certificate of analysis...extracts/digestion dilution and/or insuffient sample amount for analysis....

CERTIFICATE OF ANALYSIS

BUTLER PARTNERS PTY LTD 1 of 6 Page :Laboratory :Client : ALS Environmental Brisbane

Contact :

Address :

Contact :

Address :P O BOX 2267 FORTITUDE VALLEY BC QLD

AUSTRALIA 4006

:MR LUKE AMIES Michael Heery EB060764032 Shand Street Stafford QLD Australia 4053

Work Order

E-mail : E-mail :[email protected] [email protected]

Telephone :

Facsimile :

Telephone :

Facsimile :

07 3852 3800 +61 (07) 3243 7222

07 3852 3808 +61 (07) 3243 7259

7 Aug 2006BN/217/06Quote number :06155BProject :

LA92Order number :

- Not provided -C-O-C number :

- Not provided -Site : Analysed :

Received :

13

15No. of samples -

23 Aug 2006Date issued :

Date received :

ALSE - Excellence in Analytical Testing

NATA Accredited Laboratory

825

This document is issued in

accordance with NATA's

accreditation requirements.

Accredited for compliance with

ISO/IEC 17025.

This document has been electronically signed by those names that appear on this report and are the authorised signatories. Electronic

signing has been carried out in compliance with procedures specified in 21 CFR Part 11.

Signatory DepartmentPosition

Carsten Emrich Organics - NATA 825 (818 - Brisbane)Senior Organic Chemist

Stephen Hislop Inorganics - NATA 825 (818 - Brisbane)Senior Inorganic Chemist

BUTLER PARTNERS PTY LTDClient :

EB0607640

2 of 6 Page Number :

:Work Order

CommentsThis report for the ALSE reference EB0607640 supersedes any previous reports with this reference. Results apply to the samples as submitted. All pages of this report have been checked and

approved for release.

This report contains the following information:

l Analytical results for samples submitted

When moisture determination has been performed, results are reported on a dry weight basis. When a reported 'less than' result is higher than the LOR, this may be due to primary sample

extracts/digestion dilution and/or insuffient sample amount for analysis. Surrogate Recovery Limits are static and based on USEPA SW846 or ALS-QWI/EN38 (in the absence of specified

USEPA limits). Where LOR of reported result differ from standard LOR, this may be due to high moisture, reduced sample amount or matrix interference. When date(s) and/or time(s) are

shown bracketed, these have been assumed by the laboratory for process purposes. Abbreviations: CAS number = Chemical Abstract Services number, LOR = Limit of Reporting. * Indicates

failed Surrogate Recoveries.

l Surrogate control limits

The analytical procedures used by ALS Environmental are based on established internationally-recognized procedures such as those published by the US EPA, APHA, AS and NEPM. In house

procedure are employed in the absence of documented standards or by client request. The following report provides brief descriptions of the analytical procedures employed for results reported

herein. Reference methods from which ALSE methods are based are provided in parenthesis.

Specific comments for Work Order EB0607640

Samples DUP7 and DUP 10 were broken in the laboratory prior to metals analysis. These samples can therefore not be reported for metals.

Client : BUTLER PARTNERS PTY LTD

EB0607640


Work Order :

Analytical ResultsDUP5DUP4DUP3DUP2DUP1Client Sample ID :

Sample Matrix Type / Description :

Sample Date / Time :

Laboratory Sample ID :

SOIL

31 Jul 2006

15:00

SOIL

31 Jul 2006

15:00

SOIL

31 Jul 2006

15:00

SOIL

31 Jul 2006

15:00

SOIL

31 Jul 2006

15:00

EB0607640-001 EB0607640-002 EB0607640-003 EB0607640-004 EB0607640-005Analyte CAS number LOR Units

EA055: Moisture Content

31.6 15.7 19.6 24.6 16.4%1.0Moisture Content (dried @ 103°C)

EG005T: Total Metals by ICP-AES

<5 <5 <5 5 <57440-38-2 mg/kg5Arsenic

<1 <1 <1 <1 <17440-43-9 mg/kg1Cadmium

30 32 20 34 407440-47-3 mg/kg2Chromium

27 23 13 32 247440-50-8 mg/kg5Copper

15 14 8 238 107439-92-1 mg/kg5Lead

6 30 7 26 287440-02-0 mg/kg2Nickel

15 73 33 240 577440-66-6 mg/kg5Zinc

EG035T: Total Mercury by FIMS

<0.1 <0.1 <0.1 0.2 <0.17439-97-6 mg/kg0.1Mercury

EP068A: Organochlorine Pesticides (OC)

---- ---- <0.05 ---- ----319-84-6 mg/kg0.05alpha-BHC

---- ---- <0.05 ---- ----118-74-1 mg/kg0.05Hexachlorobenzene (HCB)

---- ---- <0.05 ---- ----319-85-7 mg/kg0.05beta-BHC

---- ---- <0.05 ---- ----58-89-9 mg/kg0.05gamma-BHC

---- ---- <0.05 ---- ----319-86-8 mg/kg0.05delta-BHC

---- ---- <0.05 ---- ----76-44-8 mg/kg0.05Heptachlor

---- ---- <0.05 ---- ----309-00-2 mg/kg0.05Aldrin

---- ---- <0.05 ---- ----1024-57-3 mg/kg0.05Heptachlor epoxide

---- ---- <0.05 ---- ----5103-74-2 mg/kg0.05trans-Chlordane

---- ---- <0.05 ---- ----959-98-8 mg/kg0.05alpha-Endosulfan

---- ---- <0.05 ---- ----5103-71-9 mg/kg0.05cis-Chlordane

---- ---- <0.05 ---- ----60-57-1 mg/kg0.05Dieldrin

---- ---- <0.05 ---- ----72-55-9 mg/kg0.054.4’-DDE

---- ---- <0.05 ---- ----72-20-8 mg/kg0.05Endrin

---- ---- <0.05 ---- ----33213-65-9 mg/kg0.05beta-Endosulfan

---- ---- <0.05 ---- ----72-54-8 mg/kg0.054.4’-DDD

---- ---- <0.05 ---- ----7421-93-4 mg/kg0.05Endrin aldehyde

---- ---- <0.05 ---- ----1031-07-8 mg/kg0.05Endosulfan sulfate

---- ---- <0.2 ---- ----50-29-3 mg/kg0.24.4’-DDT

---- ---- <0.05 ---- ----53494-70-5 mg/kg0.05Endrin ketone

---- ---- <0.2 ---- ----72-43-5 mg/kg0.2Methoxychlor

EP068S: Organochlorine Pesticide Surrogate

---- ---- 119 ---- ----%0.1Dibromo-DDE

EP068T: Organophosphorus Pesticide Surrogate

---- ---- 102 ---- ----78-48-8 %0.1DEF

A Campbell Brothers Limited Company


EB0607640


Work Order :

Analytical ResultsDUP12DUP11DUP9DUP8DUP6Client Sample ID :




SOIL

31 Jul 2006

15:00

SOIL

31 Jul 2006

15:00

SOIL

31 Jul 2006

15:00

SOIL

1 Aug 2006

15:00

SOIL

1 Aug 2006

15:00

EB0607640-006 EB0607640-008 EB0607640-009 EB0607640-011 EB0607640-012Analyte CAS number LOR Units


17.4 18.3 19.6 13.2 21.0%1.0Moisture Content (dried @ 103°C)


8 <5 <5 <5 <57440-38-2 mg/kg5Arsenic

<1 <1 <1 <1 <17440-43-9 mg/kg1Cadmium

45 35 37 37 317440-47-3 mg/kg2Chromium

41 21 24 22 227440-50-8 mg/kg5Copper

11 11 10 9 147439-92-1 mg/kg5Lead

46 28 31 30 277440-02-0 mg/kg2Nickel

70 60 63 60 607440-66-6 mg/kg5Zinc


<0.1 <0.1 <0.1 <0.1 <0.17439-97-6 mg/kg0.1Mercury


---- <0.05 ---- ---- ----319-84-6 mg/kg0.05alpha-BHC

---- <0.05 ---- ---- ----118-74-1 mg/kg0.05Hexachlorobenzene (HCB)

---- <0.05 ---- ---- ----319-85-7 mg/kg0.05beta-BHC

---- <0.05 ---- ---- ----58-89-9 mg/kg0.05gamma-BHC

---- <0.05 ---- ---- ----319-86-8 mg/kg0.05delta-BHC

---- <0.05 ---- ---- ----76-44-8 mg/kg0.05Heptachlor

---- <0.05 ---- ---- ----309-00-2 mg/kg0.05Aldrin

---- <0.05 ---- ---- ----1024-57-3 mg/kg0.05Heptachlor epoxide

---- <0.05 ---- ---- ----5103-74-2 mg/kg0.05trans-Chlordane

---- <0.05 ---- ---- ----959-98-8 mg/kg0.05alpha-Endosulfan

---- <0.05 ---- ---- ----5103-71-9 mg/kg0.05cis-Chlordane

---- <0.05 ---- ---- ----60-57-1 mg/kg0.05Dieldrin

---- <0.05 ---- ---- ----72-55-9 mg/kg0.054.4’-DDE

---- <0.05 ---- ---- ----72-20-8 mg/kg0.05Endrin

---- <0.05 ---- ---- ----33213-65-9 mg/kg0.05beta-Endosulfan

---- <0.05 ---- ---- ----72-54-8 mg/kg0.054.4’-DDD

---- <0.05 ---- ---- ----7421-93-4 mg/kg0.05Endrin aldehyde

---- <0.05 ---- ---- ----1031-07-8 mg/kg0.05Endosulfan sulfate

---- <0.2 ---- ---- ----50-29-3 mg/kg0.24.4’-DDT

---- <0.05 ---- ---- ----53494-70-5 mg/kg0.05Endrin ketone

---- <0.2 ---- ---- ----72-43-5 mg/kg0.2Methoxychlor


---- 120 ---- ---- ----%0.1Dibromo-DDE


---- 107 ---- ---- ----78-48-8 %0.1DEF



EB0607640


Work Order :

Analytical ResultsDUP16DUP15DUP14Client Sample ID :




SOIL

2 Aug 2006

15:00

SOIL

2 Aug 2006

15:00

SOIL

2 Aug 2006

15:00

EB0607640-013 EB0607640-014 EB0607640-015Analyte CAS number LOR Units


20.4 26.6 15.7%1.0Moisture Content (dried @ 103°C)


<5 6 <57440-38-2 mg/kg5Arsenic

<1 <1 <17440-43-9 mg/kg1Cadmium

31 32 147440-47-3 mg/kg2Chromium

20 27 127440-50-8 mg/kg5Copper

17 24 587439-92-1 mg/kg5Lead

23 22 67440-02-0 mg/kg2Nickel

65 91 677440-66-6 mg/kg5Zinc


<0.1 <0.1 <0.17439-97-6 mg/kg0.1Mercury


---- ---- <0.05319-84-6 mg/kg0.05alpha-BHC

---- ---- <0.05118-74-1 mg/kg0.05Hexachlorobenzene (HCB)

---- ---- <0.05319-85-7 mg/kg0.05beta-BHC

---- ---- <0.0558-89-9 mg/kg0.05gamma-BHC

---- ---- <0.05319-86-8 mg/kg0.05delta-BHC

---- ---- <0.0576-44-8 mg/kg0.05Heptachlor

---- ---- <0.05309-00-2 mg/kg0.05Aldrin

---- ---- <0.051024-57-3 mg/kg0.05Heptachlor epoxide

---- ---- <0.055103-74-2 mg/kg0.05trans-Chlordane

---- ---- <0.05959-98-8 mg/kg0.05alpha-Endosulfan

---- ---- <0.055103-71-9 mg/kg0.05cis-Chlordane

---- ---- <0.0560-57-1 mg/kg0.05Dieldrin

---- ---- <0.0572-55-9 mg/kg0.054.4’-DDE

---- ---- <0.0572-20-8 mg/kg0.05Endrin

---- ---- <0.0533213-65-9 mg/kg0.05beta-Endosulfan

---- ---- <0.0572-54-8 mg/kg0.054.4’-DDD

---- ---- <0.057421-93-4 mg/kg0.05Endrin aldehyde

---- ---- <0.051031-07-8 mg/kg0.05Endosulfan sulfate

---- ---- <0.250-29-3 mg/kg0.24.4’-DDT

---- ---- <0.0553494-70-5 mg/kg0.05Endrin ketone

---- ---- <0.272-43-5 mg/kg0.2Methoxychlor


---- ---- 123%0.1Dibromo-DDE


---- ---- 99.778-48-8 %0.1DEF



EB0607640


Work Order :

Surrogate Control Limits

Surrogate Control LimitsMatrix Type: SOIL - Surrogate Control Limits

Upper LimitLower LimitAnalyte nameMethod name

EP068: Pesticides by GCMS

EP068S: Organochlorine Pesticide Surrogate 10 136Dibromo-DDE

EP068T: Organophosphorus Pesticide Surrogate 10 110DEF

A Campbell Brothers Limited CompanyReport version : COANA 3.02

QUALITY CONTROL REPORT

1 of 9 Page :Laboratory :Client : ALS Environmental BrisbaneBUTLER PARTNERS PTY LTD

Contact :

Address :

Contact :

Address : Work order :

Amendment No. :

MR LUKE AMIES

32 Shand Street Stafford

QLD Australia 4053EB0607640

Michael Heery

P O BOX 2267 FORTITUDE VALLEY BC

QLD AUSTRALIA 4006

7 Aug 2006BN/217/06Quote number :06155B Date received :Project :

Date issued :LA92Order number :

C-O-C number : - Not provided -

- Not provided -Site :

[email protected] E-mail :E-mail :

07 3852 3800 Telephone :Telephone :

07 3852 3808 Facsimile :Facsimile : Analysed :

Received :

No. of samples

23 Aug 2006

[email protected]

+61 (07) 3243 7222

+61 (07) 3243 7259

15

13

Results apply to the samples as submitted. All pages of this report have been checked and approved for release.


l Laboratory Duplicates (DUP); Relative Percentage Difference (RPD) and Acceptance Limits

l Method Blank (MB) and Laboratory Control Samples (LCS); Recovery and Acceptance Limits

l Matrix Spikes (MS); Recovery and Acceptance Limits

This final report for the ALSE work order reference EB0607640 supersedes any previous reports with this reference.

Work order specific comments

Samples DUP7 and DUP 10 were broken in the laboratory prior to metals analysis. These samples can therefore not be reported for metals.


NATA Accredited Laboratory - 825 This document has been electronically signed by those names that appear on this report and are the authorised signatories. Electronic

signing has been carried out in compliance with procedures specified in 21 CFR Part 11.

Signatory Department

Carsten Emrich Organics - NATA 825 (818 - Brisbane)

Stephen Hislop Inorganics - NATA 825 (818 - Brisbane)


accordance with NATA's


Accredited for compliance

with ISO/IED 17025

Project :

Client : Work Order :

ALS Quote Reference :

Page Number :

Issue Date :

2 of 9

06155B BN/217/06 23 Aug 2006

BUTLER PARTNERS PTY LTD EB0607640

Quality Control Report - Laboratory Duplicates (DUP)The quality control term Laboratory Duplicate refers to an intralaboratory split sample randomly selected from the sample batch. Laboratory duplicates provide information on method precision and sample heterogeneity.

- Anonymous - Client Sample IDs refer to samples which are not specifically part of this work order but formed part of the QC process lot. Abbreviations: LOR = Limit of Reporting, RPD = Relative Percent Difference.

* Indicates failed QC. The permitted ranges for the RPD of Laboratory Duplicates (relative percent deviation) are specified in ALS Method QWI-EN/38 and are dependent on the magnitude of results in comparison to the level

of reporting:- Result < 10 times LOR, no limit - Result between 10 and 20 times LOR, 0% - 50% - Result > 20 times LOR, 0% - 20%

Matrix Type: SOIL Laboratory Duplicates (DUP) Report

LOR RPDDuplicate ResultOriginal ResultAnalyte nameClient Sample IDLaboratory Sample ID


%EA055: Moisture Content - ( QC Lot: 255136 ) % %

1.0 % 0.424.6Moisture Content (dried @ 103°C)EB0607640-004 DUP4 24.7

1.0 % 1.313.2Moisture Content (dried @ 103°C)EB0607640-011 DUP11 13.4


%EG005T: Total Metals by ICP-AES - ( QC Lot: 255845 ) mg/kg mg/kg

5 mg/kg 0.0<5ArsenicEB0607640-009 DUP9 <5

1 mg/kg 0.0<1Cadmium <1

2 mg/kg 2.837Chromium 36

5 mg/kg 0.024Copper 24

5 mg/kg 0.010Lead 10

2 mg/kg 0.031Nickel 31

5 mg/kg 0.063Zinc 62


%EG035T: Total Mercury by FIMS - ( QC Lot: 255846 ) mg/kg mg/kg

0.1 mg/kg 0.0<0.1MercuryEB0607640-009 DUP9 <0.1


%EP068A: Organochlorine Pesticides (OC) - ( QC Lot: 255141 ) mg/kg mg/kg

0.05 mg/kg 0.0<0.05alpha-BHCEB0607614-001 Anonymous <0.05

0.05 mg/kg 0.0<0.05Hexachlorobenzene (HCB) <0.05

0.05 mg/kg 0.0<0.05beta-BHC <0.05

0.05 mg/kg 0.0<0.05gamma-BHC <0.05

0.05 mg/kg 0.0<0.05delta-BHC <0.05

0.05 mg/kg 0.0<0.05Heptachlor <0.05

0.05 mg/kg 0.0<0.05Aldrin <0.05

0.05 mg/kg 0.0<0.05Heptachlor epoxide <0.05

0.05 mg/kg 0.0<0.05trans-Chlordane <0.05


Project :



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Issue Date :

3 of 9

06155B BN/217/06 23 Aug 2006




EP068A: Organochlorine Pesticides (OC) - continued

%mg/kg mg/kgEP068A: Organochlorine Pesticides (OC) - ( QC Lot: 255141 ) - continued

0.05 mg/kg 0.0<0.05alpha-EndosulfanEB0607614-001 Anonymous <0.05

0.05 mg/kg 0.0<0.05cis-Chlordane <0.05

0.05 mg/kg 0.0<0.05Dieldrin <0.05

0.05 mg/kg 0.0<0.054,4’-DDE <0.05

0.05 mg/kg 0.0<0.05Endrin <0.05

0.05 mg/kg 0.0<0.05beta-Endosulfan <0.05

0.05 mg/kg 0.0<0.054,4’-DDD <0.05

0.05 mg/kg 0.0<0.05Endrin aldehyde <0.05

0.05 mg/kg 0.0<0.05Endosulfan sulfate <0.05

0.2 mg/kg 0.0<0.24,4’-DDT <0.2

0.05 mg/kg 0.0<0.05Endrin ketone <0.05

0.2 mg/kg 0.0<0.2Methoxychlor <0.2

0.05 mg/kg 0.0<0.05alpha-BHCEB0607692-003 Anonymous <0.05

0.05 mg/kg 0.0<0.05Hexachlorobenzene (HCB) <0.05

0.05 mg/kg 0.0<0.05beta-BHC <0.05

0.05 mg/kg 0.0<0.05gamma-BHC <0.05

0.05 mg/kg 0.0<0.05delta-BHC <0.05

0.05 mg/kg 0.0<0.05Heptachlor <0.05

0.05 mg/kg 0.0<0.05Aldrin <0.05

0.05 mg/kg 0.0<0.05Heptachlor epoxide <0.05

0.05 mg/kg 0.0<0.05trans-Chlordane <0.05

0.05 mg/kg 0.0<0.05alpha-Endosulfan <0.05

0.05 mg/kg 0.0<0.05cis-Chlordane <0.05

0.05 mg/kg 0.0<0.05Dieldrin <0.05

0.05 mg/kg 0.0<0.054,4’-DDE <0.05

0.05 mg/kg 0.0<0.05Endrin <0.05

0.05 mg/kg 0.0<0.05beta-Endosulfan <0.05

0.05 mg/kg 0.0<0.054,4’-DDD <0.05

0.05 mg/kg 0.0<0.05Endrin aldehyde <0.05


Project :



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06155B BN/217/06 23 Aug 2006





%mg/kg mg/kgEP068A: Organochlorine Pesticides (OC) - ( QC Lot: 255141 ) - continued

0.05 mg/kg 0.0<0.05Endosulfan sulfateEB0607692-003 Anonymous <0.05

0.2 mg/kg 0.0<0.24,4’-DDT <0.2

0.05 mg/kg 0.0<0.05Endrin ketone <0.05

0.2 mg/kg 0.0<0.2Methoxychlor <0.2


Project :



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06155B BN/217/06 23 Aug 2006


Quality Control Report - Method Blank (MB) and Laboratory Control Samples (LCS)

The quality control term Method / Laboratory Blank refers to an analyte free matrix to which all reagents are added in the same volumes or proportions as used in standard sample preparation. The purpose of this QC type is

to monitor potential laboratory contamination. The quality control term Laboratory Control Sample (LCS) refers to a known, interference free matrix spiked with target analytes or certified reference material. The purpose of

this QC type is to monitor method precision and accuracy independent of sample matrix. Dynamic Recovery Limits are based on statistical evaluation of actual laboratory data. Abbreviations: LOR = Limit of reporting.

Matrix Type: SOIL Method Blank (MB) and Laboratory Control Samples (LCS) Report

Analyte name Low

Recovery Limits

Dynamic Recovery Limits

(% Recovery) HighLCS

Spike Recovery

Actual Results

Spike concentration

Method

blank

result

LOR


EG005T: Total Metals by ICP-AES - ( QC Lot: 255845 ) mg/kg mg/kg %%%

5 mg/kg ---- 70 130105Arsenic 13.8

5 mg/kg <5 ---- ------------

1 mg/kg ---- 70 130108Cadmium 2.82

1 mg/kg <1 ---- ------------

2 mg/kg ---- 70 130114Chromium 61.6

2 mg/kg <2 ---- ------------

5 mg/kg ---- 70 130117Copper 54.7

5 mg/kg <5 ---- ------------

5 mg/kg <5 ---- --------Lead ----

5 mg/kg ---- 70 13011355.5

2 mg/kg ---- 70 130118Nickel 55.1

2 mg/kg <2 ---- ------------

5 mg/kg <5 ---- --------Zinc ----

5 mg/kg ---- 70 130114105


EG035T: Total Mercury by FIMS - ( QC Lot: 255846 ) mg/kg mg/kg %%%

0.10 mg/kg ---- 70 13086.4Mercury 1.34

0.1 mg/kg <0.1 ---- ------------


EP068A: Organochlorine Pesticides (OC) - ( QC Lot: 255141 ) mg/kg mg/kg %%%

0.05 mg/kg <0.05 ---- --------4,4’-DDD ----

0.025 mg/kg ---- 61 12288.40.25

0.025 mg/kg ---- 63 12195.74,4’-DDE 0.25

0.05 mg/kg <0.05 ---- ------------


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06155B BN/217/06 23 Aug 2006



Analyte name Low

Recovery Limits



Spike Recovery

Actual Results

Spike concentration

Method

blank

result

LOR


mg/kg mg/kg %%%EP068A: Organochlorine Pesticides (OC) - ( QC Lot: 255141 ) - continued

0.2 mg/kg <0.2 ---- --------4,4’-DDT ----

0.025 mg/kg ---- 40 12689.20.25

0.025 mg/kg ---- 73 11194.4Aldrin 0.25

0.05 mg/kg <0.05 ---- ------------

0.025 mg/kg ---- 69 112103alpha-BHC 0.25

0.05 mg/kg <0.05 ----

0.025 mg/kg ---- 66 12098.9alpha-Endosulfan 0.25

0.05 mg/kg <0.05 ---- ------------

0.025 mg/kg ---- 57 122104beta-BHC 0.25

0.05 mg/kg <0.05 ---- ------------

0.025 mg/kg ---- 60 11195.7beta-Endosulfan 0.25

0.05 mg/kg <0.05 ---- ------------

0.025 mg/kg ---- 71 10897.7cis-Chlordane 0.25

0.05 mg/kg <0.05 ---- ------------

0.025 mg/kg ---- 69 10897.0delta-BHC 0.25

0.05 mg/kg <0.05 ---- ------------

0.025 mg/kg ---- 70 11196.6Dieldrin 0.25

0.05 mg/kg <0.05 ---- ------------

0.05 mg/kg <0.05 ---- --------Endosulfan sulfate ----

0.025 mg/kg ---- 63 11296.60.25

0.05 mg/kg <0.05 ---- --------Endrin ----

0.025 mg/kg ---- 63 11385.00.25

0.05 mg/kg <0.05 ---- --------Endrin aldehyde ----

0.025 mg/kg ---- 38 12692.30.25

0.05 mg/kg <0.05 ---- --------Endrin ketone ----

0.025 mg/kg ---- 72 1051030.25

0.05 mg/kg <0.05 ---- --------gamma-BHC ----

0.025 mg/kg ---- 70 10798.10.25

0.025 mg/kg ---- 67 10692.9Heptachlor 0.25

0.05 mg/kg <0.05 ---- ------------


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Analyte name Low

Recovery Limits



Spike Recovery

Actual Results

Spike concentration

Method

blank

result

LOR


mg/kg mg/kg %%%EP068A: Organochlorine Pesticides (OC) - ( QC Lot: 255141 ) - continued

0.025 mg/kg ---- 66 11594.6Heptachlor epoxide 0.25

0.05 mg/kg <0.05 ---- ------------

0.05 mg/kg <0.05 ---- --------Hexachlorobenzene (HCB) ----

0.025 mg/kg ---- 68 1171010.25

0.025 mg/kg ---- 40 12795.1Methoxychlor 0.25

0.2 mg/kg <0.2 ---- ------------

0.05 mg/kg <0.05 ---- --------trans-Chlordane ----

0.025 mg/kg ---- 67 11597.10.25


Project :



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06155B BN/217/06 23 Aug 2006


Quality Control Report - Matrix Spikes (MS)

The quality control term Matrix Spike (MS) refers to an intralaboratory split sample spiked with a representative set of target analytes. The purpose of this QC type is to monitor potential matrix effects on analyte recoveries.

Static Recovery Limits as per laboratory Data Quality Objectives (DQO's). 'Ideal' recovery ranges stated may be waived in the event of sample matrix interferences. - Anonymous - Client Sample IDs refer to samples which

are not specifically part of this work order but formed part of the QC process lot. Abbreviations: LOR = Limit of Reporting, RPD = Relative Percent Difference.

* Indicates failed QC

Matrix Type: SOIL Matrix Spike (MS) Report

Analyte name Client Sample ID

Actual Results Recovery Limits

Static LimitsSpike Recovery

Spike ConcentrationLaboratory Sample ID HighLowMSLOR

Sample Result


EG005T: Total Metals by ICP-AES - ( QC Lot: 255845 ) %%%mg/kgmg/kg

75 mg/kgArsenic 70 13050AnonymousEB0607614-002 96.1

<11 mg/kgCadmium 70 13050 109

172 mg/kgChromium 70 13050 108

95 mg/kgCopper 70 13050 107

65 mg/kgLead 70 13050 104

62 mg/kgNickel 70 13050 108

205 mg/kgZinc 70 13050 110

EG005T: Total Metals by ICP-AES - ( QC Lot: 255847 ) %%%mg/kgmg/kg

<55 mg/kgArsenic 70 13050DUP16EB0607640-015 97.8

<11 mg/kgCadmium 70 13050 104

142 mg/kgChromium 70 13050 114

125 mg/kgCopper 70 13050 119

585 mg/kgLead 70 13050 86.4

62 mg/kgNickel 70 13050 115

675 mg/kgZinc 70 13050 110


EG035T: Total Mercury by FIMS - ( QC Lot: 255846 ) %%%mg/kgmg/kg

<0.10.1 mg/kgMercury 70 1305.0DUP1EB0607640-001 85.7


EP068A: Organochlorine Pesticides (OC) - ( QC Lot: 255141 ) %%%mg/kgmg/kg

<0.050.05 mg/kggamma-BHC 70 1300.25AnonymousEB0607614-002 89.4

<0.050.05 mg/kgHeptachlor 70 1300.25 84.7

<0.050.05 mg/kgAldrin 70 1300.25 72.5

<0.050.05 mg/kgDieldrin 70 1300.25 91.0


Project :



Page Number :

Issue Date :

9 of 9

06155B BN/217/06 23 Aug 2006


Matrix Type: SOIL Matrix Spike (MS) Report

Analyte name Client Sample ID

Actual Results Recovery Limits

Static LimitsSpike Recovery

Spike ConcentrationLaboratory Sample ID HighLowMSLOR

Sample Result


%%%mg/kgEP068A: Organochlorine Pesticides (OC) - ( QC Lot: 255141 ) - continued mg/kg

<0.050.05 mg/kgEndrin 70 1300.25AnonymousEB0607614-002 88.2

<0.20.20 mg/kg4,4’-DDT 70 1300.25 72.3

A Campbell Brothers Limited CompanyReport version : QC_NA 3.03

INTERPRETIVE QUALITY CONTROL REPORT

ALS Environmental Brisbane 1 of 6 Page :Laboratory :BUTLER PARTNERS PTY LTDClient :

Contact :

Address :

Contact :

Address :

Michael Heery

32 Shand Street Stafford

QLD Australia 4053

MR LUKE AMIES

P O BOX 2267 FORTITUDE VALLEY BC QLD

AUSTRALIA 4006Work order : EB0607640

Amendment No. :

7 Aug 2006BN/217/06Quote number :06155B Date received :Project :

Date issued :LA92Order number :

C-O-C number : - Not provided -

- Not provided -Site :

[email protected] [email protected] :E-mail :

07 3852 3800 +61 (07) 3243 7222Telephone :Telephone :

07 3852 3808 +61 (07) 3243 7259Facsimile :Facsimile : 13

15

Analysed :

Received :

No. of samples

23 Aug 2006

This Interpretive Quality Control Report was issued on 23 Aug 2006 for the ALS work order reference EB0607640 and supersedes any previous reports with this reference.


l Analysis Holding Time Compliance

l Quality Control Type Frequency Compliance

l Summary of all Quality Control Outliers

l Brief Method Summaries


Project :

Client : BUTLER PARTNERS PTY LTD Work Order :


Page Number :

Issue Date :

EB0607640 2 of 6

06155B BN/217/06 23 Aug 2006

Interpretive Quality Control Report - Analysis Holding Time

The following report summarises extraction / preparation and analysis times and compares with recommended holding times. Dates reported represent first date of extraction or analysis and preclude subsequent dilutions and

reruns. Information is also provided re the sample container (preservative) from which the sample aliquot was taken. Elapsed time to analysis represents time from sampling where no extraction / digestion is involved or time

from extraction / digestion where this is present. For composite samples, sampling date/time is taken as that of the oldest sample contributing to that composite. Sample date/time for laboratory produced leaches are taken

from the completion date/time of the leaching process. Outliers for holding time are based on USEPA SW846, APHA, AS and NEPM (1999). Failed outliers, refer to the 'Summary of Outliers'.

Matrix Type: SOIL Analysis Holding Time and Preservation

AnalysisExtraction / Preparation

Due for analysisDate analysedDue for extractionDate extracted

Date SampledMethod

Container / Client Sample ID(s) Pass? Pass?

EA055-103: Moisture Content

Soil Glass Jar - Unpreserved

---- Fail by 3 days8 Aug 2006----DUP11, DUP12 11 Aug 2006----1 Aug 2006


---- Fail by 2 days9 Aug 2006----DUP14, DUP15,

DUP16

11 Aug 2006----2 Aug 2006



DUP3, DUP4,

DUP5, DUP6,

DUP8, DUP9

11 Aug 2006----31 Jul 2006



Pass Pass28 Jan 200728 Jan 2007DUP11, DUP12 14 Aug 200614 Aug 20061 Aug 2006


Pass Pass29 Jan 200729 Jan 2007DUP14, DUP15,

DUP16

14 Aug 200614 Aug 20062 Aug 2006


Pass Pass27 Jan 200727 Jan 2007DUP1, DUP2,

DUP3, DUP4,

DUP5, DUP6,

DUP8, DUP9

14 Aug 200614 Aug 200631 Jul 2006



Pass Pass29 Aug 200629 Aug 2006DUP11, DUP12 15 Aug 200614 Aug 20061 Aug 2006


Pass Pass30 Aug 200630 Aug 2006DUP14, DUP15,

DUP16

15 Aug 200614 Aug 20062 Aug 2006


Pass Pass28 Aug 200628 Aug 2006DUP1, DUP2,

DUP3, DUP4,

DUP5, DUP6,

DUP8, DUP9

15 Aug 200614 Aug 200631 Jul 2006

EP068: Pesticides by GCMS


Pass Pass20 Sep 200616 Aug 2006DUP16 21 Aug 200611 Aug 20062 Aug 2006


Project :



Page Number :

Issue Date :

EB0607640 3 of 6

06155B BN/217/06 23 Aug 2006

Matrix Type: SOIL Analysis Holding Time and Preservation


Due for analysisDate analysedDue for extractionDate extracted

Date SampledMethod

Container / Client Sample ID(s) Pass? Pass?

EP068: Pesticides by GCMS - continued


Pass Pass20 Sep 200614 Aug 2006DUP3, DUP8 21 Aug 200611 Aug 200631 Jul 2006


Project :



Page Number :

Issue Date :

EB0607640 4 of 6

06155B BN/217/06 23 Aug 2006

The following report summarises the frequency of laboratory QC samples analysed within the analytical lot(s) in which this work order was processed. Actual rate should be greater than or equal to the expected rate.

Interpretive Quality Control Report - Frequency of Quality Control Samples

Matrix Type: SOIL Frequency of Quality Control Samples

Quality Control Sample Type Count Rate (%) Quality Control Specification

QC Actual ExpectedRegularMethod

Laboratory Duplicates (DUP)

EA055-103: Moisture Content 2 20 10.0 10.0 NEPM 1999 Schedule B(3) and ALSE QCS3 requirement

EG005T: Total Metals by ICP-AES 3 20 15.0 10.0 NEPM 1999 Schedule B(3) and ALSE QCS3 requirement

EG035T: Total Mercury by FIMS 2 14 14.3 10.0 NEPM 1999 Schedule B(3) and ALSE QCS3 requirement

EP068: Pesticides by GCMS 2 11 18.2 10.0 NEPM 1999 Schedule B(3) and ALSE QCS3 requirement

Laboratory Control Samples (LCS)




Method Blanks (MB)




Matrix Spikes (MS)





Project :



Page Number :

Issue Date :

EB0607640 5 of 6

06155B BN/217/06 23 Aug 2006

Interpretive Quality Control Report - Summary of Outliers

Outliers : Quality Control Samples

The following report highlights outliers flagged on the 'Quality Control Report'. Surrogate recovery limits are static and based on USEPA SW846 or ALS-QWI/EN/38 (in the absence of specific USEPA limits). - Anonymous -

Client Sample IDs refer to samples which are not specifically part of this work order but formed part of the QC process lot.

Non-surrogates

l For all matrices, no RPD recovery outliers occur for the duplicate analysis.

l For all matrices, no method blank result outliers occur.

l For all matrices, no laboratory spike recoveries breaches occur.

l For all matrices, no matrix spike recoveries breaches occur.

Surrogates

l For all matrices, no surrogate recovery outliers occur.

Outliers : Analysis Holding Time

The following report highlights outliers within this 'Interpretive Quality Control Report - Analysis Holding Time'.

Method

Container / Client Sample ID(s)

Date Sampled Extraction / Preparation

Date extracted Due for extraction Pass? Date analysed Due for analysis Pass?

Analysis



---- Fail by 3 days8 Aug 2006----DUP11, DUP12 11 Aug 2006----1 Aug 2006




DUP16

11 Aug 2006----2 Aug 2006




DUP3, DUP4,

DUP5, DUP6,

DUP8, DUP9

11 Aug 2006----31 Jul 2006

Outliers : Frequency of Quality Control Samples

The following report highlights outliers within this 'Interpretive Quality Control Report - Frequency of Quality Control Samples'.

l No frequency outliers occur.


Project :



Page Number :

Issue Date :

EB0607640 6 of 6

06155B BN/217/06 23 Aug 2006

Method Reference Summary

The analytical procedures used by ALS Environmental are based on established internationally-recognized procedures such as those published by the US EPA, APHA, AS and NEPM. In house procedure are employed in the

absence of documented standards or by client request. The following report provides brief descriptions of the analytical procedures employed for results reported herein. Reference methods from which ALSE methods are

based are provided in parenthesis.

Matrix Type: SOIL Method Reference Summary

Preparation Methods

EN69 : Hot Block Digest for metals in soils sediments and sludges - USEPA 200.2 Mod. Hot Block Acid Digestion 1.0g of sample is heated with Nitric and Hydrochloric acids, then cooled.

Peroxide is added and samples heated and cooled again before being filtered and bulked to volume for analysis. Digest is appropriate for determination of selected metals in sludge, sediments,

and soils. This method is compliant with NEPM (1999) Schedule B(3) (Method 202)

ORG17A : Tumbler Extraction of Solids (Option A - Concentrating) - In-house, Mechanical agitation (tumbler). 20g of sample, Na2SO4 and surrogate are extracted with 150mL 1:1

DCM/Acetone by end over end tumble. The solvent is decanted, dehydrated and concentrated (by KD) to the desired volume for analysis.

Analytical Methods

EA055-103 : Moisture Content - A gravimetric procedure based on weight loss over a 12 hour drying period at 103-105 degrees C. This method is compliant with NEPM (1999) Schedule B(3)

(Method 102)

EG005T : Total Metals by ICP-AES - (APHA 20th ed., 3120; USEPA SW 846 - 6010) (ICPAES) Metals are determined following an appropriate acid digestion of the soil. The ICPAES technique

ionises samples in a plasma, emitting a characteristic spectrum based on metals present. Intensities at selected wavelengths are compared against those of matrix matched standards. This

method is compliant with NEPM (1999) Schedule B(3)

EG035T : Total Mercury by FIMS - AS 3550, APHA 3112 Hg - B (Flow-injection (SnCl2)(Cold Vapour generation) AAS) FIM-AAS is an automated flameless atomic absorption technique.

Mercury in solids are determined following an appropriate acid digestion. Ionic mercury is reduced online to atomic mercury vapour by SnCl2 which is then purged into a heated quartz cell.

Quantification is by comparing absorbance against a calibration curve. This method is compliant with NEPM (1999) Schedule B(3)

EP068 : Pesticides by GCMS - (USEPA SW 846 - 8270B) Extracts are analysed by Capillary GC/MS and quantification is by comparison against an established 5 point calibration curve. This

technique is compliant with NEPM (1999) Schedule B(3) (Method 504,505)

A Campbell Brothers Limited CompanyReport version : 1QCINA 2.08

AUSTRALIAN LABORATORY SERVICES PTY LTD ABN 84 009 936 029

Stafford QLD 4053 Australia

Telephone: 61-7-32437222 Facsimile: 61-7-32437259 http://www.alsenviro.com/

SAMPLE RECEIPT NOTIFICATION (SRN)Comprehensive report

Client Details Laboratory Details

BUTLER PARTNERS PTY LTD ALS Environmental BrisbaneLaboratory :Client :

Manager :MR LUKE AMIESContact : Michael Heery

Address : Stafford QLD Australia 4053P O BOX 2267 FORTITUDE VALLEY BC QLD

AUSTRALIA 4006

Address :

06155B EB20060169Quote number :Project :

LA92Order number :

Site :

Luke Amies

Work order : EB0607640C-O-C Number : - Not provided -

- Not provided -Sampler :

E-mail : [email protected] E-mail : [email protected]

Telephone :

Facsimile :

07 3852 3800 Telephone :

Facsimile :

61-7-32437222

61-7-3243725907 3852 3808

Dates

Scheduled Reporting Date

7 Aug 2006 SRA Issue DateDate Samples Received

22 Aug 2006

10 Aug 2006::

: :Client Requested Date 22 Aug 2006

Delivery DetailsMode of Delivery Carrier.

