0009 NO NO u 0008 NO NO u 0009
0012 007 u 0022 L49 477 0029
0088 o56 0024 NO NO u 0016 ND NO u 0023 NO NO u 0020 NO ND u 0025
0178 096 0025
NO NO u 0022 NO NO u 0022
0094 039 0022 NO NO u 0025 NO NO u 0025
276 10400 D 0040 r~O NO u 0021
Eastern Research Group The results m this repon apply only to the samples cmolylld in accordance wilh the chain of cUStOdy docWMnt This arwlytlcal rJort mu~middott be reproduced in its entirety
Page 13 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMITTED 0808111 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECA wa1lt
Description 75 north of Oak St on Plummer Lab ID 1092909-01 Sampled 092811 0000
Pressure Receipt 65 Hg canister 140 Received 0929111057
Comments Analyzed 0930112034
Air Toxics by EPA Compendium Method T0-15 Results lmb
Analyte mmx ugm3 flil on 12-Dibromoethane NO NO u 0018
n-Octane 0193 090 0015 Tetrachloroethylene 0019 013 0018
Chlorobenzene NO NO u 0021
Ethyl benzene 0356 155 p017 mp-Xylene 1oamp 461 OOl4
Bromoform NO NO u 6025
Sty~Wte 0060 026 0022 lll2-Tetrachloroethane NO NO u 0-024
o-Xylene P422 184 01118 135-TrlmethylbenEene 0094 046 0026 1124-Trlmethylbenzene 0340 167 0028
m-Dichlorobenzene 0043 016 0034 Chloromethylbenzene NO NO u 0039
p-Dichlorobenzene 0019 011 u 0035
rDichlorobenzellE NO NO u 0037 121-Trochlorobenzene NO NO u 0-036
Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The ll$Ults in rhis repon appl) NIhbull to the samples analyted in accordance with the cham of custody document Thta analybullical rrporl must he reproduced in in entirety
Page 14 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII FILE tl 027800001 030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS66101 SUBMmED 080811 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX~ (913) 551-5000 SITE CODE OECAwork
IAnalyte Result Units SOurce Result RPD
RPD Umit Note
Eastern Research Group ~ resulu in this reprJrt apply oraly to the samples analyed 111 accordance with the chain of crutody docunumt 1his anulmcal report must be reprodu~ed In its enrlnty
Page 15 of 16
CERTIFICATE OF ANALYSISRG EPA Region VII FILEmiddot 027800001 030
300 Minnesota Avenue REPORTED 1110 11 09middot03
Kansas City KS 66101 SUBMITTED 08101311 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX~ (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
u Under Detection Umlt
o Th1s result obtained by dilution
ND Analyte NOT DETECTED at or above the Method Detecbon Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group T1r results in thH report apply on() w the sample tmayzed il occordancltt with the cham of bullur1ody dotumnt This anayllcai report must be prwiuced in its entirety
Page 16 of 16
~RG Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
December 05 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 111511 1121
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the amtract for NMOC UATMP PAMS CSATAM and NATTS support (US EPA Contract No EPD-09-D48) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please oontact me at 919-468-7930
Sincerely
Laura Van Enwyck Project Manager lauravanenwyckergcom
The information contained in this report and its attachment(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauraJnenwyckergcom and delete the report without retairring any copies
Page 1 of6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 120511 1059
Kansas City KS 66101 SUBMITTED 111511
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Lincoln amp 39 Highway 1111501-01 Air 111411 0000 111511 1121 (111 W Lincoln)
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wfth the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001030
REPORTED 120511 1059
SUBMITTED 111511
AQS SITE CODE
SITE CODE OECAwork
DesaiptionUncoln amp 39 Highway (111 W Uncoln) Lab ID 1111501-01 Sampled 111411 0000
Pressure Receipt 8 Hg canister 636 Received 1115111121
Comments Analyzed 111611 0932
Air Toxics by EPA Compendium Method T0-15 blulb lmL
Analvte Jmbx Yllm fiG JlRbl Acetylene 0171 018 A-Ql 0016 Propylene 0272 OA7 A-Ql 0039 Dlchlorodlfluoromethane 0503 2A9 A-Ql 0011 Chloromethane OA74 098 A-Ql 0011 Dichlorobtraftuoroethane 0016 011 A-Ql 0009 Vinyl chloride ND ND A-Ql U 0008 13-Buladlene 0020 004 A-Ql 0007 Bromomethane 0011 004 AmiddotOl 0009 Chloroethane ND ND A-Ql U 0009 Acetonitrile 0138 023 A-Ql 0024 Trichloroftuoromethane D304 L71 A-Ql 0010 Acrylonitrile ND ND A-Q1 U 0012
11-Dichloroethene ND ND A-Q1 U 0009 Dichloromethane 0266 093 A-Ql 0010 Carbon Disulfide 0129 040 A-Ql 0033 Trichlorotrifluoroethane 0079 061 A-Ql 0011 trans-12-0ichloroethylene ND ND A-Ql U 0008 11-Dichloroethane ND ND A-Ql U 0008 Methyl tert-Butyl Ether ND NO A-Q1 U 0008 Methyl Ethyl Ketone 0760 us AmiddotOl 0157 Chloroprene ND NO A-Ql U 0008
cis-12-Dichloroethylene NO NO A-Ql U 0009 Bromochloromethane NO NO A-Ql U 0008 Chloroform NO NO A-Ql U 0009
Ethyl tert-Butyl Ether NO NO Amiddot01 U 0008 12-Dichloroethane 0026 011 A-Ql 0009 111-Trichloroethane 0006 003 A-Q1 U 0022 Benzene 113 362 A-Q1 0029 Carbon Tetrachloride 0069 OA4 A-Q1 0024 tert-Amyl Methyl Ether ND ND A-Ql U 0016 12-Dichloropropane ND NO A-Ql U 0023
Ethyl Acrylate NO NO A-Ql U 0020
Bromodlchloromethane ND NO A-o1 u 0025 Trichloroethylene NO ND A-01 U 0025
Methyl Methacrylate ND NO A-Q1 U 0022 cis-13-Dichloropropene NO NO A-Ql U 0022 Methyl Isobutyl Ketone 0047 019 A-Ql 0022 trans-13-Dichloropropene NO ND A-Q1 U 0025 112-Trichloroethane NO NO A-Q1 U 0025
Toluene 0661 250 A-01 0016 Dibromochloromethane NO ND A-Q1 U 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repoTt must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1210511 1059
Kansas City KS 66101 SUBMITTED 1115 11
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption Uncoln amp 39 Highway (111 W Lincoln) Lab ID 1111501-01 Sampled 111411 0000
Pressure Receipt 8 Hg canister 636 Received 1115111121
Comments Analyzed 111611 0932
Air Toxics by EPA Compendium Method T0-15 RuJID mL
AnaMe IU1bll ~ BiSl IU1bll 12-Dlbromoethane NO NO A-Ql U 0018
n-Oct3ne 0025 012 A-Ql 0015
Tetrachloroethylene 0016 011 A-Ql U 0018
Ollorobenzene NO NO A-Ql U 0021
Ethylbenzene 0068 030 A-Ql 0017
mp-Xylene 0144 063 A-Ql 0034
Bromoform NO NO A-Ql U 0025
Styrene 0058 025 A-Ql 0022
1122-Tetrachloroethane NO NO A-Ql U 0024
o-Xylene 0058 025 A-ol 0018
135-Trlmetflylbenzene 0050 025 A-01 0026
124-Trimetflylbenzene 0130 064 A-Ql 0028
m-Dichlorobenzene NO NO A-Ql U 0034
Chloromelhylbenzene NO NO A-ol U 0039
p-Oichlorobenzene 0027 016 A-Ql U 0035
o-Oichlorobenzene NO NO A-Ql U 0037
124-Trichlorobenzene NO NO A-ol U 0036
Hexachloro-13-butadiene NO NO A-ol U 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 120511 1059
Kansas City KS 66101 SUBMITTED 111511
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance witlz tlze chain of custody documellt This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1205111 1 059
Kansas City KS 66101 SUBMITTED 11151 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
A-ol Estimated value due to possible canister leak
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical re-port must be reproduced in its entirety
Page 6 of 6
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
December 15 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 1206111229
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for NMOC UATMP PAMS CSATAM and NATTS support (US EPA Contract No EPD-09-048) This rover page is an integral part of this report and any exceptions or oomments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Project Manager lauravanenwyckergcom
The information contained in this report and its attachment(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify laura vanenwyck ergcom and delete the report without retaining any copies
Page 1 of 6
RG CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111 1041
Kansas City KS 66101 SUBMITTED 1206 11
ATTN Michael F Davis AQS SITE CODE
PHONE 913) 551-5042 FAX 913) 551-5000 SITE CODE OECAwork
ANALYTlCAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Ash amp Forest SE Corner 1120611-01 Air 120411 0000 120611 1229
middotI I
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytirol repon must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
ALE 027800001030
REPORTED 1215111041
SUBMmED 1210611
AQS SITE CODE
SITE CODE OECAwork
Desaiptlon Ash amp Forest SE Comer Lab ID 1120611-01 sampled 120411 oooo Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 BuYltl MQL
AnaMe IUlllll lWm Bag IUlllll Acetylene OA36 OA7 0016 Propylene 0304 052 0039 Dichlorodiftuoromethane 0567 281 0011 Chloromethane 0566 117 0012 Dlchlorotetnlftuoroethane 0019 013 0009 Vinyl chloride NO NO u 0008 13-Butadiene NO NO u 0007 Bromomethane 0012 005 0009 Chloroethane NO NO u 0009 Acetonitrile 0111 019 0024 Trichlorofluoromethane 0284 160 0010 Aaylonitrile ND NO u 0012 11-Dichloroethene ND ND u 0009 Dichloromethane 0083 029 0010 Carbon Disulfide 0019 006 u 0033
Trlchlorotrlftuoroethane 0099 076 0011 trans-12-Dichloroethylene ND ND u 0008 11-Dichloroethane ND NO u 0008 Methyl tert-Butyl Ether NO NO u 0008 Methyl Ethyl Ketone 0536 158 0157 Chloroprene NO NO u 0008 cis-12-Dichloroethylene NO ND u 0009 Bromochloromethane NO NO u 0008 Chloroform 0022 011 0009 Ethyl tert-Butyl Ether NO NO u 0008 12-Dichloroethane 0025 010 0009 111-Trichloroethane 0011 006 u 0022 Benzene 0188 060 0029 carbon Tetrachloride 0106 067 0024 tert-Amyl Methyl Ether NO NO u 0016 12-Dichloropropane NO NO u 0023 Ethyl Acrylate ND NO u 0020
Bromodichloromethane NO NO u 0025 Trichloroethylene NO NO u 0025 Methyl Methacrylate NO NO u 0022 cis-13-Dichloropropene NO NO u 0022
Methyl Isobutyl Ketone 0042 017 0022 trans-13-Dichloropropene ND NO u 0025 112-Trichloroethane NO NO u 0025
Toluene 0149 056 0016 Oibromochloromethane 0003 003 u 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproducedin its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 121511 1041
Kansas City KS 66101 SUBMmED 1210611
ATTN Michael F Davis AQS SITE CODE
PHONE (913 551-5042 FAX (913 551-5000 SITE CODE OECAwork
Description Ash amp Forest SE Comer Lab ID 1120611-01 Sampled 120411 0000
Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 llWdtl MID
Analyte ubll IUllm Bag ubll 12-0ibromoethane NO NO u 0018 nmiddotOctane 0044 021 0015 Tetrachloroethylene 0006 004 u 0018
Chlorobenzene NO NO u 0021 Ethylbenzene 0047 021 0017 mp-Xylene 0070 031 0034 Bromoform NO NO u 0025 Styrene 0034 015 0022 1122-Tetrachloroethane NO NO u 0024 o-Xylene 0036 016 0018 135-Trlmethylbenzene 0025 012 u 0026 124-Trlmetllylbenzene 0047 023 0028 m-Oichlorobenzene NO NO u 0034
Chloromethylbenzene NO NO u 0039 p-Dichlorcbenzene 0005 003 u 0348 a-Dichlorobenzene NO NO u 0037
124-Trlchlorobenzene NO NO u 0036 Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repon must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS~RG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 66101 SUBMITTED 12061 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPDIAnalyte Result Units Result RPD um1t Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 661 01 SUBMITTED 120611
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its enJirety
Page 6 of 6
i
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
March 12 2012
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 030512 0916
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for UATMP NATTS CSATAM PAMS and NMOC support (US EPA Contract No 68-D-Q9-048) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Program Manager lauravanenwyckergcom
The information contained in this report and its attachmcnt(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauravanenwyckergcom and delete the report dthout retaining any copies
Page 1 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 0312112 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
6th St between Central amp 2030501-01 Air 030212 0000 030512 0916 Malcom
Eastern Research Group The results in this report apply only to the samples anal zed in accordance With the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Aven ue REPORTED 031212 1 051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 ~ tml
Analvte RRbll Y9lD1 flu RRbll Acetylene 0627 067 0072 Propylene 0484 084 0033
Dichlorodllluoromethane 0500 248 0023 Chloromethane 0557 115 0033
Dichlorotetrafluoroethane 0015 011 0012 Vinyl chloride NO NO u 0011
13-Butadlene 0036 oo8 0011
Bromomethane 0012 005 0012 Chloroethane NO NO u 0017
Acetonitrile 0073 012 0073
Trichlorofluoromethane 0258 145 0015 Acrylonitrile NO NO u 0020
11-0ichloroethene NO NO u 0014
Dichloromethane 0185 064 0023
Carbon Disulfide 0037 012 0014 Trichlorobitluoroethane 0119 091 0017
trans-12-0ichloroethylene NO NO u 0012
11-0ichloroethane NO NO u 0015
Methyl tert-Butyl Ether NO NO u 0011
Chloroprene NO NO u 0012
ds-12-0ich loroethylene NO NO u OD18
Bromochloromethane NO NO u 0014
Chloroform NO ND u 0014
Ethyl tert-Butyl Ether NO NO u 0011
12-Dichloroethane 0019 008 0016
111-Trichloroethane 0012 007 u 0020
Benzene 0344 L10 0061 Carbon Tetrachloride 0088 056 0024
tert-Amyl Methyl Ether NO NO u 0016
12-0ichloropropane ND NO u 0019
Ethyl Acrylate ND NO u 0014
Bromodichloromethane ND NO u 0021
Trichloroethylene NO ND u 0022
Methyl Methacrylate ND NO u 0025
ds-13-0ichloropropene NO NO u 0015
Methyl Isobutyl Ketone 0015 oo6 0015
trans-13-0ichloropropene NO ND u 0016
112-Trichloroethane NO NO u 0021
Toluene 0416 157 0045
Oibromochloromethane ND NO u 0018
12-0ibromoethane ND NO u 0017
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551 -5000
FILE 027800001030
REPORTED 0312 12 1051
SUBMITTED 030512
AQS SITE CODE
SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 Bwdtl MJlL
Analvte Jmbll Y9Lm Big Jmbx nmiddotOclane 0039 018 0020 Tetrachloroethylene 0005 003 u 0020
Chlorobenzene ND ND u 0025
Ethylbenzene 0045 020 0023 mp-Xylene 0112 OA9 0037 Bromoform ND ND u 0020
Styrene 0030 013 0024 1122-Tetrachloroethane ND ND u 0018
o-Xylene 0050 022 0020
135-Trimethylbenzene 0019 009 u 0022
124-Trimethylbenzene 0047 023 0025 m-Dichlorobenzene ND ND u 0024
p-Dichlorobenzene 0004 002 u 0019
a-Dichlorobenzene NO ND u 0021
124-Trichlorobenzene ND ND u 0022
Hexachloro-13-butadiene ND ND u 0022
Eastern Research Group The results in this report apply only 1o the samples analyzed in accordance with the chain of custody document This analytical rep ort must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 031212 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wilh the chain of custody document This analytical report must be reproduced in its enrirety
Page 5 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 03121121051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report nutst be reproduced in its entirety
Page 6 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F DaVIS
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001 030
REPORTED 111011 0903
SUBMITTED 080811 to 092911
AQS SITE CODE
SITE CODE OECAwork
Description Ash amp Forest Intersection Lab ID 1080801-01 sampled 080511 ooOO
Pressure Receipt 7 Hg canister 607 Received 080B11 0853
Comments Background Sample Analyzed 0809111226
Air Taxies by EPA Compendium Method T0-15 ampwdb MDL
Analvte DRin Yllm Elm ~ 12-Dlbromoethane NO NO u 0-018
n-Octane 0251 118 0015 Tetrachloroethylene NO NO u Ollld
Chlornbenzene NO NO u 0021
Etllylbenzene 0661 z88 0017
mp-xylene 202 879 0034
Bromoform NO NO u 0025
Styrene 0314 138 oou 1122-Tetrachloroethane NO NO u 0024
o-Xylene 0884 385 0018
135-Trlmethylbenzene 02Z8 111 0016
124-Trimethylbenzene 0873 430 0018
m-DichlorobenzenP NO NO u 0034
Chlllromethylbenzene NO NO u 0039
p-Dkhlorobenzene ND ND u 0035
o-OichlorobtnzEne NO NO u 0037
124-Trichlorobenzene ND NO u 0036
Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The bullbulljults in this rtpqrt appty onlgt to the Sltanpl~ m1alyzod 111 accordQIICe with the chain of cuSI(Jdy docunumt 11ti~ dllQytical report nuISI be rf)roduted i11 its entirety
Page 4 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 111011 09middot03
Kansas City KS 66101 SUBMITTED 0810811 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Description Ash amp Forest Intersection Lab ID 1080909-01 Sampled 080611 0000
Pressure 0 Receipt 65 Hg Canister 401 Received 080911 1120
Comments Background Sample Analyzed 0809112309
Air Toxics by EPA Compendium Method T0-15 Results MJU
AnaMe ~ liILm flu ~ Acetylene 0421 045 0016 lropylene 03151 055 00351
Dlchlorodlfluoromethane 0753 373 oou Chloromethane 0752 156 0012 Dldllorotetrafluoraethane 0023 016 00051 Vinyl chloride NO NO u ooos 13-Butadlene 0034 008 0007
Bromametune 0011 007 0~9
Ollarollhane NO NO u 0009
Aaltllnitrile 0270 045 0024
Trlchlorafluorometllane 0313 L76 0010
Auvlonitrile NO NO u 0012
11-0ichloiIEllllene NO NO u 01)09 Dlchlorormithane 0123 OA3 0010
Carbon DISulfide OOS9 028 0033 TriChlorotrlfiUDroethene 0122 094 0011
trans-12-0ichloroethylene NO NO u OOOB U-Dichloroethane NO NO u 00()8 Methyl tert-Butyl Ether NO NO u OOOB Methyl Ethyl Ketone 06051 180 0157 Olloroprene NO NO u OOOB ci5-1Hlichloroethylene NO NO u 0009
Bromochloromethane NO NO u OOOB
Chloroform 0027 013 0009
Eth-(1 tert-Butyl Ether NO NO u OOOB
12-0ichlorothane ND NO u ooog 111-Trichloroethane 00~3 007 u 0022
Benzene 0210 067 0029
~rbon Tetrbullchloride 0132 083 0024 tert-Amyf Melt1yl Ether NO NO u 0016
12-0lChloroptcpane NO NO u 0023
Ethyl Aaylate NO NO u 0020
Bromodichloromethane NO NO u 0025
Trlchloroetbylene NO NO u 0025
Methyl Methacrylate NO NO u 0022
cis-1J-Oichloropropene ND NO u 0022
Methyl Isobutyl Ketone 0040 016 0022
trans-13-Dichloropropene NO NO u 0025
112-Tnchloroethane NO NO u 0025
TDIUIHie 0334 126 0016
Olbromochloromethane NO NO u 0021
Eastern Research Group Th~ r~sults in tins report apoly only ro the sanrptes fDiaylted in accordance With the chain of Cltstody doc11ment 111is mwlylicalnport muft be reproduced in Its enttrtty
Page 5 of 16
RG CERTIFICATE OF ANALYSIS
EPA Reg1on VII FILE 027800001030
300 Minnesota Avenue REPORTED 1111011 0903
Kansas City KS 66101 SUBMITTED 0808111 to 092911
ATTN Michael F DaviS AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption Ash amp Forest Intersection Lab ID 1080909-01 Sampled 080611 0000
Pressure Receipt 65 Hg Canister 401 Received 0809111120
Comments Background Sample Analyzed 080911 2309
Air Toxics by EPA Compendium Method T0-15 Results lmL
Analvte JmiDt Y9Lm flu Jmbx 12-Dibromoethane ND ND u 0018
n-Ociane 0039 018 0015
Tetrachloroethylene ND NO 0018u
Oilorobenzene ND NO u 0021
Ethyl benzene 0074 032 0017
mp-Xylene ()140 061 0034
Bromoform NO NO u 0025
Styrene 0034 015 0022
1122-Tetrachloroethane NO NO u 0024
o-Xylene 0067 029 0018
135-Trimethylbenane 0031 015 0026
124-Trimethylbenzene 0078 038 0028
m-Dichlorobanzene NO NO 0031u Ollcromethylbenzene ND ND u 0039
p-Dichlorobenzene NO NO 0-035u o-Dichlorobemenl ND ND u 0037
12+Trichlorobenzene NO NO 0036u Hexachlnro-13-butadiene ND NO 0037u
Eastern Research Group lhtJ resutu in thrs r~~porl apply tmly io tht ronrpler onaly~d in accordanc6 wrth the chain of curtoay dOIumelll This analytical report mllSt ~ reprfJduccd rn its lntirety
Page 6 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN~ Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001 030
REPORTEDmiddot 111011 0903
SUBMITIED 080811 tci 092911
AQS SITE CODE
SITE CODE OECAwork
Description Ash amp Forest Intersection Lab ID 1082901-01 Sampled 082611 oomiddotoo Pressure Receipt 8 Hg canister 020 Received 082911 0948
COmments Background Sample Analyzed 083011 0036
Air Taxies by EPA Compendium Method T0-15 Results MnL
Analvte mmx Y9lm fml ~ Acetylene 0A94 053 0016 Propylena OA34 o7s 0039 Dlchlorocllrluoromllthane 0553 274 0011 chloR)IIIIIthane 0604 125 0012 Dldlorollltniftuoroethane 0024 017 0009 VInyl dlorlde 0008 002 opoa 13-Butadlene 0028 0 06 op01 Bromomethane 0016 006 0009
Olloroethane NO NO u 0009 Aatonitrila 0217 037 0024 Tr1dtlorofluorometllane 0211 164 0010
Aaylonltrile NO NO u 0012
11-Didlloroethene NO NO u 0009
Dlchloromethane 0404 141 0010 carbon Disulfide 0161 0 50 0033 Trldlorotrlfluoroethane 0117 otO 0011 trans-12-0khloroeth~ene NO NO u ooos 11-0ichloroethane NO NO u 0008
Methyl tPrt-sutvt Ether NO NO u 0008
Methyl Ethyl Ketone 111 328 0157
Chloroprene ND NO u 0008 ds-12-Dichloroethvlent NO NO u 0009
Bromochloromethane NO NO u 0008
Chlororgtnn 0043 021 0001
Ethyl tert-iutyl Ether NO ND u 0008 12middotDichloroethene 0030 012 0001 111middot TriChloroethane 0018 010 u op22
Benzene 0225 072 OOZ9
Carbon Tetrachloride 0098 0amp2 Op24
tert-Amyl Methyl Ether ND NO u 0016
12-0ichloropropane NO NO u 0023
Ethyl Acrylate ND NO u 0020
Bromod1chloromethane 0011 007 u 0025
Trichloroethylene 0 015 008 U 0025
Methyl Methaaylate NO NO u 0022
ds-13-0idlloropropene NO NO u 0022
Methyl Isobutyl Ketone 0052 021 0022
trans-13-0ichloropropene ND NO u 0025
112middot Tnrhloroethane ND NO u 0025
Toluene 514 1940 0016
Olbromochloromethane 0008 007 u 0021
Eastern Research Group lh~ results in this report apply only to the sample 011alyud in accordance with tht rhain of cusrody documtmr This OJialytlcal nport musliM -Produced in its mirery
Page 7 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN~ Michael F DaviS
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001 030
REPORTED 111 Oi11 0903
SUBMITTED 08108111 to 092911
AQS SITE CODE
SITE CODE OECAwork
Description Ash amp Fcorest Intersection Lab ID 1082901-01 Sampled 082611 0000
Pressure I Receipt 8 Hg Canister 020 Received 082911 09~48
Comments Background Sample Analyzed 083011 0036
Air Toxics by EPA Compendium Method T0-15 Results MW
Anayte DDIn Y9lm Eiim IU2bll 12-Dibromoethane NO ND u 0018
n-Ocblne 0074 035 0015
Ttrachloroethylene 0026 018 0018
Chlorobenzene ND ND u 0021
Ethylbenzene 0218 0-95 0017
mp-Xylene 0551 2AO 0034
Bromoform ND ND u (105
Styrene 0089 038 0022
1122-Tetrachloroethane 0010 0 07 u 0024
a-Xylene 0189 082 0018
135-Trlmethylbenzene 0062 031 0026
124-Trimethylbenzene 0150 074 0028
m-Dichlorobenzene 0006 004 u 0034
Chloromethylbenzene NO ND u 0039
p-Dichlorobenzene 0032 019 u 0348
o-Ochlorobenzene 0006 004 u 0037
124-Trlchlorobenzene 1110 NO u 0036
Hexachloro-13-bullldlene 0008 009 u 0037
Eastern Research Group Tlze bullesuJs m this repon apply on)middot to the sanrpfamp nnalyud ill acordance wh lht chain of custody Joumumt Thi~ OIIOI)middottical report musbull be teptoJduced In its elltiJtty
Page 8 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMilTED 0808111 to 0929111
ATTN Michael F Davts AQS SITE CODE
PHONE 913) 551-5042 FAX (913) 551middot5000 SITE CODE OECAwork
Description 4th and Santa Fe Lab ID 1090818-01 Sampled 090711 0000
Pressure 0 Receipt 6 5 Hg Canister EROOB Received 0908111247
Comments Analyzed 090911 0137
AirToxics by EPA Compendium Method T0-15 BciYlb MQI
Analyte lUlblpound usLm fOOl ~ Acetylene 0175 029 0016 Propylene 0333 057 op39 Dichlorodifluoromethane 0521 258 0011 Chloromethane 0507 LOS oou Okhlorotetrafluoroeihane NO NO u 0009
Vinyl chloride NO NO u OOilll 13-Butadlene NO NO u 0007
Bromomethane NO NO u 0009 Chloroethane NO NO u 0009 AletDnibile 0122 021 0024
Tr1dlloroftuoromethane 0252 142 0010 Acrylonlbile NO NO u 0012 11-0ldlloroethPne NO NO u 0009 Dldlloromethane 0159 055 0010
Carbon Disulfide 0063 020 0033 Trlchlorotrlfluoroethane 0094 072 OJ11
trans-12-Dichloroethylene NO NO u 0008
11-0lchloroethane NO NO u ouoa Methyl tert-BlJtyl Ether NO NO u o~
Ne~IEthyiKetone 0472 139 0157 Chloroprene NO NO u 0008
ds-12-Dichloroethylene NO NO u 0109
Bromochloromethane NO NO u oooa Chlorofomi NO NO u 0009 Ethyl ~Butyl Ether NO NO u 0008
12-Didlloroethane NO NO u 0009
111middot Trtdlloroethane NO NO u 0022
Benzene 0168 054 0029 Carbon Telrldllorlde 0095 oeo 0024
tertmiddotAmyl Methyl Ether NO NO u 0016
12-0Chlolgtpropane NO ND u 0023
ethyl Acrtlate NO NO u 0020
Bromodichloromethane NO NO u OOlS Trichloroethylene ND NO u 0025
MettwiMethacrylate NO NO u oc22 cis-13-0ichloropropene NO NO u 0022
~yiiiObutyiKetone 0035 014 0022
trans-13-0ichloropropene NO NO u oo2S 112middot Trichloroethane NO NO u 0025
Toluene 0373 141 0016
OibromQchloromethane NO NO u 0071
Eastern Research Group The nsults in this nport apply only to the saltlples D11alyzed in acordance with the chain Df cuampmiddottody docWMnt This analytical rttport must be repriJduced in its elllirety
Page 9 of 16
RG CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMIITED 080811 to 09291 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 4th and Santa Fe Lab ID 1090818-01 Sampled 090711 0000
Pressure Receipt 65 Hg canister ER008 Received 09081112~47
Comments Analyzed 090911 0137
Air Toxics by EPA Compendium Method T0-15 Results tmL
Analvte IUllm ll9lm flil Jmbll 12-0ibromoethane NO NO u 0018
n-Octane 0038 018 0015
Tetradiloroethylene ND NO u 0018 Chlomhenllne NO NO u 002
Ethyl benzene 0064 028 0017
mp-Xylene 0148 064 0034
Bromoform NO NO u 0025
Styrene NO NO u 0022
1122-TlliiChloroetllane NO NO u 0021
omiddotXylene 0070 031 0018
135middotTrimethylbenzene ND NO u 0026
124-Trimethylbenzene 0078 038 0028
m-Oiehlorobenzene NO NO u 0034
Chloromethylbenzene NO NO u 0019
p-Orchlorobenzene ND NO u 0348
o-Oidllorobenzene ND NO u 0037
124-Trichlorobenzene NO NO u 0036
Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The results rn Jhis teport apply cmJy 10 the samples (Uraly~ed in ac~ordant-e wilh the chain of CIISiody docunum This atwlytiral report 11111s1 be reprculuced i11 ils e11tirrty
Page 10 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN MIChael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001 030
REPORTED~ 1110111 0903
SUBMmED 0810811 to 092911
AQS SITE CODE
SITE CODE OECAwork
Description 150 west of Hwys 169 and 39 Lab ID 1091501-01 sampled 091411 oooo Pressure 0 ReClelpt 13 Hg canister 709 Received 091511 10~42
Comments Analyzed 0915111926
Air Taxies by EPA Compendium Method T0-15 BHIIIm MDI
Analyte JUlbll li9Lm fJJg JlRinl AcBtylene 0234 025 0-016 Propylene 0258 045 0-0~11
Dlchlorodlfluoromettmne 0544 270 oo11 Chloromethane 0526 109 0 012
DichlorolelrifAJoroethane NO NO u Otgt09 Vinyl chloride NO NO u 0008 13-Butildlene NO NO u 0007 Bromomettlane NO NO u 0009 Chloroethane NO NO u 0009
Acetonitrile 0130 022 0024
Trlchlorcrfluoromethane 0263 lAB 0010 Aaylonltrile NO NP u 0012 11-DIChloroethene NO NO u 0009
Dldloromelhane NO NO u (IOlD
carbon Disulfide 0032 010 u 0033 T~hlo~fluonHdhane 0107 082 0011 tr~ns-12-0ichloroethyler~ NO NO u 0008 11-Dichloroethane ljO NO u 0008 Methl tert-Butyl Ether NO NO u 0008 Methyl Ethyl Ketone 0382 113 0157
Chloroprene NO NO u 0008 ciamp-12-0ichloroethylene NO NO u 0009 Bromochloromethane NO NO u 0008 011oroform NO NO u 0009 Ethyl tert-Butyl Ether NO NO u 0008 JI-Dichloroethilne NO NO u 0009 111-Trichloroethane NO NO u (l022
Benzene ozos 067 0029
Carbon Tetrachloride 0101 064 0024 tert-Amyl Methyl Ether NO NO u 1)016 12-DJChiOropropane NO NO u 0023 Ethyl Acrylate NO NO u (1 020
Bromodichloromethane NO NO u 0025 Trichloroethylene NO NO u 0025
Methyl Methacrylilte NO NO u 0022 cis-13-Dichloropropene NO NO u 0022 Methyl Isobutyl llteDM NCI NO u 0022 trans-13-0ichloropropene NO NO u 0025 112-Trldlloroetflane NO NO u 0025 Toluene 0095 036 0016 Olbromodloromelhane NO NO u 0021
Eastern Research Group The results 111 Jhis r~port apply only to the samplts waalylui in accordance with tht chain of custody document This cuuzlytical report must in reprod~~eed in its entirety
Page 11 of 16
CERTIFICATE OF ANALYSISRG EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 111 011 0903
Kansas City KS 66101 SUBMirrED OBiOB11 to 092911
ATTN~ M1chael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE ~ OECAw(irk
Description 150 west of Hwys 169 and 39 Lab ID 1091501-01 Sampled 091411 00 00
Pressure Receipt 13 Hg canister 709 Received 0915111042
Comments Analyzed 0915111926
Air Toxlcs by EPA Compendium Method T0-15 ~ MW
Analvte wmx uqm fli1g RRint 12-Dibromoethane ND IID u 0()18
n-Oddne ND ND u 0015
Tetrachloroethylene ND ND u 0018
Ollorobenzene ND ND u 0021
Ethylbenzene 0035 015 Q017
mpmiddotXylene 0041 018 0034
Bromoform ND NO 11 0025
Styrene NO ND u 002
11-22-Tetradlloroelhane ND ND u 0024
o-Xylene ND NO u 0018
135-Trimethylbenzene NO NO u 0026
124middotTrlrnathylbenzene 0-042 021 0028
m-Dichlorohenzene ND ND u 0034
Chloromethylbenzene ND ND u 0039
p-OIChlorobenzene NO NO u 0348
o-Dichlorobenzere NO NO u 0037
12+Trlchlorobenzene NO ND u 0036
Hexachloro-13-butadlene ND ND u 0037
Eastern Research Group The result in thrs reoort applgt ltmly to the samplts mral1zed m accordanc11 ~ith thilhain of custodgt document This am1lytical report m11st be rbullpmJuced ill it~ entirety
Page 12 of 16
CERTIFrCATE OF ANALYSIS
EPA Region VII FILE tl 027800001030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMITTED 080811 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Description 73 north of Oak St on Plummer Lab ID 1092909-01 Sampled 0928110000
Pressure 0 Receipt 65 Hg canister 140 Received 0929111057
Comments Analyzed 093011 20 34
Analyte
Acetylene middotPropylene
Dldllorodifluoromethane Chlolomettlane
Dlchlorotetrafluoroethllne VInyl chloride 13-Butadlene Bromometl1dne
Chloroethane
Acetunitrile Trldllorotluoromethane
Acrylonitrile
11-0ithloroethene Dichloromethane Carbon DisulfJde
Trlchlorotrlfkloroetftane lranr1 2-0khloroethylene
11-Dithloroelhane
Methyl tert-Butyl Ether Methyl Ethyl Ketone Chloroprene ds-1HllchloiJethylene Bromochloromethane Chlorofvnn
Ethyl tert-Butyl Ether 12-Dichloroethane 111middotTriChloroethane
Benzene carbon Tetrachloride tert-Amyl Methyl Ether 12-Didlonopropane Ethyl Acrylate Bromodlchlorornelhane Trichloroethylene
Methyl MetllacrylaJ
ds-13-Dithloropropene Methyl Isobutyl KetDne trans-13-0khlorapropene 112-Trichloroethane
Toluene Olbromochloromethane
Air Toxics by EPA Compendium Method T0-15 Results mL
ORb YIiID Eiilg I1IZD 223 238 016 123 212 0039
0564 280 0~11
0525 109 0012 0018 013 ooot
NO NO u 0008 0181 040 0~07
NO NO u o009 NO NO u 0009
0157 028 0024 ozgo 163 0010
NO NO u 0(112 NO NO u 0009
0154 054 0010 0045 0 14 0033 0092 071 0011
NO NO u 0008 NO NO u 0008 NO NO u 0~08
0624 184 0157 NO NO u 0008 NO NO u 0009 NO NO u 0008
0035 017 0009 NO NO u 0008 NO NO u 0009
0012 007 u 0022 L49 477 0029
0088 o56 0024 NO NO u 0016 ND NO u 0023 NO NO u 0020 NO ND u 0025
0178 096 0025
NO NO u 0022 NO NO u 0022
0094 039 0022 NO NO u 0025 NO NO u 0025
276 10400 D 0040 r~O NO u 0021
Eastern Research Group The results m this repon apply only to the samples cmolylld in accordance wilh the chain of cUStOdy docWMnt This arwlytlcal rJort mu~middott be reproduced in its entirety
Page 13 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMITTED 0808111 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECA wa1lt
Description 75 north of Oak St on Plummer Lab ID 1092909-01 Sampled 092811 0000
Pressure Receipt 65 Hg canister 140 Received 0929111057
Comments Analyzed 0930112034
Air Toxics by EPA Compendium Method T0-15 Results lmb
Analyte mmx ugm3 flil on 12-Dibromoethane NO NO u 0018
n-Octane 0193 090 0015 Tetrachloroethylene 0019 013 0018
Chlorobenzene NO NO u 0021
Ethyl benzene 0356 155 p017 mp-Xylene 1oamp 461 OOl4
Bromoform NO NO u 6025
Sty~Wte 0060 026 0022 lll2-Tetrachloroethane NO NO u 0-024
o-Xylene P422 184 01118 135-TrlmethylbenEene 0094 046 0026 1124-Trlmethylbenzene 0340 167 0028
m-Dichlorobenzene 0043 016 0034 Chloromethylbenzene NO NO u 0039
p-Dichlorobenzene 0019 011 u 0035
rDichlorobenzellE NO NO u 0037 121-Trochlorobenzene NO NO u 0-036
Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The ll$Ults in rhis repon appl) NIhbull to the samples analyted in accordance with the cham of custody document Thta analybullical rrporl must he reproduced in in entirety
Page 14 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII FILE tl 027800001 030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS66101 SUBMmED 080811 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX~ (913) 551-5000 SITE CODE OECAwork
IAnalyte Result Units SOurce Result RPD
RPD Umit Note
Eastern Research Group ~ resulu in this reprJrt apply oraly to the samples analyed 111 accordance with the chain of crutody docunumt 1his anulmcal report must be reprodu~ed In its enrlnty
Page 15 of 16
CERTIFICATE OF ANALYSISRG EPA Region VII FILEmiddot 027800001 030
300 Minnesota Avenue REPORTED 1110 11 09middot03
Kansas City KS 66101 SUBMITTED 08101311 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX~ (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
u Under Detection Umlt
o Th1s result obtained by dilution
ND Analyte NOT DETECTED at or above the Method Detecbon Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group T1r results in thH report apply on() w the sample tmayzed il occordancltt with the cham of bullur1ody dotumnt This anayllcai report must be prwiuced in its entirety
Page 16 of 16
~RG Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
December 05 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 111511 1121
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the amtract for NMOC UATMP PAMS CSATAM and NATTS support (US EPA Contract No EPD-09-D48) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please oontact me at 919-468-7930
Sincerely
Laura Van Enwyck Project Manager lauravanenwyckergcom
The information contained in this report and its attachment(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauraJnenwyckergcom and delete the report without retairring any copies
Page 1 of6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 120511 1059
Kansas City KS 66101 SUBMITTED 111511
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Lincoln amp 39 Highway 1111501-01 Air 111411 0000 111511 1121 (111 W Lincoln)
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wfth the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001030
REPORTED 120511 1059
SUBMITTED 111511
AQS SITE CODE
SITE CODE OECAwork
DesaiptionUncoln amp 39 Highway (111 W Uncoln) Lab ID 1111501-01 Sampled 111411 0000
Pressure Receipt 8 Hg canister 636 Received 1115111121
Comments Analyzed 111611 0932
Air Toxics by EPA Compendium Method T0-15 blulb lmL
Analvte Jmbx Yllm fiG JlRbl Acetylene 0171 018 A-Ql 0016 Propylene 0272 OA7 A-Ql 0039 Dlchlorodlfluoromethane 0503 2A9 A-Ql 0011 Chloromethane OA74 098 A-Ql 0011 Dichlorobtraftuoroethane 0016 011 A-Ql 0009 Vinyl chloride ND ND A-Ql U 0008 13-Buladlene 0020 004 A-Ql 0007 Bromomethane 0011 004 AmiddotOl 0009 Chloroethane ND ND A-Ql U 0009 Acetonitrile 0138 023 A-Ql 0024 Trichloroftuoromethane D304 L71 A-Ql 0010 Acrylonitrile ND ND A-Q1 U 0012
11-Dichloroethene ND ND A-Q1 U 0009 Dichloromethane 0266 093 A-Ql 0010 Carbon Disulfide 0129 040 A-Ql 0033 Trichlorotrifluoroethane 0079 061 A-Ql 0011 trans-12-0ichloroethylene ND ND A-Ql U 0008 11-Dichloroethane ND ND A-Ql U 0008 Methyl tert-Butyl Ether ND NO A-Q1 U 0008 Methyl Ethyl Ketone 0760 us AmiddotOl 0157 Chloroprene ND NO A-Ql U 0008
cis-12-Dichloroethylene NO NO A-Ql U 0009 Bromochloromethane NO NO A-Ql U 0008 Chloroform NO NO A-Ql U 0009
Ethyl tert-Butyl Ether NO NO Amiddot01 U 0008 12-Dichloroethane 0026 011 A-Ql 0009 111-Trichloroethane 0006 003 A-Q1 U 0022 Benzene 113 362 A-Q1 0029 Carbon Tetrachloride 0069 OA4 A-Q1 0024 tert-Amyl Methyl Ether ND ND A-Ql U 0016 12-Dichloropropane ND NO A-Ql U 0023
Ethyl Acrylate NO NO A-Ql U 0020
Bromodlchloromethane ND NO A-o1 u 0025 Trichloroethylene NO ND A-01 U 0025
Methyl Methacrylate ND NO A-Q1 U 0022 cis-13-Dichloropropene NO NO A-Ql U 0022 Methyl Isobutyl Ketone 0047 019 A-Ql 0022 trans-13-Dichloropropene NO ND A-Q1 U 0025 112-Trichloroethane NO NO A-Q1 U 0025
Toluene 0661 250 A-01 0016 Dibromochloromethane NO ND A-Q1 U 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repoTt must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1210511 1059
Kansas City KS 66101 SUBMITTED 1115 11
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption Uncoln amp 39 Highway (111 W Lincoln) Lab ID 1111501-01 Sampled 111411 0000
Pressure Receipt 8 Hg canister 636 Received 1115111121
Comments Analyzed 111611 0932
Air Toxics by EPA Compendium Method T0-15 RuJID mL
AnaMe IU1bll ~ BiSl IU1bll 12-Dlbromoethane NO NO A-Ql U 0018
n-Oct3ne 0025 012 A-Ql 0015
Tetrachloroethylene 0016 011 A-Ql U 0018
Ollorobenzene NO NO A-Ql U 0021
Ethylbenzene 0068 030 A-Ql 0017
mp-Xylene 0144 063 A-Ql 0034
Bromoform NO NO A-Ql U 0025
Styrene 0058 025 A-Ql 0022
1122-Tetrachloroethane NO NO A-Ql U 0024
o-Xylene 0058 025 A-ol 0018
135-Trlmetflylbenzene 0050 025 A-01 0026
124-Trimetflylbenzene 0130 064 A-Ql 0028
m-Dichlorobenzene NO NO A-Ql U 0034
Chloromelhylbenzene NO NO A-ol U 0039
p-Oichlorobenzene 0027 016 A-Ql U 0035
o-Oichlorobenzene NO NO A-Ql U 0037
124-Trichlorobenzene NO NO A-ol U 0036
Hexachloro-13-butadiene NO NO A-ol U 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 120511 1059
Kansas City KS 66101 SUBMITTED 111511
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance witlz tlze chain of custody documellt This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1205111 1 059
Kansas City KS 66101 SUBMITTED 11151 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
A-ol Estimated value due to possible canister leak
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical re-port must be reproduced in its entirety
Page 6 of 6
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
December 15 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 1206111229
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for NMOC UATMP PAMS CSATAM and NATTS support (US EPA Contract No EPD-09-048) This rover page is an integral part of this report and any exceptions or oomments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Project Manager lauravanenwyckergcom
The information contained in this report and its attachment(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify laura vanenwyck ergcom and delete the report without retaining any copies
Page 1 of 6
RG CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111 1041
Kansas City KS 66101 SUBMITTED 1206 11
ATTN Michael F Davis AQS SITE CODE
PHONE 913) 551-5042 FAX 913) 551-5000 SITE CODE OECAwork
ANALYTlCAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Ash amp Forest SE Corner 1120611-01 Air 120411 0000 120611 1229
middotI I
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytirol repon must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
ALE 027800001030
REPORTED 1215111041
SUBMmED 1210611
AQS SITE CODE
SITE CODE OECAwork
Desaiptlon Ash amp Forest SE Comer Lab ID 1120611-01 sampled 120411 oooo Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 BuYltl MQL
AnaMe IUlllll lWm Bag IUlllll Acetylene OA36 OA7 0016 Propylene 0304 052 0039 Dichlorodiftuoromethane 0567 281 0011 Chloromethane 0566 117 0012 Dlchlorotetnlftuoroethane 0019 013 0009 Vinyl chloride NO NO u 0008 13-Butadiene NO NO u 0007 Bromomethane 0012 005 0009 Chloroethane NO NO u 0009 Acetonitrile 0111 019 0024 Trichlorofluoromethane 0284 160 0010 Aaylonitrile ND NO u 0012 11-Dichloroethene ND ND u 0009 Dichloromethane 0083 029 0010 Carbon Disulfide 0019 006 u 0033
Trlchlorotrlftuoroethane 0099 076 0011 trans-12-Dichloroethylene ND ND u 0008 11-Dichloroethane ND NO u 0008 Methyl tert-Butyl Ether NO NO u 0008 Methyl Ethyl Ketone 0536 158 0157 Chloroprene NO NO u 0008 cis-12-Dichloroethylene NO ND u 0009 Bromochloromethane NO NO u 0008 Chloroform 0022 011 0009 Ethyl tert-Butyl Ether NO NO u 0008 12-Dichloroethane 0025 010 0009 111-Trichloroethane 0011 006 u 0022 Benzene 0188 060 0029 carbon Tetrachloride 0106 067 0024 tert-Amyl Methyl Ether NO NO u 0016 12-Dichloropropane NO NO u 0023 Ethyl Acrylate ND NO u 0020
Bromodichloromethane NO NO u 0025 Trichloroethylene NO NO u 0025 Methyl Methacrylate NO NO u 0022 cis-13-Dichloropropene NO NO u 0022
Methyl Isobutyl Ketone 0042 017 0022 trans-13-Dichloropropene ND NO u 0025 112-Trichloroethane NO NO u 0025
Toluene 0149 056 0016 Oibromochloromethane 0003 003 u 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproducedin its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 121511 1041
Kansas City KS 66101 SUBMmED 1210611
ATTN Michael F Davis AQS SITE CODE
PHONE (913 551-5042 FAX (913 551-5000 SITE CODE OECAwork
Description Ash amp Forest SE Comer Lab ID 1120611-01 Sampled 120411 0000
Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 llWdtl MID
Analyte ubll IUllm Bag ubll 12-0ibromoethane NO NO u 0018 nmiddotOctane 0044 021 0015 Tetrachloroethylene 0006 004 u 0018
Chlorobenzene NO NO u 0021 Ethylbenzene 0047 021 0017 mp-Xylene 0070 031 0034 Bromoform NO NO u 0025 Styrene 0034 015 0022 1122-Tetrachloroethane NO NO u 0024 o-Xylene 0036 016 0018 135-Trlmethylbenzene 0025 012 u 0026 124-Trlmetllylbenzene 0047 023 0028 m-Oichlorobenzene NO NO u 0034
Chloromethylbenzene NO NO u 0039 p-Dichlorcbenzene 0005 003 u 0348 a-Dichlorobenzene NO NO u 0037
124-Trlchlorobenzene NO NO u 0036 Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repon must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS~RG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 66101 SUBMITTED 12061 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPDIAnalyte Result Units Result RPD um1t Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 661 01 SUBMITTED 120611
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its enJirety
Page 6 of 6
i
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
March 12 2012
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 030512 0916
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for UATMP NATTS CSATAM PAMS and NMOC support (US EPA Contract No 68-D-Q9-048) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Program Manager lauravanenwyckergcom
The information contained in this report and its attachmcnt(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauravanenwyckergcom and delete the report dthout retaining any copies
Page 1 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 0312112 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
6th St between Central amp 2030501-01 Air 030212 0000 030512 0916 Malcom
Eastern Research Group The results in this report apply only to the samples anal zed in accordance With the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Aven ue REPORTED 031212 1 051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 ~ tml
Analvte RRbll Y9lD1 flu RRbll Acetylene 0627 067 0072 Propylene 0484 084 0033
Dichlorodllluoromethane 0500 248 0023 Chloromethane 0557 115 0033
Dichlorotetrafluoroethane 0015 011 0012 Vinyl chloride NO NO u 0011
13-Butadlene 0036 oo8 0011
Bromomethane 0012 005 0012 Chloroethane NO NO u 0017
Acetonitrile 0073 012 0073
Trichlorofluoromethane 0258 145 0015 Acrylonitrile NO NO u 0020
11-0ichloroethene NO NO u 0014
Dichloromethane 0185 064 0023
Carbon Disulfide 0037 012 0014 Trichlorobitluoroethane 0119 091 0017
trans-12-0ichloroethylene NO NO u 0012
11-0ichloroethane NO NO u 0015
Methyl tert-Butyl Ether NO NO u 0011
Chloroprene NO NO u 0012
ds-12-0ich loroethylene NO NO u OD18
Bromochloromethane NO NO u 0014
Chloroform NO ND u 0014
Ethyl tert-Butyl Ether NO NO u 0011
12-Dichloroethane 0019 008 0016
111-Trichloroethane 0012 007 u 0020
Benzene 0344 L10 0061 Carbon Tetrachloride 0088 056 0024
tert-Amyl Methyl Ether NO NO u 0016
12-0ichloropropane ND NO u 0019
Ethyl Acrylate ND NO u 0014
Bromodichloromethane ND NO u 0021
Trichloroethylene NO ND u 0022
Methyl Methacrylate ND NO u 0025
ds-13-0ichloropropene NO NO u 0015
Methyl Isobutyl Ketone 0015 oo6 0015
trans-13-0ichloropropene NO ND u 0016
112-Trichloroethane NO NO u 0021
Toluene 0416 157 0045
Oibromochloromethane ND NO u 0018
12-0ibromoethane ND NO u 0017
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551 -5000
FILE 027800001030
REPORTED 0312 12 1051
SUBMITTED 030512
AQS SITE CODE
SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 Bwdtl MJlL
Analvte Jmbll Y9Lm Big Jmbx nmiddotOclane 0039 018 0020 Tetrachloroethylene 0005 003 u 0020
Chlorobenzene ND ND u 0025
Ethylbenzene 0045 020 0023 mp-Xylene 0112 OA9 0037 Bromoform ND ND u 0020
Styrene 0030 013 0024 1122-Tetrachloroethane ND ND u 0018
o-Xylene 0050 022 0020
135-Trimethylbenzene 0019 009 u 0022
124-Trimethylbenzene 0047 023 0025 m-Dichlorobenzene ND ND u 0024
p-Dichlorobenzene 0004 002 u 0019
a-Dichlorobenzene NO ND u 0021
124-Trichlorobenzene ND ND u 0022
Hexachloro-13-butadiene ND ND u 0022
Eastern Research Group The results in this report apply only 1o the samples analyzed in accordance with the chain of custody document This analytical rep ort must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 031212 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wilh the chain of custody document This analytical report must be reproduced in its enrirety
Page 5 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 03121121051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report nutst be reproduced in its entirety
Page 6 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 111011 09middot03
Kansas City KS 66101 SUBMITTED 0810811 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Description Ash amp Forest Intersection Lab ID 1080909-01 Sampled 080611 0000
Pressure 0 Receipt 65 Hg Canister 401 Received 080911 1120
Comments Background Sample Analyzed 0809112309
Air Toxics by EPA Compendium Method T0-15 Results MJU
AnaMe ~ liILm flu ~ Acetylene 0421 045 0016 lropylene 03151 055 00351
Dlchlorodlfluoromethane 0753 373 oou Chloromethane 0752 156 0012 Dldllorotetrafluoraethane 0023 016 00051 Vinyl chloride NO NO u ooos 13-Butadlene 0034 008 0007
Bromametune 0011 007 0~9
Ollarollhane NO NO u 0009
Aaltllnitrile 0270 045 0024
Trlchlorafluorometllane 0313 L76 0010
Auvlonitrile NO NO u 0012
11-0ichloiIEllllene NO NO u 01)09 Dlchlorormithane 0123 OA3 0010
Carbon DISulfide OOS9 028 0033 TriChlorotrlfiUDroethene 0122 094 0011
trans-12-0ichloroethylene NO NO u OOOB U-Dichloroethane NO NO u 00()8 Methyl tert-Butyl Ether NO NO u OOOB Methyl Ethyl Ketone 06051 180 0157 Olloroprene NO NO u OOOB ci5-1Hlichloroethylene NO NO u 0009
Bromochloromethane NO NO u OOOB
Chloroform 0027 013 0009
Eth-(1 tert-Butyl Ether NO NO u OOOB
12-0ichlorothane ND NO u ooog 111-Trichloroethane 00~3 007 u 0022
Benzene 0210 067 0029
~rbon Tetrbullchloride 0132 083 0024 tert-Amyf Melt1yl Ether NO NO u 0016
12-0lChloroptcpane NO NO u 0023
Ethyl Aaylate NO NO u 0020
Bromodichloromethane NO NO u 0025
Trlchloroetbylene NO NO u 0025
Methyl Methacrylate NO NO u 0022
cis-1J-Oichloropropene ND NO u 0022
Methyl Isobutyl Ketone 0040 016 0022
trans-13-Dichloropropene NO NO u 0025
112-Tnchloroethane NO NO u 0025
TDIUIHie 0334 126 0016
Olbromochloromethane NO NO u 0021
Eastern Research Group Th~ r~sults in tins report apoly only ro the sanrptes fDiaylted in accordance With the chain of Cltstody doc11ment 111is mwlylicalnport muft be reproduced in Its enttrtty
Page 5 of 16
RG CERTIFICATE OF ANALYSIS
EPA Reg1on VII FILE 027800001030
300 Minnesota Avenue REPORTED 1111011 0903
Kansas City KS 66101 SUBMITTED 0808111 to 092911
ATTN Michael F DaviS AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption Ash amp Forest Intersection Lab ID 1080909-01 Sampled 080611 0000
Pressure Receipt 65 Hg Canister 401 Received 0809111120
Comments Background Sample Analyzed 080911 2309
Air Toxics by EPA Compendium Method T0-15 Results lmL
Analvte JmiDt Y9Lm flu Jmbx 12-Dibromoethane ND ND u 0018
n-Ociane 0039 018 0015
Tetrachloroethylene ND NO 0018u
Oilorobenzene ND NO u 0021
Ethyl benzene 0074 032 0017
mp-Xylene ()140 061 0034
Bromoform NO NO u 0025
Styrene 0034 015 0022
1122-Tetrachloroethane NO NO u 0024
o-Xylene 0067 029 0018
135-Trimethylbenane 0031 015 0026
124-Trimethylbenzene 0078 038 0028
m-Dichlorobanzene NO NO 0031u Ollcromethylbenzene ND ND u 0039
p-Dichlorobenzene NO NO 0-035u o-Dichlorobemenl ND ND u 0037
12+Trichlorobenzene NO NO 0036u Hexachlnro-13-butadiene ND NO 0037u
Eastern Research Group lhtJ resutu in thrs r~~porl apply tmly io tht ronrpler onaly~d in accordanc6 wrth the chain of curtoay dOIumelll This analytical report mllSt ~ reprfJduccd rn its lntirety
Page 6 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN~ Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001 030
REPORTEDmiddot 111011 0903
SUBMITIED 080811 tci 092911
AQS SITE CODE
SITE CODE OECAwork
Description Ash amp Forest Intersection Lab ID 1082901-01 Sampled 082611 oomiddotoo Pressure Receipt 8 Hg canister 020 Received 082911 0948
COmments Background Sample Analyzed 083011 0036
Air Taxies by EPA Compendium Method T0-15 Results MnL
Analvte mmx Y9lm fml ~ Acetylene 0A94 053 0016 Propylena OA34 o7s 0039 Dlchlorocllrluoromllthane 0553 274 0011 chloR)IIIIIthane 0604 125 0012 Dldlorollltniftuoroethane 0024 017 0009 VInyl dlorlde 0008 002 opoa 13-Butadlene 0028 0 06 op01 Bromomethane 0016 006 0009
Olloroethane NO NO u 0009 Aatonitrila 0217 037 0024 Tr1dtlorofluorometllane 0211 164 0010
Aaylonltrile NO NO u 0012
11-Didlloroethene NO NO u 0009
Dlchloromethane 0404 141 0010 carbon Disulfide 0161 0 50 0033 Trldlorotrlfluoroethane 0117 otO 0011 trans-12-0khloroeth~ene NO NO u ooos 11-0ichloroethane NO NO u 0008
Methyl tPrt-sutvt Ether NO NO u 0008
Methyl Ethyl Ketone 111 328 0157
Chloroprene ND NO u 0008 ds-12-Dichloroethvlent NO NO u 0009
Bromochloromethane NO NO u 0008
Chlororgtnn 0043 021 0001