Security Seal Intact.

19 C - Ice bricks presentTemperature :

1 MEDIUMNo. of coolers/boxes No. of samples

:

:

:

- Received :

- Analysed :

15

15

Comments

Samples received in appropriately pretreated and preserved containers.l

Sample(s) have been received within recommended holding times.l

Analytical work for this work order will be conducted at ALSE Brisbane.l

Please direct any queries related to sample condition / numbering / breakages to Charles Allom.l

Sample Disposal - Aqueous (14 days), Solid (90 days) from date of completion of work order.l

Please direct any turn around / technical queries to the laboratory contact designated above.l

lWhen the sampling time is not supplied on the COC documentation, ALSE defaults the sampling time to that of the COC

'relinquishment' time (if supplied). If this also is not supplied, ALSE defaults the sampling time to the 'time of receipt at Laboratory'.

Disclaimer : This document contains privileged and confidential information intended only for the use of the addressee. If you are not the

addressee, you are hereby notified that you must not disseminate, copy or take action of its contents. If you have received this

document in error, please notify ALS immediately.

A Campbell Brothers Limited CompanyPage 1 of 3 ALSE - Excellence in Analytical Testing

Project :



EB0607640

06155B EB20060169

SAMPLE RECEIPT NOTIFICATION (SRN) - continued

Summary of Sample(s) / Container(s) and Requested Analysis

Some items described below may be part of a laboratory process neccessary for the execution of client requested tasks. Packages may contain additional

analyses, such as moisture and preparation tasks, that form an implicit part of that package.

ALS Sample ID. Client Sample ID - Sample Date Requested Analysis

Mo

istu

re C

on

ten

t

EA

05

5-1

03

- S

OIL

EP

06

8A

(s

oli

ds

) -

SO

IL

Org

an

och

lorin

e P

esticid

es b

y G

CM

S

S-0

2 -

SO

IL

8 M

eta

ls (

incl. D

ige

stio

n)

lEB0607640-001 DUP1 - 31 Jul 2006

lEB0607640-002 DUP2 - 31 Jul 2006

lllEB0607640-003 DUP3 - 31 Jul 2006

lEB0607640-004 DUP4 - 31 Jul 2006

lEB0607640-005 DUP5 - 31 Jul 2006

lEB0607640-006 DUP6 - 31 Jul 2006

lEB0607640-007 DUP7 - 31 Jul 2006

lllEB0607640-008 DUP8 - 31 Jul 2006

lEB0607640-009 DUP9 - 31 Jul 2006

lEB0607640-010 DUP10 - 1 Aug 2006

lEB0607640-011 DUP11 - 1 Aug 2006

lEB0607640-012 DUP12 - 1 Aug 2006

lEB0607640-013 DUP14 - 2 Aug 2006

lEB0607640-014 DUP15 - 2 Aug 2006

lllEB0607640-015 DUP16 - 2 Aug 2006

3Total(s) : 3 15

A Campbell Brothers Limited CompanyPage 2 of 3 ALSE - Excellence in Analytical Testing

Project :



EB0607640

06155B EB20060169

SAMPLE RECEIPT NOTIFICATION (SRN) - continued

Requested Reports

ANN PATTENl

Invoice- [email protected]

MR LUKE AMIESl

A4 - Certificate of Analysis - NEPM format- [email protected]

A4 - Quality Control Report - NEPM format- [email protected]

A4 - Interpretive Quality Control Report - NEPM format- [email protected]

ENMRG Export Format- [email protected]

Chain of Custody Acknowledgement- [email protected]

A4 - Sample Receipt Notification - Comprehensive format- [email protected]

MS SUZANNE WALKERl

A4 - Certificate of Analysis - NEPM format- [email protected]

A4 - Quality Control Report - NEPM format- [email protected]

A4 - Interpretive Quality Control Report - NEPM format- [email protected]

ENMRG Export Format- [email protected]

Chain of Custody Acknowledgement- [email protected]

A4 - Sample Receipt Notification - Comprehensive format- [email protected]

Sample Container(s) / Preservation Non-Compliance Log

All comparisons are made against pretreatment/preservation AS, APHA, USEPA standards.

l No sample container / preservation non-compliance exist.

A Campbell Brothers Limited CompanyPage 3 of 3 ALSE - Excellence in Analytical TestingReport version : SRAEA 2.04

This document is issued in accordance with NATA's accreditation requirements.

Accredited for compliance with ISO/IEC 17205

Accreditation Number: 14356

Certificate of Analysis

Butler Partners Pty Ltd

79 Doggett Street, Fortitude Valley Qld 4006

79 Doggett Street

FORTITUDE VALLEY QLD 4006

Australia

Attention: Luke Amies

Project 07ENBR0013083

Client Reference 06155C

Order Number LA76

Received Date 18/07/2007 10:30:00 AM

Customer Sample ID BV-A5 BV-A9 BV-A10

Amdel Sample Number 547429 547430 547431

Date Sampled 17/07/2007 17/07/2007 17/07/2007

Metals

Test/Reference UnitPQL

3200 Total Metals in Soil by ICP/AES

mg/kg 8.5 5.3Arsenic 3 7.6

mg/kg <1 <1Cadmium 1 <1

mg/kg 41 36Chromium 2 37

mg/kg 12 8.2Copper 1 13

mg/kg 17 11Lead 5 14

mg/kg 3.6 6.7Nickel 2 3.7

mg/kg 35 31Zinc 2 30

3400 Total Mercury in Soil by ICP-AES

mg/kg <0.05 <0.05Total Mercury 0.05 0.09

Miscellaneous


5000 Moisture Content

% 17 11% Moisture 1 17



Date Sampled 17/07/2007 17/07/2007 17/07/2007

Metals






mg/kg 9.1 12Copper 1 15





mg/kg <0.05 <0.05Total Mercury 0.05 <0.05

Miscellaneous



% 12 17% Moisture 1 19

First Reported: 19 July 2007 Page 1 of 8

Date Printed: 23 July 2007 Final Report Number :

Amdel Ltd 1/21 Smallwood Pl Murarrie QLD Australia 4172

ABN: 30 008 127 802 Telephone: (07) 3902 4600 Facsimile: (07) 3902 4646

232601

Customer Sample ID BV-A18 BV-A19 WV-A7


Date Sampled 17/07/2007 17/07/2007 17/07/2007

Metals






mg/kg 14 11Copper 1 14





mg/kg <0.05 <0.05Total Mercury 0.05 <0.05

Miscellaneous



% 21 15% Moisture 1 17

Customer Sample ID WV-A8 WV-A9 A1-SP1


Date Sampled 17/07/2007 17/07/2007 17/07/2007

Metals



mg/kg 210 9.8Arsenic 3 8.9

mg/kg 6.0 <1Cadmium 1 <1



mg/kg 4600 49Lead 5 18

mg/kg 150 5.9Nickel 2 2.4

mg/kg 7600 63Zinc 2 26


mg/kg 0.32 <0.05Total Mercury 0.05 <0.05

Miscellaneous



% 24 12% Moisture 1 17

Customer Sample ID A1-SP2 A1-SP3 A1-SP4


Date Sampled 17/07/2007 17/07/2007 17/07/2007

Metals



mg/kg 11 10Arsenic 3 8.8






232601



Date Sampled 17/07/2007 17/07/2007 17/07/2007

Metals




mg/kg 130 32Lead 5 33


mg/kg 270 40Zinc 2 52


mg/kg 0.28 0.1Total Mercury 0.05 0.05

Miscellaneous



% 14 14% Moisture 1 13



Date Sampled 17/07/2007 17/07/2007 17/07/2007

Metals



mg/kg 7.6 12Arsenic 3 7.1








mg/kg <0.05 0.05Total Mercury 0.05 0.11

Miscellaneous



% 16 12% Moisture 1 14

Customer Sample ID A2-SP3 DUP27 DUP29


Date Sampled 17/07/2007 17/07/2007 17/07/2007

Metals



mg/kg 9.9 4.4Arsenic 3 14

mg/kg <1 <1Cadmium 1 3.4



mg/kg 46 13Lead 5 510

mg/kg 6.1 9.3Nickel 2 15





232601

Customer Sample ID A2-SP3 DUP27 DUP29


Date Sampled 17/07/2007 17/07/2007 17/07/2007

Metals


mg/kg 63 38Zinc 2 1500



Miscellaneous



% 12 12% Moisture 1 13

Customer Sample ID FB-170707 RB-170707 BLANK


Date Sampled 17/07/2007 17/07/2007 17/07/2007

Metals


3300 Dissolved Metals in Water by AAS

µg/L <1 -Arsenic 1 <1

µg/L <0.1 -Cadmium 0.1 <0.1

µg/L <1 -Lead 1 <1

3300 Total Metals in Water By AAS

µg/L - <1Arsenic 1 -

µg/L - <0.1Cadmium 0.1 -

µg/L - <1Lead 1 -

3200 Dissolved Metals in Water - ICP/AES

µg/L <1 -Chromium 1 <1

µg/L <2 -Copper 2 <2

µg/L <5 -Nickel 5 <5

µg/L <5 -Zinc 5 <5

3200 Total Metals in Water by ICP/AES

µg/L - <2Chromium 2 -

µg/L - <2Copper 2 -

µg/L - <5Nickel 5 -

µg/L - <10Zinc 10 -

3400 Total Mercury in Water by ICP-AES

µg/L - <1Total Mercury 1 -

3400 Dissolved Mercury in Water by ICPA

µg/L <1 -Mercury 1 <1

Sample History

Where samples are submitted/analysed over several days, the last date of extraction and analysis is reported.

Description AnalysedExtracted

3200 Dissolved Metals in Water - ICP/AES 20/07/2007

3200 Total Metals in Soil by ICP/AES 19/07/2007

3200 Total Metals in Water by ICP/AES 20/07/2007

3300 Dissolved Metals in Water by AAS 19/07/2007

3300 Total Metals in Water By AAS 23/07/2007

3400 Dissolved Mercury in Water by ICPA 23/07/2007

3400 Total Mercury in Soil by ICP-AES 20/07/2007

3400 Total Mercury in Water by ICP-AES 23/07/2007

5000 Moisture Content 19/07/2007





232601

Amdel Internal Quality Control Review

General

1. Laboratory QC results for Method Blanks, Duplicates, Matrix Spikes, and Laboratory Control Samples

are included in this QC report where applicable. Additional QC data may be available on request.

2. Amdel QC Acceptance/Rejection criteria are available on request.

3. Proficiency trial results are available on request.

4. Actual PQLs are matrix dependant. Quotes PQLs may be raised where sample extracts are diluted due to interferences.

5. Results are uncorrected for matrix spike or surrogate recoveries.

6. Test samples duplicated or spiked, are for this job only and are identified in the following QC report.

7. SVOC analyses on waters are performed on homogenized, unfiltered sample, unless noted otherwise.

8. When individual results are qualified in the body of a report, refer to the qualifier descriptions that follow.

Holding Times

Please refer to 'Sampling and Preservation Chart for Soils & Waters' for holding times. (Amdel form AD-FOR_ADM-020)

For samples received on the last day of holding time, notification of testing requirements should have been received at least

6 hours prior to sample receipt deadlines as stated on the Sample Receipt Acknowledgement.

If the Laboratory did not receive the information in the required timeframe, and regardless of any other integrity issues,

suitablity qualified results may still be reported.

Holding times apply from the date of sampling, therefore compliance to these may be outside the laboratory's control.

Quality Control Results

Laboratory: EN_METALS

Acceptance

Limits

Result 1UnitsSample, Test, Result Reference

Pass

Limits

Qualifying

Codes

547722 [ Method Blank ]


Arsenic mg/kg <3 < 3 T

Cadmium mg/kg <1 < 1 T

Chromium mg/kg <2 < 2 T

Copper mg/kg <1 < 1 T

Lead mg/kg <5 < 5 T

Nickel mg/kg <2 < 2 T

Zinc mg/kg <2 < 2 T







Lead mg/kg <5 < 5 T


Zinc mg/kg <2 < 2 T



Mercury mg/kg <0.05 < 0.05 T






Chromium µg/L <1 < 1 T

Copper µg/L <2 < 2 T

Nickel µg/L <5 < 5 T

Zinc µg/L <5 < 5 T



Mercury µg/L <1 < 1 T





232601


Acceptance

Limits


Pass

Limits

Qualifying

Codes


3400 Total Mercury in Water by ICP-AES

Total Mercury µg/L <1 < 1 T



Arsenic µg/L <1 < 1 T

Cadmium µg/L <0.1 < 0.1 T

Lead µg/L <1 < 1 T


3300 Total Metals in Water By AAS



Lead µg/L <1 < 1 T

547723 [ Laboratory Control Sample ]

3200 Total Metals in Soil by ICP/AES Expected Value Percent Recovery

Arsenic mg/kg 52 50.0 105 70-130 % T

Cadmium mg/kg 53 50.0 107 70-130 % T

Chromium mg/kg 52 50.0 105 70-130 % T

Copper mg/kg 53 50.0 105 70-130 % T

Lead mg/kg 53 50.0 105 70-130 % T

Nickel mg/kg 53 50.0 105 70-130 % T

Zinc mg/kg 54 50.0 107 70-130 % T



Arsenic mg/kg 52 50.0 104 70-130 % T

Cadmium mg/kg 52 50.0 105 70-130 % T

Chromium mg/kg 52 50.0 104 70-130 % T

Copper mg/kg 52 50.0 105 70-130 % T

Lead mg/kg 52 50.0 104 70-130 % T

Nickel mg/kg 52 50.0 104 70-130 % T

Zinc mg/kg 53 50.0 107 70-130 % T


3400 Total Mercury in Soil by ICP-AES Expected Value Percent Recovery

Mercury mg/kg 0.43 0.5 87 75-125 % T



Mercury mg/kg 0.57 0.5 115 75-125 % T


3200 Dissolved Metals in Water - ICP/AES Expected Value Percent Recovery

Chromium µg/L 990 N/A N/A N/A N/A

Copper µg/L 1000 1000.0 101 80-120 % T

Nickel µg/L 1000 1000.0 101 80-120 % T

Zinc µg/L 1100 1000.0 106 80-120 % T


3400 Dissolved Mercury in Water by ICPA Expected Value Percent Recovery

Mercury µg/L 9.2 0.01 92 80-120 % T


3400 Total Mercury in Water by ICP-AES Expected Value Percent Recovery

Total Mercury µg/L 8.9 N/A N/A N/A N/A


3300 Dissolved Metals in Water by AAS Expected Value Percent Recovery

Arsenic µg/L 10 10.0 102.0 80-120 % T

Cadmium µg/L 1.8 2.0 90.6 80-120 % T

Lead µg/L 11 10.0 106.86 80-120 % T


3300 Total Metals in Water By AAS Expected Value Percent Recovery

Arsenic µg/L 10 10.0 101 80-120 % T

Cadmium µg/L 2.1 2.0 103 80-120 % T

Lead µg/L 11 10.0 106 80-120 % T





232601


Acceptance

Limits


Pass

Limits

Qualifying

Codes

547700 [ Duplicate of 547429 ]

3200 Total Metals in Soil by ICP/AES Result 2 RPD

ArsenicDB mg/kg 8.6 7.6 13 0-30 % T

CadmiumDB mg/kg <1 <1 <1 0-30 % T

ChromiumDB mg/kg 50 37 30 0-30 % T

CopperDB mg/kg 13 13 3 0-30 % T

LeadDB mg/kg 20 14 36 0-30 % F Q15

NickelDB mg/kg 5.2 3.7 34 0-30 % F Q15

ZincDB mg/kg 30 30 3 0-30 % T

547702 [ Duplicate of 547430 ]






LeadDB mg/kg 13 17 28 0-30 % T

NickelDB mg/kg 3.9 3.6 8 0-30 % T

ZincDB mg/kg 34 35 2 0-30 % T

547704 [ Duplicate of 547431 ]





CopperDB mg/kg 9.5 8.2 15 0-30 % T

LeadDB mg/kg 12 11 12 0-30 % T

NickelDB mg/kg 6.0 6.7 11 0-30 % T

ZincDB mg/kg 34 31 8 0-30 % T

547706 [ Duplicate of 547429 ]

3400 Total Mercury in Soil by ICP-AES Result 2 RPD

MercuryDB mg/kg <0.05 0.09 55 0-30 % F Q15

547707 [ Duplicate of 547430 ]


MercuryDB mg/kg <0.05 <0.05 <0.05 0-30 % T

547709 [ Duplicate of 547431 ]


MercuryDB mg/kg <0.05 <0.05 <0.05 0-30 % T

547710 [ Spike of 547432 ]

3200 Total Metals in Soil by ICP/AES Spike Value Percent Recovery

ArsenicDB mg/kg 65 N/A N/A N/A N/A

CadmiumDB mg/kg 61 N/A N/A N/A N/A

ChromiumDB mg/kg 100 N/A N/A N/A N/A

CopperDB mg/kg 77 N/A N/A N/A N/A

LeadDB mg/kg 73 N/A N/A N/A N/A

NickelDB mg/kg 64 N/A N/A N/A N/A

ZincDB mg/kg 100 N/A N/A N/A N/A

547711 [ Spike of 547433 ]









547712 [ Spike of 547432 ]

3400 Total Mercury in Soil by ICP-AES Spike Value Percent Recovery

MercuryDB mg/kg 0.52 N/A N/A N/A N/A





232601


Acceptance

Limits


Pass

Limits

Qualifying

Codes

547713 [ Spike of 547433 ]



Sample Integrity

YesCustody Seals Intact (if used)

YesAttempt to Chill was evident

YesSamples correctly preserved

YesOrganic samples had Teflon liners

YesSamples received with Zero Headspace

YesSamples received within HoldingTime

NoSome samples have been subcontracted

Qualifier Codes/Comments

DescriptionCode

Q15 The RPD reported passes Amdel's Acceptance Criteria as stipulated in AS-POL-002. The Criteria displayed in this

report are for results >10 x PQL; the results of this sample are < 10 x PQL

Authorised By

Accreditation Number: 14356Michael Mowle Team Leader

Laboratory Manager

Team LeaderMichael Mowle

Final Report

- Indicates Not Requested * Indicates NATA accreditation does not cover the performance of this service

Amdel Limited shall not be liable for loss, cost, damages or expenses incurred by the client, or any other person or company, resulting from the use of any information or interpretaton given

in this report. In no case shall Amdel Limited be liable for consequential damages including, but not limited to, lost profits, damages for failure to meet deadlines and lost production arising

from this report. This document shall not be reproduced except in full and relates only to the items tested. Unless indicated otherwise, the tests were performed on the samples as received.

Sampled dates quoted in this report are those listed on the COC or sample jars; if no sample dates are noted, the date the samples are received at the laboratory have been used.

The samples were not collected by Amdel staff.





232601

Sample Receipt Advice

Customer Service - 1300 552 389

Client Name: Butler Partners Pty Ltd Date Received: 18 July 2007

Attention: Luke Amies Due Date: 20 July 2007

Client Reference number: Turnaround: 48 Hour06155C

Amdel Reference number: 07ENBR0013083 Your Amdel Contact: David Bates+61 7 3902 4600

If you have any queries regarding turnaround and sample progress, technical queries or wish to make changes please contact the laboratory immediately.

Job Information

Sample Integrity

Attempt to Chill was evident Yes

Samples correctly preserved Yes

Organic samples had Teflon liners Yes

Samples received with Zero Headspace Yes

Samples received within HoldingTime Yes

Some samples have been subcontracted No

Custody Seals Intact (if used) Yes

Analysis Requested

Analysis Requested Method Code Number Of Samples

3300Dissolved Metals in Water by AAS 2

3300Total Metals in Water By AAS 1

3200Total Metals in Soil by ICP/AES 21

3400Total Mercury in Soil by ICP-AES 21

3200Dissolved Metals in Water - ICP/AES 2

3200Total Metals in Water by ICP/AES 1

3400Dissolved Mercury in Water by ICPA 2

3400Total Mercury in Water by ICP-AES 1

5000Moisture Content 21

Note

- Turnaround time starts when samples are received at the Laboratory

- For samples received after 4pm, turnaround time starts the next working day

- For samples received on the last day of holding time, notification of testing requirements must be

given at least 6 hours prior to the sample receipt deadlines; Should the laboratory not receive

the information in the required timeframe a suitably qualified results may still be reported.

- Surcharges may apply for 24 and 48 hour turnaround.

- Water samples will be discarded after 4 weeks unless notified.

- Soil samples are chilled for 1 month and will be discarded after 3 months unless notified.

- UNLESS ADVISED OTHERWISE - Sample analysis will commence regardless of integrity

issues and / or non-conformance and these will be recorded on the final report.

- Samples submitted for Micro analysis on a Friday may incur a $150 surcharge and / or be

analysed outside holding time (24 Hour Holding Time).

Logged in by : Patricia Chew Date : Wed 18 July 2007






Certificate of AnalysisButler Partners Pty Ltd


79 Doggett Street


Australia




Order Number LA77

Received Date 18/07/2007 02:30:00 PM



Date Sampled 18/07/2007 18/07/2007 18/07/2007

Metals


3200 Total Metals in Soil by ICP/AES mg/kg 7.0 6.4Arsenic 3 11



mg/kg 6.9 10Copper 1 9.9


mg/kg 3.8 2.5Nickel 2 <2


3400 Total Mercury in Soil by ICP-AES mg/kg <0.05 <0.05Total Mercury 0.05 0.14

Miscellaneous


5000 Moisture Content % 13 19% Moisture 1 18



Date Sampled 18/07/2007 18/07/2007 18/07/2007

Metals


3200 Total Metals in Soil by ICP/AES mg/kg 8.2 7.2Arsenic 3 7.2



mg/kg 7.7 5.5Copper 1 9.2




3400 Total Mercury in Soil by ICP-AES mg/kg <0.05 <0.05Total Mercury 0.05 <0.05

Miscellaneous






ABN: 30 008 127 802 Telephone: (07) 3902 4600 Facsimile: (07) 3902 4646 233028



Date Sampled 18/07/2007 18/07/2007 18/07/2007

Miscellaneous


% 13 13% Moisture 1 18



Date Sampled 18/07/2007 18/07/2007 18/07/2007

Metals










Miscellaneous





Date Sampled 18/07/2007 18/07/2007 18/07/2007

Metals







mg/kg 2.3 <2Nickel 2 2.4



Miscellaneous







Customer Sample ID WV-A1 WV-A2 WV-A3


Date Sampled 18/07/2007 18/07/2007 18/07/2007

Metals






mg/kg 11 12Lead 5 9.3




Miscellaneous



Customer Sample ID WV-A4 WV-A5 WV-A6


Date Sampled 18/07/2007 18/07/2007 18/07/2007

Metals







mg/kg 2.3 <2Nickel 2 2.7



Miscellaneous



Customer Sample ID WV-A10 DUP28 DUP30


Date Sampled 18/07/2007 18/07/2007 18/07/2007

Metals









Customer Sample ID WV-A10 DUP28 DUP30


Date Sampled 18/07/2007 18/07/2007 18/07/2007

Metals




mg/kg <2 <2Nickel 2 <2



Miscellaneous



Customer Sample ID DUP31 A3-SP1 A3-SP2


Date Sampled 18/07/2007 18/07/2007 18/07/2007

Metals





mg/kg 7.4 8.2Copper 1 10


mg/kg 2.3 3.1Nickel 2 <2



Miscellaneous



Customer Sample ID A3-SP3 FB-180707 RB-180707


Date Sampled 18/07/2007 18/07/2007 18/07/2007

Metals


3300 Dissolved Metals in Water by AAS µg/L <1 <1Arsenic 1 -

µg/L <0.1 <0.1Cadmium 0.1 -

µg/L <1 <1Lead 1 -

3200 Total Metals in Soil by ICP/AES mg/kg - -Arsenic 3 5.9

mg/kg - -Cadmium 1 <1

mg/kg - -Chromium 2 35





Customer Sample ID A3-SP3 FB-180707 RB-180707


Date Sampled 18/07/2007 18/07/2007 18/07/2007

Metals


mg/kg - -Copper 1 8.8

mg/kg - -Lead 5 22

mg/kg - -Nickel 2 2.9

mg/kg - -Zinc 2 31

3400 Total Mercury in Soil by ICP-AES mg/kg - -Total Mercury 0.05 <0.05

3200 Dissolved Metals in Water - ICP/AES µg/L <1 <1Chromium 1 -

µg/L <2 <2Copper 2 -

µg/L <5 <5Nickel 5 -

µg/L <5 <5Zinc 5 -

3400 Dissolved Mercury in Water by ICPA µg/L <1 <1Mercury 1 -

Miscellaneous


5000 Moisture Content % - -% Moisture 1 15

Sample History














General

1. Laboratory QC results for Method Blanks, Duplicates, Matrix Spikes, and Laboratory Control Samples are included in this QC report where applicable. Additional QC data may be available on request.2. Amdel QC Acceptance/Rejection criteria are available on request.3. Proficiency trial results are available on request.4. Actual PQLs are matrix dependant. Quotes PQLs may be raised where sample extracts are diluted due to interferences.5. Results are uncorrected for matrix spike or surrogate recoveries.6. Test samples duplicated or spiked, are for this job only and are identified in the following QC report.7. SVOC analyses on waters are performed on homogenized, unfiltered sample, unless noted otherwise.8. When individual results are qualified in the body of a report, refer to the qualifier descriptions that follow.

Holding Times


For samples received on the last day of holding time, notification of testing requirements should have been received at least6 hours prior to sample receipt deadlines as stated on the Sample Receipt Acknowledgement.If the Laboratory did not receive the information in the required timeframe, and regardless of any other integrity issues,suitablity qualified results may still be reported.




Acceptance

LimitsResult 1UnitsSample, Test, Result Reference

Pass

Limits

Qualifying

Codes






Zinc µg/L <5 < 5 T








Lead µg/L <1 < 1 T







Lead mg/kg <5 < 5 T


Zinc mg/kg <2 < 2 T







Lead mg/kg <5 < 5 T


Zinc mg/kg <2 < 2 T






Acceptance


Pass

Limits

Qualifying

Codes










Copper µg/L 1000 1000.0 101 80-120 % T

Nickel µg/L 1000 1000.0 101 80-120 % T

Zinc µg/L 1100 1000.0 106 80-120 % T



Mercury µg/L 9.2 0.01 92 80-120 % T



Arsenic µg/L 10 10.0 102.0 80-120 % T

Cadmium µg/L 1.8 2.0 90.6 80-120 % T

Lead µg/L 11 10.0 106.86 80-120 % T



Arsenic mg/kg 48 50.0 96 70-130 % T

Cadmium mg/kg 50 50.0 99 70-130 % T

Chromium mg/kg 50 50.0 99 70-130 % T

Copper mg/kg 51 50.0 102 70-130 % T

Lead mg/kg 49 50.0 98 70-130 % T

Nickel mg/kg 49 50.0 97 70-130 % T

Zinc mg/kg 49 50.0 99 70-130 % T



Arsenic mg/kg 48 50.0 97 70-130 % T

Cadmium mg/kg 49 50.0 98 70-130 % T

Chromium mg/kg 49 50.0 98 70-130 % T

Copper mg/kg 49 50.0 99 70-130 % T

Lead mg/kg 48 50.0 97 70-130 % T

Nickel mg/kg 49 50.0 97 70-130 % T

Zinc mg/kg 49 50.0 98 70-130 % T



Mercury mg/kg 0.47 0.5 95 75-125 % T



Mercury mg/kg 0.43 0.5 85 75-125 % T

548798 [ Duplicate of 548148 ]


ArsenicDB mg/kg 8.9 11 19 0-30 % T



CopperDB mg/kg 9.6 9.9 3 0-30 % T

LeadDB mg/kg 15 15 4 0-30 % T

NickelDB mg/kg <2 <2 <1 0-30 % T

ZincDB mg/kg 21 20 3 0-30 % T






Acceptance


Pass

Limits

Qualifying

Codes

548805 [ Duplicate of 548149 ]




ChromiumDB mg/kg 26 38 36 0-30 % F Q15

CopperDB mg/kg 7.5 6.9 8 0-30 % T

LeadDB mg/kg 8.2 11 27 0-30 % T

NickelDB mg/kg 3.8 3.8 1 0-30 % T

ZincDB mg/kg 24 26 9 0-30 % T

548820 [ Duplicate of 548150 ]






LeadDB mg/kg 15 14 6 0-30 % T

NickelDB mg/kg 2.6 2.5 4 0-30 % T

ZincDB mg/kg 27 26 2 0-30 % T

548821 [ Duplicate of 548148 ]



548822 [ Duplicate of 548149 ]


MercuryDB mg/kg <0.05 <0.05 <0.05 0-30 % T

548823 [ Duplicate of 548150 ]


MercuryDB mg/kg <0.05 <0.05 <0.05 0-30 % T

548824 [ Spike of 548151 ]









548825 [ Spike of 548152 ]









548826 [ Spike of 548151 ]



548827 [ Spike of 548152 ]







Sample Integrity









DescriptionCode

Q02 The duplicate %RPD is outside the recommended acceptance criteria. Further analysis indicates sample

heterogeneity as the cause.



Authorised By

Accreditation Number: 14356Elizabeth Button Senior Analyst


Laboratory Manager


Final Report

















79 Doggett Street


Australia




Order Number LA68

Received Date 11/07/2007 11:00:00 AM

Customer Sample ID BV-B11 BV-B16 BV-B21


Date Sampled 10/07/2007 10/07/2007 10/07/2007

SVOC


2300 OC Pest in Soil (Low Level) GC-ECD mg/kg <0.02 <0.02a-BHCDB 0.02 <0.02

mg/kg <0.02 <0.02a-ChlordaneDB 0.02 <0.02

mg/kg <0.02 <0.02a-EndosulfanDB 0.02 <0.02

mg/kg <0.02 <0.02AldrinDB 0.02 <0.02

mg/kg <0.02 <0.02b-BHCDB 0.02 <0.02

mg/kg <0.02 <0.02b-EndosulfanDB 0.02 <0.02

mg/kg <0.02 <0.02d-BHCDB 0.02 <0.02

mg/kg <0.02 <0.02DDDDB 0.02 <0.02

mg/kg <0.02 <0.02DDEDB 0.02 <0.02

mg/kg <0.02 <0.02DDTDB 0.02 <0.02

mg/kg <0.02 <0.02DieldrinDB 0.02 <0.02

mg/kg <0.02 <0.02Endosulfan sulfateDB 0.02 <0.02

mg/kg <0.02 <0.02EndrinDB 0.02 <0.02

mg/kg <0.02 <0.02Endrin AldehydeDB 0.02 <0.02

mg/kg <0.02 <0.02Endrin KetoneDB 0.02 <0.02

mg/kg <0.02 <0.02g-BHCDB 0.02 <0.02

mg/kg <0.02 <0.02g-ChlordaneDB 0.02 <0.02

mg/kg <0.02 <0.02HeptachlorDB 0.02 <0.02

mg/kg <0.02 <0.02Heptachlor epoxideDB 0.02 <0.02

mg/kg <0.02 <0.02Hexachlorobenzene (HCB)DB 0.02 <0.02

mg/kg <0.02 <0.02MethoxychlorDB 0.02 <0.02

mg/kg <0.02 <0.02OxychlordaneDB 0.02 <0.02

% 80 1052.4.5.6-tetrachloro-m-xylene-SURROGA

TE

1 84

Metals






mg/kg 8.4 8.1Lead 5 8.7

mg/kg 21 17Nickel 2 23









Date Sampled 10/07/2007 10/07/2007 10/07/2007

Metals


Miscellaneous





Date Sampled 10/07/2007 10/07/2007 10/07/2007

SVOC





mg/kg <0.02 <0.02AldrinDB 0.02 <0.02

mg/kg <0.02 <0.02b-BHCDB 0.02 <0.02


mg/kg <0.02 <0.02d-BHCDB 0.02 <0.02

mg/kg <0.02 <0.02DDDDB 0.02 <0.02

mg/kg 0.04 <0.02DDEDB 0.02 <0.02

mg/kg <0.02 <0.02DDTDB 0.02 <0.02

mg/kg <0.02 <0.02DieldrinDB 0.02 <0.02


mg/kg <0.02 <0.02EndrinDB 0.02 <0.02



mg/kg <0.02 <0.02g-BHCDB 0.02 <0.02








TE

1 83

Metals






mg/kg 7.8 7.8Lead 5 8.0










Date Sampled 10/07/2007 10/07/2007 10/07/2007

Miscellaneous



Customer Sample ID BV-B41 BV-B46 WV-B10


Date Sampled 10/07/2007 10/07/2007 10/07/2007

SVOC





mg/kg <0.02 <0.02AldrinDB 0.02 <0.02

mg/kg <0.02 <0.02b-BHCDB 0.02 <0.02


mg/kg <0.02 <0.02d-BHCDB 0.02 <0.02

mg/kg <0.02 <0.02DDDDB 0.02 <0.02

mg/kg <0.02 <0.02DDEDB 0.02 <0.02

mg/kg <0.02 <0.02DDTDB 0.02 <0.02

mg/kg <0.02 <0.02DieldrinDB 0.02 <0.02


mg/kg <0.02 <0.02EndrinDB 0.02 <0.02



mg/kg <0.02 <0.02g-BHCDB 0.02 <0.02








TE

1 78

Metals






mg/kg 8.4 8.7Lead 5 7.9




Miscellaneous








Date Sampled 10/07/2007 10/07/2007 10/07/2007

Miscellaneous



Customer Sample ID WV-B11 WV-B12 WV-B13


Date Sampled 10/07/2007 10/07/2007 10/07/2007

SVOC





mg/kg <0.02 <0.02AldrinDB 0.02 <0.02

mg/kg <0.02 <0.02b-BHCDB 0.02 <0.02


mg/kg <0.02 <0.02d-BHCDB 0.02 <0.02

mg/kg <0.02 <0.02DDDDB 0.02 <0.02

mg/kg <0.02 <0.02DDEDB 0.02 <0.02

mg/kg <0.02 <0.02DDTDB 0.02 <0.02

mg/kg <0.02 <0.02DieldrinDB 0.02 <0.02


mg/kg <0.02 <0.02EndrinDB 0.02 <0.02



mg/kg <0.02 <0.02g-BHCDB 0.02 <0.02








TE

1 85

Metals






mg/kg 7.4 7.7Lead 5 8.7




Miscellaneous






Customer Sample ID WV-B11 WV-B12 WV-B13


Date Sampled 10/07/2007 10/07/2007 10/07/2007

Miscellaneous



Customer Sample ID B1-SP1A B1-SP2A B1-SP3A


Date Sampled 10/07/2007 10/07/2007 10/07/2007

SVOC





mg/kg <0.02 <0.02AldrinDB 0.02 <0.02

mg/kg <0.02 <0.02b-BHCDB 0.02 <0.02


mg/kg <0.02 <0.02d-BHCDB 0.02 <0.02

mg/kg <0.02 <0.02DDDDB 0.02 <0.02

mg/kg 0.03 0.12DDEDB 0.02 0.04

mg/kg 0.13 0.53DDTDB 0.02 0.2

mg/kg 0.05 <0.02DieldrinDB 0.02 <0.02


mg/kg <0.02 <0.02EndrinDB 0.02 <0.02



mg/kg <0.02 <0.02g-BHCDB 0.02 <0.02








TE

1 86

Metals






mg/kg 190 12Lead 5 15


mg/kg 110 71Zinc 2 70


Miscellaneous








Date Sampled 10/07/2007 10/07/2007 10/07/2007

Miscellaneous





Date Sampled 10/07/2007 10/07/2007 10/07/2007

SVOC





mg/kg <0.02 <0.02AldrinDB 0.02 <0.02

mg/kg <0.02 <0.02b-BHCDB 0.02 <0.02


mg/kg <0.02 0.03d-BHCDB 0.02 <0.02

mg/kg <0.02 0.02DDDDB 0.02 <0.02

mg/kg 0.15 0.28DDEDB 0.02 0.13

mg/kg 0.84 1.1DDTDB 0.02 0.25

mg/kg <0.02 <0.02DieldrinDB 0.02 <0.02


mg/kg <0.02 <0.02EndrinDB 0.02 <0.02



mg/kg <0.02 <0.02g-BHCDB 0.02 <0.02








TE

1 77

Metals








mg/kg 100 110Zinc 2 67


Miscellaneous








Date Sampled 10/07/2007 10/07/2007 10/07/2007

Miscellaneous



Customer Sample ID B1-SP7A B1-SP8A DUP14


Date Sampled 10/07/2007 10/07/2007 10/07/2007

SVOC





mg/kg <0.02 <0.02AldrinDB 0.02 <0.02

mg/kg <0.02 <0.02b-BHCDB 0.02 <0.02


mg/kg <0.02 <0.02d-BHCDB 0.02 <0.02

mg/kg <0.02 <0.02DDDDB 0.02 0.06

mg/kg 0.08 <0.02DDEDB 0.02 0.31

mg/kg 0.12 <0.02DDTDB 0.02 1.4

mg/kg <0.02 <0.02DieldrinDB 0.02 <0.02


mg/kg <0.02 <0.02EndrinDB 0.02 <0.02



mg/kg <0.02 <0.02g-BHCDB 0.02 <0.02








TE

1 88

Metals






mg/kg 13 8.3Lead 5 19


mg/kg 72 44Zinc 2 130

3400 Total Mercury in Soil by ICP-AES mg/kg 0.09 <0.05Total Mercury 0.05 0.11

Miscellaneous






Customer Sample ID B1-SP7A B1-SP8A DUP14


Date Sampled 10/07/2007 10/07/2007 10/07/2007

Miscellaneous



Customer Sample ID DUP15 DUP16 TB-100707


Date Sampled 10/07/2007 10/07/2007 10/07/2007

SVOC


2300 OC Pesticides in Water by GC-ECD µg/L - <1a-BHC 1 -

µg/L - <1a-Chlordane 1 -

µg/L - <1a-Endosulphan 1 -

µg/L - <1Aldrin 1 -

µg/L - <2b-BHC 2 -

µg/L - <1b-Endosulphan 1 -

µg/L - <1d-BHC 1 -

µg/L - <1DDD 1 -

µg/L - <1DDE 1 -

µg/L - <1DDT 1 -

µg/L - <1Dieldrin 1 -

µg/L - <1Endosulfan sulfate 1 -

µg/L - <1Endrin 1 -

µg/L - <2Endrin Aldehyde 2 -

µg/L - <1g-BHC Lindane 1 -

µg/L - <1g-Chlordane 1 -

µg/L - <1Heptachlor 1 -

µg/L - <1Heptachlor epoxide 1 -

µg/L - <1Hexachlorobenzene (HCB) 1 -

µg/L - <2Methoxychlor 2 -

µg/L - <1Oxychlordane 1 -

% - 1032.4.5.6-tetrachloro-m-xylene-SURROGA

TE

1 -

2300 OC Pest in Soil (Low Level) GC-ECD mg/kg <0.02 -a-BHCDB 0.02 <0.02

mg/kg <0.02 -a-ChlordaneDB 0.02 <0.02

mg/kg <0.02 -a-EndosulfanDB 0.02 <0.02

mg/kg <0.02 -AldrinDB 0.02 <0.02

mg/kg <0.02 -b-BHCDB 0.02 <0.02

mg/kg <0.02 -b-EndosulfanDB 0.02 <0.02

mg/kg <0.02 -d-BHCDB 0.02 <0.02

mg/kg 0.03 -DDDDB 0.02 <0.02

mg/kg 0.05 -DDEDB 0.02 <0.02

mg/kg 0.2 -DDTDB 0.02 <0.02

mg/kg <0.02 -DieldrinDB 0.02 <0.02

mg/kg <0.02 -Endosulfan sulfateDB 0.02 <0.02

mg/kg <0.02 -EndrinDB 0.02 <0.02

mg/kg <0.02 -Endrin AldehydeDB 0.02 <0.02

mg/kg <0.02 -Endrin KetoneDB 0.02 <0.02





Customer Sample ID DUP15 DUP16 TB-100707


Date Sampled 10/07/2007 10/07/2007 10/07/2007

SVOC


mg/kg <0.02 -g-BHCDB 0.02 <0.02

mg/kg <0.02 -g-ChlordaneDB 0.02 <0.02

mg/kg <0.02 -HeptachlorDB 0.02 <0.02

mg/kg <0.02 -Heptachlor epoxideDB 0.02 <0.02

mg/kg <0.02 -Hexachlorobenzene (HCB)DB 0.02 <0.02

mg/kg <0.02 -MethoxychlorDB 0.02 <0.02

mg/kg <0.02 -OxychlordaneDB 0.02 <0.02

% 76 -2.4.5.6-tetrachloro-m-xylene-SURROGA

TE

1 77

Metals


3300 Dissolved Metals in Water by AAS µg/L - <1Arsenic 1 -


µg/L - <1Lead 1 -

3200 Total Metals in Soil by ICP/AES mg/kg 4.1 -Arsenic 3 3.4

mg/kg <1 -Cadmium 1 <1

mg/kg 23 -Chromium 2 29

mg/kg 17 -Copper 1 13

mg/kg 14 -Lead 5 7.0

mg/kg 15 -Nickel 2 16

mg/kg 100 -Zinc 2 38

3400 Total Mercury in Soil by ICP-AES mg/kg <0.05 -Total Mercury 0.05 <0.05

3200 Dissolved Metals in Water - ICP/AES µg/L - <1Chromium 1 -



µg/L - <5Zinc 5 -

3400 Dissolved Mercury in Water by ICPA µg/L - <1Mercury 1 -

Miscellaneous


5000 Moisture Content % 11 -% Moisture 1 10

Customer Sample ID FB-100707 RB-100707

Amdel Sample Number 538013 538014

Date Sampled 10/07/2007 10/07/2007

SVOC


2300 OC Pesticides in Water by GC-ECD µg/L <1a-BHC 1 <1

µg/L <1a-Chlordane 1 <1

µg/L <1a-Endosulphan 1 <1

µg/L <1Aldrin 1 <1







Date Sampled 10/07/2007 10/07/2007

SVOC


µg/L <2b-BHC 2 <2

µg/L <1b-Endosulphan 1 <1

µg/L <1d-BHC 1 <1

µg/L <1DDD 1 <1

µg/L <1DDE 1 <1

µg/L <1DDT 1 <1

µg/L <1Dieldrin 1 <1

µg/L <1Endosulfan sulfate 1 <1

µg/L <1Endrin 1 <1

µg/L <2Endrin Aldehyde 2 <2

µg/L <1g-BHC Lindane 1 <1

µg/L <1g-Chlordane 1 <1

µg/L <1Heptachlor 1 <1

µg/L <1Heptachlor epoxide 1 <1

µg/L <1Hexachlorobenzene (HCB) 1 <1

µg/L <2Methoxychlor 2 <2

µg/L <1Oxychlordane 1 <1

% 1052.4.5.6-tetrachloro-m-xylene-SURROGA

TE

1 106

Metals


3300 Dissolved Metals in Water by AAS µg/L <1Arsenic 1 <1

µg/L <0.1Cadmium 0.1 <0.1

µg/L <1Lead 1 <1

3200 Dissolved Metals in Water - ICP/AES µg/L <1Chromium 1 <1

µg/L <2Copper 2 <2

µg/L <5Nickel 5 <5

µg/L <5Zinc 5 <5

3400 Dissolved Mercury in Water by ICPA µg/L <1Mercury 1 <1

Sample History



2300 OC Pest in Soil (Low Level) GC-ECD 13/07/2007 18/07/2007

2300 OC Pesticides in Water by GC-ECD 13/07/2007












General










Holding Times









Acceptance

LimitsResult 1UnitsSample, Test, Result ReferencePass

Limits

Qualifying

Codes







Lead mg/kg <5 < 5 T


Zinc mg/kg <2 < 2 T







Lead mg/kg <5 < 5 T


Zinc mg/kg <2 < 2 T






Mercury mg/kg <0.05 < 0.05 T Q15






Zinc µg/L <5 < 5 T









Acceptance


Limits

Qualifying

Codes





Lead µg/L <1 < 1 T



Arsenic mg/kg 49 50.0 97 70-130 % T

Cadmium mg/kg 51 50.0 101 70-130 % T

Chromium mg/kg 50 50.0 101 70-130 % T

Copper mg/kg 51 50.0 101 70-130 % T

Lead mg/kg 51 50.0 101 70-130 % T

Nickel mg/kg 49 50.0 98 70-130 % T

Zinc mg/kg 49 50.0 99 70-130 % T



Arsenic mg/kg 47 50.0 94 70-130 % T

Cadmium mg/kg 50 50.0 99 70-130 % T

Chromium mg/kg 49 50.0 99 70-130 % T

Copper mg/kg 50 50.0 100 70-130 % T

Lead mg/kg 49 50.0 99 70-130 % T

Nickel mg/kg 48 50.0 96 70-130 % T

Zinc mg/kg 49 50.0 97 70-130 % T



Mercury mg/kg 0.45 N/A N/A N/A N/A






Chromium µg/L 950 1000.0 95 80-120 % T

Copper µg/L 960 1000.0 96 80-120 % T

Nickel µg/L 960 1000.0 96 80-120 % T

Zinc µg/L 1000 1000.0 101 80-120 % T



Mercury µg/L 10.0 0.01 100 80-120 % T



Arsenic µg/L 10 10.0 104.1 80-120 % T

Cadmium µg/L 2.1 2.0 103.55 80-120 % T

Lead µg/L 11 10.0 109.46 80-120 % T

538655 [ Duplicate of 538007 ]






LeadDB mg/kg 19 19 2 0-30 % T

NickelDB mg/kg 16 20 23 0-30 % T

ZincDB mg/kg 110 130 14 0-30 % T






Acceptance


Limits

Qualifying

Codes

538656 [ Duplicate of 538004 ]




ChromiumDB mg/kg 30 30 <1 0-30 % T


LeadDB mg/kg 10.0 10 4 0-30 % T


ZincDB mg/kg 81 67 19 0-30 % T

538657 [ Duplicate of 537995 ]





CopperDB mg/kg 17 17 <1 0-30 % T

LeadDB mg/kg 8.8 8.7 1 0-30 % T

NickelDB mg/kg 23 23 <1 0-30 % T

ZincDB mg/kg 48 50 5 0-30 % T

538658 [ Duplicate of 538007 ]


MercuryDB mg/kg 0.09 0.11 N/A N/A N/A

538659 [ Duplicate of 538004 ]


MercuryDB mg/kg 0.11 <0.05 73 0-30 % F Q15

538660 [ Duplicate of 537995 ]


MercuryDB mg/kg <0.05 <0.05 N/A N/A N/A

538665 [ Spike of 537992 ]









538666 [ Spike of 538006 ]









538667 [ Spike of 537992 ]



538668 [ Spike of 538006 ]



Laboratory: EN_PREP

Acceptance


Limits

Qualifying

Codes

538662 [ Duplicate of 538251 ]

5000 Moisture Content Result 2 RPD

%Moisture % 10 10 N/A N/A N/A





Laboratory: EN_PREP

Acceptance


Limits

Qualifying

Codes

538663 [ Duplicate of 538215 ]



538664 [ Duplicate of 538236 ]



538669 [ Spike of 538229 ]

5000 Moisture Content Spike Value Percent Recovery

%Moisture % 8 N/A N/A N/A N/A

538670 [ Spike of 538227 ]



Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes


2300 OC Pesticides in Water by GC-ECD

a-BHC µg/L <1 < 1 T

a-Chlordane µg/L <1 < 1 T

a-Endosulphan µg/L <1 < 1 T

Aldrin µg/L <1 < 1 T

b-BHC µg/L <2 < 2 T

b-Endosulphan µg/L <1 < 1 T

d-BHC µg/L <1 < 1 T

DDD µg/L <1 < 1 T

DDE µg/L <1 < 1 T

DDT µg/L <1 < 1 T

Dieldrin µg/L <1 < 1 T

Endosulfan sulfate µg/L <1 < 1 T

Endrin µg/L <1 < 1 T

Endrin Aldehyde µg/L <2 < 2 T

g-BHC Lindane µg/L <1 < 1 T

g-Chlordane µg/L <1 < 1 T

Heptachlor µg/L <1 < 1 T

Heptachlor epoxide µg/L <1 < 1 T

Hexachlorobenzene (HCB) µg/L <1 < 1 T

Methoxychlor µg/L <2 < 2 T

Oxychlordane µg/L <1 < 1 T

2.4.5.6-tetrachloro-m-xylene-SURROGATE % 97 70-130 % T





Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes


2300 OC Pest in Soil (Low Level) GC-ECD

a-BHC mg/kg <0.02 < 0.02 T

a-Chlordane mg/kg <0.02 < 0.02 T

a-Endosulfan mg/kg <0.02 < 0.02 T

Aldrin mg/kg <0.02 < 0.02 T

b-BHC mg/kg <0.02 < 0.02 T

b-Endosulfan mg/kg <0.02 < 0.02 T

d-BHC mg/kg <0.02 < 0.02 T

DDD mg/kg <0.02 < 0.02 T

DDE - <0.02 < 0.02 T

DDT mg/kg <0.02 < 0.02 T

Dieldrin mg/kg <0.02 < 0.02 T

Endosulfan sulfate mg/kg <0.02 < 0.02 T

Endrin mg/kg <0.02 < 0.02 T

Endrin Aldehyde mg/kg <0.02 < 0.02 T

Endrin Ketone mg/kg <0.02 < 0.02 T

g-BHC mg/kg <0.02 < 0.02 T

g-Chlordane mg/kg <0.02 < 0.02 T

Heptachlor mg/kg <0.02 < 0.02 T

Heptachlor epoxide mg/kg <0.02 < 0.02 T

Hexachlorobenzene (HCB) mg/kg <0.02 < 0.02 T

Methoxychlor mg/kg <0.02 < 0.02 T

Oxychlordane mg/kg <0.02 < 0.02 T

Trans-Nonachlor mg/kg <0.02 < 0.02 T




a-BHC mg/kg <0.02 < 0.02 T




b-BHC mg/kg <0.02 < 0.02 T


d-BHC mg/kg <0.02 < 0.02 T

DDD mg/kg <0.02 < 0.02 T

DDE - <0.02 < 0.02 T

DDT mg/kg <0.02 < 0.02 T






g-BHC mg/kg <0.02 < 0.02 T













Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes


2300 OC Pesticides in Water by GC-ECD Expected Value Percent Recovery

a-BHC µg/L 4.5 4.0 111 70-130 % T

a-Chlordane µg/L 4.6 4.0 114 70-130 % T

a-Endosulphan µg/L 4.8 4.0 121 70-130 % T

Aldrin µg/L 4.4 4.0 109 70-130 % T

b-BHC µg/L 4.6 4.0 115 70-130 % T

b-Endosulphan µg/L 4.4 4.0 109 70-130 % T

d-BHC µg/L 5.1 4.0 128 70-130 % T

DDD µg/L 4.3 4.0 106 70-130 % T

DDE µg/L 4.6 4.0 114 70-130 % T

DDT µg/L 4.6 4.0 114 70-130 % T

Dieldrin µg/L 5.0 4.0 125 70-130 % T

Endosulfan sulfate µg/L 4.4 4.0 109 70-130 % T

Endrin µg/L 4.5 4.0 112 70-130 % T

Endrin Aldehyde µg/L 4.9 4.0 123 70-130 % T

g-BHC Lindane µg/L 4.5 4.0 112 70-130 % T

g-Chlordane µg/L 4.2 4.0 104 70-130 % T

Heptachlor µg/L 3.8 4.0 94 70-130 % T

Heptachlor epoxide µg/L 3.9 4.0 97 70-130 % T

Hexachlorobenzene (HCB) µg/L <1 N/A N/A N/A N/A

Methoxychlor µg/L 3.7 4.0 94 70-130 % T

Oxychlordane µg/L <1 N/A N/A N/A N/A

2.4.5.6-tetrachloro-m-xylene-SURROGATE % 108 N/A N/A 70-130 % T


2300 OC Pest in Soil (Low Level) GC-ECD Expected Value Percent Recovery

a-BHC mg/kg 0.05 0.05 94 70-130 % T

a-Chlordane mg/kg 0.04 0.05 86 70-130 % T

a-Endosulfan mg/kg 1.1 N/A 106 70-130 % T

Aldrin mg/kg 0.04 0.05 90 70-130 % T

b-BHC mg/kg 0.04 0.05 79 70-130 % T

b-Endosulfan mg/kg 1.0 N/A 103 70-130 % T

d-BHC mg/kg 0.05 0.05 97 70-130 % T

DDD mg/kg 0.09 0.1 87 70-130 % T

DDE - 0.09 0.1 86 70-130 % T

DDT mg/kg 0.12 0.1 124 70-130 % T

Dieldrin mg/kg 0.03 0.05 67 70-130 % F Q13

Endosulfan sulfate mg/kg 0.04 0.05 77 70-130 % T

Endrin mg/kg 0.05 0.05 94 70-130 % T

Endrin Aldehyde mg/kg 1.1 N/A 108 70-130 % T

Endrin Ketone mg/kg 1.0635 N/A 106 70-130 % T

g-BHC mg/kg 0.05 0.05 95 70-130 % T

g-Chlordane mg/kg 0.05 0.05 90 70-130 % T

Heptachlor mg/kg 0.05 0.05 97 70-130 % T

Heptachlor epoxide mg/kg 0.04 0.05 84 70-130 % T

Methoxychlor mg/kg 0.05 0.05 99 70-130 % T






Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes



a-BHC mg/kg 0.06 0.05 118 70-130 % T


a-Endosulfan mg/kg 1.0 N/A 102 70-130 % T

Aldrin mg/kg 0.05 0.05 107 70-130 % T

b-BHC mg/kg 0.05 0.05 95 70-130 % T

b-Endosulfan mg/kg 0.96 N/A 96 70-130 % T

d-BHC mg/kg 0.06 0.05 116 70-130 % T

DDD mg/kg 0.11 0.1 106 70-130 % T

DDE - 0.1 0.1 105 70-130 % T

DDT mg/kg 0.15 0.1 149 70-130 % F

Dieldrin mg/kg 0.04 0.05 82 70-130 % T


Endrin mg/kg 0.06 0.05 111 70-130 % T

Endrin Aldehyde mg/kg 1.1 N/A 113 70-130 % T

Endrin Ketone mg/kg 0.970333 N/A 97 70-130 % T

g-BHC mg/kg 0.06 0.05 115 70-130 % T






538662 [ Duplicate of 538251 ]

2300 OC Pest in Soil (Low Level) GC-ECD Result 2 RPD

a-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T

a-ChlordaneDB mg/kg <0.02 <0.02 <1 0-30 % T

a-EndosulfanDB mg/kg <0.02 <0.02 <1 0-30 % T

AldrinDB mg/kg <0.02 <0.02 <1 0-30 % T

b-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T

b-EndosulfanDB mg/kg <0.02 <0.02 <1 0-30 % T

d-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T

DDDDB mg/kg <0.02 <0.02 <1 0-30 % T

DDEDB mg/kg <0.02 <0.02 <1 0-30 % T

DDTDB mg/kg <0.02 <0.02 <1 0-30 % T

DieldrinDB mg/kg <0.02 <0.02 <1 0-30 % T

Endosulfan sulfateDB mg/kg <0.02 <0.02 <1 0-30 % T

Endrin AldehydeDB mg/kg <0.02 <0.02 <1 0-30 % T

Endrin KetoneDB mg/kg <0.02 <0.02 <1 0-30 % T

EndrinDB mg/kg <0.02 <0.02 <1 0-30 % T

g-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T

g-ChlordaneDB mg/kg <0.02 <0.02 <1 0-30 % T

Heptachlor epoxideDB mg/kg <0.02 <0.02 <1 0-30 % T

HeptachlorDB mg/kg <0.02 <0.02 <1 0-30 % T

Hexachlorobenzene (HCB)DB mg/kg <0.02 <0.02 <1 0-30 % T

MethoxychlorDB mg/kg <0.02 <0.02 <1 0-30 % T

OxychlordaneDB mg/kg <0.02 <0.02 <1 0-30 % T






Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes

538663 [ Duplicate of 538215 ]


a-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T



AldrinDB mg/kg <0.02 <0.02 <1 0-30 % T

b-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T


d-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T

DDDDB mg/kg <0.02 <0.02 <1 0-30 % T

DDEDB mg/kg <0.02 <0.02 <1 0-30 % T

DDTDB mg/kg <0.02 <0.02 <1 0-30 % T





EndrinDB mg/kg <0.02 <0.02 <1 0-30 % T

g-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T








538664 [ Duplicate of 538236 ]


a-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T



AldrinDB mg/kg <0.02 <0.02 <1 0-30 % T

b-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T


d-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T

DDDDB mg/kg 0.05 <0.02 83 0-30 % F Q02

DDEDB mg/kg 0.14 0.12 16 0-30 % T

DDTDB mg/kg 0.95 0.53 57 0-30 % F Q02





EndrinDB mg/kg <0.02 <0.02 <1 0-30 % T

g-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T












Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes

538669 [ Spike of 538229 ]

2300 OC Pest in Soil (Low Level) GC-ECD Spike Value Percent Recovery

a-BHCDB mg/kg 0.06 N/A N/A N/A N/A

a-ChlordaneDB mg/kg 0.05 N/A N/A N/A N/A

a-EndosulfanDB mg/kg 1.1 N/A N/A N/A N/A

AldrinDB mg/kg 0.06 N/A N/A N/A N/A

b-BHCDB mg/kg 0.05 N/A N/A N/A N/A

b-EndosulfanDB mg/kg 1.0 N/A N/A N/A N/A

d-BHCDB mg/kg 0.06 N/A N/A N/A N/A

DDDDB mg/kg 0.1 N/A N/A N/A N/A

DDEDB mg/kg 0.1 N/A N/A N/A N/A

DDTDB mg/kg 0.14 N/A N/A N/A N/A Q13

DieldrinDB mg/kg 0.06 N/A N/A N/A N/A

Endosulfan sulfateDB mg/kg 0.05 N/A N/A N/A N/A

Endrin AldehydeDB mg/kg 1.1 N/A N/A N/A N/A

Endrin KetoneDB mg/kg 1.1 N/A N/A N/A N/A

EndrinDB mg/kg 0.06 N/A N/A N/A N/A

g-BHCDB mg/kg 0.06 N/A N/A N/A N/A

g-ChlordaneDB mg/kg 0.06 N/A N/A N/A N/A

Heptachlor epoxideDB mg/kg 0.05 N/A N/A N/A N/A

HeptachlorDB mg/kg 0.05 N/A N/A N/A N/A

MethoxychlorDB mg/kg 0.05 N/A N/A N/A N/A


538670 [ Spike of 538227 ]























Sample Integrity







YesSome samples have been subcontracted






DescriptionCode



Q13 Some individual compounds for this analysis have failed. However the QC sample is considered acceptable if 80% of

the compounds meet Acceptance Criteria.



Authorised By

Accreditation Number: 1464Anthony Crane Operations Manager


Laboratory Manager


Final Report















Client Reference number: Turnaround: Standard06155C



Job Information

Sample Integrity






Some samples have been subcontracted Yes


Analysis Requested








2300OC Pesticides in Water by GC-ECD 3

2300OC Pest in Soil (Low Level) GC-ECD 23

538662 538663 538664 538669 538670

Note













Logged in by : Jane Walker Date : Wed 11 July 2007









79 Doggett Street


Australia




Order Number LA70

Received Date 12/07/2007 08:00:00 AM

Customer Sample ID B1-SP1B B1-SP2B B1-SP3B


Date Sampled 11/07/2007 11/07/2007 11/07/2007

SVOC





mg/kg <1.0 <0.1AldrinDB 0.02 <1.0

mg/kg <0.02 <0.1b-BHCDB 0.02 <0.02


mg/kg <40.0 <0.1d-BHCDB 0.02 <1.0

mg/kg 45 1.1DDDDB 0.02 1.5

mg/kg <40.0 0.27DDEDB 0.02 <1.0

mg/kg 130 2.1DDTDB 0.02 4.3

mg/kg <40.0 <0.1DieldrinDB 0.02 <1.0


mg/kg <40.0 <0.1EndrinDB 0.02 <1.0



mg/kg <40.0 <0.1g-BHCDB 0.02 <1.0







mg/kg <0.02 <0.02Trans-NonachlorDB 0.02 <0.02

% <1 122.4.5.6-tetrachloro-m-xylene-SURROGA

TE

1 Q11 Q1114 Q11

Metals








mg/kg 100 98Zinc 2 100








Date Sampled 11/07/2007 11/07/2007 11/07/2007

Metals



Miscellaneous





Date Sampled 11/07/2007 11/07/2007 11/07/2007

SVOC





mg/kg <0.02 <0.1AldrinDB 0.02 <0.02

mg/kg <0.02 <0.1b-BHCDB 0.02 <0.02

mg/kg <0.02 <0.1b-EndosulfanDB 0.02 0.06

mg/kg <0.02 <0.1d-BHCDB 0.02 <0.02

mg/kg <0.02 <0.1DDDDB 0.02 0.02

mg/kg 0.03 <0.1DDEDB 0.02 0.06

mg/kg <0.02 0.25DDTDB 0.02 0.05

mg/kg <0.02 <0.1DieldrinDB 0.02 <0.02


mg/kg <0.02 <0.1EndrinDB 0.02 <0.02



mg/kg <0.02 <0.1g-BHCDB 0.02 <0.02









TE

1 73 Q11

Metals








mg/kg 120 150Zinc 2 300







Date Sampled 11/07/2007 11/07/2007 11/07/2007

Metals



Miscellaneous





Date Sampled 11/07/2007 11/07/2007 11/07/2007

SVOC





mg/kg <0.02 <0.02AldrinDB 0.02 <0.02

mg/kg <0.02 <0.02b-BHCDB 0.02 <0.02


mg/kg <0.02 <0.02d-BHCDB 0.02 <0.02

mg/kg <0.02 <0.1DDDDB 0.02 <0.02

mg/kg 0.13 0.51DDEDB 0.02 0.11

mg/kg 0.07 0.27DDTDB 0.02 0.14

mg/kg <0.02 <0.1DieldrinDB 0.02 <0.02


mg/kg <0.02 <0.1EndrinDB 0.02 <0.02



mg/kg <0.02 <0.1g-BHCDB 0.02 <0.02









TE

1 92 Q11

Metals


3200 Total Metals in Soil by ICP/AES mg/kg 7.4 11Arsenic 3 6.8












Date Sampled 11/07/2007 11/07/2007 11/07/2007

Metals


mg/kg 100 260Zinc 2 130

3400 Total Mercury in Soil by ICP-AES mg/kg <0.05 0.08Total Mercury 0.05 <0.05

Miscellaneous





Date Sampled 11/07/2007 11/07/2007 11/07/2007

SVOC





mg/kg <0.02 <0.1AldrinDB 0.02 <0.02

mg/kg <0.02 <0.1b-BHCDB 0.02 <0.02


mg/kg <0.02 <0.1d-BHCDB 0.02 <0.02

mg/kg <0.02 <0.1DDDDB 0.02 <0.02

mg/kg 0.08 <0.1DDEDB 0.02 0.04

mg/kg 0.21 0.29DDTDB 0.02 0.1

mg/kg <0.02 <0.1DieldrinDB 0.02 <0.02


mg/kg <0.02 <0.1EndrinDB 0.02 <0.02



mg/kg <0.02 <0.1g-BHCDB 0.02 <0.02









TE

1 98 Q11

Metals













Date Sampled 11/07/2007 11/07/2007 11/07/2007

Metals



mg/kg 100 120Zinc 2 110


Miscellaneous





Date Sampled 11/07/2007 11/07/2007 11/07/2007

SVOC





mg/kg <0.02 <0.02AldrinDB 0.02 <0.02

mg/kg <0.02 <0.02b-BHCDB 0.02 <0.02


mg/kg <0.02 <0.02d-BHCDB 0.02 <0.02

mg/kg <0.02 <0.02DDDDB 0.02 <0.02

mg/kg 0.03 <0.02DDEDB 0.02 0.07

mg/kg 0.1 0.02DDTDB 0.02 0.11

mg/kg <0.02 <0.02DieldrinDB 0.02 <0.02


mg/kg <0.02 <0.02EndrinDB 0.02 <0.02



mg/kg <0.02 <0.02g-BHCDB 0.02 <0.02









TE

1 95

Metals












Date Sampled 11/07/2007 11/07/2007 11/07/2007

Metals




mg/kg 110 91Zinc 2 130

3400 Total Mercury in Soil by ICP-AES mg/kg 0.08 0.13Total Mercury 0.05 <0.05

Miscellaneous





Date Sampled 11/07/2007 11/07/2007 11/07/2007

SVOC





mg/kg <0.02 <0.02AldrinDB 0.02 <0.1

mg/kg <0.02 <0.02b-BHCDB 0.02 <0.1


mg/kg <0.02 <0.02d-BHCDB 0.02 <0.1

mg/kg <0.02 <0.02DDDDB 0.02 <0.1

mg/kg <0.02 <0.02DDEDB 0.02 <0.1

mg/kg <0.02 <0.02DDTDB 0.02 0.42

mg/kg <0.02 <0.02DieldrinDB 0.02 <0.1


mg/kg <0.02 <0.02EndrinDB 0.02 <0.1



mg/kg <0.02 <0.02g-BHCDB 0.02 <0.1









TE

1 Q11 18

Metals











Date Sampled 11/07/2007 11/07/2007 11/07/2007

Metals





mg/kg 100 110Zinc 2 100

3400 Total Mercury in Soil by ICP-AES mg/kg 0.06 0.12Total Mercury 0.05 0.18

Miscellaneous





Date Sampled 11/07/2007 11/07/2007 11/07/2007

SVOC





mg/kg <0.02 <0.02AldrinDB 0.02 <0.02

mg/kg <0.02 <0.02b-BHCDB 0.02 <0.02


mg/kg <0.02 <0.02d-BHCDB 0.02 <0.02

mg/kg <0.02 <0.02DDDDB 0.02 <0.02

mg/kg <0.02 <0.02DDEDB 0.02 <0.02

mg/kg 0.06 <0.02DDTDB 0.02 <0.02

mg/kg <0.02 <0.02DieldrinDB 0.02 <0.02


mg/kg <0.02 <0.02EndrinDB 0.02 <0.02



mg/kg <0.02 <0.02g-BHCDB 0.02 <0.02









TE

1 108

Metals










Date Sampled 11/07/2007 11/07/2007 11/07/2007

Metals






mg/kg 110 110Zinc 2 110

3400 Total Mercury in Soil by ICP-AES mg/kg <0.05 0.05Total Mercury 0.05 0.06

Miscellaneous





Date Sampled 11/07/2007 11/07/2007 11/07/2007

SVOC





mg/kg <0.02 <0.02AldrinDB 0.02 <0.02

mg/kg <0.02 <0.02b-BHCDB 0.02 <0.02


mg/kg <0.02 <0.02d-BHCDB 0.02 <0.02

mg/kg <0.02 <0.02DDDDB 0.02 <0.02

mg/kg 0.03 0.04DDEDB 0.02 0.02

mg/kg 0.03 0.1DDTDB 0.02 0.08

mg/kg <0.02 <0.02DieldrinDB 0.02 <0.02


mg/kg <0.02 <0.02EndrinDB 0.02 <0.02



mg/kg <0.02 <0.02g-BHCDB 0.02 <0.02









TE

1 105

Metals









Date Sampled 11/07/2007 11/07/2007 11/07/2007

Metals







mg/kg 110 110Zinc 2 120


Miscellaneous



Customer Sample ID B1-SP25B DUP20 DUP21


Date Sampled 11/07/2007 11/07/2007 11/07/2007

SVOC





mg/kg <0.1 <0.02AldrinDB 0.02 <0.02

mg/kg <0.1 <0.02b-BHCDB 0.02 <0.02


mg/kg <0.1 <0.02d-BHCDB 0.02 <0.02

mg/kg 0.52 <0.02DDDDB 0.02 <0.02

mg/kg 0.21 0.03DDEDB 0.02 <0.02

mg/kg 1.0 0.02DDTDB 0.02 <0.02

mg/kg <0.1 <0.02DieldrinDB 0.02 <0.02


mg/kg <0.1 <0.02EndrinDB 0.02 <0.02



mg/kg <0.1 <0.02g-BHCDB 0.02 <0.02









TE

1 Q1194

Metals







Customer Sample ID B1-SP25B DUP20 DUP21


Date Sampled 11/07/2007 11/07/2007 11/07/2007

Metals








mg/kg 110 99Zinc 2 90


Miscellaneous



Customer Sample ID DUP22 BV-B19 BV-B20


Date Sampled 11/07/2007 11/07/2007 11/07/2007

SVOC





mg/kg <0.02 <0.02AldrinDB 0.02 <0.02

mg/kg <0.02 <0.02b-BHCDB 0.02 <0.02


mg/kg <0.02 <0.02d-BHCDB 0.02 <0.02

mg/kg <0.02 <0.02DDDDB 0.02 <0.02

mg/kg <0.02 <0.02DDEDB 0.02 <0.02

mg/kg <0.02 <0.02DDTDB 0.02 <0.02

mg/kg <0.02 <0.02DieldrinDB 0.02 <0.02


mg/kg <0.02 <0.02EndrinDB 0.02 <0.02



mg/kg <0.02 <0.02g-BHCDB 0.02 <0.02









TE

1 100

Metals






Customer Sample ID DUP22 BV-B19 BV-B20


Date Sampled 11/07/2007 11/07/2007 11/07/2007

Metals






mg/kg 1500 59Lead 5 31


mg/kg 210 90Zinc 2 100


Miscellaneous





Date Sampled 11/07/2007 11/07/2007 11/07/2007

SVOC





mg/kg <0.02 <0.1AldrinDB 0.02 <0.02

mg/kg <0.02 <0.1b-BHCDB 0.02 <0.02


mg/kg <0.02 <0.1d-BHCDB 0.02 <0.02

mg/kg <0.02 <0.1DDDDB 0.02 <0.02

mg/kg <0.02 0.69DDEDB 0.02 <0.02

mg/kg <0.02 <0.1DDTDB 0.02 <0.02

mg/kg <0.02 <0.1DieldrinDB 0.02 <0.02


mg/kg <0.02 <0.1EndrinDB 0.02 <0.02



mg/kg <0.02 <0.1g-BHCDB 0.02 <0.02









TE

1 85 Q11

Metals







Date Sampled 11/07/2007 11/07/2007 11/07/2007

Metals






mg/kg 14 110Lead 5 170


mg/kg 55 140Zinc 2 120


Miscellaneous





Date Sampled 11/07/2007 11/07/2007 11/07/2007

SVOC





mg/kg <0.4 <0.1AldrinDB 0.02 <0.02

mg/kg <0.4 <0.1b-BHCDB 0.02 <0.02


mg/kg <0.4 <0.1d-BHCDB 0.02 <0.02

mg/kg <0.4 <0.1DDDDB 0.02 <0.02

mg/kg 1.3 0.28DDEDB 0.02 <0.02

mg/kg <0.4 <0.1DDTDB 0.02 <0.02

mg/kg <0.4 <0.1DieldrinDB 0.02 <0.02


mg/kg <0.4 <0.1EndrinDB 0.02 <0.02



mg/kg <0.4 <0.1g-BHCDB 0.02 <0.02









TE

1 Q1182

Metals







Date Sampled 11/07/2007 11/07/2007 11/07/2007

Metals






mg/kg 39 35Lead 5 8.0


mg/kg 120 150Zinc 2 48


Miscellaneous





Date Sampled 11/07/2007 11/07/2007 11/07/2007

SVOC





mg/kg <0.4 <0.02AldrinDB 0.02 <0.02

mg/kg <0.4 <0.02b-BHCDB 0.02 <0.02


mg/kg <0.4 0.02d-BHCDB 0.02 <0.02

mg/kg <0.4 <0.02DDDDB 0.02 0.15

mg/kg 1.5 <0.02DDEDB 0.02 <0.02

mg/kg <0.4 <0.02DDTDB 0.02 <0.02

mg/kg <0.4 <0.02DieldrinDB 0.02 <0.02


mg/kg <0.4 <0.02EndrinDB 0.02 <0.02



mg/kg <0.4 <0.02g-BHCDB 0.02 <0.02









TE

1 113

Metals







Date Sampled 11/07/2007 11/07/2007 11/07/2007

Metals






mg/kg 26 7.7Lead 5 17


mg/kg 110 53Zinc 2 83


Miscellaneous



Customer Sample ID WV-B1 DUP17 DUP18


Date Sampled 11/07/2007 11/07/2007 11/07/2007

SVOC





mg/kg <0.02 <0.02AldrinDB 0.02 <0.02

mg/kg <0.02 <0.02b-BHCDB 0.02 <0.02


mg/kg <0.02 <0.02d-BHCDB 0.02 <0.02

mg/kg <0.02 <0.02DDDDB 0.02 <0.02

mg/kg <0.02 <0.02DDEDB 0.02 <0.02

mg/kg <0.02 <0.02DDTDB 0.02 <0.02

mg/kg <0.02 <0.02DieldrinDB 0.02 <0.02


mg/kg <0.02 <0.02EndrinDB 0.02 <0.02



mg/kg 0.06 <0.02g-BHCDB 0.02 <0.02









TE

1 124

Metals





Customer Sample ID WV-B1 DUP17 DUP18


Date Sampled 11/07/2007 11/07/2007 11/07/2007

Metals








mg/kg 88 56Zinc 2 130


Miscellaneous



Customer Sample ID TB-110707 FB-110707 RB-110707


Date Sampled 11/07/2007 11/07/2007 11/07/2007

SVOC


2300 OC Pesticides in Water by GC-ECD µg/L <1 <1a-BHC 1 <1

µg/L <1 <1a-Chlordane 1 <1

µg/L <1 <1a-Endosulphan 1 <1

µg/L <1 <1Aldrin 1 <1

µg/L <2 <2b-BHC 2 <2

µg/L <1 <1b-Endosulphan 1 <1

µg/L <1 <1d-BHC 1 <1

µg/L <1 <1DDD 1 <1

µg/L <1 <1DDE 1 <1

µg/L <1 <1DDT 1 <1

µg/L <1 <1Dieldrin 1 <1

µg/L <1 <1Endosulfan sulfate 1 <1

µg/L <1 <1Endrin 1 <1

µg/L <2 <2Endrin Aldehyde 2 <2

µg/L <1 <1g-BHC Lindane 1 <1

µg/L <1 <1g-Chlordane 1 <1

µg/L <1 <1Heptachlor 1 <1

µg/L <1 <1Heptachlor epoxide 1 <1

µg/L <1 <1Hexachlorobenzene (HCB) 1 <1

µg/L <2 <2Methoxychlor 2 <2

µg/L <1 <1Oxychlordane 1 <1


TE

1 89

Metals







Customer Sample ID TB-110707 FB-110707 RB-110707


Date Sampled 11/07/2007 11/07/2007 11/07/2007

Metals


µg/L <1 <1Arsenic 1 <1

µg/L <0.1 <0.1Cadmium 0.1 <0.1

µg/L <1 <1Lead 1 <1

3200 Dissolved Metals in Water - ICP/AES µg/L 1.8 2.5Chromium 1 2.3

µg/L <2 <2Copper 2 <2

µg/L <5 <5Nickel 5 <5

µg/L 30 54Zinc 5 140

3400 Dissolved Mercury in Water by ICPA µg/L <1 <1Mercury 1 <1

Sample History



2300 OC Pest in Soil (Low Level) GC-ECD 27/07/2007







5000 Moisture Content 13/07/2007 13/07/2007






General










Holding Times









Acceptance


Limits

Qualifying

Codes







Lead mg/kg <5 < 5 T


Zinc mg/kg <2 < 2 T







Lead mg/kg <5 < 5 T


Zinc mg/kg <2 < 2 T







Lead mg/kg <5 < 5 T


Zinc mg/kg <2 < 2 T






Zinc µg/L <5 < 5 T






Acceptance


Limits

Qualifying

Codes



Mercury µg/L <1 < 1 T Q15





Lead µg/L <1 < 1 T












Arsenic mg/kg 51 50.0 102 70-130 % T

Cadmium mg/kg 52 50.0 104 70-130 % T

Chromium mg/kg 50 50.0 101 70-130 % T

Copper mg/kg 52 50.0 105 70-130 % T

Lead mg/kg 52 50.0 104 70-130 % T

Nickel mg/kg 51 50.0 101 70-130 % T

Zinc mg/kg 52 50.0 103 70-130 % T



Arsenic mg/kg 50 50.0 100 70-130 % T

Cadmium mg/kg 52 50.0 103 70-130 % T

Chromium mg/kg 50 50.0 100 70-130 % T

Copper mg/kg 52 50.0 103 70-130 % T

Lead mg/kg 51 50.0 103 70-130 % T

Nickel mg/kg 50 50.0 100 70-130 % T

Zinc mg/kg 51 50.0 103 70-130 % T



Arsenic mg/kg 49 50.0 98 70-130 % T

Cadmium mg/kg 50 50.0 100 70-130 % T

Chromium mg/kg 49 50.0 98 70-130 % T

Copper mg/kg 51 50.0 102 70-130 % T

Lead mg/kg 50 50.0 100 70-130 % T

Nickel mg/kg 49 50.0 97 70-130 % T

Zinc mg/kg 51 50.0 101 70-130 % T



Chromium µg/L 980 1000.0 98 80-120 % T

Copper µg/L 1000 1000.0 102 80-120 % T

Nickel µg/L 1000 1000.0 100 80-120 % T

Zinc µg/L 1100 1000.0 107 80-120 % T



Mercury µg/L 8.95 0.01 90 80-120 % T



Arsenic µg/L 10 10.0 104.1 80-120 % T

Cadmium µg/L 2.1 2.0 103.55 80-120 % T

Lead µg/L 11 10.0 109.46 80-120 % T






Acceptance


Limits

Qualifying

Codes









Mercury mg/kg 0.54 0.5 109 75-125 % T

540550 [ Duplicate of 539307 ]






LeadDB mg/kg 17 23 28 0-30 % T


ZincDB mg/kg 96 110 14 0-30 % T

540551 [ Duplicate of 539345 ]






LeadDB mg/kg 11 12 6 0-30 % T


ZincDB mg/kg 57 56 1 0-30 % T

540552 [ Duplicate of 539301 ]






LeadDB mg/kg 31 42 31 0-30 % F Q15


ZincDB mg/kg 110 100 7 0-30 % T

540553 [ Duplicate of 539338 ]






LeadDB mg/kg 50 39 24 0-30 % T


ZincDB mg/kg 130 120 7 0-30 % T

540554 [ Duplicate of 539313 ]