Ethyl tert-iutyl Ether NO ND u 0008 12middotDichloroethene 0030 012 0001 111middot TriChloroethane 0018 010 u op22
Benzene 0225 072 OOZ9
Carbon Tetrachloride 0098 0amp2 Op24
tert-Amyl Methyl Ether ND NO u 0016
12-0ichloropropane NO NO u 0023
Ethyl Acrylate ND NO u 0020
Bromod1chloromethane 0011 007 u 0025
Trichloroethylene 0 015 008 U 0025
Methyl Methaaylate NO NO u 0022
ds-13-0idlloropropene NO NO u 0022
Methyl Isobutyl Ketone 0052 021 0022
trans-13-0ichloropropene ND NO u 0025
112middot Tnrhloroethane ND NO u 0025
Toluene 514 1940 0016
Olbromochloromethane 0008 007 u 0021
Eastern Research Group lh~ results in this report apply only to the sample 011alyud in accordance with tht rhain of cusrody documtmr This OJialytlcal nport musliM -Produced in its mirery
Page 7 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN~ Michael F DaviS
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001 030
REPORTED 111 Oi11 0903
SUBMITTED 08108111 to 092911
AQS SITE CODE
SITE CODE OECAwork
Description Ash amp Fcorest Intersection Lab ID 1082901-01 Sampled 082611 0000
Pressure I Receipt 8 Hg Canister 020 Received 082911 09~48
Comments Background Sample Analyzed 083011 0036
Air Toxics by EPA Compendium Method T0-15 Results MW
Anayte DDIn Y9lm Eiim IU2bll 12-Dibromoethane NO ND u 0018
n-Ocblne 0074 035 0015
Ttrachloroethylene 0026 018 0018
Chlorobenzene ND ND u 0021
Ethylbenzene 0218 0-95 0017
mp-Xylene 0551 2AO 0034
Bromoform ND ND u (105
Styrene 0089 038 0022
1122-Tetrachloroethane 0010 0 07 u 0024
a-Xylene 0189 082 0018
135-Trlmethylbenzene 0062 031 0026
124-Trimethylbenzene 0150 074 0028
m-Dichlorobenzene 0006 004 u 0034
Chloromethylbenzene NO ND u 0039
p-Dichlorobenzene 0032 019 u 0348
o-Ochlorobenzene 0006 004 u 0037
124-Trlchlorobenzene 1110 NO u 0036
Hexachloro-13-bullldlene 0008 009 u 0037
Eastern Research Group Tlze bullesuJs m this repon apply on)middot to the sanrpfamp nnalyud ill acordance wh lht chain of custody Joumumt Thi~ OIIOI)middottical report musbull be teptoJduced In its elltiJtty
Page 8 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMilTED 0808111 to 0929111
ATTN Michael F Davts AQS SITE CODE
PHONE 913) 551-5042 FAX (913) 551middot5000 SITE CODE OECAwork
Description 4th and Santa Fe Lab ID 1090818-01 Sampled 090711 0000
Pressure 0 Receipt 6 5 Hg Canister EROOB Received 0908111247
Comments Analyzed 090911 0137
AirToxics by EPA Compendium Method T0-15 BciYlb MQI
Analyte lUlblpound usLm fOOl ~ Acetylene 0175 029 0016 Propylene 0333 057 op39 Dichlorodifluoromethane 0521 258 0011 Chloromethane 0507 LOS oou Okhlorotetrafluoroeihane NO NO u 0009
Vinyl chloride NO NO u OOilll 13-Butadlene NO NO u 0007
Bromomethane NO NO u 0009 Chloroethane NO NO u 0009 AletDnibile 0122 021 0024
Tr1dlloroftuoromethane 0252 142 0010 Acrylonlbile NO NO u 0012 11-0ldlloroethPne NO NO u 0009 Dldlloromethane 0159 055 0010
Carbon Disulfide 0063 020 0033 Trlchlorotrlfluoroethane 0094 072 OJ11
trans-12-Dichloroethylene NO NO u 0008
11-0lchloroethane NO NO u ouoa Methyl tert-BlJtyl Ether NO NO u o~
Ne~IEthyiKetone 0472 139 0157 Chloroprene NO NO u 0008
ds-12-Dichloroethylene NO NO u 0109
Bromochloromethane NO NO u oooa Chlorofomi NO NO u 0009 Ethyl ~Butyl Ether NO NO u 0008
12-Didlloroethane NO NO u 0009
111middot Trtdlloroethane NO NO u 0022
Benzene 0168 054 0029 Carbon Telrldllorlde 0095 oeo 0024
tertmiddotAmyl Methyl Ether NO NO u 0016
12-0Chlolgtpropane NO ND u 0023
ethyl Acrtlate NO NO u 0020
Bromodichloromethane NO NO u OOlS Trichloroethylene ND NO u 0025
MettwiMethacrylate NO NO u oc22 cis-13-0ichloropropene NO NO u 0022
~yiiiObutyiKetone 0035 014 0022
trans-13-0ichloropropene NO NO u oo2S 112middot Trichloroethane NO NO u 0025
Toluene 0373 141 0016
OibromQchloromethane NO NO u 0071
Eastern Research Group The nsults in this nport apply only to the saltlples D11alyzed in acordance with the chain Df cuampmiddottody docWMnt This analytical rttport must be repriJduced in its elllirety
Page 9 of 16
RG CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMIITED 080811 to 09291 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 4th and Santa Fe Lab ID 1090818-01 Sampled 090711 0000
Pressure Receipt 65 Hg canister ER008 Received 09081112~47
Comments Analyzed 090911 0137
Air Toxics by EPA Compendium Method T0-15 Results tmL
Analvte IUllm ll9lm flil Jmbll 12-0ibromoethane NO NO u 0018
n-Octane 0038 018 0015
Tetradiloroethylene ND NO u 0018 Chlomhenllne NO NO u 002
Ethyl benzene 0064 028 0017
mp-Xylene 0148 064 0034
Bromoform NO NO u 0025
Styrene NO NO u 0022
1122-TlliiChloroetllane NO NO u 0021
omiddotXylene 0070 031 0018
135middotTrimethylbenzene ND NO u 0026
124-Trimethylbenzene 0078 038 0028
m-Oiehlorobenzene NO NO u 0034
Chloromethylbenzene NO NO u 0019
p-Orchlorobenzene ND NO u 0348
o-Oidllorobenzene ND NO u 0037
124-Trichlorobenzene NO NO u 0036
Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The results rn Jhis teport apply cmJy 10 the samples (Uraly~ed in ac~ordant-e wilh the chain of CIISiody docunum This atwlytiral report 11111s1 be reprculuced i11 ils e11tirrty
Page 10 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN MIChael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001 030
REPORTED~ 1110111 0903
SUBMmED 0810811 to 092911
AQS SITE CODE
SITE CODE OECAwork
Description 150 west of Hwys 169 and 39 Lab ID 1091501-01 sampled 091411 oooo Pressure 0 ReClelpt 13 Hg canister 709 Received 091511 10~42
Comments Analyzed 0915111926
Air Taxies by EPA Compendium Method T0-15 BHIIIm MDI
Analyte JUlbll li9Lm fJJg JlRinl AcBtylene 0234 025 0-016 Propylene 0258 045 0-0~11
Dlchlorodlfluoromettmne 0544 270 oo11 Chloromethane 0526 109 0 012
DichlorolelrifAJoroethane NO NO u Otgt09 Vinyl chloride NO NO u 0008 13-Butildlene NO NO u 0007 Bromomettlane NO NO u 0009 Chloroethane NO NO u 0009
Acetonitrile 0130 022 0024
Trlchlorcrfluoromethane 0263 lAB 0010 Aaylonltrile NO NP u 0012 11-DIChloroethene NO NO u 0009
Dldloromelhane NO NO u (IOlD
carbon Disulfide 0032 010 u 0033 T~hlo~fluonHdhane 0107 082 0011 tr~ns-12-0ichloroethyler~ NO NO u 0008 11-Dichloroethane ljO NO u 0008 Methl tert-Butyl Ether NO NO u 0008 Methyl Ethyl Ketone 0382 113 0157
Chloroprene NO NO u 0008 ciamp-12-0ichloroethylene NO NO u 0009 Bromochloromethane NO NO u 0008 011oroform NO NO u 0009 Ethyl tert-Butyl Ether NO NO u 0008 JI-Dichloroethilne NO NO u 0009 111-Trichloroethane NO NO u (l022
Benzene ozos 067 0029
Carbon Tetrachloride 0101 064 0024 tert-Amyl Methyl Ether NO NO u 1)016 12-DJChiOropropane NO NO u 0023 Ethyl Acrylate NO NO u (1 020
Bromodichloromethane NO NO u 0025 Trichloroethylene NO NO u 0025
Methyl Methacrylilte NO NO u 0022 cis-13-Dichloropropene NO NO u 0022 Methyl Isobutyl llteDM NCI NO u 0022 trans-13-0ichloropropene NO NO u 0025 112-Trldlloroetflane NO NO u 0025 Toluene 0095 036 0016 Olbromodloromelhane NO NO u 0021
Eastern Research Group The results 111 Jhis r~port apply only to the samplts waalylui in accordance with tht chain of custody document This cuuzlytical report must in reprod~~eed in its entirety
Page 11 of 16
CERTIFICATE OF ANALYSISRG EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 111 011 0903
Kansas City KS 66101 SUBMirrED OBiOB11 to 092911
ATTN~ M1chael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE ~ OECAw(irk
Description 150 west of Hwys 169 and 39 Lab ID 1091501-01 Sampled 091411 00 00
Pressure Receipt 13 Hg canister 709 Received 0915111042
Comments Analyzed 0915111926
Air Toxlcs by EPA Compendium Method T0-15 ~ MW
Analvte wmx uqm fli1g RRint 12-Dibromoethane ND IID u 0()18
n-Oddne ND ND u 0015
Tetrachloroethylene ND ND u 0018
Ollorobenzene ND ND u 0021
Ethylbenzene 0035 015 Q017
mpmiddotXylene 0041 018 0034
Bromoform ND NO 11 0025
Styrene NO ND u 002
11-22-Tetradlloroelhane ND ND u 0024
o-Xylene ND NO u 0018
135-Trimethylbenzene NO NO u 0026
124middotTrlrnathylbenzene 0-042 021 0028
m-Dichlorohenzene ND ND u 0034
Chloromethylbenzene ND ND u 0039
p-OIChlorobenzene NO NO u 0348
o-Dichlorobenzere NO NO u 0037
12+Trlchlorobenzene NO ND u 0036
Hexachloro-13-butadlene ND ND u 0037
Eastern Research Group The result in thrs reoort applgt ltmly to the samplts mral1zed m accordanc11 ~ith thilhain of custodgt document This am1lytical report m11st be rbullpmJuced ill it~ entirety
Page 12 of 16
CERTIFrCATE OF ANALYSIS
EPA Region VII FILE tl 027800001030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMITTED 080811 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Description 73 north of Oak St on Plummer Lab ID 1092909-01 Sampled 0928110000
Pressure 0 Receipt 65 Hg canister 140 Received 0929111057
Comments Analyzed 093011 20 34
Analyte
Acetylene middotPropylene
Dldllorodifluoromethane Chlolomettlane
Dlchlorotetrafluoroethllne VInyl chloride 13-Butadlene Bromometl1dne
Chloroethane
Acetunitrile Trldllorotluoromethane
Acrylonitrile
11-0ithloroethene Dichloromethane Carbon DisulfJde
Trlchlorotrlfkloroetftane lranr1 2-0khloroethylene
11-Dithloroelhane
Methyl tert-Butyl Ether Methyl Ethyl Ketone Chloroprene ds-1HllchloiJethylene Bromochloromethane Chlorofvnn
Ethyl tert-Butyl Ether 12-Dichloroethane 111middotTriChloroethane
Benzene carbon Tetrachloride tert-Amyl Methyl Ether 12-Didlonopropane Ethyl Acrylate Bromodlchlorornelhane Trichloroethylene
Methyl MetllacrylaJ
ds-13-Dithloropropene Methyl Isobutyl KetDne trans-13-0khlorapropene 112-Trichloroethane
Toluene Olbromochloromethane
Air Toxics by EPA Compendium Method T0-15 Results mL
ORb YIiID Eiilg I1IZD 223 238 016 123 212 0039
0564 280 0~11
0525 109 0012 0018 013 ooot
NO NO u 0008 0181 040 0~07
NO NO u o009 NO NO u 0009
0157 028 0024 ozgo 163 0010
NO NO u 0(112 NO NO u 0009
0154 054 0010 0045 0 14 0033 0092 071 0011
NO NO u 0008 NO NO u 0008 NO NO u 0~08
0624 184 0157 NO NO u 0008 NO NO u 0009 NO NO u 0008
0035 017 0009 NO NO u 0008 NO NO u 0009
0012 007 u 0022 L49 477 0029
0088 o56 0024 NO NO u 0016 ND NO u 0023 NO NO u 0020 NO ND u 0025
0178 096 0025
NO NO u 0022 NO NO u 0022
0094 039 0022 NO NO u 0025 NO NO u 0025
276 10400 D 0040 r~O NO u 0021
Eastern Research Group The results m this repon apply only to the samples cmolylld in accordance wilh the chain of cUStOdy docWMnt This arwlytlcal rJort mu~middott be reproduced in its entirety
Page 13 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMITTED 0808111 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECA wa1lt
Description 75 north of Oak St on Plummer Lab ID 1092909-01 Sampled 092811 0000
Pressure Receipt 65 Hg canister 140 Received 0929111057
Comments Analyzed 0930112034
Air Toxics by EPA Compendium Method T0-15 Results lmb
Analyte mmx ugm3 flil on 12-Dibromoethane NO NO u 0018
n-Octane 0193 090 0015 Tetrachloroethylene 0019 013 0018
Chlorobenzene NO NO u 0021
Ethyl benzene 0356 155 p017 mp-Xylene 1oamp 461 OOl4
Bromoform NO NO u 6025
Sty~Wte 0060 026 0022 lll2-Tetrachloroethane NO NO u 0-024
o-Xylene P422 184 01118 135-TrlmethylbenEene 0094 046 0026 1124-Trlmethylbenzene 0340 167 0028
m-Dichlorobenzene 0043 016 0034 Chloromethylbenzene NO NO u 0039
p-Dichlorobenzene 0019 011 u 0035
rDichlorobenzellE NO NO u 0037 121-Trochlorobenzene NO NO u 0-036
Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The ll$Ults in rhis repon appl) NIhbull to the samples analyted in accordance with the cham of custody document Thta analybullical rrporl must he reproduced in in entirety
Page 14 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII FILE tl 027800001 030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS66101 SUBMmED 080811 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX~ (913) 551-5000 SITE CODE OECAwork
IAnalyte Result Units SOurce Result RPD
RPD Umit Note
Eastern Research Group ~ resulu in this reprJrt apply oraly to the samples analyed 111 accordance with the chain of crutody docunumt 1his anulmcal report must be reprodu~ed In its enrlnty
Page 15 of 16
CERTIFICATE OF ANALYSISRG EPA Region VII FILEmiddot 027800001 030
300 Minnesota Avenue REPORTED 1110 11 09middot03
Kansas City KS 66101 SUBMITTED 08101311 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX~ (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
u Under Detection Umlt
o Th1s result obtained by dilution
ND Analyte NOT DETECTED at or above the Method Detecbon Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group T1r results in thH report apply on() w the sample tmayzed il occordancltt with the cham of bullur1ody dotumnt This anayllcai report must be prwiuced in its entirety
Page 16 of 16
~RG Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
December 05 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 111511 1121
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the amtract for NMOC UATMP PAMS CSATAM and NATTS support (US EPA Contract No EPD-09-D48) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please oontact me at 919-468-7930
Sincerely
Laura Van Enwyck Project Manager lauravanenwyckergcom
The information contained in this report and its attachment(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauraJnenwyckergcom and delete the report without retairring any copies
Page 1 of6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 120511 1059
Kansas City KS 66101 SUBMITTED 111511
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Lincoln amp 39 Highway 1111501-01 Air 111411 0000 111511 1121 (111 W Lincoln)
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wfth the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001030
REPORTED 120511 1059
SUBMITTED 111511
AQS SITE CODE
SITE CODE OECAwork
DesaiptionUncoln amp 39 Highway (111 W Uncoln) Lab ID 1111501-01 Sampled 111411 0000
Pressure Receipt 8 Hg canister 636 Received 1115111121
Comments Analyzed 111611 0932
Air Toxics by EPA Compendium Method T0-15 blulb lmL
Analvte Jmbx Yllm fiG JlRbl Acetylene 0171 018 A-Ql 0016 Propylene 0272 OA7 A-Ql 0039 Dlchlorodlfluoromethane 0503 2A9 A-Ql 0011 Chloromethane OA74 098 A-Ql 0011 Dichlorobtraftuoroethane 0016 011 A-Ql 0009 Vinyl chloride ND ND A-Ql U 0008 13-Buladlene 0020 004 A-Ql 0007 Bromomethane 0011 004 AmiddotOl 0009 Chloroethane ND ND A-Ql U 0009 Acetonitrile 0138 023 A-Ql 0024 Trichloroftuoromethane D304 L71 A-Ql 0010 Acrylonitrile ND ND A-Q1 U 0012
11-Dichloroethene ND ND A-Q1 U 0009 Dichloromethane 0266 093 A-Ql 0010 Carbon Disulfide 0129 040 A-Ql 0033 Trichlorotrifluoroethane 0079 061 A-Ql 0011 trans-12-0ichloroethylene ND ND A-Ql U 0008 11-Dichloroethane ND ND A-Ql U 0008 Methyl tert-Butyl Ether ND NO A-Q1 U 0008 Methyl Ethyl Ketone 0760 us AmiddotOl 0157 Chloroprene ND NO A-Ql U 0008
cis-12-Dichloroethylene NO NO A-Ql U 0009 Bromochloromethane NO NO A-Ql U 0008 Chloroform NO NO A-Ql U 0009
Ethyl tert-Butyl Ether NO NO Amiddot01 U 0008 12-Dichloroethane 0026 011 A-Ql 0009 111-Trichloroethane 0006 003 A-Q1 U 0022 Benzene 113 362 A-Q1 0029 Carbon Tetrachloride 0069 OA4 A-Q1 0024 tert-Amyl Methyl Ether ND ND A-Ql U 0016 12-Dichloropropane ND NO A-Ql U 0023
Ethyl Acrylate NO NO A-Ql U 0020
Bromodlchloromethane ND NO A-o1 u 0025 Trichloroethylene NO ND A-01 U 0025
Methyl Methacrylate ND NO A-Q1 U 0022 cis-13-Dichloropropene NO NO A-Ql U 0022 Methyl Isobutyl Ketone 0047 019 A-Ql 0022 trans-13-Dichloropropene NO ND A-Q1 U 0025 112-Trichloroethane NO NO A-Q1 U 0025
Toluene 0661 250 A-01 0016 Dibromochloromethane NO ND A-Q1 U 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repoTt must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1210511 1059
Kansas City KS 66101 SUBMITTED 1115 11
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption Uncoln amp 39 Highway (111 W Lincoln) Lab ID 1111501-01 Sampled 111411 0000
Pressure Receipt 8 Hg canister 636 Received 1115111121
Comments Analyzed 111611 0932
Air Toxics by EPA Compendium Method T0-15 RuJID mL
AnaMe IU1bll ~ BiSl IU1bll 12-Dlbromoethane NO NO A-Ql U 0018
n-Oct3ne 0025 012 A-Ql 0015
Tetrachloroethylene 0016 011 A-Ql U 0018
Ollorobenzene NO NO A-Ql U 0021
Ethylbenzene 0068 030 A-Ql 0017
mp-Xylene 0144 063 A-Ql 0034
Bromoform NO NO A-Ql U 0025
Styrene 0058 025 A-Ql 0022
1122-Tetrachloroethane NO NO A-Ql U 0024
o-Xylene 0058 025 A-ol 0018
135-Trlmetflylbenzene 0050 025 A-01 0026
124-Trimetflylbenzene 0130 064 A-Ql 0028
m-Dichlorobenzene NO NO A-Ql U 0034
Chloromelhylbenzene NO NO A-ol U 0039
p-Oichlorobenzene 0027 016 A-Ql U 0035
o-Oichlorobenzene NO NO A-Ql U 0037
124-Trichlorobenzene NO NO A-ol U 0036
Hexachloro-13-butadiene NO NO A-ol U 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 120511 1059
Kansas City KS 66101 SUBMITTED 111511
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance witlz tlze chain of custody documellt This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1205111 1 059
Kansas City KS 66101 SUBMITTED 11151 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
A-ol Estimated value due to possible canister leak
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical re-port must be reproduced in its entirety
Page 6 of 6
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
December 15 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 1206111229
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for NMOC UATMP PAMS CSATAM and NATTS support (US EPA Contract No EPD-09-048) This rover page is an integral part of this report and any exceptions or oomments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Project Manager lauravanenwyckergcom
The information contained in this report and its attachment(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify laura vanenwyck ergcom and delete the report without retaining any copies
Page 1 of 6
RG CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111 1041
Kansas City KS 66101 SUBMITTED 1206 11
ATTN Michael F Davis AQS SITE CODE
PHONE 913) 551-5042 FAX 913) 551-5000 SITE CODE OECAwork
ANALYTlCAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Ash amp Forest SE Corner 1120611-01 Air 120411 0000 120611 1229
middotI I
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytirol repon must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
ALE 027800001030
REPORTED 1215111041
SUBMmED 1210611
AQS SITE CODE
SITE CODE OECAwork
Desaiptlon Ash amp Forest SE Comer Lab ID 1120611-01 sampled 120411 oooo Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 BuYltl MQL
AnaMe IUlllll lWm Bag IUlllll Acetylene OA36 OA7 0016 Propylene 0304 052 0039 Dichlorodiftuoromethane 0567 281 0011 Chloromethane 0566 117 0012 Dlchlorotetnlftuoroethane 0019 013 0009 Vinyl chloride NO NO u 0008 13-Butadiene NO NO u 0007 Bromomethane 0012 005 0009 Chloroethane NO NO u 0009 Acetonitrile 0111 019 0024 Trichlorofluoromethane 0284 160 0010 Aaylonitrile ND NO u 0012 11-Dichloroethene ND ND u 0009 Dichloromethane 0083 029 0010 Carbon Disulfide 0019 006 u 0033
Trlchlorotrlftuoroethane 0099 076 0011 trans-12-Dichloroethylene ND ND u 0008 11-Dichloroethane ND NO u 0008 Methyl tert-Butyl Ether NO NO u 0008 Methyl Ethyl Ketone 0536 158 0157 Chloroprene NO NO u 0008 cis-12-Dichloroethylene NO ND u 0009 Bromochloromethane NO NO u 0008 Chloroform 0022 011 0009 Ethyl tert-Butyl Ether NO NO u 0008 12-Dichloroethane 0025 010 0009 111-Trichloroethane 0011 006 u 0022 Benzene 0188 060 0029 carbon Tetrachloride 0106 067 0024 tert-Amyl Methyl Ether NO NO u 0016 12-Dichloropropane NO NO u 0023 Ethyl Acrylate ND NO u 0020
Bromodichloromethane NO NO u 0025 Trichloroethylene NO NO u 0025 Methyl Methacrylate NO NO u 0022 cis-13-Dichloropropene NO NO u 0022
Methyl Isobutyl Ketone 0042 017 0022 trans-13-Dichloropropene ND NO u 0025 112-Trichloroethane NO NO u 0025
Toluene 0149 056 0016 Oibromochloromethane 0003 003 u 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproducedin its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 121511 1041
Kansas City KS 66101 SUBMmED 1210611
ATTN Michael F Davis AQS SITE CODE
PHONE (913 551-5042 FAX (913 551-5000 SITE CODE OECAwork
Description Ash amp Forest SE Comer Lab ID 1120611-01 Sampled 120411 0000
Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 llWdtl MID
Analyte ubll IUllm Bag ubll 12-0ibromoethane NO NO u 0018 nmiddotOctane 0044 021 0015 Tetrachloroethylene 0006 004 u 0018
Chlorobenzene NO NO u 0021 Ethylbenzene 0047 021 0017 mp-Xylene 0070 031 0034 Bromoform NO NO u 0025 Styrene 0034 015 0022 1122-Tetrachloroethane NO NO u 0024 o-Xylene 0036 016 0018 135-Trlmethylbenzene 0025 012 u 0026 124-Trlmetllylbenzene 0047 023 0028 m-Oichlorobenzene NO NO u 0034
Chloromethylbenzene NO NO u 0039 p-Dichlorcbenzene 0005 003 u 0348 a-Dichlorobenzene NO NO u 0037
124-Trlchlorobenzene NO NO u 0036 Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repon must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS~RG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 66101 SUBMITTED 12061 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPDIAnalyte Result Units Result RPD um1t Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 661 01 SUBMITTED 120611
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its enJirety
Page 6 of 6
i
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
March 12 2012
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 030512 0916
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for UATMP NATTS CSATAM PAMS and NMOC support (US EPA Contract No 68-D-Q9-048) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Program Manager lauravanenwyckergcom
The information contained in this report and its attachmcnt(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauravanenwyckergcom and delete the report dthout retaining any copies
Page 1 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 0312112 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
6th St between Central amp 2030501-01 Air 030212 0000 030512 0916 Malcom
Eastern Research Group The results in this report apply only to the samples anal zed in accordance With the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Aven ue REPORTED 031212 1 051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 ~ tml
Analvte RRbll Y9lD1 flu RRbll Acetylene 0627 067 0072 Propylene 0484 084 0033
Dichlorodllluoromethane 0500 248 0023 Chloromethane 0557 115 0033
Dichlorotetrafluoroethane 0015 011 0012 Vinyl chloride NO NO u 0011
13-Butadlene 0036 oo8 0011
Bromomethane 0012 005 0012 Chloroethane NO NO u 0017
Acetonitrile 0073 012 0073
Trichlorofluoromethane 0258 145 0015 Acrylonitrile NO NO u 0020
11-0ichloroethene NO NO u 0014
Dichloromethane 0185 064 0023
Carbon Disulfide 0037 012 0014 Trichlorobitluoroethane 0119 091 0017
trans-12-0ichloroethylene NO NO u 0012
11-0ichloroethane NO NO u 0015
Methyl tert-Butyl Ether NO NO u 0011
Chloroprene NO NO u 0012
ds-12-0ich loroethylene NO NO u OD18
Bromochloromethane NO NO u 0014
Chloroform NO ND u 0014
Ethyl tert-Butyl Ether NO NO u 0011
12-Dichloroethane 0019 008 0016
111-Trichloroethane 0012 007 u 0020
Benzene 0344 L10 0061 Carbon Tetrachloride 0088 056 0024
tert-Amyl Methyl Ether NO NO u 0016
12-0ichloropropane ND NO u 0019
Ethyl Acrylate ND NO u 0014
Bromodichloromethane ND NO u 0021
Trichloroethylene NO ND u 0022
Methyl Methacrylate ND NO u 0025
ds-13-0ichloropropene NO NO u 0015
Methyl Isobutyl Ketone 0015 oo6 0015
trans-13-0ichloropropene NO ND u 0016
112-Trichloroethane NO NO u 0021
Toluene 0416 157 0045
Oibromochloromethane ND NO u 0018
12-0ibromoethane ND NO u 0017
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551 -5000
FILE 027800001030
REPORTED 0312 12 1051
SUBMITTED 030512
AQS SITE CODE
SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 Bwdtl MJlL
Analvte Jmbll Y9Lm Big Jmbx nmiddotOclane 0039 018 0020 Tetrachloroethylene 0005 003 u 0020
Chlorobenzene ND ND u 0025
Ethylbenzene 0045 020 0023 mp-Xylene 0112 OA9 0037 Bromoform ND ND u 0020
Styrene 0030 013 0024 1122-Tetrachloroethane ND ND u 0018
o-Xylene 0050 022 0020
135-Trimethylbenzene 0019 009 u 0022
124-Trimethylbenzene 0047 023 0025 m-Dichlorobenzene ND ND u 0024
p-Dichlorobenzene 0004 002 u 0019
a-Dichlorobenzene NO ND u 0021
124-Trichlorobenzene ND ND u 0022
Hexachloro-13-butadiene ND ND u 0022
Eastern Research Group The results in this report apply only 1o the samples analyzed in accordance with the chain of custody document This analytical rep ort must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 031212 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wilh the chain of custody document This analytical report must be reproduced in its enrirety
Page 5 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 03121121051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report nutst be reproduced in its entirety
Page 6 of 6
RG CERTIFICATE OF ANALYSIS
EPA Reg1on VII FILE 027800001030
300 Minnesota Avenue REPORTED 1111011 0903
Kansas City KS 66101 SUBMITTED 0808111 to 092911
ATTN Michael F DaviS AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption Ash amp Forest Intersection Lab ID 1080909-01 Sampled 080611 0000
Pressure Receipt 65 Hg Canister 401 Received 0809111120
Comments Background Sample Analyzed 080911 2309
Air Toxics by EPA Compendium Method T0-15 Results lmL
Analvte JmiDt Y9Lm flu Jmbx 12-Dibromoethane ND ND u 0018
n-Ociane 0039 018 0015
Tetrachloroethylene ND NO 0018u
Oilorobenzene ND NO u 0021
Ethyl benzene 0074 032 0017
mp-Xylene ()140 061 0034
Bromoform NO NO u 0025
Styrene 0034 015 0022
1122-Tetrachloroethane NO NO u 0024
o-Xylene 0067 029 0018
135-Trimethylbenane 0031 015 0026
124-Trimethylbenzene 0078 038 0028
m-Dichlorobanzene NO NO 0031u Ollcromethylbenzene ND ND u 0039
p-Dichlorobenzene NO NO 0-035u o-Dichlorobemenl ND ND u 0037
12+Trichlorobenzene NO NO 0036u Hexachlnro-13-butadiene ND NO 0037u
Eastern Research Group lhtJ resutu in thrs r~~porl apply tmly io tht ronrpler onaly~d in accordanc6 wrth the chain of curtoay dOIumelll This analytical report mllSt ~ reprfJduccd rn its lntirety
Page 6 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN~ Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001 030
REPORTEDmiddot 111011 0903
SUBMITIED 080811 tci 092911
AQS SITE CODE
SITE CODE OECAwork
Description Ash amp Forest Intersection Lab ID 1082901-01 Sampled 082611 oomiddotoo Pressure Receipt 8 Hg canister 020 Received 082911 0948
COmments Background Sample Analyzed 083011 0036
Air Taxies by EPA Compendium Method T0-15 Results MnL
Analvte mmx Y9lm fml ~ Acetylene 0A94 053 0016 Propylena OA34 o7s 0039 Dlchlorocllrluoromllthane 0553 274 0011 chloR)IIIIIthane 0604 125 0012 Dldlorollltniftuoroethane 0024 017 0009 VInyl dlorlde 0008 002 opoa 13-Butadlene 0028 0 06 op01 Bromomethane 0016 006 0009
Olloroethane NO NO u 0009 Aatonitrila 0217 037 0024 Tr1dtlorofluorometllane 0211 164 0010
Aaylonltrile NO NO u 0012
11-Didlloroethene NO NO u 0009
Dlchloromethane 0404 141 0010 carbon Disulfide 0161 0 50 0033 Trldlorotrlfluoroethane 0117 otO 0011 trans-12-0khloroeth~ene NO NO u ooos 11-0ichloroethane NO NO u 0008
Methyl tPrt-sutvt Ether NO NO u 0008
Methyl Ethyl Ketone 111 328 0157
Chloroprene ND NO u 0008 ds-12-Dichloroethvlent NO NO u 0009
Bromochloromethane NO NO u 0008
Chlororgtnn 0043 021 0001
Ethyl tert-iutyl Ether NO ND u 0008 12middotDichloroethene 0030 012 0001 111middot TriChloroethane 0018 010 u op22
Benzene 0225 072 OOZ9
Carbon Tetrachloride 0098 0amp2 Op24
tert-Amyl Methyl Ether ND NO u 0016
12-0ichloropropane NO NO u 0023
Ethyl Acrylate ND NO u 0020
Bromod1chloromethane 0011 007 u 0025
Trichloroethylene 0 015 008 U 0025
Methyl Methaaylate NO NO u 0022
ds-13-0idlloropropene NO NO u 0022
Methyl Isobutyl Ketone 0052 021 0022
trans-13-0ichloropropene ND NO u 0025
112middot Tnrhloroethane ND NO u 0025
Toluene 514 1940 0016
Olbromochloromethane 0008 007 u 0021
Eastern Research Group lh~ results in this report apply only to the sample 011alyud in accordance with tht rhain of cusrody documtmr This OJialytlcal nport musliM -Produced in its mirery
Page 7 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN~ Michael F DaviS
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001 030
REPORTED 111 Oi11 0903
SUBMITTED 08108111 to 092911
AQS SITE CODE
SITE CODE OECAwork
Description Ash amp Fcorest Intersection Lab ID 1082901-01 Sampled 082611 0000
Pressure I Receipt 8 Hg Canister 020 Received 082911 09~48
Comments Background Sample Analyzed 083011 0036
Air Toxics by EPA Compendium Method T0-15 Results MW
Anayte DDIn Y9lm Eiim IU2bll 12-Dibromoethane NO ND u 0018
n-Ocblne 0074 035 0015
Ttrachloroethylene 0026 018 0018
Chlorobenzene ND ND u 0021
Ethylbenzene 0218 0-95 0017
mp-Xylene 0551 2AO 0034
Bromoform ND ND u (105
Styrene 0089 038 0022
1122-Tetrachloroethane 0010 0 07 u 0024
a-Xylene 0189 082 0018
135-Trlmethylbenzene 0062 031 0026
124-Trimethylbenzene 0150 074 0028
m-Dichlorobenzene 0006 004 u 0034
Chloromethylbenzene NO ND u 0039
p-Dichlorobenzene 0032 019 u 0348
o-Ochlorobenzene 0006 004 u 0037
124-Trlchlorobenzene 1110 NO u 0036
Hexachloro-13-bullldlene 0008 009 u 0037
Eastern Research Group Tlze bullesuJs m this repon apply on)middot to the sanrpfamp nnalyud ill acordance wh lht chain of custody Joumumt Thi~ OIIOI)middottical report musbull be teptoJduced In its elltiJtty
Page 8 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMilTED 0808111 to 0929111
ATTN Michael F Davts AQS SITE CODE
PHONE 913) 551-5042 FAX (913) 551middot5000 SITE CODE OECAwork
Description 4th and Santa Fe Lab ID 1090818-01 Sampled 090711 0000
Pressure 0 Receipt 6 5 Hg Canister EROOB Received 0908111247
Comments Analyzed 090911 0137
AirToxics by EPA Compendium Method T0-15 BciYlb MQI
Analyte lUlblpound usLm fOOl ~ Acetylene 0175 029 0016 Propylene 0333 057 op39 Dichlorodifluoromethane 0521 258 0011 Chloromethane 0507 LOS oou Okhlorotetrafluoroeihane NO NO u 0009
Vinyl chloride NO NO u OOilll 13-Butadlene NO NO u 0007
Bromomethane NO NO u 0009 Chloroethane NO NO u 0009 AletDnibile 0122 021 0024
Tr1dlloroftuoromethane 0252 142 0010 Acrylonlbile NO NO u 0012 11-0ldlloroethPne NO NO u 0009 Dldlloromethane 0159 055 0010
Carbon Disulfide 0063 020 0033 Trlchlorotrlfluoroethane 0094 072 OJ11
trans-12-Dichloroethylene NO NO u 0008
11-0lchloroethane NO NO u ouoa Methyl tert-BlJtyl Ether NO NO u o~
Ne~IEthyiKetone 0472 139 0157 Chloroprene NO NO u 0008
ds-12-Dichloroethylene NO NO u 0109
Bromochloromethane NO NO u oooa Chlorofomi NO NO u 0009 Ethyl ~Butyl Ether NO NO u 0008
12-Didlloroethane NO NO u 0009
111middot Trtdlloroethane NO NO u 0022
Benzene 0168 054 0029 Carbon Telrldllorlde 0095 oeo 0024
tertmiddotAmyl Methyl Ether NO NO u 0016
12-0Chlolgtpropane NO ND u 0023
ethyl Acrtlate NO NO u 0020
Bromodichloromethane NO NO u OOlS Trichloroethylene ND NO u 0025
MettwiMethacrylate NO NO u oc22 cis-13-0ichloropropene NO NO u 0022
~yiiiObutyiKetone 0035 014 0022
trans-13-0ichloropropene NO NO u oo2S 112middot Trichloroethane NO NO u 0025
Toluene 0373 141 0016
OibromQchloromethane NO NO u 0071
Eastern Research Group The nsults in this nport apply only to the saltlples D11alyzed in acordance with the chain Df cuampmiddottody docWMnt This analytical rttport must be repriJduced in its elllirety
Page 9 of 16
RG CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMIITED 080811 to 09291 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 4th and Santa Fe Lab ID 1090818-01 Sampled 090711 0000
Pressure Receipt 65 Hg canister ER008 Received 09081112~47
Comments Analyzed 090911 0137
Air Toxics by EPA Compendium Method T0-15 Results tmL
Analvte IUllm ll9lm flil Jmbll 12-0ibromoethane NO NO u 0018
n-Octane 0038 018 0015
Tetradiloroethylene ND NO u 0018 Chlomhenllne NO NO u 002
Ethyl benzene 0064 028 0017
mp-Xylene 0148 064 0034
Bromoform NO NO u 0025
Styrene NO NO u 0022
1122-TlliiChloroetllane NO NO u 0021
omiddotXylene 0070 031 0018
135middotTrimethylbenzene ND NO u 0026
124-Trimethylbenzene 0078 038 0028
m-Oiehlorobenzene NO NO u 0034
Chloromethylbenzene NO NO u 0019
p-Orchlorobenzene ND NO u 0348
o-Oidllorobenzene ND NO u 0037
124-Trichlorobenzene NO NO u 0036
Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The results rn Jhis teport apply cmJy 10 the samples (Uraly~ed in ac~ordant-e wilh the chain of CIISiody docunum This atwlytiral report 11111s1 be reprculuced i11 ils e11tirrty
Page 10 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN MIChael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001 030
REPORTED~ 1110111 0903
SUBMmED 0810811 to 092911
AQS SITE CODE
SITE CODE OECAwork
Description 150 west of Hwys 169 and 39 Lab ID 1091501-01 sampled 091411 oooo Pressure 0 ReClelpt 13 Hg canister 709 Received 091511 10~42
Comments Analyzed 0915111926
Air Taxies by EPA Compendium Method T0-15 BHIIIm MDI
Analyte JUlbll li9Lm fJJg JlRinl AcBtylene 0234 025 0-016 Propylene 0258 045 0-0~11
Dlchlorodlfluoromettmne 0544 270 oo11 Chloromethane 0526 109 0 012
DichlorolelrifAJoroethane NO NO u Otgt09 Vinyl chloride NO NO u 0008 13-Butildlene NO NO u 0007 Bromomettlane NO NO u 0009 Chloroethane NO NO u 0009
Acetonitrile 0130 022 0024
Trlchlorcrfluoromethane 0263 lAB 0010 Aaylonltrile NO NP u 0012 11-DIChloroethene NO NO u 0009
Dldloromelhane NO NO u (IOlD
carbon Disulfide 0032 010 u 0033 T~hlo~fluonHdhane 0107 082 0011 tr~ns-12-0ichloroethyler~ NO NO u 0008 11-Dichloroethane ljO NO u 0008 Methl tert-Butyl Ether NO NO u 0008 Methyl Ethyl Ketone 0382 113 0157
Chloroprene NO NO u 0008 ciamp-12-0ichloroethylene NO NO u 0009 Bromochloromethane NO NO u 0008 011oroform NO NO u 0009 Ethyl tert-Butyl Ether NO NO u 0008 JI-Dichloroethilne NO NO u 0009 111-Trichloroethane NO NO u (l022
Benzene ozos 067 0029
Carbon Tetrachloride 0101 064 0024 tert-Amyl Methyl Ether NO NO u 1)016 12-DJChiOropropane NO NO u 0023 Ethyl Acrylate NO NO u (1 020
Bromodichloromethane NO NO u 0025 Trichloroethylene NO NO u 0025
Methyl Methacrylilte NO NO u 0022 cis-13-Dichloropropene NO NO u 0022 Methyl Isobutyl llteDM NCI NO u 0022 trans-13-0ichloropropene NO NO u 0025 112-Trldlloroetflane NO NO u 0025 Toluene 0095 036 0016 Olbromodloromelhane NO NO u 0021
Eastern Research Group The results 111 Jhis r~port apply only to the samplts waalylui in accordance with tht chain of custody document This cuuzlytical report must in reprod~~eed in its entirety
Page 11 of 16
CERTIFICATE OF ANALYSISRG EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 111 011 0903
Kansas City KS 66101 SUBMirrED OBiOB11 to 092911
ATTN~ M1chael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE ~ OECAw(irk
Description 150 west of Hwys 169 and 39 Lab ID 1091501-01 Sampled 091411 00 00
Pressure Receipt 13 Hg canister 709 Received 0915111042
Comments Analyzed 0915111926
Air Toxlcs by EPA Compendium Method T0-15 ~ MW
Analvte wmx uqm fli1g RRint 12-Dibromoethane ND IID u 0()18
n-Oddne ND ND u 0015
Tetrachloroethylene ND ND u 0018
Ollorobenzene ND ND u 0021
Ethylbenzene 0035 015 Q017
mpmiddotXylene 0041 018 0034
Bromoform ND NO 11 0025
Styrene NO ND u 002
11-22-Tetradlloroelhane ND ND u 0024
o-Xylene ND NO u 0018
135-Trimethylbenzene NO NO u 0026
124middotTrlrnathylbenzene 0-042 021 0028
m-Dichlorohenzene ND ND u 0034
Chloromethylbenzene ND ND u 0039
p-OIChlorobenzene NO NO u 0348
o-Dichlorobenzere NO NO u 0037
12+Trlchlorobenzene NO ND u 0036
Hexachloro-13-butadlene ND ND u 0037
Eastern Research Group The result in thrs reoort applgt ltmly to the samplts mral1zed m accordanc11 ~ith thilhain of custodgt document This am1lytical report m11st be rbullpmJuced ill it~ entirety
Page 12 of 16
CERTIFrCATE OF ANALYSIS
EPA Region VII FILE tl 027800001030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMITTED 080811 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Description 73 north of Oak St on Plummer Lab ID 1092909-01 Sampled 0928110000
Pressure 0 Receipt 65 Hg canister 140 Received 0929111057
Comments Analyzed 093011 20 34
Analyte
Acetylene middotPropylene
Dldllorodifluoromethane Chlolomettlane
Dlchlorotetrafluoroethllne VInyl chloride 13-Butadlene Bromometl1dne
Chloroethane
Acetunitrile Trldllorotluoromethane
Acrylonitrile
11-0ithloroethene Dichloromethane Carbon DisulfJde
Trlchlorotrlfkloroetftane lranr1 2-0khloroethylene
11-Dithloroelhane
Methyl tert-Butyl Ether Methyl Ethyl Ketone Chloroprene ds-1HllchloiJethylene Bromochloromethane Chlorofvnn
Ethyl tert-Butyl Ether 12-Dichloroethane 111middotTriChloroethane
Benzene carbon Tetrachloride tert-Amyl Methyl Ether 12-Didlonopropane Ethyl Acrylate Bromodlchlorornelhane Trichloroethylene
Methyl MetllacrylaJ
ds-13-Dithloropropene Methyl Isobutyl KetDne trans-13-0khlorapropene 112-Trichloroethane
Toluene Olbromochloromethane
Air Toxics by EPA Compendium Method T0-15 Results mL
ORb YIiID Eiilg I1IZD 223 238 016 123 212 0039
0564 280 0~11
0525 109 0012 0018 013 ooot
NO NO u 0008 0181 040 0~07
NO NO u o009 NO NO u 0009
0157 028 0024 ozgo 163 0010
NO NO u 0(112 NO NO u 0009
0154 054 0010 0045 0 14 0033 0092 071 0011
NO NO u 0008 NO NO u 0008 NO NO u 0~08
0624 184 0157 NO NO u 0008 NO NO u 0009 NO NO u 0008
0035 017 0009 NO NO u 0008 NO NO u 0009
0012 007 u 0022 L49 477 0029
0088 o56 0024 NO NO u 0016 ND NO u 0023 NO NO u 0020 NO ND u 0025
0178 096 0025
NO NO u 0022 NO NO u 0022
0094 039 0022 NO NO u 0025 NO NO u 0025
276 10400 D 0040 r~O NO u 0021
Eastern Research Group The results m this repon apply only to the samples cmolylld in accordance wilh the chain of cUStOdy docWMnt This arwlytlcal rJort mu~middott be reproduced in its entirety
Page 13 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMITTED 0808111 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECA wa1lt
Description 75 north of Oak St on Plummer Lab ID 1092909-01 Sampled 092811 0000
Pressure Receipt 65 Hg canister 140 Received 0929111057
Comments Analyzed 0930112034
Air Toxics by EPA Compendium Method T0-15 Results lmb
Analyte mmx ugm3 flil on 12-Dibromoethane NO NO u 0018
n-Octane 0193 090 0015 Tetrachloroethylene 0019 013 0018
Chlorobenzene NO NO u 0021
Ethyl benzene 0356 155 p017 mp-Xylene 1oamp 461 OOl4
Bromoform NO NO u 6025
Sty~Wte 0060 026 0022 lll2-Tetrachloroethane NO NO u 0-024
o-Xylene P422 184 01118 135-TrlmethylbenEene 0094 046 0026 1124-Trlmethylbenzene 0340 167 0028
m-Dichlorobenzene 0043 016 0034 Chloromethylbenzene NO NO u 0039
p-Dichlorobenzene 0019 011 u 0035
rDichlorobenzellE NO NO u 0037 121-Trochlorobenzene NO NO u 0-036
Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The ll$Ults in rhis repon appl) NIhbull to the samples analyted in accordance with the cham of custody document Thta analybullical rrporl must he reproduced in in entirety
Page 14 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII FILE tl 027800001 030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS66101 SUBMmED 080811 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX~ (913) 551-5000 SITE CODE OECAwork
IAnalyte Result Units SOurce Result RPD
RPD Umit Note
Eastern Research Group ~ resulu in this reprJrt apply oraly to the samples analyed 111 accordance with the chain of crutody docunumt 1his anulmcal report must be reprodu~ed In its enrlnty
Page 15 of 16
CERTIFICATE OF ANALYSISRG EPA Region VII FILEmiddot 027800001 030
300 Minnesota Avenue REPORTED 1110 11 09middot03
Kansas City KS 66101 SUBMITTED 08101311 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX~ (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
u Under Detection Umlt
o Th1s result obtained by dilution
ND Analyte NOT DETECTED at or above the Method Detecbon Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group T1r results in thH report apply on() w the sample tmayzed il occordancltt with the cham of bullur1ody dotumnt This anayllcai report must be prwiuced in its entirety
Page 16 of 16
~RG Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
December 05 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 111511 1121
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the amtract for NMOC UATMP PAMS CSATAM and NATTS support (US EPA Contract No EPD-09-D48) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please oontact me at 919-468-7930
Sincerely
Laura Van Enwyck Project Manager lauravanenwyckergcom
The information contained in this report and its attachment(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauraJnenwyckergcom and delete the report without retairring any copies
Page 1 of6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 120511 1059
Kansas City KS 66101 SUBMITTED 111511
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Lincoln amp 39 Highway 1111501-01 Air 111411 0000 111511 1121 (111 W Lincoln)
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wfth the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001030
REPORTED 120511 1059
SUBMITTED 111511
AQS SITE CODE
SITE CODE OECAwork
DesaiptionUncoln amp 39 Highway (111 W Uncoln) Lab ID 1111501-01 Sampled 111411 0000
Pressure Receipt 8 Hg canister 636 Received 1115111121
Comments Analyzed 111611 0932
Air Toxics by EPA Compendium Method T0-15 blulb lmL
Analvte Jmbx Yllm fiG JlRbl Acetylene 0171 018 A-Ql 0016 Propylene 0272 OA7 A-Ql 0039 Dlchlorodlfluoromethane 0503 2A9 A-Ql 0011 Chloromethane OA74 098 A-Ql 0011 Dichlorobtraftuoroethane 0016 011 A-Ql 0009 Vinyl chloride ND ND A-Ql U 0008 13-Buladlene 0020 004 A-Ql 0007 Bromomethane 0011 004 AmiddotOl 0009 Chloroethane ND ND A-Ql U 0009 Acetonitrile 0138 023 A-Ql 0024 Trichloroftuoromethane D304 L71 A-Ql 0010 Acrylonitrile ND ND A-Q1 U 0012
11-Dichloroethene ND ND A-Q1 U 0009 Dichloromethane 0266 093 A-Ql 0010 Carbon Disulfide 0129 040 A-Ql 0033 Trichlorotrifluoroethane 0079 061 A-Ql 0011 trans-12-0ichloroethylene ND ND A-Ql U 0008 11-Dichloroethane ND ND A-Ql U 0008 Methyl tert-Butyl Ether ND NO A-Q1 U 0008 Methyl Ethyl Ketone 0760 us AmiddotOl 0157 Chloroprene ND NO A-Ql U 0008
cis-12-Dichloroethylene NO NO A-Ql U 0009 Bromochloromethane NO NO A-Ql U 0008 Chloroform NO NO A-Ql U 0009
Ethyl tert-Butyl Ether NO NO Amiddot01 U 0008 12-Dichloroethane 0026 011 A-Ql 0009 111-Trichloroethane 0006 003 A-Q1 U 0022 Benzene 113 362 A-Q1 0029 Carbon Tetrachloride 0069 OA4 A-Q1 0024 tert-Amyl Methyl Ether ND ND A-Ql U 0016 12-Dichloropropane ND NO A-Ql U 0023
Ethyl Acrylate NO NO A-Ql U 0020
Bromodlchloromethane ND NO A-o1 u 0025 Trichloroethylene NO ND A-01 U 0025
Methyl Methacrylate ND NO A-Q1 U 0022 cis-13-Dichloropropene NO NO A-Ql U 0022 Methyl Isobutyl Ketone 0047 019 A-Ql 0022 trans-13-Dichloropropene NO ND A-Q1 U 0025 112-Trichloroethane NO NO A-Q1 U 0025
Toluene 0661 250 A-01 0016 Dibromochloromethane NO ND A-Q1 U 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repoTt must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1210511 1059
Kansas City KS 66101 SUBMITTED 1115 11
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption Uncoln amp 39 Highway (111 W Lincoln) Lab ID 1111501-01 Sampled 111411 0000
Pressure Receipt 8 Hg canister 636 Received 1115111121
Comments Analyzed 111611 0932
Air Toxics by EPA Compendium Method T0-15 RuJID mL
AnaMe IU1bll ~ BiSl IU1bll 12-Dlbromoethane NO NO A-Ql U 0018
n-Oct3ne 0025 012 A-Ql 0015
Tetrachloroethylene 0016 011 A-Ql U 0018
Ollorobenzene NO NO A-Ql U 0021
Ethylbenzene 0068 030 A-Ql 0017
mp-Xylene 0144 063 A-Ql 0034
Bromoform NO NO A-Ql U 0025
Styrene 0058 025 A-Ql 0022
1122-Tetrachloroethane NO NO A-Ql U 0024
o-Xylene 0058 025 A-ol 0018
135-Trlmetflylbenzene 0050 025 A-01 0026
124-Trimetflylbenzene 0130 064 A-Ql 0028
m-Dichlorobenzene NO NO A-Ql U 0034
Chloromelhylbenzene NO NO A-ol U 0039
p-Oichlorobenzene 0027 016 A-Ql U 0035
o-Oichlorobenzene NO NO A-Ql U 0037
124-Trichlorobenzene NO NO A-ol U 0036
Hexachloro-13-butadiene NO NO A-ol U 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 120511 1059
Kansas City KS 66101 SUBMITTED 111511
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance witlz tlze chain of custody documellt This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1205111 1 059
Kansas City KS 66101 SUBMITTED 11151 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
A-ol Estimated value due to possible canister leak
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical re-port must be reproduced in its entirety
Page 6 of 6
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
December 15 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 1206111229
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for NMOC UATMP PAMS CSATAM and NATTS support (US EPA Contract No EPD-09-048) This rover page is an integral part of this report and any exceptions or oomments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Project Manager lauravanenwyckergcom
The information contained in this report and its attachment(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify laura vanenwyck ergcom and delete the report without retaining any copies
Page 1 of 6
RG CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111 1041
Kansas City KS 66101 SUBMITTED 1206 11
ATTN Michael F Davis AQS SITE CODE
PHONE 913) 551-5042 FAX 913) 551-5000 SITE CODE OECAwork
ANALYTlCAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Ash amp Forest SE Corner 1120611-01 Air 120411 0000 120611 1229
middotI I
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytirol repon must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
ALE 027800001030
REPORTED 1215111041
SUBMmED 1210611
AQS SITE CODE
SITE CODE OECAwork
Desaiptlon Ash amp Forest SE Comer Lab ID 1120611-01 sampled 120411 oooo Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 BuYltl MQL
AnaMe IUlllll lWm Bag IUlllll Acetylene OA36 OA7 0016 Propylene 0304 052 0039 Dichlorodiftuoromethane 0567 281 0011 Chloromethane 0566 117 0012 Dlchlorotetnlftuoroethane 0019 013 0009 Vinyl chloride NO NO u 0008 13-Butadiene NO NO u 0007 Bromomethane 0012 005 0009 Chloroethane NO NO u 0009 Acetonitrile 0111 019 0024 Trichlorofluoromethane 0284 160 0010 Aaylonitrile ND NO u 0012 11-Dichloroethene ND ND u 0009 Dichloromethane 0083 029 0010 Carbon Disulfide 0019 006 u 0033
Trlchlorotrlftuoroethane 0099 076 0011 trans-12-Dichloroethylene ND ND u 0008 11-Dichloroethane ND NO u 0008 Methyl tert-Butyl Ether NO NO u 0008 Methyl Ethyl Ketone 0536 158 0157 Chloroprene NO NO u 0008 cis-12-Dichloroethylene NO ND u 0009 Bromochloromethane NO NO u 0008 Chloroform 0022 011 0009 Ethyl tert-Butyl Ether NO NO u 0008 12-Dichloroethane 0025 010 0009 111-Trichloroethane 0011 006 u 0022 Benzene 0188 060 0029 carbon Tetrachloride 0106 067 0024 tert-Amyl Methyl Ether NO NO u 0016 12-Dichloropropane NO NO u 0023 Ethyl Acrylate ND NO u 0020
Bromodichloromethane NO NO u 0025 Trichloroethylene NO NO u 0025 Methyl Methacrylate NO NO u 0022 cis-13-Dichloropropene NO NO u 0022
Methyl Isobutyl Ketone 0042 017 0022 trans-13-Dichloropropene ND NO u 0025 112-Trichloroethane NO NO u 0025
Toluene 0149 056 0016 Oibromochloromethane 0003 003 u 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproducedin its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 121511 1041
Kansas City KS 66101 SUBMmED 1210611
ATTN Michael F Davis AQS SITE CODE
PHONE (913 551-5042 FAX (913 551-5000 SITE CODE OECAwork
Description Ash amp Forest SE Comer Lab ID 1120611-01 Sampled 120411 0000
Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 llWdtl MID
Analyte ubll IUllm Bag ubll 12-0ibromoethane NO NO u 0018 nmiddotOctane 0044 021 0015 Tetrachloroethylene 0006 004 u 0018
Chlorobenzene NO NO u 0021 Ethylbenzene 0047 021 0017 mp-Xylene 0070 031 0034 Bromoform NO NO u 0025 Styrene 0034 015 0022 1122-Tetrachloroethane NO NO u 0024 o-Xylene 0036 016 0018 135-Trlmethylbenzene 0025 012 u 0026 124-Trlmetllylbenzene 0047 023 0028 m-Oichlorobenzene NO NO u 0034
Chloromethylbenzene NO NO u 0039 p-Dichlorcbenzene 0005 003 u 0348 a-Dichlorobenzene NO NO u 0037
124-Trlchlorobenzene NO NO u 0036 Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repon must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS~RG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 66101 SUBMITTED 12061 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPDIAnalyte Result Units Result RPD um1t Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 661 01 SUBMITTED 120611
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its enJirety
Page 6 of 6
i
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
March 12 2012
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 030512 0916
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for UATMP NATTS CSATAM PAMS and NMOC support (US EPA Contract No 68-D-Q9-048) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Program Manager lauravanenwyckergcom
The information contained in this report and its attachmcnt(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauravanenwyckergcom and delete the report dthout retaining any copies
Page 1 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 0312112 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
6th St between Central amp 2030501-01 Air 030212 0000 030512 0916 Malcom
Eastern Research Group The results in this report apply only to the samples anal zed in accordance With the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Aven ue REPORTED 031212 1 051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 ~ tml
Analvte RRbll Y9lD1 flu RRbll Acetylene 0627 067 0072 Propylene 0484 084 0033
Dichlorodllluoromethane 0500 248 0023 Chloromethane 0557 115 0033
Dichlorotetrafluoroethane 0015 011 0012 Vinyl chloride NO NO u 0011
13-Butadlene 0036 oo8 0011
Bromomethane 0012 005 0012 Chloroethane NO NO u 0017
Acetonitrile 0073 012 0073