CopperDB mg/kg 30 52 54 0-30 % F Q02

LeadDB mg/kg 28 30 7 0-30 % T


ZincDB mg/kg 100 110 2 0-30 % T

540555 [ Duplicate of 539307 ]


MercuryDB mg/kg 0.09 0.08 6 0-30 % T






Acceptance


Limits

Qualifying

Codes

540556 [ Duplicate of 539345 ]


MercuryDB mg/kg 0.05 0.07 33 0-30 % F Q15

540557 [ Duplicate of 539301 ]


MercuryDB mg/kg <0.05 <0.05 <0.05 0-30 % T

540558 [ Duplicate of 539338 ]



540559 [ Duplicate of 539313 ]


MercuryDB mg/kg 0.06 <0.05 13 0-30 % T

540565 [ Spike of 539315 ]









540566 [ Spike of 539295 ]









540567 [ Spike of 539318 ]









540568 [ Spike of 539315 ]



540569 [ Spike of 539295 ]



540570 [ Spike of 539318 ]



Laboratory: EN_PREP

Acceptance


Limits

Qualifying

Codes

540560 [ Duplicate of 539406 ]



540561 [ Duplicate of 539405 ]







Laboratory: EN_PREP

Acceptance


Limits

Qualifying

Codes

540562 [ Duplicate of 539377 ]



540563 [ Duplicate of 539414 ]



540564 [ Duplicate of 539387 ]



540571 [ Spike of 539383 ]



540572 [ Spike of 539408 ]



540573 [ Spike of 539415 ]



Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes



a-BHC mg/kg <0.02 < 0.02 T




b-BHC mg/kg <0.02 < 0.02 T


d-BHC mg/kg <0.02 < 0.02 T

DDD mg/kg <0.02 < 0.02 T

DDE - <0.02 < 0.02 T

DDT mg/kg <0.02 < 0.02 T






g-BHC mg/kg <0.02 < 0.02 T













Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes



a-BHC mg/kg <0.02 < 0.02 T




b-BHC mg/kg <0.02 < 0.02 T


d-BHC mg/kg <0.02 < 0.02 T

DDD mg/kg <0.02 < 0.02 T

DDE - <0.02 < 0.02 T

DDT mg/kg <0.02 < 0.02 T






g-BHC mg/kg <0.02 < 0.02 T











a-BHC mg/kg <0.02 < 0.02 T




b-BHC mg/kg <0.02 < 0.02 T


d-BHC mg/kg <0.02 < 0.02 T

DDD mg/kg <0.02 < 0.02 T

DDE - <0.02 < 0.02 T

DDT mg/kg <0.02 < 0.02 T






g-BHC mg/kg <0.02 < 0.02 T













Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes










DDD µg/L <1 < 1 T

DDE µg/L <1 < 1 T

DDT µg/L <1 < 1 T















a-BHC mg/kg 0.04 0.05 84 70-130 % T


a-Endosulfan mg/kg N/A N/A N/A N/A

Aldrin mg/kg 0.04 0.05 78 70-130 % T

b-BHC mg/kg 0.04 0.05 72 70-130 % T

d-BHC mg/kg 0.04 0.05 84 70-130 % T

DDD mg/kg 0.07 0.1 70 70-130 % T

DDE - 0.07 0.1 74 70-130 % T

DDT mg/kg 0.09 0.1 92 70-130 % T

Dieldrin mg/kg 0.04 0.05 74 70-130 % T


Endrin mg/kg 0.04 0.05 80 70-130 % T

Endrin Aldehyde mg/kg N/A N/A N/A N/A

Endrin Ketone mg/kg N/A N/A N/A N/A

g-BHC mg/kg 0.04 0.05 82 70-130 % T





Oxychlordane mg/kg N/A N/A N/A N/A

Trans-Nonachlor mg/kg N/A N/A N/A N/A






Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes



a-BHC mg/kg 0.04 0.05 84 70-130 % T


a-Endosulfan mg/kg N/A N/A N/A N/A

Aldrin mg/kg 0.04 0.05 78 70-130 % T

b-BHC mg/kg 0.04 0.05 72 70-130 % T

b-Endosulfan mg/kg N/A N/A N/A N/A

d-BHC mg/kg 0.04 0.05 82 70-130 % T

DDD mg/kg 0.11 0.1 112 70-130 % T

DDE - 0.08 0.1 77 70-130 % T

DDT mg/kg 0.1 0.1 104 70-130 % T

Dieldrin mg/kg 0.04 0.05 78 70-130 % T


Endrin mg/kg 0.04 0.05 82 70-130 % T

Endrin Aldehyde mg/kg N/A N/A N/A N/A

Endrin Ketone mg/kg N/A N/A N/A N/A

g-BHC mg/kg 0.04 0.05 82 70-130 % T





Oxychlordane mg/kg N/A N/A N/A N/A





a-BHC mg/kg 0.04 0.05 82 70-130 % T


Aldrin mg/kg 0.04 0.05 78 70-130 % T

b-BHC mg/kg 0.04 0.05 70 70-130 % T

d-BHC mg/kg 0.04 0.05 80 70-130 % T

DDD mg/kg 0.07 0.1 74 70-130 % T

DDE - 0.08 0.1 84 70-130 % T

DDT mg/kg 0.1 0.1 96 70-130 % T

Dieldrin mg/kg 0.04 0.05 86 70-130 % T

Endosulfan sulfate mg/kg 0.03 0.05 66 70-130 % F Q13

Endrin mg/kg 0.05 0.05 90 70-130 % T

g-BHC mg/kg 0.04 0.05 78 70-130 % T











Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes



a-BHC µg/L 4.8 4.0 120 70-130 % T

a-Chlordane µg/L 4.5 4.0 112 70-130 % T


Aldrin µg/L 4.3 4.0 107 70-130 % T

b-BHC µg/L 5.1 4.0 127 70-130 % T


d-BHC µg/L 5.7 4.0 141 70-130 % F Q13

DDD µg/L 4.7 4.0 118 70-130 % T

DDE µg/L 4.4 4.0 111 70-130 % T

DDT µg/L 3.9 4.0 98 70-130 % T

Dieldrin µg/L 4.6 4.0 116 70-130 % T


Endrin µg/L 4.9 4.0 124 70-130 % T



g-Chlordane µg/L 4.5 4.0 114 70-130 % T

Heptachlor µg/L 4.3 4.0 108 70-130 % T






540560 [ Duplicate of 539406 ]


a-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T



AldrinDB mg/kg <0.02 <0.02 <1 0-30 % T

b-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T


d-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T

DDDDB mg/kg <0.02 <0.02 <1 0-30 % T

DDEDB mg/kg <0.02 <0.02 <1 0-30 % T

DDTDB mg/kg <0.02 <0.02 <1 0-30 % T





EndrinDB mg/kg <0.02 <0.02 <1 0-30 % T

g-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T







Trans-NonachlorDB mg/kg <0.02 <0.02 <1 0-30 % T






Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes

540561 [ Duplicate of 539405 ]


a-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T



AldrinDB mg/kg <0.02 <0.02 <1 0-30 % T

b-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T


d-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T

DDDDB mg/kg <0.02 <0.02 <1 0-30 % T

DDEDB mg/kg <0.02 <0.02 <1 0-30 % T

DDTDB mg/kg <0.02 <0.02 <1 0-30 % T





EndrinDB mg/kg <0.02 <0.02 <1 0-30 % T

g-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T









540562 [ Duplicate of 539377 ]


a-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T



AldrinDB mg/kg <0.02 <0.02 <1 0-30 % T

b-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T

b-EndosulfanDB mg/kg 0.03 0.06 48 0-30 % F Q15

d-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T

DDDDB mg/kg 0.03 0.02 18 0-30 % T

DDEDB mg/kg 0.03 0.06 68 0-30 % F Q15

DDTDB mg/kg 0.06 0.05 28 0-30 % T





EndrinDB mg/kg <0.02 <0.02 <1 0-30 % T

g-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T













Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes

540563 [ Duplicate of 539414 ]


a-BHCDB mg/kg <0.1 <0.1 <1 0-30 % T



AldrinDB mg/kg <0.1 <0.1 <1 0-30 % T

b-BHCDB mg/kg <0.1 <0.1 <1 0-30 % T


d-BHCDB mg/kg <0.1 <0.1 <1 0-30 % T

DDDDB mg/kg <0.1 <0.1 9 0-30 % T

DDEDB mg/kg 0.58 0.28 70 0-30 % F

DDTDB mg/kg <0.1 <0.1 <1 0-30 % T





EndrinDB mg/kg <0.1 <0.1 <1 0-30 % T

g-BHCDB mg/kg <0.1 <0.1 <1 0-30 % T








2.4.5.6-tetrachloro-m-xylene-SURROGATE % 10 N/A N/A 70-130 % F

540564 [ Duplicate of 539387 ]


a-BHCDB mg/kg <0.02 <0.1 <1 0-30 % T



AldrinDB mg/kg <0.02 <0.1 <1 0-30 % T

b-BHCDB mg/kg <0.02 <0.1 <1 0-30 % T


d-BHCDB mg/kg <0.02 <0.1 <1 0-30 % T

DDDDB mg/kg <0.02 <0.1 117 0-30 % F

DDEDB mg/kg 0.08 <0.1 5 0-30 % T

DDTDB mg/kg 0.11 0.29 88 0-30 % F





EndrinDB mg/kg <0.02 <0.1 <1 0-30 % T

g-BHCDB mg/kg <0.02 <0.1 <1 0-30 % T













Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes

540571 [ Spike of 539383 ]




a-EndosulfanDB mg/kg N/A N/A N/A N/A



b-EndosulfanDB mg/kg N/A N/A N/A N/A




DDTDB mg/kg 0.41 N/A N/A N/A N/A



Endrin AldehydeDB mg/kg N/A N/A N/A N/A

Endrin KetoneDB mg/kg N/A N/A N/A N/A






Hexachlorobenzene (HCB)DB mg/kg N/A N/A N/A N/A


OxychlordaneDB mg/kg N/A N/A N/A N/A

Trans-NonachlorDB mg/kg N/A N/A N/A N/A


540572 [ Spike of 539408 ]






























Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes

540573 [ Spike of 539415 ]


























Sample Integrity









DescriptionCode



Q11 Surrogate recoveries could not be determined due to the dilution required to quantify the analyte.





Authorised By


Accreditation Number: 14356Elizabeth Button Senior Analyst - Environmental

Accreditation Number: 14356Michael Mowle Team Leader - Environmental

Laboratory Manager

Team Leader - EnvironmentalMichael Mowle

Final Report











If you have any queries regarding turnaround and sample progress, technical queries or wish to make changes please contact the laboratory

Job Information

Sample Integrity








Analysis Requested










540560 540561 540562 540563 540564 540571 540572 540573

Note













Logged in by : Jane Walker Date : Thu 12 July 2007



Australian Government____________________________________________National Measurement Institute

REPORT OF ANALYSISPage: 1 of 19

Report No. RN626439Client : BUTLER PARTNERS P/L Job No. : BUTL01/070710/2

79 DOGGETT STREET Quote No. : QT-00782 FORTITUDE VALLEY QLD 4006 Order No. : LA66 Date Sampled : Date Received : 10-JUL-2007

Attention : LUKE AMIES Sampled By : CLIENTProject Name : Your Client Services Manager : BRIAN WOODWARD Phone : (02) 94490151

Lab Reg No. Sample Ref Sample DescriptionN07/025662 BV-B2 SOIL JOB 06155C 06/07/07N07/025663 BV-B3 SOIL JOB 06155C 06/07/07N07/025664 BV-B4 SOIL JOB 06155C 06/07/07N07/025665 BV-B5 SOIL JOB 06155C 06/07/07

Lab Reg No. N07/025662 N07/025663 N07/025664 N07/025665Sample Reference BV-B2 BV-B3 BV-B4 BV-B5

Units MethodOrganochlorine (OC) Pesticides HCB mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 Heptachlor mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 Heptachlor epoxide mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 Aldrin mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 gamma-BHC (Lindane) mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 alpha-BHC mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 beta-BHC mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 delta-BHC mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 trans-Chlordane mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 cis-Chlordane mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 Oxychlordane mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 Dieldrin mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 pp-DDE mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 pp-DDD mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 pp-DDT mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 Endrin mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 Endrin Aldehyde mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 Endrin Ketone mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 alpha-Endosulfan mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 beta-Endosulfan mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 Endosulfan Sulfate mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 Methoxychlor mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 Surrogate Surrogate OC Rec. % 95 117 118 118 NR_19 Dates Date extracted 11-JUL-2007 11-JUL-2007 11-JUL-2007 11-JUL-2007 Date analysed 13-JUL-2007 13-JUL-2007 13-JUL-2007 13-JUL-2007

This report is issued in accordance with NATA’s accreditation requirements1 Suakin Street, Pymble NSW 2073 Tel: +61 2 9449 0111 Fax: +61 2 9449 1653 www.measurement.gov.au_______________________________________________________________________________________

N a t i o n a l M e a s u r e m e n t I n s t i t u t e


Report No. RN626439Lab Reg No. N07/025662 N07/025663 N07/025664 N07/025665Sample Reference BV-B2 BV-B3 BV-B4 BV-B5

Units Method

Luke Baker, AnalystOrganics - NSWAccreditation No. 198

13-JUL-2007


Units MethodTrace Elements Arsenic mg/kg 4.4 4.7 4.6 4.5 NT2_49 Cadmium mg/kg <0.5 <0.5 <0.5 <0.5 NT2_49 Chromium mg/kg 50 51 44 44 NT2_49 Copper mg/kg 22 25 20 21 NT2_49 Lead mg/kg 11 11 9.5 9.6 NT2_49 Mercury mg/kg <0.2 <0.2 <0.2 <0.2 NT2_49 Nickel mg/kg 27 33 30 32 NT2_49 Zinc mg/kg 60 67 56 58 NT2_49 Total Solids % 86.7 90.8 83.9 90.6 NT2_49

Jim Huang, AnalystInorganics - NSWAccreditation No. 198

13-JUL-2007

1 Suakin Street, Pymble NSW 2073 Tel: +61 2 9449 0111 Fax: +61 2 9449 1653 www.measurement.gov.au_______________________________________________________________________________________




Units Method


13-JUL-2007


Units MethodTrace Elements Arsenic mg/kg 4.8 4.7 4.6 4.9 NT2_49 Cadmium mg/kg <0.5 <0.5 <0.5 <0.5 NT2_49 Chromium mg/kg 50 50 46 51 NT2_49 Copper mg/kg 23 24 21 23 NT2_49 Lead mg/kg 11 11 9.9 10 NT2_49 Mercury mg/kg <0.2 <0.2 <0.2 <0.2 NT2_49 Nickel mg/kg 30 35 35 38 NT2_49 Zinc mg/kg 64 65 65 61 NT2_49 Total Solids % 86.3 91.3 87.4 89.5 NT2_49


13-JUL-2007





Units Method


13-JUL-2007


Units MethodTrace Elements Arsenic mg/kg 4.3 4.7 4.5 4.4 NT2_49 Cadmium mg/kg <0.5 <0.5 <0.5 <0.5 NT2_49 Chromium mg/kg 54 50 54 50 NT2_49 Copper mg/kg 23 22 24 21 NT2_49 Lead mg/kg 10 9.9 10 10 NT2_49 Mercury mg/kg <0.2 <0.2 <0.2 <0.2 NT2_49 Nickel mg/kg 35 37 37 29 NT2_49 Zinc mg/kg 66 67 65 58 NT2_49 Total Solids % 87.3 89.6 84.4 92.5 NT2_49


13-JUL-2007







Lab Reg No. Sample Ref Sample DescriptionN07/025674 WV-B4 SOIL JOB 06155C 06/07/07N07/025675 WV-B5 SOIL JOB 06155C 06/07/07N07/025676 WV-B6 SOIL JOB 06155C 06/07/07N07/025677 WV-B7 SOIL JOB 06155C 06/07/07

Lab Reg No. N07/025674 N07/025675 N07/025676 N07/025677Sample Reference WV-B4 WV-B5 WV-B6 WV-B7

Units MethodOrganochlorine (OC) Pesticides HCB mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 Heptachlor mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 Heptachlor epoxide mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 Aldrin mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 gamma-BHC (Lindane) mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 alpha-BHC mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 beta-BHC mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 delta-BHC mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 trans-Chlordane mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 cis-Chlordane mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 Oxychlordane mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 Dieldrin mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 pp-DDE mg/kg 0.087 <0.01 <0.01 <0.01 NR_19 pp-DDD mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 pp-DDT mg/kg 0.046 <0.01 <0.01 <0.01 NR_19 Endrin mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 Endrin Aldehyde mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 Endrin Ketone mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 alpha-Endosulfan mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 beta-Endosulfan mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 Endosulfan Sulfate mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 Methoxychlor mg/kg <0.01 <0.01 <0.01 <0.01 NR_19 Surrogate Surrogate OC Rec. % 117 115 111 120 NR_19 Dates Date extracted 11-JUL-2007 11-JUL-2007 11-JUL-2007 11-JUL-2007 Date analysed 13-JUL-2007 13-JUL-2007 13-JUL-2007 13-JUL-2007




Report No. RN626439Lab Reg No. N07/025674 N07/025675 N07/025676 N07/025677Sample Reference WV-B4 WV-B5 WV-B6 WV-B7

Units Method


13-JUL-2007

Lab Reg No. N07/025674 N07/025675 N07/025676 N07/025677Sample Reference WV-B4 WV-B5 WV-B6 WV-B7

Units MethodTrace Elements Arsenic mg/kg 9.8 8.1 6.2 4.5 NT2_49 Cadmium mg/kg <0.5 <0.5 <0.5 <0.5 NT2_49 Chromium mg/kg 33 47 51 45 NT2_49 Copper mg/kg 34 26 28 23 NT2_49 Lead mg/kg 88 46 14 9.3 NT2_49 Mercury mg/kg <0.2 <0.2 <0.2 <0.2 NT2_49 Nickel mg/kg 17 34 44 32 NT2_49 Zinc mg/kg 100 86 90 57 NT2_49 Total Solids % 88.8 88.5 92.4 84.4 NT2_49


13-JUL-2007







Lab Reg No. Sample Ref Sample DescriptionN07/025678 WV-B8 SOIL JOB 06155C 06/07/07N07/025679 DUP13 SOIL JOB 06155C 06/07/07N07/025683 BV-B1 SOIL JOB 06155C 09/07/07N07/025684 BV-B6 SOIL JOB 06155C 09/07/07

Lab Reg No. N07/025678 N07/025679 N07/025683 N07/025684Sample Reference WV-B8 DUP13 BV-B1 BV-B6





Report No. RN626439Lab Reg No. N07/025678 N07/025679 N07/025683 N07/025684Sample Reference WV-B8 DUP13 BV-B1 BV-B6

Units Method


13-JUL-2007

Lab Reg No. N07/025678 N07/025679 N07/025683 N07/025684Sample Reference WV-B8 DUP13 BV-B1 BV-B6

Units MethodTrace Elements Arsenic mg/kg 4.8 4.5 3.9 4.2 NT2_49 Cadmium mg/kg <0.5 <0.5 <0.5 <0.5 NT2_49 Chromium mg/kg 51 53 50 51 NT2_49 Copper mg/kg 22 23 20 20 NT2_49 Lead mg/kg 10 10 9.1 9 NT2_49 Mercury mg/kg <0.2 <0.2 <0.2 <0.2 NT2_49 Nickel mg/kg 29 38 27 27 NT2_49 Zinc mg/kg 59 62 57 57 NT2_49 Total Solids % 81.8 89.6 89.3 84.3 NT2_49


13-JUL-2007





Units Method


13-JUL-2007


Units MethodTrace Elements Arsenic mg/kg 4.2 4.5 4.3 4.6 NT2_49 Cadmium mg/kg <0.5 <0.5 <0.5 <0.5 NT2_49 Chromium mg/kg 51 51 52 49 NT2_49 Copper mg/kg 22 24 23 22 NT2_49 Lead mg/kg 9.7 9.6 9.7 26 NT2_49 Mercury mg/kg <0.2 <0.2 <0.2 <0.2 NT2_49 Nickel mg/kg 34 37 34 27 NT2_49 Zinc mg/kg 66 68 65 70 NT2_49 Total Solids % 86.4 85.6 88.4 90.4 NT2_49


13-JUL-2007





Units Method


13-JUL-2007


Units MethodTrace Elements Arsenic mg/kg 4.9 4.6 4.4 4.3 NT2_49 Cadmium mg/kg <0.5 <0.5 <0.5 <0.5 NT2_49 Chromium mg/kg 52 56 54 50 NT2_49 Copper mg/kg 23 21 22 22 NT2_49 Lead mg/kg 9.5 9.2 9.1 9 NT2_49 Mercury mg/kg <0.2 <0.2 <0.2 <0.2 NT2_49 Nickel mg/kg 40 38 36 36 NT2_49 Zinc mg/kg 69 69 65 64 NT2_49 Total Solids % 90.3 90.6 90.5 90.6 NT2_49


13-JUL-2007





Units Method


13-JUL-2007


Units MethodTrace Elements Arsenic mg/kg 4.1 3.9 4 4.1 NT2_49 Cadmium mg/kg <0.5 <0.5 <0.5 <0.5 NT2_49 Chromium mg/kg 50 48 48 49 NT2_49 Copper mg/kg 21 20 21 19 NT2_49 Lead mg/kg 9 8.5 8 8.2 NT2_49 Mercury mg/kg <0.2 <0.2 <0.2 <0.2 NT2_49 Nickel mg/kg 33 33 27 28 NT2_49 Zinc mg/kg 59 59 55 56 NT2_49 Total Solids % 91.6 91.8 85.2 84.2 NT2_49


13-JUL-2007







Lab Reg No. Sample Ref Sample DescriptionN07/025697 BV-B47 SOIL JOB 06155C 09/07/07N07/025698 BV-B48 SOIL JOB 06155C 09/07/07N07/025702 WV-B9 SOIL JOB 06155C 09/07/07

Lab Reg No. N07/025697 N07/025698 N07/025702Sample Reference BV-B47 BV-B48 WV-B9

Units MethodOrganochlorine (OC) Pesticides HCB mg/kg <0.01 <0.01 <0.01 NR_19 Heptachlor mg/kg <0.01 <0.01 <0.01 NR_19 Heptachlor epoxide mg/kg <0.01 <0.01 <0.01 NR_19 Aldrin mg/kg <0.01 <0.01 <0.01 NR_19 gamma-BHC (Lindane) mg/kg <0.01 <0.01 <0.01 NR_19 alpha-BHC mg/kg <0.01 <0.01 <0.01 NR_19 beta-BHC mg/kg <0.01 <0.01 <0.01 NR_19 delta-BHC mg/kg <0.01 <0.01 <0.01 NR_19 trans-Chlordane mg/kg <0.01 <0.01 <0.01 NR_19 cis-Chlordane mg/kg <0.01 <0.01 <0.01 NR_19 Oxychlordane mg/kg <0.01 <0.01 <0.01 NR_19 Dieldrin mg/kg <0.01 <0.01 <0.01 NR_19 pp-DDE mg/kg <0.01 <0.01 <0.01 NR_19 pp-DDD mg/kg <0.01 <0.01 <0.01 NR_19 pp-DDT mg/kg <0.01 <0.01 <0.01 NR_19 Endrin mg/kg <0.01 <0.01 <0.01 NR_19 Endrin Aldehyde mg/kg <0.01 <0.01 <0.01 NR_19 Endrin Ketone mg/kg <0.01 <0.01 <0.01 NR_19 alpha-Endosulfan mg/kg <0.01 <0.01 <0.01 NR_19 beta-Endosulfan mg/kg <0.01 <0.01 <0.01 NR_19 Endosulfan Sulfate mg/kg <0.01 <0.01 <0.01 NR_19 Methoxychlor mg/kg <0.01 <0.01 <0.01 NR_19 Surrogate Surrogate OC Rec. % 120 113 100 NR_19 Dates Date extracted 11-JUL-2007 11-JUL-2007 11-JUL-2007 Date analysed 13-JUL-2007 13-JUL-2007 13-JUL-2007




Report No. RN626439Lab Reg No. N07/025697 N07/025698 N07/025702Sample Reference BV-B47 BV-B48 WV-B9

Units Method


13-JUL-2007

Lab Reg No. N07/025697 N07/025698 N07/025702Sample Reference BV-B47 BV-B48 WV-B9

Units MethodTrace Elements Arsenic mg/kg 3.8 3.9 4 NT2_49 Cadmium mg/kg <0.5 <0.5 <0.5 NT2_49 Chromium mg/kg 47 49 50 NT2_49 Copper mg/kg 20 19 20 NT2_49 Lead mg/kg 8.6 8.4 8.8 NT2_49 Mercury mg/kg <0.2 <0.2 <0.2 NT2_49 Nickel mg/kg 29 31 28 NT2_49 Zinc mg/kg 54 57 58 NT2_49 Total Solids % 89.6 84.2 87.2 NT2_49


13-JUL-2007

All results are expressed on a dry weight basis.

This report is issued in accordance with NATA’saccreditation requirements.Accreditated for compliance with ISO/IEC 17025.This report shall not be reproduced except in full.Results relate only to the sample(s) tested.




Report No. RN626439

This Report supersedes reports: RN626354 RN626419



Australian Government____________________________________________National Measurement Institute





Lab Reg No. Sample Ref Sample DescriptionN07/025680 TB-060707 WATER JOB 06155C 06/07/07N07/025681 FB-060707 WATER JOB 06155C 06/07/07N07/025682 RB-060707 WATER JOB 06155C 06/07/07N07/025699 TB-090707 WATER JOB 06155C 09/07/07

Lab Reg No. N07/025680 N07/025681 N07/025682 N07/025699Sample Reference TB-060707 FB-060707 RB-060707 TB-090707

Units MethodOrganochlorine (OC) Pesticides HCB ug/L <0.01 <0.01 <0.01 <0.01 NR_19 Heptachlor ug/L <0.01 <0.01 <0.01 <0.01 NR_19 Heptachlor epoxide ug/L <0.01 <0.01 <0.01 <0.01 NR_19 Aldrin ug/L <0.01 <0.01 <0.01 <0.01 NR_19 gamma-BHC (Lindane) ug/L <0.01 <0.01 <0.01 <0.01 NR_19 alpha-BHC ug/L <0.01 <0.01 <0.01 <0.01 NR_19 beta-BHC ug/L <0.01 <0.01 <0.01 <0.01 NR_19 delta-BHC ug/L <0.01 <0.01 <0.01 <0.01 NR_19 trans-Chlordane ug/L <0.01 <0.01 <0.01 <0.01 NR_19 cis-Chlordane ug/L <0.01 <0.01 <0.01 <0.01 NR_19 Oxychlordane ug/L <0.01 <0.01 <0.01 <0.01 NR_19 Dieldrin ug/L <0.01 <0.01 <0.01 <0.01 NR_19 p,p-DDE ug/L <0.01 <0.01 <0.01 <0.01 NR_19 p,p-DDD ug/L <0.01 <0.01 <0.01 <0.01 NR_19 p,p-DDT ug/L <0.01 <0.01 <0.01 <0.01 NR_19 Endrin ug/L <0.01 <0.01 <0.01 <0.01 NR_19 Endrin Aldehyde ug/L <0.01 <0.01 <0.01 <0.01 NR_19 Endrin Ketone ug/L <0.01 <0.01 <0.01 <0.01 NR_19 alpha-Endosulfan ug/L <0.01 <0.01 <0.01 <0.01 NR_19 beta-Endosulfan ug/L <0.01 <0.01 <0.01 <0.01 NR_19 Endosulfan Sulfate ug/L <0.01 <0.01 <0.01 <0.01 NR_19 Methoxychlor ug/L <0.01 <0.01 <0.01 <0.01 NR_19 Surrogate Surrogate OC Rec. % 119 108 122 109 NR_19 Dates Date extracted 11-JUL-2007 11-JUL-2007 11-JUL-2007 11-JUL-2007 Date analysed 13-JUL-2007 13-JUL-2007 13-JUL-2007 13-JUL-2007

This report is issued in accordance with NATA’s accreditation requirements1 Suakin Street, Pymble NSW 2073 Tel: +61 2 9449 0111 Fax: +61 2 9449 1653 www.measurement.gov.au_______________________________________________________________________________________



Report No. RN626711Lab Reg No. N07/025680 N07/025681 N07/025682 N07/025699Sample Reference TB-060707 FB-060707 RB-060707 TB-090707

Units Method


16-JUL-2007

Lab Reg No. N07/025680 N07/025681 N07/025682 N07/025699Sample Reference TB-060707 FB-060707 RB-060707 TB-090707

Units MethodTrace Elements Arsenic-Total ug/L <1 <1 <1 <1 NT247_251 Cadmium-Total ug/L <0.1 <0.1 <0.1 <0.1 NT2_47 Chromium-Total ug/L <1 <1 <1 <1 NT2_47 Copper-Total ug/L <1 <1 <1 <1 NT2_47 Lead-Total ug/L <1 <1 <1 <1 NT2_47 Mercury-Total ug/L <0.1 <0.1 <0.1 <0.1 NT2_47_244 Nickel-Total ug/L <1 <1 <1 <1 NT2_47 Zinc-Total ug/L 2.1 1.9 1.7 1.9 NT2_47

Lisa Liu, AnalystInorganics - NSWAccreditation No. 198

16-JUL-2007







Lab Reg No. Sample Ref Sample DescriptionN07/025700 FB-090707 WATER JOB 06155C 09/07/07N07/025701 RB-090707 WATER JOB 06155C 09/07/07

Lab Reg No. N07/025700 N07/025701Sample Reference FB-090707 RB-090707

Units MethodOrganochlorine (OC) Pesticides HCB ug/L <0.01 <0.01 NR_19 Heptachlor ug/L <0.01 <0.01 NR_19 Heptachlor epoxide ug/L <0.01 <0.01 NR_19 Aldrin ug/L <0.01 <0.01 NR_19 gamma-BHC (Lindane) ug/L <0.01 <0.01 NR_19 alpha-BHC ug/L <0.01 <0.01 NR_19 beta-BHC ug/L <0.01 <0.01 NR_19 delta-BHC ug/L <0.01 <0.01 NR_19 trans-Chlordane ug/L <0.01 <0.01 NR_19 cis-Chlordane ug/L <0.01 <0.01 NR_19 Oxychlordane ug/L <0.01 <0.01 NR_19 Dieldrin ug/L <0.01 <0.01 NR_19 p,p-DDE ug/L <0.01 <0.01 NR_19 p,p-DDD ug/L <0.01 <0.01 NR_19 p,p-DDT ug/L <0.01 <0.01 NR_19 Endrin ug/L <0.01 <0.01 NR_19 Endrin Aldehyde ug/L <0.01 <0.01 NR_19 Endrin Ketone ug/L <0.01 <0.01 NR_19 alpha-Endosulfan ug/L <0.01 <0.01 NR_19 beta-Endosulfan ug/L <0.01 <0.01 NR_19 Endosulfan Sulfate ug/L <0.01 <0.01 NR_19 Methoxychlor ug/L <0.01 <0.01 NR_19 Surrogate Surrogate OC Rec. % 108 100 NR_19 Dates Date extracted 11-JUL-2007 11-JUL-2007 Date analysed 13-JUL-2007 13-JUL-2007




Report No. RN626711Lab Reg No. N07/025700 N07/025701Sample Reference FB-090707 RB-090707

Units Method


16-JUL-2007

Lab Reg No. N07/025700 N07/025701Sample Reference FB-090707 RB-090707

Units MethodTrace Elements Arsenic-Total ug/L <1 <1 NT247_251 Cadmium-Total ug/L <0.1 <0.1 NT2_47 Chromium-Total ug/L <1 <1 NT2_47 Copper-Total ug/L <1 <1 NT2_47 Lead-Total ug/L <1 <1 NT2_47 Mercury-Total ug/L <0.1 <0.1 NT2_47_244 Nickel-Total ug/L <1 <1 NT2_47 Zinc-Total ug/L 1.1 <1 NT2_47

Lisa Liu, AnalystInorganics - NSWAccreditation No. 198

16-JUL-2007

Total = Acid extractable trace elements.

This report is issued in accordance with NATA’saccreditation requirements.Accreditated for compliance with ISO/IEC 17025.This report shall not be reproduced except in full.Results relate only to the sample(s) tested.




Report No. RN626711

This Report supersedes reports: RN626419 RN626629 RN626661 RN626675



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Client: BUTLER PARTNERS P/L

NMI QA Report No: BUTL01/070710/2T1 Sample Matrix: Water

Analyte Method LOR Blank Duplicates

Sample Duplicate RPD LCS Matrix Spike

ug/L ug/L ug/L ug/L % % %

Inorganics SectionArsenic NT2.47/2.51 1 <1 ND ND ND 106 105

Cadmium NT2.47 0.1 <0.1 ND ND ND 108 93

Chromium NT2.47 1 <1 ND ND ND 99 118

Copper NT2.47 1 <1 ND ND ND 115 106

Lead NT2.47 1 <1 ND ND ND 115 107

Mercury NT2.47/2.44 0.1 <0.1 ND ND ND 100 102

Nickel NT2.47 1 <1 ND ND ND 116 108

Zinc NT2.47 1 <1 ND ND ND 96 96

Filename = C:\Documents and Settings\rlynch\My Documents\

Legend:

Acceptable recovery is 75-120%.

Acceptable RPDs on duplicates is 44% at concentrations >5 times LOR. Greater RPD may be expected at <5 times LOR.LOR = Limit Of Reporting ND = Not Determined

RPD = Relative Percent Difference NA = Not Applicable

LCS = Laboratory Control Sample.

#: Spike level is less than 50% of the sample's concentration, hence the recovery data is not reliable.

Comments:

Results greater than ten times LOR have been rounded to two significant figures.This report shall not be reproduced except in full.

Signed:

Dr Honway Louie

Inorganics Manager, NMI-Pymble

Date: 16/07/2007

QUALITY ASSURANCE REPORT

Recoveries

Australian Government

National Measurement Institute

1 Suakin Street, Pymble NSW 2073 Tel: +61 2 9449 0111 Fax: +61 2 9449 1653 www.measurement.gov.au


of 1


NMI QA Report No: BUTL01/070710_1, 10_2T1 Sample Matrix: Soil

Analyte Method LOR Blank Duplicates


N07/025664 N07/025664

mg/kg mg/kg mg/kg mg/kg % % %

Inorganics Section AGAL12

Arsenic NT2.49 0.5 <0.5 4.7 4.5 4 111 105

Cadmium NT2.49 0.5 <0.5 <0.5 <0.5 ND 95 104

Chromium NT2.49 0.5 <0.5 44 44 0 103 105

Copper NT2.49 0.5 <0.5 20 19 5 100 101

Lead NT2.49 0.5 <0.5 9.6 9.4 2 112 108

Mercury NT2.49 0.2 <0.2 <0.2 <0.2 ND 78 103

Nickel NT2.49 0.5 <0.5 31 30 3 101 102

Zinc NT2.49 0.5 <0.5 57 55 3 100 101

Filename = C:\Documents and Settings\rlynch\My Documents\

Legend:

Acceptable recovery is 75-120%.

Acceptable RPDs on duplicates is 44% at concentrations >5 times LOR. Greater RPD may be expected at <5 times LOR.LOR = Limit Of Reporting ND = Not Determined

RPD = Relative Percent Difference NA = Not Applicable

LCS = Laboratory Control Sample.

#: Spike level is less than 50% of the sample's concentration, hence the recovery data is not reliable.**: reference value not available

* sample was not spiked for this element

Comments:

Results greater than ten times LOR have been rounded to two significant figures.This report shall not be reproduced except in full.

Signed:

Dr Honway Louie

Inorganics Manager, NMI-Pymble

Date: 13/07/2007


Recoveries





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NMI QA Report No: BUTL01/070710/2 Sample Matrix: Soil

Analyte Method LOR Blank Sample Duplicates



Organics SectionOC Pesticides N07/025669 Blank Soil

HCB NR19 0.01 <0.01 <0.01 <0.01 - - -

Heptachlor NR19 0.01 <0.01 <0.01 <0.01 - 111 121

Heptachlor epoxide NR19 0.01 <0.01 <0.01 <0.01 - - -

Aldrin NR19 0.01 <0.01 <0.01 <0.01 - 101 101

gamma-BHC (Lindane) NR19 0.01 <0.01 <0.01 <0.01 - 95 100

alpha-BHC NR19 0.01 <0.01 <0.01 <0.01 - - -

beta-BHC NR19 0.01 <0.01 <0.01 <0.01 - - -

delta-BHC NR19 0.01 <0.01 <0.01 <0.01 - - -

trans-Chlordane NR19 0.01 <0.01 <0.01 <0.01 - - -

cis-Chlordane NR19 0.01 <0.01 <0.01 <0.01 - - -

Oxychlordane NR19 0.01 <0.01 <0.01 <0.01 - - -

Dieldrin NR19 0.01 <0.01 <0.01 <0.01 - 89 92

pp-DDE NR19 0.01 <0.01 <0.01 <0.01 - - -

pp-DDD NR19 0.01 <0.01 <0.01 <0.01 - - -

pp-DDT NR19 0.01 <0.01 <0.01 <0.01 - 138 145

Endrin NR19 0.01 <0.01 <0.01 <0.01 - 95 102

Endrin Aldehyde NR19 0.01 <0.01 <0.01 <0.01 - - -

Endrin Ketone NR19 0.01 <0.01 <0.01 <0.01 - - -

alpha-Endosulfan NR19 0.01 <0.01 <0.01 <0.01 - - -

beta-Endosulfan NR19 0.01 <0.01 <0.01 <0.01 - - -

Endosulfan Sulfate NR19 0.01 <0.01 <0.01 <0.01 - - -

Methoxychlor NR19 0.01 <0.01 <0.01 <0.01 - - -

Surrogate OC Rec. NR19 - - 113 121 - 87 90

Results expressed in percentage (%) or mg/kg wherever appropriate.

Acceptable Spike recovery is 50-150%

Acceptable RPDs on spikes and duplicates is 40%.

RPD= Relative Percentage Difference.

This report shall not be reproduced except in full.

Signed:Danny SleeOrganics Manager, NMI-Pymble

Date: 16/07/2007

Recoveries





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NMI QA Report No: BUTL01/070710/2 Sample Matrix: Soil




Organics SectionOC Pesticides N07/025678 Blank Soil

HCB NR19 0.01 <0.01 <0.01 <0.01 - - -

Heptachlor NR19 0.01 <0.01 <0.01 <0.01 - 129 123

Heptachlor epoxide NR19 0.01 <0.01 <0.01 <0.01 - - -

Aldrin NR19 0.01 <0.01 <0.01 <0.01 - 113 106

gamma-BHC (Lindane) NR19 0.01 <0.01 <0.01 <0.01 - 108 102

alpha-BHC NR19 0.01 <0.01 <0.01 <0.01 - - -

beta-BHC NR19 0.01 <0.01 <0.01 <0.01 - - -

delta-BHC NR19 0.01 <0.01 <0.01 <0.01 - - -

trans-Chlordane NR19 0.01 <0.01 <0.01 <0.01 - - -

cis-Chlordane NR19 0.01 <0.01 <0.01 <0.01 - - -

Oxychlordane NR19 0.01 <0.01 <0.01 <0.01 - - -

Dieldrin NR19 0.01 <0.01 <0.01 <0.01 - 102 95

pp-DDE NR19 0.01 <0.01 <0.01 <0.01 - - -

pp-DDD NR19 0.01 <0.01 <0.01 <0.01 - - -

pp-DDT NR19 0.01 <0.01 <0.01 <0.01 - 142 146

Endrin NR19 0.01 <0.01 <0.01 <0.01 - 107 105

Endrin Aldehyde NR19 0.01 <0.01 <0.01 <0.01 - - -

Endrin Ketone NR19 0.01 <0.01 <0.01 <0.01 - - -

alpha-Endosulfan NR19 0.01 <0.01 <0.01 <0.01 - - -

beta-Endosulfan NR19 0.01 <0.01 <0.01 <0.01 - - -

Endosulfan Sulfate NR19 0.01 <0.01 <0.01 <0.01 - - -

Methoxychlor NR19 0.01 <0.01 <0.01 <0.01 - - -

Surrogate OC Rec. NR19 - - 119 111 - 103 99

Results expressed in percentage (%) or mg/kg wherever appropriate.

Acceptable Spike recovery is 50-150%

Acceptable RPDs on spikes and duplicates is 40%.



Signed:Danny SleeOrganics Manager, NMI-Pymble

Date: 16/07/2007

Recoveries





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NMI QA Report No: BUTL01/070710/2 Sample Matrix: Water



ug/L ug/L ug/L ug/L % % %

Organics SectionOC Pesticides

HCB NR19 0.01 <0.01 NA NA NA - NA

Heptachlor NR19 0.01 <0.01 NA NA NA 89 NA

Heptachlor epoxide NR19 0.01 <0.01 NA NA NA - NA

Aldrin NR19 0.01 <0.01 NA NA NA 86 NA

gamma-BHC (Lindane) NR19 0.01 <0.01 NA NA NA 87 NA

alpha-BHC NR19 0.01 <0.01 NA NA NA - NA

beta-BHC NR19 0.01 <0.01 NA NA NA - NA

delta-BHC NR19 0.01 <0.01 NA NA NA - NA

trans-Chlordane NR19 0.01 <0.01 NA NA NA - NA

cis-Chlordane NR19 0.01 <0.01 NA NA NA - NA

Oxychlordane NR19 0.01 <0.01 NA NA NA - NA

Dieldrin NR19 0.01 <0.01 NA NA NA 92 NA

pp-DDE NR19 0.01 <0.01 NA NA NA - NA

pp-DDD NR19 0.01 <0.01 NA NA NA - NA

pp-DDT NR19 0.01 <0.01 NA NA NA 118 NA

Endrin NR19 0.01 <0.01 NA NA NA 87 NA

Endrin Aldehyde NR19 0.01 <0.01 NA NA NA - NA

Endrin Ketone NR19 0.01 <0.01 NA NA NA - NA

alpha-Endosulfan NR19 0.01 <0.01 NA NA NA - NA

beta-Endosulfan NR19 0.01 <0.01 NA NA NA - NA

Endosulfan Sulfate NR19 0.01 <0.01 NA NA NA - NA

Methoxychlor NR19 0.01 <0.01 NA NA NA - NA

Surrogate OC Rec. NR19 - - NA NA NA 81 NA

OP Pesticides

Dichlorvos NR19 0.1 <0.1 NA NA NA - NA

Demeton-S-Methyl NR19 0.1 <0.1 NA NA NA - NA

Diazinon NR19 0.1 <0.1 NA NA NA 75 NA

Dimethoate NR19 0.1 <0.1 NA NA NA - NA

Chlorpyrifos NR19 0.1 <0.1 NA NA NA 70 NA

Chlorpyrifos Methyl NR19 0.1 <0.1 NA NA NA - NA

Malathion (Maldison) NR19 0.1 <0.1 NA NA NA - NA

Fenthion NR19 0.1 <0.1 NA NA NA - NA

Ethion NR19 0.1 <0.1 NA NA NA 73 NA

Fenitrothion NR19 0.1 <0.1 NA NA NA - NA

Chlorfenvinphos (E) NR19 0.1 <0.1 NA NA NA - NA

Chlorfenvinphos (Z) NR19 0.1 <0.1 NA NA NA - NA

Parathion (Ethyl) NR19 0.1 <0.1 NA NA NA 67 NA

Parathion Methyl NR19 0.1 <0.1 NA NA NA - NA

Pirimiphos Ethyl NR19 0.1 <0.1 NA NA NA - NA

Pirimiphos Methyl NR19 0.1 <0.1 NA NA NA - NA

Azinphos Methyl NR19 0.1 <0.1 NA NA NA - NA

Azinphos Ethyl NR19 0.1 <0.1 NA NA NA - NA

Surrogate OP Rec. - - NA NA NA 82 NA

Results expressed in percentage (%) or ug/L wherever appropriate.Acceptable Spike recovery is 50-150%Acceptable RPDs on spikes and duplicates is 40%.

'NA ' = Not Applicable.



Signed:

Danny SleeOrganics Manager, NMI-Pymble

Date: 16/07/2007

Recoveries











79 Doggett Street


Australia




Order Number LA82

Received Date 26/07/2007 10:10:00 AM

Customer Sample ID BV-C12 BV-C13 BV-C16


Date Sampled 23/07/2007 23/07/2007 23/07/2007

SVOC





mg/kg <0.02 <0.02AldrinDB 0.02 <0.1

mg/kg <0.02 <0.02b-BHCDB 0.02 <0.1

mg/kg - -b-EndosulfanDB 0.02 <0.1

mg/kg <0.02 <0.02d-BHCDB 0.02 <0.1

mg/kg 0.2 <0.02DDDDB 0.02 0.32

mg/kg 0.32 <0.02DDEDB 0.02 0.11

mg/kg <0.02 <0.02DDTDB 0.02 0.27

mg/kg <0.02 <0.02DieldrinDB 0.02 <0.1


mg/kg <0.02 <0.02EndrinDB 0.02 <0.1



mg/kg <0.02 <0.02g-BHCDB 0.02 <0.1







mg/kg - -Trans-NonachlorDB 0.02 <0.1


TE

1 Q11 17

Metals


3200 Total Metals in Soil by ICP/AES mg/kg 62 6.0Arsenic 3 4.9




mg/kg 10 33Lead 5 9.3


mg/kg 61 120Zinc 2 59



Date Printed: 3 August 2007 Final Report Number :





Date Sampled 23/07/2007 23/07/2007 23/07/2007

Metals



Miscellaneous





Date Sampled 23/07/2007 23/07/2007 23/07/2007

SVOC





mg/kg <0.02 <0.02AldrinDB 0.02 <0.02

mg/kg <0.02 <0.02b-BHCDB 0.02 <0.02


mg/kg <0.02 <0.02d-BHCDB 0.02 <0.02

mg/kg <0.02 0.23DDDDB 0.02 <0.02

mg/kg <0.02 0.11DDEDB 0.02 <0.02

mg/kg <0.02 0.17DDTDB 0.02 <0.02

mg/kg <0.02 <0.02DieldrinDB 0.02 <0.02


mg/kg <0.02 <0.02EndrinDB 0.02 <0.02



mg/kg <0.02 <0.02g-BHCDB 0.02 <0.02









TE

1 82

Metals






mg/kg 8.4 34Lead 5 31


mg/kg 51 110Zinc 2 120







Date Sampled 23/07/2007 23/07/2007 23/07/2007

Metals



Miscellaneous





Date Sampled 23/07/2007 23/07/2007 23/07/2007

SVOC





mg/kg <0.02 <0.02AldrinDB 0.02 <0.02

mg/kg <0.02 <0.02b-BHCDB 0.02 <0.02

mg/kg <0.02 <0.02d-BHCDB 0.02 <0.02

mg/kg <0.02 <0.02DDDDB 0.02 <0.02

mg/kg <0.02 <0.02DDEDB 0.02 <0.02

mg/kg <0.02 <0.02DDTDB 0.02 <0.02

mg/kg <0.02 <0.02DieldrinDB 0.02 <0.02


mg/kg <0.02 <0.02EndrinDB 0.02 <0.02



mg/kg <0.02 <0.02g-BHCDB 0.02 <0.02








TE

1 74

Metals








mg/kg 56 64Zinc 2 190








Date Sampled 23/07/2007 23/07/2007 23/07/2007

Metals


mg/kg 0.05 <0.05Total Mercury 0.05 0.4

Miscellaneous



Customer Sample ID BV-C27 WV-C3 WV-C4


Date Sampled 23/07/2007 23/07/2007 23/07/2007

SVOC





mg/kg <0.02 <0.02AldrinDB 0.02 <0.02

mg/kg <0.02 <0.02b-BHCDB 0.02 <0.02

mg/kg <0.02 -b-EndosulfanDB 0.02 -

mg/kg <0.02 <0.02d-BHCDB 0.02 <0.02

mg/kg <0.02 <0.02DDDDB 0.02 <0.02

mg/kg <0.02 <0.02DDEDB 0.02 <0.02

mg/kg <0.02 <0.02DDTDB 0.02 <0.02

mg/kg <0.02 <0.02DieldrinDB 0.02 <0.02


mg/kg <0.02 <0.02EndrinDB 0.02 <0.02



mg/kg <0.02 <0.02g-BHCDB 0.02 <0.02







mg/kg <0.02 -Trans-NonachlorDB 0.02 -


TE

1 71

Metals








mg/kg 100 94Zinc 2 67





Customer Sample ID BV-C27 WV-C3 WV-C4


Date Sampled 23/07/2007 23/07/2007 23/07/2007

Metals



Miscellaneous



Customer Sample ID DUP36 C1-SP1B C1-SP2B


Date Sampled 23/07/2007 23/07/2007 23/07/2007

SVOC





mg/kg <10.0 <10.0AldrinDB 0.02 <0.02

mg/kg <10.0 <10.0b-BHCDB 0.02 <0.02


mg/kg <10.0 <10.0d-BHCDB 0.02 <0.02

mg/kg 90 16DDDDB 0.02 0.37

mg/kg <10.0 <10.0DDEDB 0.02 0.06

mg/kg 240 43DDTDB 0.02 0.22

mg/kg <10.0 <10.0DieldrinDB 0.02 <0.02


mg/kg <10.0 <10.0EndrinDB 0.02 <0.02



mg/kg <10.0 <10.0g-BHCDB 0.02 <0.02








% <1 <12.4.5.6-tetrachloro-m-xylene-SURROGA

TE

1 72 Q11

Metals


3200 Total Metals in Soil by ICP/AES mg/kg 52 12Arsenic 3 4.1










Customer Sample ID DUP36 C1-SP1B C1-SP2B


Date Sampled 23/07/2007 23/07/2007 23/07/2007

Metals


mg/kg 340 210Zinc 2 250

3400 Total Mercury in Soil by ICP-AES mg/kg 0.06 <0.05Total Mercury 0.05 <0.05

Miscellaneous



Customer Sample ID C1-SP3B TB-230707 RB-230707


Date Sampled 23/07/2007 23/07/2007 23/07/2007

SVOC


2300 OC Pesticides in Water by GC-ECD µg/L <1 <1a-BHC 1 -

µg/L <1 <1a-Chlordane 1 -

µg/L <1 <1a-Endosulphan 1 -

µg/L <1 <1Aldrin 1 -

µg/L <2 <2b-BHC 2 -

µg/L <1 <1b-Endosulphan 1 -

µg/L <1 <1d-BHC 1 -

µg/L <1 <1DDD 1 -

µg/L <1 <1DDE 1 -

µg/L <1 <1DDT 1 -

µg/L <1 <1Dieldrin 1 -

µg/L <1 <1Endosulfan sulfate 1 -

µg/L <1 <1Endrin 1 -

µg/L <2 <2Endrin Aldehyde 2 -

µg/L <1 <1g-BHC Lindane 1 -

µg/L <1 <1g-Chlordane 1 -

µg/L <1 <1Heptachlor 1 -

µg/L <1 <1Heptachlor epoxide 1 -

µg/L <1 <1Hexachlorobenzene (HCB) 1 -

µg/L <2 <2Methoxychlor 2 -

µg/L <1 <1Oxychlordane 1 -


TE

1 -

2300 OC Pest in Soil (Low Level) GC-ECD mg/kg - -a-BHCDB 0.02 <10.0

mg/kg - -a-ChlordaneDB 0.02 <10.0

mg/kg - -a-EndosulfanDB 0.02 <10.0

mg/kg - -AldrinDB 0.02 <10.0

mg/kg - -b-BHCDB 0.02 <10.0


mg/kg - -d-BHCDB 0.02 <10.0

mg/kg - -DDDDB 0.02 <10.0

mg/kg - -DDEDB 0.02 <10.0





Customer Sample ID C1-SP3B TB-230707 RB-230707


Date Sampled 23/07/2007 23/07/2007 23/07/2007

SVOC


mg/kg - -DDTDB 0.02 26

mg/kg - -DieldrinDB 0.02 <10.0

mg/kg - -Endosulfan sulfateDB 0.02 <10.0

mg/kg - -EndrinDB 0.02 <10.0

mg/kg - -Endrin AldehydeDB 0.02 <10.0

mg/kg - -Endrin KetoneDB 0.02 <10.0

mg/kg - -g-BHCDB 0.02 <10.0

mg/kg - -g-ChlordaneDB 0.02 <10.0

mg/kg - -HeptachlorDB 0.02 <10.0

mg/kg - -Heptachlor epoxideDB 0.02 <10.0

mg/kg - -Hexachlorobenzene (HCB)DB 0.02 <10.0

mg/kg - -MethoxychlorDB 0.02 <10.0

mg/kg - -OxychlordaneDB 0.02 <10.0


% - -2.4.5.6-tetrachloro-m-xylene-SURROGA

TE

1 Q11 <1

Metals



µg/L <0.1 <0.1Cadmium 0.1 -

µg/L 1.1 <1Lead 1 -




mg/kg - -Copper 1 29

mg/kg - -Lead 5 25

mg/kg - -Nickel 2 12

mg/kg - -Zinc 2 330

3400 Total Mercury in Soil by ICP-AES mg/kg - -Total Mercury 0.05 0.07


µg/L 2.2 <2Copper 2 -


µg/L <5 7.0Zinc 5 -


Miscellaneous



Customer Sample ID FB-230707 TB-250707 RB-250707


Date Sampled 23/07/2007 23/07/2007 23/07/2007

SVOC





Customer Sample ID FB-230707 TB-250707 RB-250707


Date Sampled 23/07/2007 23/07/2007 23/07/2007

SVOC






µg/L <2 <2b-BHC 2 <2


µg/L <1 <1d-BHC 1 <1

µg/L <1 <1DDD 1 <1

µg/L <1 <1DDE 1 <1

µg/L <1 <1DDT 1 <1













TE

1 80

Metals


3300 Dissolved Metals in Water by AAS µg/L <1 <1Arsenic 1 <1

µg/L <0.1 <0.1Cadmium 0.1 <0.1

µg/L <1 <1Lead 1 <1

3200 Dissolved Metals in Water - ICP/AES µg/L <1 <1Chromium 1 <1



µg/L <5 6.0Zinc 5 6.7


Customer Sample ID FB-250707

Amdel Sample Number 557555

Date Sampled 23/07/2007

SVOC


2300 OC Pesticides in Water by GC-ECD µg/La-BHC 1 <1

µg/La-Chlordane 1 <1

µg/La-Endosulphan 1 <1





Customer Sample ID FB-250707



SVOC


µg/LAldrin 1 <1

µg/Lb-BHC 2 <2

µg/Lb-Endosulphan 1 <1

µg/Ld-BHC 1 <1

µg/LDDD 1 <1

µg/LDDE 1 <1

µg/LDDT 1 <1

µg/LDieldrin 1 <1

µg/LEndosulfan sulfate 1 <1

µg/LEndrin 1 <1

µg/LEndrin Aldehyde 2 <2

µg/Lg-BHC Lindane 1 <1

µg/Lg-Chlordane 1 <1

µg/LHeptachlor 1 <1

µg/LHeptachlor epoxide 1 <1

µg/LHexachlorobenzene (HCB) 1 <1

µg/LMethoxychlor 2 <2

µg/LOxychlordane 1 <1

%2.4.5.6-tetrachloro-m-xylene-SURROGA

TE

1 95

Metals


3300 Dissolved Metals in Water by AAS µg/LArsenic 1 <1

µg/LCadmium 0.1 <0.1

µg/LLead 1 <1

3200 Dissolved Metals in Water - ICP/AES µg/LChromium 1 <1

µg/LCopper 2 <2

µg/LNickel 5 <5

µg/LZinc 5 5.0

3400 Dissolved Mercury in Water by ICPA µg/LMercury 1 <1

Sample History
















General










Holding Times









Acceptance


Limits

Qualifying

Codes







Lead mg/kg <5 < 5 T


Zinc mg/kg <2 < 2 T






Antimony µg/L <50 < 50 T


Barium µg/L <5 < 2 F

Beryllium µg/L <1 < 1 T

Boron µg/L <100 < 100 T

Cadmium µg/L <1 < 1 T


Cobalt µg/L <5 < 5 T


Lead µg/L <20 < 20 T

Manganese µg/L <5 < 5 T

Molybdenum µg/L <10 < 10 T


Selenium µg/L <50 < 50 T

Tin µg/L <50 < 50 T

Vanadium µg/L <5 < 5 T

Zinc µg/L <5 < 5 T









Acceptance


Limits

Qualifying

Codes





Lead µg/L <1 < 1 T



Arsenic mg/kg 47 50.0 94 70-130 % T

Cadmium mg/kg 48 50.0 96 70-130 % T

Chromium mg/kg 46 50.0 93 70-130 % T

Copper mg/kg 48 50.0 97 70-130 % T

Lead mg/kg 50 50.0 100 70-130 % T

Nickel mg/kg 47 50.0 94 70-130 % T

Zinc mg/kg 50 50.0 100 70-130 % T



Mercury mg/kg 0.46 N/A 92 75-125 % T



Antimony µg/L 870 1000.0 87 80-120 % T

Arsenic µg/L 960 1000.0 96 80-120 % T

Barium µg/L 980 1000.0 98 80-120 % T

Beryllium µg/L 1000 1000.0 103 80-120 % T

Boron µg/L 1010 1000.0 101 80-120 % T

Cadmium µg/L 980 1000.0 98 80-120 % T

Chromium µg/L 950 1000.0 95 80-120 % T

Cobalt µg/L 1100 1000.0 105 80-120 % T

Copper µg/L 970 1000.0 97 80-120 % T

Lead µg/L 1000 1000.0 105 80-120 % T

Manganese µg/L 1000 1000.0 105 80-120 % T

Molybdenum µg/L 970 N/A N/A N/A N/A

Nickel µg/L 970 1000.0 97 80-120 % T

Selenium µg/L 900 1000.0 90 80-120 % T

Tin µg/L 1100 1000.0 105 80-120 % T

Vanadium µg/L 1100 1000.0 105 80-120 % T

Zinc µg/L 1100 1000.0 107 80-120 % T



Mercury µg/L 9.82 10.0 98 80-120 % T



Arsenic µg/L 10 10.0 104 80-120 % T

Cadmium µg/L 2.0 2.0 98 80-120 % T

Lead µg/L 10.0 10.0 100 80-120 % T

557814 [ Duplicate of 557552 ]

3300 Dissolved Metals in Water by AAS Result 2 RPD

Arsenic µg/L <1 <1 <1 0-30 % T

Cadmium µg/L <0.1 <0.1 <1 0-30 % T

Lead µg/L <1 <1 <1 0-30 % T

557815 [ Duplicate of 557538 ]


ArsenicDB mg/kg 14 8.0 55 0-30 % F Q15




LeadDB mg/kg 52 49 7 0-30 % T


ZincDB mg/kg 210 190 13 0-30 % T






Acceptance


Limits

Qualifying

Codes

557819 [ Duplicate of 557538 ]


MercuryDB mg/kg 0.45 0.4 10 0-30 % T

557825 [ Duplicate of 557552 ]

3200 Dissolved Metals in Water - ICP/AES Result 2 RPD

Chromium µg/L <1 <1 <1 0-10 % T

Copper µg/L <2 <2 <1 0-10 % T

Nickel µg/L <5 <5 <1 0-10 % T

Zinc µg/L 6.2 6.7 N/A N/A N/A

557840 [ Duplicate of 557552 ]

3400 Dissolved Mercury in Water by ICPA Result 2 RPD

Mercury µg/L <1 <1 <1 0-10 % T

557860 [ Duplicate of 557537 ]








CopperDB mg/kg 39 60 43 0-30 % F Q02

CopperDB mg/kg 39 60 43 0-30 % F Q02

LeadDB mg/kg 20 34 52 0-30 % F Q15

LeadDB mg/kg 20 34 52 0-30 % F Q15



ZincDB mg/kg 210 110 66 0-30 % F Q02

ZincDB mg/kg 210 110 66 0-30 % F Q02




557848 [ Spike of 557535 ]









557849 [ Spike of 557535 ]



557851 [ Spike of 557554 ]

3400 Dissolved Mercury in Water by ICPA Spike Value Percent Recovery

Mercury µg/L 10.7 0.01 107 80-120 % T

Laboratory: EN_PREP

Acceptance


Limits

Qualifying

Codes

557845 [ Duplicate of 557567 ]



557846 [ Duplicate of 557577 ]



557853 [ Spike of 557575 ]



Laboratory: EN_SVOC





Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes










DDD µg/L <1 < 1 T

DDE µg/L <1 < 1 T

DDT µg/L <1 < 1 T















a-BHC mg/kg <0.02 < 0.02 T




b-BHC mg/kg <0.02 < 0.02 T


d-BHC mg/kg <0.02 < 0.02 T

DDD mg/kg <0.02 < 0.02 T

DDE - <0.02 < 0.02 T

DDT mg/kg <0.02 < 0.02 T






g-BHC mg/kg <0.02 < 0.02 T













Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes



a-BHC µg/L 3.6 4.0 91 70-130 % T

a-Chlordane µg/L 4.4 4.0 111 70-130 % T


Aldrin µg/L 4.1 4.0 103 70-130 % T

b-BHC µg/L 3.9 4.0 97 70-130 % T


d-BHC µg/L 4.3 4.0 106 70-130 % T

DDD µg/L 4.7 4.0 116 70-130 % T

DDE µg/L 4.6 4.0 115 70-130 % T

DDT µg/L 3.9 4.0 98 70-130 % T

Dieldrin µg/L 4.4 4.0 111 70-130 % T


Endrin µg/L 4.2 4.0 106 70-130 % T



g-Chlordane µg/L 4.4 4.0 110 70-130 % T

Heptachlor µg/L 3.9 4.0 96 70-130 % T








a-BHC mg/kg 0.05 0.05 104 70-130 % T


a-Endosulfan mg/kg 0.04 N/A 4 70-130 % F

Aldrin mg/kg 0.05 0.05 90 70-130 % T

b-BHC mg/kg 0.04 0.05 82 70-130 % T

b-Endosulfan mg/kg 0.04 N/A 4 70-130 % F

d-BHC mg/kg 0.05 0.05 104 70-130 % T

DDD mg/kg 0.09 0.1 89 70-130 % T

DDE - 0.09 0.1 88 70-130 % T

DDT mg/kg 0.07 0.1 74 70-130 % T

Dieldrin mg/kg 0.05 0.05 90 70-130 % T


Endrin mg/kg 0.05 0.05 92 70-130 % T

Endrin Aldehyde mg/kg 0.05 N/A 4 70-130 % F

Endrin Ketone mg/kg 0.05 N/A 5 70-130 % F

g-BHC mg/kg 0.05 0.05 100 70-130 % T










Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes

557845 [ Duplicate of 557567 ]


a-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T



AldrinDB mg/kg <0.02 <0.02 <1 0-30 % T

b-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T


d-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T

DDDDB mg/kg <0.02 <0.02 <1 0-30 % T

DDEDB mg/kg <0.02 <0.02 <1 0-30 % T

DDTDB mg/kg <0.02 <0.02 <1 0-30 % T





EndrinDB mg/kg <0.02 <0.02 <1 0-30 % T

g-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T









557846 [ Duplicate of 557577 ]


a-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T



AldrinDB mg/kg <0.02 <0.02 <1 0-30 % T

b-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T


d-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T

DDDDB mg/kg 0.09 0.37 122 0-30 % F Q02

DDEDB mg/kg 0.05 0.06 24 0-30 % T

DDTDB mg/kg 0.27 0.22 22 0-30 % T





EndrinDB mg/kg <0.02 <0.02 <1 0-30 % T

g-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T













Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes

557853 [ Spike of 557575 ]





















Hexachlorobenzene (HCB)DB mg/kg <0.02 N/A N/A N/A N/A




Sample Integrity









DescriptionCode








Authorised By

Senior Analyst - VOCGreg Towers




Laboratory Manager


Final Report











If you have any queries regarding turnaround and sample progress, technical queries or wish to make changes please contact the laboratory

Job Information

Sample Integrity








Analysis Requested










557845 557846 557853

Note













Logged in by : Jane Walker Date : Thu 26 July 2007









79 Doggett Street


Australia




Order Number LA86

Received Date 31/07/2007 08:00:00 AM



Date Sampled 30/07/2007 30/07/2007 30/07/2007

SVOC





mg/kg <0.02 <0.02AldrinDB 0.02 <1.0

mg/kg <0.02 <0.02b-BHCDB 0.02 <1.0


mg/kg <0.02 <0.02d-BHCDB 0.02 <1.0

mg/kg 0.02 <0.02DDDDB 0.02 5.1

mg/kg 0.09 <0.02DDEDB 0.02 1.4

mg/kg 0.05 <0.02DDTDB 0.02 3.2

mg/kg <0.02 <0.02DieldrinDB 0.02 <1.0


mg/kg <0.02 <0.02EndrinDB 0.02 <1.0



mg/kg <0.02 <0.02g-BHCDB 0.02 <1.0









TE

1 Q11 2

Metals



mg/kg <1 <1Cadmium 1 2.1



mg/kg 12 14Lead 5 120


mg/kg 51 49Zinc 2 480


First Reported: 3 August 2007 Page 1 of 13






Date Sampled 30/07/2007 30/07/2007 30/07/2007

Metals



Miscellaneous





Date Sampled 30/07/2007 30/07/2007 30/07/2007

SVOC





mg/kg <0.02 <0.02AldrinDB 0.02 <0.02

mg/kg <0.02 <0.02b-BHCDB 0.02 <0.02


mg/kg <0.02 <0.02d-BHCDB 0.02 <0.02

mg/kg <0.02 <0.02DDDDB 0.02 <0.02

mg/kg <0.02 <0.02DDEDB 0.02 <0.02

mg/kg <0.02 <0.02DDTDB 0.02 <0.02

mg/kg <0.02 <0.02DieldrinDB 0.02 <0.02


mg/kg <0.02 <0.02EndrinDB 0.02 <0.02



mg/kg <0.02 <0.02g-BHCDB 0.02 <0.02









TE

1 78

Metals






mg/kg 8.6 8.2Lead 5 9.8









Date Sampled 30/07/2007 30/07/2007 30/07/2007

Metals



Miscellaneous



Customer Sample ID WV-C5 WV-C6 WV-C11


Date Sampled 30/07/2007 30/07/2007 30/07/2007

SVOC





mg/kg <0.02 <2.0AldrinDB 0.02 <0.1

mg/kg <0.02 <2.0b-BHCDB 0.02 <0.1


mg/kg <0.02 <2.0d-BHCDB 0.02 <0.1

mg/kg <0.02 <2.0DDDDB 0.02 <0.1

mg/kg <0.02 5.9DDEDB 0.02 0.15

mg/kg <0.02 9.2DDTDB 0.02 0.15

mg/kg <0.02 <2.0DieldrinDB 0.02 0.72


mg/kg <0.02 <2.0EndrinDB 0.02 <0.1



mg/kg <0.02 <2.0g-BHCDB 0.02 <0.1









TE

1 Q11 17 Q11

Metals






mg/kg 9.3 110Lead 5 11

mg/kg 26 9.8Nickel 2 19







Date Sampled 30/07/2007 30/07/2007 30/07/2007

Metals


mg/kg 53 360Zinc 2 54


Miscellaneous



Customer Sample ID WV-C12 C1-SP1C C1-SP2C


Date Sampled 30/07/2007 30/07/2007 30/07/2007

SVOC





mg/kg <4.0 <0.2AldrinDB 0.02 <0.02

mg/kg <4.0 <0.2b-BHCDB 0.02 <0.02


mg/kg <4.0 <0.2d-BHCDB 0.02 <0.02

mg/kg <4.0 0.26DDDDB 0.02 <0.02

mg/kg <4.0 0.32DDEDB 0.02 <0.02

mg/kg 22 0.95DDTDB 0.02 <0.02

mg/kg <4.0 <0.2DieldrinDB 0.02 <0.02


mg/kg <4.0 <0.2EndrinDB 0.02 <0.02



mg/kg <4.0 <0.2g-BHCDB 0.02 <0.02








% <1 82.4.5.6-tetrachloro-m-xylene-SURROGA

TE

1 Q1172 Q11

Metals



mg/kg 1.1 1.0Cadmium 1 <1



mg/kg 320 150Lead 5 8.1





Customer Sample ID WV-C12 C1-SP1C C1-SP2C


Date Sampled 30/07/2007 30/07/2007 30/07/2007

Metals



mg/kg 1300 790Zinc 2 44


Miscellaneous



Customer Sample ID C1-SP3C TB-300707 FB-300707


Date Sampled 30/07/2007 30/07/2007 30/07/2007

SVOC






µg/L <2 <2b-BHC 2 -


µg/L <1 <1d-BHC 1 -

µg/L <1 <1DDD 1 -

µg/L <1 <1DDE 1 -

µg/L <1 <1DDT 1 -













TE

1 -





mg/kg - -b-BHCDB 0.02 <0.4


mg/kg - -d-BHCDB 0.02 <0.4

mg/kg - -DDDDB 0.02 1.2





Customer Sample ID C1-SP3C TB-300707 FB-300707


Date Sampled 30/07/2007 30/07/2007 30/07/2007

SVOC


mg/kg - -DDEDB 0.02 0.64

mg/kg - -DDTDB 0.02 2.1






mg/kg - -g-BHCDB 0.02 <0.4









TE

1 Q11 4

Metals



µg/L <0.1 <0.1Cadmium 0.1 -

µg/L <1 <1Lead 1 -


mg/kg - -Cadmium 1 1.1



mg/kg - -Lead 5 130


mg/kg - -Zinc 2 790

3400 Total Mercury in Soil by ICP-AES mg/kg - -Total Mercury 0.05 0.83




µg/L <5 11Zinc 5 -


Miscellaneous







Customer Sample ID RB-300707



SVOC





µg/LAldrin 1 <1

µg/Lb-BHC 2 <2


µg/Ld-BHC 1 <1

µg/LDDD 1 <1

µg/LDDE 1 <1

µg/LDDT 1 <1

µg/LDieldrin 1 <1


µg/LEndrin 1 <1










TE

1 93

Metals




µg/LLead 1 <1


µg/LCopper 2 <2

µg/LNickel 5 <5

µg/LZinc 5 7.7


Sample History
















General










Holding Times









Acceptance


Limits

Qualifying

Codes







Lead mg/kg <5 < 5 T


Zinc mg/kg <2 < 2 T









Zinc µg/L <5 < 5 T








Lead µg/L <1 < 1 T






Acceptance


Limits

Qualifying

Codes



Arsenic mg/kg 44 50.0 87 70-130 % T

Cadmium mg/kg 46 50.0 93 70-130 % T

Chromium mg/kg 45 50.0 90 70-130 % T

Copper mg/kg 46 50.0 92 70-130 % T

Lead mg/kg 46 50.0 92 70-130 % T

Nickel mg/kg 45 50.0 90 70-130 % T

Zinc mg/kg 46 50.0 91 70-130 % T



Mercury mg/kg 0.49 0.5 98 75-125 % T




Copper µg/L 970 1000.0 97 80-120 % T

Nickel µg/L 960 1000.0 96 80-120 % T

Zinc µg/L 1000 1000.0 104 80-120 % T



Mercury µg/L 9.94 10.0 99 80-120 % T



Arsenic µg/L 11 10.0 108 80-120 % T

Cadmium µg/L 2.0 2.0 99 80-120 % T

Lead µg/L 10 10.0 103 80-120 % T

563253 [ Duplicate of 562598 ]






LeadDB mg/kg 11 14 28 0-30 % T


ZincDB mg/kg 46 49 7 0-30 % T

563254 [ Duplicate of 562607 ]






LeadDB mg/kg 140 110 25 0-30 % T

NickelDB mg/kg 9.3 9.8 6 0-30 % T

ZincDB mg/kg 400 360 11 0-30 % T

563255 [ Duplicate of 562598 ]


MercuryDB mg/kg <0.05 0.05 N/A N/A N/A

563256 [ Duplicate of 562607 ]



563260 [ Spike of 562610 ]



Laboratory: EN_PREP

Acceptance


Limits

Qualifying

Codes

563257 [ Duplicate of 562641 ]







Laboratory: EN_PREP

Acceptance


Limits

Qualifying

Codes

563258 [ Duplicate of 562647 ]



563261 [ Spike of 562648 ]



Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes










DDD µg/L <1 < 1 T

DDE µg/L <1 < 1 T

DDT µg/L <1 < 1 T















a-BHC mg/kg <0.02 < 0.02 T




b-BHC mg/kg <0.02 < 0.02 T


d-BHC mg/kg <0.02 < 0.02 T

DDD mg/kg <0.02 < 0.02 T

DDE - <0.02 < 0.02 T

DDT mg/kg <0.02 < 0.02 T






g-BHC mg/kg <0.02 < 0.02 T













Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes



a-BHC mg/kg 0.05 0.05 99 70-130 % T



Aldrin mg/kg 0.05 0.05 92 70-130 % T

b-BHC mg/kg 0.05 0.05 92 70-130 % T


d-BHC mg/kg 0.05 0.05 100 70-130 % T

DDD mg/kg 0.08 0.1 79 70-130 % T

DDE - 0.08 0.1 84 70-130 % T

DDT mg/kg 0.11 0.1 113 70-130 % T

Dieldrin mg/kg 0.04 0.05 76 70-130 % T


Endrin mg/kg <0.02 0.05 13 70-130 % F



g-BHC mg/kg 0.05 0.05 96 70-130 % T






563257 [ Duplicate of 562641 ]


a-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T



AldrinDB mg/kg <0.02 <0.02 <1 0-30 % T

b-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T


d-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T

DDDDB mg/kg <0.02 <0.02 <1 0-30 % T

DDEDB mg/kg <0.02 <0.02 <1 0-30 % T

DDTDB mg/kg <0.02 <0.02 <1 0-30 % T





EndrinDB mg/kg <0.02 <0.02 <1 0-30 % T

g-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T













Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes

563258 [ Duplicate of 562647 ]


a-BHCDB mg/kg <4.0 <4.0 <1 0-30 % T



AldrinDB mg/kg <4.0 <4.0 <1 0-30 % T

b-BHCDB mg/kg <4.0 <4.0 <1 0-30 % T


d-BHCDB mg/kg <4.0 <4.0 <1 0-30 % T

DDDDB mg/kg <4.0 <4.0 <1 0-30 % T

DDEDB mg/kg 5.3 <4.0 118 0-30 % F Q02

DDTDB mg/kg 42 22 62 0-30 % F Q02





EndrinDB mg/kg <4.0 <4.0 <1 0-30 % T

g-BHCDB mg/kg <4.0 <4.0 <1 0-30 % T








2.4.5.6-tetrachloro-m-xylene-SURROGATE % <1 N/A N/A 70-130 % F Q11

563261 [ Spike of 562648 ]


a-BHCDB mg/kg <0.2 N/A N/A N/A N/A

a-ChlordaneDB mg/kg <0.2 N/A N/A N/A N/A

a-EndosulfanDB mg/kg <0.2 N/A N/A N/A N/A

AldrinDB mg/kg <0.2 N/A N/A N/A N/A

b-BHCDB mg/kg <0.2 N/A N/A N/A N/A

b-EndosulfanDB mg/kg <0.2 N/A N/A N/A N/A

d-BHCDB mg/kg <0.2 N/A N/A N/A N/A




DieldrinDB mg/kg 0.24 N/A N/A N/A N/A Q05

Endosulfan sulfateDB mg/kg <0.2 N/A N/A N/A N/A

Endrin AldehydeDB mg/kg <0.2 N/A N/A N/A N/A

Endrin KetoneDB mg/kg <0.2 N/A N/A N/A N/A

EndrinDB mg/kg <0.2 N/A N/A N/A N/A

g-BHCDB mg/kg <0.2 N/A N/A N/A N/A

g-ChlordaneDB mg/kg <0.2 N/A N/A N/A N/A

Heptachlor epoxideDB mg/kg <0.2 N/A N/A N/A N/A

HeptachlorDB mg/kg <0.2 N/A N/A N/A N/A


MethoxychlorDB mg/kg <0.2 N/A N/A N/A N/A

OxychlordaneDB mg/kg <0.2 N/A N/A N/A N/A

Trans-NonachlorDB mg/kg <0.2 N/A N/A N/A N/A

2.4.5.6-tetrachloro-m-xylene-SURROGATE % 8 N/A N/A 70-130 % F Q11





Sample Integrity









DescriptionCode



Q05 The matrix spike concentration is less than five times the background concentration in the sample - therefore the

spike recovery can not be determined.