Trichlorofluoromethane 0258 145 0015 Acrylonitrile NO NO u 0020
11-0ichloroethene NO NO u 0014
Dichloromethane 0185 064 0023
Carbon Disulfide 0037 012 0014 Trichlorobitluoroethane 0119 091 0017
trans-12-0ichloroethylene NO NO u 0012
11-0ichloroethane NO NO u 0015
Methyl tert-Butyl Ether NO NO u 0011
Chloroprene NO NO u 0012
ds-12-0ich loroethylene NO NO u OD18
Bromochloromethane NO NO u 0014
Chloroform NO ND u 0014
Ethyl tert-Butyl Ether NO NO u 0011
12-Dichloroethane 0019 008 0016
111-Trichloroethane 0012 007 u 0020
Benzene 0344 L10 0061 Carbon Tetrachloride 0088 056 0024
tert-Amyl Methyl Ether NO NO u 0016
12-0ichloropropane ND NO u 0019
Ethyl Acrylate ND NO u 0014
Bromodichloromethane ND NO u 0021
Trichloroethylene NO ND u 0022
Methyl Methacrylate ND NO u 0025
ds-13-0ichloropropene NO NO u 0015
Methyl Isobutyl Ketone 0015 oo6 0015
trans-13-0ichloropropene NO ND u 0016
112-Trichloroethane NO NO u 0021
Toluene 0416 157 0045
Oibromochloromethane ND NO u 0018
12-0ibromoethane ND NO u 0017
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551 -5000
FILE 027800001030
REPORTED 0312 12 1051
SUBMITTED 030512
AQS SITE CODE
SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 Bwdtl MJlL
Analvte Jmbll Y9Lm Big Jmbx nmiddotOclane 0039 018 0020 Tetrachloroethylene 0005 003 u 0020
Chlorobenzene ND ND u 0025
Ethylbenzene 0045 020 0023 mp-Xylene 0112 OA9 0037 Bromoform ND ND u 0020
Styrene 0030 013 0024 1122-Tetrachloroethane ND ND u 0018
o-Xylene 0050 022 0020
135-Trimethylbenzene 0019 009 u 0022
124-Trimethylbenzene 0047 023 0025 m-Dichlorobenzene ND ND u 0024
p-Dichlorobenzene 0004 002 u 0019
a-Dichlorobenzene NO ND u 0021
124-Trichlorobenzene ND ND u 0022
Hexachloro-13-butadiene ND ND u 0022
Eastern Research Group The results in this report apply only 1o the samples analyzed in accordance with the chain of custody document This analytical rep ort must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 031212 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wilh the chain of custody document This analytical report must be reproduced in its enrirety
Page 5 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 03121121051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report nutst be reproduced in its entirety
Page 6 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN~ Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001 030
REPORTEDmiddot 111011 0903
SUBMITIED 080811 tci 092911
AQS SITE CODE
SITE CODE OECAwork
Description Ash amp Forest Intersection Lab ID 1082901-01 Sampled 082611 oomiddotoo Pressure Receipt 8 Hg canister 020 Received 082911 0948
COmments Background Sample Analyzed 083011 0036
Air Taxies by EPA Compendium Method T0-15 Results MnL
Analvte mmx Y9lm fml ~ Acetylene 0A94 053 0016 Propylena OA34 o7s 0039 Dlchlorocllrluoromllthane 0553 274 0011 chloR)IIIIIthane 0604 125 0012 Dldlorollltniftuoroethane 0024 017 0009 VInyl dlorlde 0008 002 opoa 13-Butadlene 0028 0 06 op01 Bromomethane 0016 006 0009
Olloroethane NO NO u 0009 Aatonitrila 0217 037 0024 Tr1dtlorofluorometllane 0211 164 0010
Aaylonltrile NO NO u 0012
11-Didlloroethene NO NO u 0009
Dlchloromethane 0404 141 0010 carbon Disulfide 0161 0 50 0033 Trldlorotrlfluoroethane 0117 otO 0011 trans-12-0khloroeth~ene NO NO u ooos 11-0ichloroethane NO NO u 0008
Methyl tPrt-sutvt Ether NO NO u 0008
Methyl Ethyl Ketone 111 328 0157
Chloroprene ND NO u 0008 ds-12-Dichloroethvlent NO NO u 0009
Bromochloromethane NO NO u 0008
Chlororgtnn 0043 021 0001
Ethyl tert-iutyl Ether NO ND u 0008 12middotDichloroethene 0030 012 0001 111middot TriChloroethane 0018 010 u op22
Benzene 0225 072 OOZ9
Carbon Tetrachloride 0098 0amp2 Op24
tert-Amyl Methyl Ether ND NO u 0016
12-0ichloropropane NO NO u 0023
Ethyl Acrylate ND NO u 0020
Bromod1chloromethane 0011 007 u 0025
Trichloroethylene 0 015 008 U 0025
Methyl Methaaylate NO NO u 0022
ds-13-0idlloropropene NO NO u 0022
Methyl Isobutyl Ketone 0052 021 0022
trans-13-0ichloropropene ND NO u 0025
112middot Tnrhloroethane ND NO u 0025
Toluene 514 1940 0016
Olbromochloromethane 0008 007 u 0021
Eastern Research Group lh~ results in this report apply only to the sample 011alyud in accordance with tht rhain of cusrody documtmr This OJialytlcal nport musliM -Produced in its mirery
Page 7 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN~ Michael F DaviS
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001 030
REPORTED 111 Oi11 0903
SUBMITTED 08108111 to 092911
AQS SITE CODE
SITE CODE OECAwork
Description Ash amp Fcorest Intersection Lab ID 1082901-01 Sampled 082611 0000
Pressure I Receipt 8 Hg Canister 020 Received 082911 09~48
Comments Background Sample Analyzed 083011 0036
Air Toxics by EPA Compendium Method T0-15 Results MW
Anayte DDIn Y9lm Eiim IU2bll 12-Dibromoethane NO ND u 0018
n-Ocblne 0074 035 0015
Ttrachloroethylene 0026 018 0018
Chlorobenzene ND ND u 0021
Ethylbenzene 0218 0-95 0017
mp-Xylene 0551 2AO 0034
Bromoform ND ND u (105
Styrene 0089 038 0022
1122-Tetrachloroethane 0010 0 07 u 0024
a-Xylene 0189 082 0018
135-Trlmethylbenzene 0062 031 0026
124-Trimethylbenzene 0150 074 0028
m-Dichlorobenzene 0006 004 u 0034
Chloromethylbenzene NO ND u 0039
p-Dichlorobenzene 0032 019 u 0348
o-Ochlorobenzene 0006 004 u 0037
124-Trlchlorobenzene 1110 NO u 0036
Hexachloro-13-bullldlene 0008 009 u 0037
Eastern Research Group Tlze bullesuJs m this repon apply on)middot to the sanrpfamp nnalyud ill acordance wh lht chain of custody Joumumt Thi~ OIIOI)middottical report musbull be teptoJduced In its elltiJtty
Page 8 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMilTED 0808111 to 0929111
ATTN Michael F Davts AQS SITE CODE
PHONE 913) 551-5042 FAX (913) 551middot5000 SITE CODE OECAwork
Description 4th and Santa Fe Lab ID 1090818-01 Sampled 090711 0000
Pressure 0 Receipt 6 5 Hg Canister EROOB Received 0908111247
Comments Analyzed 090911 0137
AirToxics by EPA Compendium Method T0-15 BciYlb MQI
Analyte lUlblpound usLm fOOl ~ Acetylene 0175 029 0016 Propylene 0333 057 op39 Dichlorodifluoromethane 0521 258 0011 Chloromethane 0507 LOS oou Okhlorotetrafluoroeihane NO NO u 0009
Vinyl chloride NO NO u OOilll 13-Butadlene NO NO u 0007
Bromomethane NO NO u 0009 Chloroethane NO NO u 0009 AletDnibile 0122 021 0024
Tr1dlloroftuoromethane 0252 142 0010 Acrylonlbile NO NO u 0012 11-0ldlloroethPne NO NO u 0009 Dldlloromethane 0159 055 0010
Carbon Disulfide 0063 020 0033 Trlchlorotrlfluoroethane 0094 072 OJ11
trans-12-Dichloroethylene NO NO u 0008
11-0lchloroethane NO NO u ouoa Methyl tert-BlJtyl Ether NO NO u o~
Ne~IEthyiKetone 0472 139 0157 Chloroprene NO NO u 0008
ds-12-Dichloroethylene NO NO u 0109
Bromochloromethane NO NO u oooa Chlorofomi NO NO u 0009 Ethyl ~Butyl Ether NO NO u 0008
12-Didlloroethane NO NO u 0009
111middot Trtdlloroethane NO NO u 0022
Benzene 0168 054 0029 Carbon Telrldllorlde 0095 oeo 0024
tertmiddotAmyl Methyl Ether NO NO u 0016
12-0Chlolgtpropane NO ND u 0023
ethyl Acrtlate NO NO u 0020
Bromodichloromethane NO NO u OOlS Trichloroethylene ND NO u 0025
MettwiMethacrylate NO NO u oc22 cis-13-0ichloropropene NO NO u 0022
~yiiiObutyiKetone 0035 014 0022
trans-13-0ichloropropene NO NO u oo2S 112middot Trichloroethane NO NO u 0025
Toluene 0373 141 0016
OibromQchloromethane NO NO u 0071
Eastern Research Group The nsults in this nport apply only to the saltlples D11alyzed in acordance with the chain Df cuampmiddottody docWMnt This analytical rttport must be repriJduced in its elllirety
Page 9 of 16
RG CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMIITED 080811 to 09291 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 4th and Santa Fe Lab ID 1090818-01 Sampled 090711 0000
Pressure Receipt 65 Hg canister ER008 Received 09081112~47
Comments Analyzed 090911 0137
Air Toxics by EPA Compendium Method T0-15 Results tmL
Analvte IUllm ll9lm flil Jmbll 12-0ibromoethane NO NO u 0018
n-Octane 0038 018 0015
Tetradiloroethylene ND NO u 0018 Chlomhenllne NO NO u 002
Ethyl benzene 0064 028 0017
mp-Xylene 0148 064 0034
Bromoform NO NO u 0025
Styrene NO NO u 0022
1122-TlliiChloroetllane NO NO u 0021
omiddotXylene 0070 031 0018
135middotTrimethylbenzene ND NO u 0026
124-Trimethylbenzene 0078 038 0028
m-Oiehlorobenzene NO NO u 0034
Chloromethylbenzene NO NO u 0019
p-Orchlorobenzene ND NO u 0348
o-Oidllorobenzene ND NO u 0037
124-Trichlorobenzene NO NO u 0036
Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The results rn Jhis teport apply cmJy 10 the samples (Uraly~ed in ac~ordant-e wilh the chain of CIISiody docunum This atwlytiral report 11111s1 be reprculuced i11 ils e11tirrty
Page 10 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN MIChael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001 030
REPORTED~ 1110111 0903
SUBMmED 0810811 to 092911
AQS SITE CODE
SITE CODE OECAwork
Description 150 west of Hwys 169 and 39 Lab ID 1091501-01 sampled 091411 oooo Pressure 0 ReClelpt 13 Hg canister 709 Received 091511 10~42
Comments Analyzed 0915111926
Air Taxies by EPA Compendium Method T0-15 BHIIIm MDI
Analyte JUlbll li9Lm fJJg JlRinl AcBtylene 0234 025 0-016 Propylene 0258 045 0-0~11
Dlchlorodlfluoromettmne 0544 270 oo11 Chloromethane 0526 109 0 012
DichlorolelrifAJoroethane NO NO u Otgt09 Vinyl chloride NO NO u 0008 13-Butildlene NO NO u 0007 Bromomettlane NO NO u 0009 Chloroethane NO NO u 0009
Acetonitrile 0130 022 0024
Trlchlorcrfluoromethane 0263 lAB 0010 Aaylonltrile NO NP u 0012 11-DIChloroethene NO NO u 0009
Dldloromelhane NO NO u (IOlD
carbon Disulfide 0032 010 u 0033 T~hlo~fluonHdhane 0107 082 0011 tr~ns-12-0ichloroethyler~ NO NO u 0008 11-Dichloroethane ljO NO u 0008 Methl tert-Butyl Ether NO NO u 0008 Methyl Ethyl Ketone 0382 113 0157
Chloroprene NO NO u 0008 ciamp-12-0ichloroethylene NO NO u 0009 Bromochloromethane NO NO u 0008 011oroform NO NO u 0009 Ethyl tert-Butyl Ether NO NO u 0008 JI-Dichloroethilne NO NO u 0009 111-Trichloroethane NO NO u (l022
Benzene ozos 067 0029
Carbon Tetrachloride 0101 064 0024 tert-Amyl Methyl Ether NO NO u 1)016 12-DJChiOropropane NO NO u 0023 Ethyl Acrylate NO NO u (1 020
Bromodichloromethane NO NO u 0025 Trichloroethylene NO NO u 0025
Methyl Methacrylilte NO NO u 0022 cis-13-Dichloropropene NO NO u 0022 Methyl Isobutyl llteDM NCI NO u 0022 trans-13-0ichloropropene NO NO u 0025 112-Trldlloroetflane NO NO u 0025 Toluene 0095 036 0016 Olbromodloromelhane NO NO u 0021
Eastern Research Group The results 111 Jhis r~port apply only to the samplts waalylui in accordance with tht chain of custody document This cuuzlytical report must in reprod~~eed in its entirety
Page 11 of 16
CERTIFICATE OF ANALYSISRG EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 111 011 0903
Kansas City KS 66101 SUBMirrED OBiOB11 to 092911
ATTN~ M1chael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE ~ OECAw(irk
Description 150 west of Hwys 169 and 39 Lab ID 1091501-01 Sampled 091411 00 00
Pressure Receipt 13 Hg canister 709 Received 0915111042
Comments Analyzed 0915111926
Air Toxlcs by EPA Compendium Method T0-15 ~ MW
Analvte wmx uqm fli1g RRint 12-Dibromoethane ND IID u 0()18
n-Oddne ND ND u 0015
Tetrachloroethylene ND ND u 0018
Ollorobenzene ND ND u 0021
Ethylbenzene 0035 015 Q017
mpmiddotXylene 0041 018 0034
Bromoform ND NO 11 0025
Styrene NO ND u 002
11-22-Tetradlloroelhane ND ND u 0024
o-Xylene ND NO u 0018
135-Trimethylbenzene NO NO u 0026
124middotTrlrnathylbenzene 0-042 021 0028
m-Dichlorohenzene ND ND u 0034
Chloromethylbenzene ND ND u 0039
p-OIChlorobenzene NO NO u 0348
o-Dichlorobenzere NO NO u 0037
12+Trlchlorobenzene NO ND u 0036
Hexachloro-13-butadlene ND ND u 0037
Eastern Research Group The result in thrs reoort applgt ltmly to the samplts mral1zed m accordanc11 ~ith thilhain of custodgt document This am1lytical report m11st be rbullpmJuced ill it~ entirety
Page 12 of 16
CERTIFrCATE OF ANALYSIS
EPA Region VII FILE tl 027800001030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMITTED 080811 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Description 73 north of Oak St on Plummer Lab ID 1092909-01 Sampled 0928110000
Pressure 0 Receipt 65 Hg canister 140 Received 0929111057
Comments Analyzed 093011 20 34
Analyte
Acetylene middotPropylene
Dldllorodifluoromethane Chlolomettlane
Dlchlorotetrafluoroethllne VInyl chloride 13-Butadlene Bromometl1dne
Chloroethane
Acetunitrile Trldllorotluoromethane
Acrylonitrile
11-0ithloroethene Dichloromethane Carbon DisulfJde
Trlchlorotrlfkloroetftane lranr1 2-0khloroethylene
11-Dithloroelhane
Methyl tert-Butyl Ether Methyl Ethyl Ketone Chloroprene ds-1HllchloiJethylene Bromochloromethane Chlorofvnn
Ethyl tert-Butyl Ether 12-Dichloroethane 111middotTriChloroethane
Benzene carbon Tetrachloride tert-Amyl Methyl Ether 12-Didlonopropane Ethyl Acrylate Bromodlchlorornelhane Trichloroethylene
Methyl MetllacrylaJ
ds-13-Dithloropropene Methyl Isobutyl KetDne trans-13-0khlorapropene 112-Trichloroethane
Toluene Olbromochloromethane
Air Toxics by EPA Compendium Method T0-15 Results mL
ORb YIiID Eiilg I1IZD 223 238 016 123 212 0039
0564 280 0~11
0525 109 0012 0018 013 ooot
NO NO u 0008 0181 040 0~07
NO NO u o009 NO NO u 0009
0157 028 0024 ozgo 163 0010
NO NO u 0(112 NO NO u 0009
0154 054 0010 0045 0 14 0033 0092 071 0011
NO NO u 0008 NO NO u 0008 NO NO u 0~08
0624 184 0157 NO NO u 0008 NO NO u 0009 NO NO u 0008
0035 017 0009 NO NO u 0008 NO NO u 0009
0012 007 u 0022 L49 477 0029
0088 o56 0024 NO NO u 0016 ND NO u 0023 NO NO u 0020 NO ND u 0025
0178 096 0025
NO NO u 0022 NO NO u 0022
0094 039 0022 NO NO u 0025 NO NO u 0025
276 10400 D 0040 r~O NO u 0021
Eastern Research Group The results m this repon apply only to the samples cmolylld in accordance wilh the chain of cUStOdy docWMnt This arwlytlcal rJort mu~middott be reproduced in its entirety
Page 13 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMITTED 0808111 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECA wa1lt
Description 75 north of Oak St on Plummer Lab ID 1092909-01 Sampled 092811 0000
Pressure Receipt 65 Hg canister 140 Received 0929111057
Comments Analyzed 0930112034
Air Toxics by EPA Compendium Method T0-15 Results lmb
Analyte mmx ugm3 flil on 12-Dibromoethane NO NO u 0018
n-Octane 0193 090 0015 Tetrachloroethylene 0019 013 0018
Chlorobenzene NO NO u 0021
Ethyl benzene 0356 155 p017 mp-Xylene 1oamp 461 OOl4
Bromoform NO NO u 6025
Sty~Wte 0060 026 0022 lll2-Tetrachloroethane NO NO u 0-024
o-Xylene P422 184 01118 135-TrlmethylbenEene 0094 046 0026 1124-Trlmethylbenzene 0340 167 0028
m-Dichlorobenzene 0043 016 0034 Chloromethylbenzene NO NO u 0039
p-Dichlorobenzene 0019 011 u 0035
rDichlorobenzellE NO NO u 0037 121-Trochlorobenzene NO NO u 0-036
Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The ll$Ults in rhis repon appl) NIhbull to the samples analyted in accordance with the cham of custody document Thta analybullical rrporl must he reproduced in in entirety
Page 14 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII FILE tl 027800001 030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS66101 SUBMmED 080811 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX~ (913) 551-5000 SITE CODE OECAwork
IAnalyte Result Units SOurce Result RPD
RPD Umit Note
Eastern Research Group ~ resulu in this reprJrt apply oraly to the samples analyed 111 accordance with the chain of crutody docunumt 1his anulmcal report must be reprodu~ed In its enrlnty
Page 15 of 16
CERTIFICATE OF ANALYSISRG EPA Region VII FILEmiddot 027800001 030
300 Minnesota Avenue REPORTED 1110 11 09middot03
Kansas City KS 66101 SUBMITTED 08101311 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX~ (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
u Under Detection Umlt
o Th1s result obtained by dilution
ND Analyte NOT DETECTED at or above the Method Detecbon Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group T1r results in thH report apply on() w the sample tmayzed il occordancltt with the cham of bullur1ody dotumnt This anayllcai report must be prwiuced in its entirety
Page 16 of 16
~RG Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
December 05 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 111511 1121
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the amtract for NMOC UATMP PAMS CSATAM and NATTS support (US EPA Contract No EPD-09-D48) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please oontact me at 919-468-7930
Sincerely
Laura Van Enwyck Project Manager lauravanenwyckergcom
The information contained in this report and its attachment(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauraJnenwyckergcom and delete the report without retairring any copies
Page 1 of6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 120511 1059
Kansas City KS 66101 SUBMITTED 111511
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Lincoln amp 39 Highway 1111501-01 Air 111411 0000 111511 1121 (111 W Lincoln)
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wfth the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001030
REPORTED 120511 1059
SUBMITTED 111511
AQS SITE CODE
SITE CODE OECAwork
DesaiptionUncoln amp 39 Highway (111 W Uncoln) Lab ID 1111501-01 Sampled 111411 0000
Pressure Receipt 8 Hg canister 636 Received 1115111121
Comments Analyzed 111611 0932
Air Toxics by EPA Compendium Method T0-15 blulb lmL
Analvte Jmbx Yllm fiG JlRbl Acetylene 0171 018 A-Ql 0016 Propylene 0272 OA7 A-Ql 0039 Dlchlorodlfluoromethane 0503 2A9 A-Ql 0011 Chloromethane OA74 098 A-Ql 0011 Dichlorobtraftuoroethane 0016 011 A-Ql 0009 Vinyl chloride ND ND A-Ql U 0008 13-Buladlene 0020 004 A-Ql 0007 Bromomethane 0011 004 AmiddotOl 0009 Chloroethane ND ND A-Ql U 0009 Acetonitrile 0138 023 A-Ql 0024 Trichloroftuoromethane D304 L71 A-Ql 0010 Acrylonitrile ND ND A-Q1 U 0012
11-Dichloroethene ND ND A-Q1 U 0009 Dichloromethane 0266 093 A-Ql 0010 Carbon Disulfide 0129 040 A-Ql 0033 Trichlorotrifluoroethane 0079 061 A-Ql 0011 trans-12-0ichloroethylene ND ND A-Ql U 0008 11-Dichloroethane ND ND A-Ql U 0008 Methyl tert-Butyl Ether ND NO A-Q1 U 0008 Methyl Ethyl Ketone 0760 us AmiddotOl 0157 Chloroprene ND NO A-Ql U 0008
cis-12-Dichloroethylene NO NO A-Ql U 0009 Bromochloromethane NO NO A-Ql U 0008 Chloroform NO NO A-Ql U 0009
Ethyl tert-Butyl Ether NO NO Amiddot01 U 0008 12-Dichloroethane 0026 011 A-Ql 0009 111-Trichloroethane 0006 003 A-Q1 U 0022 Benzene 113 362 A-Q1 0029 Carbon Tetrachloride 0069 OA4 A-Q1 0024 tert-Amyl Methyl Ether ND ND A-Ql U 0016 12-Dichloropropane ND NO A-Ql U 0023
Ethyl Acrylate NO NO A-Ql U 0020
Bromodlchloromethane ND NO A-o1 u 0025 Trichloroethylene NO ND A-01 U 0025
Methyl Methacrylate ND NO A-Q1 U 0022 cis-13-Dichloropropene NO NO A-Ql U 0022 Methyl Isobutyl Ketone 0047 019 A-Ql 0022 trans-13-Dichloropropene NO ND A-Q1 U 0025 112-Trichloroethane NO NO A-Q1 U 0025
Toluene 0661 250 A-01 0016 Dibromochloromethane NO ND A-Q1 U 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repoTt must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1210511 1059
Kansas City KS 66101 SUBMITTED 1115 11
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption Uncoln amp 39 Highway (111 W Lincoln) Lab ID 1111501-01 Sampled 111411 0000
Pressure Receipt 8 Hg canister 636 Received 1115111121
Comments Analyzed 111611 0932
Air Toxics by EPA Compendium Method T0-15 RuJID mL
AnaMe IU1bll ~ BiSl IU1bll 12-Dlbromoethane NO NO A-Ql U 0018
n-Oct3ne 0025 012 A-Ql 0015
Tetrachloroethylene 0016 011 A-Ql U 0018
Ollorobenzene NO NO A-Ql U 0021
Ethylbenzene 0068 030 A-Ql 0017
mp-Xylene 0144 063 A-Ql 0034
Bromoform NO NO A-Ql U 0025
Styrene 0058 025 A-Ql 0022
1122-Tetrachloroethane NO NO A-Ql U 0024
o-Xylene 0058 025 A-ol 0018
135-Trlmetflylbenzene 0050 025 A-01 0026
124-Trimetflylbenzene 0130 064 A-Ql 0028
m-Dichlorobenzene NO NO A-Ql U 0034
Chloromelhylbenzene NO NO A-ol U 0039
p-Oichlorobenzene 0027 016 A-Ql U 0035
o-Oichlorobenzene NO NO A-Ql U 0037
124-Trichlorobenzene NO NO A-ol U 0036
Hexachloro-13-butadiene NO NO A-ol U 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 120511 1059
Kansas City KS 66101 SUBMITTED 111511
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance witlz tlze chain of custody documellt This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1205111 1 059
Kansas City KS 66101 SUBMITTED 11151 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
A-ol Estimated value due to possible canister leak
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical re-port must be reproduced in its entirety
Page 6 of 6
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
December 15 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 1206111229
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for NMOC UATMP PAMS CSATAM and NATTS support (US EPA Contract No EPD-09-048) This rover page is an integral part of this report and any exceptions or oomments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Project Manager lauravanenwyckergcom
The information contained in this report and its attachment(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify laura vanenwyck ergcom and delete the report without retaining any copies
Page 1 of 6
RG CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111 1041
Kansas City KS 66101 SUBMITTED 1206 11
ATTN Michael F Davis AQS SITE CODE
PHONE 913) 551-5042 FAX 913) 551-5000 SITE CODE OECAwork
ANALYTlCAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Ash amp Forest SE Corner 1120611-01 Air 120411 0000 120611 1229
middotI I
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytirol repon must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
ALE 027800001030
REPORTED 1215111041
SUBMmED 1210611
AQS SITE CODE
SITE CODE OECAwork
Desaiptlon Ash amp Forest SE Comer Lab ID 1120611-01 sampled 120411 oooo Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 BuYltl MQL
AnaMe IUlllll lWm Bag IUlllll Acetylene OA36 OA7 0016 Propylene 0304 052 0039 Dichlorodiftuoromethane 0567 281 0011 Chloromethane 0566 117 0012 Dlchlorotetnlftuoroethane 0019 013 0009 Vinyl chloride NO NO u 0008 13-Butadiene NO NO u 0007 Bromomethane 0012 005 0009 Chloroethane NO NO u 0009 Acetonitrile 0111 019 0024 Trichlorofluoromethane 0284 160 0010 Aaylonitrile ND NO u 0012 11-Dichloroethene ND ND u 0009 Dichloromethane 0083 029 0010 Carbon Disulfide 0019 006 u 0033
Trlchlorotrlftuoroethane 0099 076 0011 trans-12-Dichloroethylene ND ND u 0008 11-Dichloroethane ND NO u 0008 Methyl tert-Butyl Ether NO NO u 0008 Methyl Ethyl Ketone 0536 158 0157 Chloroprene NO NO u 0008 cis-12-Dichloroethylene NO ND u 0009 Bromochloromethane NO NO u 0008 Chloroform 0022 011 0009 Ethyl tert-Butyl Ether NO NO u 0008 12-Dichloroethane 0025 010 0009 111-Trichloroethane 0011 006 u 0022 Benzene 0188 060 0029 carbon Tetrachloride 0106 067 0024 tert-Amyl Methyl Ether NO NO u 0016 12-Dichloropropane NO NO u 0023 Ethyl Acrylate ND NO u 0020
Bromodichloromethane NO NO u 0025 Trichloroethylene NO NO u 0025 Methyl Methacrylate NO NO u 0022 cis-13-Dichloropropene NO NO u 0022
Methyl Isobutyl Ketone 0042 017 0022 trans-13-Dichloropropene ND NO u 0025 112-Trichloroethane NO NO u 0025
Toluene 0149 056 0016 Oibromochloromethane 0003 003 u 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproducedin its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 121511 1041
Kansas City KS 66101 SUBMmED 1210611
ATTN Michael F Davis AQS SITE CODE
PHONE (913 551-5042 FAX (913 551-5000 SITE CODE OECAwork
Description Ash amp Forest SE Comer Lab ID 1120611-01 Sampled 120411 0000
Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 llWdtl MID
Analyte ubll IUllm Bag ubll 12-0ibromoethane NO NO u 0018 nmiddotOctane 0044 021 0015 Tetrachloroethylene 0006 004 u 0018
Chlorobenzene NO NO u 0021 Ethylbenzene 0047 021 0017 mp-Xylene 0070 031 0034 Bromoform NO NO u 0025 Styrene 0034 015 0022 1122-Tetrachloroethane NO NO u 0024 o-Xylene 0036 016 0018 135-Trlmethylbenzene 0025 012 u 0026 124-Trlmetllylbenzene 0047 023 0028 m-Oichlorobenzene NO NO u 0034
Chloromethylbenzene NO NO u 0039 p-Dichlorcbenzene 0005 003 u 0348 a-Dichlorobenzene NO NO u 0037
124-Trlchlorobenzene NO NO u 0036 Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repon must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS~RG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 66101 SUBMITTED 12061 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPDIAnalyte Result Units Result RPD um1t Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 661 01 SUBMITTED 120611
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its enJirety
Page 6 of 6
i
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
March 12 2012
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 030512 0916
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for UATMP NATTS CSATAM PAMS and NMOC support (US EPA Contract No 68-D-Q9-048) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Program Manager lauravanenwyckergcom
The information contained in this report and its attachmcnt(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauravanenwyckergcom and delete the report dthout retaining any copies
Page 1 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 0312112 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
6th St between Central amp 2030501-01 Air 030212 0000 030512 0916 Malcom
Eastern Research Group The results in this report apply only to the samples anal zed in accordance With the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Aven ue REPORTED 031212 1 051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 ~ tml
Analvte RRbll Y9lD1 flu RRbll Acetylene 0627 067 0072 Propylene 0484 084 0033
Dichlorodllluoromethane 0500 248 0023 Chloromethane 0557 115 0033
Dichlorotetrafluoroethane 0015 011 0012 Vinyl chloride NO NO u 0011
13-Butadlene 0036 oo8 0011
Bromomethane 0012 005 0012 Chloroethane NO NO u 0017
Acetonitrile 0073 012 0073
Trichlorofluoromethane 0258 145 0015 Acrylonitrile NO NO u 0020
11-0ichloroethene NO NO u 0014
Dichloromethane 0185 064 0023
Carbon Disulfide 0037 012 0014 Trichlorobitluoroethane 0119 091 0017
trans-12-0ichloroethylene NO NO u 0012
11-0ichloroethane NO NO u 0015
Methyl tert-Butyl Ether NO NO u 0011
Chloroprene NO NO u 0012
ds-12-0ich loroethylene NO NO u OD18
Bromochloromethane NO NO u 0014
Chloroform NO ND u 0014
Ethyl tert-Butyl Ether NO NO u 0011
12-Dichloroethane 0019 008 0016
111-Trichloroethane 0012 007 u 0020
Benzene 0344 L10 0061 Carbon Tetrachloride 0088 056 0024
tert-Amyl Methyl Ether NO NO u 0016
12-0ichloropropane ND NO u 0019
Ethyl Acrylate ND NO u 0014
Bromodichloromethane ND NO u 0021
Trichloroethylene NO ND u 0022
Methyl Methacrylate ND NO u 0025
ds-13-0ichloropropene NO NO u 0015
Methyl Isobutyl Ketone 0015 oo6 0015
trans-13-0ichloropropene NO ND u 0016
112-Trichloroethane NO NO u 0021
Toluene 0416 157 0045
Oibromochloromethane ND NO u 0018
12-0ibromoethane ND NO u 0017
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551 -5000
FILE 027800001030
REPORTED 0312 12 1051
SUBMITTED 030512
AQS SITE CODE
SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 Bwdtl MJlL
Analvte Jmbll Y9Lm Big Jmbx nmiddotOclane 0039 018 0020 Tetrachloroethylene 0005 003 u 0020
Chlorobenzene ND ND u 0025
Ethylbenzene 0045 020 0023 mp-Xylene 0112 OA9 0037 Bromoform ND ND u 0020
Styrene 0030 013 0024 1122-Tetrachloroethane ND ND u 0018
o-Xylene 0050 022 0020
135-Trimethylbenzene 0019 009 u 0022
124-Trimethylbenzene 0047 023 0025 m-Dichlorobenzene ND ND u 0024
p-Dichlorobenzene 0004 002 u 0019
a-Dichlorobenzene NO ND u 0021
124-Trichlorobenzene ND ND u 0022
Hexachloro-13-butadiene ND ND u 0022
Eastern Research Group The results in this report apply only 1o the samples analyzed in accordance with the chain of custody document This analytical rep ort must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 031212 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wilh the chain of custody document This analytical report must be reproduced in its enrirety
Page 5 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 03121121051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report nutst be reproduced in its entirety
Page 6 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN~ Michael F DaviS
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001 030
REPORTED 111 Oi11 0903
SUBMITTED 08108111 to 092911
AQS SITE CODE
SITE CODE OECAwork
Description Ash amp Fcorest Intersection Lab ID 1082901-01 Sampled 082611 0000
Pressure I Receipt 8 Hg Canister 020 Received 082911 09~48
Comments Background Sample Analyzed 083011 0036
Air Toxics by EPA Compendium Method T0-15 Results MW
Anayte DDIn Y9lm Eiim IU2bll 12-Dibromoethane NO ND u 0018
n-Ocblne 0074 035 0015
Ttrachloroethylene 0026 018 0018
Chlorobenzene ND ND u 0021
Ethylbenzene 0218 0-95 0017
mp-Xylene 0551 2AO 0034
Bromoform ND ND u (105
Styrene 0089 038 0022
1122-Tetrachloroethane 0010 0 07 u 0024
a-Xylene 0189 082 0018
135-Trlmethylbenzene 0062 031 0026
124-Trimethylbenzene 0150 074 0028
m-Dichlorobenzene 0006 004 u 0034
Chloromethylbenzene NO ND u 0039
p-Dichlorobenzene 0032 019 u 0348
o-Ochlorobenzene 0006 004 u 0037
124-Trlchlorobenzene 1110 NO u 0036
Hexachloro-13-bullldlene 0008 009 u 0037
Eastern Research Group Tlze bullesuJs m this repon apply on)middot to the sanrpfamp nnalyud ill acordance wh lht chain of custody Joumumt Thi~ OIIOI)middottical report musbull be teptoJduced In its elltiJtty
Page 8 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMilTED 0808111 to 0929111
ATTN Michael F Davts AQS SITE CODE
PHONE 913) 551-5042 FAX (913) 551middot5000 SITE CODE OECAwork
Description 4th and Santa Fe Lab ID 1090818-01 Sampled 090711 0000
Pressure 0 Receipt 6 5 Hg Canister EROOB Received 0908111247
Comments Analyzed 090911 0137
AirToxics by EPA Compendium Method T0-15 BciYlb MQI
Analyte lUlblpound usLm fOOl ~ Acetylene 0175 029 0016 Propylene 0333 057 op39 Dichlorodifluoromethane 0521 258 0011 Chloromethane 0507 LOS oou Okhlorotetrafluoroeihane NO NO u 0009
Vinyl chloride NO NO u OOilll 13-Butadlene NO NO u 0007
Bromomethane NO NO u 0009 Chloroethane NO NO u 0009 AletDnibile 0122 021 0024
Tr1dlloroftuoromethane 0252 142 0010 Acrylonlbile NO NO u 0012 11-0ldlloroethPne NO NO u 0009 Dldlloromethane 0159 055 0010
Carbon Disulfide 0063 020 0033 Trlchlorotrlfluoroethane 0094 072 OJ11
trans-12-Dichloroethylene NO NO u 0008
11-0lchloroethane NO NO u ouoa Methyl tert-BlJtyl Ether NO NO u o~
Ne~IEthyiKetone 0472 139 0157 Chloroprene NO NO u 0008
ds-12-Dichloroethylene NO NO u 0109
Bromochloromethane NO NO u oooa Chlorofomi NO NO u 0009 Ethyl ~Butyl Ether NO NO u 0008
12-Didlloroethane NO NO u 0009
111middot Trtdlloroethane NO NO u 0022
Benzene 0168 054 0029 Carbon Telrldllorlde 0095 oeo 0024
tertmiddotAmyl Methyl Ether NO NO u 0016
12-0Chlolgtpropane NO ND u 0023
ethyl Acrtlate NO NO u 0020
Bromodichloromethane NO NO u OOlS Trichloroethylene ND NO u 0025
MettwiMethacrylate NO NO u oc22 cis-13-0ichloropropene NO NO u 0022
~yiiiObutyiKetone 0035 014 0022
trans-13-0ichloropropene NO NO u oo2S 112middot Trichloroethane NO NO u 0025
Toluene 0373 141 0016
OibromQchloromethane NO NO u 0071
Eastern Research Group The nsults in this nport apply only to the saltlples D11alyzed in acordance with the chain Df cuampmiddottody docWMnt This analytical rttport must be repriJduced in its elllirety
Page 9 of 16
RG CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMIITED 080811 to 09291 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 4th and Santa Fe Lab ID 1090818-01 Sampled 090711 0000
Pressure Receipt 65 Hg canister ER008 Received 09081112~47
Comments Analyzed 090911 0137
Air Toxics by EPA Compendium Method T0-15 Results tmL
Analvte IUllm ll9lm flil Jmbll 12-0ibromoethane NO NO u 0018
n-Octane 0038 018 0015
Tetradiloroethylene ND NO u 0018 Chlomhenllne NO NO u 002
Ethyl benzene 0064 028 0017
mp-Xylene 0148 064 0034
Bromoform NO NO u 0025
Styrene NO NO u 0022
1122-TlliiChloroetllane NO NO u 0021
omiddotXylene 0070 031 0018
135middotTrimethylbenzene ND NO u 0026
124-Trimethylbenzene 0078 038 0028
m-Oiehlorobenzene NO NO u 0034
Chloromethylbenzene NO NO u 0019
p-Orchlorobenzene ND NO u 0348
o-Oidllorobenzene ND NO u 0037
124-Trichlorobenzene NO NO u 0036
Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The results rn Jhis teport apply cmJy 10 the samples (Uraly~ed in ac~ordant-e wilh the chain of CIISiody docunum This atwlytiral report 11111s1 be reprculuced i11 ils e11tirrty
Page 10 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN MIChael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001 030
REPORTED~ 1110111 0903
SUBMmED 0810811 to 092911
AQS SITE CODE
SITE CODE OECAwork
Description 150 west of Hwys 169 and 39 Lab ID 1091501-01 sampled 091411 oooo Pressure 0 ReClelpt 13 Hg canister 709 Received 091511 10~42
Comments Analyzed 0915111926
Air Taxies by EPA Compendium Method T0-15 BHIIIm MDI
Analyte JUlbll li9Lm fJJg JlRinl AcBtylene 0234 025 0-016 Propylene 0258 045 0-0~11
Dlchlorodlfluoromettmne 0544 270 oo11 Chloromethane 0526 109 0 012
DichlorolelrifAJoroethane NO NO u Otgt09 Vinyl chloride NO NO u 0008 13-Butildlene NO NO u 0007 Bromomettlane NO NO u 0009 Chloroethane NO NO u 0009
Acetonitrile 0130 022 0024
Trlchlorcrfluoromethane 0263 lAB 0010 Aaylonltrile NO NP u 0012 11-DIChloroethene NO NO u 0009
Dldloromelhane NO NO u (IOlD
carbon Disulfide 0032 010 u 0033 T~hlo~fluonHdhane 0107 082 0011 tr~ns-12-0ichloroethyler~ NO NO u 0008 11-Dichloroethane ljO NO u 0008 Methl tert-Butyl Ether NO NO u 0008 Methyl Ethyl Ketone 0382 113 0157
Chloroprene NO NO u 0008 ciamp-12-0ichloroethylene NO NO u 0009 Bromochloromethane NO NO u 0008 011oroform NO NO u 0009 Ethyl tert-Butyl Ether NO NO u 0008 JI-Dichloroethilne NO NO u 0009 111-Trichloroethane NO NO u (l022
Benzene ozos 067 0029
Carbon Tetrachloride 0101 064 0024 tert-Amyl Methyl Ether NO NO u 1)016 12-DJChiOropropane NO NO u 0023 Ethyl Acrylate NO NO u (1 020
Bromodichloromethane NO NO u 0025 Trichloroethylene NO NO u 0025
Methyl Methacrylilte NO NO u 0022 cis-13-Dichloropropene NO NO u 0022 Methyl Isobutyl llteDM NCI NO u 0022 trans-13-0ichloropropene NO NO u 0025 112-Trldlloroetflane NO NO u 0025 Toluene 0095 036 0016 Olbromodloromelhane NO NO u 0021
Eastern Research Group The results 111 Jhis r~port apply only to the samplts waalylui in accordance with tht chain of custody document This cuuzlytical report must in reprod~~eed in its entirety
Page 11 of 16
CERTIFICATE OF ANALYSISRG EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 111 011 0903
Kansas City KS 66101 SUBMirrED OBiOB11 to 092911
ATTN~ M1chael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE ~ OECAw(irk
Description 150 west of Hwys 169 and 39 Lab ID 1091501-01 Sampled 091411 00 00
Pressure Receipt 13 Hg canister 709 Received 0915111042
Comments Analyzed 0915111926
Air Toxlcs by EPA Compendium Method T0-15 ~ MW
Analvte wmx uqm fli1g RRint 12-Dibromoethane ND IID u 0()18
n-Oddne ND ND u 0015
Tetrachloroethylene ND ND u 0018
Ollorobenzene ND ND u 0021
Ethylbenzene 0035 015 Q017
mpmiddotXylene 0041 018 0034
Bromoform ND NO 11 0025
Styrene NO ND u 002
11-22-Tetradlloroelhane ND ND u 0024
o-Xylene ND NO u 0018
135-Trimethylbenzene NO NO u 0026
124middotTrlrnathylbenzene 0-042 021 0028
m-Dichlorohenzene ND ND u 0034
Chloromethylbenzene ND ND u 0039
p-OIChlorobenzene NO NO u 0348
o-Dichlorobenzere NO NO u 0037
12+Trlchlorobenzene NO ND u 0036
Hexachloro-13-butadlene ND ND u 0037
Eastern Research Group The result in thrs reoort applgt ltmly to the samplts mral1zed m accordanc11 ~ith thilhain of custodgt document This am1lytical report m11st be rbullpmJuced ill it~ entirety
Page 12 of 16
CERTIFrCATE OF ANALYSIS
EPA Region VII FILE tl 027800001030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMITTED 080811 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Description 73 north of Oak St on Plummer Lab ID 1092909-01 Sampled 0928110000
Pressure 0 Receipt 65 Hg canister 140 Received 0929111057
Comments Analyzed 093011 20 34
Analyte
Acetylene middotPropylene
Dldllorodifluoromethane Chlolomettlane
Dlchlorotetrafluoroethllne VInyl chloride 13-Butadlene Bromometl1dne
Chloroethane
Acetunitrile Trldllorotluoromethane
Acrylonitrile
11-0ithloroethene Dichloromethane Carbon DisulfJde
Trlchlorotrlfkloroetftane lranr1 2-0khloroethylene
11-Dithloroelhane
Methyl tert-Butyl Ether Methyl Ethyl Ketone Chloroprene ds-1HllchloiJethylene Bromochloromethane Chlorofvnn
Ethyl tert-Butyl Ether 12-Dichloroethane 111middotTriChloroethane
Benzene carbon Tetrachloride tert-Amyl Methyl Ether 12-Didlonopropane Ethyl Acrylate Bromodlchlorornelhane Trichloroethylene
Methyl MetllacrylaJ
ds-13-Dithloropropene Methyl Isobutyl KetDne trans-13-0khlorapropene 112-Trichloroethane
Toluene Olbromochloromethane
Air Toxics by EPA Compendium Method T0-15 Results mL
ORb YIiID Eiilg I1IZD 223 238 016 123 212 0039
0564 280 0~11
0525 109 0012 0018 013 ooot
NO NO u 0008 0181 040 0~07
NO NO u o009 NO NO u 0009
0157 028 0024 ozgo 163 0010
NO NO u 0(112 NO NO u 0009
0154 054 0010 0045 0 14 0033 0092 071 0011
NO NO u 0008 NO NO u 0008 NO NO u 0~08
0624 184 0157 NO NO u 0008 NO NO u 0009 NO NO u 0008
0035 017 0009 NO NO u 0008 NO NO u 0009
0012 007 u 0022 L49 477 0029
0088 o56 0024 NO NO u 0016 ND NO u 0023 NO NO u 0020 NO ND u 0025
0178 096 0025
NO NO u 0022 NO NO u 0022
0094 039 0022 NO NO u 0025 NO NO u 0025
276 10400 D 0040 r~O NO u 0021
Eastern Research Group The results m this repon apply only to the samples cmolylld in accordance wilh the chain of cUStOdy docWMnt This arwlytlcal rJort mu~middott be reproduced in its entirety
Page 13 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMITTED 0808111 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECA wa1lt
Description 75 north of Oak St on Plummer Lab ID 1092909-01 Sampled 092811 0000
Pressure Receipt 65 Hg canister 140 Received 0929111057
Comments Analyzed 0930112034
Air Toxics by EPA Compendium Method T0-15 Results lmb
Analyte mmx ugm3 flil on 12-Dibromoethane NO NO u 0018
n-Octane 0193 090 0015 Tetrachloroethylene 0019 013 0018
Chlorobenzene NO NO u 0021
Ethyl benzene 0356 155 p017 mp-Xylene 1oamp 461 OOl4
Bromoform NO NO u 6025
Sty~Wte 0060 026 0022 lll2-Tetrachloroethane NO NO u 0-024
o-Xylene P422 184 01118 135-TrlmethylbenEene 0094 046 0026 1124-Trlmethylbenzene 0340 167 0028
m-Dichlorobenzene 0043 016 0034 Chloromethylbenzene NO NO u 0039
p-Dichlorobenzene 0019 011 u 0035
rDichlorobenzellE NO NO u 0037 121-Trochlorobenzene NO NO u 0-036
Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The ll$Ults in rhis repon appl) NIhbull to the samples analyted in accordance with the cham of custody document Thta analybullical rrporl must he reproduced in in entirety
Page 14 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII FILE tl 027800001 030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS66101 SUBMmED 080811 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX~ (913) 551-5000 SITE CODE OECAwork
IAnalyte Result Units SOurce Result RPD
RPD Umit Note
Eastern Research Group ~ resulu in this reprJrt apply oraly to the samples analyed 111 accordance with the chain of crutody docunumt 1his anulmcal report must be reprodu~ed In its enrlnty
Page 15 of 16
CERTIFICATE OF ANALYSISRG EPA Region VII FILEmiddot 027800001 030
300 Minnesota Avenue REPORTED 1110 11 09middot03
Kansas City KS 66101 SUBMITTED 08101311 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX~ (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
u Under Detection Umlt
o Th1s result obtained by dilution
ND Analyte NOT DETECTED at or above the Method Detecbon Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group T1r results in thH report apply on() w the sample tmayzed il occordancltt with the cham of bullur1ody dotumnt This anayllcai report must be prwiuced in its entirety
Page 16 of 16
~RG Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
December 05 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 111511 1121
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the amtract for NMOC UATMP PAMS CSATAM and NATTS support (US EPA Contract No EPD-09-D48) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please oontact me at 919-468-7930
Sincerely
Laura Van Enwyck Project Manager lauravanenwyckergcom
The information contained in this report and its attachment(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauraJnenwyckergcom and delete the report without retairring any copies
Page 1 of6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 120511 1059
Kansas City KS 66101 SUBMITTED 111511
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Lincoln amp 39 Highway 1111501-01 Air 111411 0000 111511 1121 (111 W Lincoln)
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wfth the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001030
REPORTED 120511 1059
SUBMITTED 111511
AQS SITE CODE
SITE CODE OECAwork
DesaiptionUncoln amp 39 Highway (111 W Uncoln) Lab ID 1111501-01 Sampled 111411 0000
Pressure Receipt 8 Hg canister 636 Received 1115111121
Comments Analyzed 111611 0932
Air Toxics by EPA Compendium Method T0-15 blulb lmL
Analvte Jmbx Yllm fiG JlRbl Acetylene 0171 018 A-Ql 0016 Propylene 0272 OA7 A-Ql 0039 Dlchlorodlfluoromethane 0503 2A9 A-Ql 0011 Chloromethane OA74 098 A-Ql 0011 Dichlorobtraftuoroethane 0016 011 A-Ql 0009 Vinyl chloride ND ND A-Ql U 0008 13-Buladlene 0020 004 A-Ql 0007 Bromomethane 0011 004 AmiddotOl 0009 Chloroethane ND ND A-Ql U 0009 Acetonitrile 0138 023 A-Ql 0024 Trichloroftuoromethane D304 L71 A-Ql 0010 Acrylonitrile ND ND A-Q1 U 0012
11-Dichloroethene ND ND A-Q1 U 0009 Dichloromethane 0266 093 A-Ql 0010 Carbon Disulfide 0129 040 A-Ql 0033 Trichlorotrifluoroethane 0079 061 A-Ql 0011 trans-12-0ichloroethylene ND ND A-Ql U 0008 11-Dichloroethane ND ND A-Ql U 0008 Methyl tert-Butyl Ether ND NO A-Q1 U 0008 Methyl Ethyl Ketone 0760 us AmiddotOl 0157 Chloroprene ND NO A-Ql U 0008
cis-12-Dichloroethylene NO NO A-Ql U 0009 Bromochloromethane NO NO A-Ql U 0008 Chloroform NO NO A-Ql U 0009
Ethyl tert-Butyl Ether NO NO Amiddot01 U 0008 12-Dichloroethane 0026 011 A-Ql 0009 111-Trichloroethane 0006 003 A-Q1 U 0022 Benzene 113 362 A-Q1 0029 Carbon Tetrachloride 0069 OA4 A-Q1 0024 tert-Amyl Methyl Ether ND ND A-Ql U 0016 12-Dichloropropane ND NO A-Ql U 0023
Ethyl Acrylate NO NO A-Ql U 0020
Bromodlchloromethane ND NO A-o1 u 0025 Trichloroethylene NO ND A-01 U 0025
Methyl Methacrylate ND NO A-Q1 U 0022 cis-13-Dichloropropene NO NO A-Ql U 0022 Methyl Isobutyl Ketone 0047 019 A-Ql 0022 trans-13-Dichloropropene NO ND A-Q1 U 0025 112-Trichloroethane NO NO A-Q1 U 0025
Toluene 0661 250 A-01 0016 Dibromochloromethane NO ND A-Q1 U 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repoTt must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1210511 1059
Kansas City KS 66101 SUBMITTED 1115 11
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption Uncoln amp 39 Highway (111 W Lincoln) Lab ID 1111501-01 Sampled 111411 0000
Pressure Receipt 8 Hg canister 636 Received 1115111121
Comments Analyzed 111611 0932
Air Toxics by EPA Compendium Method T0-15 RuJID mL
AnaMe IU1bll ~ BiSl IU1bll 12-Dlbromoethane NO NO A-Ql U 0018
n-Oct3ne 0025 012 A-Ql 0015
Tetrachloroethylene 0016 011 A-Ql U 0018
Ollorobenzene NO NO A-Ql U 0021
Ethylbenzene 0068 030 A-Ql 0017
mp-Xylene 0144 063 A-Ql 0034
Bromoform NO NO A-Ql U 0025
Styrene 0058 025 A-Ql 0022
1122-Tetrachloroethane NO NO A-Ql U 0024
o-Xylene 0058 025 A-ol 0018
135-Trlmetflylbenzene 0050 025 A-01 0026
124-Trimetflylbenzene 0130 064 A-Ql 0028
m-Dichlorobenzene NO NO A-Ql U 0034
Chloromelhylbenzene NO NO A-ol U 0039
p-Oichlorobenzene 0027 016 A-Ql U 0035
o-Oichlorobenzene NO NO A-Ql U 0037
124-Trichlorobenzene NO NO A-ol U 0036
Hexachloro-13-butadiene NO NO A-ol U 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 120511 1059
Kansas City KS 66101 SUBMITTED 111511
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance witlz tlze chain of custody documellt This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1205111 1 059
Kansas City KS 66101 SUBMITTED 11151 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
A-ol Estimated value due to possible canister leak
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical re-port must be reproduced in its entirety
Page 6 of 6
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
December 15 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 1206111229
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for NMOC UATMP PAMS CSATAM and NATTS support (US EPA Contract No EPD-09-048) This rover page is an integral part of this report and any exceptions or oomments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Project Manager lauravanenwyckergcom
The information contained in this report and its attachment(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify laura vanenwyck ergcom and delete the report without retaining any copies
Page 1 of 6
RG CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111 1041
Kansas City KS 66101 SUBMITTED 1206 11
ATTN Michael F Davis AQS SITE CODE
PHONE 913) 551-5042 FAX 913) 551-5000 SITE CODE OECAwork
ANALYTlCAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Ash amp Forest SE Corner 1120611-01 Air 120411 0000 120611 1229
middotI I
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytirol repon must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
ALE 027800001030
REPORTED 1215111041
SUBMmED 1210611
AQS SITE CODE
SITE CODE OECAwork
Desaiptlon Ash amp Forest SE Comer Lab ID 1120611-01 sampled 120411 oooo Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 BuYltl MQL
AnaMe IUlllll lWm Bag IUlllll Acetylene OA36 OA7 0016 Propylene 0304 052 0039 Dichlorodiftuoromethane 0567 281 0011 Chloromethane 0566 117 0012 Dlchlorotetnlftuoroethane 0019 013 0009 Vinyl chloride NO NO u 0008 13-Butadiene NO NO u 0007 Bromomethane 0012 005 0009 Chloroethane NO NO u 0009 Acetonitrile 0111 019 0024 Trichlorofluoromethane 0284 160 0010 Aaylonitrile ND NO u 0012 11-Dichloroethene ND ND u 0009 Dichloromethane 0083 029 0010 Carbon Disulfide 0019 006 u 0033
Trlchlorotrlftuoroethane 0099 076 0011 trans-12-Dichloroethylene ND ND u 0008 11-Dichloroethane ND NO u 0008 Methyl tert-Butyl Ether NO NO u 0008 Methyl Ethyl Ketone 0536 158 0157 Chloroprene NO NO u 0008 cis-12-Dichloroethylene NO ND u 0009 Bromochloromethane NO NO u 0008 Chloroform 0022 011 0009 Ethyl tert-Butyl Ether NO NO u 0008 12-Dichloroethane 0025 010 0009 111-Trichloroethane 0011 006 u 0022 Benzene 0188 060 0029 carbon Tetrachloride 0106 067 0024 tert-Amyl Methyl Ether NO NO u 0016 12-Dichloropropane NO NO u 0023 Ethyl Acrylate ND NO u 0020
Bromodichloromethane NO NO u 0025 Trichloroethylene NO NO u 0025 Methyl Methacrylate NO NO u 0022 cis-13-Dichloropropene NO NO u 0022
Methyl Isobutyl Ketone 0042 017 0022 trans-13-Dichloropropene ND NO u 0025 112-Trichloroethane NO NO u 0025
Toluene 0149 056 0016 Oibromochloromethane 0003 003 u 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproducedin its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 121511 1041
Kansas City KS 66101 SUBMmED 1210611
ATTN Michael F Davis AQS SITE CODE
PHONE (913 551-5042 FAX (913 551-5000 SITE CODE OECAwork
Description Ash amp Forest SE Comer Lab ID 1120611-01 Sampled 120411 0000
Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 llWdtl MID
Analyte ubll IUllm Bag ubll 12-0ibromoethane NO NO u 0018 nmiddotOctane 0044 021 0015 Tetrachloroethylene 0006 004 u 0018
Chlorobenzene NO NO u 0021 Ethylbenzene 0047 021 0017 mp-Xylene 0070 031 0034 Bromoform NO NO u 0025 Styrene 0034 015 0022 1122-Tetrachloroethane NO NO u 0024 o-Xylene 0036 016 0018 135-Trlmethylbenzene 0025 012 u 0026 124-Trlmetllylbenzene 0047 023 0028 m-Oichlorobenzene NO NO u 0034
Chloromethylbenzene NO NO u 0039 p-Dichlorcbenzene 0005 003 u 0348 a-Dichlorobenzene NO NO u 0037
124-Trlchlorobenzene NO NO u 0036 Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repon must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS~RG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 66101 SUBMITTED 12061 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPDIAnalyte Result Units Result RPD um1t Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 661 01 SUBMITTED 120611
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its enJirety
Page 6 of 6
i
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
March 12 2012
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 030512 0916
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for UATMP NATTS CSATAM PAMS and NMOC support (US EPA Contract No 68-D-Q9-048) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Program Manager lauravanenwyckergcom
The information contained in this report and its attachmcnt(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauravanenwyckergcom and delete the report dthout retaining any copies
Page 1 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 0312112 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
6th St between Central amp 2030501-01 Air 030212 0000 030512 0916 Malcom
Eastern Research Group The results in this report apply only to the samples anal zed in accordance With the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Aven ue REPORTED 031212 1 051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 ~ tml
Analvte RRbll Y9lD1 flu RRbll Acetylene 0627 067 0072 Propylene 0484 084 0033