Authorised By



Accreditation Number: 1464Darrel Luck Production Manager - Inorganics



Laboratory Manager


Final Report














Attention: Luke Amies Due Date: 3 August 2007




Job Information

Sample Integrity








Analysis Requested










563257 563258 563261

72HRS

Note













Logged in by : Jane Walker Date : Tue 31 July 2007









79 Doggett Street


Australia




Order Number LA87

Received Date 03/08/2007 08:00:00 AM



Date Sampled 31/07/2007 31/07/2007 31/07/2007

SVOC





mg/kg <0.02 <0.02AldrinDB 0.02 <1.0

mg/kg <0.02 <0.02b-BHCDB 0.02 <1.0


mg/kg <0.02 <0.02d-BHCDB 0.02 <1.0

mg/kg <0.02 <0.02DDDDB 0.02 3.6

mg/kg <0.02 <0.02DDEDB 0.02 7.9

mg/kg <0.02 <0.02DDTDB 0.02 <1.0

mg/kg <0.02 <0.02DieldrinDB 0.02 <1.0


mg/kg <0.02 <0.02EndrinDB 0.02 <1.0



mg/kg <0.02 <0.02g-BHCDB 0.02 <1.0









TE

1 Q11 3

Metals






mg/kg 10.0 11Lead 5 11










Date Sampled 31/07/2007 31/07/2007 31/07/2007

Metals


mg/kg 0.07 <0.05Total Mercury 0.05 0.12

Miscellaneous





Date Sampled 31/07/2007 01/08/2007 01/08/2007

SVOC





mg/kg <0.02 <0.02AldrinDB 0.02 <0.02

mg/kg <0.02 <0.02b-BHCDB 0.02 <0.02


mg/kg <0.02 <0.02d-BHCDB 0.02 <0.02

mg/kg <0.02 <0.02DDDDB 0.02 0.29

mg/kg <0.02 <0.02DDEDB 0.02 0.51

mg/kg <0.02 <0.02DDTDB 0.02 1.3

mg/kg <0.02 <0.02DieldrinDB 0.02 <0.02


mg/kg <0.02 <0.02EndrinDB 0.02 <0.04



mg/kg <0.02 <0.02g-BHCDB 0.02 <0.02









TE

1 Q11 59

Metals


3200 Total Metals in Soil by ICP/AES mg/kg 7.9 <3Arsenic 3 5.3




mg/kg 9.4 6.8Lead 5 11









Date Sampled 31/07/2007 01/08/2007 01/08/2007

Metals



Miscellaneous





Date Sampled 01/08/2007 01/08/2007 01/08/2007

SVOC





mg/kg <0.02 <0.02AldrinDB 0.02 <0.02

mg/kg <0.02 <0.02b-BHCDB 0.02 <0.02


mg/kg <0.02 <0.02d-BHCDB 0.02 <0.02

mg/kg 0.08 <0.02DDDDB 0.02 <0.02

mg/kg 0.12 <0.02DDEDB 0.02 <0.02

mg/kg 0.04 <0.02DDTDB 0.02 0.07

mg/kg <0.02 <0.02DieldrinDB 0.02 <0.02


mg/kg <0.02 <0.02EndrinDB 0.02 <0.02



mg/kg <0.02 <0.02g-BHCDB 0.02 <0.02









TE

1 82

Metals














Date Sampled 01/08/2007 01/08/2007 01/08/2007

Metals


mg/kg 97 150Zinc 2 61


Miscellaneous





Date Sampled 01/08/2007 01/08/2007 01/08/2007

SVOC





mg/kg <0.02 <0.02AldrinDB 0.02 <0.02

mg/kg <0.02 <0.02b-BHCDB 0.02 <0.02


mg/kg <0.02 <0.02d-BHCDB 0.02 <0.02

mg/kg <0.02 <0.02DDDDB 0.02 <0.02

mg/kg <0.02 <0.02DDEDB 0.02 <0.02

mg/kg <0.02 <0.02DDTDB 0.02 <0.02

mg/kg <0.02 <0.02DieldrinDB 0.02 <0.02


mg/kg <0.02 <0.02EndrinDB 0.02 <0.02



mg/kg <0.02 <0.02g-BHCDB 0.02 <0.02









TE

1 85

Metals






mg/kg 9.9 10Lead 5 8.9







Date Sampled 01/08/2007 01/08/2007 01/08/2007

Metals





Miscellaneous





Date Sampled 01/08/2007 01/08/2007 01/08/2007

SVOC





mg/kg <0.02 <0.02AldrinDB 0.02 <0.02

mg/kg <0.02 <0.02b-BHCDB 0.02 <0.02


mg/kg <0.02 <0.02d-BHCDB 0.02 <0.02

mg/kg <0.02 0.16DDDDB 0.02 <0.02

mg/kg <0.02 0.19DDEDB 0.02 <0.02

mg/kg <0.02 0.03DDTDB 0.02 <0.02

mg/kg <0.02 <0.02DieldrinDB 0.02 <0.02


mg/kg <0.02 <0.02EndrinDB 0.02 <0.02



mg/kg <0.02 <0.02g-BHCDB 0.02 <0.02









TE

1 86

Metals












Date Sampled 01/08/2007 01/08/2007 01/08/2007

Metals




mg/kg 98 170Zinc 2 67


Miscellaneous



Customer Sample ID WV-C10 DUP38 DUP39


Date Sampled 31/07/2007 31/07/2007 31/07/2007

SVOC





mg/kg <0.02 <0.02AldrinDB 0.02 <0.02

mg/kg <0.02 <0.02b-BHCDB 0.02 <0.02


mg/kg <0.02 <0.02d-BHCDB 0.02 <0.02

mg/kg <0.02 <0.02DDDDB 0.02 <0.02

mg/kg 0.03 0.02DDEDB 0.02 <0.02

mg/kg <0.02 <0.02DDTDB 0.02 <0.02

mg/kg <0.02 <0.02DieldrinDB 0.02 <0.02


mg/kg <0.02 <0.02EndrinDB 0.02 <0.02



mg/kg <0.02 <0.02g-BHCDB 0.02 <0.02









TE

1 83

Metals









Customer Sample ID WV-C10 DUP38 DUP39


Date Sampled 31/07/2007 31/07/2007 31/07/2007

Metals



mg/kg 9.6 12Lead 5 15




Miscellaneous



Customer Sample ID DUP40 SP-A2-BV TB-310707


Date Sampled 01/08/2007 01/08/2007 31/07/2007

SVOC






µg/L - <2b-BHC 2 -


µg/L - <1d-BHC 1 -

µg/L - <1DDD 1 -

µg/L - <1DDE 1 -

µg/L - <1DDT 1 -
















mg/kg - -b-BHCDB 0.02 <0.02


mg/kg - -d-BHCDB 0.02 <0.02

mg/kg - -DDDDB 0.02 <0.02





Customer Sample ID DUP40 SP-A2-BV TB-310707


Date Sampled 01/08/2007 01/08/2007 31/07/2007

SVOC


mg/kg - -DDEDB 0.02 <0.02

mg/kg - -DDTDB 0.02 <0.02






mg/kg - -g-BHCDB 0.02 <0.02









TE

1 103

Metals


3300 Dissolved Metals in Water by AAS µg/L - <1Arsenic 1 -


µg/L - <1Lead 1 -





mg/kg 40 -Lead 5 7.3

mg/kg 5.6 -Nickel 2 21

mg/kg 50 -Zinc 2 50





µg/L - <5Zinc 5 -


Miscellaneous







Customer Sample ID RB-310707 FB-310707 TB-010807


Date Sampled 31/07/2007 31/07/2007 01/08/2007

SVOC






µg/L <2 <2b-BHC 2 <2


µg/L <1 <1d-BHC 1 <1

µg/L <1 <1DDD 1 <1

µg/L <1 <1DDE 1 <1

µg/L <1 <1DDT 1 <1












Metals



µg/L <0.1 <0.1Cadmium 0.1 <0.1

µg/L <1 <1Lead 1 <1




µg/L <5 <5Zinc 5 5.5


Customer Sample ID RB-010807 FB-010807


Date Sampled 01/08/2007 01/08/2007

SVOC





µg/L <1Aldrin 1 <1

µg/L <2b-BHC 2 <2





Customer Sample ID RB-010807 FB-010807


Date Sampled 01/08/2007 01/08/2007

SVOC



µg/L <1d-BHC 1 <1

µg/L <1DDD 1 <1

µg/L <1DDE 1 <1

µg/L <1DDT 1 <1



µg/L <1Endrin 1 <1









Metals




µg/L <1Lead 1 <1


µg/L <2Copper 2 <2

µg/L <5Nickel 5 <5

µg/L <5Zinc 5 <5


Sample History









3400 Total Mercury in Soil by ICP-AES 03/08/2007 06/08/2007







General










Holding Times









Acceptance


Limits

Qualifying

Codes







Lead mg/kg <5 < 5 T


Zinc mg/kg <2 < 2 T







Lead mg/kg <5 < 5 T


Zinc mg/kg <2 < 2 T












Acceptance


Limits

Qualifying

Codes




Boron µg/L <100 < 100 T

Cadmium µg/L <1 < 1 T



Lead µg/L <20 < 20 T



Zinc µg/L <5 < 5 T








Lead µg/L <1 < 1 T



Arsenic mg/kg 45 50.0 91 70-130 % T

Cadmium mg/kg 46 50.0 93 70-130 % T

Chromium mg/kg 44 50.0 89 70-130 % T

Copper mg/kg 48 50.0 95 70-130 % T

Lead mg/kg 46 50.0 93 70-130 % T

Nickel mg/kg 45 50.0 90 70-130 % T

Zinc mg/kg 46 50.0 93 70-130 % T



Arsenic mg/kg 46 50.0 92 70-130 % T

Cadmium mg/kg 47 50.0 94 70-130 % T

Chromium mg/kg 46 50.0 92 70-130 % T

Copper mg/kg 48 50.0 96 70-130 % T

Lead mg/kg 47 50.0 94 70-130 % T

Nickel mg/kg 46 50.0 92 70-130 % T

Zinc mg/kg 47 50.0 94 70-130 % T



Mercury mg/kg 0.47 0.5 93 75-125 % T



Mercury mg/kg 0.43 0.5 86 75-125 % T



Arsenic µg/L 940 1000.0 94 80-120 % T

Boron µg/L 1010 1000.0 101 80-120 % T

Cadmium µg/L 1000 1000.0 100 80-120 % T

Chromium µg/L 950 1000.0 95 80-120 % T

Copper µg/L 980 1000.0 98 80-120 % T

Lead µg/L 1000 1000.0 100 80-120 % T

Manganese µg/L 990 1000.0 99 80-120 % T

Nickel µg/L 960 1000.0 96 80-120 % T

Zinc µg/L 1000 1000.0 100 80-120 % T



Mercury µg/L 10.1 10.0 101 80-120 % T






Acceptance


Limits

Qualifying

Codes



Arsenic µg/L 10 10.0 103 80-120 % T

Cadmium µg/L 2.0 2.0 100 80-120 % T

Lead µg/L 10 10.0 101 80-120 % T

567094 [ Duplicate of 566589 ]

3300 Dissolved Metals in Water by AAS Result 2 RPD

Arsenic µg/L <1 <1 <1 0-30 % T

Cadmium µg/L <0.1 <0.1 <1 0-30 % T

Lead µg/L <1 <1 <1 0-30 % T

567095 [ Duplicate of 566573 ]






LeadDB mg/kg 38 41 7 0-30 % T


ZincDB mg/kg 140 150 4 0-30 % T

567096 [ Duplicate of 566583 ]






LeadDB mg/kg 12 12 2 0-30 % T


ZincDB mg/kg 34 34 <1 0-30 % T

567097 [ Duplicate of 566573 ]


MercuryDB mg/kg 0.22 0.23 6 0-30 % T

567098 [ Duplicate of 566583 ]


MercuryDB mg/kg <0.05 0.06 25 0-30 % T

567100 [ Duplicate of 566589 ]

3400 Dissolved Mercury in Water by ICPA Result 2 RPD

Mercury µg/L <1 <1 N/A N/A N/A

Laboratory: EN_PREP

Acceptance


Limits

Qualifying

Codes

567103 [ Duplicate of 566605 ]



567104 [ Duplicate of 566612 ]



567121 [ Spike of 566615 ]



Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes





Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes



a-BHC mg/kg <0.02 < 0.02 T




b-BHC mg/kg <0.02 < 0.02 T


d-BHC mg/kg <0.02 < 0.02 T

DDD mg/kg <0.02 < 0.02 T

DDE - <0.02 < 0.02 T

DDT mg/kg <0.02 < 0.02 T






g-BHC mg/kg <0.02 < 0.02 T


















DDD µg/L <1 < 1 T

DDE µg/L <1 < 1 T

DDT µg/L <1 < 1 T
















Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes



a-BHC mg/kg 0.05 0.05 90 70-130 % T



Aldrin mg/kg 0.04 0.05 84 70-130 % T

b-BHC mg/kg 0.04 0.05 75 70-130 % T


d-BHC mg/kg 0.05 0.05 91 70-130 % T

DDD mg/kg 0.07 0.1 70 70-130 % T

DDE - 0.08 0.1 77 70-130 % T

DDT mg/kg 0.09 0.1 86 70-130 % T

Dieldrin mg/kg 0.04 0.05 80 70-130 % T


Endrin mg/kg 0.04 0.05 80 70-130 % T



g-BHC mg/kg 0.04 0.05 84 70-130 % T





Oxychlordane mg/kg 0.04 N/A 4 70-130 % F




a-BHC µg/L 3.9 4.0 97 70-130 % T

a-Chlordane µg/L 3.9 4.0 97 70-130 % T


Aldrin µg/L 3.9 4.0 98 70-130 % T

b-BHC µg/L 5.5 4.0 137 70-130 % F Q13


d-BHC µg/L 4.4 4.0 111 70-130 % T

DDD µg/L 3.9 4.0 97 70-130 % T

DDE µg/L 4.0 4.0 100 70-130 % T

DDT µg/L 3.5 4.0 87 70-130 % T

Dieldrin µg/L 3.8 4.0 95 70-130 % T


Endrin µg/L 3.4 4.0 85 70-130 % T



g-Chlordane µg/L 3.8 4.0 95 70-130 % T

Heptachlor µg/L 3.6 4.0 89 70-130 % T









Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes

567103 [ Duplicate of 566605 ]


a-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T



AldrinDB mg/kg <0.02 <0.02 <1 0-30 % T

b-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T


d-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T

DDDDB mg/kg <0.02 <0.02 <1 0-30 % T

DDEDB mg/kg <0.02 <0.02 <1 0-30 % T

DDTDB mg/kg <0.02 <0.02 <1 0-30 % T





EndrinDB mg/kg <0.02 <0.02 <1 0-30 % T

g-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T









567104 [ Duplicate of 566612 ]


a-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T



AldrinDB mg/kg <0.02 <0.02 <1 0-30 % T

b-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T


d-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T

DDDDB mg/kg <0.02 <0.02 <1 0-30 % T

DDEDB mg/kg <0.02 <0.02 <1 0-30 % T

DDTDB mg/kg <0.02 <0.02 <1 0-30 % T





EndrinDB mg/kg <0.02 <0.02 <1 0-30 % T

g-BHCDB mg/kg <0.02 <0.02 <1 0-30 % T













Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes

567121 [ Spike of 566615 ]























OxychlordaneDB mg/kg 0.05 N/A N/A N/A N/A

Trans-NonachlorDB mg/kg <0.02 N/A N/A N/A N/A


Sample Integrity



NoSamples correctly preserved






DescriptionCode




Authorised By




Laboratory Manager


Final Report







Client Name: Butler Partners Pty Ltd Date Received: 3 August 2007

Attention: Luke Amies Due Date: 8 August 2007




Job Information

Sample Integrity


Samples correctly preserved No






Analysis Requested










567103 567104 567121

Note













Logged in by : Jane Walker Date : Thu 2 August 2007








79 Doggett Street


Australia




Order Number LA55

Received Date 29/06/2007 12:36:00 PM

Customer Sample ID BV-D1 BV-D2 BV-D3


Date Sampled 28/06/2007 28/06/2007 28/06/2007

SVOC


2300 OC Pesticides in Soil by GC-ECD mg/kg <0.5 <0.5a-BHC 0.5 <0.5

mg/kg <0.5 <0.5a-Chlordane 0.5 <0.5

mg/kg <0.5 <0.5a-Endosulfan 0.5 <0.5

mg/kg <0.5 <0.5Aldrin 0.5 <0.5

mg/kg <0.5 <0.5b-BHC 0.5 <0.5

mg/kg <0.5 <0.5b-Endosulfan 0.5 <0.5

mg/kg <0.5 <0.5d-BHC 0.5 <0.5

mg/kg <0.5 <0.5DDD 0.5 <0.5

mg/kg <0.5 <0.5DDE 0.5 <0.5

mg/kg <0.5 <0.5DDT 0.5 <0.5

mg/kg <0.5 <0.5Dieldrin 0.5 <0.5

mg/kg <0.5 <0.5Endosulfan sulfate 0.5 <0.5

mg/kg <0.5 <0.5Endrin 0.5 <0.5

mg/kg <0.5 <0.5Endrin Aldehyde 0.5 <0.5

mg/kg <0.5 <0.5g-BHC 0.5 <0.5

mg/kg <0.5 <0.5g-Chlordane 0.5 <0.5

mg/kg <0.5 <0.5Heptachlor 0.5 <0.5

mg/kg <0.5 <0.5Heptachlor epoxide 0.5 <0.5

mg/kg <0.5 <0.5Hexachlorobenzene (HCB) 0.5 <0.5

mg/kg <0.5 <0.5Methoxychlor 0.5 <0.5

mg/kg <0.5 <0.5Oxychlordane 0.5 <0.5


TE

1 101

Metals






mg/kg 8.8 10.0Lead 5 6.4




Miscellaneous







Date Sampled 28/06/2007 28/06/2007 28/06/2007

Miscellaneous





Date Sampled 28/06/2007 28/06/2007 28/06/2007

SVOC





mg/kg <0.5 <0.5Aldrin 0.5 <0.5

mg/kg <0.5 <0.5b-BHC 0.5 <0.5


mg/kg <0.5 <0.5d-BHC 0.5 <0.5

mg/kg <0.5 <0.5DDD 0.5 <0.5

mg/kg <0.5 <0.5DDE 0.5 <0.5

mg/kg <0.5 <0.5DDT 0.5 <0.5

mg/kg <0.5 <0.5Dieldrin 0.5 <0.5


mg/kg <0.5 <0.5Endrin 0.5 <0.5

mg/kg 0.6 <0.5Endrin Aldehyde 0.5 <0.5

mg/kg <0.5 <0.5g-BHC 0.5 <0.5








TE

1 100

Metals






mg/kg 9.3 9.7Lead 5 9.1




Miscellaneous









Date Sampled 28/06/2007 28/06/2007 28/06/2007

Miscellaneous


% 16 11% Moisture 1 16



Date Sampled 28/06/2007 28/06/2007 28/06/2007

SVOC





mg/kg <0.5 <0.5Aldrin 0.5 <0.5

mg/kg <0.5 <0.5b-BHC 0.5 <0.5


mg/kg <0.5 <0.5d-BHC 0.5 <0.5

mg/kg <0.5 <0.5DDD 0.5 <0.5

mg/kg <0.5 <0.5DDE 0.5 <0.5

mg/kg <0.5 <0.5DDT 0.5 <0.5

mg/kg <0.5 <0.5Dieldrin 0.5 <0.5


mg/kg <0.5 <0.5Endrin 0.5 <0.5


mg/kg <0.5 <0.5g-BHC 0.5 <0.5








TE

1 105

Metals






mg/kg 9.8 10Lead 5 9.9




Miscellaneous







Customer Sample ID BV-D25 BV-D31 WV-D1


Date Sampled 28/06/2007 28/06/2007 28/06/2007

SVOC





mg/kg <0.5 <0.5Aldrin 0.5 <0.5

mg/kg <0.5 <0.5b-BHC 0.5 <0.5


mg/kg <0.5 <0.5d-BHC 0.5 <0.5

mg/kg <0.5 <0.5DDD 0.5 <0.5

mg/kg <0.5 <0.5DDE 0.5 <0.5

mg/kg <0.5 <0.5DDT 0.5 <0.5

mg/kg <0.5 <0.5Dieldrin 0.5 <0.5


mg/kg <0.5 <0.5Endrin 0.5 <0.5


mg/kg <0.5 <0.5g-BHC 0.5 <0.5








TE

1 105

Metals






mg/kg 10 9.6Lead 5 9.6




Miscellaneous



Customer Sample ID WV-D2 WV-D3 WV-D6


Date Sampled 28/06/2007 28/06/2007 28/06/2007

SVOC







Date Sampled 28/06/2007 28/06/2007 28/06/2007

SVOC





mg/kg <0.5 <0.5Aldrin 0.5 <0.5

mg/kg <0.5 <0.5b-BHC 0.5 <0.5


mg/kg <0.5 <0.5d-BHC 0.5 <0.5

mg/kg <0.5 <0.5DDD 0.5 <0.5

mg/kg <0.5 <0.5DDE 0.5 <0.5

mg/kg <0.5 <0.5DDT 0.5 <0.5

mg/kg <0.5 <0.5Dieldrin 0.5 <0.5


mg/kg <0.5 <0.5Endrin 0.5 <0.5


mg/kg <0.5 <0.5g-BHC 0.5 <0.5








TE

1 104

Metals






mg/kg 11 8.1Lead 5 11




Miscellaneous



Customer Sample ID FB-280607 RB-280607 TB-280607


Date Sampled 28/06/2007 28/06/2007 28/06/2007

SVOC









Date Sampled 28/06/2007 28/06/2007 28/06/2007

SVOC


µg/L <1 <1a-BHC 1 <1




µg/L <2 <2b-BHC 2 <2


µg/L <1 <1d-BHC 1 <1

µg/L <1 <1DDD 1 <1

µg/L <1 <1DDE 1 <1

µg/L <1 <1DDT 1 <1












% 98.162 100.8152.4.5.6-tetrachloro-m-xylene-SURROGA

TE

1 105.456

Metals



µg/L <0.1 <0.1Cadmium 0.1 <0.1

µg/L <1 <1Lead 1 <1




µg/L <5 <5Zinc 5 <5


Sample History



2300 OC Pesticides in Soil by GC-ECD 02/07/2007 04/07/2007



3200 Total Metals in Soil by ICP/AES 02/07/2007 03/07/2007










General










Holding Times









Acceptance


Limits

Qualifying

Codes







Lead mg/kg <5 < 5 T


Zinc mg/kg <2 < 2 T



Antimony mg/kg <5 < 5 T


Barium mg/kg <5 < 5 T

Beryllium mg/kg <5 < 5 T

Boron mg/kg <10 < 10 T



Cobalt mg/kg <5 < 5 T


Lead mg/kg <5 < 5 T

Manganese mg/kg <5 < 5 T

Molybdenum mg/kg <5 < 5 T


Selenium mg/kg <5 < 5 T

Tin mg/kg <5 < 5 T

Vanadium mg/kg <5 < 5 T

Zinc mg/kg <2 < 2 T









Acceptance


Limits

Qualifying

Codes






Boron µg/L <100 < 100 T







Tin µg/L <50 < 50 T


Zinc µg/L <5 < 5 T








Lead µg/L <1 < 1 T




Arsenic mg/kg 52 50.0 104 70-130 % T

Cadmium mg/kg 54 50.0 109 70-130 % T

Chromium mg/kg 53 50.0 107 70-130 % T

Copper mg/kg 54 50.0 108 70-130 % T

Lead mg/kg 55 50.0 109 70-130 % T

Nickel mg/kg 53 50.0 106 70-130 % T

Zinc mg/kg 55 50.0 110 70-130 % T



Antimony mg/kg 54 50.0 108 70-130 % T

Arsenic mg/kg 50 50.0 101 70-130 % T

Barium mg/kg 50 50.0 100 70-130 % T

Beryllium mg/kg 52 50.0 105 70-130 % T

Boron mg/kg 53 50.0 105 70-130 % T

Cadmium mg/kg 52 50.0 104 70-130 % T

Chromium mg/kg 51 50.0 102 70-130 % T

Cobalt mg/kg 53 50.0 107 70-130 % T

Copper mg/kg 51 50.0 102 70-130 % T

Lead mg/kg 52 50.0 105 70-130 % T

Manganese mg/kg 54 50.0 107 70-130 % T

Molybdenum mg/kg 53 N/A N/A N/A N/A

Nickel mg/kg 51 50.0 102 70-130 % T

Selenium mg/kg 49 50.0 98 70-130 % T

Tin mg/kg 54 50.0 108 70-130 % T

Vanadium mg/kg 54 50.0 107 70-130 % T

Zinc mg/kg 52 50.0 105 70-130 % T



Mercury mg/kg 0.48 0.5 96 75-125 % T






Acceptance


Limits

Qualifying

Codes



Antimony µg/L 910 1000.0 91 80-120 % T

Barium µg/L 970 1000.0 97 80-120 % T

Beryllium µg/L 1000 1000.0 100 80-120 % T

Boron µg/L 959 1000.0 96 80-120 % T

Chromium µg/L 960 1000.0 96 80-120 % T

Cobalt µg/L 1000 1000.0 100 80-120 % T

Copper µg/L 950 1000.0 95 80-120 % T

Manganese µg/L 1000 1000.0 100 80-120 % T


Nickel µg/L 960 1000.0 96 80-120 % T

Tin µg/L 1000 1000.0 101 80-120 % T

Vanadium µg/L 1000 1000.0 101 80-120 % T

Zinc µg/L 1000 1000.0 104 80-120 % T



Arsenic µg/L 11 10.0 107.2 80-120 % T

Cadmium µg/L 2.0 2.0 99.75 80-120 % T

Lead µg/L 11 10.0 107.71 80-120 % T

Selenium µg/L 10 10.0 101.5 80-120 % T

522883 [ Duplicate of 522389 ]


MercuryDB mg/kg <0.05 0.06 19 0-30 % T

522884 [ Duplicate of 522390 ]


MercuryDB mg/kg <0.05 <0.05 <0.05 0-30 % T

Q06522887 [ Spike of 522391 ]









522888 [ Spike of 522391 ]



Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes





Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes










DDD µg/L <1 < 1 T

DDE µg/L <1 < 1 T

DDT µg/L <1 < 1 T














2300 OC Pesticides in Soil by GC-ECD

a-BHC mg/kg <0.5 < 0.5 T




b-BHC mg/kg <0.5 < 0.5 T


d-BHC mg/kg <0.5 < 0.5 T

DDD mg/kg <0.5 < 0.5 T

DDE mg/kg <0.5 < 0.5 T

DDT mg/kg <0.5 < 0.5 T





g-BHC mg/kg <0.5 < 0.5 T












Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes


2300 OC Pesticides in Soil by GC-ECD Expected Value Percent Recovery

a-BHC mg/kg 2.0 2.0 98 70-130 % T


a-Endosulfan mg/kg 2.2 2.0 109 70-130 % T

Aldrin mg/kg 2.1 2.0 107 70-130 % T

b-BHC mg/kg 1.8 2.0 91 70-130 % T

b-Endosulfan mg/kg 1.9 2.0 95 70-130 % T

d-BHC mg/kg 1.9 2.0 94 70-130 % T

DDD mg/kg 1.7 2.0 86 70-130 % T

DDE mg/kg 2.0 2.0 99 70-130 % T

DDT mg/kg 1.6 2.0 80 70-130 % T

Dieldrin mg/kg 2.1 2.0 105 70-130 % T


Endrin mg/kg 1.8 2.0 89 70-130 % T

Endrin Aldehyde mg/kg 1.5 2.0 77 70-130 % T

g-BHC mg/kg 2.0 2.0 100 70-130 % T




Hexachlorobenzene (HCB) mg/kg <0.5 N/A N/A N/A N/A

Methoxychlor mg/kg 1.2 N/A N/A N/A N/A


522885 [ Duplicate of 522389 ]

2300 OC Pesticides in Soil by GC-ECD Result 2 RPD

a-BHCDB mg/kg <0.5 <0.5 <1 0-30 % T



AldrinDB mg/kg <0.5 <0.5 <1 0-30 % T

b-BHCDB mg/kg <0.5 <0.5 <1 0-30 % T


d-BHCDB mg/kg <0.5 <0.5 <1 0-30 % T

DDDDB mg/kg <0.5 <0.5 <1 0-30 % T

DDEDB mg/kg <0.5 <0.5 <1 0-30 % T

DDTDB mg/kg <0.5 <0.5 <1 0-30 % T




EndrinDB mg/kg <0.5 <0.5 <1 0-30 % T

g-BHCDB mg/kg <0.5 <0.5 <1 0-30 % T












Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes

522886 [ Duplicate of 522390 ]


a-BHCDB mg/kg <0.5 <0.5 <1 0-30 % T



AldrinDB mg/kg <0.5 <0.5 <1 0-30 % T

b-BHCDB mg/kg <0.5 <0.5 <1 0-30 % T


d-BHCDB mg/kg <0.5 <0.5 <1 0-30 % T

DDDDB mg/kg <0.5 <0.5 <1 0-30 % T

DDEDB mg/kg <0.5 <0.5 <1 0-30 % T

DDTDB mg/kg <0.5 <0.5 <1 0-30 % T




EndrinDB mg/kg <0.5 <0.5 <1 0-30 % T

g-BHCDB mg/kg <0.5 <0.5 <1 0-30 % T








522889 [ Spike of 522391 ]

2300 OC Pesticides in Soil by GC-ECD Spike Value Percent Recovery























Sample Integrity













DescriptionCode

Q06 The matrix spike recovery is outside the recommended acceptance criteria. Further analysis indicates sample


Authorised By



Laboratory Manager


Final Report

















79 Doggett Street


Australia




Order Number LA55

Received Date 29/06/2007 12:36:00 PM



Date Sampled 28/06/2007 28/06/2007 28/06/2007

SVOC





mg/kg <0.5 <0.5Aldrin 0.5 <0.5

mg/kg <0.5 <0.5b-BHC 0.5 <0.5


mg/kg <0.5 <0.5d-BHC 0.5 <0.5

mg/kg <0.5 <0.5DDD 0.5 <0.5

mg/kg <0.5 <0.5DDE 0.5 <0.5

mg/kg <0.5 <0.5DDT 0.5 <0.5

mg/kg <0.5 <0.5Dieldrin 0.5 <0.5


mg/kg <0.5 <0.5Endrin 0.5 <0.5


mg/kg <0.5 <0.5g-BHC 0.5 <0.5








TE

1 101

2300 OC Pest in Soil (Low Level) GC-ECD mg/kg <0.02 <0.02a-BHCDB 0.02 -

mg/kg <0.02 <0.02a-ChlordaneDB 0.02 -

mg/kg <0.02 <0.02a-EndosulfanDB 0.02 -

mg/kg <0.02 <0.02AldrinDB 0.02 -

mg/kg <0.02 <0.02b-BHCDB 0.02 -

mg/kg <0.02 <0.02b-EndosulfanDB 0.02 -

mg/kg <0.02 <0.02d-BHCDB 0.02 -

mg/kg <0.02 <0.02DDDDB 0.02 -

mg/kg <0.02 <0.02DDEDB 0.02 -

mg/kg <0.02 <0.02DDTDB 0.02 -

mg/kg <0.02 <0.02DieldrinDB 0.02 -

mg/kg <0.02 <0.02Endosulfan sulfateDB 0.02 -







Date Sampled 28/06/2007 28/06/2007 28/06/2007

SVOC


mg/kg <0.02 <0.02EndrinDB 0.02 -

mg/kg <0.02 <0.02Endrin AldehydeDB 0.02 -

mg/kg <0.02 <0.02Endrin KetoneDB 0.02 -

mg/kg <0.02 <0.02g-BHCDB 0.02 -

mg/kg <0.02 <0.02g-ChlordaneDB 0.02 -

mg/kg <0.02 <0.02HeptachlorDB 0.02 -

mg/kg <0.02 <0.02Heptachlor epoxideDB 0.02 -

mg/kg <0.02 <0.02Hexachlorobenzene (HCB)DB 0.02 -

mg/kg <0.02 <0.02MethoxychlorDB 0.02 -

mg/kg <0.02 <0.02OxychlordaneDB 0.02 -

mg/kg <0.02 <0.02Trans-NonachlorDB 0.02 -


TE

1 -

Metals






mg/kg 8.8 10.0Lead 5 6.4




Miscellaneous





Date Sampled 28/06/2007 28/06/2007 28/06/2007

SVOC





mg/kg <0.5 <0.5Aldrin 0.5 <0.5

mg/kg <0.5 <0.5b-BHC 0.5 <0.5


mg/kg <0.5 <0.5d-BHC 0.5 <0.5

mg/kg <0.5 <0.5DDD 0.5 <0.5

mg/kg <0.5 <0.5DDE 0.5 <0.5

mg/kg <0.5 <0.5DDT 0.5 <0.5

mg/kg <0.5 <0.5Dieldrin 0.5 <0.5







Date Sampled 28/06/2007 28/06/2007 28/06/2007

SVOC



mg/kg <0.5 <0.5Endrin 0.5 <0.5

mg/kg 0.6 <0.5Endrin Aldehyde 0.5 <0.5

mg/kg <0.5 <0.5g-BHC 0.5 <0.5








TE

1 100




mg/kg <0.02 <0.02AldrinDB 0.02 <0.02

mg/kg <0.02 <0.02b-BHCDB 0.02 <0.02


mg/kg <0.02 <0.02d-BHCDB 0.02 <0.02

mg/kg <0.02 <0.02DDDDB 0.02 <0.02

mg/kg <0.02 <0.02DDEDB 0.02 <0.02

mg/kg <0.02 <0.02DDTDB 0.02 <0.02

mg/kg <0.02 <0.02DieldrinDB 0.02 <0.02


mg/kg <0.02 <0.02EndrinDB 0.02 <0.02



mg/kg <0.02 <0.02g-BHCDB 0.02 <0.02









TE

1 88

Metals






mg/kg 9.3 9.7Lead 5 9.1










Date Sampled 28/06/2007 28/06/2007 28/06/2007

Miscellaneous





Date Sampled 28/06/2007 28/06/2007 28/06/2007

SVOC





mg/kg <0.5 <0.5Aldrin 0.5 <0.5

mg/kg <0.5 <0.5b-BHC 0.5 <0.5


mg/kg <0.5 <0.5d-BHC 0.5 <0.5

mg/kg <0.5 <0.5DDD 0.5 <0.5

mg/kg <0.5 <0.5DDE 0.5 <0.5

mg/kg <0.5 <0.5DDT 0.5 <0.5

mg/kg <0.5 <0.5Dieldrin 0.5 <0.5


mg/kg <0.5 <0.5Endrin 0.5 <0.5


mg/kg <0.5 <0.5g-BHC 0.5 <0.5








TE

1 105




mg/kg <0.02 <0.02AldrinDB 0.02 <0.02

mg/kg <0.02 <0.02b-BHCDB 0.02 <0.02


mg/kg <0.02 <0.02d-BHCDB 0.02 <0.02

mg/kg <0.02 <0.02DDDDB 0.02 <0.02

mg/kg <0.02 <0.02DDEDB 0.02 <0.02

mg/kg <0.02 <0.02DDTDB 0.02 <0.02

mg/kg <0.02 <0.02DieldrinDB 0.02 <0.02


mg/kg <0.02 <0.02EndrinDB 0.02 <0.02









Date Sampled 28/06/2007 28/06/2007 28/06/2007

SVOC


mg/kg <0.02 <0.02g-BHCDB 0.02 <0.02









TE

1 84

Metals






mg/kg 9.8 10Lead 5 9.9




Miscellaneous





Date Sampled 28/06/2007 28/06/2007 28/06/2007

SVOC





mg/kg <0.5 <0.5Aldrin 0.5 <0.5

mg/kg <0.5 <0.5b-BHC 0.5 <0.5


mg/kg <0.5 <0.5d-BHC 0.5 <0.5

mg/kg <0.5 <0.5DDD 0.5 <0.5

mg/kg <0.5 <0.5DDE 0.5 <0.5

mg/kg <0.5 <0.5DDT 0.5 <0.5

mg/kg <0.5 <0.5Dieldrin 0.5 <0.5


mg/kg <0.5 <0.5Endrin 0.5 <0.5








Date Sampled 28/06/2007 28/06/2007 28/06/2007

SVOC


mg/kg <0.5 <0.5g-BHC 0.5 <0.5








TE

1 105




mg/kg <0.02 <0.02AldrinDB 0.02 <0.02

mg/kg <0.02 <0.02b-BHCDB 0.02 <0.02


mg/kg <0.02 <0.02d-BHCDB 0.02 <0.02

mg/kg <0.02 <0.02DDDDB 0.02 <0.02

mg/kg <0.02 <0.02DDEDB 0.02 0.21

mg/kg <0.02 <0.02DDTDB 0.02 <0.02

mg/kg <0.02 <0.02DieldrinDB 0.02 <0.02


mg/kg <0.02 <0.02EndrinDB 0.02 <0.02



mg/kg <0.02 <0.02g-BHCDB 0.02 <0.02









TE

1 128

Metals






mg/kg 10 9.6Lead 5 9.6




Miscellaneous








Date Sampled 28/06/2007 28/06/2007 28/06/2007

Miscellaneous





Date Sampled 28/06/2007 28/06/2007 28/06/2007

SVOC





mg/kg <0.5 <0.5Aldrin 0.5 <0.5

mg/kg <0.5 <0.5b-BHC 0.5 <0.5


mg/kg <0.5 <0.5d-BHC 0.5 <0.5

mg/kg <0.5 <0.5DDD 0.5 <0.5

mg/kg <0.5 <0.5DDE 0.5 <0.5

mg/kg <0.5 <0.5DDT 0.5 <0.5

mg/kg <0.5 <0.5Dieldrin 0.5 <0.5


mg/kg <0.5 <0.5Endrin 0.5 <0.5


mg/kg <0.5 <0.5g-BHC 0.5 <0.5








TE

1 104




mg/kg <0.02 <0.02AldrinDB 0.02 <0.02

mg/kg <0.02 <0.02b-BHCDB 0.02 <0.02


mg/kg <0.02 <0.02d-BHCDB 0.02 <0.02

mg/kg <0.02 <0.02DDDDB 0.02 <0.02

mg/kg 0.42 <0.02DDEDB 0.02 <0.02

mg/kg <0.02 <0.02DDTDB 0.02 <0.02

mg/kg <0.02 <0.02DieldrinDB 0.02 <0.02


mg/kg <0.02 <0.02EndrinDB 0.02 <0.02









Date Sampled 28/06/2007 28/06/2007 28/06/2007

SVOC


mg/kg <0.02 <0.02g-BHCDB 0.02 <0.02









TE

1 111

Metals






mg/kg 11 8.1Lead 5 11




Miscellaneous





Date Sampled 28/06/2007 28/06/2007 28/06/2007

SVOC






µg/L <2 <2b-BHC 2 <2


µg/L <1 <1d-BHC 1 <1

µg/L <1 <1DDD 1 <1

µg/L <1 <1DDE 1 <1

µg/L <1 <1DDT 1 <1











Date Sampled 28/06/2007 28/06/2007 28/06/2007

SVOC









% 98.162 100.8152.4.5.6-tetrachloro-m-xylene-SURROGA

TE

1 105.456

Metals



µg/L <0.1 <0.1Cadmium 0.1 <0.1

µg/L <1 <1Lead 1 <1




µg/L <5 <5Zinc 5 <5


Sample History



2300 OC Pest in Soil (Low Level) GC-ECD 24/07/2007




3200 Total Metals in Soil by ICP/AES 02/07/2007 03/07/2007










General










Holding Times









Acceptance


Limits

Qualifying

Codes







Lead mg/kg <5 < 5 T


Zinc mg/kg <2 < 2 T



Antimony mg/kg <5 < 5 T


Barium mg/kg <5 < 5 T

Beryllium mg/kg <5 < 5 T

Boron mg/kg <10 < 10 T



Cobalt mg/kg <5 < 5 T


Lead mg/kg <5 < 5 T

Manganese mg/kg <5 < 5 T

Molybdenum mg/kg <5 < 5 T


Selenium mg/kg <5 < 5 T

Tin mg/kg <5 < 5 T

Vanadium mg/kg <5 < 5 T

Zinc mg/kg <2 < 2 T









Acceptance


Limits

Qualifying

Codes






Boron µg/L <100 < 100 T







Tin µg/L <50 < 50 T


Zinc µg/L <5 < 5 T








Lead µg/L <1 < 1 T




Arsenic mg/kg 52 50.0 104 70-130 % T

Cadmium mg/kg 54 50.0 109 70-130 % T

Chromium mg/kg 53 50.0 107 70-130 % T

Copper mg/kg 54 50.0 108 70-130 % T

Lead mg/kg 55 50.0 109 70-130 % T

Nickel mg/kg 53 50.0 106 70-130 % T

Zinc mg/kg 55 50.0 110 70-130 % T



Antimony mg/kg 54 50.0 108 70-130 % T

Arsenic mg/kg 50 50.0 101 70-130 % T

Barium mg/kg 50 50.0 100 70-130 % T

Beryllium mg/kg 52 50.0 105 70-130 % T

Boron mg/kg 53 50.0 105 70-130 % T

Cadmium mg/kg 52 50.0 104 70-130 % T

Chromium mg/kg 51 50.0 102 70-130 % T

Cobalt mg/kg 53 50.0 107 70-130 % T

Copper mg/kg 51 50.0 102 70-130 % T

Lead mg/kg 52 50.0 105 70-130 % T

Manganese mg/kg 54 50.0 107 70-130 % T

Molybdenum mg/kg 53 N/A N/A N/A N/A

Nickel mg/kg 51 50.0 102 70-130 % T

Selenium mg/kg 49 50.0 98 70-130 % T

Tin mg/kg 54 50.0 108 70-130 % T

Vanadium mg/kg 54 50.0 107 70-130 % T

Zinc mg/kg 52 50.0 105 70-130 % T



Mercury mg/kg 0.48 0.5 96 75-125 % T






Acceptance


Limits

Qualifying

Codes



Antimony µg/L 910 1000.0 91 80-120 % T

Barium µg/L 970 1000.0 97 80-120 % T

Beryllium µg/L 1000 1000.0 100 80-120 % T

Boron µg/L 959 1000.0 96 80-120 % T

Chromium µg/L 960 1000.0 96 80-120 % T

Cobalt µg/L 1000 1000.0 100 80-120 % T

Copper µg/L 950 1000.0 95 80-120 % T

Manganese µg/L 1000 1000.0 100 80-120 % T


Nickel µg/L 960 1000.0 96 80-120 % T

Tin µg/L 1000 1000.0 101 80-120 % T

Vanadium µg/L 1000 1000.0 101 80-120 % T

Zinc µg/L 1000 1000.0 104 80-120 % T



Arsenic µg/L 11 10.0 107.2 80-120 % T

Cadmium µg/L 2.0 2.0 99.75 80-120 % T

Lead µg/L 11 10.0 107.71 80-120 % T

Selenium µg/L 10 10.0 101.5 80-120 % T

522883 [ Duplicate of 522389 ]