Dichlorodllluoromethane 0500 248 0023 Chloromethane 0557 115 0033
Dichlorotetrafluoroethane 0015 011 0012 Vinyl chloride NO NO u 0011
13-Butadlene 0036 oo8 0011
Bromomethane 0012 005 0012 Chloroethane NO NO u 0017
Acetonitrile 0073 012 0073
Trichlorofluoromethane 0258 145 0015 Acrylonitrile NO NO u 0020
11-0ichloroethene NO NO u 0014
Dichloromethane 0185 064 0023
Carbon Disulfide 0037 012 0014 Trichlorobitluoroethane 0119 091 0017
trans-12-0ichloroethylene NO NO u 0012
11-0ichloroethane NO NO u 0015
Methyl tert-Butyl Ether NO NO u 0011
Chloroprene NO NO u 0012
ds-12-0ich loroethylene NO NO u OD18
Bromochloromethane NO NO u 0014
Chloroform NO ND u 0014
Ethyl tert-Butyl Ether NO NO u 0011
12-Dichloroethane 0019 008 0016
111-Trichloroethane 0012 007 u 0020
Benzene 0344 L10 0061 Carbon Tetrachloride 0088 056 0024
tert-Amyl Methyl Ether NO NO u 0016
12-0ichloropropane ND NO u 0019
Ethyl Acrylate ND NO u 0014
Bromodichloromethane ND NO u 0021
Trichloroethylene NO ND u 0022
Methyl Methacrylate ND NO u 0025
ds-13-0ichloropropene NO NO u 0015
Methyl Isobutyl Ketone 0015 oo6 0015
trans-13-0ichloropropene NO ND u 0016
112-Trichloroethane NO NO u 0021
Toluene 0416 157 0045
Oibromochloromethane ND NO u 0018
12-0ibromoethane ND NO u 0017
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551 -5000
FILE 027800001030
REPORTED 0312 12 1051
SUBMITTED 030512
AQS SITE CODE
SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 Bwdtl MJlL
Analvte Jmbll Y9Lm Big Jmbx nmiddotOclane 0039 018 0020 Tetrachloroethylene 0005 003 u 0020
Chlorobenzene ND ND u 0025
Ethylbenzene 0045 020 0023 mp-Xylene 0112 OA9 0037 Bromoform ND ND u 0020
Styrene 0030 013 0024 1122-Tetrachloroethane ND ND u 0018
o-Xylene 0050 022 0020
135-Trimethylbenzene 0019 009 u 0022
124-Trimethylbenzene 0047 023 0025 m-Dichlorobenzene ND ND u 0024
p-Dichlorobenzene 0004 002 u 0019
a-Dichlorobenzene NO ND u 0021
124-Trichlorobenzene ND ND u 0022
Hexachloro-13-butadiene ND ND u 0022
Eastern Research Group The results in this report apply only 1o the samples analyzed in accordance with the chain of custody document This analytical rep ort must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 031212 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wilh the chain of custody document This analytical report must be reproduced in its enrirety
Page 5 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 03121121051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report nutst be reproduced in its entirety
Page 6 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMilTED 0808111 to 0929111
ATTN Michael F Davts AQS SITE CODE
PHONE 913) 551-5042 FAX (913) 551middot5000 SITE CODE OECAwork
Description 4th and Santa Fe Lab ID 1090818-01 Sampled 090711 0000
Pressure 0 Receipt 6 5 Hg Canister EROOB Received 0908111247
Comments Analyzed 090911 0137
AirToxics by EPA Compendium Method T0-15 BciYlb MQI
Analyte lUlblpound usLm fOOl ~ Acetylene 0175 029 0016 Propylene 0333 057 op39 Dichlorodifluoromethane 0521 258 0011 Chloromethane 0507 LOS oou Okhlorotetrafluoroeihane NO NO u 0009
Vinyl chloride NO NO u OOilll 13-Butadlene NO NO u 0007
Bromomethane NO NO u 0009 Chloroethane NO NO u 0009 AletDnibile 0122 021 0024
Tr1dlloroftuoromethane 0252 142 0010 Acrylonlbile NO NO u 0012 11-0ldlloroethPne NO NO u 0009 Dldlloromethane 0159 055 0010
Carbon Disulfide 0063 020 0033 Trlchlorotrlfluoroethane 0094 072 OJ11
trans-12-Dichloroethylene NO NO u 0008
11-0lchloroethane NO NO u ouoa Methyl tert-BlJtyl Ether NO NO u o~
Ne~IEthyiKetone 0472 139 0157 Chloroprene NO NO u 0008
ds-12-Dichloroethylene NO NO u 0109
Bromochloromethane NO NO u oooa Chlorofomi NO NO u 0009 Ethyl ~Butyl Ether NO NO u 0008
12-Didlloroethane NO NO u 0009
111middot Trtdlloroethane NO NO u 0022
Benzene 0168 054 0029 Carbon Telrldllorlde 0095 oeo 0024
tertmiddotAmyl Methyl Ether NO NO u 0016
12-0Chlolgtpropane NO ND u 0023
ethyl Acrtlate NO NO u 0020
Bromodichloromethane NO NO u OOlS Trichloroethylene ND NO u 0025
MettwiMethacrylate NO NO u oc22 cis-13-0ichloropropene NO NO u 0022
~yiiiObutyiKetone 0035 014 0022
trans-13-0ichloropropene NO NO u oo2S 112middot Trichloroethane NO NO u 0025
Toluene 0373 141 0016
OibromQchloromethane NO NO u 0071
Eastern Research Group The nsults in this nport apply only to the saltlples D11alyzed in acordance with the chain Df cuampmiddottody docWMnt This analytical rttport must be repriJduced in its elllirety
Page 9 of 16
RG CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMIITED 080811 to 09291 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 4th and Santa Fe Lab ID 1090818-01 Sampled 090711 0000
Pressure Receipt 65 Hg canister ER008 Received 09081112~47
Comments Analyzed 090911 0137
Air Toxics by EPA Compendium Method T0-15 Results tmL
Analvte IUllm ll9lm flil Jmbll 12-0ibromoethane NO NO u 0018
n-Octane 0038 018 0015
Tetradiloroethylene ND NO u 0018 Chlomhenllne NO NO u 002
Ethyl benzene 0064 028 0017
mp-Xylene 0148 064 0034
Bromoform NO NO u 0025
Styrene NO NO u 0022
1122-TlliiChloroetllane NO NO u 0021
omiddotXylene 0070 031 0018
135middotTrimethylbenzene ND NO u 0026
124-Trimethylbenzene 0078 038 0028
m-Oiehlorobenzene NO NO u 0034
Chloromethylbenzene NO NO u 0019
p-Orchlorobenzene ND NO u 0348
o-Oidllorobenzene ND NO u 0037
124-Trichlorobenzene NO NO u 0036
Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The results rn Jhis teport apply cmJy 10 the samples (Uraly~ed in ac~ordant-e wilh the chain of CIISiody docunum This atwlytiral report 11111s1 be reprculuced i11 ils e11tirrty
Page 10 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN MIChael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001 030
REPORTED~ 1110111 0903
SUBMmED 0810811 to 092911
AQS SITE CODE
SITE CODE OECAwork
Description 150 west of Hwys 169 and 39 Lab ID 1091501-01 sampled 091411 oooo Pressure 0 ReClelpt 13 Hg canister 709 Received 091511 10~42
Comments Analyzed 0915111926
Air Taxies by EPA Compendium Method T0-15 BHIIIm MDI
Analyte JUlbll li9Lm fJJg JlRinl AcBtylene 0234 025 0-016 Propylene 0258 045 0-0~11
Dlchlorodlfluoromettmne 0544 270 oo11 Chloromethane 0526 109 0 012
DichlorolelrifAJoroethane NO NO u Otgt09 Vinyl chloride NO NO u 0008 13-Butildlene NO NO u 0007 Bromomettlane NO NO u 0009 Chloroethane NO NO u 0009
Acetonitrile 0130 022 0024
Trlchlorcrfluoromethane 0263 lAB 0010 Aaylonltrile NO NP u 0012 11-DIChloroethene NO NO u 0009
Dldloromelhane NO NO u (IOlD
carbon Disulfide 0032 010 u 0033 T~hlo~fluonHdhane 0107 082 0011 tr~ns-12-0ichloroethyler~ NO NO u 0008 11-Dichloroethane ljO NO u 0008 Methl tert-Butyl Ether NO NO u 0008 Methyl Ethyl Ketone 0382 113 0157
Chloroprene NO NO u 0008 ciamp-12-0ichloroethylene NO NO u 0009 Bromochloromethane NO NO u 0008 011oroform NO NO u 0009 Ethyl tert-Butyl Ether NO NO u 0008 JI-Dichloroethilne NO NO u 0009 111-Trichloroethane NO NO u (l022
Benzene ozos 067 0029
Carbon Tetrachloride 0101 064 0024 tert-Amyl Methyl Ether NO NO u 1)016 12-DJChiOropropane NO NO u 0023 Ethyl Acrylate NO NO u (1 020
Bromodichloromethane NO NO u 0025 Trichloroethylene NO NO u 0025
Methyl Methacrylilte NO NO u 0022 cis-13-Dichloropropene NO NO u 0022 Methyl Isobutyl llteDM NCI NO u 0022 trans-13-0ichloropropene NO NO u 0025 112-Trldlloroetflane NO NO u 0025 Toluene 0095 036 0016 Olbromodloromelhane NO NO u 0021
Eastern Research Group The results 111 Jhis r~port apply only to the samplts waalylui in accordance with tht chain of custody document This cuuzlytical report must in reprod~~eed in its entirety
Page 11 of 16
CERTIFICATE OF ANALYSISRG EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 111 011 0903
Kansas City KS 66101 SUBMirrED OBiOB11 to 092911
ATTN~ M1chael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE ~ OECAw(irk
Description 150 west of Hwys 169 and 39 Lab ID 1091501-01 Sampled 091411 00 00
Pressure Receipt 13 Hg canister 709 Received 0915111042
Comments Analyzed 0915111926
Air Toxlcs by EPA Compendium Method T0-15 ~ MW
Analvte wmx uqm fli1g RRint 12-Dibromoethane ND IID u 0()18
n-Oddne ND ND u 0015
Tetrachloroethylene ND ND u 0018
Ollorobenzene ND ND u 0021
Ethylbenzene 0035 015 Q017
mpmiddotXylene 0041 018 0034
Bromoform ND NO 11 0025
Styrene NO ND u 002
11-22-Tetradlloroelhane ND ND u 0024
o-Xylene ND NO u 0018
135-Trimethylbenzene NO NO u 0026
124middotTrlrnathylbenzene 0-042 021 0028
m-Dichlorohenzene ND ND u 0034
Chloromethylbenzene ND ND u 0039
p-OIChlorobenzene NO NO u 0348
o-Dichlorobenzere NO NO u 0037
12+Trlchlorobenzene NO ND u 0036
Hexachloro-13-butadlene ND ND u 0037
Eastern Research Group The result in thrs reoort applgt ltmly to the samplts mral1zed m accordanc11 ~ith thilhain of custodgt document This am1lytical report m11st be rbullpmJuced ill it~ entirety
Page 12 of 16
CERTIFrCATE OF ANALYSIS
EPA Region VII FILE tl 027800001030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMITTED 080811 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Description 73 north of Oak St on Plummer Lab ID 1092909-01 Sampled 0928110000
Pressure 0 Receipt 65 Hg canister 140 Received 0929111057
Comments Analyzed 093011 20 34
Analyte
Acetylene middotPropylene
Dldllorodifluoromethane Chlolomettlane
Dlchlorotetrafluoroethllne VInyl chloride 13-Butadlene Bromometl1dne
Chloroethane
Acetunitrile Trldllorotluoromethane
Acrylonitrile
11-0ithloroethene Dichloromethane Carbon DisulfJde
Trlchlorotrlfkloroetftane lranr1 2-0khloroethylene
11-Dithloroelhane
Methyl tert-Butyl Ether Methyl Ethyl Ketone Chloroprene ds-1HllchloiJethylene Bromochloromethane Chlorofvnn
Ethyl tert-Butyl Ether 12-Dichloroethane 111middotTriChloroethane
Benzene carbon Tetrachloride tert-Amyl Methyl Ether 12-Didlonopropane Ethyl Acrylate Bromodlchlorornelhane Trichloroethylene
Methyl MetllacrylaJ
ds-13-Dithloropropene Methyl Isobutyl KetDne trans-13-0khlorapropene 112-Trichloroethane
Toluene Olbromochloromethane
Air Toxics by EPA Compendium Method T0-15 Results mL
ORb YIiID Eiilg I1IZD 223 238 016 123 212 0039
0564 280 0~11
0525 109 0012 0018 013 ooot
NO NO u 0008 0181 040 0~07
NO NO u o009 NO NO u 0009
0157 028 0024 ozgo 163 0010
NO NO u 0(112 NO NO u 0009
0154 054 0010 0045 0 14 0033 0092 071 0011
NO NO u 0008 NO NO u 0008 NO NO u 0~08
0624 184 0157 NO NO u 0008 NO NO u 0009 NO NO u 0008
0035 017 0009 NO NO u 0008 NO NO u 0009
0012 007 u 0022 L49 477 0029
0088 o56 0024 NO NO u 0016 ND NO u 0023 NO NO u 0020 NO ND u 0025
0178 096 0025
NO NO u 0022 NO NO u 0022
0094 039 0022 NO NO u 0025 NO NO u 0025
276 10400 D 0040 r~O NO u 0021
Eastern Research Group The results m this repon apply only to the samples cmolylld in accordance wilh the chain of cUStOdy docWMnt This arwlytlcal rJort mu~middott be reproduced in its entirety
Page 13 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMITTED 0808111 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECA wa1lt
Description 75 north of Oak St on Plummer Lab ID 1092909-01 Sampled 092811 0000
Pressure Receipt 65 Hg canister 140 Received 0929111057
Comments Analyzed 0930112034
Air Toxics by EPA Compendium Method T0-15 Results lmb
Analyte mmx ugm3 flil on 12-Dibromoethane NO NO u 0018
n-Octane 0193 090 0015 Tetrachloroethylene 0019 013 0018
Chlorobenzene NO NO u 0021
Ethyl benzene 0356 155 p017 mp-Xylene 1oamp 461 OOl4
Bromoform NO NO u 6025
Sty~Wte 0060 026 0022 lll2-Tetrachloroethane NO NO u 0-024
o-Xylene P422 184 01118 135-TrlmethylbenEene 0094 046 0026 1124-Trlmethylbenzene 0340 167 0028
m-Dichlorobenzene 0043 016 0034 Chloromethylbenzene NO NO u 0039
p-Dichlorobenzene 0019 011 u 0035
rDichlorobenzellE NO NO u 0037 121-Trochlorobenzene NO NO u 0-036
Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The ll$Ults in rhis repon appl) NIhbull to the samples analyted in accordance with the cham of custody document Thta analybullical rrporl must he reproduced in in entirety
Page 14 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII FILE tl 027800001 030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS66101 SUBMmED 080811 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX~ (913) 551-5000 SITE CODE OECAwork
IAnalyte Result Units SOurce Result RPD
RPD Umit Note
Eastern Research Group ~ resulu in this reprJrt apply oraly to the samples analyed 111 accordance with the chain of crutody docunumt 1his anulmcal report must be reprodu~ed In its enrlnty
Page 15 of 16
CERTIFICATE OF ANALYSISRG EPA Region VII FILEmiddot 027800001 030
300 Minnesota Avenue REPORTED 1110 11 09middot03
Kansas City KS 66101 SUBMITTED 08101311 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX~ (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
u Under Detection Umlt
o Th1s result obtained by dilution
ND Analyte NOT DETECTED at or above the Method Detecbon Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group T1r results in thH report apply on() w the sample tmayzed il occordancltt with the cham of bullur1ody dotumnt This anayllcai report must be prwiuced in its entirety
Page 16 of 16
~RG Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
December 05 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 111511 1121
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the amtract for NMOC UATMP PAMS CSATAM and NATTS support (US EPA Contract No EPD-09-D48) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please oontact me at 919-468-7930
Sincerely
Laura Van Enwyck Project Manager lauravanenwyckergcom
The information contained in this report and its attachment(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauraJnenwyckergcom and delete the report without retairring any copies
Page 1 of6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 120511 1059
Kansas City KS 66101 SUBMITTED 111511
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Lincoln amp 39 Highway 1111501-01 Air 111411 0000 111511 1121 (111 W Lincoln)
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wfth the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001030
REPORTED 120511 1059
SUBMITTED 111511
AQS SITE CODE
SITE CODE OECAwork
DesaiptionUncoln amp 39 Highway (111 W Uncoln) Lab ID 1111501-01 Sampled 111411 0000
Pressure Receipt 8 Hg canister 636 Received 1115111121
Comments Analyzed 111611 0932
Air Toxics by EPA Compendium Method T0-15 blulb lmL
Analvte Jmbx Yllm fiG JlRbl Acetylene 0171 018 A-Ql 0016 Propylene 0272 OA7 A-Ql 0039 Dlchlorodlfluoromethane 0503 2A9 A-Ql 0011 Chloromethane OA74 098 A-Ql 0011 Dichlorobtraftuoroethane 0016 011 A-Ql 0009 Vinyl chloride ND ND A-Ql U 0008 13-Buladlene 0020 004 A-Ql 0007 Bromomethane 0011 004 AmiddotOl 0009 Chloroethane ND ND A-Ql U 0009 Acetonitrile 0138 023 A-Ql 0024 Trichloroftuoromethane D304 L71 A-Ql 0010 Acrylonitrile ND ND A-Q1 U 0012
11-Dichloroethene ND ND A-Q1 U 0009 Dichloromethane 0266 093 A-Ql 0010 Carbon Disulfide 0129 040 A-Ql 0033 Trichlorotrifluoroethane 0079 061 A-Ql 0011 trans-12-0ichloroethylene ND ND A-Ql U 0008 11-Dichloroethane ND ND A-Ql U 0008 Methyl tert-Butyl Ether ND NO A-Q1 U 0008 Methyl Ethyl Ketone 0760 us AmiddotOl 0157 Chloroprene ND NO A-Ql U 0008
cis-12-Dichloroethylene NO NO A-Ql U 0009 Bromochloromethane NO NO A-Ql U 0008 Chloroform NO NO A-Ql U 0009
Ethyl tert-Butyl Ether NO NO Amiddot01 U 0008 12-Dichloroethane 0026 011 A-Ql 0009 111-Trichloroethane 0006 003 A-Q1 U 0022 Benzene 113 362 A-Q1 0029 Carbon Tetrachloride 0069 OA4 A-Q1 0024 tert-Amyl Methyl Ether ND ND A-Ql U 0016 12-Dichloropropane ND NO A-Ql U 0023
Ethyl Acrylate NO NO A-Ql U 0020
Bromodlchloromethane ND NO A-o1 u 0025 Trichloroethylene NO ND A-01 U 0025
Methyl Methacrylate ND NO A-Q1 U 0022 cis-13-Dichloropropene NO NO A-Ql U 0022 Methyl Isobutyl Ketone 0047 019 A-Ql 0022 trans-13-Dichloropropene NO ND A-Q1 U 0025 112-Trichloroethane NO NO A-Q1 U 0025
Toluene 0661 250 A-01 0016 Dibromochloromethane NO ND A-Q1 U 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repoTt must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1210511 1059
Kansas City KS 66101 SUBMITTED 1115 11
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption Uncoln amp 39 Highway (111 W Lincoln) Lab ID 1111501-01 Sampled 111411 0000
Pressure Receipt 8 Hg canister 636 Received 1115111121
Comments Analyzed 111611 0932
Air Toxics by EPA Compendium Method T0-15 RuJID mL
AnaMe IU1bll ~ BiSl IU1bll 12-Dlbromoethane NO NO A-Ql U 0018
n-Oct3ne 0025 012 A-Ql 0015
Tetrachloroethylene 0016 011 A-Ql U 0018
Ollorobenzene NO NO A-Ql U 0021
Ethylbenzene 0068 030 A-Ql 0017
mp-Xylene 0144 063 A-Ql 0034
Bromoform NO NO A-Ql U 0025
Styrene 0058 025 A-Ql 0022
1122-Tetrachloroethane NO NO A-Ql U 0024
o-Xylene 0058 025 A-ol 0018
135-Trlmetflylbenzene 0050 025 A-01 0026
124-Trimetflylbenzene 0130 064 A-Ql 0028
m-Dichlorobenzene NO NO A-Ql U 0034
Chloromelhylbenzene NO NO A-ol U 0039
p-Oichlorobenzene 0027 016 A-Ql U 0035
o-Oichlorobenzene NO NO A-Ql U 0037
124-Trichlorobenzene NO NO A-ol U 0036
Hexachloro-13-butadiene NO NO A-ol U 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 120511 1059
Kansas City KS 66101 SUBMITTED 111511
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance witlz tlze chain of custody documellt This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1205111 1 059
Kansas City KS 66101 SUBMITTED 11151 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
A-ol Estimated value due to possible canister leak
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical re-port must be reproduced in its entirety
Page 6 of 6
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
December 15 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 1206111229
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for NMOC UATMP PAMS CSATAM and NATTS support (US EPA Contract No EPD-09-048) This rover page is an integral part of this report and any exceptions or oomments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Project Manager lauravanenwyckergcom
The information contained in this report and its attachment(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify laura vanenwyck ergcom and delete the report without retaining any copies
Page 1 of 6
RG CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111 1041
Kansas City KS 66101 SUBMITTED 1206 11
ATTN Michael F Davis AQS SITE CODE
PHONE 913) 551-5042 FAX 913) 551-5000 SITE CODE OECAwork
ANALYTlCAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Ash amp Forest SE Corner 1120611-01 Air 120411 0000 120611 1229
middotI I
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytirol repon must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
ALE 027800001030
REPORTED 1215111041
SUBMmED 1210611
AQS SITE CODE
SITE CODE OECAwork
Desaiptlon Ash amp Forest SE Comer Lab ID 1120611-01 sampled 120411 oooo Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 BuYltl MQL
AnaMe IUlllll lWm Bag IUlllll Acetylene OA36 OA7 0016 Propylene 0304 052 0039 Dichlorodiftuoromethane 0567 281 0011 Chloromethane 0566 117 0012 Dlchlorotetnlftuoroethane 0019 013 0009 Vinyl chloride NO NO u 0008 13-Butadiene NO NO u 0007 Bromomethane 0012 005 0009 Chloroethane NO NO u 0009 Acetonitrile 0111 019 0024 Trichlorofluoromethane 0284 160 0010 Aaylonitrile ND NO u 0012 11-Dichloroethene ND ND u 0009 Dichloromethane 0083 029 0010 Carbon Disulfide 0019 006 u 0033
Trlchlorotrlftuoroethane 0099 076 0011 trans-12-Dichloroethylene ND ND u 0008 11-Dichloroethane ND NO u 0008 Methyl tert-Butyl Ether NO NO u 0008 Methyl Ethyl Ketone 0536 158 0157 Chloroprene NO NO u 0008 cis-12-Dichloroethylene NO ND u 0009 Bromochloromethane NO NO u 0008 Chloroform 0022 011 0009 Ethyl tert-Butyl Ether NO NO u 0008 12-Dichloroethane 0025 010 0009 111-Trichloroethane 0011 006 u 0022 Benzene 0188 060 0029 carbon Tetrachloride 0106 067 0024 tert-Amyl Methyl Ether NO NO u 0016 12-Dichloropropane NO NO u 0023 Ethyl Acrylate ND NO u 0020
Bromodichloromethane NO NO u 0025 Trichloroethylene NO NO u 0025 Methyl Methacrylate NO NO u 0022 cis-13-Dichloropropene NO NO u 0022
Methyl Isobutyl Ketone 0042 017 0022 trans-13-Dichloropropene ND NO u 0025 112-Trichloroethane NO NO u 0025
Toluene 0149 056 0016 Oibromochloromethane 0003 003 u 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproducedin its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 121511 1041
Kansas City KS 66101 SUBMmED 1210611
ATTN Michael F Davis AQS SITE CODE
PHONE (913 551-5042 FAX (913 551-5000 SITE CODE OECAwork
Description Ash amp Forest SE Comer Lab ID 1120611-01 Sampled 120411 0000
Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 llWdtl MID
Analyte ubll IUllm Bag ubll 12-0ibromoethane NO NO u 0018 nmiddotOctane 0044 021 0015 Tetrachloroethylene 0006 004 u 0018
Chlorobenzene NO NO u 0021 Ethylbenzene 0047 021 0017 mp-Xylene 0070 031 0034 Bromoform NO NO u 0025 Styrene 0034 015 0022 1122-Tetrachloroethane NO NO u 0024 o-Xylene 0036 016 0018 135-Trlmethylbenzene 0025 012 u 0026 124-Trlmetllylbenzene 0047 023 0028 m-Oichlorobenzene NO NO u 0034
Chloromethylbenzene NO NO u 0039 p-Dichlorcbenzene 0005 003 u 0348 a-Dichlorobenzene NO NO u 0037
124-Trlchlorobenzene NO NO u 0036 Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repon must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS~RG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 66101 SUBMITTED 12061 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPDIAnalyte Result Units Result RPD um1t Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 661 01 SUBMITTED 120611
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its enJirety
Page 6 of 6
i
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
March 12 2012
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 030512 0916
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for UATMP NATTS CSATAM PAMS and NMOC support (US EPA Contract No 68-D-Q9-048) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Program Manager lauravanenwyckergcom
The information contained in this report and its attachmcnt(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauravanenwyckergcom and delete the report dthout retaining any copies
Page 1 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 0312112 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
6th St between Central amp 2030501-01 Air 030212 0000 030512 0916 Malcom
Eastern Research Group The results in this report apply only to the samples anal zed in accordance With the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Aven ue REPORTED 031212 1 051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 ~ tml
Analvte RRbll Y9lD1 flu RRbll Acetylene 0627 067 0072 Propylene 0484 084 0033
Dichlorodllluoromethane 0500 248 0023 Chloromethane 0557 115 0033
Dichlorotetrafluoroethane 0015 011 0012 Vinyl chloride NO NO u 0011
13-Butadlene 0036 oo8 0011
Bromomethane 0012 005 0012 Chloroethane NO NO u 0017
Acetonitrile 0073 012 0073
Trichlorofluoromethane 0258 145 0015 Acrylonitrile NO NO u 0020
11-0ichloroethene NO NO u 0014
Dichloromethane 0185 064 0023
Carbon Disulfide 0037 012 0014 Trichlorobitluoroethane 0119 091 0017
trans-12-0ichloroethylene NO NO u 0012
11-0ichloroethane NO NO u 0015
Methyl tert-Butyl Ether NO NO u 0011
Chloroprene NO NO u 0012
ds-12-0ich loroethylene NO NO u OD18
Bromochloromethane NO NO u 0014
Chloroform NO ND u 0014
Ethyl tert-Butyl Ether NO NO u 0011
12-Dichloroethane 0019 008 0016
111-Trichloroethane 0012 007 u 0020
Benzene 0344 L10 0061 Carbon Tetrachloride 0088 056 0024
tert-Amyl Methyl Ether NO NO u 0016
12-0ichloropropane ND NO u 0019
Ethyl Acrylate ND NO u 0014
Bromodichloromethane ND NO u 0021
Trichloroethylene NO ND u 0022
Methyl Methacrylate ND NO u 0025
ds-13-0ichloropropene NO NO u 0015
Methyl Isobutyl Ketone 0015 oo6 0015
trans-13-0ichloropropene NO ND u 0016
112-Trichloroethane NO NO u 0021
Toluene 0416 157 0045
Oibromochloromethane ND NO u 0018
12-0ibromoethane ND NO u 0017
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551 -5000
FILE 027800001030
REPORTED 0312 12 1051
SUBMITTED 030512
AQS SITE CODE
SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 Bwdtl MJlL
Analvte Jmbll Y9Lm Big Jmbx nmiddotOclane 0039 018 0020 Tetrachloroethylene 0005 003 u 0020
Chlorobenzene ND ND u 0025
Ethylbenzene 0045 020 0023 mp-Xylene 0112 OA9 0037 Bromoform ND ND u 0020
Styrene 0030 013 0024 1122-Tetrachloroethane ND ND u 0018
o-Xylene 0050 022 0020
135-Trimethylbenzene 0019 009 u 0022
124-Trimethylbenzene 0047 023 0025 m-Dichlorobenzene ND ND u 0024
p-Dichlorobenzene 0004 002 u 0019
a-Dichlorobenzene NO ND u 0021
124-Trichlorobenzene ND ND u 0022
Hexachloro-13-butadiene ND ND u 0022
Eastern Research Group The results in this report apply only 1o the samples analyzed in accordance with the chain of custody document This analytical rep ort must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 031212 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wilh the chain of custody document This analytical report must be reproduced in its enrirety
Page 5 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 03121121051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report nutst be reproduced in its entirety
Page 6 of 6
RG CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMIITED 080811 to 09291 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 4th and Santa Fe Lab ID 1090818-01 Sampled 090711 0000
Pressure Receipt 65 Hg canister ER008 Received 09081112~47
Comments Analyzed 090911 0137
Air Toxics by EPA Compendium Method T0-15 Results tmL
Analvte IUllm ll9lm flil Jmbll 12-0ibromoethane NO NO u 0018
n-Octane 0038 018 0015
Tetradiloroethylene ND NO u 0018 Chlomhenllne NO NO u 002
Ethyl benzene 0064 028 0017
mp-Xylene 0148 064 0034
Bromoform NO NO u 0025
Styrene NO NO u 0022
1122-TlliiChloroetllane NO NO u 0021
omiddotXylene 0070 031 0018
135middotTrimethylbenzene ND NO u 0026
124-Trimethylbenzene 0078 038 0028
m-Oiehlorobenzene NO NO u 0034
Chloromethylbenzene NO NO u 0019
p-Orchlorobenzene ND NO u 0348
o-Oidllorobenzene ND NO u 0037
124-Trichlorobenzene NO NO u 0036
Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The results rn Jhis teport apply cmJy 10 the samples (Uraly~ed in ac~ordant-e wilh the chain of CIISiody docunum This atwlytiral report 11111s1 be reprculuced i11 ils e11tirrty
Page 10 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN MIChael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001 030
REPORTED~ 1110111 0903
SUBMmED 0810811 to 092911
AQS SITE CODE
SITE CODE OECAwork
Description 150 west of Hwys 169 and 39 Lab ID 1091501-01 sampled 091411 oooo Pressure 0 ReClelpt 13 Hg canister 709 Received 091511 10~42
Comments Analyzed 0915111926
Air Taxies by EPA Compendium Method T0-15 BHIIIm MDI
Analyte JUlbll li9Lm fJJg JlRinl AcBtylene 0234 025 0-016 Propylene 0258 045 0-0~11
Dlchlorodlfluoromettmne 0544 270 oo11 Chloromethane 0526 109 0 012
DichlorolelrifAJoroethane NO NO u Otgt09 Vinyl chloride NO NO u 0008 13-Butildlene NO NO u 0007 Bromomettlane NO NO u 0009 Chloroethane NO NO u 0009
Acetonitrile 0130 022 0024
Trlchlorcrfluoromethane 0263 lAB 0010 Aaylonltrile NO NP u 0012 11-DIChloroethene NO NO u 0009
Dldloromelhane NO NO u (IOlD
carbon Disulfide 0032 010 u 0033 T~hlo~fluonHdhane 0107 082 0011 tr~ns-12-0ichloroethyler~ NO NO u 0008 11-Dichloroethane ljO NO u 0008 Methl tert-Butyl Ether NO NO u 0008 Methyl Ethyl Ketone 0382 113 0157
Chloroprene NO NO u 0008 ciamp-12-0ichloroethylene NO NO u 0009 Bromochloromethane NO NO u 0008 011oroform NO NO u 0009 Ethyl tert-Butyl Ether NO NO u 0008 JI-Dichloroethilne NO NO u 0009 111-Trichloroethane NO NO u (l022
Benzene ozos 067 0029
Carbon Tetrachloride 0101 064 0024 tert-Amyl Methyl Ether NO NO u 1)016 12-DJChiOropropane NO NO u 0023 Ethyl Acrylate NO NO u (1 020
Bromodichloromethane NO NO u 0025 Trichloroethylene NO NO u 0025
Methyl Methacrylilte NO NO u 0022 cis-13-Dichloropropene NO NO u 0022 Methyl Isobutyl llteDM NCI NO u 0022 trans-13-0ichloropropene NO NO u 0025 112-Trldlloroetflane NO NO u 0025 Toluene 0095 036 0016 Olbromodloromelhane NO NO u 0021
Eastern Research Group The results 111 Jhis r~port apply only to the samplts waalylui in accordance with tht chain of custody document This cuuzlytical report must in reprod~~eed in its entirety
Page 11 of 16
CERTIFICATE OF ANALYSISRG EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 111 011 0903
Kansas City KS 66101 SUBMirrED OBiOB11 to 092911
ATTN~ M1chael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE ~ OECAw(irk
Description 150 west of Hwys 169 and 39 Lab ID 1091501-01 Sampled 091411 00 00
Pressure Receipt 13 Hg canister 709 Received 0915111042
Comments Analyzed 0915111926
Air Toxlcs by EPA Compendium Method T0-15 ~ MW
Analvte wmx uqm fli1g RRint 12-Dibromoethane ND IID u 0()18
n-Oddne ND ND u 0015
Tetrachloroethylene ND ND u 0018
Ollorobenzene ND ND u 0021
Ethylbenzene 0035 015 Q017
mpmiddotXylene 0041 018 0034
Bromoform ND NO 11 0025
Styrene NO ND u 002
11-22-Tetradlloroelhane ND ND u 0024
o-Xylene ND NO u 0018
135-Trimethylbenzene NO NO u 0026
124middotTrlrnathylbenzene 0-042 021 0028
m-Dichlorohenzene ND ND u 0034
Chloromethylbenzene ND ND u 0039
p-OIChlorobenzene NO NO u 0348
o-Dichlorobenzere NO NO u 0037
12+Trlchlorobenzene NO ND u 0036
Hexachloro-13-butadlene ND ND u 0037
Eastern Research Group The result in thrs reoort applgt ltmly to the samplts mral1zed m accordanc11 ~ith thilhain of custodgt document This am1lytical report m11st be rbullpmJuced ill it~ entirety
Page 12 of 16
CERTIFrCATE OF ANALYSIS
EPA Region VII FILE tl 027800001030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMITTED 080811 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Description 73 north of Oak St on Plummer Lab ID 1092909-01 Sampled 0928110000
Pressure 0 Receipt 65 Hg canister 140 Received 0929111057
Comments Analyzed 093011 20 34
Analyte
Acetylene middotPropylene
Dldllorodifluoromethane Chlolomettlane
Dlchlorotetrafluoroethllne VInyl chloride 13-Butadlene Bromometl1dne
Chloroethane
Acetunitrile Trldllorotluoromethane
Acrylonitrile
11-0ithloroethene Dichloromethane Carbon DisulfJde
Trlchlorotrlfkloroetftane lranr1 2-0khloroethylene
11-Dithloroelhane
Methyl tert-Butyl Ether Methyl Ethyl Ketone Chloroprene ds-1HllchloiJethylene Bromochloromethane Chlorofvnn
Ethyl tert-Butyl Ether 12-Dichloroethane 111middotTriChloroethane
Benzene carbon Tetrachloride tert-Amyl Methyl Ether 12-Didlonopropane Ethyl Acrylate Bromodlchlorornelhane Trichloroethylene
Methyl MetllacrylaJ
ds-13-Dithloropropene Methyl Isobutyl KetDne trans-13-0khlorapropene 112-Trichloroethane
Toluene Olbromochloromethane
Air Toxics by EPA Compendium Method T0-15 Results mL
ORb YIiID Eiilg I1IZD 223 238 016 123 212 0039
0564 280 0~11
0525 109 0012 0018 013 ooot
NO NO u 0008 0181 040 0~07
NO NO u o009 NO NO u 0009
0157 028 0024 ozgo 163 0010
NO NO u 0(112 NO NO u 0009
0154 054 0010 0045 0 14 0033 0092 071 0011
NO NO u 0008 NO NO u 0008 NO NO u 0~08
0624 184 0157 NO NO u 0008 NO NO u 0009 NO NO u 0008
0035 017 0009 NO NO u 0008 NO NO u 0009
0012 007 u 0022 L49 477 0029
0088 o56 0024 NO NO u 0016 ND NO u 0023 NO NO u 0020 NO ND u 0025
0178 096 0025
NO NO u 0022 NO NO u 0022
0094 039 0022 NO NO u 0025 NO NO u 0025
276 10400 D 0040 r~O NO u 0021
Eastern Research Group The results m this repon apply only to the samples cmolylld in accordance wilh the chain of cUStOdy docWMnt This arwlytlcal rJort mu~middott be reproduced in its entirety
Page 13 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMITTED 0808111 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECA wa1lt
Description 75 north of Oak St on Plummer Lab ID 1092909-01 Sampled 092811 0000
Pressure Receipt 65 Hg canister 140 Received 0929111057
Comments Analyzed 0930112034
Air Toxics by EPA Compendium Method T0-15 Results lmb
Analyte mmx ugm3 flil on 12-Dibromoethane NO NO u 0018
n-Octane 0193 090 0015 Tetrachloroethylene 0019 013 0018
Chlorobenzene NO NO u 0021
Ethyl benzene 0356 155 p017 mp-Xylene 1oamp 461 OOl4
Bromoform NO NO u 6025
Sty~Wte 0060 026 0022 lll2-Tetrachloroethane NO NO u 0-024
o-Xylene P422 184 01118 135-TrlmethylbenEene 0094 046 0026 1124-Trlmethylbenzene 0340 167 0028
m-Dichlorobenzene 0043 016 0034 Chloromethylbenzene NO NO u 0039
p-Dichlorobenzene 0019 011 u 0035
rDichlorobenzellE NO NO u 0037 121-Trochlorobenzene NO NO u 0-036
Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The ll$Ults in rhis repon appl) NIhbull to the samples analyted in accordance with the cham of custody document Thta analybullical rrporl must he reproduced in in entirety
Page 14 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII FILE tl 027800001 030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS66101 SUBMmED 080811 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX~ (913) 551-5000 SITE CODE OECAwork
IAnalyte Result Units SOurce Result RPD
RPD Umit Note
Eastern Research Group ~ resulu in this reprJrt apply oraly to the samples analyed 111 accordance with the chain of crutody docunumt 1his anulmcal report must be reprodu~ed In its enrlnty
Page 15 of 16
CERTIFICATE OF ANALYSISRG EPA Region VII FILEmiddot 027800001 030
300 Minnesota Avenue REPORTED 1110 11 09middot03
Kansas City KS 66101 SUBMITTED 08101311 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX~ (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
u Under Detection Umlt
o Th1s result obtained by dilution
ND Analyte NOT DETECTED at or above the Method Detecbon Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group T1r results in thH report apply on() w the sample tmayzed il occordancltt with the cham of bullur1ody dotumnt This anayllcai report must be prwiuced in its entirety
Page 16 of 16
~RG Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
December 05 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 111511 1121
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the amtract for NMOC UATMP PAMS CSATAM and NATTS support (US EPA Contract No EPD-09-D48) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please oontact me at 919-468-7930
Sincerely
Laura Van Enwyck Project Manager lauravanenwyckergcom
The information contained in this report and its attachment(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauraJnenwyckergcom and delete the report without retairring any copies
Page 1 of6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 120511 1059
Kansas City KS 66101 SUBMITTED 111511
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Lincoln amp 39 Highway 1111501-01 Air 111411 0000 111511 1121 (111 W Lincoln)
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wfth the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001030
REPORTED 120511 1059
SUBMITTED 111511
AQS SITE CODE
SITE CODE OECAwork
DesaiptionUncoln amp 39 Highway (111 W Uncoln) Lab ID 1111501-01 Sampled 111411 0000
Pressure Receipt 8 Hg canister 636 Received 1115111121
Comments Analyzed 111611 0932
Air Toxics by EPA Compendium Method T0-15 blulb lmL
Analvte Jmbx Yllm fiG JlRbl Acetylene 0171 018 A-Ql 0016 Propylene 0272 OA7 A-Ql 0039 Dlchlorodlfluoromethane 0503 2A9 A-Ql 0011 Chloromethane OA74 098 A-Ql 0011 Dichlorobtraftuoroethane 0016 011 A-Ql 0009 Vinyl chloride ND ND A-Ql U 0008 13-Buladlene 0020 004 A-Ql 0007 Bromomethane 0011 004 AmiddotOl 0009 Chloroethane ND ND A-Ql U 0009 Acetonitrile 0138 023 A-Ql 0024 Trichloroftuoromethane D304 L71 A-Ql 0010 Acrylonitrile ND ND A-Q1 U 0012
11-Dichloroethene ND ND A-Q1 U 0009 Dichloromethane 0266 093 A-Ql 0010 Carbon Disulfide 0129 040 A-Ql 0033 Trichlorotrifluoroethane 0079 061 A-Ql 0011 trans-12-0ichloroethylene ND ND A-Ql U 0008 11-Dichloroethane ND ND A-Ql U 0008 Methyl tert-Butyl Ether ND NO A-Q1 U 0008 Methyl Ethyl Ketone 0760 us AmiddotOl 0157 Chloroprene ND NO A-Ql U 0008
cis-12-Dichloroethylene NO NO A-Ql U 0009 Bromochloromethane NO NO A-Ql U 0008 Chloroform NO NO A-Ql U 0009
Ethyl tert-Butyl Ether NO NO Amiddot01 U 0008 12-Dichloroethane 0026 011 A-Ql 0009 111-Trichloroethane 0006 003 A-Q1 U 0022 Benzene 113 362 A-Q1 0029 Carbon Tetrachloride 0069 OA4 A-Q1 0024 tert-Amyl Methyl Ether ND ND A-Ql U 0016 12-Dichloropropane ND NO A-Ql U 0023
Ethyl Acrylate NO NO A-Ql U 0020
Bromodlchloromethane ND NO A-o1 u 0025 Trichloroethylene NO ND A-01 U 0025
Methyl Methacrylate ND NO A-Q1 U 0022 cis-13-Dichloropropene NO NO A-Ql U 0022 Methyl Isobutyl Ketone 0047 019 A-Ql 0022 trans-13-Dichloropropene NO ND A-Q1 U 0025 112-Trichloroethane NO NO A-Q1 U 0025
Toluene 0661 250 A-01 0016 Dibromochloromethane NO ND A-Q1 U 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repoTt must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1210511 1059
Kansas City KS 66101 SUBMITTED 1115 11
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption Uncoln amp 39 Highway (111 W Lincoln) Lab ID 1111501-01 Sampled 111411 0000
Pressure Receipt 8 Hg canister 636 Received 1115111121
Comments Analyzed 111611 0932
Air Toxics by EPA Compendium Method T0-15 RuJID mL
AnaMe IU1bll ~ BiSl IU1bll 12-Dlbromoethane NO NO A-Ql U 0018
n-Oct3ne 0025 012 A-Ql 0015
Tetrachloroethylene 0016 011 A-Ql U 0018
Ollorobenzene NO NO A-Ql U 0021
Ethylbenzene 0068 030 A-Ql 0017
mp-Xylene 0144 063 A-Ql 0034
Bromoform NO NO A-Ql U 0025
Styrene 0058 025 A-Ql 0022
1122-Tetrachloroethane NO NO A-Ql U 0024
o-Xylene 0058 025 A-ol 0018
135-Trlmetflylbenzene 0050 025 A-01 0026
124-Trimetflylbenzene 0130 064 A-Ql 0028
m-Dichlorobenzene NO NO A-Ql U 0034
Chloromelhylbenzene NO NO A-ol U 0039
p-Oichlorobenzene 0027 016 A-Ql U 0035
o-Oichlorobenzene NO NO A-Ql U 0037
124-Trichlorobenzene NO NO A-ol U 0036
Hexachloro-13-butadiene NO NO A-ol U 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 120511 1059
Kansas City KS 66101 SUBMITTED 111511
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance witlz tlze chain of custody documellt This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1205111 1 059
Kansas City KS 66101 SUBMITTED 11151 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
A-ol Estimated value due to possible canister leak
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical re-port must be reproduced in its entirety
Page 6 of 6
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
December 15 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 1206111229
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for NMOC UATMP PAMS CSATAM and NATTS support (US EPA Contract No EPD-09-048) This rover page is an integral part of this report and any exceptions or oomments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Project Manager lauravanenwyckergcom
The information contained in this report and its attachment(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify laura vanenwyck ergcom and delete the report without retaining any copies
Page 1 of 6
RG CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111 1041
Kansas City KS 66101 SUBMITTED 1206 11
ATTN Michael F Davis AQS SITE CODE
PHONE 913) 551-5042 FAX 913) 551-5000 SITE CODE OECAwork
ANALYTlCAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Ash amp Forest SE Corner 1120611-01 Air 120411 0000 120611 1229
middotI I
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytirol repon must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
ALE 027800001030
REPORTED 1215111041
SUBMmED 1210611
AQS SITE CODE
SITE CODE OECAwork
Desaiptlon Ash amp Forest SE Comer Lab ID 1120611-01 sampled 120411 oooo Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 BuYltl MQL
AnaMe IUlllll lWm Bag IUlllll Acetylene OA36 OA7 0016 Propylene 0304 052 0039 Dichlorodiftuoromethane 0567 281 0011 Chloromethane 0566 117 0012 Dlchlorotetnlftuoroethane 0019 013 0009 Vinyl chloride NO NO u 0008 13-Butadiene NO NO u 0007 Bromomethane 0012 005 0009 Chloroethane NO NO u 0009 Acetonitrile 0111 019 0024 Trichlorofluoromethane 0284 160 0010 Aaylonitrile ND NO u 0012 11-Dichloroethene ND ND u 0009 Dichloromethane 0083 029 0010 Carbon Disulfide 0019 006 u 0033
Trlchlorotrlftuoroethane 0099 076 0011 trans-12-Dichloroethylene ND ND u 0008 11-Dichloroethane ND NO u 0008 Methyl tert-Butyl Ether NO NO u 0008 Methyl Ethyl Ketone 0536 158 0157 Chloroprene NO NO u 0008 cis-12-Dichloroethylene NO ND u 0009 Bromochloromethane NO NO u 0008 Chloroform 0022 011 0009 Ethyl tert-Butyl Ether NO NO u 0008 12-Dichloroethane 0025 010 0009 111-Trichloroethane 0011 006 u 0022 Benzene 0188 060 0029 carbon Tetrachloride 0106 067 0024 tert-Amyl Methyl Ether NO NO u 0016 12-Dichloropropane NO NO u 0023 Ethyl Acrylate ND NO u 0020
Bromodichloromethane NO NO u 0025 Trichloroethylene NO NO u 0025 Methyl Methacrylate NO NO u 0022 cis-13-Dichloropropene NO NO u 0022
Methyl Isobutyl Ketone 0042 017 0022 trans-13-Dichloropropene ND NO u 0025 112-Trichloroethane NO NO u 0025
Toluene 0149 056 0016 Oibromochloromethane 0003 003 u 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproducedin its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 121511 1041
Kansas City KS 66101 SUBMmED 1210611
ATTN Michael F Davis AQS SITE CODE
PHONE (913 551-5042 FAX (913 551-5000 SITE CODE OECAwork
Description Ash amp Forest SE Comer Lab ID 1120611-01 Sampled 120411 0000
Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 llWdtl MID
Analyte ubll IUllm Bag ubll 12-0ibromoethane NO NO u 0018 nmiddotOctane 0044 021 0015 Tetrachloroethylene 0006 004 u 0018
Chlorobenzene NO NO u 0021 Ethylbenzene 0047 021 0017 mp-Xylene 0070 031 0034 Bromoform NO NO u 0025 Styrene 0034 015 0022 1122-Tetrachloroethane NO NO u 0024 o-Xylene 0036 016 0018 135-Trlmethylbenzene 0025 012 u 0026 124-Trlmetllylbenzene 0047 023 0028 m-Oichlorobenzene NO NO u 0034
Chloromethylbenzene NO NO u 0039 p-Dichlorcbenzene 0005 003 u 0348 a-Dichlorobenzene NO NO u 0037
124-Trlchlorobenzene NO NO u 0036 Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repon must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS~RG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 66101 SUBMITTED 12061 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPDIAnalyte Result Units Result RPD um1t Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 661 01 SUBMITTED 120611
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its enJirety
Page 6 of 6
i
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
March 12 2012
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 030512 0916
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for UATMP NATTS CSATAM PAMS and NMOC support (US EPA Contract No 68-D-Q9-048) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Program Manager lauravanenwyckergcom
The information contained in this report and its attachmcnt(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauravanenwyckergcom and delete the report dthout retaining any copies
Page 1 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 0312112 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
6th St between Central amp 2030501-01 Air 030212 0000 030512 0916 Malcom
Eastern Research Group The results in this report apply only to the samples anal zed in accordance With the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Aven ue REPORTED 031212 1 051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 ~ tml
Analvte RRbll Y9lD1 flu RRbll Acetylene 0627 067 0072 Propylene 0484 084 0033
Dichlorodllluoromethane 0500 248 0023 Chloromethane 0557 115 0033
Dichlorotetrafluoroethane 0015 011 0012 Vinyl chloride NO NO u 0011
13-Butadlene 0036 oo8 0011
Bromomethane 0012 005 0012 Chloroethane NO NO u 0017
Acetonitrile 0073 012 0073
Trichlorofluoromethane 0258 145 0015 Acrylonitrile NO NO u 0020
11-0ichloroethene NO NO u 0014
Dichloromethane 0185 064 0023
Carbon Disulfide 0037 012 0014 Trichlorobitluoroethane 0119 091 0017
trans-12-0ichloroethylene NO NO u 0012
11-0ichloroethane NO NO u 0015
Methyl tert-Butyl Ether NO NO u 0011
Chloroprene NO NO u 0012
ds-12-0ich loroethylene NO NO u OD18
Bromochloromethane NO NO u 0014
Chloroform NO ND u 0014
Ethyl tert-Butyl Ether NO NO u 0011
12-Dichloroethane 0019 008 0016
111-Trichloroethane 0012 007 u 0020
Benzene 0344 L10 0061 Carbon Tetrachloride 0088 056 0024
tert-Amyl Methyl Ether NO NO u 0016
12-0ichloropropane ND NO u 0019
Ethyl Acrylate ND NO u 0014
Bromodichloromethane ND NO u 0021
Trichloroethylene NO ND u 0022
Methyl Methacrylate ND NO u 0025
ds-13-0ichloropropene NO NO u 0015
Methyl Isobutyl Ketone 0015 oo6 0015
trans-13-0ichloropropene NO ND u 0016
112-Trichloroethane NO NO u 0021
Toluene 0416 157 0045
Oibromochloromethane ND NO u 0018
12-0ibromoethane ND NO u 0017
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551 -5000
FILE 027800001030
REPORTED 0312 12 1051
SUBMITTED 030512
AQS SITE CODE
SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 Bwdtl MJlL
Analvte Jmbll Y9Lm Big Jmbx nmiddotOclane 0039 018 0020 Tetrachloroethylene 0005 003 u 0020
Chlorobenzene ND ND u 0025
Ethylbenzene 0045 020 0023 mp-Xylene 0112 OA9 0037 Bromoform ND ND u 0020
Styrene 0030 013 0024 1122-Tetrachloroethane ND ND u 0018
o-Xylene 0050 022 0020
135-Trimethylbenzene 0019 009 u 0022
124-Trimethylbenzene 0047 023 0025 m-Dichlorobenzene ND ND u 0024
p-Dichlorobenzene 0004 002 u 0019
a-Dichlorobenzene NO ND u 0021
124-Trichlorobenzene ND ND u 0022
Hexachloro-13-butadiene ND ND u 0022
Eastern Research Group The results in this report apply only 1o the samples analyzed in accordance with the chain of custody document This analytical rep ort must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 031212 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wilh the chain of custody document This analytical report must be reproduced in its enrirety
Page 5 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 03121121051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report nutst be reproduced in its entirety
Page 6 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN MIChael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001 030
REPORTED~ 1110111 0903
SUBMmED 0810811 to 092911
AQS SITE CODE
SITE CODE OECAwork
Description 150 west of Hwys 169 and 39 Lab ID 1091501-01 sampled 091411 oooo Pressure 0 ReClelpt 13 Hg canister 709 Received 091511 10~42
Comments Analyzed 0915111926
Air Taxies by EPA Compendium Method T0-15 BHIIIm MDI
Analyte JUlbll li9Lm fJJg JlRinl AcBtylene 0234 025 0-016 Propylene 0258 045 0-0~11
Dlchlorodlfluoromettmne 0544 270 oo11 Chloromethane 0526 109 0 012
DichlorolelrifAJoroethane NO NO u Otgt09 Vinyl chloride NO NO u 0008 13-Butildlene NO NO u 0007 Bromomettlane NO NO u 0009 Chloroethane NO NO u 0009
Acetonitrile 0130 022 0024
Trlchlorcrfluoromethane 0263 lAB 0010 Aaylonltrile NO NP u 0012 11-DIChloroethene NO NO u 0009
Dldloromelhane NO NO u (IOlD
carbon Disulfide 0032 010 u 0033 T~hlo~fluonHdhane 0107 082 0011 tr~ns-12-0ichloroethyler~ NO NO u 0008 11-Dichloroethane ljO NO u 0008 Methl tert-Butyl Ether NO NO u 0008 Methyl Ethyl Ketone 0382 113 0157
Chloroprene NO NO u 0008 ciamp-12-0ichloroethylene NO NO u 0009 Bromochloromethane NO NO u 0008 011oroform NO NO u 0009 Ethyl tert-Butyl Ether NO NO u 0008 JI-Dichloroethilne NO NO u 0009 111-Trichloroethane NO NO u (l022
Benzene ozos 067 0029
Carbon Tetrachloride 0101 064 0024 tert-Amyl Methyl Ether NO NO u 1)016 12-DJChiOropropane NO NO u 0023 Ethyl Acrylate NO NO u (1 020
Bromodichloromethane NO NO u 0025 Trichloroethylene NO NO u 0025
Methyl Methacrylilte NO NO u 0022 cis-13-Dichloropropene NO NO u 0022 Methyl Isobutyl llteDM NCI NO u 0022 trans-13-0ichloropropene NO NO u 0025 112-Trldlloroetflane NO NO u 0025 Toluene 0095 036 0016 Olbromodloromelhane NO NO u 0021
Eastern Research Group The results 111 Jhis r~port apply only to the samplts waalylui in accordance with tht chain of custody document This cuuzlytical report must in reprod~~eed in its entirety
Page 11 of 16
CERTIFICATE OF ANALYSISRG EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 111 011 0903
Kansas City KS 66101 SUBMirrED OBiOB11 to 092911
ATTN~ M1chael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE ~ OECAw(irk
Description 150 west of Hwys 169 and 39 Lab ID 1091501-01 Sampled 091411 00 00
Pressure Receipt 13 Hg canister 709 Received 0915111042
Comments Analyzed 0915111926
Air Toxlcs by EPA Compendium Method T0-15 ~ MW
Analvte wmx uqm fli1g RRint 12-Dibromoethane ND IID u 0()18
n-Oddne ND ND u 0015
Tetrachloroethylene ND ND u 0018
Ollorobenzene ND ND u 0021
Ethylbenzene 0035 015 Q017
mpmiddotXylene 0041 018 0034
Bromoform ND NO 11 0025
Styrene NO ND u 002
11-22-Tetradlloroelhane ND ND u 0024
o-Xylene ND NO u 0018
135-Trimethylbenzene NO NO u 0026
124middotTrlrnathylbenzene 0-042 021 0028
m-Dichlorohenzene ND ND u 0034
Chloromethylbenzene ND ND u 0039
p-OIChlorobenzene NO NO u 0348
o-Dichlorobenzere NO NO u 0037
12+Trlchlorobenzene NO ND u 0036
Hexachloro-13-butadlene ND ND u 0037
Eastern Research Group The result in thrs reoort applgt ltmly to the samplts mral1zed m accordanc11 ~ith thilhain of custodgt document This am1lytical report m11st be rbullpmJuced ill it~ entirety
Page 12 of 16
CERTIFrCATE OF ANALYSIS
EPA Region VII FILE tl 027800001030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMITTED 080811 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Description 73 north of Oak St on Plummer Lab ID 1092909-01 Sampled 0928110000
Pressure 0 Receipt 65 Hg canister 140 Received 0929111057
Comments Analyzed 093011 20 34
Analyte
Acetylene middotPropylene
Dldllorodifluoromethane Chlolomettlane
Dlchlorotetrafluoroethllne VInyl chloride 13-Butadlene Bromometl1dne