MercuryDB mg/kg <0.05 0.06 19 0-30 % T

522884 [ Duplicate of 522390 ]


MercuryDB mg/kg <0.05 <0.05 <0.05 0-30 % T

Q06522887 [ Spike of 522391 ]









522888 [ Spike of 522391 ]



Laboratory: EN_PREP

Acceptance


Limits

Qualifying

Codes

532150 [ Duplicate of 530887 ]



532156 [ Duplicate of 530888 ]



532175 [ Spike of 530889 ]



Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes





Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes










DDD µg/L <1 < 1 T

DDE µg/L <1 < 1 T

DDT µg/L <1 < 1 T















a-BHC mg/kg <0.5 < 0.5 T




b-BHC mg/kg <0.5 < 0.5 T


d-BHC mg/kg <0.5 < 0.5 T

DDD mg/kg <0.5 < 0.5 T

DDE mg/kg <0.5 < 0.5 T

DDT mg/kg <0.5 < 0.5 T





g-BHC mg/kg <0.5 < 0.5 T












Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes



a-BHC mg/kg <0.5 < 0.5 T




b-BHC mg/kg <0.5 < 0.5 T


d-BHC mg/kg <0.5 < 0.5 T

DDD mg/kg <0.5 < 0.5 T

DDE mg/kg <0.5 < 0.5 T

DDT mg/kg <0.5 < 0.5 T












a-BHC mg/kg 2.0 2.0 98 70-130 % T



Aldrin mg/kg 2.1 2.0 107 70-130 % T

b-BHC mg/kg 1.8 2.0 91 70-130 % T


d-BHC mg/kg 1.9 2.0 94 70-130 % T

DDD mg/kg 1.7 2.0 86 70-130 % T

DDE mg/kg 2.0 2.0 99 70-130 % T

DDT mg/kg 1.6 2.0 80 70-130 % T

Dieldrin mg/kg 2.1 2.0 105 70-130 % T


Endrin mg/kg 1.8 2.0 89 70-130 % T


g-BHC mg/kg 2.0 2.0 100 70-130 % T





Methoxychlor mg/kg 1.2 N/A N/A N/A N/A






Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes



a-BHC mg/kg 4.9 5.0 98 70-130 % T



Aldrin mg/kg 4.6 5.0 92 70-130 % T

b-BHC mg/kg 4.6 5.0 91 70-130 % T


d-BHC mg/kg 4.6 5.0 91 70-130 % T

DDD mg/kg 9.7 10.0 97 70-130 % T

DDE mg/kg 9.0 10.0 90 70-130 % T

DDT mg/kg 12 10.0 122 70-130 % T

Dieldrin mg/kg 4.6 5.0 92 70-130 % T


Endrin mg/kg 4.6 5.0 92 70-130 % T

Endrin Aldehyde mg/kg 6.6 5.0 132 70-130 % F Q13





Oxychlordane mg/kg 4.6 5.0 92 70-130 % T


522885 [ Duplicate of 522389 ]


a-BHCDB mg/kg <0.5 <0.5 <1 0-30 % T



AldrinDB mg/kg <0.5 <0.5 <1 0-30 % T

b-BHCDB mg/kg <0.5 <0.5 <1 0-30 % T


d-BHCDB mg/kg <0.5 <0.5 <1 0-30 % T

DDDDB mg/kg <0.5 <0.5 <1 0-30 % T

DDEDB mg/kg <0.5 <0.5 <1 0-30 % T

DDTDB mg/kg <0.5 <0.5 <1 0-30 % T




EndrinDB mg/kg <0.5 <0.5 <1 0-30 % T

g-BHCDB mg/kg <0.5 <0.5 <1 0-30 % T












Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes

522886 [ Duplicate of 522390 ]


a-BHCDB mg/kg <0.5 <0.5 <1 0-30 % T



AldrinDB mg/kg <0.5 <0.5 <1 0-30 % T

b-BHCDB mg/kg <0.5 <0.5 <1 0-30 % T


d-BHCDB mg/kg <0.5 <0.5 <1 0-30 % T

DDDDB mg/kg <0.5 <0.5 <1 0-30 % T

DDEDB mg/kg <0.5 <0.5 <1 0-30 % T

DDTDB mg/kg <0.5 <0.5 <1 0-30 % T




EndrinDB mg/kg <0.5 <0.5 <1 0-30 % T

g-BHCDB mg/kg <0.5 <0.5 <1 0-30 % T








532150 [ Duplicate of 530887 ]


a-BHCDB mg/kg <0.5 N/A <1 0-30 % T

a-ChlordaneDB mg/kg <0.5 N/A <1 0-30 % T

a-EndosulfanDB mg/kg <0.5 N/A <1 0-30 % T

AldrinDB mg/kg <0.5 N/A <1 0-30 % T

b-BHCDB mg/kg <0.5 N/A <1 0-30 % T

b-EndosulfanDB mg/kg <0.5 N/A <1 0-30 % T

d-BHCDB mg/kg <0.5 N/A <1 0-30 % T

DDDDB mg/kg <0.5 N/A <1 0-30 % T

DDEDB mg/kg <0.5 N/A <1 0-30 % T

DDTDB mg/kg <0.5 N/A <1 0-30 % T

DieldrinDB mg/kg <0.5 N/A <1 0-30 % T

Endosulfan sulfateDB mg/kg <0.5 N/A <1 0-30 % T

Endrin AldehydeDB mg/kg <0.5 N/A <1 0-30 % T

EndrinDB mg/kg <0.5 N/A <1 0-30 % T

g-BHCDB mg/kg <0.5 N/A <1 0-30 % T

g-ChlordaneDB mg/kg <0.5 N/A <1 0-30 % T

Heptachlor epoxideDB mg/kg <0.5 N/A <1 0-30 % T

HeptachlorDB mg/kg <0.5 N/A <1 0-30 % T

Hexachlorobenzene (HCB)DB mg/kg <0.5 N/A <1 0-30 % T

MethoxychlorDB mg/kg <0.5 N/A <1 0-30 % T

OxychlordaneDB mg/kg <0.5 N/A <1 0-30 % T






Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes

532156 [ Duplicate of 530888 ]


a-BHCDB mg/kg <0.5 N/A <1 0-30 % T

a-ChlordaneDB mg/kg <0.5 N/A <1 0-30 % T

a-EndosulfanDB mg/kg <0.5 N/A <1 0-30 % T

AldrinDB mg/kg <0.5 N/A <1 0-30 % T

b-BHCDB mg/kg <0.5 N/A <1 0-30 % T

b-EndosulfanDB mg/kg <0.5 N/A <1 0-30 % T

d-BHCDB mg/kg <0.5 N/A <1 0-30 % T

DDDDB mg/kg <0.5 N/A <1 0-30 % T

DDEDB mg/kg <0.5 N/A <1 0-30 % T

DDTDB mg/kg <0.5 N/A <1 0-30 % T

DieldrinDB mg/kg <0.5 N/A <1 0-30 % T

Endosulfan sulfateDB mg/kg <0.5 N/A <1 0-30 % T

Endrin AldehydeDB mg/kg <0.5 N/A <1 0-30 % T

EndrinDB mg/kg <0.5 N/A <1 0-30 % T

g-BHCDB mg/kg <0.5 N/A <1 0-30 % T

g-ChlordaneDB mg/kg <0.5 N/A <1 0-30 % T

Heptachlor epoxideDB mg/kg <0.5 N/A <1 0-30 % T

HeptachlorDB mg/kg <0.5 N/A <1 0-30 % T

Hexachlorobenzene (HCB)DB mg/kg <0.5 N/A <1 0-30 % T

MethoxychlorDB mg/kg <0.5 N/A <1 0-30 % T

OxychlordaneDB mg/kg <0.5 N/A <1 0-30 % T


522889 [ Spike of 522391 ]




























Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes

532175 [ Spike of 530889 ]









DDDDB mg/kg 11 N/A N/A N/A N/A

DDEDB mg/kg 11 N/A N/A N/A N/A

DDTDB mg/kg 14 N/A N/A N/A N/A



Endrin AldehydeDB mg/kg 9.3 N/A N/A N/A N/A Q13





HeptachlorDB mg/kg 3.7 N/A N/A N/A N/A Q13





Sample Integrity









DescriptionCode

Q06 The matrix spike recovery is outside the recommended acceptance criteria. Further analysis indicates sample




Authorised By



Accreditation Number: 1464Darrel Luck Production Manager - Inorganics



Laboratory Manager


Final Report







Client Name: Butler Partners Pty Ltd Date Received: 29 June 2007



Amdel Reference number: 07ENBR0011495 Your Amdel Contact: Michael Mowle+61 7 3902 4600


Job Information

Sample Integrity








Analysis Requested








2300OC Pesticides in Soil by GC-ECD 15


Note













Logged in by : Patricia Chew Date : Fri 29 June 2007








79 Doggett Street


Australia




Order Number LA56

Received Date 29/06/2007 02:00:00 PM



Date Sampled 29/06/2007 29/06/2007 29/06/2007

SVOC





mg/kg <0.5 <0.5Aldrin 0.5 <0.5

mg/kg <0.5 <0.5b-BHC 0.5 <0.5


mg/kg <0.5 <0.5d-BHC 0.5 <0.5

mg/kg <0.5 <0.5DDD 0.5 <0.5

mg/kg <0.5 <0.5DDE 0.5 <0.5

mg/kg <0.5 0.6DDT 0.5 <0.5

mg/kg <0.5 <0.5Dieldrin 0.5 <0.5


mg/kg <0.5 <0.5Endrin 0.5 <0.5


mg/kg <0.5 <0.5g-BHC 0.5 <0.5








TE

1 105

Metals






mg/kg 9.8 8.6Lead 5 9.0




Miscellaneous







Date Sampled 29/06/2007 29/06/2007 29/06/2007

Miscellaneous





Date Sampled 29/06/2007 29/06/2007 29/06/2007

SVOC





mg/kg <0.5 <0.5Aldrin 0.5 <0.5

mg/kg <0.5 <0.5b-BHC 0.5 <0.5


mg/kg <0.5 <0.5d-BHC 0.5 <0.5

mg/kg <0.5 <0.5DDD 0.5 <0.5

mg/kg 2.3 <0.5DDE 0.5 <0.5

mg/kg 0.7 0.9DDT 0.5 <0.5

mg/kg <0.5 <0.5Dieldrin 0.5 <0.5


mg/kg <0.5 <0.5Endrin 0.5 <0.5


mg/kg <0.5 <0.5g-BHC 0.5 <0.5








TE

1 106

Metals






mg/kg 12 11Lead 5 8.0




Miscellaneous









Date Sampled 29/06/2007 29/06/2007 29/06/2007

Miscellaneous


% 12 20% Moisture 1 16



Date Sampled 29/06/2007 29/06/2007 29/06/2007

SVOC





mg/kg <0.5 <0.5Aldrin 0.5 <0.5

mg/kg <0.5 <0.5b-BHC 0.5 <0.5


mg/kg <0.5 <0.5d-BHC 0.5 <0.5

mg/kg <0.5 <0.5DDD 0.5 <0.5

mg/kg <0.5 <0.5DDE 0.5 <0.5

mg/kg 0.9 <0.5DDT 0.5 <0.5

mg/kg <0.5 <0.5Dieldrin 0.5 <0.5


mg/kg <0.5 <0.5Endrin 0.5 <0.5


mg/kg <0.5 <0.5g-BHC 0.5 <0.5








TE

1 107

Metals






mg/kg 10.0 8.6Lead 5 9.7




Miscellaneous









Date Sampled 29/06/2007 29/06/2007 29/06/2007

SVOC





mg/kg <0.5 <0.5Aldrin 0.5 <0.5

mg/kg <0.5 <0.5b-BHC 0.5 <0.5


mg/kg <0.5 <0.5d-BHC 0.5 <0.5

mg/kg <0.5 <0.5DDD 0.5 <0.5

mg/kg <0.5 <0.5DDE 0.5 <0.5

mg/kg <0.5 <0.5DDT 0.5 <0.5

mg/kg <0.5 <0.5Dieldrin 0.5 <0.5


mg/kg <0.5 <0.5Endrin 0.5 <0.5


mg/kg <0.5 <0.5g-BHC 0.5 <0.5








TE

1 103

Metals






mg/kg 9.2 8.7Lead 5 6.6




Miscellaneous





Date Sampled 29/06/2007 29/06/2007 29/06/2007

SVOC







Date Sampled 29/06/2007 29/06/2007 29/06/2007

SVOC





mg/kg <0.5 <0.5Aldrin 0.5 <0.5

mg/kg <0.5 <0.5b-BHC 0.5 <0.5


mg/kg <0.5 <0.5d-BHC 0.5 <0.5

mg/kg <0.5 <0.5DDD 0.5 <0.5

mg/kg <0.5 <0.5DDE 0.5 <0.5

mg/kg <0.5 <0.5DDT 0.5 <0.5

mg/kg <0.5 <0.5Dieldrin 0.5 <0.5


mg/kg <0.5 <0.5Endrin 0.5 <0.5


mg/kg <0.5 <0.5g-BHC 0.5 <0.5








TE

1 107

Metals






mg/kg 8.2 7.9Lead 5 7.8




Miscellaneous



Customer Sample ID WV-D5 DUP01 TB-290607


Date Sampled 29/06/2007 29/06/2007 29/06/2007

SVOC









Date Sampled 29/06/2007 29/06/2007 29/06/2007

SVOC


mg/kg <0.5 -a-BHC 0.5 <0.5

mg/kg <0.5 -a-Chlordane 0.5 <0.5

mg/kg <0.5 -a-Endosulfan 0.5 <0.5

mg/kg <0.5 -Aldrin 0.5 <0.5

mg/kg <0.5 -b-BHC 0.5 <0.5

mg/kg <0.5 -b-Endosulfan 0.5 <0.5

mg/kg <0.5 -d-BHC 0.5 <0.5

mg/kg <0.5 -DDD 0.5 <0.5

mg/kg <0.5 -DDE 0.5 <0.5

mg/kg <0.5 -DDT 0.5 <0.5

mg/kg <0.5 -Dieldrin 0.5 <0.5

mg/kg <0.5 -Endosulfan sulfate 0.5 <0.5

mg/kg <0.5 -Endrin 0.5 <0.5

mg/kg <0.5 -Endrin Aldehyde 0.5 <0.5

mg/kg <0.5 -g-BHC 0.5 <0.5

mg/kg <0.5 -g-Chlordane 0.5 <0.5

mg/kg <0.5 -Heptachlor 0.5 <0.5

mg/kg <0.5 -Heptachlor epoxide 0.5 <0.5

mg/kg <0.5 -Hexachlorobenzene (HCB) 0.5 <0.5

mg/kg <0.5 -Methoxychlor 0.5 <0.5

mg/kg <0.5 -Oxychlordane 0.5 <0.5

% 101 -2.4.5.6-tetrachloro-m-xylene-SURROGA

TE

1 107





µg/L - <2b-BHC 2 -


µg/L - <1d-BHC 1 -

µg/L - <1DDD 1 -

µg/L - <1DDE 1 -

µg/L - <1DDT 1 -












% - 96.8842.4.5.6-tetrachloro-m-xylene-SURROGA

TE

1 -

Metals









Date Sampled 29/06/2007 29/06/2007 29/06/2007

Metals


µg/L - <1Arsenic 1 -


µg/L - <1Lead 1 -





mg/kg 8.6 -Lead 5 11

mg/kg 28 -Nickel 2 8.8

mg/kg 62 -Zinc 2 31





µg/L - <5Zinc 5 -


Miscellaneous





Date Sampled 29/06/2007 29/06/2007

SVOC





µg/L <1Aldrin 1 <1

µg/L <2b-BHC 2 <2


µg/L <1d-BHC 1 <1

µg/L <1DDD 1 <1

µg/L <1DDE 1 <1

µg/L <1DDT 1 <1



µg/L <1Endrin 1 <1










Date Sampled 29/06/2007 29/06/2007

SVOC







% 102.9462.4.5.6-tetrachloro-m-xylene-SURROGA

TE

1 102.342

Metals




µg/L <1Lead 1 <1


µg/L <2Copper 2 <2

µg/L <5Nickel 5 <5

µg/L <5Zinc 5 <5


Sample History



2300 OC Pesticides in Soil by GC-ECD 06/07/2007













General










Holding Times









Acceptance


Limits

Qualifying

Codes






Boron µg/L <100 < 100 T







Tin µg/L <50 < 50 T


Zinc µg/L <5 < 5 T








Lead µg/L <1 < 1 T








Lead mg/kg <5 < 5 T


Zinc mg/kg <2 < 2 T






Acceptance


Limits

Qualifying

Codes






Antimony µg/L 940 1000.0 94 80-120 % T

Barium µg/L 980 1000.0 98 80-120 % T

Beryllium µg/L 1000 1000.0 101 80-120 % T

Boron µg/L 980 1000.0 98 80-120 % T

Chromium µg/L 970 1000.0 97 80-120 % T

Cobalt µg/L 1000 1000.0 101 80-120 % T

Copper µg/L 980 1000.0 98 80-120 % T

Manganese µg/L 1000 1000.0 101 80-120 % T


Nickel µg/L 990 1000.0 99 80-120 % T

Tin µg/L 1000 1000.0 101 80-120 % T

Vanadium µg/L 1000 1000.0 102 80-120 % T

Zinc µg/L 1000 1000.0 104 80-120 % T



Mercury µg/L 9.57 0.01 96 80-120 % T



Arsenic µg/L 10 10.0 100.0 80-120 % T

Cadmium µg/L 2.0 2.0 100.85 80-120 % T

Lead µg/L 11 10.0 108.19 80-120 % T

Selenium µg/L 11 10.0 107.8 80-120 % T



Arsenic mg/kg 49 50.0 98 70-130 % T

Cadmium mg/kg 50 50.0 101 70-130 % T

Chromium mg/kg 47 50.0 94 70-130 % T

Copper mg/kg 50 50.0 99 70-130 % T

Lead mg/kg 48 50.0 96 70-130 % T

Nickel mg/kg 46 50.0 93 70-130 % T

Zinc mg/kg 48 50.0 97 70-130 % T



Mercury mg/kg 0.45 0.5 91 75-125 % T

525385 [ Duplicate of 522832 ]




ChromiumDB mg/kg 42 42 <1 0-30 % T


LeadDB mg/kg 9.2 9.0 3 0-30 % T


ZincDB mg/kg 66 66 <1 0-30 % T

525386 [ Duplicate of 522833 ]






LeadDB mg/kg 9.5 9.8 3 0-30 % T


ZincDB mg/kg 65 66 2 0-30 % T






Acceptance


Limits

Qualifying

Codes

525387 [ Duplicate of 522832 ]



525388 [ Duplicate of 522833 ]


MercuryDB mg/kg <0.05 <0.05 <0.05 0-30 % T

525391 [ Spike of 522834 ]









525392 [ Spike of 522834 ]



Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes










DDD µg/L <1 < 1 T

DDE µg/L <1 < 1 T

DDT µg/L <1 < 1 T

















Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes



a-BHC mg/kg <0.5 < 0.5 T




b-BHC mg/kg <0.5 < 0.5 T


d-BHC mg/kg <0.5 < 0.5 T

DDD mg/kg <0.5 < 0.5 T

DDE mg/kg <0.5 < 0.5 T

DDT mg/kg <0.5 < 0.5 T





g-BHC mg/kg <0.5 < 0.5 T










a-BHC µg/L 4.1 4.0 101 70-130 % T

a-Chlordane µg/L 4.5 4.0 112 70-130 % T


Aldrin µg/L 4.0 4.0 100 70-130 % T

b-BHC µg/L 4.4 4.0 110 70-130 % T


d-BHC µg/L 4.4 4.0 109 70-130 % T

DDD µg/L 4.5 4.0 112 70-130 % T

DDE µg/L 4.3 4.0 108 70-130 % T

DDT µg/L 3.3 4.0 83 70-130 % T

Dieldrin µg/L 4.2 4.0 105 70-130 % T


Endrin µg/L 3.7 4.0 93 70-130 % T



g-Chlordane µg/L 4.8 4.0 120 70-130 % T

Heptachlor µg/L 3.3 4.0 82 70-130 % T










Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes

525389 [ Duplicate of 522832 ]


a-BHCDB mg/kg <0.5 <0.5 <1 0-30 % T



AldrinDB mg/kg <0.5 <0.5 <1 0-30 % T

b-BHCDB mg/kg <0.5 <0.5 <1 0-30 % T


d-BHCDB mg/kg <0.5 <0.5 <1 0-30 % T

DDDDB mg/kg <0.5 <0.5 <1 0-30 % T

DDEDB mg/kg <0.5 <0.5 <1 0-30 % T

DDTDB mg/kg <0.5 <0.5 <1 0-30 % T




EndrinDB mg/kg <0.5 <0.5 <1 0-30 % T

g-BHCDB mg/kg <0.5 <0.5 <1 0-30 % T








525390 [ Duplicate of 522833 ]


a-BHCDB mg/kg <0.5 <0.5 <1 0-30 % T



AldrinDB mg/kg <0.5 <0.5 <1 0-30 % T

b-BHCDB mg/kg <0.5 <0.5 <1 0-30 % T


d-BHCDB mg/kg <0.5 <0.5 <1 0-30 % T

DDDDB mg/kg <0.5 <0.5 <1 0-30 % T

DDEDB mg/kg <0.5 <0.5 <1 0-30 % T

DDTDB mg/kg <0.5 <0.5 <1 0-30 % T




EndrinDB mg/kg <0.5 <0.5 <1 0-30 % T

g-BHCDB mg/kg <0.5 <0.5 <1 0-30 % T












Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes

525393 [ Spike of 522834 ]
























Sample Integrity









DescriptionCode



Authorised By



Laboratory Manager


Final Report













Client Name: Butler Partners Pty Ltd Date Received: 29 June 2007





Job Information

Sample Integrity








Analysis Requested










Note













Logged in by : Patricia Chew Date : Fri 29 June 2007








79 Doggett Street


Australia




Received Date 03/07/2007 08:00:00 AM

Customer Sample ID D1-SP1A D1-SP2A D1-SP3A


Date Sampled 02/07/2007 02/07/2007 02/07/2007

SVOC





mg/kg <0.5 <0.5Aldrin 0.5 <0.5

mg/kg <0.5 <0.5b-BHC 0.5 <0.5


mg/kg <0.5 <0.5d-BHC 0.5 <0.5

mg/kg 5.2 0.5DDD 0.5 16

mg/kg 0.7 <0.5DDE 0.5 3.7

mg/kg 50 4.5DDT 0.5 65

mg/kg <0.5 <0.5Dieldrin 0.5 <0.5


mg/kg <0.5 <0.5Endrin 0.5 <0.5


mg/kg <0.5 <0.5g-BHC 0.5 <0.5








TE

1 122

Metals








mg/kg 130 100Zinc 2 110


Miscellaneous








Date Sampled 02/07/2007 02/07/2007 02/07/2007

Miscellaneous





Date Sampled 02/07/2007 02/07/2007 02/07/2007

SVOC





mg/kg <0.5 <0.5Aldrin 0.5 <0.5

mg/kg <0.5 <0.5b-BHC 0.5 <0.5


mg/kg <0.5 <0.5d-BHC 0.5 <0.5

mg/kg <0.5 3.1DDD 0.5 1.8

mg/kg <0.5 1.3DDE 0.5 1.2

mg/kg 2.1 34DDT 0.5 7.4

mg/kg <0.5 <0.5Dieldrin 0.5 <0.5


mg/kg <0.5 <0.5Endrin 0.5 <0.5


mg/kg <0.5 <0.5g-BHC 0.5 <0.5








TE

1 106

Metals








mg/kg 97 110Zinc 2 110


Miscellaneous









Date Sampled 02/07/2007 02/07/2007 02/07/2007

Miscellaneous


% 16 21% Moisture 1 16



Date Sampled 02/07/2007 02/07/2007 02/07/2007

SVOC





mg/kg <0.5 <0.5Aldrin 0.5 <0.5

mg/kg <0.5 <0.5b-BHC 0.5 <0.5


mg/kg <0.5 <0.5d-BHC 0.5 <0.5

mg/kg 2.3 2.2DDD 0.5 3.1

mg/kg 1.2 0.6DDE 0.5 0.8

mg/kg 17 7.4DDT 0.5 22

mg/kg <0.5 <0.5Dieldrin 0.5 <0.5


mg/kg <0.5 <0.5Endrin 0.5 <0.5


mg/kg <0.5 <0.5g-BHC 0.5 <0.5








TE

1 107

Metals








mg/kg 110 98Zinc 2 110


Miscellaneous









Date Sampled 02/07/2007 02/07/2007 02/07/2007

SVOC





mg/kg <0.5 <0.5Aldrin 0.5 <0.5

mg/kg <0.5 <0.5b-BHC 0.5 <0.5


mg/kg <0.5 <0.5d-BHC 0.5 <0.5

mg/kg 2.1 2.2DDD 0.5 4.4

mg/kg 0.8 0.5DDE 0.5 1.5

mg/kg 15 13DDT 0.5 37

mg/kg <0.5 <0.5Dieldrin 0.5 <0.5


mg/kg <0.5 <0.5Endrin 0.5 <0.5


mg/kg <0.5 <0.5g-BHC 0.5 <0.5








TE

1 104

Metals








mg/kg 110 120Zinc 2 130


Miscellaneous



Customer Sample ID D1-SP1B D1-SP2B D1-SP3B


Date Sampled 02/07/2007 02/07/2007 02/07/2007

SVOC







Date Sampled 02/07/2007 02/07/2007 02/07/2007

SVOC





mg/kg <0.5 <0.5Aldrin 0.5 <0.5

mg/kg <0.5 <0.5b-BHC 0.5 <0.5


mg/kg <0.5 <0.5d-BHC 0.5 <0.5

mg/kg 9.2 2.9DDD 0.5 4.1

mg/kg 0.6 0.7DDE 0.5 0.5

mg/kg 30 18DDT 0.5 23

mg/kg <0.5 <0.5Dieldrin 0.5 <0.5


mg/kg <0.5 <0.5Endrin 0.5 <0.5


mg/kg <0.5 <0.5g-BHC 0.5 <0.5








TE

1 107

Metals








mg/kg 95 110Zinc 2 72


Miscellaneous





Date Sampled 02/07/2007 02/07/2007 02/07/2007

SVOC









Date Sampled 02/07/2007 02/07/2007 02/07/2007

SVOC


mg/kg <0.5 <0.5a-BHC 0.5 <0.5



mg/kg <0.5 <0.5Aldrin 0.5 <0.5

mg/kg <0.5 <0.5b-BHC 0.5 <0.5


mg/kg <0.5 <0.5d-BHC 0.5 <0.5

mg/kg 9.6 3.4DDD 0.5 2.9

mg/kg 0.9 0.5DDE 0.5 0.5

mg/kg 42 10DDT 0.5 15

mg/kg <0.5 <0.5Dieldrin 0.5 <0.5


mg/kg <0.5 <0.5Endrin 0.5 <0.5


mg/kg <0.5 <0.5g-BHC 0.5 <0.5








TE

1 97

Metals


3200 Total Metals in Soil by ICP/AES mg/kg 13 7.4Arsenic 3 10








Miscellaneous



Customer Sample ID D1-SP7B D1-SP8B BV-D30


Date Sampled 02/07/2007 02/07/2007 02/07/2007

SVOC







Customer Sample ID D1-SP7B D1-SP8B BV-D30


Date Sampled 02/07/2007 02/07/2007 02/07/2007

SVOC




mg/kg <0.5 <0.5Aldrin 0.5 <0.5

mg/kg <0.5 <0.5b-BHC 0.5 <0.5


mg/kg <0.5 <0.5d-BHC 0.5 <0.5

mg/kg 1.0 <0.5DDD 0.5 13

mg/kg <0.5 <0.5DDE 0.5 1.1

mg/kg 2.5 <0.5DDT 0.5 96

mg/kg <0.5 <0.5Dieldrin 0.5 <0.5


mg/kg <0.5 <0.5Endrin 0.5 <0.5


mg/kg <0.5 <0.5g-BHC 0.5 <0.5








TE

1 93

Metals






mg/kg 9.6 8.0Lead 5 19

mg/kg 7.5 24Nickel 2 23



Miscellaneous





Date Sampled 02/07/2007 02/07/2007 02/07/2007

SVOC










Date Sampled 02/07/2007 02/07/2007 02/07/2007

SVOC



mg/kg <0.5 <0.5Aldrin 0.5 <0.5

mg/kg <0.5 <0.5b-BHC 0.5 <0.5


mg/kg <0.5 <0.5d-BHC 0.5 <0.5

mg/kg <0.5 <0.5DDD 0.5 <0.5

mg/kg <0.5 <0.5DDE 0.5 <0.5

mg/kg <0.5 <0.5DDT 0.5 <0.5

mg/kg <0.5 <0.5Dieldrin 0.5 <0.5


mg/kg <0.5 <0.5Endrin 0.5 <0.5


mg/kg <0.5 <0.5g-BHC 0.5 <0.5








TE

1 107

Metals






mg/kg 9.5 7.8Lead 5 8.8




Miscellaneous





Date Sampled 02/07/2007 02/07/2007 02/07/2007

SVOC











Date Sampled 02/07/2007 02/07/2007 02/07/2007

SVOC


mg/kg <0.5 <0.5Aldrin 0.5 <0.5

mg/kg <0.5 <0.5b-BHC 0.5 <0.5


mg/kg <0.5 <0.5d-BHC 0.5 <0.5

mg/kg <0.5 44DDD 0.5 <0.5

mg/kg <0.5 2.1DDE 0.5 <0.5

mg/kg <0.5 170DDT 0.5 <0.5

mg/kg <0.5 <0.5Dieldrin 0.5 <0.5


mg/kg <0.5 <0.5Endrin 0.5 <0.5


mg/kg <0.5 <0.5g-BHC 0.5 <0.5








TE

1 107

Metals






mg/kg 6.0 8.6Lead 5 5.6


mg/kg 46 130Zinc 2 40


Miscellaneous



Customer Sample ID DUP02 DUP03 DUP04


Date Sampled 02/07/2007 02/07/2007 02/07/2007

SVOC





mg/kg <0.5 <0.5Aldrin 0.5 <0.5







Date Sampled 02/07/2007 02/07/2007 02/07/2007

SVOC


mg/kg <0.5 <0.5b-BHC 0.5 <0.5


mg/kg <0.5 <0.5d-BHC 0.5 <0.5

mg/kg 56 2.9DDD 0.5 <0.5

mg/kg 3.6 2.4DDE 0.5 <0.5

mg/kg 240 10DDT 0.5 <0.5

mg/kg <0.5 <0.5Dieldrin 0.5 <0.5


mg/kg <0.5 <0.5Endrin 0.5 <0.5


mg/kg <0.5 <0.5g-BHC 0.5 <0.5








TE

1 102

Metals






mg/kg 8.8 24Lead 5 7.5


mg/kg 90 100Zinc 2 57


Miscellaneous





Date Sampled 02/07/2007 02/07/2007 02/07/2007

SVOC





mg/kg <0.5 <0.5Aldrin 0.5 <0.5

mg/kg <0.5 <0.5b-BHC 0.5 <0.5







Date Sampled 02/07/2007 02/07/2007 02/07/2007

SVOC



mg/kg <0.5 <0.5d-BHC 0.5 <0.5

mg/kg 6.2 <0.5DDD 0.5 3.5

mg/kg 0.7 <0.5DDE 0.5 1.4

mg/kg 13 <0.5DDT 0.5 11

mg/kg <0.5 <0.5Dieldrin 0.5 <0.5


mg/kg <0.5 <0.5Endrin 0.5 <0.5


mg/kg <0.5 <0.5g-BHC 0.5 <0.5








TE

1 102

Metals






mg/kg 13 7.6Lead 5 22


mg/kg 82 51Zinc 2 110


Miscellaneous



Customer Sample ID D3-BV1 D3-BV2 D3-NV1


Date Sampled 02/07/2007 02/07/2007 02/07/2007

SVOC





mg/kg <0.5 <0.5Aldrin 0.5 <0.5

mg/kg <0.5 <0.5b-BHC 0.5 <0.5






Customer Sample ID D3-BV1 D3-BV2 D3-NV1


Date Sampled 02/07/2007 02/07/2007 02/07/2007

SVOC


mg/kg <0.5 <0.5d-BHC 0.5 <0.5

mg/kg <0.5 <0.5DDD 0.5 <0.5

mg/kg <0.5 <0.5DDE 0.5 <0.5

mg/kg <0.5 <0.5DDT 0.5 <0.5

mg/kg <0.5 <0.5Dieldrin 0.5 <0.5


mg/kg <0.5 <0.5Endrin 0.5 <0.5


mg/kg <0.5 <0.5g-BHC 0.5 <0.5








TE

1 98

Metals






mg/kg 7.6 6.3Lead 5 7.2




Miscellaneous



Customer Sample ID D3-EV1 D3-EV2 D3-WV1


Date Sampled 02/07/2007 02/07/2007 02/07/2007

SVOC





mg/kg <0.5 <0.5Aldrin 0.5 <0.5

mg/kg <0.5 <0.5b-BHC 0.5 <0.5


mg/kg <0.5 <0.5d-BHC 0.5 <0.5





Customer Sample ID D3-EV1 D3-EV2 D3-WV1


Date Sampled 02/07/2007 02/07/2007 02/07/2007

SVOC


mg/kg <0.5 <0.5DDD 0.5 <0.5

mg/kg <0.5 <0.5DDE 0.5 <0.5

mg/kg <0.5 <0.5DDT 0.5 <0.5

mg/kg <0.5 <0.5Dieldrin 0.5 <0.5


mg/kg <0.5 <0.5Endrin 0.5 <0.5


mg/kg <0.5 <0.5g-BHC 0.5 <0.5








TE

1 114

Metals






mg/kg 7.6 6.9Lead 5 7.5




Miscellaneous



Customer Sample ID D3-WV2 TB-020707 FB-020707


Date Sampled 02/07/2007 02/07/2007 02/07/2007

SVOC


2300 OC Pesticides in Soil by GC-ECD mg/kg - -a-BHC 0.5 <0.5

mg/kg - -a-Chlordane 0.5 <0.5

mg/kg - -a-Endosulfan 0.5 <0.5

mg/kg - -Aldrin 0.5 <0.5

mg/kg - -b-BHC 0.5 <0.5

mg/kg - -b-Endosulfan 0.5 <0.5

mg/kg - -d-BHC 0.5 <0.5

mg/kg - -DDD 0.5 <0.5







Date Sampled 02/07/2007 02/07/2007 02/07/2007

SVOC


mg/kg - -DDE 0.5 <0.5

mg/kg - -DDT 0.5 <0.5

mg/kg - -Dieldrin 0.5 <0.5

mg/kg - -Endosulfan sulfate 0.5 <0.5

mg/kg - -Endrin 0.5 <0.5

mg/kg - -Endrin Aldehyde 0.5 <0.5

mg/kg - -g-BHC 0.5 <0.5

mg/kg - -g-Chlordane 0.5 <0.5

mg/kg - -Heptachlor 0.5 <0.5

mg/kg - -Heptachlor epoxide 0.5 <0.5

mg/kg - -Hexachlorobenzene (HCB) 0.5 <0.5

mg/kg - -Methoxychlor 0.5 <0.5

mg/kg - -Oxychlordane 0.5 <0.5


TE

1 97





µg/L <2 <2b-BHC 2 -


µg/L <1 <1d-BHC 1 -

µg/L <1 <1DDD 1 -

µg/L <1 <1DDE 1 -

µg/L <1 <1DDT 1 -













TE

1 -

Metals



µg/L <0.1 <0.1Cadmium 0.1 -

µg/L <1 <1Lead 1 -











Date Sampled 02/07/2007 02/07/2007 02/07/2007

Metals


mg/kg - -Lead 5 7.4


mg/kg - -Zinc 2 49

3400 Total Mercury in Soil by ICP-AES mg/kg - -Total Mercury 0.05 <0.05




µg/L <5 <5Zinc 5 -


Miscellaneous






SVOC





µg/LAldrin 1 <1

µg/Lb-BHC 2 <2


µg/Ld-BHC 1 <1

µg/LDDD 1 <1

µg/LDDE 1 <1

µg/LDDT 1 <1

µg/LDieldrin 1 <1


µg/LEndrin 1 <1










TE

1 100

Metals









Metals




µg/LLead 1 <1


µg/LCopper 2 <2

µg/LNickel 5 <5

µg/LZinc 5 6.0


Sample History
















General










Holding Times









Acceptance


Limits

Qualifying

Codes






Boron µg/L <100 < 100 T







Tin µg/L <50 < 50 T


Zinc µg/L <5 < 5 T








Lead µg/L <1 < 1 T








Lead mg/kg <5 < 5 T


Zinc mg/kg <2 < 2 T






Acceptance


Limits

Qualifying

Codes







Lead mg/kg <5 < 5 T


Zinc mg/kg <2 < 2 T







Lead mg/kg <5 < 5 T


Zinc mg/kg <2 < 2 T












Antimony µg/L 940 1000.0 94 80-120 % T

Barium µg/L 980 1000.0 98 80-120 % T

Beryllium µg/L 1000 1000.0 101 80-120 % T

Boron µg/L 980 1000.0 98 80-120 % T

Chromium µg/L 970 1000.0 97 80-120 % T

Cobalt µg/L 1000 1000.0 101 80-120 % T

Copper µg/L 980 1000.0 98 80-120 % T

Manganese µg/L 1000 1000.0 101 80-120 % T


Nickel µg/L 990 1000.0 99 80-120 % T

Tin µg/L 1000 1000.0 101 80-120 % T

Vanadium µg/L 1000 1000.0 102 80-120 % T

Zinc µg/L 1000 1000.0 104 80-120 % T



Mercury µg/L 9.57 0.01 96 80-120 % T



Arsenic µg/L 10 10.0 100.0 80-120 % T

Cadmium µg/L 2.0 2.0 100.85 80-120 % T

Lead µg/L 11 10.0 108.19 80-120 % T

Selenium µg/L 11 10.0 107.8 80-120 % T






Acceptance


Limits

Qualifying

Codes



Arsenic mg/kg 51 50.0 101 70-130 % T

Cadmium mg/kg 52 50.0 104 70-130 % T

Chromium mg/kg 49 50.0 97 70-130 % T

Copper mg/kg 51 50.0 102 70-130 % T

Lead mg/kg 50 50.0 99 70-130 % T

Nickel mg/kg 48 50.0 96 70-130 % T

Zinc mg/kg 50 50.0 100 70-130 % T



Arsenic mg/kg 50 50.0 100 70-130 % T

Cadmium mg/kg 52 50.0 104 70-130 % T

Chromium mg/kg 49 50.0 98 70-130 % T

Copper mg/kg 52 50.0 104 70-130 % T

Lead mg/kg 49 50.0 99 70-130 % T

Nickel mg/kg 48 50.0 97 70-130 % T

Zinc mg/kg 50 50.0 101 70-130 % T



Arsenic mg/kg 49 50.0 98 70-130 % T

Cadmium mg/kg 50 50.0 101 70-130 % T

Chromium mg/kg 47 50.0 94 70-130 % T

Copper mg/kg 50 50.0 99 70-130 % T

Lead mg/kg 48 50.0 96 70-130 % T

Nickel mg/kg 46 50.0 93 70-130 % T

Zinc mg/kg 48 50.0 97 70-130 % T



Mercury mg/kg 0.47 0.5 95 75-125 % T



Mercury mg/kg 0.45 0.5 89 75-125 % T



Mercury mg/kg 0.53 0.5 106 75-125 % T

526133 [ Duplicate of 525962 ]