Chloroethane
Acetunitrile Trldllorotluoromethane
Acrylonitrile
11-0ithloroethene Dichloromethane Carbon DisulfJde
Trlchlorotrlfkloroetftane lranr1 2-0khloroethylene
11-Dithloroelhane
Methyl tert-Butyl Ether Methyl Ethyl Ketone Chloroprene ds-1HllchloiJethylene Bromochloromethane Chlorofvnn
Ethyl tert-Butyl Ether 12-Dichloroethane 111middotTriChloroethane
Benzene carbon Tetrachloride tert-Amyl Methyl Ether 12-Didlonopropane Ethyl Acrylate Bromodlchlorornelhane Trichloroethylene
Methyl MetllacrylaJ
ds-13-Dithloropropene Methyl Isobutyl KetDne trans-13-0khlorapropene 112-Trichloroethane
Toluene Olbromochloromethane
Air Toxics by EPA Compendium Method T0-15 Results mL
ORb YIiID Eiilg I1IZD 223 238 016 123 212 0039
0564 280 0~11
0525 109 0012 0018 013 ooot
NO NO u 0008 0181 040 0~07
NO NO u o009 NO NO u 0009
0157 028 0024 ozgo 163 0010
NO NO u 0(112 NO NO u 0009
0154 054 0010 0045 0 14 0033 0092 071 0011
NO NO u 0008 NO NO u 0008 NO NO u 0~08
0624 184 0157 NO NO u 0008 NO NO u 0009 NO NO u 0008
0035 017 0009 NO NO u 0008 NO NO u 0009
0012 007 u 0022 L49 477 0029
0088 o56 0024 NO NO u 0016 ND NO u 0023 NO NO u 0020 NO ND u 0025
0178 096 0025
NO NO u 0022 NO NO u 0022
0094 039 0022 NO NO u 0025 NO NO u 0025
276 10400 D 0040 r~O NO u 0021
Eastern Research Group The results m this repon apply only to the samples cmolylld in accordance wilh the chain of cUStOdy docWMnt This arwlytlcal rJort mu~middott be reproduced in its entirety
Page 13 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMITTED 0808111 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECA wa1lt
Description 75 north of Oak St on Plummer Lab ID 1092909-01 Sampled 092811 0000
Pressure Receipt 65 Hg canister 140 Received 0929111057
Comments Analyzed 0930112034
Air Toxics by EPA Compendium Method T0-15 Results lmb
Analyte mmx ugm3 flil on 12-Dibromoethane NO NO u 0018
n-Octane 0193 090 0015 Tetrachloroethylene 0019 013 0018
Chlorobenzene NO NO u 0021
Ethyl benzene 0356 155 p017 mp-Xylene 1oamp 461 OOl4
Bromoform NO NO u 6025
Sty~Wte 0060 026 0022 lll2-Tetrachloroethane NO NO u 0-024
o-Xylene P422 184 01118 135-TrlmethylbenEene 0094 046 0026 1124-Trlmethylbenzene 0340 167 0028
m-Dichlorobenzene 0043 016 0034 Chloromethylbenzene NO NO u 0039
p-Dichlorobenzene 0019 011 u 0035
rDichlorobenzellE NO NO u 0037 121-Trochlorobenzene NO NO u 0-036
Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The ll$Ults in rhis repon appl) NIhbull to the samples analyted in accordance with the cham of custody document Thta analybullical rrporl must he reproduced in in entirety
Page 14 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII FILE tl 027800001 030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS66101 SUBMmED 080811 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX~ (913) 551-5000 SITE CODE OECAwork
IAnalyte Result Units SOurce Result RPD
RPD Umit Note
Eastern Research Group ~ resulu in this reprJrt apply oraly to the samples analyed 111 accordance with the chain of crutody docunumt 1his anulmcal report must be reprodu~ed In its enrlnty
Page 15 of 16
CERTIFICATE OF ANALYSISRG EPA Region VII FILEmiddot 027800001 030
300 Minnesota Avenue REPORTED 1110 11 09middot03
Kansas City KS 66101 SUBMITTED 08101311 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX~ (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
u Under Detection Umlt
o Th1s result obtained by dilution
ND Analyte NOT DETECTED at or above the Method Detecbon Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group T1r results in thH report apply on() w the sample tmayzed il occordancltt with the cham of bullur1ody dotumnt This anayllcai report must be prwiuced in its entirety
Page 16 of 16
~RG Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
December 05 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 111511 1121
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the amtract for NMOC UATMP PAMS CSATAM and NATTS support (US EPA Contract No EPD-09-D48) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please oontact me at 919-468-7930
Sincerely
Laura Van Enwyck Project Manager lauravanenwyckergcom
The information contained in this report and its attachment(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauraJnenwyckergcom and delete the report without retairring any copies
Page 1 of6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 120511 1059
Kansas City KS 66101 SUBMITTED 111511
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Lincoln amp 39 Highway 1111501-01 Air 111411 0000 111511 1121 (111 W Lincoln)
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wfth the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001030
REPORTED 120511 1059
SUBMITTED 111511
AQS SITE CODE
SITE CODE OECAwork
DesaiptionUncoln amp 39 Highway (111 W Uncoln) Lab ID 1111501-01 Sampled 111411 0000
Pressure Receipt 8 Hg canister 636 Received 1115111121
Comments Analyzed 111611 0932
Air Toxics by EPA Compendium Method T0-15 blulb lmL
Analvte Jmbx Yllm fiG JlRbl Acetylene 0171 018 A-Ql 0016 Propylene 0272 OA7 A-Ql 0039 Dlchlorodlfluoromethane 0503 2A9 A-Ql 0011 Chloromethane OA74 098 A-Ql 0011 Dichlorobtraftuoroethane 0016 011 A-Ql 0009 Vinyl chloride ND ND A-Ql U 0008 13-Buladlene 0020 004 A-Ql 0007 Bromomethane 0011 004 AmiddotOl 0009 Chloroethane ND ND A-Ql U 0009 Acetonitrile 0138 023 A-Ql 0024 Trichloroftuoromethane D304 L71 A-Ql 0010 Acrylonitrile ND ND A-Q1 U 0012
11-Dichloroethene ND ND A-Q1 U 0009 Dichloromethane 0266 093 A-Ql 0010 Carbon Disulfide 0129 040 A-Ql 0033 Trichlorotrifluoroethane 0079 061 A-Ql 0011 trans-12-0ichloroethylene ND ND A-Ql U 0008 11-Dichloroethane ND ND A-Ql U 0008 Methyl tert-Butyl Ether ND NO A-Q1 U 0008 Methyl Ethyl Ketone 0760 us AmiddotOl 0157 Chloroprene ND NO A-Ql U 0008
cis-12-Dichloroethylene NO NO A-Ql U 0009 Bromochloromethane NO NO A-Ql U 0008 Chloroform NO NO A-Ql U 0009
Ethyl tert-Butyl Ether NO NO Amiddot01 U 0008 12-Dichloroethane 0026 011 A-Ql 0009 111-Trichloroethane 0006 003 A-Q1 U 0022 Benzene 113 362 A-Q1 0029 Carbon Tetrachloride 0069 OA4 A-Q1 0024 tert-Amyl Methyl Ether ND ND A-Ql U 0016 12-Dichloropropane ND NO A-Ql U 0023
Ethyl Acrylate NO NO A-Ql U 0020
Bromodlchloromethane ND NO A-o1 u 0025 Trichloroethylene NO ND A-01 U 0025
Methyl Methacrylate ND NO A-Q1 U 0022 cis-13-Dichloropropene NO NO A-Ql U 0022 Methyl Isobutyl Ketone 0047 019 A-Ql 0022 trans-13-Dichloropropene NO ND A-Q1 U 0025 112-Trichloroethane NO NO A-Q1 U 0025
Toluene 0661 250 A-01 0016 Dibromochloromethane NO ND A-Q1 U 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repoTt must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1210511 1059
Kansas City KS 66101 SUBMITTED 1115 11
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption Uncoln amp 39 Highway (111 W Lincoln) Lab ID 1111501-01 Sampled 111411 0000
Pressure Receipt 8 Hg canister 636 Received 1115111121
Comments Analyzed 111611 0932
Air Toxics by EPA Compendium Method T0-15 RuJID mL
AnaMe IU1bll ~ BiSl IU1bll 12-Dlbromoethane NO NO A-Ql U 0018
n-Oct3ne 0025 012 A-Ql 0015
Tetrachloroethylene 0016 011 A-Ql U 0018
Ollorobenzene NO NO A-Ql U 0021
Ethylbenzene 0068 030 A-Ql 0017
mp-Xylene 0144 063 A-Ql 0034
Bromoform NO NO A-Ql U 0025
Styrene 0058 025 A-Ql 0022
1122-Tetrachloroethane NO NO A-Ql U 0024
o-Xylene 0058 025 A-ol 0018
135-Trlmetflylbenzene 0050 025 A-01 0026
124-Trimetflylbenzene 0130 064 A-Ql 0028
m-Dichlorobenzene NO NO A-Ql U 0034
Chloromelhylbenzene NO NO A-ol U 0039
p-Oichlorobenzene 0027 016 A-Ql U 0035
o-Oichlorobenzene NO NO A-Ql U 0037
124-Trichlorobenzene NO NO A-ol U 0036
Hexachloro-13-butadiene NO NO A-ol U 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 120511 1059
Kansas City KS 66101 SUBMITTED 111511
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance witlz tlze chain of custody documellt This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1205111 1 059
Kansas City KS 66101 SUBMITTED 11151 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
A-ol Estimated value due to possible canister leak
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical re-port must be reproduced in its entirety
Page 6 of 6
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
December 15 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 1206111229
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for NMOC UATMP PAMS CSATAM and NATTS support (US EPA Contract No EPD-09-048) This rover page is an integral part of this report and any exceptions or oomments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Project Manager lauravanenwyckergcom
The information contained in this report and its attachment(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify laura vanenwyck ergcom and delete the report without retaining any copies
Page 1 of 6
RG CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111 1041
Kansas City KS 66101 SUBMITTED 1206 11
ATTN Michael F Davis AQS SITE CODE
PHONE 913) 551-5042 FAX 913) 551-5000 SITE CODE OECAwork
ANALYTlCAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Ash amp Forest SE Corner 1120611-01 Air 120411 0000 120611 1229
middotI I
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytirol repon must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
ALE 027800001030
REPORTED 1215111041
SUBMmED 1210611
AQS SITE CODE
SITE CODE OECAwork
Desaiptlon Ash amp Forest SE Comer Lab ID 1120611-01 sampled 120411 oooo Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 BuYltl MQL
AnaMe IUlllll lWm Bag IUlllll Acetylene OA36 OA7 0016 Propylene 0304 052 0039 Dichlorodiftuoromethane 0567 281 0011 Chloromethane 0566 117 0012 Dlchlorotetnlftuoroethane 0019 013 0009 Vinyl chloride NO NO u 0008 13-Butadiene NO NO u 0007 Bromomethane 0012 005 0009 Chloroethane NO NO u 0009 Acetonitrile 0111 019 0024 Trichlorofluoromethane 0284 160 0010 Aaylonitrile ND NO u 0012 11-Dichloroethene ND ND u 0009 Dichloromethane 0083 029 0010 Carbon Disulfide 0019 006 u 0033
Trlchlorotrlftuoroethane 0099 076 0011 trans-12-Dichloroethylene ND ND u 0008 11-Dichloroethane ND NO u 0008 Methyl tert-Butyl Ether NO NO u 0008 Methyl Ethyl Ketone 0536 158 0157 Chloroprene NO NO u 0008 cis-12-Dichloroethylene NO ND u 0009 Bromochloromethane NO NO u 0008 Chloroform 0022 011 0009 Ethyl tert-Butyl Ether NO NO u 0008 12-Dichloroethane 0025 010 0009 111-Trichloroethane 0011 006 u 0022 Benzene 0188 060 0029 carbon Tetrachloride 0106 067 0024 tert-Amyl Methyl Ether NO NO u 0016 12-Dichloropropane NO NO u 0023 Ethyl Acrylate ND NO u 0020
Bromodichloromethane NO NO u 0025 Trichloroethylene NO NO u 0025 Methyl Methacrylate NO NO u 0022 cis-13-Dichloropropene NO NO u 0022
Methyl Isobutyl Ketone 0042 017 0022 trans-13-Dichloropropene ND NO u 0025 112-Trichloroethane NO NO u 0025
Toluene 0149 056 0016 Oibromochloromethane 0003 003 u 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproducedin its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 121511 1041
Kansas City KS 66101 SUBMmED 1210611
ATTN Michael F Davis AQS SITE CODE
PHONE (913 551-5042 FAX (913 551-5000 SITE CODE OECAwork
Description Ash amp Forest SE Comer Lab ID 1120611-01 Sampled 120411 0000
Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 llWdtl MID
Analyte ubll IUllm Bag ubll 12-0ibromoethane NO NO u 0018 nmiddotOctane 0044 021 0015 Tetrachloroethylene 0006 004 u 0018
Chlorobenzene NO NO u 0021 Ethylbenzene 0047 021 0017 mp-Xylene 0070 031 0034 Bromoform NO NO u 0025 Styrene 0034 015 0022 1122-Tetrachloroethane NO NO u 0024 o-Xylene 0036 016 0018 135-Trlmethylbenzene 0025 012 u 0026 124-Trlmetllylbenzene 0047 023 0028 m-Oichlorobenzene NO NO u 0034
Chloromethylbenzene NO NO u 0039 p-Dichlorcbenzene 0005 003 u 0348 a-Dichlorobenzene NO NO u 0037
124-Trlchlorobenzene NO NO u 0036 Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repon must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS~RG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 66101 SUBMITTED 12061 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPDIAnalyte Result Units Result RPD um1t Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 661 01 SUBMITTED 120611
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its enJirety
Page 6 of 6
i
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
March 12 2012
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 030512 0916
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for UATMP NATTS CSATAM PAMS and NMOC support (US EPA Contract No 68-D-Q9-048) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Program Manager lauravanenwyckergcom
The information contained in this report and its attachmcnt(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauravanenwyckergcom and delete the report dthout retaining any copies
Page 1 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 0312112 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
6th St between Central amp 2030501-01 Air 030212 0000 030512 0916 Malcom
Eastern Research Group The results in this report apply only to the samples anal zed in accordance With the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Aven ue REPORTED 031212 1 051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 ~ tml
Analvte RRbll Y9lD1 flu RRbll Acetylene 0627 067 0072 Propylene 0484 084 0033
Dichlorodllluoromethane 0500 248 0023 Chloromethane 0557 115 0033
Dichlorotetrafluoroethane 0015 011 0012 Vinyl chloride NO NO u 0011
13-Butadlene 0036 oo8 0011
Bromomethane 0012 005 0012 Chloroethane NO NO u 0017
Acetonitrile 0073 012 0073
Trichlorofluoromethane 0258 145 0015 Acrylonitrile NO NO u 0020
11-0ichloroethene NO NO u 0014
Dichloromethane 0185 064 0023
Carbon Disulfide 0037 012 0014 Trichlorobitluoroethane 0119 091 0017
trans-12-0ichloroethylene NO NO u 0012
11-0ichloroethane NO NO u 0015
Methyl tert-Butyl Ether NO NO u 0011
Chloroprene NO NO u 0012
ds-12-0ich loroethylene NO NO u OD18
Bromochloromethane NO NO u 0014
Chloroform NO ND u 0014
Ethyl tert-Butyl Ether NO NO u 0011
12-Dichloroethane 0019 008 0016
111-Trichloroethane 0012 007 u 0020
Benzene 0344 L10 0061 Carbon Tetrachloride 0088 056 0024
tert-Amyl Methyl Ether NO NO u 0016
12-0ichloropropane ND NO u 0019
Ethyl Acrylate ND NO u 0014
Bromodichloromethane ND NO u 0021
Trichloroethylene NO ND u 0022
Methyl Methacrylate ND NO u 0025
ds-13-0ichloropropene NO NO u 0015
Methyl Isobutyl Ketone 0015 oo6 0015
trans-13-0ichloropropene NO ND u 0016
112-Trichloroethane NO NO u 0021
Toluene 0416 157 0045
Oibromochloromethane ND NO u 0018
12-0ibromoethane ND NO u 0017
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551 -5000
FILE 027800001030
REPORTED 0312 12 1051
SUBMITTED 030512
AQS SITE CODE
SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 Bwdtl MJlL
Analvte Jmbll Y9Lm Big Jmbx nmiddotOclane 0039 018 0020 Tetrachloroethylene 0005 003 u 0020
Chlorobenzene ND ND u 0025
Ethylbenzene 0045 020 0023 mp-Xylene 0112 OA9 0037 Bromoform ND ND u 0020
Styrene 0030 013 0024 1122-Tetrachloroethane ND ND u 0018
o-Xylene 0050 022 0020
135-Trimethylbenzene 0019 009 u 0022
124-Trimethylbenzene 0047 023 0025 m-Dichlorobenzene ND ND u 0024
p-Dichlorobenzene 0004 002 u 0019
a-Dichlorobenzene NO ND u 0021
124-Trichlorobenzene ND ND u 0022
Hexachloro-13-butadiene ND ND u 0022
Eastern Research Group The results in this report apply only 1o the samples analyzed in accordance with the chain of custody document This analytical rep ort must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 031212 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wilh the chain of custody document This analytical report must be reproduced in its enrirety
Page 5 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 03121121051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report nutst be reproduced in its entirety
Page 6 of 6
CERTIFICATE OF ANALYSISRG EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 111 011 0903
Kansas City KS 66101 SUBMirrED OBiOB11 to 092911
ATTN~ M1chael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE ~ OECAw(irk
Description 150 west of Hwys 169 and 39 Lab ID 1091501-01 Sampled 091411 00 00
Pressure Receipt 13 Hg canister 709 Received 0915111042
Comments Analyzed 0915111926
Air Toxlcs by EPA Compendium Method T0-15 ~ MW
Analvte wmx uqm fli1g RRint 12-Dibromoethane ND IID u 0()18
n-Oddne ND ND u 0015
Tetrachloroethylene ND ND u 0018
Ollorobenzene ND ND u 0021
Ethylbenzene 0035 015 Q017
mpmiddotXylene 0041 018 0034
Bromoform ND NO 11 0025
Styrene NO ND u 002
11-22-Tetradlloroelhane ND ND u 0024
o-Xylene ND NO u 0018
135-Trimethylbenzene NO NO u 0026
124middotTrlrnathylbenzene 0-042 021 0028
m-Dichlorohenzene ND ND u 0034
Chloromethylbenzene ND ND u 0039
p-OIChlorobenzene NO NO u 0348
o-Dichlorobenzere NO NO u 0037
12+Trlchlorobenzene NO ND u 0036
Hexachloro-13-butadlene ND ND u 0037
Eastern Research Group The result in thrs reoort applgt ltmly to the samplts mral1zed m accordanc11 ~ith thilhain of custodgt document This am1lytical report m11st be rbullpmJuced ill it~ entirety
Page 12 of 16
CERTIFrCATE OF ANALYSIS
EPA Region VII FILE tl 027800001030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMITTED 080811 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Description 73 north of Oak St on Plummer Lab ID 1092909-01 Sampled 0928110000
Pressure 0 Receipt 65 Hg canister 140 Received 0929111057
Comments Analyzed 093011 20 34
Analyte
Acetylene middotPropylene
Dldllorodifluoromethane Chlolomettlane
Dlchlorotetrafluoroethllne VInyl chloride 13-Butadlene Bromometl1dne
Chloroethane
Acetunitrile Trldllorotluoromethane
Acrylonitrile
11-0ithloroethene Dichloromethane Carbon DisulfJde
Trlchlorotrlfkloroetftane lranr1 2-0khloroethylene
11-Dithloroelhane
Methyl tert-Butyl Ether Methyl Ethyl Ketone Chloroprene ds-1HllchloiJethylene Bromochloromethane Chlorofvnn
Ethyl tert-Butyl Ether 12-Dichloroethane 111middotTriChloroethane
Benzene carbon Tetrachloride tert-Amyl Methyl Ether 12-Didlonopropane Ethyl Acrylate Bromodlchlorornelhane Trichloroethylene
Methyl MetllacrylaJ
ds-13-Dithloropropene Methyl Isobutyl KetDne trans-13-0khlorapropene 112-Trichloroethane
Toluene Olbromochloromethane
Air Toxics by EPA Compendium Method T0-15 Results mL
ORb YIiID Eiilg I1IZD 223 238 016 123 212 0039
0564 280 0~11
0525 109 0012 0018 013 ooot
NO NO u 0008 0181 040 0~07
NO NO u o009 NO NO u 0009
0157 028 0024 ozgo 163 0010
NO NO u 0(112 NO NO u 0009
0154 054 0010 0045 0 14 0033 0092 071 0011
NO NO u 0008 NO NO u 0008 NO NO u 0~08
0624 184 0157 NO NO u 0008 NO NO u 0009 NO NO u 0008
0035 017 0009 NO NO u 0008 NO NO u 0009
0012 007 u 0022 L49 477 0029
0088 o56 0024 NO NO u 0016 ND NO u 0023 NO NO u 0020 NO ND u 0025
0178 096 0025
NO NO u 0022 NO NO u 0022
0094 039 0022 NO NO u 0025 NO NO u 0025
276 10400 D 0040 r~O NO u 0021
Eastern Research Group The results m this repon apply only to the samples cmolylld in accordance wilh the chain of cUStOdy docWMnt This arwlytlcal rJort mu~middott be reproduced in its entirety
Page 13 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMITTED 0808111 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECA wa1lt
Description 75 north of Oak St on Plummer Lab ID 1092909-01 Sampled 092811 0000
Pressure Receipt 65 Hg canister 140 Received 0929111057
Comments Analyzed 0930112034
Air Toxics by EPA Compendium Method T0-15 Results lmb
Analyte mmx ugm3 flil on 12-Dibromoethane NO NO u 0018
n-Octane 0193 090 0015 Tetrachloroethylene 0019 013 0018
Chlorobenzene NO NO u 0021
Ethyl benzene 0356 155 p017 mp-Xylene 1oamp 461 OOl4
Bromoform NO NO u 6025
Sty~Wte 0060 026 0022 lll2-Tetrachloroethane NO NO u 0-024
o-Xylene P422 184 01118 135-TrlmethylbenEene 0094 046 0026 1124-Trlmethylbenzene 0340 167 0028
m-Dichlorobenzene 0043 016 0034 Chloromethylbenzene NO NO u 0039
p-Dichlorobenzene 0019 011 u 0035
rDichlorobenzellE NO NO u 0037 121-Trochlorobenzene NO NO u 0-036
Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The ll$Ults in rhis repon appl) NIhbull to the samples analyted in accordance with the cham of custody document Thta analybullical rrporl must he reproduced in in entirety
Page 14 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII FILE tl 027800001 030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS66101 SUBMmED 080811 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX~ (913) 551-5000 SITE CODE OECAwork
IAnalyte Result Units SOurce Result RPD
RPD Umit Note
Eastern Research Group ~ resulu in this reprJrt apply oraly to the samples analyed 111 accordance with the chain of crutody docunumt 1his anulmcal report must be reprodu~ed In its enrlnty
Page 15 of 16
CERTIFICATE OF ANALYSISRG EPA Region VII FILEmiddot 027800001 030
300 Minnesota Avenue REPORTED 1110 11 09middot03
Kansas City KS 66101 SUBMITTED 08101311 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX~ (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
u Under Detection Umlt
o Th1s result obtained by dilution
ND Analyte NOT DETECTED at or above the Method Detecbon Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group T1r results in thH report apply on() w the sample tmayzed il occordancltt with the cham of bullur1ody dotumnt This anayllcai report must be prwiuced in its entirety
Page 16 of 16
~RG Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
December 05 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 111511 1121
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the amtract for NMOC UATMP PAMS CSATAM and NATTS support (US EPA Contract No EPD-09-D48) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please oontact me at 919-468-7930
Sincerely
Laura Van Enwyck Project Manager lauravanenwyckergcom
The information contained in this report and its attachment(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauraJnenwyckergcom and delete the report without retairring any copies
Page 1 of6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 120511 1059
Kansas City KS 66101 SUBMITTED 111511
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Lincoln amp 39 Highway 1111501-01 Air 111411 0000 111511 1121 (111 W Lincoln)
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wfth the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001030
REPORTED 120511 1059
SUBMITTED 111511
AQS SITE CODE
SITE CODE OECAwork
DesaiptionUncoln amp 39 Highway (111 W Uncoln) Lab ID 1111501-01 Sampled 111411 0000
Pressure Receipt 8 Hg canister 636 Received 1115111121
Comments Analyzed 111611 0932
Air Toxics by EPA Compendium Method T0-15 blulb lmL
Analvte Jmbx Yllm fiG JlRbl Acetylene 0171 018 A-Ql 0016 Propylene 0272 OA7 A-Ql 0039 Dlchlorodlfluoromethane 0503 2A9 A-Ql 0011 Chloromethane OA74 098 A-Ql 0011 Dichlorobtraftuoroethane 0016 011 A-Ql 0009 Vinyl chloride ND ND A-Ql U 0008 13-Buladlene 0020 004 A-Ql 0007 Bromomethane 0011 004 AmiddotOl 0009 Chloroethane ND ND A-Ql U 0009 Acetonitrile 0138 023 A-Ql 0024 Trichloroftuoromethane D304 L71 A-Ql 0010 Acrylonitrile ND ND A-Q1 U 0012
11-Dichloroethene ND ND A-Q1 U 0009 Dichloromethane 0266 093 A-Ql 0010 Carbon Disulfide 0129 040 A-Ql 0033 Trichlorotrifluoroethane 0079 061 A-Ql 0011 trans-12-0ichloroethylene ND ND A-Ql U 0008 11-Dichloroethane ND ND A-Ql U 0008 Methyl tert-Butyl Ether ND NO A-Q1 U 0008 Methyl Ethyl Ketone 0760 us AmiddotOl 0157 Chloroprene ND NO A-Ql U 0008
cis-12-Dichloroethylene NO NO A-Ql U 0009 Bromochloromethane NO NO A-Ql U 0008 Chloroform NO NO A-Ql U 0009
Ethyl tert-Butyl Ether NO NO Amiddot01 U 0008 12-Dichloroethane 0026 011 A-Ql 0009 111-Trichloroethane 0006 003 A-Q1 U 0022 Benzene 113 362 A-Q1 0029 Carbon Tetrachloride 0069 OA4 A-Q1 0024 tert-Amyl Methyl Ether ND ND A-Ql U 0016 12-Dichloropropane ND NO A-Ql U 0023
Ethyl Acrylate NO NO A-Ql U 0020
Bromodlchloromethane ND NO A-o1 u 0025 Trichloroethylene NO ND A-01 U 0025
Methyl Methacrylate ND NO A-Q1 U 0022 cis-13-Dichloropropene NO NO A-Ql U 0022 Methyl Isobutyl Ketone 0047 019 A-Ql 0022 trans-13-Dichloropropene NO ND A-Q1 U 0025 112-Trichloroethane NO NO A-Q1 U 0025
Toluene 0661 250 A-01 0016 Dibromochloromethane NO ND A-Q1 U 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repoTt must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1210511 1059
Kansas City KS 66101 SUBMITTED 1115 11
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption Uncoln amp 39 Highway (111 W Lincoln) Lab ID 1111501-01 Sampled 111411 0000
Pressure Receipt 8 Hg canister 636 Received 1115111121
Comments Analyzed 111611 0932
Air Toxics by EPA Compendium Method T0-15 RuJID mL
AnaMe IU1bll ~ BiSl IU1bll 12-Dlbromoethane NO NO A-Ql U 0018
n-Oct3ne 0025 012 A-Ql 0015
Tetrachloroethylene 0016 011 A-Ql U 0018
Ollorobenzene NO NO A-Ql U 0021
Ethylbenzene 0068 030 A-Ql 0017
mp-Xylene 0144 063 A-Ql 0034
Bromoform NO NO A-Ql U 0025
Styrene 0058 025 A-Ql 0022
1122-Tetrachloroethane NO NO A-Ql U 0024
o-Xylene 0058 025 A-ol 0018
135-Trlmetflylbenzene 0050 025 A-01 0026
124-Trimetflylbenzene 0130 064 A-Ql 0028
m-Dichlorobenzene NO NO A-Ql U 0034
Chloromelhylbenzene NO NO A-ol U 0039
p-Oichlorobenzene 0027 016 A-Ql U 0035
o-Oichlorobenzene NO NO A-Ql U 0037
124-Trichlorobenzene NO NO A-ol U 0036
Hexachloro-13-butadiene NO NO A-ol U 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 120511 1059
Kansas City KS 66101 SUBMITTED 111511
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance witlz tlze chain of custody documellt This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1205111 1 059
Kansas City KS 66101 SUBMITTED 11151 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
A-ol Estimated value due to possible canister leak
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical re-port must be reproduced in its entirety
Page 6 of 6
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
December 15 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 1206111229
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for NMOC UATMP PAMS CSATAM and NATTS support (US EPA Contract No EPD-09-048) This rover page is an integral part of this report and any exceptions or oomments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Project Manager lauravanenwyckergcom
The information contained in this report and its attachment(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify laura vanenwyck ergcom and delete the report without retaining any copies
Page 1 of 6
RG CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111 1041
Kansas City KS 66101 SUBMITTED 1206 11
ATTN Michael F Davis AQS SITE CODE
PHONE 913) 551-5042 FAX 913) 551-5000 SITE CODE OECAwork
ANALYTlCAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Ash amp Forest SE Corner 1120611-01 Air 120411 0000 120611 1229
middotI I
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytirol repon must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
ALE 027800001030
REPORTED 1215111041
SUBMmED 1210611
AQS SITE CODE
SITE CODE OECAwork
Desaiptlon Ash amp Forest SE Comer Lab ID 1120611-01 sampled 120411 oooo Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 BuYltl MQL
AnaMe IUlllll lWm Bag IUlllll Acetylene OA36 OA7 0016 Propylene 0304 052 0039 Dichlorodiftuoromethane 0567 281 0011 Chloromethane 0566 117 0012 Dlchlorotetnlftuoroethane 0019 013 0009 Vinyl chloride NO NO u 0008 13-Butadiene NO NO u 0007 Bromomethane 0012 005 0009 Chloroethane NO NO u 0009 Acetonitrile 0111 019 0024 Trichlorofluoromethane 0284 160 0010 Aaylonitrile ND NO u 0012 11-Dichloroethene ND ND u 0009 Dichloromethane 0083 029 0010 Carbon Disulfide 0019 006 u 0033
Trlchlorotrlftuoroethane 0099 076 0011 trans-12-Dichloroethylene ND ND u 0008 11-Dichloroethane ND NO u 0008 Methyl tert-Butyl Ether NO NO u 0008 Methyl Ethyl Ketone 0536 158 0157 Chloroprene NO NO u 0008 cis-12-Dichloroethylene NO ND u 0009 Bromochloromethane NO NO u 0008 Chloroform 0022 011 0009 Ethyl tert-Butyl Ether NO NO u 0008 12-Dichloroethane 0025 010 0009 111-Trichloroethane 0011 006 u 0022 Benzene 0188 060 0029 carbon Tetrachloride 0106 067 0024 tert-Amyl Methyl Ether NO NO u 0016 12-Dichloropropane NO NO u 0023 Ethyl Acrylate ND NO u 0020
Bromodichloromethane NO NO u 0025 Trichloroethylene NO NO u 0025 Methyl Methacrylate NO NO u 0022 cis-13-Dichloropropene NO NO u 0022
Methyl Isobutyl Ketone 0042 017 0022 trans-13-Dichloropropene ND NO u 0025 112-Trichloroethane NO NO u 0025
Toluene 0149 056 0016 Oibromochloromethane 0003 003 u 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproducedin its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 121511 1041
Kansas City KS 66101 SUBMmED 1210611
ATTN Michael F Davis AQS SITE CODE
PHONE (913 551-5042 FAX (913 551-5000 SITE CODE OECAwork
Description Ash amp Forest SE Comer Lab ID 1120611-01 Sampled 120411 0000
Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 llWdtl MID
Analyte ubll IUllm Bag ubll 12-0ibromoethane NO NO u 0018 nmiddotOctane 0044 021 0015 Tetrachloroethylene 0006 004 u 0018
Chlorobenzene NO NO u 0021 Ethylbenzene 0047 021 0017 mp-Xylene 0070 031 0034 Bromoform NO NO u 0025 Styrene 0034 015 0022 1122-Tetrachloroethane NO NO u 0024 o-Xylene 0036 016 0018 135-Trlmethylbenzene 0025 012 u 0026 124-Trlmetllylbenzene 0047 023 0028 m-Oichlorobenzene NO NO u 0034
Chloromethylbenzene NO NO u 0039 p-Dichlorcbenzene 0005 003 u 0348 a-Dichlorobenzene NO NO u 0037
124-Trlchlorobenzene NO NO u 0036 Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repon must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS~RG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 66101 SUBMITTED 12061 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPDIAnalyte Result Units Result RPD um1t Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 661 01 SUBMITTED 120611
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its enJirety
Page 6 of 6
i
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
March 12 2012
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 030512 0916
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for UATMP NATTS CSATAM PAMS and NMOC support (US EPA Contract No 68-D-Q9-048) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Program Manager lauravanenwyckergcom
The information contained in this report and its attachmcnt(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauravanenwyckergcom and delete the report dthout retaining any copies
Page 1 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 0312112 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
6th St between Central amp 2030501-01 Air 030212 0000 030512 0916 Malcom
Eastern Research Group The results in this report apply only to the samples anal zed in accordance With the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Aven ue REPORTED 031212 1 051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 ~ tml
Analvte RRbll Y9lD1 flu RRbll Acetylene 0627 067 0072 Propylene 0484 084 0033
Dichlorodllluoromethane 0500 248 0023 Chloromethane 0557 115 0033
Dichlorotetrafluoroethane 0015 011 0012 Vinyl chloride NO NO u 0011
13-Butadlene 0036 oo8 0011
Bromomethane 0012 005 0012 Chloroethane NO NO u 0017
Acetonitrile 0073 012 0073
Trichlorofluoromethane 0258 145 0015 Acrylonitrile NO NO u 0020
11-0ichloroethene NO NO u 0014
Dichloromethane 0185 064 0023
Carbon Disulfide 0037 012 0014 Trichlorobitluoroethane 0119 091 0017
trans-12-0ichloroethylene NO NO u 0012
11-0ichloroethane NO NO u 0015
Methyl tert-Butyl Ether NO NO u 0011
Chloroprene NO NO u 0012
ds-12-0ich loroethylene NO NO u OD18
Bromochloromethane NO NO u 0014
Chloroform NO ND u 0014
Ethyl tert-Butyl Ether NO NO u 0011
12-Dichloroethane 0019 008 0016
111-Trichloroethane 0012 007 u 0020
Benzene 0344 L10 0061 Carbon Tetrachloride 0088 056 0024
tert-Amyl Methyl Ether NO NO u 0016
12-0ichloropropane ND NO u 0019
Ethyl Acrylate ND NO u 0014
Bromodichloromethane ND NO u 0021
Trichloroethylene NO ND u 0022
Methyl Methacrylate ND NO u 0025
ds-13-0ichloropropene NO NO u 0015
Methyl Isobutyl Ketone 0015 oo6 0015
trans-13-0ichloropropene NO ND u 0016
112-Trichloroethane NO NO u 0021
Toluene 0416 157 0045
Oibromochloromethane ND NO u 0018
12-0ibromoethane ND NO u 0017
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551 -5000
FILE 027800001030
REPORTED 0312 12 1051
SUBMITTED 030512
AQS SITE CODE
SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 Bwdtl MJlL
Analvte Jmbll Y9Lm Big Jmbx nmiddotOclane 0039 018 0020 Tetrachloroethylene 0005 003 u 0020
Chlorobenzene ND ND u 0025
Ethylbenzene 0045 020 0023 mp-Xylene 0112 OA9 0037 Bromoform ND ND u 0020
Styrene 0030 013 0024 1122-Tetrachloroethane ND ND u 0018
o-Xylene 0050 022 0020
135-Trimethylbenzene 0019 009 u 0022
124-Trimethylbenzene 0047 023 0025 m-Dichlorobenzene ND ND u 0024
p-Dichlorobenzene 0004 002 u 0019
a-Dichlorobenzene NO ND u 0021
124-Trichlorobenzene ND ND u 0022
Hexachloro-13-butadiene ND ND u 0022
Eastern Research Group The results in this report apply only 1o the samples analyzed in accordance with the chain of custody document This analytical rep ort must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 031212 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wilh the chain of custody document This analytical report must be reproduced in its enrirety
Page 5 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 03121121051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report nutst be reproduced in its entirety
Page 6 of 6
CERTIFrCATE OF ANALYSIS
EPA Region VII FILE tl 027800001030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMITTED 080811 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Description 73 north of Oak St on Plummer Lab ID 1092909-01 Sampled 0928110000
Pressure 0 Receipt 65 Hg canister 140 Received 0929111057
Comments Analyzed 093011 20 34
Analyte
Acetylene middotPropylene
Dldllorodifluoromethane Chlolomettlane
Dlchlorotetrafluoroethllne VInyl chloride 13-Butadlene Bromometl1dne
Chloroethane
Acetunitrile Trldllorotluoromethane
Acrylonitrile
11-0ithloroethene Dichloromethane Carbon DisulfJde
Trlchlorotrlfkloroetftane lranr1 2-0khloroethylene
11-Dithloroelhane
Methyl tert-Butyl Ether Methyl Ethyl Ketone Chloroprene ds-1HllchloiJethylene Bromochloromethane Chlorofvnn
Ethyl tert-Butyl Ether 12-Dichloroethane 111middotTriChloroethane
Benzene carbon Tetrachloride tert-Amyl Methyl Ether 12-Didlonopropane Ethyl Acrylate Bromodlchlorornelhane Trichloroethylene
Methyl MetllacrylaJ
ds-13-Dithloropropene Methyl Isobutyl KetDne trans-13-0khlorapropene 112-Trichloroethane
Toluene Olbromochloromethane
Air Toxics by EPA Compendium Method T0-15 Results mL
ORb YIiID Eiilg I1IZD 223 238 016 123 212 0039
0564 280 0~11
0525 109 0012 0018 013 ooot
NO NO u 0008 0181 040 0~07
NO NO u o009 NO NO u 0009
0157 028 0024 ozgo 163 0010
NO NO u 0(112 NO NO u 0009
0154 054 0010 0045 0 14 0033 0092 071 0011
NO NO u 0008 NO NO u 0008 NO NO u 0~08
0624 184 0157 NO NO u 0008 NO NO u 0009 NO NO u 0008
0035 017 0009 NO NO u 0008 NO NO u 0009
0012 007 u 0022 L49 477 0029
0088 o56 0024 NO NO u 0016 ND NO u 0023 NO NO u 0020 NO ND u 0025
0178 096 0025
NO NO u 0022 NO NO u 0022
0094 039 0022 NO NO u 0025 NO NO u 0025
276 10400 D 0040 r~O NO u 0021
Eastern Research Group The results m this repon apply only to the samples cmolylld in accordance wilh the chain of cUStOdy docWMnt This arwlytlcal rJort mu~middott be reproduced in its entirety
Page 13 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMITTED 0808111 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECA wa1lt
Description 75 north of Oak St on Plummer Lab ID 1092909-01 Sampled 092811 0000
Pressure Receipt 65 Hg canister 140 Received 0929111057
Comments Analyzed 0930112034
Air Toxics by EPA Compendium Method T0-15 Results lmb
Analyte mmx ugm3 flil on 12-Dibromoethane NO NO u 0018
n-Octane 0193 090 0015 Tetrachloroethylene 0019 013 0018
Chlorobenzene NO NO u 0021
Ethyl benzene 0356 155 p017 mp-Xylene 1oamp 461 OOl4
Bromoform NO NO u 6025
Sty~Wte 0060 026 0022 lll2-Tetrachloroethane NO NO u 0-024
o-Xylene P422 184 01118 135-TrlmethylbenEene 0094 046 0026 1124-Trlmethylbenzene 0340 167 0028
m-Dichlorobenzene 0043 016 0034 Chloromethylbenzene NO NO u 0039
p-Dichlorobenzene 0019 011 u 0035
rDichlorobenzellE NO NO u 0037 121-Trochlorobenzene NO NO u 0-036
Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The ll$Ults in rhis repon appl) NIhbull to the samples analyted in accordance with the cham of custody document Thta analybullical rrporl must he reproduced in in entirety
Page 14 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII FILE tl 027800001 030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS66101 SUBMmED 080811 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX~ (913) 551-5000 SITE CODE OECAwork
IAnalyte Result Units SOurce Result RPD
RPD Umit Note
Eastern Research Group ~ resulu in this reprJrt apply oraly to the samples analyed 111 accordance with the chain of crutody docunumt 1his anulmcal report must be reprodu~ed In its enrlnty
Page 15 of 16
CERTIFICATE OF ANALYSISRG EPA Region VII FILEmiddot 027800001 030
300 Minnesota Avenue REPORTED 1110 11 09middot03
Kansas City KS 66101 SUBMITTED 08101311 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX~ (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
u Under Detection Umlt
o Th1s result obtained by dilution
ND Analyte NOT DETECTED at or above the Method Detecbon Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group T1r results in thH report apply on() w the sample tmayzed il occordancltt with the cham of bullur1ody dotumnt This anayllcai report must be prwiuced in its entirety
Page 16 of 16
~RG Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
December 05 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 111511 1121
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the amtract for NMOC UATMP PAMS CSATAM and NATTS support (US EPA Contract No EPD-09-D48) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please oontact me at 919-468-7930
Sincerely
Laura Van Enwyck Project Manager lauravanenwyckergcom
The information contained in this report and its attachment(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauraJnenwyckergcom and delete the report without retairring any copies
Page 1 of6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 120511 1059
Kansas City KS 66101 SUBMITTED 111511
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Lincoln amp 39 Highway 1111501-01 Air 111411 0000 111511 1121 (111 W Lincoln)
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wfth the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001030
REPORTED 120511 1059
SUBMITTED 111511
AQS SITE CODE
SITE CODE OECAwork
DesaiptionUncoln amp 39 Highway (111 W Uncoln) Lab ID 1111501-01 Sampled 111411 0000
Pressure Receipt 8 Hg canister 636 Received 1115111121
Comments Analyzed 111611 0932
Air Toxics by EPA Compendium Method T0-15 blulb lmL
Analvte Jmbx Yllm fiG JlRbl Acetylene 0171 018 A-Ql 0016 Propylene 0272 OA7 A-Ql 0039 Dlchlorodlfluoromethane 0503 2A9 A-Ql 0011 Chloromethane OA74 098 A-Ql 0011 Dichlorobtraftuoroethane 0016 011 A-Ql 0009 Vinyl chloride ND ND A-Ql U 0008 13-Buladlene 0020 004 A-Ql 0007 Bromomethane 0011 004 AmiddotOl 0009 Chloroethane ND ND A-Ql U 0009 Acetonitrile 0138 023 A-Ql 0024 Trichloroftuoromethane D304 L71 A-Ql 0010 Acrylonitrile ND ND A-Q1 U 0012
11-Dichloroethene ND ND A-Q1 U 0009 Dichloromethane 0266 093 A-Ql 0010 Carbon Disulfide 0129 040 A-Ql 0033 Trichlorotrifluoroethane 0079 061 A-Ql 0011 trans-12-0ichloroethylene ND ND A-Ql U 0008 11-Dichloroethane ND ND A-Ql U 0008 Methyl tert-Butyl Ether ND NO A-Q1 U 0008 Methyl Ethyl Ketone 0760 us AmiddotOl 0157 Chloroprene ND NO A-Ql U 0008
cis-12-Dichloroethylene NO NO A-Ql U 0009 Bromochloromethane NO NO A-Ql U 0008 Chloroform NO NO A-Ql U 0009
Ethyl tert-Butyl Ether NO NO Amiddot01 U 0008 12-Dichloroethane 0026 011 A-Ql 0009 111-Trichloroethane 0006 003 A-Q1 U 0022 Benzene 113 362 A-Q1 0029 Carbon Tetrachloride 0069 OA4 A-Q1 0024 tert-Amyl Methyl Ether ND ND A-Ql U 0016 12-Dichloropropane ND NO A-Ql U 0023
Ethyl Acrylate NO NO A-Ql U 0020
Bromodlchloromethane ND NO A-o1 u 0025 Trichloroethylene NO ND A-01 U 0025
Methyl Methacrylate ND NO A-Q1 U 0022 cis-13-Dichloropropene NO NO A-Ql U 0022 Methyl Isobutyl Ketone 0047 019 A-Ql 0022 trans-13-Dichloropropene NO ND A-Q1 U 0025 112-Trichloroethane NO NO A-Q1 U 0025
Toluene 0661 250 A-01 0016 Dibromochloromethane NO ND A-Q1 U 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repoTt must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1210511 1059
Kansas City KS 66101 SUBMITTED 1115 11
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption Uncoln amp 39 Highway (111 W Lincoln) Lab ID 1111501-01 Sampled 111411 0000
Pressure Receipt 8 Hg canister 636 Received 1115111121
Comments Analyzed 111611 0932
Air Toxics by EPA Compendium Method T0-15 RuJID mL
AnaMe IU1bll ~ BiSl IU1bll 12-Dlbromoethane NO NO A-Ql U 0018
n-Oct3ne 0025 012 A-Ql 0015
Tetrachloroethylene 0016 011 A-Ql U 0018
Ollorobenzene NO NO A-Ql U 0021
Ethylbenzene 0068 030 A-Ql 0017
mp-Xylene 0144 063 A-Ql 0034
Bromoform NO NO A-Ql U 0025
Styrene 0058 025 A-Ql 0022
1122-Tetrachloroethane NO NO A-Ql U 0024
o-Xylene 0058 025 A-ol 0018
135-Trlmetflylbenzene 0050 025 A-01 0026
124-Trimetflylbenzene 0130 064 A-Ql 0028
m-Dichlorobenzene NO NO A-Ql U 0034
Chloromelhylbenzene NO NO A-ol U 0039
p-Oichlorobenzene 0027 016 A-Ql U 0035
o-Oichlorobenzene NO NO A-Ql U 0037
124-Trichlorobenzene NO NO A-ol U 0036
Hexachloro-13-butadiene NO NO A-ol U 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 120511 1059
Kansas City KS 66101 SUBMITTED 111511
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance witlz tlze chain of custody documellt This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1205111 1 059
Kansas City KS 66101 SUBMITTED 11151 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
A-ol Estimated value due to possible canister leak
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical re-port must be reproduced in its entirety
Page 6 of 6
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
December 15 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 1206111229
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for NMOC UATMP PAMS CSATAM and NATTS support (US EPA Contract No EPD-09-048) This rover page is an integral part of this report and any exceptions or oomments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Project Manager lauravanenwyckergcom
The information contained in this report and its attachment(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify laura vanenwyck ergcom and delete the report without retaining any copies
Page 1 of 6
RG CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111 1041
Kansas City KS 66101 SUBMITTED 1206 11
ATTN Michael F Davis AQS SITE CODE
PHONE 913) 551-5042 FAX 913) 551-5000 SITE CODE OECAwork
ANALYTlCAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Ash amp Forest SE Corner 1120611-01 Air 120411 0000 120611 1229
middotI I
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytirol repon must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
ALE 027800001030
REPORTED 1215111041
SUBMmED 1210611
AQS SITE CODE
SITE CODE OECAwork
Desaiptlon Ash amp Forest SE Comer Lab ID 1120611-01 sampled 120411 oooo Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 BuYltl MQL
AnaMe IUlllll lWm Bag IUlllll Acetylene OA36 OA7 0016 Propylene 0304 052 0039 Dichlorodiftuoromethane 0567 281 0011 Chloromethane 0566 117 0012 Dlchlorotetnlftuoroethane 0019 013 0009 Vinyl chloride NO NO u 0008 13-Butadiene NO NO u 0007 Bromomethane 0012 005 0009 Chloroethane NO NO u 0009 Acetonitrile 0111 019 0024 Trichlorofluoromethane 0284 160 0010 Aaylonitrile ND NO u 0012 11-Dichloroethene ND ND u 0009 Dichloromethane 0083 029 0010 Carbon Disulfide 0019 006 u 0033
Trlchlorotrlftuoroethane 0099 076 0011 trans-12-Dichloroethylene ND ND u 0008 11-Dichloroethane ND NO u 0008 Methyl tert-Butyl Ether NO NO u 0008 Methyl Ethyl Ketone 0536 158 0157 Chloroprene NO NO u 0008 cis-12-Dichloroethylene NO ND u 0009 Bromochloromethane NO NO u 0008 Chloroform 0022 011 0009 Ethyl tert-Butyl Ether NO NO u 0008 12-Dichloroethane 0025 010 0009 111-Trichloroethane 0011 006 u 0022 Benzene 0188 060 0029 carbon Tetrachloride 0106 067 0024 tert-Amyl Methyl Ether NO NO u 0016 12-Dichloropropane NO NO u 0023 Ethyl Acrylate ND NO u 0020
Bromodichloromethane NO NO u 0025 Trichloroethylene NO NO u 0025 Methyl Methacrylate NO NO u 0022 cis-13-Dichloropropene NO NO u 0022
Methyl Isobutyl Ketone 0042 017 0022 trans-13-Dichloropropene ND NO u 0025 112-Trichloroethane NO NO u 0025
Toluene 0149 056 0016 Oibromochloromethane 0003 003 u 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproducedin its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 121511 1041
Kansas City KS 66101 SUBMmED 1210611
ATTN Michael F Davis AQS SITE CODE
PHONE (913 551-5042 FAX (913 551-5000 SITE CODE OECAwork
Description Ash amp Forest SE Comer Lab ID 1120611-01 Sampled 120411 0000
Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 llWdtl MID
Analyte ubll IUllm Bag ubll 12-0ibromoethane NO NO u 0018 nmiddotOctane 0044 021 0015 Tetrachloroethylene 0006 004 u 0018
Chlorobenzene NO NO u 0021 Ethylbenzene 0047 021 0017 mp-Xylene 0070 031 0034 Bromoform NO NO u 0025 Styrene 0034 015 0022 1122-Tetrachloroethane NO NO u 0024 o-Xylene 0036 016 0018 135-Trlmethylbenzene 0025 012 u 0026 124-Trlmetllylbenzene 0047 023 0028 m-Oichlorobenzene NO NO u 0034
Chloromethylbenzene NO NO u 0039 p-Dichlorcbenzene 0005 003 u 0348 a-Dichlorobenzene NO NO u 0037
124-Trlchlorobenzene NO NO u 0036 Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repon must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS~RG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 66101 SUBMITTED 12061 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPDIAnalyte Result Units Result RPD um1t Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 661 01 SUBMITTED 120611
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its enJirety
Page 6 of 6
i
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
March 12 2012
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 030512 0916
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for UATMP NATTS CSATAM PAMS and NMOC support (US EPA Contract No 68-D-Q9-048) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Program Manager lauravanenwyckergcom
The information contained in this report and its attachmcnt(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauravanenwyckergcom and delete the report dthout retaining any copies
Page 1 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 0312112 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
6th St between Central amp 2030501-01 Air 030212 0000 030512 0916 Malcom
Eastern Research Group The results in this report apply only to the samples anal zed in accordance With the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Aven ue REPORTED 031212 1 051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 ~ tml
Analvte RRbll Y9lD1 flu RRbll Acetylene 0627 067 0072 Propylene 0484 084 0033
Dichlorodllluoromethane 0500 248 0023 Chloromethane 0557 115 0033
Dichlorotetrafluoroethane 0015 011 0012 Vinyl chloride NO NO u 0011
13-Butadlene 0036 oo8 0011
Bromomethane 0012 005 0012 Chloroethane NO NO u 0017
Acetonitrile 0073 012 0073
Trichlorofluoromethane 0258 145 0015 Acrylonitrile NO NO u 0020
11-0ichloroethene NO NO u 0014
Dichloromethane 0185 064 0023
Carbon Disulfide 0037 012 0014 Trichlorobitluoroethane 0119 091 0017
trans-12-0ichloroethylene NO NO u 0012
11-0ichloroethane NO NO u 0015
Methyl tert-Butyl Ether NO NO u 0011
Chloroprene NO NO u 0012
ds-12-0ich loroethylene NO NO u OD18
Bromochloromethane NO NO u 0014
Chloroform NO ND u 0014
Ethyl tert-Butyl Ether NO NO u 0011
12-Dichloroethane 0019 008 0016
111-Trichloroethane 0012 007 u 0020
Benzene 0344 L10 0061 Carbon Tetrachloride 0088 056 0024
tert-Amyl Methyl Ether NO NO u 0016
12-0ichloropropane ND NO u 0019
Ethyl Acrylate ND NO u 0014
Bromodichloromethane ND NO u 0021
Trichloroethylene NO ND u 0022
Methyl Methacrylate ND NO u 0025
ds-13-0ichloropropene NO NO u 0015
Methyl Isobutyl Ketone 0015 oo6 0015
trans-13-0ichloropropene NO ND u 0016
112-Trichloroethane NO NO u 0021
Toluene 0416 157 0045
Oibromochloromethane ND NO u 0018
12-0ibromoethane ND NO u 0017
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551 -5000
FILE 027800001030
REPORTED 0312 12 1051
SUBMITTED 030512
AQS SITE CODE
SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 Bwdtl MJlL
Analvte Jmbll Y9Lm Big Jmbx nmiddotOclane 0039 018 0020 Tetrachloroethylene 0005 003 u 0020
Chlorobenzene ND ND u 0025
Ethylbenzene 0045 020 0023 mp-Xylene 0112 OA9 0037 Bromoform ND ND u 0020
Styrene 0030 013 0024 1122-Tetrachloroethane ND ND u 0018
o-Xylene 0050 022 0020
135-Trimethylbenzene 0019 009 u 0022
124-Trimethylbenzene 0047 023 0025 m-Dichlorobenzene ND ND u 0024
p-Dichlorobenzene 0004 002 u 0019
a-Dichlorobenzene NO ND u 0021
124-Trichlorobenzene ND ND u 0022
Hexachloro-13-butadiene ND ND u 0022
Eastern Research Group The results in this report apply only 1o the samples analyzed in accordance with the chain of custody document This analytical rep ort must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 031212 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wilh the chain of custody document This analytical report must be reproduced in its enrirety
Page 5 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 03121121051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report nutst be reproduced in its entirety
Page 6 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS 66101 SUBMITTED 0808111 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECA wa1lt
Description 75 north of Oak St on Plummer Lab ID 1092909-01 Sampled 092811 0000
Pressure Receipt 65 Hg canister 140 Received 0929111057
Comments Analyzed 0930112034
Air Toxics by EPA Compendium Method T0-15 Results lmb
Analyte mmx ugm3 flil on 12-Dibromoethane NO NO u 0018
n-Octane 0193 090 0015 Tetrachloroethylene 0019 013 0018
Chlorobenzene NO NO u 0021
Ethyl benzene 0356 155 p017 mp-Xylene 1oamp 461 OOl4
Bromoform NO NO u 6025
Sty~Wte 0060 026 0022 lll2-Tetrachloroethane NO NO u 0-024
o-Xylene P422 184 01118 135-TrlmethylbenEene 0094 046 0026 1124-Trlmethylbenzene 0340 167 0028
m-Dichlorobenzene 0043 016 0034 Chloromethylbenzene NO NO u 0039
p-Dichlorobenzene 0019 011 u 0035
rDichlorobenzellE NO NO u 0037 121-Trochlorobenzene NO NO u 0-036
Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The ll$Ults in rhis repon appl) NIhbull to the samples analyted in accordance with the cham of custody document Thta analybullical rrporl must he reproduced in in entirety
Page 14 of 16
CERTIFICATE OF ANALYSIS
EPA Region VII FILE tl 027800001 030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS66101 SUBMmED 080811 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX~ (913) 551-5000 SITE CODE OECAwork
IAnalyte Result Units SOurce Result RPD
RPD Umit Note
Eastern Research Group ~ resulu in this reprJrt apply oraly to the samples analyed 111 accordance with the chain of crutody docunumt 1his anulmcal report must be reprodu~ed In its enrlnty
Page 15 of 16
CERTIFICATE OF ANALYSISRG EPA Region VII FILEmiddot 027800001 030
300 Minnesota Avenue REPORTED 1110 11 09middot03
Kansas City KS 66101 SUBMITTED 08101311 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX~ (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
u Under Detection Umlt
o Th1s result obtained by dilution
ND Analyte NOT DETECTED at or above the Method Detecbon Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group T1r results in thH report apply on() w the sample tmayzed il occordancltt with the cham of bullur1ody dotumnt This anayllcai report must be prwiuced in its entirety
Page 16 of 16
~RG Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
December 05 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 111511 1121
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the amtract for NMOC UATMP PAMS CSATAM and NATTS support (US EPA Contract No EPD-09-D48) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please oontact me at 919-468-7930
Sincerely
Laura Van Enwyck Project Manager lauravanenwyckergcom
The information contained in this report and its attachment(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauraJnenwyckergcom and delete the report without retairring any copies
Page 1 of6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 120511 1059
Kansas City KS 66101 SUBMITTED 111511
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Lincoln amp 39 Highway 1111501-01 Air 111411 0000 111511 1121 (111 W Lincoln)
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wfth the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001030
REPORTED 120511 1059
SUBMITTED 111511
AQS SITE CODE
SITE CODE OECAwork
DesaiptionUncoln amp 39 Highway (111 W Uncoln) Lab ID 1111501-01 Sampled 111411 0000
Pressure Receipt 8 Hg canister 636 Received 1115111121
Comments Analyzed 111611 0932
Air Toxics by EPA Compendium Method T0-15 blulb lmL
Analvte Jmbx Yllm fiG JlRbl Acetylene 0171 018 A-Ql 0016 Propylene 0272 OA7 A-Ql 0039 Dlchlorodlfluoromethane 0503 2A9 A-Ql 0011 Chloromethane OA74 098 A-Ql 0011 Dichlorobtraftuoroethane 0016 011 A-Ql 0009 Vinyl chloride ND ND A-Ql U 0008 13-Buladlene 0020 004 A-Ql 0007 Bromomethane 0011 004 AmiddotOl 0009 Chloroethane ND ND A-Ql U 0009 Acetonitrile 0138 023 A-Ql 0024 Trichloroftuoromethane D304 L71 A-Ql 0010 Acrylonitrile ND ND A-Q1 U 0012
11-Dichloroethene ND ND A-Q1 U 0009 Dichloromethane 0266 093 A-Ql 0010 Carbon Disulfide 0129 040 A-Ql 0033 Trichlorotrifluoroethane 0079 061 A-Ql 0011 trans-12-0ichloroethylene ND ND A-Ql U 0008 11-Dichloroethane ND ND A-Ql U 0008 Methyl tert-Butyl Ether ND NO A-Q1 U 0008 Methyl Ethyl Ketone 0760 us AmiddotOl 0157 Chloroprene ND NO A-Ql U 0008
cis-12-Dichloroethylene NO NO A-Ql U 0009 Bromochloromethane NO NO A-Ql U 0008 Chloroform NO NO A-Ql U 0009
Ethyl tert-Butyl Ether NO NO Amiddot01 U 0008 12-Dichloroethane 0026 011 A-Ql 0009 111-Trichloroethane 0006 003 A-Q1 U 0022 Benzene 113 362 A-Q1 0029 Carbon Tetrachloride 0069 OA4 A-Q1 0024 tert-Amyl Methyl Ether ND ND A-Ql U 0016 12-Dichloropropane ND NO A-Ql U 0023
Ethyl Acrylate NO NO A-Ql U 0020
Bromodlchloromethane ND NO A-o1 u 0025 Trichloroethylene NO ND A-01 U 0025
Methyl Methacrylate ND NO A-Q1 U 0022 cis-13-Dichloropropene NO NO A-Ql U 0022 Methyl Isobutyl Ketone 0047 019 A-Ql 0022 trans-13-Dichloropropene NO ND A-Q1 U 0025 112-Trichloroethane NO NO A-Q1 U 0025
Toluene 0661 250 A-01 0016 Dibromochloromethane NO ND A-Q1 U 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repoTt must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1210511 1059
Kansas City KS 66101 SUBMITTED 1115 11
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption Uncoln amp 39 Highway (111 W Lincoln) Lab ID 1111501-01 Sampled 111411 0000
Pressure Receipt 8 Hg canister 636 Received 1115111121
Comments Analyzed 111611 0932
Air Toxics by EPA Compendium Method T0-15 RuJID mL
AnaMe IU1bll ~ BiSl IU1bll 12-Dlbromoethane NO NO A-Ql U 0018
n-Oct3ne 0025 012 A-Ql 0015
Tetrachloroethylene 0016 011 A-Ql U 0018
Ollorobenzene NO NO A-Ql U 0021
Ethylbenzene 0068 030 A-Ql 0017
mp-Xylene 0144 063 A-Ql 0034
Bromoform NO NO A-Ql U 0025
Styrene 0058 025 A-Ql 0022
1122-Tetrachloroethane NO NO A-Ql U 0024
o-Xylene 0058 025 A-ol 0018
135-Trlmetflylbenzene 0050 025 A-01 0026
124-Trimetflylbenzene 0130 064 A-Ql 0028
m-Dichlorobenzene NO NO A-Ql U 0034
Chloromelhylbenzene NO NO A-ol U 0039
p-Oichlorobenzene 0027 016 A-Ql U 0035
o-Oichlorobenzene NO NO A-Ql U 0037
124-Trichlorobenzene NO NO A-ol U 0036
Hexachloro-13-butadiene NO NO A-ol U 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 120511 1059
Kansas City KS 66101 SUBMITTED 111511
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance witlz tlze chain of custody documellt This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1205111 1 059
Kansas City KS 66101 SUBMITTED 11151 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
A-ol Estimated value due to possible canister leak
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical re-port must be reproduced in its entirety
Page 6 of 6
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
December 15 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 1206111229
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for NMOC UATMP PAMS CSATAM and NATTS support (US EPA Contract No EPD-09-048) This rover page is an integral part of this report and any exceptions or oomments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Project Manager lauravanenwyckergcom
The information contained in this report and its attachment(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify laura vanenwyck ergcom and delete the report without retaining any copies
Page 1 of 6
RG CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111 1041
Kansas City KS 66101 SUBMITTED 1206 11
ATTN Michael F Davis AQS SITE CODE
PHONE 913) 551-5042 FAX 913) 551-5000 SITE CODE OECAwork
ANALYTlCAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Ash amp Forest SE Corner 1120611-01 Air 120411 0000 120611 1229
middotI I
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytirol repon must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
ALE 027800001030
REPORTED 1215111041
SUBMmED 1210611
AQS SITE CODE
SITE CODE OECAwork
Desaiptlon Ash amp Forest SE Comer Lab ID 1120611-01 sampled 120411 oooo Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 BuYltl MQL
AnaMe IUlllll lWm Bag IUlllll Acetylene OA36 OA7 0016 Propylene 0304 052 0039 Dichlorodiftuoromethane 0567 281 0011 Chloromethane 0566 117 0012 Dlchlorotetnlftuoroethane 0019 013 0009 Vinyl chloride NO NO u 0008 13-Butadiene NO NO u 0007 Bromomethane 0012 005 0009 Chloroethane NO NO u 0009 Acetonitrile 0111 019 0024 Trichlorofluoromethane 0284 160 0010 Aaylonitrile ND NO u 0012 11-Dichloroethene ND ND u 0009 Dichloromethane 0083 029 0010 Carbon Disulfide 0019 006 u 0033
Trlchlorotrlftuoroethane 0099 076 0011 trans-12-Dichloroethylene ND ND u 0008 11-Dichloroethane ND NO u 0008 Methyl tert-Butyl Ether NO NO u 0008 Methyl Ethyl Ketone 0536 158 0157 Chloroprene NO NO u 0008 cis-12-Dichloroethylene NO ND u 0009 Bromochloromethane NO NO u 0008 Chloroform 0022 011 0009 Ethyl tert-Butyl Ether NO NO u 0008 12-Dichloroethane 0025 010 0009 111-Trichloroethane 0011 006 u 0022 Benzene 0188 060 0029 carbon Tetrachloride 0106 067 0024 tert-Amyl Methyl Ether NO NO u 0016 12-Dichloropropane NO NO u 0023 Ethyl Acrylate ND NO u 0020
Bromodichloromethane NO NO u 0025 Trichloroethylene NO NO u 0025 Methyl Methacrylate NO NO u 0022 cis-13-Dichloropropene NO NO u 0022
Methyl Isobutyl Ketone 0042 017 0022 trans-13-Dichloropropene ND NO u 0025 112-Trichloroethane NO NO u 0025
Toluene 0149 056 0016 Oibromochloromethane 0003 003 u 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproducedin its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 121511 1041
Kansas City KS 66101 SUBMmED 1210611
ATTN Michael F Davis AQS SITE CODE
PHONE (913 551-5042 FAX (913 551-5000 SITE CODE OECAwork
Description Ash amp Forest SE Comer Lab ID 1120611-01 Sampled 120411 0000
Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 llWdtl MID
Analyte ubll IUllm Bag ubll 12-0ibromoethane NO NO u 0018 nmiddotOctane 0044 021 0015 Tetrachloroethylene 0006 004 u 0018
Chlorobenzene NO NO u 0021 Ethylbenzene 0047 021 0017 mp-Xylene 0070 031 0034 Bromoform NO NO u 0025 Styrene 0034 015 0022 1122-Tetrachloroethane NO NO u 0024 o-Xylene 0036 016 0018 135-Trlmethylbenzene 0025 012 u 0026 124-Trlmetllylbenzene 0047 023 0028 m-Oichlorobenzene NO NO u 0034
Chloromethylbenzene NO NO u 0039 p-Dichlorcbenzene 0005 003 u 0348 a-Dichlorobenzene NO NO u 0037
124-Trlchlorobenzene NO NO u 0036 Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repon must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS~RG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 66101 SUBMITTED 12061 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPDIAnalyte Result Units Result RPD um1t Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 661 01 SUBMITTED 120611
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its enJirety
Page 6 of 6
i
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
March 12 2012
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 030512 0916
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for UATMP NATTS CSATAM PAMS and NMOC support (US EPA Contract No 68-D-Q9-048) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Program Manager lauravanenwyckergcom
The information contained in this report and its attachmcnt(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauravanenwyckergcom and delete the report dthout retaining any copies
Page 1 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 0312112 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
6th St between Central amp 2030501-01 Air 030212 0000 030512 0916 Malcom
Eastern Research Group The results in this report apply only to the samples anal zed in accordance With the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Aven ue REPORTED 031212 1 051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 ~ tml
Analvte RRbll Y9lD1 flu RRbll Acetylene 0627 067 0072 Propylene 0484 084 0033
Dichlorodllluoromethane 0500 248 0023 Chloromethane 0557 115 0033
Dichlorotetrafluoroethane 0015 011 0012 Vinyl chloride NO NO u 0011
13-Butadlene 0036 oo8 0011
Bromomethane 0012 005 0012 Chloroethane NO NO u 0017
Acetonitrile 0073 012 0073
Trichlorofluoromethane 0258 145 0015 Acrylonitrile NO NO u 0020
11-0ichloroethene NO NO u 0014
Dichloromethane 0185 064 0023
Carbon Disulfide 0037 012 0014 Trichlorobitluoroethane 0119 091 0017
trans-12-0ichloroethylene NO NO u 0012
11-0ichloroethane NO NO u 0015
Methyl tert-Butyl Ether NO NO u 0011
Chloroprene NO NO u 0012
ds-12-0ich loroethylene NO NO u OD18
Bromochloromethane NO NO u 0014
Chloroform NO ND u 0014
Ethyl tert-Butyl Ether NO NO u 0011
12-Dichloroethane 0019 008 0016
111-Trichloroethane 0012 007 u 0020
Benzene 0344 L10 0061 Carbon Tetrachloride 0088 056 0024
tert-Amyl Methyl Ether NO NO u 0016
12-0ichloropropane ND NO u 0019
Ethyl Acrylate ND NO u 0014
Bromodichloromethane ND NO u 0021
Trichloroethylene NO ND u 0022
Methyl Methacrylate ND NO u 0025
ds-13-0ichloropropene NO NO u 0015
Methyl Isobutyl Ketone 0015 oo6 0015
trans-13-0ichloropropene NO ND u 0016
112-Trichloroethane NO NO u 0021
Toluene 0416 157 0045
Oibromochloromethane ND NO u 0018
12-0ibromoethane ND NO u 0017
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551 -5000
FILE 027800001030
REPORTED 0312 12 1051
SUBMITTED 030512
AQS SITE CODE
SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 Bwdtl MJlL
Analvte Jmbll Y9Lm Big Jmbx nmiddotOclane 0039 018 0020 Tetrachloroethylene 0005 003 u 0020
Chlorobenzene ND ND u 0025
Ethylbenzene 0045 020 0023 mp-Xylene 0112 OA9 0037 Bromoform ND ND u 0020
Styrene 0030 013 0024 1122-Tetrachloroethane ND ND u 0018
o-Xylene 0050 022 0020
135-Trimethylbenzene 0019 009 u 0022
124-Trimethylbenzene 0047 023 0025 m-Dichlorobenzene ND ND u 0024
p-Dichlorobenzene 0004 002 u 0019
a-Dichlorobenzene NO ND u 0021
124-Trichlorobenzene ND ND u 0022
Hexachloro-13-butadiene ND ND u 0022
Eastern Research Group The results in this report apply only 1o the samples analyzed in accordance with the chain of custody document This analytical rep ort must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 031212 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wilh the chain of custody document This analytical report must be reproduced in its enrirety
Page 5 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 03121121051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report nutst be reproduced in its entirety
Page 6 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE tl 027800001 030
300 Minnesota Avenue REPORTED 111011 0903
Kansas City KS66101 SUBMmED 080811 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX~ (913) 551-5000 SITE CODE OECAwork
IAnalyte Result Units SOurce Result RPD
RPD Umit Note
Eastern Research Group ~ resulu in this reprJrt apply oraly to the samples analyed 111 accordance with the chain of crutody docunumt 1his anulmcal report must be reprodu~ed In its enrlnty
Page 15 of 16
CERTIFICATE OF ANALYSISRG EPA Region VII FILEmiddot 027800001 030
300 Minnesota Avenue REPORTED 1110 11 09middot03
Kansas City KS 66101 SUBMITTED 08101311 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX~ (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
u Under Detection Umlt
o Th1s result obtained by dilution
ND Analyte NOT DETECTED at or above the Method Detecbon Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group T1r results in thH report apply on() w the sample tmayzed il occordancltt with the cham of bullur1ody dotumnt This anayllcai report must be prwiuced in its entirety
Page 16 of 16
~RG Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
December 05 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 111511 1121
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the amtract for NMOC UATMP PAMS CSATAM and NATTS support (US EPA Contract No EPD-09-D48) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please oontact me at 919-468-7930
Sincerely
Laura Van Enwyck Project Manager lauravanenwyckergcom
The information contained in this report and its attachment(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauraJnenwyckergcom and delete the report without retairring any copies
Page 1 of6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 120511 1059
Kansas City KS 66101 SUBMITTED 111511
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Lincoln amp 39 Highway 1111501-01 Air 111411 0000 111511 1121 (111 W Lincoln)
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wfth the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001030
REPORTED 120511 1059
SUBMITTED 111511
AQS SITE CODE
SITE CODE OECAwork
DesaiptionUncoln amp 39 Highway (111 W Uncoln) Lab ID 1111501-01 Sampled 111411 0000
Pressure Receipt 8 Hg canister 636 Received 1115111121
Comments Analyzed 111611 0932
Air Toxics by EPA Compendium Method T0-15 blulb lmL
Analvte Jmbx Yllm fiG JlRbl Acetylene 0171 018 A-Ql 0016 Propylene 0272 OA7 A-Ql 0039 Dlchlorodlfluoromethane 0503 2A9 A-Ql 0011 Chloromethane OA74 098 A-Ql 0011 Dichlorobtraftuoroethane 0016 011 A-Ql 0009 Vinyl chloride ND ND A-Ql U 0008 13-Buladlene 0020 004 A-Ql 0007 Bromomethane 0011 004 AmiddotOl 0009 Chloroethane ND ND A-Ql U 0009 Acetonitrile 0138 023 A-Ql 0024 Trichloroftuoromethane D304 L71 A-Ql 0010 Acrylonitrile ND ND A-Q1 U 0012
11-Dichloroethene ND ND A-Q1 U 0009 Dichloromethane 0266 093 A-Ql 0010 Carbon Disulfide 0129 040 A-Ql 0033 Trichlorotrifluoroethane 0079 061 A-Ql 0011 trans-12-0ichloroethylene ND ND A-Ql U 0008 11-Dichloroethane ND ND A-Ql U 0008 Methyl tert-Butyl Ether ND NO A-Q1 U 0008 Methyl Ethyl Ketone 0760 us AmiddotOl 0157 Chloroprene ND NO A-Ql U 0008
cis-12-Dichloroethylene NO NO A-Ql U 0009 Bromochloromethane NO NO A-Ql U 0008 Chloroform NO NO A-Ql U 0009
Ethyl tert-Butyl Ether NO NO Amiddot01 U 0008 12-Dichloroethane 0026 011 A-Ql 0009 111-Trichloroethane 0006 003 A-Q1 U 0022 Benzene 113 362 A-Q1 0029 Carbon Tetrachloride 0069 OA4 A-Q1 0024 tert-Amyl Methyl Ether ND ND A-Ql U 0016 12-Dichloropropane ND NO A-Ql U 0023
Ethyl Acrylate NO NO A-Ql U 0020
Bromodlchloromethane ND NO A-o1 u 0025 Trichloroethylene NO ND A-01 U 0025
Methyl Methacrylate ND NO A-Q1 U 0022 cis-13-Dichloropropene NO NO A-Ql U 0022 Methyl Isobutyl Ketone 0047 019 A-Ql 0022 trans-13-Dichloropropene NO ND A-Q1 U 0025 112-Trichloroethane NO NO A-Q1 U 0025
Toluene 0661 250 A-01 0016 Dibromochloromethane NO ND A-Q1 U 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repoTt must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1210511 1059
Kansas City KS 66101 SUBMITTED 1115 11
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption Uncoln amp 39 Highway (111 W Lincoln) Lab ID 1111501-01 Sampled 111411 0000
Pressure Receipt 8 Hg canister 636 Received 1115111121
Comments Analyzed 111611 0932
Air Toxics by EPA Compendium Method T0-15 RuJID mL
AnaMe IU1bll ~ BiSl IU1bll 12-Dlbromoethane NO NO A-Ql U 0018
n-Oct3ne 0025 012 A-Ql 0015
Tetrachloroethylene 0016 011 A-Ql U 0018
Ollorobenzene NO NO A-Ql U 0021
Ethylbenzene 0068 030 A-Ql 0017
mp-Xylene 0144 063 A-Ql 0034
Bromoform NO NO A-Ql U 0025
Styrene 0058 025 A-Ql 0022
1122-Tetrachloroethane NO NO A-Ql U 0024
o-Xylene 0058 025 A-ol 0018
135-Trlmetflylbenzene 0050 025 A-01 0026
124-Trimetflylbenzene 0130 064 A-Ql 0028
m-Dichlorobenzene NO NO A-Ql U 0034
Chloromelhylbenzene NO NO A-ol U 0039
p-Oichlorobenzene 0027 016 A-Ql U 0035
o-Oichlorobenzene NO NO A-Ql U 0037
124-Trichlorobenzene NO NO A-ol U 0036
Hexachloro-13-butadiene NO NO A-ol U 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 120511 1059
Kansas City KS 66101 SUBMITTED 111511
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance witlz tlze chain of custody documellt This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1205111 1 059
Kansas City KS 66101 SUBMITTED 11151 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
A-ol Estimated value due to possible canister leak
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical re-port must be reproduced in its entirety
Page 6 of 6
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
December 15 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 1206111229
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for NMOC UATMP PAMS CSATAM and NATTS support (US EPA Contract No EPD-09-048) This rover page is an integral part of this report and any exceptions or oomments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Project Manager lauravanenwyckergcom
The information contained in this report and its attachment(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify laura vanenwyck ergcom and delete the report without retaining any copies
Page 1 of 6
RG CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111 1041
Kansas City KS 66101 SUBMITTED 1206 11
ATTN Michael F Davis AQS SITE CODE
PHONE 913) 551-5042 FAX 913) 551-5000 SITE CODE OECAwork
ANALYTlCAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Ash amp Forest SE Corner 1120611-01 Air 120411 0000 120611 1229
middotI I
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytirol repon must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
ALE 027800001030
REPORTED 1215111041
SUBMmED 1210611
AQS SITE CODE
SITE CODE OECAwork
Desaiptlon Ash amp Forest SE Comer Lab ID 1120611-01 sampled 120411 oooo Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 BuYltl MQL
AnaMe IUlllll lWm Bag IUlllll Acetylene OA36 OA7 0016 Propylene 0304 052 0039 Dichlorodiftuoromethane 0567 281 0011 Chloromethane 0566 117 0012 Dlchlorotetnlftuoroethane 0019 013 0009 Vinyl chloride NO NO u 0008 13-Butadiene NO NO u 0007 Bromomethane 0012 005 0009 Chloroethane NO NO u 0009 Acetonitrile 0111 019 0024 Trichlorofluoromethane 0284 160 0010 Aaylonitrile ND NO u 0012 11-Dichloroethene ND ND u 0009 Dichloromethane 0083 029 0010 Carbon Disulfide 0019 006 u 0033
Trlchlorotrlftuoroethane 0099 076 0011 trans-12-Dichloroethylene ND ND u 0008 11-Dichloroethane ND NO u 0008 Methyl tert-Butyl Ether NO NO u 0008 Methyl Ethyl Ketone 0536 158 0157 Chloroprene NO NO u 0008 cis-12-Dichloroethylene NO ND u 0009 Bromochloromethane NO NO u 0008 Chloroform 0022 011 0009 Ethyl tert-Butyl Ether NO NO u 0008 12-Dichloroethane 0025 010 0009 111-Trichloroethane 0011 006 u 0022 Benzene 0188 060 0029 carbon Tetrachloride 0106 067 0024 tert-Amyl Methyl Ether NO NO u 0016 12-Dichloropropane NO NO u 0023 Ethyl Acrylate ND NO u 0020
Bromodichloromethane NO NO u 0025 Trichloroethylene NO NO u 0025 Methyl Methacrylate NO NO u 0022 cis-13-Dichloropropene NO NO u 0022
Methyl Isobutyl Ketone 0042 017 0022 trans-13-Dichloropropene ND NO u 0025 112-Trichloroethane NO NO u 0025
Toluene 0149 056 0016 Oibromochloromethane 0003 003 u 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproducedin its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 121511 1041
Kansas City KS 66101 SUBMmED 1210611
ATTN Michael F Davis AQS SITE CODE
PHONE (913 551-5042 FAX (913 551-5000 SITE CODE OECAwork
Description Ash amp Forest SE Comer Lab ID 1120611-01 Sampled 120411 0000
Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 llWdtl MID
Analyte ubll IUllm Bag ubll 12-0ibromoethane NO NO u 0018 nmiddotOctane 0044 021 0015 Tetrachloroethylene 0006 004 u 0018
Chlorobenzene NO NO u 0021 Ethylbenzene 0047 021 0017 mp-Xylene 0070 031 0034 Bromoform NO NO u 0025 Styrene 0034 015 0022 1122-Tetrachloroethane NO NO u 0024 o-Xylene 0036 016 0018 135-Trlmethylbenzene 0025 012 u 0026 124-Trlmetllylbenzene 0047 023 0028 m-Oichlorobenzene NO NO u 0034
Chloromethylbenzene NO NO u 0039 p-Dichlorcbenzene 0005 003 u 0348 a-Dichlorobenzene NO NO u 0037
124-Trlchlorobenzene NO NO u 0036 Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repon must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS~RG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 66101 SUBMITTED 12061 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPDIAnalyte Result Units Result RPD um1t Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 661 01 SUBMITTED 120611
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its enJirety
Page 6 of 6
i
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
March 12 2012
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 030512 0916
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for UATMP NATTS CSATAM PAMS and NMOC support (US EPA Contract No 68-D-Q9-048) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Program Manager lauravanenwyckergcom
The information contained in this report and its attachmcnt(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauravanenwyckergcom and delete the report dthout retaining any copies
Page 1 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 0312112 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
6th St between Central amp 2030501-01 Air 030212 0000 030512 0916 Malcom
Eastern Research Group The results in this report apply only to the samples anal zed in accordance With the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Aven ue REPORTED 031212 1 051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 ~ tml
Analvte RRbll Y9lD1 flu RRbll Acetylene 0627 067 0072 Propylene 0484 084 0033
Dichlorodllluoromethane 0500 248 0023 Chloromethane 0557 115 0033
Dichlorotetrafluoroethane 0015 011 0012 Vinyl chloride NO NO u 0011
13-Butadlene 0036 oo8 0011
Bromomethane 0012 005 0012 Chloroethane NO NO u 0017
Acetonitrile 0073 012 0073
Trichlorofluoromethane 0258 145 0015 Acrylonitrile NO NO u 0020
11-0ichloroethene NO NO u 0014
Dichloromethane 0185 064 0023
Carbon Disulfide 0037 012 0014 Trichlorobitluoroethane 0119 091 0017
trans-12-0ichloroethylene NO NO u 0012
11-0ichloroethane NO NO u 0015
Methyl tert-Butyl Ether NO NO u 0011
Chloroprene NO NO u 0012
ds-12-0ich loroethylene NO NO u OD18
Bromochloromethane NO NO u 0014
Chloroform NO ND u 0014
Ethyl tert-Butyl Ether NO NO u 0011
12-Dichloroethane 0019 008 0016
111-Trichloroethane 0012 007 u 0020
Benzene 0344 L10 0061 Carbon Tetrachloride 0088 056 0024
tert-Amyl Methyl Ether NO NO u 0016
12-0ichloropropane ND NO u 0019
Ethyl Acrylate ND NO u 0014
Bromodichloromethane ND NO u 0021
Trichloroethylene NO ND u 0022
Methyl Methacrylate ND NO u 0025
ds-13-0ichloropropene NO NO u 0015
Methyl Isobutyl Ketone 0015 oo6 0015
trans-13-0ichloropropene NO ND u 0016
112-Trichloroethane NO NO u 0021
Toluene 0416 157 0045
Oibromochloromethane ND NO u 0018
12-0ibromoethane ND NO u 0017
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551 -5000
FILE 027800001030
REPORTED 0312 12 1051
SUBMITTED 030512
AQS SITE CODE
SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 Bwdtl MJlL
Analvte Jmbll Y9Lm Big Jmbx nmiddotOclane 0039 018 0020 Tetrachloroethylene 0005 003 u 0020
Chlorobenzene ND ND u 0025
Ethylbenzene 0045 020 0023 mp-Xylene 0112 OA9 0037 Bromoform ND ND u 0020
Styrene 0030 013 0024 1122-Tetrachloroethane ND ND u 0018
o-Xylene 0050 022 0020
135-Trimethylbenzene 0019 009 u 0022
124-Trimethylbenzene 0047 023 0025 m-Dichlorobenzene ND ND u 0024
p-Dichlorobenzene 0004 002 u 0019
a-Dichlorobenzene NO ND u 0021
124-Trichlorobenzene ND ND u 0022
Hexachloro-13-butadiene ND ND u 0022
Eastern Research Group The results in this report apply only 1o the samples analyzed in accordance with the chain of custody document This analytical rep ort must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 031212 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wilh the chain of custody document This analytical report must be reproduced in its enrirety
Page 5 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 03121121051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report nutst be reproduced in its entirety
Page 6 of 6
CERTIFICATE OF ANALYSISRG EPA Region VII FILEmiddot 027800001 030
300 Minnesota Avenue REPORTED 1110 11 09middot03
Kansas City KS 66101 SUBMITTED 08101311 to 092911
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX~ (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
u Under Detection Umlt
o Th1s result obtained by dilution
ND Analyte NOT DETECTED at or above the Method Detecbon Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group T1r results in thH report apply on() w the sample tmayzed il occordancltt with the cham of bullur1ody dotumnt This anayllcai report must be prwiuced in its entirety
Page 16 of 16
~RG Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
December 05 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 111511 1121
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the amtract for NMOC UATMP PAMS CSATAM and NATTS support (US EPA Contract No EPD-09-D48) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please oontact me at 919-468-7930
Sincerely
Laura Van Enwyck Project Manager lauravanenwyckergcom
The information contained in this report and its attachment(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauraJnenwyckergcom and delete the report without retairring any copies
Page 1 of6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 120511 1059
Kansas City KS 66101 SUBMITTED 111511
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Lincoln amp 39 Highway 1111501-01 Air 111411 0000 111511 1121 (111 W Lincoln)
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wfth the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001030
REPORTED 120511 1059
SUBMITTED 111511
AQS SITE CODE
SITE CODE OECAwork
DesaiptionUncoln amp 39 Highway (111 W Uncoln) Lab ID 1111501-01 Sampled 111411 0000
Pressure Receipt 8 Hg canister 636 Received 1115111121
Comments Analyzed 111611 0932
Air Toxics by EPA Compendium Method T0-15 blulb lmL
Analvte Jmbx Yllm fiG JlRbl Acetylene 0171 018 A-Ql 0016 Propylene 0272 OA7 A-Ql 0039 Dlchlorodlfluoromethane 0503 2A9 A-Ql 0011 Chloromethane OA74 098 A-Ql 0011 Dichlorobtraftuoroethane 0016 011 A-Ql 0009 Vinyl chloride ND ND A-Ql U 0008 13-Buladlene 0020 004 A-Ql 0007 Bromomethane 0011 004 AmiddotOl 0009 Chloroethane ND ND A-Ql U 0009 Acetonitrile 0138 023 A-Ql 0024 Trichloroftuoromethane D304 L71 A-Ql 0010 Acrylonitrile ND ND A-Q1 U 0012
11-Dichloroethene ND ND A-Q1 U 0009 Dichloromethane 0266 093 A-Ql 0010 Carbon Disulfide 0129 040 A-Ql 0033 Trichlorotrifluoroethane 0079 061 A-Ql 0011 trans-12-0ichloroethylene ND ND A-Ql U 0008 11-Dichloroethane ND ND A-Ql U 0008 Methyl tert-Butyl Ether ND NO A-Q1 U 0008 Methyl Ethyl Ketone 0760 us AmiddotOl 0157 Chloroprene ND NO A-Ql U 0008
cis-12-Dichloroethylene NO NO A-Ql U 0009 Bromochloromethane NO NO A-Ql U 0008 Chloroform NO NO A-Ql U 0009
Ethyl tert-Butyl Ether NO NO Amiddot01 U 0008 12-Dichloroethane 0026 011 A-Ql 0009 111-Trichloroethane 0006 003 A-Q1 U 0022 Benzene 113 362 A-Q1 0029 Carbon Tetrachloride 0069 OA4 A-Q1 0024 tert-Amyl Methyl Ether ND ND A-Ql U 0016 12-Dichloropropane ND NO A-Ql U 0023
Ethyl Acrylate NO NO A-Ql U 0020
Bromodlchloromethane ND NO A-o1 u 0025 Trichloroethylene NO ND A-01 U 0025
Methyl Methacrylate ND NO A-Q1 U 0022 cis-13-Dichloropropene NO NO A-Ql U 0022 Methyl Isobutyl Ketone 0047 019 A-Ql 0022 trans-13-Dichloropropene NO ND A-Q1 U 0025 112-Trichloroethane NO NO A-Q1 U 0025
Toluene 0661 250 A-01 0016 Dibromochloromethane NO ND A-Q1 U 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repoTt must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1210511 1059
Kansas City KS 66101 SUBMITTED 1115 11
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption Uncoln amp 39 Highway (111 W Lincoln) Lab ID 1111501-01 Sampled 111411 0000
Pressure Receipt 8 Hg canister 636 Received 1115111121
Comments Analyzed 111611 0932
Air Toxics by EPA Compendium Method T0-15 RuJID mL
AnaMe IU1bll ~ BiSl IU1bll 12-Dlbromoethane NO NO A-Ql U 0018
n-Oct3ne 0025 012 A-Ql 0015
Tetrachloroethylene 0016 011 A-Ql U 0018
Ollorobenzene NO NO A-Ql U 0021
Ethylbenzene 0068 030 A-Ql 0017
mp-Xylene 0144 063 A-Ql 0034
Bromoform NO NO A-Ql U 0025
Styrene 0058 025 A-Ql 0022
1122-Tetrachloroethane NO NO A-Ql U 0024
o-Xylene 0058 025 A-ol 0018
135-Trlmetflylbenzene 0050 025 A-01 0026
124-Trimetflylbenzene 0130 064 A-Ql 0028
m-Dichlorobenzene NO NO A-Ql U 0034
Chloromelhylbenzene NO NO A-ol U 0039
p-Oichlorobenzene 0027 016 A-Ql U 0035
o-Oichlorobenzene NO NO A-Ql U 0037
124-Trichlorobenzene NO NO A-ol U 0036
Hexachloro-13-butadiene NO NO A-ol U 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 120511 1059
Kansas City KS 66101 SUBMITTED 111511
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance witlz tlze chain of custody documellt This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1205111 1 059
Kansas City KS 66101 SUBMITTED 11151 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
A-ol Estimated value due to possible canister leak
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical re-port must be reproduced in its entirety
Page 6 of 6
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
December 15 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 1206111229
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for NMOC UATMP PAMS CSATAM and NATTS support (US EPA Contract No EPD-09-048) This rover page is an integral part of this report and any exceptions or oomments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Project Manager lauravanenwyckergcom
The information contained in this report and its attachment(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify laura vanenwyck ergcom and delete the report without retaining any copies
Page 1 of 6
RG CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111 1041
Kansas City KS 66101 SUBMITTED 1206 11
ATTN Michael F Davis AQS SITE CODE
PHONE 913) 551-5042 FAX 913) 551-5000 SITE CODE OECAwork
ANALYTlCAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Ash amp Forest SE Corner 1120611-01 Air 120411 0000 120611 1229
middotI I
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytirol repon must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
ALE 027800001030
REPORTED 1215111041
SUBMmED 1210611
AQS SITE CODE
SITE CODE OECAwork
Desaiptlon Ash amp Forest SE Comer Lab ID 1120611-01 sampled 120411 oooo Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 BuYltl MQL
AnaMe IUlllll lWm Bag IUlllll Acetylene OA36 OA7 0016 Propylene 0304 052 0039 Dichlorodiftuoromethane 0567 281 0011 Chloromethane 0566 117 0012 Dlchlorotetnlftuoroethane 0019 013 0009 Vinyl chloride NO NO u 0008 13-Butadiene NO NO u 0007 Bromomethane 0012 005 0009 Chloroethane NO NO u 0009 Acetonitrile 0111 019 0024 Trichlorofluoromethane 0284 160 0010 Aaylonitrile ND NO u 0012 11-Dichloroethene ND ND u 0009 Dichloromethane 0083 029 0010 Carbon Disulfide 0019 006 u 0033
Trlchlorotrlftuoroethane 0099 076 0011 trans-12-Dichloroethylene ND ND u 0008 11-Dichloroethane ND NO u 0008 Methyl tert-Butyl Ether NO NO u 0008 Methyl Ethyl Ketone 0536 158 0157 Chloroprene NO NO u 0008 cis-12-Dichloroethylene NO ND u 0009 Bromochloromethane NO NO u 0008 Chloroform 0022 011 0009 Ethyl tert-Butyl Ether NO NO u 0008 12-Dichloroethane 0025 010 0009 111-Trichloroethane 0011 006 u 0022 Benzene 0188 060 0029 carbon Tetrachloride 0106 067 0024 tert-Amyl Methyl Ether NO NO u 0016 12-Dichloropropane NO NO u 0023 Ethyl Acrylate ND NO u 0020
Bromodichloromethane NO NO u 0025 Trichloroethylene NO NO u 0025 Methyl Methacrylate NO NO u 0022 cis-13-Dichloropropene NO NO u 0022
Methyl Isobutyl Ketone 0042 017 0022 trans-13-Dichloropropene ND NO u 0025 112-Trichloroethane NO NO u 0025
Toluene 0149 056 0016 Oibromochloromethane 0003 003 u 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproducedin its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 121511 1041
Kansas City KS 66101 SUBMmED 1210611
ATTN Michael F Davis AQS SITE CODE
PHONE (913 551-5042 FAX (913 551-5000 SITE CODE OECAwork
Description Ash amp Forest SE Comer Lab ID 1120611-01 Sampled 120411 0000
Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 llWdtl MID
Analyte ubll IUllm Bag ubll 12-0ibromoethane NO NO u 0018 nmiddotOctane 0044 021 0015 Tetrachloroethylene 0006 004 u 0018
Chlorobenzene NO NO u 0021 Ethylbenzene 0047 021 0017 mp-Xylene 0070 031 0034 Bromoform NO NO u 0025 Styrene 0034 015 0022 1122-Tetrachloroethane NO NO u 0024 o-Xylene 0036 016 0018 135-Trlmethylbenzene 0025 012 u 0026 124-Trlmetllylbenzene 0047 023 0028 m-Oichlorobenzene NO NO u 0034
Chloromethylbenzene NO NO u 0039 p-Dichlorcbenzene 0005 003 u 0348 a-Dichlorobenzene NO NO u 0037
124-Trlchlorobenzene NO NO u 0036 Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repon must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS~RG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 66101 SUBMITTED 12061 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPDIAnalyte Result Units Result RPD um1t Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 661 01 SUBMITTED 120611
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its enJirety
Page 6 of 6
i
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
March 12 2012
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 030512 0916
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for UATMP NATTS CSATAM PAMS and NMOC support (US EPA Contract No 68-D-Q9-048) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Program Manager lauravanenwyckergcom
The information contained in this report and its attachmcnt(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauravanenwyckergcom and delete the report dthout retaining any copies
Page 1 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 0312112 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
6th St between Central amp 2030501-01 Air 030212 0000 030512 0916 Malcom
Eastern Research Group The results in this report apply only to the samples anal zed in accordance With the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Aven ue REPORTED 031212 1 051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 ~ tml
Analvte RRbll Y9lD1 flu RRbll Acetylene 0627 067 0072 Propylene 0484 084 0033
Dichlorodllluoromethane 0500 248 0023 Chloromethane 0557 115 0033
Dichlorotetrafluoroethane 0015 011 0012 Vinyl chloride NO NO u 0011
13-Butadlene 0036 oo8 0011
Bromomethane 0012 005 0012 Chloroethane NO NO u 0017
Acetonitrile 0073 012 0073
Trichlorofluoromethane 0258 145 0015 Acrylonitrile NO NO u 0020
11-0ichloroethene NO NO u 0014
Dichloromethane 0185 064 0023
Carbon Disulfide 0037 012 0014 Trichlorobitluoroethane 0119 091 0017
trans-12-0ichloroethylene NO NO u 0012
11-0ichloroethane NO NO u 0015
Methyl tert-Butyl Ether NO NO u 0011
Chloroprene NO NO u 0012
ds-12-0ich loroethylene NO NO u OD18
Bromochloromethane NO NO u 0014
Chloroform NO ND u 0014
Ethyl tert-Butyl Ether NO NO u 0011
12-Dichloroethane 0019 008 0016
111-Trichloroethane 0012 007 u 0020
Benzene 0344 L10 0061 Carbon Tetrachloride 0088 056 0024
tert-Amyl Methyl Ether NO NO u 0016
12-0ichloropropane ND NO u 0019
Ethyl Acrylate ND NO u 0014
Bromodichloromethane ND NO u 0021
Trichloroethylene NO ND u 0022
Methyl Methacrylate ND NO u 0025
ds-13-0ichloropropene NO NO u 0015
Methyl Isobutyl Ketone 0015 oo6 0015
trans-13-0ichloropropene NO ND u 0016
112-Trichloroethane NO NO u 0021
Toluene 0416 157 0045
Oibromochloromethane ND NO u 0018
12-0ibromoethane ND NO u 0017
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551 -5000
FILE 027800001030
REPORTED 0312 12 1051
SUBMITTED 030512
AQS SITE CODE
SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 Bwdtl MJlL
Analvte Jmbll Y9Lm Big Jmbx nmiddotOclane 0039 018 0020 Tetrachloroethylene 0005 003 u 0020
Chlorobenzene ND ND u 0025
Ethylbenzene 0045 020 0023 mp-Xylene 0112 OA9 0037 Bromoform ND ND u 0020
Styrene 0030 013 0024 1122-Tetrachloroethane ND ND u 0018
o-Xylene 0050 022 0020
135-Trimethylbenzene 0019 009 u 0022
124-Trimethylbenzene 0047 023 0025 m-Dichlorobenzene ND ND u 0024
p-Dichlorobenzene 0004 002 u 0019
a-Dichlorobenzene NO ND u 0021
124-Trichlorobenzene ND ND u 0022
Hexachloro-13-butadiene ND ND u 0022
Eastern Research Group The results in this report apply only 1o the samples analyzed in accordance with the chain of custody document This analytical rep ort must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 031212 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wilh the chain of custody document This analytical report must be reproduced in its enrirety
Page 5 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 03121121051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report nutst be reproduced in its entirety
Page 6 of 6
~RG Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
December 05 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 111511 1121
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the amtract for NMOC UATMP PAMS CSATAM and NATTS support (US EPA Contract No EPD-09-D48) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please oontact me at 919-468-7930
Sincerely
Laura Van Enwyck Project Manager lauravanenwyckergcom
The information contained in this report and its attachment(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauraJnenwyckergcom and delete the report without retairring any copies
Page 1 of6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 120511 1059
Kansas City KS 66101 SUBMITTED 111511
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Lincoln amp 39 Highway 1111501-01 Air 111411 0000 111511 1121 (111 W Lincoln)
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wfth the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001030
REPORTED 120511 1059
SUBMITTED 111511
AQS SITE CODE
SITE CODE OECAwork
DesaiptionUncoln amp 39 Highway (111 W Uncoln) Lab ID 1111501-01 Sampled 111411 0000
Pressure Receipt 8 Hg canister 636 Received 1115111121
Comments Analyzed 111611 0932
Air Toxics by EPA Compendium Method T0-15 blulb lmL
Analvte Jmbx Yllm fiG JlRbl Acetylene 0171 018 A-Ql 0016 Propylene 0272 OA7 A-Ql 0039 Dlchlorodlfluoromethane 0503 2A9 A-Ql 0011 Chloromethane OA74 098 A-Ql 0011 Dichlorobtraftuoroethane 0016 011 A-Ql 0009 Vinyl chloride ND ND A-Ql U 0008 13-Buladlene 0020 004 A-Ql 0007 Bromomethane 0011 004 AmiddotOl 0009 Chloroethane ND ND A-Ql U 0009 Acetonitrile 0138 023 A-Ql 0024 Trichloroftuoromethane D304 L71 A-Ql 0010 Acrylonitrile ND ND A-Q1 U 0012
11-Dichloroethene ND ND A-Q1 U 0009 Dichloromethane 0266 093 A-Ql 0010 Carbon Disulfide 0129 040 A-Ql 0033 Trichlorotrifluoroethane 0079 061 A-Ql 0011 trans-12-0ichloroethylene ND ND A-Ql U 0008 11-Dichloroethane ND ND A-Ql U 0008 Methyl tert-Butyl Ether ND NO A-Q1 U 0008 Methyl Ethyl Ketone 0760 us AmiddotOl 0157 Chloroprene ND NO A-Ql U 0008
cis-12-Dichloroethylene NO NO A-Ql U 0009 Bromochloromethane NO NO A-Ql U 0008 Chloroform NO NO A-Ql U 0009
Ethyl tert-Butyl Ether NO NO Amiddot01 U 0008 12-Dichloroethane 0026 011 A-Ql 0009 111-Trichloroethane 0006 003 A-Q1 U 0022 Benzene 113 362 A-Q1 0029 Carbon Tetrachloride 0069 OA4 A-Q1 0024 tert-Amyl Methyl Ether ND ND A-Ql U 0016 12-Dichloropropane ND NO A-Ql U 0023
Ethyl Acrylate NO NO A-Ql U 0020
Bromodlchloromethane ND NO A-o1 u 0025 Trichloroethylene NO ND A-01 U 0025
Methyl Methacrylate ND NO A-Q1 U 0022 cis-13-Dichloropropene NO NO A-Ql U 0022 Methyl Isobutyl Ketone 0047 019 A-Ql 0022 trans-13-Dichloropropene NO ND A-Q1 U 0025 112-Trichloroethane NO NO A-Q1 U 0025
Toluene 0661 250 A-01 0016 Dibromochloromethane NO ND A-Q1 U 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repoTt must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1210511 1059
Kansas City KS 66101 SUBMITTED 1115 11
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption Uncoln amp 39 Highway (111 W Lincoln) Lab ID 1111501-01 Sampled 111411 0000
Pressure Receipt 8 Hg canister 636 Received 1115111121
Comments Analyzed 111611 0932
Air Toxics by EPA Compendium Method T0-15 RuJID mL
AnaMe IU1bll ~ BiSl IU1bll 12-Dlbromoethane NO NO A-Ql U 0018
n-Oct3ne 0025 012 A-Ql 0015
Tetrachloroethylene 0016 011 A-Ql U 0018
Ollorobenzene NO NO A-Ql U 0021
Ethylbenzene 0068 030 A-Ql 0017
mp-Xylene 0144 063 A-Ql 0034
Bromoform NO NO A-Ql U 0025
Styrene 0058 025 A-Ql 0022
1122-Tetrachloroethane NO NO A-Ql U 0024
o-Xylene 0058 025 A-ol 0018
135-Trlmetflylbenzene 0050 025 A-01 0026
124-Trimetflylbenzene 0130 064 A-Ql 0028
m-Dichlorobenzene NO NO A-Ql U 0034
Chloromelhylbenzene NO NO A-ol U 0039
p-Oichlorobenzene 0027 016 A-Ql U 0035
o-Oichlorobenzene NO NO A-Ql U 0037
124-Trichlorobenzene NO NO A-ol U 0036
Hexachloro-13-butadiene NO NO A-ol U 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 120511 1059
Kansas City KS 66101 SUBMITTED 111511
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance witlz tlze chain of custody documellt This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1205111 1 059
Kansas City KS 66101 SUBMITTED 11151 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
A-ol Estimated value due to possible canister leak
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical re-port must be reproduced in its entirety
Page 6 of 6
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
December 15 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 1206111229
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for NMOC UATMP PAMS CSATAM and NATTS support (US EPA Contract No EPD-09-048) This rover page is an integral part of this report and any exceptions or oomments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Project Manager lauravanenwyckergcom
The information contained in this report and its attachment(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify laura vanenwyck ergcom and delete the report without retaining any copies
Page 1 of 6
RG CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111 1041
Kansas City KS 66101 SUBMITTED 1206 11
ATTN Michael F Davis AQS SITE CODE
PHONE 913) 551-5042 FAX 913) 551-5000 SITE CODE OECAwork
ANALYTlCAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Ash amp Forest SE Corner 1120611-01 Air 120411 0000 120611 1229
middotI I
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytirol repon must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
ALE 027800001030
REPORTED 1215111041
SUBMmED 1210611
AQS SITE CODE
SITE CODE OECAwork
Desaiptlon Ash amp Forest SE Comer Lab ID 1120611-01 sampled 120411 oooo Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 BuYltl MQL
AnaMe IUlllll lWm Bag IUlllll Acetylene OA36 OA7 0016 Propylene 0304 052 0039 Dichlorodiftuoromethane 0567 281 0011 Chloromethane 0566 117 0012 Dlchlorotetnlftuoroethane 0019 013 0009 Vinyl chloride NO NO u 0008 13-Butadiene NO NO u 0007 Bromomethane 0012 005 0009 Chloroethane NO NO u 0009 Acetonitrile 0111 019 0024 Trichlorofluoromethane 0284 160 0010 Aaylonitrile ND NO u 0012 11-Dichloroethene ND ND u 0009 Dichloromethane 0083 029 0010 Carbon Disulfide 0019 006 u 0033
Trlchlorotrlftuoroethane 0099 076 0011 trans-12-Dichloroethylene ND ND u 0008 11-Dichloroethane ND NO u 0008 Methyl tert-Butyl Ether NO NO u 0008 Methyl Ethyl Ketone 0536 158 0157 Chloroprene NO NO u 0008 cis-12-Dichloroethylene NO ND u 0009 Bromochloromethane NO NO u 0008 Chloroform 0022 011 0009 Ethyl tert-Butyl Ether NO NO u 0008 12-Dichloroethane 0025 010 0009 111-Trichloroethane 0011 006 u 0022 Benzene 0188 060 0029 carbon Tetrachloride 0106 067 0024 tert-Amyl Methyl Ether NO NO u 0016 12-Dichloropropane NO NO u 0023 Ethyl Acrylate ND NO u 0020
Bromodichloromethane NO NO u 0025 Trichloroethylene NO NO u 0025 Methyl Methacrylate NO NO u 0022 cis-13-Dichloropropene NO NO u 0022
Methyl Isobutyl Ketone 0042 017 0022 trans-13-Dichloropropene ND NO u 0025 112-Trichloroethane NO NO u 0025
Toluene 0149 056 0016 Oibromochloromethane 0003 003 u 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproducedin its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 121511 1041
Kansas City KS 66101 SUBMmED 1210611
ATTN Michael F Davis AQS SITE CODE
PHONE (913 551-5042 FAX (913 551-5000 SITE CODE OECAwork
Description Ash amp Forest SE Comer Lab ID 1120611-01 Sampled 120411 0000
Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 llWdtl MID
Analyte ubll IUllm Bag ubll 12-0ibromoethane NO NO u 0018 nmiddotOctane 0044 021 0015 Tetrachloroethylene 0006 004 u 0018
Chlorobenzene NO NO u 0021 Ethylbenzene 0047 021 0017 mp-Xylene 0070 031 0034 Bromoform NO NO u 0025 Styrene 0034 015 0022 1122-Tetrachloroethane NO NO u 0024 o-Xylene 0036 016 0018 135-Trlmethylbenzene 0025 012 u 0026 124-Trlmetllylbenzene 0047 023 0028 m-Oichlorobenzene NO NO u 0034
Chloromethylbenzene NO NO u 0039 p-Dichlorcbenzene 0005 003 u 0348 a-Dichlorobenzene NO NO u 0037
124-Trlchlorobenzene NO NO u 0036 Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repon must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS~RG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 66101 SUBMITTED 12061 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPDIAnalyte Result Units Result RPD um1t Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 661 01 SUBMITTED 120611
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its enJirety
Page 6 of 6
i
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
March 12 2012
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 030512 0916
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for UATMP NATTS CSATAM PAMS and NMOC support (US EPA Contract No 68-D-Q9-048) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Program Manager lauravanenwyckergcom
The information contained in this report and its attachmcnt(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauravanenwyckergcom and delete the report dthout retaining any copies
Page 1 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 0312112 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
6th St between Central amp 2030501-01 Air 030212 0000 030512 0916 Malcom
Eastern Research Group The results in this report apply only to the samples anal zed in accordance With the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Aven ue REPORTED 031212 1 051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 ~ tml
Analvte RRbll Y9lD1 flu RRbll Acetylene 0627 067 0072 Propylene 0484 084 0033
Dichlorodllluoromethane 0500 248 0023 Chloromethane 0557 115 0033
Dichlorotetrafluoroethane 0015 011 0012 Vinyl chloride NO NO u 0011
13-Butadlene 0036 oo8 0011
Bromomethane 0012 005 0012 Chloroethane NO NO u 0017
Acetonitrile 0073 012 0073
Trichlorofluoromethane 0258 145 0015 Acrylonitrile NO NO u 0020
11-0ichloroethene NO NO u 0014
Dichloromethane 0185 064 0023
Carbon Disulfide 0037 012 0014 Trichlorobitluoroethane 0119 091 0017
trans-12-0ichloroethylene NO NO u 0012
11-0ichloroethane NO NO u 0015
Methyl tert-Butyl Ether NO NO u 0011
Chloroprene NO NO u 0012
ds-12-0ich loroethylene NO NO u OD18
Bromochloromethane NO NO u 0014
Chloroform NO ND u 0014
Ethyl tert-Butyl Ether NO NO u 0011
12-Dichloroethane 0019 008 0016
111-Trichloroethane 0012 007 u 0020
Benzene 0344 L10 0061 Carbon Tetrachloride 0088 056 0024
tert-Amyl Methyl Ether NO NO u 0016
12-0ichloropropane ND NO u 0019
Ethyl Acrylate ND NO u 0014
Bromodichloromethane ND NO u 0021
Trichloroethylene NO ND u 0022
Methyl Methacrylate ND NO u 0025
ds-13-0ichloropropene NO NO u 0015
Methyl Isobutyl Ketone 0015 oo6 0015
trans-13-0ichloropropene NO ND u 0016
112-Trichloroethane NO NO u 0021
Toluene 0416 157 0045
Oibromochloromethane ND NO u 0018
12-0ibromoethane ND NO u 0017
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551 -5000
FILE 027800001030
REPORTED 0312 12 1051
SUBMITTED 030512
AQS SITE CODE
SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 Bwdtl MJlL
Analvte Jmbll Y9Lm Big Jmbx nmiddotOclane 0039 018 0020 Tetrachloroethylene 0005 003 u 0020
Chlorobenzene ND ND u 0025
Ethylbenzene 0045 020 0023 mp-Xylene 0112 OA9 0037 Bromoform ND ND u 0020
Styrene 0030 013 0024 1122-Tetrachloroethane ND ND u 0018
o-Xylene 0050 022 0020
135-Trimethylbenzene 0019 009 u 0022
124-Trimethylbenzene 0047 023 0025 m-Dichlorobenzene ND ND u 0024
p-Dichlorobenzene 0004 002 u 0019
a-Dichlorobenzene NO ND u 0021
124-Trichlorobenzene ND ND u 0022
Hexachloro-13-butadiene ND ND u 0022
Eastern Research Group The results in this report apply only 1o the samples analyzed in accordance with the chain of custody document This analytical rep ort must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 031212 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wilh the chain of custody document This analytical report must be reproduced in its enrirety
Page 5 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 03121121051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report nutst be reproduced in its entirety
Page 6 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 120511 1059
Kansas City KS 66101 SUBMITTED 111511
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Lincoln amp 39 Highway 1111501-01 Air 111411 0000 111511 1121 (111 W Lincoln)
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wfth the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001030
REPORTED 120511 1059
SUBMITTED 111511
AQS SITE CODE
SITE CODE OECAwork
DesaiptionUncoln amp 39 Highway (111 W Uncoln) Lab ID 1111501-01 Sampled 111411 0000
Pressure Receipt 8 Hg canister 636 Received 1115111121
Comments Analyzed 111611 0932
Air Toxics by EPA Compendium Method T0-15 blulb lmL
Analvte Jmbx Yllm fiG JlRbl Acetylene 0171 018 A-Ql 0016 Propylene 0272 OA7 A-Ql 0039 Dlchlorodlfluoromethane 0503 2A9 A-Ql 0011 Chloromethane OA74 098 A-Ql 0011 Dichlorobtraftuoroethane 0016 011 A-Ql 0009 Vinyl chloride ND ND A-Ql U 0008 13-Buladlene 0020 004 A-Ql 0007 Bromomethane 0011 004 AmiddotOl 0009 Chloroethane ND ND A-Ql U 0009 Acetonitrile 0138 023 A-Ql 0024 Trichloroftuoromethane D304 L71 A-Ql 0010 Acrylonitrile ND ND A-Q1 U 0012
11-Dichloroethene ND ND A-Q1 U 0009 Dichloromethane 0266 093 A-Ql 0010 Carbon Disulfide 0129 040 A-Ql 0033 Trichlorotrifluoroethane 0079 061 A-Ql 0011 trans-12-0ichloroethylene ND ND A-Ql U 0008 11-Dichloroethane ND ND A-Ql U 0008 Methyl tert-Butyl Ether ND NO A-Q1 U 0008 Methyl Ethyl Ketone 0760 us AmiddotOl 0157 Chloroprene ND NO A-Ql U 0008
cis-12-Dichloroethylene NO NO A-Ql U 0009 Bromochloromethane NO NO A-Ql U 0008 Chloroform NO NO A-Ql U 0009
Ethyl tert-Butyl Ether NO NO Amiddot01 U 0008 12-Dichloroethane 0026 011 A-Ql 0009 111-Trichloroethane 0006 003 A-Q1 U 0022 Benzene 113 362 A-Q1 0029 Carbon Tetrachloride 0069 OA4 A-Q1 0024 tert-Amyl Methyl Ether ND ND A-Ql U 0016 12-Dichloropropane ND NO A-Ql U 0023
Ethyl Acrylate NO NO A-Ql U 0020
Bromodlchloromethane ND NO A-o1 u 0025 Trichloroethylene NO ND A-01 U 0025
Methyl Methacrylate ND NO A-Q1 U 0022 cis-13-Dichloropropene NO NO A-Ql U 0022 Methyl Isobutyl Ketone 0047 019 A-Ql 0022 trans-13-Dichloropropene NO ND A-Q1 U 0025 112-Trichloroethane NO NO A-Q1 U 0025
Toluene 0661 250 A-01 0016 Dibromochloromethane NO ND A-Q1 U 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repoTt must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1210511 1059
Kansas City KS 66101 SUBMITTED 1115 11
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption Uncoln amp 39 Highway (111 W Lincoln) Lab ID 1111501-01 Sampled 111411 0000
Pressure Receipt 8 Hg canister 636 Received 1115111121
Comments Analyzed 111611 0932
Air Toxics by EPA Compendium Method T0-15 RuJID mL
AnaMe IU1bll ~ BiSl IU1bll 12-Dlbromoethane NO NO A-Ql U 0018
n-Oct3ne 0025 012 A-Ql 0015
Tetrachloroethylene 0016 011 A-Ql U 0018
Ollorobenzene NO NO A-Ql U 0021
Ethylbenzene 0068 030 A-Ql 0017
mp-Xylene 0144 063 A-Ql 0034
Bromoform NO NO A-Ql U 0025
Styrene 0058 025 A-Ql 0022
1122-Tetrachloroethane NO NO A-Ql U 0024
o-Xylene 0058 025 A-ol 0018
135-Trlmetflylbenzene 0050 025 A-01 0026
124-Trimetflylbenzene 0130 064 A-Ql 0028
m-Dichlorobenzene NO NO A-Ql U 0034
Chloromelhylbenzene NO NO A-ol U 0039
p-Oichlorobenzene 0027 016 A-Ql U 0035
o-Oichlorobenzene NO NO A-Ql U 0037
124-Trichlorobenzene NO NO A-ol U 0036
Hexachloro-13-butadiene NO NO A-ol U 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 120511 1059
Kansas City KS 66101 SUBMITTED 111511
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance witlz tlze chain of custody documellt This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1205111 1 059
Kansas City KS 66101 SUBMITTED 11151 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
A-ol Estimated value due to possible canister leak
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical re-port must be reproduced in its entirety
Page 6 of 6
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
December 15 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 1206111229
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for NMOC UATMP PAMS CSATAM and NATTS support (US EPA Contract No EPD-09-048) This rover page is an integral part of this report and any exceptions or oomments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Project Manager lauravanenwyckergcom
The information contained in this report and its attachment(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify laura vanenwyck ergcom and delete the report without retaining any copies
Page 1 of 6
RG CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111 1041
Kansas City KS 66101 SUBMITTED 1206 11
ATTN Michael F Davis AQS SITE CODE
PHONE 913) 551-5042 FAX 913) 551-5000 SITE CODE OECAwork
ANALYTlCAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Ash amp Forest SE Corner 1120611-01 Air 120411 0000 120611 1229
middotI I
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytirol repon must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
ALE 027800001030
REPORTED 1215111041
SUBMmED 1210611
AQS SITE CODE
SITE CODE OECAwork
Desaiptlon Ash amp Forest SE Comer Lab ID 1120611-01 sampled 120411 oooo Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 BuYltl MQL
AnaMe IUlllll lWm Bag IUlllll Acetylene OA36 OA7 0016 Propylene 0304 052 0039 Dichlorodiftuoromethane 0567 281 0011 Chloromethane 0566 117 0012 Dlchlorotetnlftuoroethane 0019 013 0009 Vinyl chloride NO NO u 0008 13-Butadiene NO NO u 0007 Bromomethane 0012 005 0009 Chloroethane NO NO u 0009 Acetonitrile 0111 019 0024 Trichlorofluoromethane 0284 160 0010 Aaylonitrile ND NO u 0012 11-Dichloroethene ND ND u 0009 Dichloromethane 0083 029 0010 Carbon Disulfide 0019 006 u 0033
Trlchlorotrlftuoroethane 0099 076 0011 trans-12-Dichloroethylene ND ND u 0008 11-Dichloroethane ND NO u 0008 Methyl tert-Butyl Ether NO NO u 0008 Methyl Ethyl Ketone 0536 158 0157 Chloroprene NO NO u 0008 cis-12-Dichloroethylene NO ND u 0009 Bromochloromethane NO NO u 0008 Chloroform 0022 011 0009 Ethyl tert-Butyl Ether NO NO u 0008 12-Dichloroethane 0025 010 0009 111-Trichloroethane 0011 006 u 0022 Benzene 0188 060 0029 carbon Tetrachloride 0106 067 0024 tert-Amyl Methyl Ether NO NO u 0016 12-Dichloropropane NO NO u 0023 Ethyl Acrylate ND NO u 0020
Bromodichloromethane NO NO u 0025 Trichloroethylene NO NO u 0025 Methyl Methacrylate NO NO u 0022 cis-13-Dichloropropene NO NO u 0022
Methyl Isobutyl Ketone 0042 017 0022 trans-13-Dichloropropene ND NO u 0025 112-Trichloroethane NO NO u 0025
Toluene 0149 056 0016 Oibromochloromethane 0003 003 u 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproducedin its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 121511 1041
Kansas City KS 66101 SUBMmED 1210611
ATTN Michael F Davis AQS SITE CODE
PHONE (913 551-5042 FAX (913 551-5000 SITE CODE OECAwork
Description Ash amp Forest SE Comer Lab ID 1120611-01 Sampled 120411 0000
Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 llWdtl MID
Analyte ubll IUllm Bag ubll 12-0ibromoethane NO NO u 0018 nmiddotOctane 0044 021 0015 Tetrachloroethylene 0006 004 u 0018
Chlorobenzene NO NO u 0021 Ethylbenzene 0047 021 0017 mp-Xylene 0070 031 0034 Bromoform NO NO u 0025 Styrene 0034 015 0022 1122-Tetrachloroethane NO NO u 0024 o-Xylene 0036 016 0018 135-Trlmethylbenzene 0025 012 u 0026 124-Trlmetllylbenzene 0047 023 0028 m-Oichlorobenzene NO NO u 0034
Chloromethylbenzene NO NO u 0039 p-Dichlorcbenzene 0005 003 u 0348 a-Dichlorobenzene NO NO u 0037
124-Trlchlorobenzene NO NO u 0036 Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repon must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS~RG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 66101 SUBMITTED 12061 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPDIAnalyte Result Units Result RPD um1t Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 661 01 SUBMITTED 120611
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its enJirety
Page 6 of 6
i
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
March 12 2012
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 030512 0916
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for UATMP NATTS CSATAM PAMS and NMOC support (US EPA Contract No 68-D-Q9-048) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Program Manager lauravanenwyckergcom
The information contained in this report and its attachmcnt(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauravanenwyckergcom and delete the report dthout retaining any copies
Page 1 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 0312112 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
6th St between Central amp 2030501-01 Air 030212 0000 030512 0916 Malcom
Eastern Research Group The results in this report apply only to the samples anal zed in accordance With the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Aven ue REPORTED 031212 1 051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 ~ tml
Analvte RRbll Y9lD1 flu RRbll Acetylene 0627 067 0072 Propylene 0484 084 0033
Dichlorodllluoromethane 0500 248 0023 Chloromethane 0557 115 0033
Dichlorotetrafluoroethane 0015 011 0012 Vinyl chloride NO NO u 0011
13-Butadlene 0036 oo8 0011
Bromomethane 0012 005 0012 Chloroethane NO NO u 0017
Acetonitrile 0073 012 0073
Trichlorofluoromethane 0258 145 0015 Acrylonitrile NO NO u 0020
11-0ichloroethene NO NO u 0014
Dichloromethane 0185 064 0023
Carbon Disulfide 0037 012 0014 Trichlorobitluoroethane 0119 091 0017
trans-12-0ichloroethylene NO NO u 0012
11-0ichloroethane NO NO u 0015
Methyl tert-Butyl Ether NO NO u 0011
Chloroprene NO NO u 0012
ds-12-0ich loroethylene NO NO u OD18
Bromochloromethane NO NO u 0014
Chloroform NO ND u 0014
Ethyl tert-Butyl Ether NO NO u 0011
12-Dichloroethane 0019 008 0016
111-Trichloroethane 0012 007 u 0020
Benzene 0344 L10 0061 Carbon Tetrachloride 0088 056 0024
tert-Amyl Methyl Ether NO NO u 0016
12-0ichloropropane ND NO u 0019
Ethyl Acrylate ND NO u 0014
Bromodichloromethane ND NO u 0021
Trichloroethylene NO ND u 0022
Methyl Methacrylate ND NO u 0025
ds-13-0ichloropropene NO NO u 0015
Methyl Isobutyl Ketone 0015 oo6 0015
trans-13-0ichloropropene NO ND u 0016
112-Trichloroethane NO NO u 0021
Toluene 0416 157 0045
Oibromochloromethane ND NO u 0018
12-0ibromoethane ND NO u 0017
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551 -5000
FILE 027800001030
REPORTED 0312 12 1051
SUBMITTED 030512
AQS SITE CODE
SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 Bwdtl MJlL
Analvte Jmbll Y9Lm Big Jmbx nmiddotOclane 0039 018 0020 Tetrachloroethylene 0005 003 u 0020
Chlorobenzene ND ND u 0025
Ethylbenzene 0045 020 0023 mp-Xylene 0112 OA9 0037 Bromoform ND ND u 0020
Styrene 0030 013 0024 1122-Tetrachloroethane ND ND u 0018
o-Xylene 0050 022 0020
135-Trimethylbenzene 0019 009 u 0022
124-Trimethylbenzene 0047 023 0025 m-Dichlorobenzene ND ND u 0024
p-Dichlorobenzene 0004 002 u 0019
a-Dichlorobenzene NO ND u 0021
124-Trichlorobenzene ND ND u 0022
Hexachloro-13-butadiene ND ND u 0022
Eastern Research Group The results in this report apply only 1o the samples analyzed in accordance with the chain of custody document This analytical rep ort must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 031212 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wilh the chain of custody document This analytical report must be reproduced in its enrirety
Page 5 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 03121121051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report nutst be reproduced in its entirety
Page 6 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
FILE 027800001030
REPORTED 120511 1059
SUBMITTED 111511
AQS SITE CODE
SITE CODE OECAwork
DesaiptionUncoln amp 39 Highway (111 W Uncoln) Lab ID 1111501-01 Sampled 111411 0000
Pressure Receipt 8 Hg canister 636 Received 1115111121
Comments Analyzed 111611 0932
Air Toxics by EPA Compendium Method T0-15 blulb lmL
Analvte Jmbx Yllm fiG JlRbl Acetylene 0171 018 A-Ql 0016 Propylene 0272 OA7 A-Ql 0039 Dlchlorodlfluoromethane 0503 2A9 A-Ql 0011 Chloromethane OA74 098 A-Ql 0011 Dichlorobtraftuoroethane 0016 011 A-Ql 0009 Vinyl chloride ND ND A-Ql U 0008 13-Buladlene 0020 004 A-Ql 0007 Bromomethane 0011 004 AmiddotOl 0009 Chloroethane ND ND A-Ql U 0009 Acetonitrile 0138 023 A-Ql 0024 Trichloroftuoromethane D304 L71 A-Ql 0010 Acrylonitrile ND ND A-Q1 U 0012
11-Dichloroethene ND ND A-Q1 U 0009 Dichloromethane 0266 093 A-Ql 0010 Carbon Disulfide 0129 040 A-Ql 0033 Trichlorotrifluoroethane 0079 061 A-Ql 0011 trans-12-0ichloroethylene ND ND A-Ql U 0008 11-Dichloroethane ND ND A-Ql U 0008 Methyl tert-Butyl Ether ND NO A-Q1 U 0008 Methyl Ethyl Ketone 0760 us AmiddotOl 0157 Chloroprene ND NO A-Ql U 0008
cis-12-Dichloroethylene NO NO A-Ql U 0009 Bromochloromethane NO NO A-Ql U 0008 Chloroform NO NO A-Ql U 0009
Ethyl tert-Butyl Ether NO NO Amiddot01 U 0008 12-Dichloroethane 0026 011 A-Ql 0009 111-Trichloroethane 0006 003 A-Q1 U 0022 Benzene 113 362 A-Q1 0029 Carbon Tetrachloride 0069 OA4 A-Q1 0024 tert-Amyl Methyl Ether ND ND A-Ql U 0016 12-Dichloropropane ND NO A-Ql U 0023
Ethyl Acrylate NO NO A-Ql U 0020
Bromodlchloromethane ND NO A-o1 u 0025 Trichloroethylene NO ND A-01 U 0025
Methyl Methacrylate ND NO A-Q1 U 0022 cis-13-Dichloropropene NO NO A-Ql U 0022 Methyl Isobutyl Ketone 0047 019 A-Ql 0022 trans-13-Dichloropropene NO ND A-Q1 U 0025 112-Trichloroethane NO NO A-Q1 U 0025
Toluene 0661 250 A-01 0016 Dibromochloromethane NO ND A-Q1 U 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repoTt must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1210511 1059
Kansas City KS 66101 SUBMITTED 1115 11
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption Uncoln amp 39 Highway (111 W Lincoln) Lab ID 1111501-01 Sampled 111411 0000
Pressure Receipt 8 Hg canister 636 Received 1115111121
Comments Analyzed 111611 0932
Air Toxics by EPA Compendium Method T0-15 RuJID mL
AnaMe IU1bll ~ BiSl IU1bll 12-Dlbromoethane NO NO A-Ql U 0018
n-Oct3ne 0025 012 A-Ql 0015
Tetrachloroethylene 0016 011 A-Ql U 0018
Ollorobenzene NO NO A-Ql U 0021
Ethylbenzene 0068 030 A-Ql 0017
mp-Xylene 0144 063 A-Ql 0034
Bromoform NO NO A-Ql U 0025
Styrene 0058 025 A-Ql 0022
1122-Tetrachloroethane NO NO A-Ql U 0024
o-Xylene 0058 025 A-ol 0018
135-Trlmetflylbenzene 0050 025 A-01 0026
124-Trimetflylbenzene 0130 064 A-Ql 0028
m-Dichlorobenzene NO NO A-Ql U 0034
Chloromelhylbenzene NO NO A-ol U 0039
p-Oichlorobenzene 0027 016 A-Ql U 0035
o-Oichlorobenzene NO NO A-Ql U 0037
124-Trichlorobenzene NO NO A-ol U 0036
Hexachloro-13-butadiene NO NO A-ol U 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 120511 1059
Kansas City KS 66101 SUBMITTED 111511
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance witlz tlze chain of custody documellt This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1205111 1 059
Kansas City KS 66101 SUBMITTED 11151 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
A-ol Estimated value due to possible canister leak
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical re-port must be reproduced in its entirety
Page 6 of 6
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
December 15 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 1206111229
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for NMOC UATMP PAMS CSATAM and NATTS support (US EPA Contract No EPD-09-048) This rover page is an integral part of this report and any exceptions or oomments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Project Manager lauravanenwyckergcom
The information contained in this report and its attachment(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify laura vanenwyck ergcom and delete the report without retaining any copies
Page 1 of 6
RG CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111 1041
Kansas City KS 66101 SUBMITTED 1206 11
ATTN Michael F Davis AQS SITE CODE
PHONE 913) 551-5042 FAX 913) 551-5000 SITE CODE OECAwork
ANALYTlCAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Ash amp Forest SE Corner 1120611-01 Air 120411 0000 120611 1229
middotI I
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytirol repon must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
ALE 027800001030
REPORTED 1215111041
SUBMmED 1210611
AQS SITE CODE
SITE CODE OECAwork
Desaiptlon Ash amp Forest SE Comer Lab ID 1120611-01 sampled 120411 oooo Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 BuYltl MQL
AnaMe IUlllll lWm Bag IUlllll Acetylene OA36 OA7 0016 Propylene 0304 052 0039 Dichlorodiftuoromethane 0567 281 0011 Chloromethane 0566 117 0012 Dlchlorotetnlftuoroethane 0019 013 0009 Vinyl chloride NO NO u 0008 13-Butadiene NO NO u 0007 Bromomethane 0012 005 0009 Chloroethane NO NO u 0009 Acetonitrile 0111 019 0024 Trichlorofluoromethane 0284 160 0010 Aaylonitrile ND NO u 0012 11-Dichloroethene ND ND u 0009 Dichloromethane 0083 029 0010 Carbon Disulfide 0019 006 u 0033
Trlchlorotrlftuoroethane 0099 076 0011 trans-12-Dichloroethylene ND ND u 0008 11-Dichloroethane ND NO u 0008 Methyl tert-Butyl Ether NO NO u 0008 Methyl Ethyl Ketone 0536 158 0157 Chloroprene NO NO u 0008 cis-12-Dichloroethylene NO ND u 0009 Bromochloromethane NO NO u 0008 Chloroform 0022 011 0009 Ethyl tert-Butyl Ether NO NO u 0008 12-Dichloroethane 0025 010 0009 111-Trichloroethane 0011 006 u 0022 Benzene 0188 060 0029 carbon Tetrachloride 0106 067 0024 tert-Amyl Methyl Ether NO NO u 0016 12-Dichloropropane NO NO u 0023 Ethyl Acrylate ND NO u 0020
Bromodichloromethane NO NO u 0025 Trichloroethylene NO NO u 0025 Methyl Methacrylate NO NO u 0022 cis-13-Dichloropropene NO NO u 0022
Methyl Isobutyl Ketone 0042 017 0022 trans-13-Dichloropropene ND NO u 0025 112-Trichloroethane NO NO u 0025
Toluene 0149 056 0016 Oibromochloromethane 0003 003 u 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproducedin its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 121511 1041
Kansas City KS 66101 SUBMmED 1210611
ATTN Michael F Davis AQS SITE CODE
PHONE (913 551-5042 FAX (913 551-5000 SITE CODE OECAwork
Description Ash amp Forest SE Comer Lab ID 1120611-01 Sampled 120411 0000
Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 llWdtl MID
Analyte ubll IUllm Bag ubll 12-0ibromoethane NO NO u 0018 nmiddotOctane 0044 021 0015 Tetrachloroethylene 0006 004 u 0018
Chlorobenzene NO NO u 0021 Ethylbenzene 0047 021 0017 mp-Xylene 0070 031 0034 Bromoform NO NO u 0025 Styrene 0034 015 0022 1122-Tetrachloroethane NO NO u 0024 o-Xylene 0036 016 0018 135-Trlmethylbenzene 0025 012 u 0026 124-Trlmetllylbenzene 0047 023 0028 m-Oichlorobenzene NO NO u 0034
Chloromethylbenzene NO NO u 0039 p-Dichlorcbenzene 0005 003 u 0348 a-Dichlorobenzene NO NO u 0037
124-Trlchlorobenzene NO NO u 0036 Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repon must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS~RG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 66101 SUBMITTED 12061 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPDIAnalyte Result Units Result RPD um1t Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 661 01 SUBMITTED 120611
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its enJirety
Page 6 of 6
i
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
March 12 2012
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 030512 0916
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for UATMP NATTS CSATAM PAMS and NMOC support (US EPA Contract No 68-D-Q9-048) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Program Manager lauravanenwyckergcom
The information contained in this report and its attachmcnt(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauravanenwyckergcom and delete the report dthout retaining any copies
Page 1 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 0312112 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
6th St between Central amp 2030501-01 Air 030212 0000 030512 0916 Malcom
Eastern Research Group The results in this report apply only to the samples anal zed in accordance With the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Aven ue REPORTED 031212 1 051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 ~ tml
Analvte RRbll Y9lD1 flu RRbll Acetylene 0627 067 0072 Propylene 0484 084 0033
Dichlorodllluoromethane 0500 248 0023 Chloromethane 0557 115 0033
Dichlorotetrafluoroethane 0015 011 0012 Vinyl chloride NO NO u 0011
13-Butadlene 0036 oo8 0011
Bromomethane 0012 005 0012 Chloroethane NO NO u 0017
Acetonitrile 0073 012 0073
Trichlorofluoromethane 0258 145 0015 Acrylonitrile NO NO u 0020
11-0ichloroethene NO NO u 0014
Dichloromethane 0185 064 0023
Carbon Disulfide 0037 012 0014 Trichlorobitluoroethane 0119 091 0017
trans-12-0ichloroethylene NO NO u 0012
11-0ichloroethane NO NO u 0015
Methyl tert-Butyl Ether NO NO u 0011
Chloroprene NO NO u 0012
ds-12-0ich loroethylene NO NO u OD18
Bromochloromethane NO NO u 0014
Chloroform NO ND u 0014
Ethyl tert-Butyl Ether NO NO u 0011
12-Dichloroethane 0019 008 0016
111-Trichloroethane 0012 007 u 0020
Benzene 0344 L10 0061 Carbon Tetrachloride 0088 056 0024
tert-Amyl Methyl Ether NO NO u 0016
12-0ichloropropane ND NO u 0019
Ethyl Acrylate ND NO u 0014
Bromodichloromethane ND NO u 0021
Trichloroethylene NO ND u 0022
Methyl Methacrylate ND NO u 0025
ds-13-0ichloropropene NO NO u 0015
Methyl Isobutyl Ketone 0015 oo6 0015
trans-13-0ichloropropene NO ND u 0016
112-Trichloroethane NO NO u 0021
Toluene 0416 157 0045
Oibromochloromethane ND NO u 0018
12-0ibromoethane ND NO u 0017
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551 -5000
FILE 027800001030
REPORTED 0312 12 1051
SUBMITTED 030512
AQS SITE CODE
SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 Bwdtl MJlL
Analvte Jmbll Y9Lm Big Jmbx nmiddotOclane 0039 018 0020 Tetrachloroethylene 0005 003 u 0020
Chlorobenzene ND ND u 0025
Ethylbenzene 0045 020 0023 mp-Xylene 0112 OA9 0037 Bromoform ND ND u 0020
Styrene 0030 013 0024 1122-Tetrachloroethane ND ND u 0018
o-Xylene 0050 022 0020
135-Trimethylbenzene 0019 009 u 0022
124-Trimethylbenzene 0047 023 0025 m-Dichlorobenzene ND ND u 0024
p-Dichlorobenzene 0004 002 u 0019
a-Dichlorobenzene NO ND u 0021
124-Trichlorobenzene ND ND u 0022
Hexachloro-13-butadiene ND ND u 0022
Eastern Research Group The results in this report apply only 1o the samples analyzed in accordance with the chain of custody document This analytical rep ort must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 031212 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wilh the chain of custody document This analytical report must be reproduced in its enrirety
Page 5 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 03121121051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report nutst be reproduced in its entirety
Page 6 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1210511 1059
Kansas City KS 66101 SUBMITTED 1115 11
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption Uncoln amp 39 Highway (111 W Lincoln) Lab ID 1111501-01 Sampled 111411 0000
Pressure Receipt 8 Hg canister 636 Received 1115111121
Comments Analyzed 111611 0932
Air Toxics by EPA Compendium Method T0-15 RuJID mL
AnaMe IU1bll ~ BiSl IU1bll 12-Dlbromoethane NO NO A-Ql U 0018
n-Oct3ne 0025 012 A-Ql 0015
Tetrachloroethylene 0016 011 A-Ql U 0018
Ollorobenzene NO NO A-Ql U 0021
Ethylbenzene 0068 030 A-Ql 0017
mp-Xylene 0144 063 A-Ql 0034
Bromoform NO NO A-Ql U 0025
Styrene 0058 025 A-Ql 0022
1122-Tetrachloroethane NO NO A-Ql U 0024
o-Xylene 0058 025 A-ol 0018
135-Trlmetflylbenzene 0050 025 A-01 0026
124-Trimetflylbenzene 0130 064 A-Ql 0028
m-Dichlorobenzene NO NO A-Ql U 0034
Chloromelhylbenzene NO NO A-ol U 0039
p-Oichlorobenzene 0027 016 A-Ql U 0035
o-Oichlorobenzene NO NO A-Ql U 0037
124-Trichlorobenzene NO NO A-ol U 0036
Hexachloro-13-butadiene NO NO A-ol U 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 120511 1059
Kansas City KS 66101 SUBMITTED 111511
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance witlz tlze chain of custody documellt This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1205111 1 059
Kansas City KS 66101 SUBMITTED 11151 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
A-ol Estimated value due to possible canister leak
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical re-port must be reproduced in its entirety
Page 6 of 6
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
December 15 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 1206111229
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for NMOC UATMP PAMS CSATAM and NATTS support (US EPA Contract No EPD-09-048) This rover page is an integral part of this report and any exceptions or oomments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Project Manager lauravanenwyckergcom
The information contained in this report and its attachment(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify laura vanenwyck ergcom and delete the report without retaining any copies
Page 1 of 6
RG CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111 1041
Kansas City KS 66101 SUBMITTED 1206 11
ATTN Michael F Davis AQS SITE CODE
PHONE 913) 551-5042 FAX 913) 551-5000 SITE CODE OECAwork
ANALYTlCAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Ash amp Forest SE Corner 1120611-01 Air 120411 0000 120611 1229
middotI I
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytirol repon must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
ALE 027800001030
REPORTED 1215111041
SUBMmED 1210611
AQS SITE CODE
SITE CODE OECAwork
Desaiptlon Ash amp Forest SE Comer Lab ID 1120611-01 sampled 120411 oooo Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 BuYltl MQL
AnaMe IUlllll lWm Bag IUlllll Acetylene OA36 OA7 0016 Propylene 0304 052 0039 Dichlorodiftuoromethane 0567 281 0011 Chloromethane 0566 117 0012 Dlchlorotetnlftuoroethane 0019 013 0009 Vinyl chloride NO NO u 0008 13-Butadiene NO NO u 0007 Bromomethane 0012 005 0009 Chloroethane NO NO u 0009 Acetonitrile 0111 019 0024 Trichlorofluoromethane 0284 160 0010 Aaylonitrile ND NO u 0012 11-Dichloroethene ND ND u 0009 Dichloromethane 0083 029 0010 Carbon Disulfide 0019 006 u 0033
Trlchlorotrlftuoroethane 0099 076 0011 trans-12-Dichloroethylene ND ND u 0008 11-Dichloroethane ND NO u 0008 Methyl tert-Butyl Ether NO NO u 0008 Methyl Ethyl Ketone 0536 158 0157 Chloroprene NO NO u 0008 cis-12-Dichloroethylene NO ND u 0009 Bromochloromethane NO NO u 0008 Chloroform 0022 011 0009 Ethyl tert-Butyl Ether NO NO u 0008 12-Dichloroethane 0025 010 0009 111-Trichloroethane 0011 006 u 0022 Benzene 0188 060 0029 carbon Tetrachloride 0106 067 0024 tert-Amyl Methyl Ether NO NO u 0016 12-Dichloropropane NO NO u 0023 Ethyl Acrylate ND NO u 0020
Bromodichloromethane NO NO u 0025 Trichloroethylene NO NO u 0025 Methyl Methacrylate NO NO u 0022 cis-13-Dichloropropene NO NO u 0022
Methyl Isobutyl Ketone 0042 017 0022 trans-13-Dichloropropene ND NO u 0025 112-Trichloroethane NO NO u 0025
Toluene 0149 056 0016 Oibromochloromethane 0003 003 u 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproducedin its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 121511 1041
Kansas City KS 66101 SUBMmED 1210611
ATTN Michael F Davis AQS SITE CODE
PHONE (913 551-5042 FAX (913 551-5000 SITE CODE OECAwork
Description Ash amp Forest SE Comer Lab ID 1120611-01 Sampled 120411 0000
Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 llWdtl MID
Analyte ubll IUllm Bag ubll 12-0ibromoethane NO NO u 0018 nmiddotOctane 0044 021 0015 Tetrachloroethylene 0006 004 u 0018
Chlorobenzene NO NO u 0021 Ethylbenzene 0047 021 0017 mp-Xylene 0070 031 0034 Bromoform NO NO u 0025 Styrene 0034 015 0022 1122-Tetrachloroethane NO NO u 0024 o-Xylene 0036 016 0018 135-Trlmethylbenzene 0025 012 u 0026 124-Trlmetllylbenzene 0047 023 0028 m-Oichlorobenzene NO NO u 0034
Chloromethylbenzene NO NO u 0039 p-Dichlorcbenzene 0005 003 u 0348 a-Dichlorobenzene NO NO u 0037
124-Trlchlorobenzene NO NO u 0036 Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repon must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS~RG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 66101 SUBMITTED 12061 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPDIAnalyte Result Units Result RPD um1t Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 661 01 SUBMITTED 120611
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its enJirety
Page 6 of 6
i
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
March 12 2012
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 030512 0916
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for UATMP NATTS CSATAM PAMS and NMOC support (US EPA Contract No 68-D-Q9-048) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Program Manager lauravanenwyckergcom
The information contained in this report and its attachmcnt(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauravanenwyckergcom and delete the report dthout retaining any copies
Page 1 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 0312112 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
6th St between Central amp 2030501-01 Air 030212 0000 030512 0916 Malcom
Eastern Research Group The results in this report apply only to the samples anal zed in accordance With the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Aven ue REPORTED 031212 1 051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 ~ tml
Analvte RRbll Y9lD1 flu RRbll Acetylene 0627 067 0072 Propylene 0484 084 0033
Dichlorodllluoromethane 0500 248 0023 Chloromethane 0557 115 0033
Dichlorotetrafluoroethane 0015 011 0012 Vinyl chloride NO NO u 0011
13-Butadlene 0036 oo8 0011
Bromomethane 0012 005 0012 Chloroethane NO NO u 0017
Acetonitrile 0073 012 0073
Trichlorofluoromethane 0258 145 0015 Acrylonitrile NO NO u 0020
11-0ichloroethene NO NO u 0014
Dichloromethane 0185 064 0023
Carbon Disulfide 0037 012 0014 Trichlorobitluoroethane 0119 091 0017
trans-12-0ichloroethylene NO NO u 0012
11-0ichloroethane NO NO u 0015
Methyl tert-Butyl Ether NO NO u 0011
Chloroprene NO NO u 0012
ds-12-0ich loroethylene NO NO u OD18
Bromochloromethane NO NO u 0014
Chloroform NO ND u 0014
Ethyl tert-Butyl Ether NO NO u 0011
12-Dichloroethane 0019 008 0016
111-Trichloroethane 0012 007 u 0020
Benzene 0344 L10 0061 Carbon Tetrachloride 0088 056 0024
tert-Amyl Methyl Ether NO NO u 0016
12-0ichloropropane ND NO u 0019
Ethyl Acrylate ND NO u 0014
Bromodichloromethane ND NO u 0021
Trichloroethylene NO ND u 0022
Methyl Methacrylate ND NO u 0025
ds-13-0ichloropropene NO NO u 0015
Methyl Isobutyl Ketone 0015 oo6 0015
trans-13-0ichloropropene NO ND u 0016
112-Trichloroethane NO NO u 0021
Toluene 0416 157 0045
Oibromochloromethane ND NO u 0018
12-0ibromoethane ND NO u 0017
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551 -5000
FILE 027800001030
REPORTED 0312 12 1051
SUBMITTED 030512
AQS SITE CODE
SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 Bwdtl MJlL
Analvte Jmbll Y9Lm Big Jmbx nmiddotOclane 0039 018 0020 Tetrachloroethylene 0005 003 u 0020
Chlorobenzene ND ND u 0025
Ethylbenzene 0045 020 0023 mp-Xylene 0112 OA9 0037 Bromoform ND ND u 0020
Styrene 0030 013 0024 1122-Tetrachloroethane ND ND u 0018
o-Xylene 0050 022 0020
135-Trimethylbenzene 0019 009 u 0022
124-Trimethylbenzene 0047 023 0025 m-Dichlorobenzene ND ND u 0024
p-Dichlorobenzene 0004 002 u 0019
a-Dichlorobenzene NO ND u 0021
124-Trichlorobenzene ND ND u 0022
Hexachloro-13-butadiene ND ND u 0022
Eastern Research Group The results in this report apply only 1o the samples analyzed in accordance with the chain of custody document This analytical rep ort must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 031212 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wilh the chain of custody document This analytical report must be reproduced in its enrirety
Page 5 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 03121121051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report nutst be reproduced in its entirety
Page 6 of 6
CERTIFICATE OF ANALYSIS-ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 120511 1059
Kansas City KS 66101 SUBMITTED 111511
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance witlz tlze chain of custody documellt This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1205111 1 059
Kansas City KS 66101 SUBMITTED 11151 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
A-ol Estimated value due to possible canister leak
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical re-port must be reproduced in its entirety
Page 6 of 6
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
December 15 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 1206111229
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for NMOC UATMP PAMS CSATAM and NATTS support (US EPA Contract No EPD-09-048) This rover page is an integral part of this report and any exceptions or oomments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Project Manager lauravanenwyckergcom
The information contained in this report and its attachment(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify laura vanenwyck ergcom and delete the report without retaining any copies
Page 1 of 6
RG CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111 1041
Kansas City KS 66101 SUBMITTED 1206 11
ATTN Michael F Davis AQS SITE CODE
PHONE 913) 551-5042 FAX 913) 551-5000 SITE CODE OECAwork
ANALYTlCAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Ash amp Forest SE Corner 1120611-01 Air 120411 0000 120611 1229
middotI I
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytirol repon must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
ALE 027800001030
REPORTED 1215111041
SUBMmED 1210611
AQS SITE CODE
SITE CODE OECAwork
Desaiptlon Ash amp Forest SE Comer Lab ID 1120611-01 sampled 120411 oooo Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 BuYltl MQL
AnaMe IUlllll lWm Bag IUlllll Acetylene OA36 OA7 0016 Propylene 0304 052 0039 Dichlorodiftuoromethane 0567 281 0011 Chloromethane 0566 117 0012 Dlchlorotetnlftuoroethane 0019 013 0009 Vinyl chloride NO NO u 0008 13-Butadiene NO NO u 0007 Bromomethane 0012 005 0009 Chloroethane NO NO u 0009 Acetonitrile 0111 019 0024 Trichlorofluoromethane 0284 160 0010 Aaylonitrile ND NO u 0012 11-Dichloroethene ND ND u 0009 Dichloromethane 0083 029 0010 Carbon Disulfide 0019 006 u 0033
Trlchlorotrlftuoroethane 0099 076 0011 trans-12-Dichloroethylene ND ND u 0008 11-Dichloroethane ND NO u 0008 Methyl tert-Butyl Ether NO NO u 0008 Methyl Ethyl Ketone 0536 158 0157 Chloroprene NO NO u 0008 cis-12-Dichloroethylene NO ND u 0009 Bromochloromethane NO NO u 0008 Chloroform 0022 011 0009 Ethyl tert-Butyl Ether NO NO u 0008 12-Dichloroethane 0025 010 0009 111-Trichloroethane 0011 006 u 0022 Benzene 0188 060 0029 carbon Tetrachloride 0106 067 0024 tert-Amyl Methyl Ether NO NO u 0016 12-Dichloropropane NO NO u 0023 Ethyl Acrylate ND NO u 0020
Bromodichloromethane NO NO u 0025 Trichloroethylene NO NO u 0025 Methyl Methacrylate NO NO u 0022 cis-13-Dichloropropene NO NO u 0022
Methyl Isobutyl Ketone 0042 017 0022 trans-13-Dichloropropene ND NO u 0025 112-Trichloroethane NO NO u 0025
Toluene 0149 056 0016 Oibromochloromethane 0003 003 u 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproducedin its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 121511 1041
Kansas City KS 66101 SUBMmED 1210611
ATTN Michael F Davis AQS SITE CODE
PHONE (913 551-5042 FAX (913 551-5000 SITE CODE OECAwork
Description Ash amp Forest SE Comer Lab ID 1120611-01 Sampled 120411 0000
Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 llWdtl MID
Analyte ubll IUllm Bag ubll 12-0ibromoethane NO NO u 0018 nmiddotOctane 0044 021 0015 Tetrachloroethylene 0006 004 u 0018
Chlorobenzene NO NO u 0021 Ethylbenzene 0047 021 0017 mp-Xylene 0070 031 0034 Bromoform NO NO u 0025 Styrene 0034 015 0022 1122-Tetrachloroethane NO NO u 0024 o-Xylene 0036 016 0018 135-Trlmethylbenzene 0025 012 u 0026 124-Trlmetllylbenzene 0047 023 0028 m-Oichlorobenzene NO NO u 0034
Chloromethylbenzene NO NO u 0039 p-Dichlorcbenzene 0005 003 u 0348 a-Dichlorobenzene NO NO u 0037
124-Trlchlorobenzene NO NO u 0036 Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repon must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS~RG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 66101 SUBMITTED 12061 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPDIAnalyte Result Units Result RPD um1t Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 661 01 SUBMITTED 120611
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its enJirety
Page 6 of 6
i
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
March 12 2012
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 030512 0916
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for UATMP NATTS CSATAM PAMS and NMOC support (US EPA Contract No 68-D-Q9-048) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Program Manager lauravanenwyckergcom
The information contained in this report and its attachmcnt(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauravanenwyckergcom and delete the report dthout retaining any copies
Page 1 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 0312112 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
6th St between Central amp 2030501-01 Air 030212 0000 030512 0916 Malcom
Eastern Research Group The results in this report apply only to the samples anal zed in accordance With the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Aven ue REPORTED 031212 1 051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 ~ tml
Analvte RRbll Y9lD1 flu RRbll Acetylene 0627 067 0072 Propylene 0484 084 0033
Dichlorodllluoromethane 0500 248 0023 Chloromethane 0557 115 0033
Dichlorotetrafluoroethane 0015 011 0012 Vinyl chloride NO NO u 0011
13-Butadlene 0036 oo8 0011
Bromomethane 0012 005 0012 Chloroethane NO NO u 0017
Acetonitrile 0073 012 0073
Trichlorofluoromethane 0258 145 0015 Acrylonitrile NO NO u 0020
11-0ichloroethene NO NO u 0014
Dichloromethane 0185 064 0023
Carbon Disulfide 0037 012 0014 Trichlorobitluoroethane 0119 091 0017
trans-12-0ichloroethylene NO NO u 0012
11-0ichloroethane NO NO u 0015
Methyl tert-Butyl Ether NO NO u 0011
Chloroprene NO NO u 0012
ds-12-0ich loroethylene NO NO u OD18
Bromochloromethane NO NO u 0014
Chloroform NO ND u 0014
Ethyl tert-Butyl Ether NO NO u 0011
12-Dichloroethane 0019 008 0016
111-Trichloroethane 0012 007 u 0020
Benzene 0344 L10 0061 Carbon Tetrachloride 0088 056 0024
tert-Amyl Methyl Ether NO NO u 0016
12-0ichloropropane ND NO u 0019
Ethyl Acrylate ND NO u 0014
Bromodichloromethane ND NO u 0021
Trichloroethylene NO ND u 0022
Methyl Methacrylate ND NO u 0025
ds-13-0ichloropropene NO NO u 0015
Methyl Isobutyl Ketone 0015 oo6 0015
trans-13-0ichloropropene NO ND u 0016
112-Trichloroethane NO NO u 0021
Toluene 0416 157 0045
Oibromochloromethane ND NO u 0018
12-0ibromoethane ND NO u 0017
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551 -5000
FILE 027800001030
REPORTED 0312 12 1051
SUBMITTED 030512
AQS SITE CODE
SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 Bwdtl MJlL
Analvte Jmbll Y9Lm Big Jmbx nmiddotOclane 0039 018 0020 Tetrachloroethylene 0005 003 u 0020
Chlorobenzene ND ND u 0025
Ethylbenzene 0045 020 0023 mp-Xylene 0112 OA9 0037 Bromoform ND ND u 0020
Styrene 0030 013 0024 1122-Tetrachloroethane ND ND u 0018
o-Xylene 0050 022 0020
135-Trimethylbenzene 0019 009 u 0022
124-Trimethylbenzene 0047 023 0025 m-Dichlorobenzene ND ND u 0024
p-Dichlorobenzene 0004 002 u 0019
a-Dichlorobenzene NO ND u 0021
124-Trichlorobenzene ND ND u 0022
Hexachloro-13-butadiene ND ND u 0022
Eastern Research Group The results in this report apply only 1o the samples analyzed in accordance with the chain of custody document This analytical rep ort must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 031212 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wilh the chain of custody document This analytical report must be reproduced in its enrirety
Page 5 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 03121121051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report nutst be reproduced in its entirety
Page 6 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1205111 1 059
Kansas City KS 66101 SUBMITTED 11151 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
A-ol Estimated value due to possible canister leak
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical re-port must be reproduced in its entirety
Page 6 of 6
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
December 15 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 1206111229
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for NMOC UATMP PAMS CSATAM and NATTS support (US EPA Contract No EPD-09-048) This rover page is an integral part of this report and any exceptions or oomments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Project Manager lauravanenwyckergcom
The information contained in this report and its attachment(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify laura vanenwyck ergcom and delete the report without retaining any copies
Page 1 of 6
RG CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111 1041
Kansas City KS 66101 SUBMITTED 1206 11
ATTN Michael F Davis AQS SITE CODE
PHONE 913) 551-5042 FAX 913) 551-5000 SITE CODE OECAwork
ANALYTlCAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Ash amp Forest SE Corner 1120611-01 Air 120411 0000 120611 1229
middotI I
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytirol repon must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
ALE 027800001030
REPORTED 1215111041
SUBMmED 1210611
AQS SITE CODE
SITE CODE OECAwork
Desaiptlon Ash amp Forest SE Comer Lab ID 1120611-01 sampled 120411 oooo Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 BuYltl MQL
AnaMe IUlllll lWm Bag IUlllll Acetylene OA36 OA7 0016 Propylene 0304 052 0039 Dichlorodiftuoromethane 0567 281 0011 Chloromethane 0566 117 0012 Dlchlorotetnlftuoroethane 0019 013 0009 Vinyl chloride NO NO u 0008 13-Butadiene NO NO u 0007 Bromomethane 0012 005 0009 Chloroethane NO NO u 0009 Acetonitrile 0111 019 0024 Trichlorofluoromethane 0284 160 0010 Aaylonitrile ND NO u 0012 11-Dichloroethene ND ND u 0009 Dichloromethane 0083 029 0010 Carbon Disulfide 0019 006 u 0033
Trlchlorotrlftuoroethane 0099 076 0011 trans-12-Dichloroethylene ND ND u 0008 11-Dichloroethane ND NO u 0008 Methyl tert-Butyl Ether NO NO u 0008 Methyl Ethyl Ketone 0536 158 0157 Chloroprene NO NO u 0008 cis-12-Dichloroethylene NO ND u 0009 Bromochloromethane NO NO u 0008 Chloroform 0022 011 0009 Ethyl tert-Butyl Ether NO NO u 0008 12-Dichloroethane 0025 010 0009 111-Trichloroethane 0011 006 u 0022 Benzene 0188 060 0029 carbon Tetrachloride 0106 067 0024 tert-Amyl Methyl Ether NO NO u 0016 12-Dichloropropane NO NO u 0023 Ethyl Acrylate ND NO u 0020
Bromodichloromethane NO NO u 0025 Trichloroethylene NO NO u 0025 Methyl Methacrylate NO NO u 0022 cis-13-Dichloropropene NO NO u 0022
Methyl Isobutyl Ketone 0042 017 0022 trans-13-Dichloropropene ND NO u 0025 112-Trichloroethane NO NO u 0025
Toluene 0149 056 0016 Oibromochloromethane 0003 003 u 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproducedin its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 121511 1041
Kansas City KS 66101 SUBMmED 1210611
ATTN Michael F Davis AQS SITE CODE
PHONE (913 551-5042 FAX (913 551-5000 SITE CODE OECAwork
Description Ash amp Forest SE Comer Lab ID 1120611-01 Sampled 120411 0000
Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 llWdtl MID
Analyte ubll IUllm Bag ubll 12-0ibromoethane NO NO u 0018 nmiddotOctane 0044 021 0015 Tetrachloroethylene 0006 004 u 0018
Chlorobenzene NO NO u 0021 Ethylbenzene 0047 021 0017 mp-Xylene 0070 031 0034 Bromoform NO NO u 0025 Styrene 0034 015 0022 1122-Tetrachloroethane NO NO u 0024 o-Xylene 0036 016 0018 135-Trlmethylbenzene 0025 012 u 0026 124-Trlmetllylbenzene 0047 023 0028 m-Oichlorobenzene NO NO u 0034
Chloromethylbenzene NO NO u 0039 p-Dichlorcbenzene 0005 003 u 0348 a-Dichlorobenzene NO NO u 0037
124-Trlchlorobenzene NO NO u 0036 Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repon must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS~RG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 66101 SUBMITTED 12061 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPDIAnalyte Result Units Result RPD um1t Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 661 01 SUBMITTED 120611
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its enJirety
Page 6 of 6
i
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
March 12 2012
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 030512 0916
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for UATMP NATTS CSATAM PAMS and NMOC support (US EPA Contract No 68-D-Q9-048) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Program Manager lauravanenwyckergcom
The information contained in this report and its attachmcnt(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauravanenwyckergcom and delete the report dthout retaining any copies
Page 1 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 0312112 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
6th St between Central amp 2030501-01 Air 030212 0000 030512 0916 Malcom
Eastern Research Group The results in this report apply only to the samples anal zed in accordance With the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Aven ue REPORTED 031212 1 051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 ~ tml
Analvte RRbll Y9lD1 flu RRbll Acetylene 0627 067 0072 Propylene 0484 084 0033
Dichlorodllluoromethane 0500 248 0023 Chloromethane 0557 115 0033
Dichlorotetrafluoroethane 0015 011 0012 Vinyl chloride NO NO u 0011
13-Butadlene 0036 oo8 0011
Bromomethane 0012 005 0012 Chloroethane NO NO u 0017
Acetonitrile 0073 012 0073
Trichlorofluoromethane 0258 145 0015 Acrylonitrile NO NO u 0020
11-0ichloroethene NO NO u 0014
Dichloromethane 0185 064 0023
Carbon Disulfide 0037 012 0014 Trichlorobitluoroethane 0119 091 0017
trans-12-0ichloroethylene NO NO u 0012
11-0ichloroethane NO NO u 0015
Methyl tert-Butyl Ether NO NO u 0011
Chloroprene NO NO u 0012
ds-12-0ich loroethylene NO NO u OD18
Bromochloromethane NO NO u 0014
Chloroform NO ND u 0014
Ethyl tert-Butyl Ether NO NO u 0011
12-Dichloroethane 0019 008 0016
111-Trichloroethane 0012 007 u 0020
Benzene 0344 L10 0061 Carbon Tetrachloride 0088 056 0024
tert-Amyl Methyl Ether NO NO u 0016
12-0ichloropropane ND NO u 0019
Ethyl Acrylate ND NO u 0014
Bromodichloromethane ND NO u 0021
Trichloroethylene NO ND u 0022
Methyl Methacrylate ND NO u 0025
ds-13-0ichloropropene NO NO u 0015
Methyl Isobutyl Ketone 0015 oo6 0015
trans-13-0ichloropropene NO ND u 0016
112-Trichloroethane NO NO u 0021
Toluene 0416 157 0045
Oibromochloromethane ND NO u 0018
12-0ibromoethane ND NO u 0017
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551 -5000
FILE 027800001030
REPORTED 0312 12 1051
SUBMITTED 030512
AQS SITE CODE
SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 Bwdtl MJlL
Analvte Jmbll Y9Lm Big Jmbx nmiddotOclane 0039 018 0020 Tetrachloroethylene 0005 003 u 0020
Chlorobenzene ND ND u 0025
Ethylbenzene 0045 020 0023 mp-Xylene 0112 OA9 0037 Bromoform ND ND u 0020
Styrene 0030 013 0024 1122-Tetrachloroethane ND ND u 0018
o-Xylene 0050 022 0020
135-Trimethylbenzene 0019 009 u 0022
124-Trimethylbenzene 0047 023 0025 m-Dichlorobenzene ND ND u 0024
p-Dichlorobenzene 0004 002 u 0019
a-Dichlorobenzene NO ND u 0021
124-Trichlorobenzene ND ND u 0022
Hexachloro-13-butadiene ND ND u 0022
Eastern Research Group The results in this report apply only 1o the samples analyzed in accordance with the chain of custody document This analytical rep ort must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 031212 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wilh the chain of custody document This analytical report must be reproduced in its enrirety
Page 5 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 03121121051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report nutst be reproduced in its entirety
Page 6 of 6
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
December 15 2011
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 1206111229
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for NMOC UATMP PAMS CSATAM and NATTS support (US EPA Contract No EPD-09-048) This rover page is an integral part of this report and any exceptions or oomments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Project Manager lauravanenwyckergcom
The information contained in this report and its attachment(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify laura vanenwyck ergcom and delete the report without retaining any copies
Page 1 of 6
RG CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111 1041
Kansas City KS 66101 SUBMITTED 1206 11
ATTN Michael F Davis AQS SITE CODE
PHONE 913) 551-5042 FAX 913) 551-5000 SITE CODE OECAwork
ANALYTlCAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Ash amp Forest SE Corner 1120611-01 Air 120411 0000 120611 1229
middotI I
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytirol repon must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
ALE 027800001030
REPORTED 1215111041
SUBMmED 1210611
AQS SITE CODE
SITE CODE OECAwork
Desaiptlon Ash amp Forest SE Comer Lab ID 1120611-01 sampled 120411 oooo Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 BuYltl MQL
AnaMe IUlllll lWm Bag IUlllll Acetylene OA36 OA7 0016 Propylene 0304 052 0039 Dichlorodiftuoromethane 0567 281 0011 Chloromethane 0566 117 0012 Dlchlorotetnlftuoroethane 0019 013 0009 Vinyl chloride NO NO u 0008 13-Butadiene NO NO u 0007 Bromomethane 0012 005 0009 Chloroethane NO NO u 0009 Acetonitrile 0111 019 0024 Trichlorofluoromethane 0284 160 0010 Aaylonitrile ND NO u 0012 11-Dichloroethene ND ND u 0009 Dichloromethane 0083 029 0010 Carbon Disulfide 0019 006 u 0033
Trlchlorotrlftuoroethane 0099 076 0011 trans-12-Dichloroethylene ND ND u 0008 11-Dichloroethane ND NO u 0008 Methyl tert-Butyl Ether NO NO u 0008 Methyl Ethyl Ketone 0536 158 0157 Chloroprene NO NO u 0008 cis-12-Dichloroethylene NO ND u 0009 Bromochloromethane NO NO u 0008 Chloroform 0022 011 0009 Ethyl tert-Butyl Ether NO NO u 0008 12-Dichloroethane 0025 010 0009 111-Trichloroethane 0011 006 u 0022 Benzene 0188 060 0029 carbon Tetrachloride 0106 067 0024 tert-Amyl Methyl Ether NO NO u 0016 12-Dichloropropane NO NO u 0023 Ethyl Acrylate ND NO u 0020
Bromodichloromethane NO NO u 0025 Trichloroethylene NO NO u 0025 Methyl Methacrylate NO NO u 0022 cis-13-Dichloropropene NO NO u 0022
Methyl Isobutyl Ketone 0042 017 0022 trans-13-Dichloropropene ND NO u 0025 112-Trichloroethane NO NO u 0025
Toluene 0149 056 0016 Oibromochloromethane 0003 003 u 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproducedin its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 121511 1041
Kansas City KS 66101 SUBMmED 1210611
ATTN Michael F Davis AQS SITE CODE
PHONE (913 551-5042 FAX (913 551-5000 SITE CODE OECAwork
Description Ash amp Forest SE Comer Lab ID 1120611-01 Sampled 120411 0000
Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 llWdtl MID
Analyte ubll IUllm Bag ubll 12-0ibromoethane NO NO u 0018 nmiddotOctane 0044 021 0015 Tetrachloroethylene 0006 004 u 0018
Chlorobenzene NO NO u 0021 Ethylbenzene 0047 021 0017 mp-Xylene 0070 031 0034 Bromoform NO NO u 0025 Styrene 0034 015 0022 1122-Tetrachloroethane NO NO u 0024 o-Xylene 0036 016 0018 135-Trlmethylbenzene 0025 012 u 0026 124-Trlmetllylbenzene 0047 023 0028 m-Oichlorobenzene NO NO u 0034
Chloromethylbenzene NO NO u 0039 p-Dichlorcbenzene 0005 003 u 0348 a-Dichlorobenzene NO NO u 0037
124-Trlchlorobenzene NO NO u 0036 Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repon must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS~RG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 66101 SUBMITTED 12061 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPDIAnalyte Result Units Result RPD um1t Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 661 01 SUBMITTED 120611
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its enJirety
Page 6 of 6
i
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
March 12 2012
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 030512 0916
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for UATMP NATTS CSATAM PAMS and NMOC support (US EPA Contract No 68-D-Q9-048) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Program Manager lauravanenwyckergcom
The information contained in this report and its attachmcnt(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauravanenwyckergcom and delete the report dthout retaining any copies
Page 1 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 0312112 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
6th St between Central amp 2030501-01 Air 030212 0000 030512 0916 Malcom
Eastern Research Group The results in this report apply only to the samples anal zed in accordance With the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Aven ue REPORTED 031212 1 051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 ~ tml
Analvte RRbll Y9lD1 flu RRbll Acetylene 0627 067 0072 Propylene 0484 084 0033
Dichlorodllluoromethane 0500 248 0023 Chloromethane 0557 115 0033
Dichlorotetrafluoroethane 0015 011 0012 Vinyl chloride NO NO u 0011
13-Butadlene 0036 oo8 0011
Bromomethane 0012 005 0012 Chloroethane NO NO u 0017
Acetonitrile 0073 012 0073
Trichlorofluoromethane 0258 145 0015 Acrylonitrile NO NO u 0020
11-0ichloroethene NO NO u 0014
Dichloromethane 0185 064 0023
Carbon Disulfide 0037 012 0014 Trichlorobitluoroethane 0119 091 0017
trans-12-0ichloroethylene NO NO u 0012
11-0ichloroethane NO NO u 0015
Methyl tert-Butyl Ether NO NO u 0011
Chloroprene NO NO u 0012
ds-12-0ich loroethylene NO NO u OD18
Bromochloromethane NO NO u 0014
Chloroform NO ND u 0014
Ethyl tert-Butyl Ether NO NO u 0011
12-Dichloroethane 0019 008 0016
111-Trichloroethane 0012 007 u 0020
Benzene 0344 L10 0061 Carbon Tetrachloride 0088 056 0024
tert-Amyl Methyl Ether NO NO u 0016
12-0ichloropropane ND NO u 0019
Ethyl Acrylate ND NO u 0014
Bromodichloromethane ND NO u 0021
Trichloroethylene NO ND u 0022
Methyl Methacrylate ND NO u 0025
ds-13-0ichloropropene NO NO u 0015
Methyl Isobutyl Ketone 0015 oo6 0015
trans-13-0ichloropropene NO ND u 0016
112-Trichloroethane NO NO u 0021
Toluene 0416 157 0045
Oibromochloromethane ND NO u 0018
12-0ibromoethane ND NO u 0017
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551 -5000
FILE 027800001030
REPORTED 0312 12 1051
SUBMITTED 030512
AQS SITE CODE
SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 Bwdtl MJlL
Analvte Jmbll Y9Lm Big Jmbx nmiddotOclane 0039 018 0020 Tetrachloroethylene 0005 003 u 0020
Chlorobenzene ND ND u 0025
Ethylbenzene 0045 020 0023 mp-Xylene 0112 OA9 0037 Bromoform ND ND u 0020
Styrene 0030 013 0024 1122-Tetrachloroethane ND ND u 0018
o-Xylene 0050 022 0020
135-Trimethylbenzene 0019 009 u 0022
124-Trimethylbenzene 0047 023 0025 m-Dichlorobenzene ND ND u 0024
p-Dichlorobenzene 0004 002 u 0019
a-Dichlorobenzene NO ND u 0021
124-Trichlorobenzene ND ND u 0022
Hexachloro-13-butadiene ND ND u 0022
Eastern Research Group The results in this report apply only 1o the samples analyzed in accordance with the chain of custody document This analytical rep ort must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 031212 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wilh the chain of custody document This analytical report must be reproduced in its enrirety
Page 5 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 03121121051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report nutst be reproduced in its entirety
Page 6 of 6
RG CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111 1041
Kansas City KS 66101 SUBMITTED 1206 11
ATTN Michael F Davis AQS SITE CODE
PHONE 913) 551-5042 FAX 913) 551-5000 SITE CODE OECAwork
ANALYTlCAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
Ash amp Forest SE Corner 1120611-01 Air 120411 0000 120611 1229
middotI I
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytirol repon must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
ALE 027800001030
REPORTED 1215111041
SUBMmED 1210611
AQS SITE CODE
SITE CODE OECAwork
Desaiptlon Ash amp Forest SE Comer Lab ID 1120611-01 sampled 120411 oooo Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 BuYltl MQL
AnaMe IUlllll lWm Bag IUlllll Acetylene OA36 OA7 0016 Propylene 0304 052 0039 Dichlorodiftuoromethane 0567 281 0011 Chloromethane 0566 117 0012 Dlchlorotetnlftuoroethane 0019 013 0009 Vinyl chloride NO NO u 0008 13-Butadiene NO NO u 0007 Bromomethane 0012 005 0009 Chloroethane NO NO u 0009 Acetonitrile 0111 019 0024 Trichlorofluoromethane 0284 160 0010 Aaylonitrile ND NO u 0012 11-Dichloroethene ND ND u 0009 Dichloromethane 0083 029 0010 Carbon Disulfide 0019 006 u 0033
Trlchlorotrlftuoroethane 0099 076 0011 trans-12-Dichloroethylene ND ND u 0008 11-Dichloroethane ND NO u 0008 Methyl tert-Butyl Ether NO NO u 0008 Methyl Ethyl Ketone 0536 158 0157 Chloroprene NO NO u 0008 cis-12-Dichloroethylene NO ND u 0009 Bromochloromethane NO NO u 0008 Chloroform 0022 011 0009 Ethyl tert-Butyl Ether NO NO u 0008 12-Dichloroethane 0025 010 0009 111-Trichloroethane 0011 006 u 0022 Benzene 0188 060 0029 carbon Tetrachloride 0106 067 0024 tert-Amyl Methyl Ether NO NO u 0016 12-Dichloropropane NO NO u 0023 Ethyl Acrylate ND NO u 0020
Bromodichloromethane NO NO u 0025 Trichloroethylene NO NO u 0025 Methyl Methacrylate NO NO u 0022 cis-13-Dichloropropene NO NO u 0022
Methyl Isobutyl Ketone 0042 017 0022 trans-13-Dichloropropene ND NO u 0025 112-Trichloroethane NO NO u 0025
Toluene 0149 056 0016 Oibromochloromethane 0003 003 u 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproducedin its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 121511 1041
Kansas City KS 66101 SUBMmED 1210611
ATTN Michael F Davis AQS SITE CODE
PHONE (913 551-5042 FAX (913 551-5000 SITE CODE OECAwork
Description Ash amp Forest SE Comer Lab ID 1120611-01 Sampled 120411 0000
Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 llWdtl MID
Analyte ubll IUllm Bag ubll 12-0ibromoethane NO NO u 0018 nmiddotOctane 0044 021 0015 Tetrachloroethylene 0006 004 u 0018
Chlorobenzene NO NO u 0021 Ethylbenzene 0047 021 0017 mp-Xylene 0070 031 0034 Bromoform NO NO u 0025 Styrene 0034 015 0022 1122-Tetrachloroethane NO NO u 0024 o-Xylene 0036 016 0018 135-Trlmethylbenzene 0025 012 u 0026 124-Trlmetllylbenzene 0047 023 0028 m-Oichlorobenzene NO NO u 0034
Chloromethylbenzene NO NO u 0039 p-Dichlorcbenzene 0005 003 u 0348 a-Dichlorobenzene NO NO u 0037
124-Trlchlorobenzene NO NO u 0036 Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repon must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS~RG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 66101 SUBMITTED 12061 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPDIAnalyte Result Units Result RPD um1t Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 661 01 SUBMITTED 120611
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its enJirety
Page 6 of 6
i
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
March 12 2012
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 030512 0916
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for UATMP NATTS CSATAM PAMS and NMOC support (US EPA Contract No 68-D-Q9-048) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Program Manager lauravanenwyckergcom
The information contained in this report and its attachmcnt(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauravanenwyckergcom and delete the report dthout retaining any copies
Page 1 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 0312112 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
6th St between Central amp 2030501-01 Air 030212 0000 030512 0916 Malcom
Eastern Research Group The results in this report apply only to the samples anal zed in accordance With the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Aven ue REPORTED 031212 1 051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 ~ tml
Analvte RRbll Y9lD1 flu RRbll Acetylene 0627 067 0072 Propylene 0484 084 0033
Dichlorodllluoromethane 0500 248 0023 Chloromethane 0557 115 0033
Dichlorotetrafluoroethane 0015 011 0012 Vinyl chloride NO NO u 0011
13-Butadlene 0036 oo8 0011
Bromomethane 0012 005 0012 Chloroethane NO NO u 0017
Acetonitrile 0073 012 0073
Trichlorofluoromethane 0258 145 0015 Acrylonitrile NO NO u 0020
11-0ichloroethene NO NO u 0014
Dichloromethane 0185 064 0023
Carbon Disulfide 0037 012 0014 Trichlorobitluoroethane 0119 091 0017
trans-12-0ichloroethylene NO NO u 0012
11-0ichloroethane NO NO u 0015
Methyl tert-Butyl Ether NO NO u 0011
Chloroprene NO NO u 0012
ds-12-0ich loroethylene NO NO u OD18
Bromochloromethane NO NO u 0014
Chloroform NO ND u 0014
Ethyl tert-Butyl Ether NO NO u 0011
12-Dichloroethane 0019 008 0016
111-Trichloroethane 0012 007 u 0020
Benzene 0344 L10 0061 Carbon Tetrachloride 0088 056 0024
tert-Amyl Methyl Ether NO NO u 0016
12-0ichloropropane ND NO u 0019
Ethyl Acrylate ND NO u 0014
Bromodichloromethane ND NO u 0021
Trichloroethylene NO ND u 0022
Methyl Methacrylate ND NO u 0025
ds-13-0ichloropropene NO NO u 0015
Methyl Isobutyl Ketone 0015 oo6 0015
trans-13-0ichloropropene NO ND u 0016
112-Trichloroethane NO NO u 0021
Toluene 0416 157 0045
Oibromochloromethane ND NO u 0018
12-0ibromoethane ND NO u 0017
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551 -5000
FILE 027800001030
REPORTED 0312 12 1051
SUBMITTED 030512
AQS SITE CODE
SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 Bwdtl MJlL
Analvte Jmbll Y9Lm Big Jmbx nmiddotOclane 0039 018 0020 Tetrachloroethylene 0005 003 u 0020
Chlorobenzene ND ND u 0025
Ethylbenzene 0045 020 0023 mp-Xylene 0112 OA9 0037 Bromoform ND ND u 0020
Styrene 0030 013 0024 1122-Tetrachloroethane ND ND u 0018
o-Xylene 0050 022 0020
135-Trimethylbenzene 0019 009 u 0022
124-Trimethylbenzene 0047 023 0025 m-Dichlorobenzene ND ND u 0024
p-Dichlorobenzene 0004 002 u 0019
a-Dichlorobenzene NO ND u 0021
124-Trichlorobenzene ND ND u 0022
Hexachloro-13-butadiene ND ND u 0022
Eastern Research Group The results in this report apply only 1o the samples analyzed in accordance with the chain of custody document This analytical rep ort must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 031212 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wilh the chain of custody document This analytical report must be reproduced in its enrirety
Page 5 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 03121121051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report nutst be reproduced in its entirety
Page 6 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551-5000
ALE 027800001030
REPORTED 1215111041
SUBMmED 1210611
AQS SITE CODE
SITE CODE OECAwork
Desaiptlon Ash amp Forest SE Comer Lab ID 1120611-01 sampled 120411 oooo Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 BuYltl MQL
AnaMe IUlllll lWm Bag IUlllll Acetylene OA36 OA7 0016 Propylene 0304 052 0039 Dichlorodiftuoromethane 0567 281 0011 Chloromethane 0566 117 0012 Dlchlorotetnlftuoroethane 0019 013 0009 Vinyl chloride NO NO u 0008 13-Butadiene NO NO u 0007 Bromomethane 0012 005 0009 Chloroethane NO NO u 0009 Acetonitrile 0111 019 0024 Trichlorofluoromethane 0284 160 0010 Aaylonitrile ND NO u 0012 11-Dichloroethene ND ND u 0009 Dichloromethane 0083 029 0010 Carbon Disulfide 0019 006 u 0033
Trlchlorotrlftuoroethane 0099 076 0011 trans-12-Dichloroethylene ND ND u 0008 11-Dichloroethane ND NO u 0008 Methyl tert-Butyl Ether NO NO u 0008 Methyl Ethyl Ketone 0536 158 0157 Chloroprene NO NO u 0008 cis-12-Dichloroethylene NO ND u 0009 Bromochloromethane NO NO u 0008 Chloroform 0022 011 0009 Ethyl tert-Butyl Ether NO NO u 0008 12-Dichloroethane 0025 010 0009 111-Trichloroethane 0011 006 u 0022 Benzene 0188 060 0029 carbon Tetrachloride 0106 067 0024 tert-Amyl Methyl Ether NO NO u 0016 12-Dichloropropane NO NO u 0023 Ethyl Acrylate ND NO u 0020
Bromodichloromethane NO NO u 0025 Trichloroethylene NO NO u 0025 Methyl Methacrylate NO NO u 0022 cis-13-Dichloropropene NO NO u 0022
Methyl Isobutyl Ketone 0042 017 0022 trans-13-Dichloropropene ND NO u 0025 112-Trichloroethane NO NO u 0025
Toluene 0149 056 0016 Oibromochloromethane 0003 003 u 0021
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproducedin its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 121511 1041
Kansas City KS 66101 SUBMmED 1210611
ATTN Michael F Davis AQS SITE CODE
PHONE (913 551-5042 FAX (913 551-5000 SITE CODE OECAwork
Description Ash amp Forest SE Comer Lab ID 1120611-01 Sampled 120411 0000
Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 llWdtl MID
Analyte ubll IUllm Bag ubll 12-0ibromoethane NO NO u 0018 nmiddotOctane 0044 021 0015 Tetrachloroethylene 0006 004 u 0018
Chlorobenzene NO NO u 0021 Ethylbenzene 0047 021 0017 mp-Xylene 0070 031 0034 Bromoform NO NO u 0025 Styrene 0034 015 0022 1122-Tetrachloroethane NO NO u 0024 o-Xylene 0036 016 0018 135-Trlmethylbenzene 0025 012 u 0026 124-Trlmetllylbenzene 0047 023 0028 m-Oichlorobenzene NO NO u 0034
Chloromethylbenzene NO NO u 0039 p-Dichlorcbenzene 0005 003 u 0348 a-Dichlorobenzene NO NO u 0037
124-Trlchlorobenzene NO NO u 0036 Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repon must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS~RG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 66101 SUBMITTED 12061 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPDIAnalyte Result Units Result RPD um1t Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 661 01 SUBMITTED 120611
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its enJirety
Page 6 of 6
i
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
March 12 2012
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 030512 0916
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for UATMP NATTS CSATAM PAMS and NMOC support (US EPA Contract No 68-D-Q9-048) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Program Manager lauravanenwyckergcom
The information contained in this report and its attachmcnt(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauravanenwyckergcom and delete the report dthout retaining any copies
Page 1 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 0312112 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
6th St between Central amp 2030501-01 Air 030212 0000 030512 0916 Malcom
Eastern Research Group The results in this report apply only to the samples anal zed in accordance With the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Aven ue REPORTED 031212 1 051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 ~ tml
Analvte RRbll Y9lD1 flu RRbll Acetylene 0627 067 0072 Propylene 0484 084 0033
Dichlorodllluoromethane 0500 248 0023 Chloromethane 0557 115 0033
Dichlorotetrafluoroethane 0015 011 0012 Vinyl chloride NO NO u 0011
13-Butadlene 0036 oo8 0011
Bromomethane 0012 005 0012 Chloroethane NO NO u 0017
Acetonitrile 0073 012 0073
Trichlorofluoromethane 0258 145 0015 Acrylonitrile NO NO u 0020
11-0ichloroethene NO NO u 0014
Dichloromethane 0185 064 0023
Carbon Disulfide 0037 012 0014 Trichlorobitluoroethane 0119 091 0017
trans-12-0ichloroethylene NO NO u 0012
11-0ichloroethane NO NO u 0015
Methyl tert-Butyl Ether NO NO u 0011
Chloroprene NO NO u 0012
ds-12-0ich loroethylene NO NO u OD18
Bromochloromethane NO NO u 0014
Chloroform NO ND u 0014
Ethyl tert-Butyl Ether NO NO u 0011
12-Dichloroethane 0019 008 0016
111-Trichloroethane 0012 007 u 0020
Benzene 0344 L10 0061 Carbon Tetrachloride 0088 056 0024
tert-Amyl Methyl Ether NO NO u 0016
12-0ichloropropane ND NO u 0019
Ethyl Acrylate ND NO u 0014
Bromodichloromethane ND NO u 0021
Trichloroethylene NO ND u 0022
Methyl Methacrylate ND NO u 0025
ds-13-0ichloropropene NO NO u 0015
Methyl Isobutyl Ketone 0015 oo6 0015
trans-13-0ichloropropene NO ND u 0016
112-Trichloroethane NO NO u 0021
Toluene 0416 157 0045
Oibromochloromethane ND NO u 0018
12-0ibromoethane ND NO u 0017
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551 -5000
FILE 027800001030
REPORTED 0312 12 1051
SUBMITTED 030512
AQS SITE CODE
SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 Bwdtl MJlL
Analvte Jmbll Y9Lm Big Jmbx nmiddotOclane 0039 018 0020 Tetrachloroethylene 0005 003 u 0020
Chlorobenzene ND ND u 0025
Ethylbenzene 0045 020 0023 mp-Xylene 0112 OA9 0037 Bromoform ND ND u 0020
Styrene 0030 013 0024 1122-Tetrachloroethane ND ND u 0018
o-Xylene 0050 022 0020
135-Trimethylbenzene 0019 009 u 0022
124-Trimethylbenzene 0047 023 0025 m-Dichlorobenzene ND ND u 0024
p-Dichlorobenzene 0004 002 u 0019
a-Dichlorobenzene NO ND u 0021
124-Trichlorobenzene ND ND u 0022
Hexachloro-13-butadiene ND ND u 0022
Eastern Research Group The results in this report apply only 1o the samples analyzed in accordance with the chain of custody document This analytical rep ort must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 031212 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wilh the chain of custody document This analytical report must be reproduced in its enrirety
Page 5 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 03121121051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report nutst be reproduced in its entirety
Page 6 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 121511 1041
Kansas City KS 66101 SUBMmED 1210611
ATTN Michael F Davis AQS SITE CODE
PHONE (913 551-5042 FAX (913 551-5000 SITE CODE OECAwork
Description Ash amp Forest SE Comer Lab ID 1120611-01 Sampled 120411 0000
Pressure Receipt 6 Hg canister 083 Received 120611 1229
Comments Analyzed 120711 0111
Air Taxies by EPA Compendium Method T0-15 llWdtl MID
Analyte ubll IUllm Bag ubll 12-0ibromoethane NO NO u 0018 nmiddotOctane 0044 021 0015 Tetrachloroethylene 0006 004 u 0018
Chlorobenzene NO NO u 0021 Ethylbenzene 0047 021 0017 mp-Xylene 0070 031 0034 Bromoform NO NO u 0025 Styrene 0034 015 0022 1122-Tetrachloroethane NO NO u 0024 o-Xylene 0036 016 0018 135-Trlmethylbenzene 0025 012 u 0026 124-Trlmetllylbenzene 0047 023 0028 m-Oichlorobenzene NO NO u 0034
Chloromethylbenzene NO NO u 0039 p-Dichlorcbenzene 0005 003 u 0348 a-Dichlorobenzene NO NO u 0037
124-Trlchlorobenzene NO NO u 0036 Hexachloro-13-butadiene NO NO u 0037
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical repon must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS~RG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 66101 SUBMITTED 12061 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPDIAnalyte Result Units Result RPD um1t Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 661 01 SUBMITTED 120611
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its enJirety
Page 6 of 6
i
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
March 12 2012
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 030512 0916
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for UATMP NATTS CSATAM PAMS and NMOC support (US EPA Contract No 68-D-Q9-048) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Program Manager lauravanenwyckergcom
The information contained in this report and its attachmcnt(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauravanenwyckergcom and delete the report dthout retaining any copies
Page 1 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 0312112 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
6th St between Central amp 2030501-01 Air 030212 0000 030512 0916 Malcom
Eastern Research Group The results in this report apply only to the samples anal zed in accordance With the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Aven ue REPORTED 031212 1 051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 ~ tml
Analvte RRbll Y9lD1 flu RRbll Acetylene 0627 067 0072 Propylene 0484 084 0033
Dichlorodllluoromethane 0500 248 0023 Chloromethane 0557 115 0033
Dichlorotetrafluoroethane 0015 011 0012 Vinyl chloride NO NO u 0011
13-Butadlene 0036 oo8 0011
Bromomethane 0012 005 0012 Chloroethane NO NO u 0017
Acetonitrile 0073 012 0073
Trichlorofluoromethane 0258 145 0015 Acrylonitrile NO NO u 0020
11-0ichloroethene NO NO u 0014
Dichloromethane 0185 064 0023
Carbon Disulfide 0037 012 0014 Trichlorobitluoroethane 0119 091 0017
trans-12-0ichloroethylene NO NO u 0012
11-0ichloroethane NO NO u 0015
Methyl tert-Butyl Ether NO NO u 0011
Chloroprene NO NO u 0012
ds-12-0ich loroethylene NO NO u OD18
Bromochloromethane NO NO u 0014
Chloroform NO ND u 0014
Ethyl tert-Butyl Ether NO NO u 0011
12-Dichloroethane 0019 008 0016
111-Trichloroethane 0012 007 u 0020
Benzene 0344 L10 0061 Carbon Tetrachloride 0088 056 0024
tert-Amyl Methyl Ether NO NO u 0016
12-0ichloropropane ND NO u 0019
Ethyl Acrylate ND NO u 0014
Bromodichloromethane ND NO u 0021
Trichloroethylene NO ND u 0022
Methyl Methacrylate ND NO u 0025
ds-13-0ichloropropene NO NO u 0015
Methyl Isobutyl Ketone 0015 oo6 0015
trans-13-0ichloropropene NO ND u 0016
112-Trichloroethane NO NO u 0021
Toluene 0416 157 0045
Oibromochloromethane ND NO u 0018
12-0ibromoethane ND NO u 0017
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551 -5000
FILE 027800001030
REPORTED 0312 12 1051
SUBMITTED 030512
AQS SITE CODE
SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 Bwdtl MJlL
Analvte Jmbll Y9Lm Big Jmbx nmiddotOclane 0039 018 0020 Tetrachloroethylene 0005 003 u 0020
Chlorobenzene ND ND u 0025
Ethylbenzene 0045 020 0023 mp-Xylene 0112 OA9 0037 Bromoform ND ND u 0020
Styrene 0030 013 0024 1122-Tetrachloroethane ND ND u 0018
o-Xylene 0050 022 0020
135-Trimethylbenzene 0019 009 u 0022
124-Trimethylbenzene 0047 023 0025 m-Dichlorobenzene ND ND u 0024
p-Dichlorobenzene 0004 002 u 0019
a-Dichlorobenzene NO ND u 0021
124-Trichlorobenzene ND ND u 0022
Hexachloro-13-butadiene ND ND u 0022
Eastern Research Group The results in this report apply only 1o the samples analyzed in accordance with the chain of custody document This analytical rep ort must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 031212 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wilh the chain of custody document This analytical report must be reproduced in its enrirety
Page 5 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 03121121051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report nutst be reproduced in its entirety
Page 6 of 6
CERTIFICATE OF ANALYSIS~RG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 66101 SUBMITTED 12061 1
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPDIAnalyte Result Units Result RPD um1t Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 5 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 661 01 SUBMITTED 120611
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its enJirety
Page 6 of 6
i
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
March 12 2012
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 030512 0916
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for UATMP NATTS CSATAM PAMS and NMOC support (US EPA Contract No 68-D-Q9-048) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Program Manager lauravanenwyckergcom
The information contained in this report and its attachmcnt(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauravanenwyckergcom and delete the report dthout retaining any copies
Page 1 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 0312112 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
6th St between Central amp 2030501-01 Air 030212 0000 030512 0916 Malcom
Eastern Research Group The results in this report apply only to the samples anal zed in accordance With the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Aven ue REPORTED 031212 1 051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 ~ tml
Analvte RRbll Y9lD1 flu RRbll Acetylene 0627 067 0072 Propylene 0484 084 0033
Dichlorodllluoromethane 0500 248 0023 Chloromethane 0557 115 0033
Dichlorotetrafluoroethane 0015 011 0012 Vinyl chloride NO NO u 0011
13-Butadlene 0036 oo8 0011
Bromomethane 0012 005 0012 Chloroethane NO NO u 0017
Acetonitrile 0073 012 0073
Trichlorofluoromethane 0258 145 0015 Acrylonitrile NO NO u 0020
11-0ichloroethene NO NO u 0014
Dichloromethane 0185 064 0023
Carbon Disulfide 0037 012 0014 Trichlorobitluoroethane 0119 091 0017
trans-12-0ichloroethylene NO NO u 0012
11-0ichloroethane NO NO u 0015
Methyl tert-Butyl Ether NO NO u 0011
Chloroprene NO NO u 0012
ds-12-0ich loroethylene NO NO u OD18
Bromochloromethane NO NO u 0014
Chloroform NO ND u 0014
Ethyl tert-Butyl Ether NO NO u 0011
12-Dichloroethane 0019 008 0016
111-Trichloroethane 0012 007 u 0020
Benzene 0344 L10 0061 Carbon Tetrachloride 0088 056 0024
tert-Amyl Methyl Ether NO NO u 0016
12-0ichloropropane ND NO u 0019
Ethyl Acrylate ND NO u 0014
Bromodichloromethane ND NO u 0021
Trichloroethylene NO ND u 0022
Methyl Methacrylate ND NO u 0025
ds-13-0ichloropropene NO NO u 0015
Methyl Isobutyl Ketone 0015 oo6 0015
trans-13-0ichloropropene NO ND u 0016
112-Trichloroethane NO NO u 0021
Toluene 0416 157 0045
Oibromochloromethane ND NO u 0018
12-0ibromoethane ND NO u 0017
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551 -5000
FILE 027800001030
REPORTED 0312 12 1051
SUBMITTED 030512
AQS SITE CODE
SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 Bwdtl MJlL
Analvte Jmbll Y9Lm Big Jmbx nmiddotOclane 0039 018 0020 Tetrachloroethylene 0005 003 u 0020
Chlorobenzene ND ND u 0025
Ethylbenzene 0045 020 0023 mp-Xylene 0112 OA9 0037 Bromoform ND ND u 0020
Styrene 0030 013 0024 1122-Tetrachloroethane ND ND u 0018
o-Xylene 0050 022 0020
135-Trimethylbenzene 0019 009 u 0022
124-Trimethylbenzene 0047 023 0025 m-Dichlorobenzene ND ND u 0024
p-Dichlorobenzene 0004 002 u 0019
a-Dichlorobenzene NO ND u 0021
124-Trichlorobenzene ND ND u 0022
Hexachloro-13-butadiene ND ND u 0022
Eastern Research Group The results in this report apply only 1o the samples analyzed in accordance with the chain of custody document This analytical rep ort must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 031212 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wilh the chain of custody document This analytical report must be reproduced in its enrirety
Page 5 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 03121121051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report nutst be reproduced in its entirety
Page 6 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 1215111041
Kansas City KS 661 01 SUBMITTED 120611
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its enJirety
Page 6 of 6
i
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
March 12 2012
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 030512 0916
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for UATMP NATTS CSATAM PAMS and NMOC support (US EPA Contract No 68-D-Q9-048) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Program Manager lauravanenwyckergcom
The information contained in this report and its attachmcnt(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauravanenwyckergcom and delete the report dthout retaining any copies
Page 1 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 0312112 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
6th St between Central amp 2030501-01 Air 030212 0000 030512 0916 Malcom
Eastern Research Group The results in this report apply only to the samples anal zed in accordance With the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Aven ue REPORTED 031212 1 051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 ~ tml
Analvte RRbll Y9lD1 flu RRbll Acetylene 0627 067 0072 Propylene 0484 084 0033
Dichlorodllluoromethane 0500 248 0023 Chloromethane 0557 115 0033
Dichlorotetrafluoroethane 0015 011 0012 Vinyl chloride NO NO u 0011
13-Butadlene 0036 oo8 0011
Bromomethane 0012 005 0012 Chloroethane NO NO u 0017
Acetonitrile 0073 012 0073
Trichlorofluoromethane 0258 145 0015 Acrylonitrile NO NO u 0020
11-0ichloroethene NO NO u 0014
Dichloromethane 0185 064 0023
Carbon Disulfide 0037 012 0014 Trichlorobitluoroethane 0119 091 0017
trans-12-0ichloroethylene NO NO u 0012
11-0ichloroethane NO NO u 0015
Methyl tert-Butyl Ether NO NO u 0011
Chloroprene NO NO u 0012
ds-12-0ich loroethylene NO NO u OD18
Bromochloromethane NO NO u 0014
Chloroform NO ND u 0014
Ethyl tert-Butyl Ether NO NO u 0011
12-Dichloroethane 0019 008 0016
111-Trichloroethane 0012 007 u 0020
Benzene 0344 L10 0061 Carbon Tetrachloride 0088 056 0024
tert-Amyl Methyl Ether NO NO u 0016
12-0ichloropropane ND NO u 0019
Ethyl Acrylate ND NO u 0014
Bromodichloromethane ND NO u 0021
Trichloroethylene NO ND u 0022
Methyl Methacrylate ND NO u 0025
ds-13-0ichloropropene NO NO u 0015
Methyl Isobutyl Ketone 0015 oo6 0015
trans-13-0ichloropropene NO ND u 0016
112-Trichloroethane NO NO u 0021
Toluene 0416 157 0045
Oibromochloromethane ND NO u 0018
12-0ibromoethane ND NO u 0017
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551 -5000
FILE 027800001030
REPORTED 0312 12 1051
SUBMITTED 030512
AQS SITE CODE
SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 Bwdtl MJlL
Analvte Jmbll Y9Lm Big Jmbx nmiddotOclane 0039 018 0020 Tetrachloroethylene 0005 003 u 0020
Chlorobenzene ND ND u 0025
Ethylbenzene 0045 020 0023 mp-Xylene 0112 OA9 0037 Bromoform ND ND u 0020
Styrene 0030 013 0024 1122-Tetrachloroethane ND ND u 0018
o-Xylene 0050 022 0020
135-Trimethylbenzene 0019 009 u 0022
124-Trimethylbenzene 0047 023 0025 m-Dichlorobenzene ND ND u 0024
p-Dichlorobenzene 0004 002 u 0019
a-Dichlorobenzene NO ND u 0021
124-Trichlorobenzene ND ND u 0022
Hexachloro-13-butadiene ND ND u 0022
Eastern Research Group The results in this report apply only 1o the samples analyzed in accordance with the chain of custody document This analytical rep ort must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 031212 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wilh the chain of custody document This analytical report must be reproduced in its enrirety
Page 5 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 03121121051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report nutst be reproduced in its entirety
Page 6 of 6
Eastern Research Group 601 Keystone Park Drive Suite 700 Morrisville NC 27560
March 12 2012
Michael F Davis EPA Region VII 300 Minnesota Avenue Kansas City KS 66101 Project Name OECA work
Dear Michael F Davis
This report oontains the analytical results for the sample(s) received under chain(s) of custody by Eastern Research Group on 030512 0916
The test results in this report are in compliance with NELAC accreditation requirements for the certified parameters All analyses were performed as described in the US EPA-approved QAPP under the oontract for UATMP NATTS CSATAM PAMS and NMOC support (US EPA Contract No 68-D-Q9-048) This cover page is an integral part of this report and any exceptions or comments are noted on the last page
The issuance of the final Certificate of Analysis takes precedence over any previous Report If you have any questions please contact me at 919-468-7930
Sincerely
Laura Van Enwyck Program Manager lauravanenwyckergcom
The information contained in this report and its attachmcnt(s) are intended only for the use of the individual to whom it is addressed and may contain information that is privileged confidential or exempt from disclosure If the reader of this message is not the intended recipient you are hereby notified that any dissemination distribution or copying of this report is strictly prohibited If you have received this report in error please notify lauravanenwyckergcom and delete the report dthout retaining any copies
Page 1 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 0312112 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
6th St between Central amp 2030501-01 Air 030212 0000 030512 0916 Malcom
Eastern Research Group The results in this report apply only to the samples anal zed in accordance With the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Aven ue REPORTED 031212 1 051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 ~ tml
Analvte RRbll Y9lD1 flu RRbll Acetylene 0627 067 0072 Propylene 0484 084 0033
Dichlorodllluoromethane 0500 248 0023 Chloromethane 0557 115 0033
Dichlorotetrafluoroethane 0015 011 0012 Vinyl chloride NO NO u 0011
13-Butadlene 0036 oo8 0011
Bromomethane 0012 005 0012 Chloroethane NO NO u 0017
Acetonitrile 0073 012 0073
Trichlorofluoromethane 0258 145 0015 Acrylonitrile NO NO u 0020
11-0ichloroethene NO NO u 0014
Dichloromethane 0185 064 0023
Carbon Disulfide 0037 012 0014 Trichlorobitluoroethane 0119 091 0017
trans-12-0ichloroethylene NO NO u 0012
11-0ichloroethane NO NO u 0015
Methyl tert-Butyl Ether NO NO u 0011
Chloroprene NO NO u 0012
ds-12-0ich loroethylene NO NO u OD18
Bromochloromethane NO NO u 0014
Chloroform NO ND u 0014
Ethyl tert-Butyl Ether NO NO u 0011
12-Dichloroethane 0019 008 0016
111-Trichloroethane 0012 007 u 0020
Benzene 0344 L10 0061 Carbon Tetrachloride 0088 056 0024
tert-Amyl Methyl Ether NO NO u 0016
12-0ichloropropane ND NO u 0019
Ethyl Acrylate ND NO u 0014
Bromodichloromethane ND NO u 0021
Trichloroethylene NO ND u 0022
Methyl Methacrylate ND NO u 0025
ds-13-0ichloropropene NO NO u 0015
Methyl Isobutyl Ketone 0015 oo6 0015
trans-13-0ichloropropene NO ND u 0016
112-Trichloroethane NO NO u 0021
Toluene 0416 157 0045
Oibromochloromethane ND NO u 0018
12-0ibromoethane ND NO u 0017
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551 -5000
FILE 027800001030
REPORTED 0312 12 1051
SUBMITTED 030512
AQS SITE CODE
SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 Bwdtl MJlL
Analvte Jmbll Y9Lm Big Jmbx nmiddotOclane 0039 018 0020 Tetrachloroethylene 0005 003 u 0020
Chlorobenzene ND ND u 0025
Ethylbenzene 0045 020 0023 mp-Xylene 0112 OA9 0037 Bromoform ND ND u 0020
Styrene 0030 013 0024 1122-Tetrachloroethane ND ND u 0018
o-Xylene 0050 022 0020
135-Trimethylbenzene 0019 009 u 0022
124-Trimethylbenzene 0047 023 0025 m-Dichlorobenzene ND ND u 0024
p-Dichlorobenzene 0004 002 u 0019
a-Dichlorobenzene NO ND u 0021
124-Trichlorobenzene ND ND u 0022
Hexachloro-13-butadiene ND ND u 0022
Eastern Research Group The results in this report apply only 1o the samples analyzed in accordance with the chain of custody document This analytical rep ort must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 031212 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wilh the chain of custody document This analytical report must be reproduced in its enrirety
Page 5 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 03121121051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report nutst be reproduced in its entirety
Page 6 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001 030
300 Minnesota Avenue REPORTED 0312112 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
ANALYTICAL REPORT FOR SAMPLES
SampleName LabNumber Matrix Sampled Received
6th St between Central amp 2030501-01 Air 030212 0000 030512 0916 Malcom
Eastern Research Group The results in this report apply only to the samples anal zed in accordance With the chain of custody document This analytical report must be reproduced in its entirety
Page 2 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Aven ue REPORTED 031212 1 051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 ~ tml
Analvte RRbll Y9lD1 flu RRbll Acetylene 0627 067 0072 Propylene 0484 084 0033
Dichlorodllluoromethane 0500 248 0023 Chloromethane 0557 115 0033
Dichlorotetrafluoroethane 0015 011 0012 Vinyl chloride NO NO u 0011
13-Butadlene 0036 oo8 0011
Bromomethane 0012 005 0012 Chloroethane NO NO u 0017
Acetonitrile 0073 012 0073
Trichlorofluoromethane 0258 145 0015 Acrylonitrile NO NO u 0020
11-0ichloroethene NO NO u 0014
Dichloromethane 0185 064 0023
Carbon Disulfide 0037 012 0014 Trichlorobitluoroethane 0119 091 0017
trans-12-0ichloroethylene NO NO u 0012
11-0ichloroethane NO NO u 0015
Methyl tert-Butyl Ether NO NO u 0011
Chloroprene NO NO u 0012
ds-12-0ich loroethylene NO NO u OD18
Bromochloromethane NO NO u 0014
Chloroform NO ND u 0014
Ethyl tert-Butyl Ether NO NO u 0011
12-Dichloroethane 0019 008 0016
111-Trichloroethane 0012 007 u 0020
Benzene 0344 L10 0061 Carbon Tetrachloride 0088 056 0024
tert-Amyl Methyl Ether NO NO u 0016
12-0ichloropropane ND NO u 0019
Ethyl Acrylate ND NO u 0014
Bromodichloromethane ND NO u 0021
Trichloroethylene NO ND u 0022
Methyl Methacrylate ND NO u 0025
ds-13-0ichloropropene NO NO u 0015
Methyl Isobutyl Ketone 0015 oo6 0015
trans-13-0ichloropropene NO ND u 0016
112-Trichloroethane NO NO u 0021
Toluene 0416 157 0045
Oibromochloromethane ND NO u 0018
12-0ibromoethane ND NO u 0017
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551 -5000
FILE 027800001030
REPORTED 0312 12 1051
SUBMITTED 030512
AQS SITE CODE
SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 Bwdtl MJlL
Analvte Jmbll Y9Lm Big Jmbx nmiddotOclane 0039 018 0020 Tetrachloroethylene 0005 003 u 0020
Chlorobenzene ND ND u 0025
Ethylbenzene 0045 020 0023 mp-Xylene 0112 OA9 0037 Bromoform ND ND u 0020
Styrene 0030 013 0024 1122-Tetrachloroethane ND ND u 0018
o-Xylene 0050 022 0020
135-Trimethylbenzene 0019 009 u 0022
124-Trimethylbenzene 0047 023 0025 m-Dichlorobenzene ND ND u 0024
p-Dichlorobenzene 0004 002 u 0019
a-Dichlorobenzene NO ND u 0021
124-Trichlorobenzene ND ND u 0022
Hexachloro-13-butadiene ND ND u 0022
Eastern Research Group The results in this report apply only 1o the samples analyzed in accordance with the chain of custody document This analytical rep ort must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 031212 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wilh the chain of custody document This analytical report must be reproduced in its enrirety
Page 5 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 03121121051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report nutst be reproduced in its entirety
Page 6 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Aven ue REPORTED 031212 1 051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 ~ tml
Analvte RRbll Y9lD1 flu RRbll Acetylene 0627 067 0072 Propylene 0484 084 0033
Dichlorodllluoromethane 0500 248 0023 Chloromethane 0557 115 0033
Dichlorotetrafluoroethane 0015 011 0012 Vinyl chloride NO NO u 0011
13-Butadlene 0036 oo8 0011
Bromomethane 0012 005 0012 Chloroethane NO NO u 0017
Acetonitrile 0073 012 0073
Trichlorofluoromethane 0258 145 0015 Acrylonitrile NO NO u 0020
11-0ichloroethene NO NO u 0014
Dichloromethane 0185 064 0023
Carbon Disulfide 0037 012 0014 Trichlorobitluoroethane 0119 091 0017
trans-12-0ichloroethylene NO NO u 0012
11-0ichloroethane NO NO u 0015
Methyl tert-Butyl Ether NO NO u 0011
Chloroprene NO NO u 0012
ds-12-0ich loroethylene NO NO u OD18
Bromochloromethane NO NO u 0014
Chloroform NO ND u 0014
Ethyl tert-Butyl Ether NO NO u 0011
12-Dichloroethane 0019 008 0016
111-Trichloroethane 0012 007 u 0020
Benzene 0344 L10 0061 Carbon Tetrachloride 0088 056 0024
tert-Amyl Methyl Ether NO NO u 0016
12-0ichloropropane ND NO u 0019
Ethyl Acrylate ND NO u 0014
Bromodichloromethane ND NO u 0021
Trichloroethylene NO ND u 0022
Methyl Methacrylate ND NO u 0025
ds-13-0ichloropropene NO NO u 0015
Methyl Isobutyl Ketone 0015 oo6 0015
trans-13-0ichloropropene NO ND u 0016
112-Trichloroethane NO NO u 0021
Toluene 0416 157 0045
Oibromochloromethane ND NO u 0018
12-0ibromoethane ND NO u 0017
Eastern Research Group The results in this report apply only to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety
Page 3 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551 -5000
FILE 027800001030
REPORTED 0312 12 1051
SUBMITTED 030512
AQS SITE CODE
SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 Bwdtl MJlL
Analvte Jmbll Y9Lm Big Jmbx nmiddotOclane 0039 018 0020 Tetrachloroethylene 0005 003 u 0020
Chlorobenzene ND ND u 0025
Ethylbenzene 0045 020 0023 mp-Xylene 0112 OA9 0037 Bromoform ND ND u 0020
Styrene 0030 013 0024 1122-Tetrachloroethane ND ND u 0018
o-Xylene 0050 022 0020
135-Trimethylbenzene 0019 009 u 0022
124-Trimethylbenzene 0047 023 0025 m-Dichlorobenzene ND ND u 0024
p-Dichlorobenzene 0004 002 u 0019
a-Dichlorobenzene NO ND u 0021
124-Trichlorobenzene ND ND u 0022
Hexachloro-13-butadiene ND ND u 0022
Eastern Research Group The results in this report apply only 1o the samples analyzed in accordance with the chain of custody document This analytical rep ort must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 031212 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wilh the chain of custody document This analytical report must be reproduced in its enrirety
Page 5 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 03121121051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report nutst be reproduced in its entirety
Page 6 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII
300 Minnesota Avenue
Kansas City KS 66101
ATTN Michael F Davis
PHONE (913) 551-5042 FAX (913) 551 -5000
FILE 027800001030
REPORTED 0312 12 1051
SUBMITTED 030512
AQS SITE CODE
SITE CODE OECAwork
Desaiption 6th St between Central amp Malcom Lab ID 2030501-01 Sampled 030212 0000
Pressure Receipt 85 Hg Canister 090 Received 030512 0916
Comments Analyzed 030512 1542
Air Toxics by EPA Compendium Method T0-15 Bwdtl MJlL
Analvte Jmbll Y9Lm Big Jmbx nmiddotOclane 0039 018 0020 Tetrachloroethylene 0005 003 u 0020
Chlorobenzene ND ND u 0025
Ethylbenzene 0045 020 0023 mp-Xylene 0112 OA9 0037 Bromoform ND ND u 0020
Styrene 0030 013 0024 1122-Tetrachloroethane ND ND u 0018
o-Xylene 0050 022 0020
135-Trimethylbenzene 0019 009 u 0022
124-Trimethylbenzene 0047 023 0025 m-Dichlorobenzene ND ND u 0024
p-Dichlorobenzene 0004 002 u 0019
a-Dichlorobenzene NO ND u 0021
124-Trichlorobenzene ND ND u 0022
Hexachloro-13-butadiene ND ND u 0022
Eastern Research Group The results in this report apply only 1o the samples analyzed in accordance with the chain of custody document This analytical rep ort must be reproduced in its entirety
Page 4 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 031212 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wilh the chain of custody document This analytical report must be reproduced in its enrirety
Page 5 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 03121121051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report nutst be reproduced in its entirety
Page 6 of 6
CERTIFICATE OF ANALYSIS
EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 031212 1051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Source RPD Analyte Result Units Result RPD Umit Notes
Eastern Research Group The results in this report apply only to the samples analyzed in accordance wilh the chain of custody document This analytical report must be reproduced in its enrirety
Page 5 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 03121121051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report nutst be reproduced in its entirety
Page 6 of 6
CERTIFICATE OF ANALYSIS -ERG EPA Region VII FILE 027800001030
300 Minnesota Avenue REPORTED 03121121051
Kansas City KS 66101 SUBMITTED 030512
ATTN Michael F Davis AQS SITE CODE
PHONE (913) 551-5042 FAX (913) 551-5000 SITE CODE OECAwork
Notes and Definitions
U Under Detection Limit
ND Analyte NOT DETECTED at or above the Method Detection Limit (MDL)
NR Not Reported
MDL Method Detection Limit
RPD Relative Percent Difference
Eastern Research Group The results in this report apply only t o the samples analyzed in accordance with the chain of custody document This analytical report nutst be reproduced in its entirety
Page 6 of 6