LeadDB mg/kg 28 21 29 0-30 % T

NickelDB mg/kg 14 24 50 0-30 % F Q02

ZincDB mg/kg 100 110 4 0-30 % T

526134 [ Duplicate of 525963 ]


ArsenicDB mg/kg 13 15 17 0-30 % T



CopperDB mg/kg 36 26 32 0-30 % F Q02

LeadDB mg/kg 24 18 27 0-30 % T


ZincDB mg/kg 150 130 18 0-30 % T






Acceptance


Limits

Qualifying

Codes

526135 [ Duplicate of 525964 ]






LeadDB mg/kg 13 18 28 0-30 % T


ZincDB mg/kg 89 100 12 0-30 % T

526136 [ Duplicate of 525965 ]






LeadDB mg/kg 210 23 160 0-30 % F Q02


ZincDB mg/kg 130 110 11 0-30 % T

526137 [ Duplicate of 525962 ]



526138 [ Duplicate of 525963 ]



526139 [ Duplicate of 525964 ]


MercuryDB mg/kg 0.06 0.06 11 0-30 % T

526141 [ Duplicate of 525965 ]


MercuryDB mg/kg 0.07 0.06 9 0-30 % T

526193 [ Spike of 525966 ]









526194 [ Spike of 525967 ]









526195 [ Spike of 525966 ]



526196 [ Spike of 525967 ]



Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes





Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes



a-BHC mg/kg <0.5 < 0.5 T




b-BHC mg/kg <0.5 < 0.5 T


d-BHC mg/kg <0.5 < 0.5 T

DDD mg/kg <0.5 < 0.5 T

DDE mg/kg <0.5 < 0.5 T

DDT mg/kg <0.5 < 0.5 T





g-BHC mg/kg <0.5 < 0.5 T










a-BHC mg/kg <0.5 < 0.5 T




b-BHC mg/kg <0.5 < 0.5 T


d-BHC mg/kg <0.5 < 0.5 T

DDD mg/kg <0.5 < 0.5 T

DDE mg/kg <0.5 < 0.5 T

DDT mg/kg <0.5 < 0.5 T





g-BHC mg/kg <0.5 < 0.5 T







2.4.5.6-tetrachloro-m-xylene-SURROGATE % <1 70-130 % F





Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes



a-BHC mg/kg <0.5 < 0.5 T




b-BHC mg/kg <0.5 < 0.5 T


d-BHC mg/kg <0.5 < 0.5 T

DDD mg/kg <0.5 < 0.5 T

DDE mg/kg <0.5 < 0.5 T

DDT mg/kg <0.5 < 0.5 T





g-BHC mg/kg <0.5 < 0.5 T

















DDD µg/L <1 < 1 T

DDE µg/L <1 < 1 T

DDT µg/L <1 < 1 T

















Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes



a-BHC mg/kg 2.1 2.0 104 70-130 % T



Aldrin mg/kg 1.9 2.0 96 70-130 % T

b-BHC mg/kg 2.1 2.0 104 70-130 % T


d-BHC mg/kg 2.2 2.0 109 70-130 % T

DDD mg/kg 2.1 2.0 104 70-130 % T

DDE mg/kg 2.1 2.0 107 70-130 % T

DDT mg/kg 1.8 2.0 92 70-130 % T

Dieldrin mg/kg 2.1 2.0 104 70-130 % T


Endrin mg/kg 1.8 2.0 90 70-130 % T


g-BHC mg/kg 2.2 2.0 109 70-130 % T




Hexachlorobenzene (HCB) mg/kg <0.5 2.0 0 70-130 % F





a-BHC mg/kg 2.2 2.0 108 70-130 % T



Aldrin mg/kg 2.3 2.0 114 70-130 % T

b-BHC mg/kg 2.1 2.0 106 70-130 % T


d-BHC mg/kg 2.0 2.0 98 70-130 % T

DDD mg/kg 1.9 2.0 97 70-130 % T

DDE mg/kg 2.0 2.0 101 70-130 % T

DDT mg/kg 1.9 2.0 95 70-130 % T

Dieldrin mg/kg 2.2 2.0 108 70-130 % T


Endrin mg/kg 2.5 2.0 123 70-130 % T


g-BHC mg/kg 2.1 2.0 107 70-130 % T











Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes



a-BHC µg/L 4.0 4.0 99 70-130 % T

a-Chlordane µg/L 4.6 4.0 114 70-130 % T


Aldrin µg/L 4.3 4.0 109 70-130 % T

b-BHC µg/L 3.9 4.0 97 70-130 % T


d-BHC µg/L 4.6 4.0 115 70-130 % T

DDD µg/L 4.8 4.0 119 70-130 % T

DDE µg/L 4.8 4.0 121 70-130 % T

DDT µg/L 4.0 4.0 101 70-130 % T

Dieldrin µg/L 5.0 4.0 124 70-130 % T


Endrin µg/L 4.2 4.0 105 70-130 % T



g-Chlordane µg/L 5.1 4.0 126 70-130 % T

Heptachlor µg/L 4.1 4.0 103 70-130 % T




Q02526142 [ Duplicate of 525962 ]


a-BHCDB mg/kg <0.5 <0.5 <1 0-30 % T



AldrinDB mg/kg <0.5 <0.5 <1 0-30 % T

b-BHCDB mg/kg <0.5 <0.5 <1 0-30 % T


d-BHCDB mg/kg <0.5 <0.5 <1 0-30 % T

DDDDB mg/kg 0.7 16 181 0-30 % F

DDEDB mg/kg 1.6 3.7 81 0-30 % F

DDTDB mg/kg 6.6 65 163 0-30 % F




EndrinDB mg/kg <0.5 <0.5 <1 0-30 % T

g-BHCDB mg/kg <0.5 <0.5 <1 0-30 % T












Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes

Q02526153 [ Duplicate of 525963 ]


a-BHCDB mg/kg <0.5 <0.5 <1 0-30 % T



AldrinDB mg/kg <0.5 <0.5 <1 0-30 % T

b-BHCDB mg/kg <0.5 <0.5 <1 0-30 % T


d-BHCDB mg/kg <0.5 <0.5 <1 0-30 % T

DDDDB mg/kg 1.5 5.2 108 0-30 % F

DDEDB mg/kg 0.7 0.7 4 0-30 % T

DDTDB mg/kg 16 50 103 0-30 % F




EndrinDB mg/kg <0.5 <0.5 <1 0-30 % T

g-BHCDB mg/kg <0.5 <0.5 <1 0-30 % T








Q08526197 [ Spike of 525966 ]




a-EndosulfanDB mg/kg <0.5 N/A N/A N/A N/A













g-ChlordaneDB mg/kg <0.5 N/A N/A N/A N/A











Laboratory: EN_SVOC

Acceptance


Limits

Qualifying

Codes

526198 [ Spike of 525967 ]











DDTDB mg/kg 43 N/A N/A N/A N/A













Sample Integrity









DescriptionCode



Q08 The Matrix Spike recovery is outside of the recommended acceptance criteria. An acceptable recovery was obtained

for the laboratory control sample indicating a sample matrix interference.



Authorised By



Laboratory Manager


Final Report









Client Reference number: Turnaround: 48 Hour06155C



Job Information

Sample Integrity








Analysis Requested










48 HOUR

Note













Logged in by : Patricia Chew Date : Tue 3 July 2007



EB1001008

False


Work Order : EB1001008 Page : 1 of 6

:: LaboratoryClient Environmental Division BrisbaneBUTLER PARTNERS PTY LTD

: :ContactContact MR LUKE AMIES Tim Kilmister

:: AddressAddress P O BOX 2267

FORTITUDE VALLEY BC QLD, AUSTRALIA 4006

32 Shand Street Stafford QLD Australia 4053

:: E-mailE-mail [email protected] [email protected]

:: TelephoneTelephone +61 38523800 +61-7-3243 7222

:: FacsimileFacsimile +61 07 38523808 +61-7-3243 7218

:Project 009-173A QC Level : NEPM 1999 Schedule B(3) and ALS QCS3 requirement

:Order number 2465

:C-O-C number 009173A/6 Date Samples Received : 19-JAN-2010

Sampler : Nick Allen Issue Date : 29-JAN-2010

Site : Yeerongpilly

45:No. of samples received

Quote number : BN/194/09 14:No. of samples analysed

This report supersedes any previous report(s) with this reference. Results apply to the sample(s) as submitted. All pages of this report have been checked and approved for

release.

This Certificate of Analysis contains the following information:

l General Comments

l Analytical Results

l Surrogate Control Limits

NATA Accredited Laboratory 825


accordance with NATA



ISO/IEC 17025.

SignatoriesThis document has been electronically signed by the authorized signatories indicated below. Electronic signing has been

carried out in compliance with procedures specified in 21 CFR Part 11.

Signatories Accreditation CategoryPosition

Xingbin Lin Instrument Chemist Organics

Environmental Division Brisbane


Tel. +61-7-3243 7222 Fax. +61-7-3243 7218 www.alsglobal.com

2 of 6:Page

Work Order :

:Client

EB1001008

BUTLER PARTNERS PTY LTD

009-173A:Project

General Comments

The analytical procedures used by the Environmental Division have been developed from established internationally recognized procedures such as those published by the USEPA, APHA, AS and NEPM. In house

developed procedures are employed in the absence of documented standards or by client request.

Where moisture determination has been performed, results are reported on a dry weight basis.

Where a reported less than (<) result is higher than the LOR, this may be due to primary sample extract/digestate dilution and/or insuffient sample for analysis.

Where the LOR of a reported result differs from standard LOR, this may be due to high moisture content, insufficient sample (reduced weight employed) or matrix interference.

When date(s) and/or time(s) are shown bracketed, these have been assumed by the laboratory for processing purposes. If the sampling time is displayed as 0:00 the information was not provided by client.

CAS Number = CAS registry number from database maintained by Chemical Abstracts Services. The Chemical Abstracts Service is a division of the American Chemical Society.

LOR = Limit of reporting

^ = This result is computed from individual analyte detections at or above the level of reporting

Key :

EP068:Particular samples required dilution prior to analysis due to matrix interferences. LOR values have been adjusted accordingly.l

3 of 6:Page

Work Order :

:Client

EB1001008


009-173A:Project

Analytical Results

B69-3B69-2B69-1B67-2B67-1Client sample IDSub-Matrix: SOIL

19-JAN-2010 15:0019-JAN-2010 15:0019-JAN-2010 15:0019-JAN-2010 15:0019-JAN-2010 15:00Client sampling date / time

EB1001008-011EB1001008-010EB1001008-009EB1001008-006EB1001008-005UnitLORCAS NumberCompound


16.916.1 10.1 11.6 10.3%1.0----^ Moisture Content (dried @ 103°C)

EP068A: Organochlorine Pesticides (OC)<0.05<0.05 <0.15 <0.05 <0.05mg/kg0.05319-84-6alpha-BHC

<0.05<0.05 <0.15 <0.05 <0.05mg/kg0.05118-74-1Hexachlorobenzene (HCB)

<0.05<0.05 <0.15 <0.05 <0.05mg/kg0.05319-85-7beta-BHC

<0.05<0.05 <0.15 <0.05 <0.05mg/kg0.0558-89-9gamma-BHC

<0.05<0.05 <0.15 <0.05 <0.05mg/kg0.05319-86-8delta-BHC

<0.05<0.05 <0.15 <0.05 <0.05mg/kg0.0576-44-8Heptachlor

<0.05<0.05 <0.15 <0.05 <0.05mg/kg0.05309-00-2Aldrin

<0.05<0.05 <0.15 <0.05 <0.05mg/kg0.051024-57-3Heptachlor epoxide

<0.05<0.05 <0.15 <0.05 <0.05mg/kg0.055103-74-2trans-Chlordane

<0.05<0.05 <0.15 <0.05 <0.05mg/kg0.05959-98-8alpha-Endosulfan

<0.05<0.05 <0.15 <0.05 <0.05mg/kg0.055103-71-9cis-Chlordane

<0.05<0.05 <0.15 <0.05 <0.05mg/kg0.0560-57-1Dieldrin

<0.05<0.05 0.52 0.42 <0.05mg/kg0.0572-55-94.4`-DDE

<0.05<0.05 <0.15 <0.05 <0.05mg/kg0.0572-20-8Endrin

<0.05<0.05 <0.15 <0.05 <0.05mg/kg0.0533213-65-9beta-Endosulfan

<0.05<0.05 1.43 0.56 <0.05mg/kg0.0572-54-84.4`-DDD

<0.05<0.05 <0.15 <0.05 <0.05mg/kg0.057421-93-4Endrin aldehyde

<0.05<0.05 <0.15 <0.05 <0.05mg/kg0.051031-07-8Endosulfan sulfate

<0.2<0.2 3.8 0.7 <0.2mg/kg0.250-29-34.4`-DDT

<0.05<0.05 <0.15 <0.05 <0.05mg/kg0.0553494-70-5Endrin ketone

<0.2<0.2 <0.6 <0.2 <0.2mg/kg0.272-43-5Methoxychlor


90.080.2 75.8 78.8 84.2%0.121655-73-2Dibromo-DDE


10492.6 94.1 98.7 98.2%0.178-48-8DEF

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Analytical Results



EB1001008-033EB1001008-032EB1001008-031EB1001008-030EB1001008-029UnitLORCAS NumberCompound





<0.05<0.05 <0.05 <0.05 <0.05mg/kg0.05319-85-7beta-BHC

<0.05<0.05 <0.05 <0.05 <0.05mg/kg0.0558-89-9gamma-BHC

<0.05<0.05 <0.05 <0.05 <0.05mg/kg0.05319-86-8delta-BHC

<0.05<0.05 <0.05 <0.05 <0.05mg/kg0.0576-44-8Heptachlor

<0.05<0.05 <0.05 <0.05 <0.05mg/kg0.05309-00-2Aldrin





<0.05<0.05 <0.05 <0.05 <0.05mg/kg0.0560-57-1Dieldrin

<0.05<0.05 <0.05 <0.05 <0.05mg/kg0.0572-55-94.4`-DDE

<0.05<0.05 <0.05 <0.05 <0.05mg/kg0.0572-20-8Endrin


<0.05<0.05 <0.05 <0.05 <0.05mg/kg0.0572-54-84.4`-DDD



<0.2<0.2 <0.2 <0.2 <0.2mg/kg0.250-29-34.4`-DDT




79.578.4 77.8 86.2 92.6%0.121655-73-2Dibromo-DDE


92.592.4 92.4 78.3 83.7%0.178-48-8DEF

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Analytical Results

----DUP113B77-3B75-3B75-2Client sample IDSub-Matrix: SOIL

----19-JAN-2010 15:0019-JAN-2010 15:0019-JAN-2010 15:0019-JAN-2010 15:00Client sampling date / time

----EB1001008-044EB1001008-043EB1001008-035EB1001008-034UnitLORCAS NumberCompound


6.66.8 13.9 11.4 ----%1.0----^ Moisture Content (dried @ 103°C)

EP068A: Organochlorine Pesticides (OC)<0.05<0.05 <0.05 <0.05 ----mg/kg0.05319-84-6alpha-BHC

<0.05<0.05 <0.05 <0.05 ----mg/kg0.05118-74-1Hexachlorobenzene (HCB)

<0.05<0.05 <0.05 <0.05 ----mg/kg0.05319-85-7beta-BHC

<0.05<0.05 <0.05 <0.05 ----mg/kg0.0558-89-9gamma-BHC

<0.05<0.05 <0.05 <0.05 ----mg/kg0.05319-86-8delta-BHC

<0.05<0.05 <0.05 <0.05 ----mg/kg0.0576-44-8Heptachlor

<0.05<0.05 <0.05 <0.05 ----mg/kg0.05309-00-2Aldrin

<0.05<0.05 <0.05 <0.05 ----mg/kg0.051024-57-3Heptachlor epoxide

<0.05<0.05 <0.05 <0.05 ----mg/kg0.055103-74-2trans-Chlordane

<0.05<0.05 <0.05 <0.05 ----mg/kg0.05959-98-8alpha-Endosulfan

<0.05<0.05 <0.05 <0.05 ----mg/kg0.055103-71-9cis-Chlordane

<0.05<0.05 <0.05 <0.05 ----mg/kg0.0560-57-1Dieldrin

<0.05<0.05 <0.05 <0.05 ----mg/kg0.0572-55-94.4`-DDE

<0.05<0.05 <0.05 <0.05 ----mg/kg0.0572-20-8Endrin

<0.05<0.05 <0.05 <0.05 ----mg/kg0.0533213-65-9beta-Endosulfan

<0.05<0.05 <0.05 <0.05 ----mg/kg0.0572-54-84.4`-DDD

<0.05<0.05 <0.05 <0.05 ----mg/kg0.057421-93-4Endrin aldehyde

<0.05<0.05 <0.05 <0.05 ----mg/kg0.051031-07-8Endosulfan sulfate

<0.2<0.2 <0.2 <0.2 ----mg/kg0.250-29-34.4`-DDT

<0.05<0.05 <0.05 <0.05 ----mg/kg0.0553494-70-5Endrin ketone

<0.2<0.2 <0.2 <0.2 ----mg/kg0.272-43-5Methoxychlor


88.780.8 87.7 88.6 ----%0.121655-73-2Dibromo-DDE


81.373.6 80.0 80.0 ----%0.178-48-8DEF

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Recovery Limits (%)Sub-Matrix: SOIL

Compound CAS Number Low High


Dibromo-DDE 21655-73-2 49 130


DEF 78-48-8 53 140

False












Site : Yeerongpilly


Sampler : Nick Allen Issue Date : 29-JAN-2010

:Order number 2465




release.

This Quality Control Report contains the following information:

l Laboratory Duplicate (DUP) Report; Relative Percentage Difference (RPD) and Acceptance Limits

l Method Blank (MB) and Laboratory Control Spike (LCS) Report ; Recovery and Acceptance Limits

l Matrix Spike (MS) Report; Recovery and Acceptance Limits






ISO/IEC 17025.




Xingbin Lin Instrument Chemist Organics




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General Comments






Anonymous = Refers to samples which are not specifically part of this work order but formed part of the QC process lot



RPD = Relative Percentage Difference

# = Indicates failed QC

Key :

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Laboratory Duplicate (DUP) Report

The quality control term Laboratory Duplicate refers to a randomly selected intralaboratory split. Laboratory duplicates provide information regarding method precision and sample heterogeneity. The permitted ranges

for the Relative Percent Deviation (RPD) of Laboratory Duplicates are specified in ALS Method QWI -EN/38 and are dependent on the magnitude of results in comparison to the level of reporting: Result < 10 times LOR:-

No Limit; Result between 10 and 20 times LOR:- 0% - 50%; Result > 20 times LOR:- 0% - 20%.

Sub-Matrix: SOIL Laboratory Duplicate (DUP) Report

Original Result RPD (%)Laboratory sample ID Client sample ID Method: Compound CAS Number LOR Unit Duplicate Result Recovery Limits (%)

EA055: Moisture Content (QC Lot: 1227293)

EA055-103: Moisture Content (dried @ 103°C) ---- 1.0 % 14.9 15.4 2.9 0% - 50%AnonymousEB1001006-009

EA055-103: Moisture Content (dried @ 103°C) ---- 1.0 % 10.2 10.5 2.5 0% - 50%B74-1EB1001008-030

EP068A: Organochlorine Pesticides (OC) (QC Lot: 1230163)

EP068: alpha-BHC 319-84-6 0.05 mg/kg <0.05 <0.05 0.0 No LimitB75-1EB1001008-033

EP068: Hexachlorobenzene (HCB) 118-74-1 0.05 mg/kg <0.05 <0.05 0.0 No Limit

EP068: beta-BHC 319-85-7 0.05 mg/kg <0.05 <0.05 0.0 No Limit

EP068: gamma-BHC 58-89-9 0.05 mg/kg <0.05 <0.05 0.0 No Limit

EP068: delta-BHC 319-86-8 0.05 mg/kg <0.05 <0.05 0.0 No Limit

EP068: Heptachlor 76-44-8 0.05 mg/kg <0.05 <0.05 0.0 No Limit

EP068: Aldrin 309-00-2 0.05 mg/kg <0.05 <0.05 0.0 No Limit

EP068: Heptachlor epoxide 1024-57-3 0.05 mg/kg <0.05 <0.05 0.0 No Limit

EP068: trans-Chlordane 5103-74-2 0.05 mg/kg <0.05 <0.05 0.0 No Limit

EP068: alpha-Endosulfan 959-98-8 0.05 mg/kg <0.05 <0.05 0.0 No Limit

EP068: cis-Chlordane 5103-71-9 0.05 mg/kg <0.05 <0.05 0.0 No Limit

EP068: Dieldrin 60-57-1 0.05 mg/kg <0.05 <0.05 0.0 No Limit

EP068: 4.4`-DDE 72-55-9 0.05 mg/kg <0.05 <0.05 0.0 No Limit

EP068: Endrin 72-20-8 0.05 mg/kg <0.05 <0.05 0.0 No Limit

EP068: beta-Endosulfan 33213-65-9 0.05 mg/kg <0.05 <0.05 0.0 No Limit

EP068: 4.4`-DDD 72-54-8 0.05 mg/kg <0.05 <0.05 0.0 No Limit

EP068: Endrin aldehyde 7421-93-4 0.05 mg/kg <0.05 <0.05 0.0 No Limit

EP068: Endosulfan sulfate 1031-07-8 0.05 mg/kg <0.05 <0.05 0.0 No Limit

EP068: Endrin ketone 53494-70-5 0.05 mg/kg <0.05 <0.05 0.0 No Limit

EP068: 4.4`-DDT 50-29-3 0.2 mg/kg <0.2 <0.2 0.0 No Limit

EP068: Methoxychlor 72-43-5 0.2 mg/kg <0.2 <0.2 0.0 No Limit

EP068: alpha-BHC 319-84-6 0.05 mg/kg <0.25 <0.25 0.0 No LimitAnonymousEM1000566-009











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EP068A: Organochlorine Pesticides (OC) (QC Lot: 1230163) - continued

EP068: Dieldrin 60-57-1 0.05 mg/kg <0.25 <0.25 0.0 No LimitAnonymousEM1000566-009










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Method Blank (MB) and Laboratory Control Spike (LCS) Report

The quality control term Method / Laboratory Blank refers to an analyte free matrix to which all reagents are added in the same volumes or proportions as used in standard sample preparation. The purpose of this QC

parameter is to monitor potential laboratory contamination. The quality control term Laboratory Control Sample (LCS) refers to a certified reference material, or a known interference free matrix spiked with target

analytes. The purpose of this QC parameter is to monitor method precision and accuracy independent of sample matrix. Dynamic Recovery Limits are based on statistical evaluation of processed LCS.

Sub-Matrix: SOIL Method Blank (MB)

Report

Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit

EP068A: Organochlorine Pesticides (OC) (QCLot: 1230163)

EP068: alpha-BHC 319-84-6 0.05 mg/kg <0.05 77.30.25 mg/kg 13047.3

EP068: Hexachlorobenzene (HCB) 118-74-1 0.05 mg/kg <0.05 77.90.25 mg/kg 12845.6

EP068: beta-BHC 319-85-7 0.05 mg/kg <0.05 78.50.25 mg/kg 13055.9

EP068: gamma-BHC 58-89-9 0.05 mg/kg <0.05 77.60.25 mg/kg 12951.1

EP068: delta-BHC 319-86-8 0.05 mg/kg <0.05 83.70.25 mg/kg 12756.1

EP068: Heptachlor 76-44-8 0.05 mg/kg <0.05 82.20.25 mg/kg 12551.6

EP068: Aldrin 309-00-2 0.05 mg/kg <0.05 77.90.25 mg/kg 12154.9

EP068: Heptachlor epoxide 1024-57-3 0.05 mg/kg <0.05 81.40.25 mg/kg 12256.9

EP068: trans-Chlordane 5103-74-2 0.05 mg/kg <0.05 81.70.25 mg/kg 12257.9

EP068: alpha-Endosulfan 959-98-8 0.05 mg/kg <0.05 83.00.25 mg/kg 12856.6

EP068: cis-Chlordane 5103-71-9 0.05 mg/kg <0.05 81.10.25 mg/kg 12357.1

EP068: Dieldrin 60-57-1 0.05 mg/kg <0.05 81.90.25 mg/kg 12356

EP068: 4.4`-DDE 72-55-9 0.05 mg/kg <0.05 81.00.25 mg/kg 12558.4

EP068: Endrin 72-20-8 0.05 mg/kg <0.05 83.80.25 mg/kg 12857.9

EP068: beta-Endosulfan 33213-65-9 0.05 mg/kg <0.05 79.70.25 mg/kg 12860.6

EP068: 4.4`-DDD 72-54-8 0.05 mg/kg <0.05 74.10.25 mg/kg 12655.7

EP068: Endrin aldehyde 7421-93-4 0.05 mg/kg <0.05 77.80.25 mg/kg 12347.1

EP068: Endosulfan sulfate 1031-07-8 0.05 mg/kg <0.05 85.80.25 mg/kg 12857.2

EP068: 4.4`-DDT 50-29-3 0.2 mg/kg <0.2 74.20.25 mg/kg 13452.5

EP068: Endrin ketone 53494-70-5 0.05 mg/kg <0.05 80.80.25 mg/kg 12657.7

EP068: Methoxychlor 72-43-5 0.2 mg/kg <0.2 82.80.25 mg/kg 13953.4

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Matrix Spike (MS) Report

The quality control term Matrix Spike (MS) refers to an intralaboratory split sample spiked with a representative set of target analytes. The purpose of this QC parameter is to monitor potential matrix effects on analyte

recoveries. Static Recovery Limits as per laboratory Data Quality Objectives (DQOs). Ideal recovery ranges stated may be waived in the event of sample matrix interference.

Sub-Matrix: SOIL Matrix Spike (MS) Report

Spike Recovery (%) Recovery Limits (%)Spike

HighLowMSConcentrationLaboratory sample ID Client sample ID Method: Compound CAS Number


B67-1EB1001008-005 58-89-9EP068: gamma-BHC 85.90.25 mg/kg 13345

76-44-8EP068: Heptachlor 91.00.25 mg/kg 12840

309-00-2EP068: Aldrin 94.10.25 mg/kg 12645

60-57-1EP068: Dieldrin 93.50.25 mg/kg 12650

72-20-8EP068: Endrin 94.20.25 mg/kg 13446

50-29-3EP068: 4.4`-DDT 73.60.25 mg/kg 13535

True












Site : Yeerongpilly


Nick Allen:Sampler Issue Date : 29-JAN-2010

:Order number 2465

No. of samples received : 45

Quote number : BN/194/09 No. of samples analysed : 14

This report supersedes any previous report(s) with this reference. Results apply to the sample(s) as submitted. All pages of this report have been checked and approved for release.

This Interpretive Quality Control Report contains the following information:


l Quality Control Parameter Frequency Compliance


l Summary of Outliers




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Analysis Holding Time Compliance

The following report summarises extraction / preparation and analysis times and compares with recommended holding times. Dates reported represent first date of extraction or analysis and precludes subsequent

dilutions and reruns. Information is also provided re the sample container (preservative) from which the analysis aliquot was taken. Elapsed period to analysis represents number of days from sampling where no

extraction / digestion is involved or period from extraction / digestion where this is present. For composite samples, sampling date is assumed to be that of the oldest sample contributing to the composite. Sample date

for laboratory produced leachates is assumed as the completion date of the leaching process. Outliers for holding time are based on USEPA SW 846, APHA, AS and NEPM (1999). A listing of breaches is provided in

the Summary of Outliers.

Holding times for leachate methods (excluding elutriates) vary according to the analytes being determined on the resulting solution. For non -volatile analytes, the holding time compliance assessment compares the

leach date with the shortest analyte holding time for the equivalent soil method. These soil holding times are: Organics (14 days); Mercury (28 days) & other metals (180 days). A recorded breach therefore does not

guarantee a breach for all non-volatile parameters.

Matrix: SOIL Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)



26-JAN-2010----B67-1, B67-2,

B69-1, B69-2,

B69-3, B73-4,

B74-1, B74-2,

B74-3, B75-1,

B75-2, B75-3,

B77-3, DUP113

22-JAN-2010----19-JAN-2010 ---- ü



08-MAR-201002-FEB-2010B67-1, B67-2,

B69-1, B69-2,

B69-3, B73-4,

B74-1, B74-2,

B74-3, B75-1,

B75-2, B75-3,

B77-3, DUP113

28-JAN-201027-JAN-201019-JAN-2010 ü ü

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Quality Control Parameter Frequency ComplianceThe following report summarises the frequency of laboratory QC samples analysed within the analytical lot(s) in which the submitted sample(s) was(where) processed. Actual rate should be greater than or equal to

the expected rate. A listing of breaches is provided in the Summary of Outliers.

Matrix: SOIL Evaluation: û = Quality Control frequency not within specification ; ü = Quality Control frequency within specification.

Quality Control SpecificationQuality Control Sample Type

ExpectedQC Regular Actual

Rate (%)Quality Control Sample Type CountEvaluationAnalytical Methods Method


NEPM 1999 Schedule B(3) and ALS QCS3 requirement 11.1 10.02 18 üMoisture Content EA055-103

NEPM 1999 Schedule B(3) and ALS QCS3 requirement 10.0 10.02 20 üPesticides by GCMS EP068



Method Blanks (MB)


Matrix Spikes (MS)

ALS QCS3 requirement 5.0 5.01 20 üPesticides by GCMS EP068

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Brief Method SummariesThe analytical procedures used by the Environmental Division have been developed from established internationally recognized procedures such as those published by the US EPA, APHA, AS and NEPM. In house

developed procedures are employed in the absence of documented standards or by client request. The following report provides brief descriptions of the analytical procedures employed for results reported in the

Certificate of Analysis. Sources from which ALS methods have been developed are provided within the Method Descriptions.

Analytical Methods Method DescriptionsMatrixMethod

A gravimetric procedure based on weight loss over a 12 hour drying period at 103-105 degrees C. This method

is compliant with NEPM (1999) Schedule B(3) (Method 102)

Moisture Content EA055-103 SOIL

(USEPA SW 846 - 8270B) Extracts are analysed by Capillary GC/MS and quantification is by comparison against

an established 5 point calibration curve. This technique is compliant with NEPM (1999) Schedule B(3) (Method

504,505)

Pesticides by GCMS EP068 SOIL

Preparation Methods Method DescriptionsMatrixMethod

In-house, Mechanical agitation (tumbler). 20g of sample, Na2SO4 and surrogate are extracted with 150mL 1:1

DCM/Acetone by end over end tumble. The solvent is decanted, dehydrated and concentrated (by KD) to the

desired volume for analysis.

Tumbler Extraction of Solids (Option A -

Concentrating)

ORG17A SOIL

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Summary of Outliers


The following report highlights outliers flagged in the Quality Control (QC) Report. Surrogate recovery limits are static and based on USEPA SW846 or ALS-QWI/EN/38 (in the absence of specific USEPA limits). This

report displays QC Outliers (breaches) only.

Duplicates, Method Blanks, Laboratory Control Samples and Matrix Spikes

l For all matrices, no Method Blank value outliers occur.

l For all matrices, no Duplicate outliers occur.

l For all matrices, no Laboratory Control outliers occur.

l For all matrices, no Matrix Spike outliers occur.

Regular Sample Surrogates

l For all regular sample matrices, no surrogate recovery outliers occur.

Outliers : Analysis Holding Time Compliance

This report displays Holding Time breaches only. Only the respective Extraction / Preparation and/or Analysis component is/are displayed.

l No Analysis Holding Time Outliers exist.


The following report highlights breaches in the Frequency of Quality Control Samples.

l No Quality Control Sample Frequency Outliers exist.

0.00

SAMPLE RECEIPT NOTIFICATION (SRN)Comprehensive Report

Work Order : EB1001008




FORTITUDE VALLEY BC QLD,

AUSTRALIA 4006

32 Shand Street Stafford QLD Australia

4053




::Project 009-173A Page 1 of 3

:Order number 2465

::C-O-C number 009173A/6 Quote number EB2009BUTPAR0323 (BN/194/09)

Site : Yeerongpilly

Sampler : :QC LevelNick Allen NEPM 1999 Schedule B(3) and ALS

QCS3 requirement

DatesDate Samples Received : 19-JAN-2010 Issue Date : 22-JAN-2010 12:38

Scheduled Reporting Date: 29-JAN-2010:Client Requested Due Date 27-JAN-2010

Delivery DetailsMode of Delivery Temperature: :Carrier 16.4 ,20.9 °C - Ice bricks

presentNo. of coolers/boxes No. of samples received: :1 MEDIUM, 1 SMALL 45

Sercurity Seal No. of samples analysed: :Intact. 14

General Comments

This report contains the following information:l

- Sample Container(s)/Preservation Non-Compliances

- Summary of Sample(s) and Requested Analysis

- Requested Deliverables

l Samples received in appropriately pretreated and preserved containers.l Sample(s) have been received within recommended holding times.

l Please direct any turn around / technical queries to the laboratory contact designated above.

l Please direct any queries related to sample condition / numbering / breakages to Maggie Kahi.

l Analytical work for this work order will be conducted at ALS Melbourne.

l Sample Disposal - Aqueous (14 days), Solid (90 days) from date of completion of work order.




22-JAN-2010 12:38:Issue Date

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Sample Container(s)/Preservation Non-Compliances



Summary of Sample(s) and Requested Analysis

Some items described below may be part of a laboratory

process neccessary for the execution of client requested

tasks. Packages may contain additional analyses, such as

the determination of moisture content and preparation

tasks, that are included in the package.

When date(s) and/or time(s) are shown bracketed, these

have been assumed by the laboratory for processing

purposes. If the sampling time is displayed as 0:00 the

information was not provided by client.

(On

Ho

ld)

SO

IL

No

an

aly

sis

req

ue

ste

d

SO

IL -

EA

05

5-1

03

Mo

istu

re C

on

ten

t

SO

IL -

EP

06

8A

(so

lids)

Org

an

och

lorin

e P

estic

ide

s b

y G

CM

S

EB1001008-001 19-JAN-2010 15:00 A9-1 ü

EB1001008-002 19-JAN-2010 15:00 A9-2 ü

EB1001008-003 19-JAN-2010 15:00 A9-3 ü

EB1001008-004 19-JAN-2010 15:00 A9-4 ü

EB1001008-005 19-JAN-2010 15:00 B67-1 ü ü

EB1001008-006 19-JAN-2010 15:00 B67-2 ü ü

EB1001008-007 19-JAN-2010 15:00 B68-1 ü

EB1001008-008 19-JAN-2010 15:00 B68-2 ü

EB1001008-009 19-JAN-2010 15:00 B69-1 ü ü

EB1001008-010 19-JAN-2010 15:00 B69-2 ü ü

EB1001008-011 19-JAN-2010 15:00 B69-3 ü ü

EB1001008-012 19-JAN-2010 15:00 B69-4 ü

EB1001008-013 19-JAN-2010 15:00 B70-1 ü

EB1001008-014 19-JAN-2010 15:00 B70-2 ü

EB1001008-015 19-JAN-2010 15:00 B70-3 ü

EB1001008-016 19-JAN-2010 15:00 B70-4 ü

EB1001008-017 19-JAN-2010 15:00 B70-5 ü

EB1001008-018 19-JAN-2010 15:00 B71-1 ü

EB1001008-019 19-JAN-2010 15:00 B71-2 ü

EB1001008-020 19-JAN-2010 15:00 B71-3 ü

EB1001008-021 19-JAN-2010 15:00 B71-4 ü

EB1001008-022 19-JAN-2010 15:00 B72-1 ü

EB1001008-023 19-JAN-2010 15:00 B72-2 ü

EB1001008-024 19-JAN-2010 15:00 B72-3 ü

EB1001008-025 19-JAN-2010 15:00 B72-4 ü

EB1001008-026 19-JAN-2010 15:00 B73-1 ü

EB1001008-027 19-JAN-2010 15:00 B73-2 ü

EB1001008-028 19-JAN-2010 15:00 B73-3 ü

EB1001008-029 19-JAN-2010 15:00 B73-4 ü ü

EB1001008-030 19-JAN-2010 15:00 B74-1 ü ü

EB1001008-031 19-JAN-2010 15:00 B74-2 ü ü

EB1001008-032 19-JAN-2010 15:00 B74-3 ü ü

EB1001008-033 19-JAN-2010 15:00 B75-1 ü ü

EB1001008-034 19-JAN-2010 15:00 B75-2 ü ü

EB1001008-035 19-JAN-2010 15:00 B75-3 ü ü

Matrix: SOIL

Client sample IDLaboratory sample

ID

Client sampling

date / time

22-JAN-2010 12:38:Issue Date

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(On

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EB1001008-036 19-JAN-2010 15:00 B75-4 ü

EB1001008-037 19-JAN-2010 15:00 B76-1 ü

EB1001008-038 19-JAN-2010 15:00 B76-2 ü

EB1001008-039 19-JAN-2010 15:00 B76-3 ü

EB1001008-040 19-JAN-2010 15:00 B76-4 ü

EB1001008-041 19-JAN-2010 15:00 B77-1 ü

EB1001008-042 19-JAN-2010 15:00 B77-2 ü

EB1001008-043 19-JAN-2010 15:00 B77-3 ü ü

EB1001008-044 19-JAN-2010 15:00 DUP113 ü ü

EB1001008-045 19-JAN-2010 15:00 DUP114 ü

Requested Deliverables

MR LUKE AMIES

- *AU Certificate of Analysis - NATA ( COA ) Email [email protected]

- *AU Interpretive QC Report - DEFAULT (Anon QCI Rep) ( QCI ) Email [email protected]

- *AU QC Report - DEFAULT (Anon QC Rep) - NATA ( QC ) Email [email protected]

- A4 - AU Sample Receipt Notification - Environmental ( SRN ) Email [email protected]

- A4 - AU Tax Invoice ( INV ) Email [email protected]

- Default - Chain of Custody ( COC ) Email [email protected]

- EDI Format - ENMRG ( ENMRG ) Email [email protected]

- EDI Format - XTab ( XTAB ) Email [email protected]

MS SUE WILLIAMS


EM1001038

False


Work Order : EM1001038 Page : 1 of 4

:: LaboratoryClient Environmental Division MelbourneBUTLER PARTNERS PTY LTD

: :ContactContact MR LUKE AMIES Steven McGrath



4 Westall Rd Springvale VIC Australia 3171




:Project 009-173A - REBATCH EB1001008 QC Level : NEPM 1999 Schedule B(3) and ALS QCS3 requirement

:Order number 2465

:C-O-C number ---- Date Samples Received : 02-FEB-2010

Sampler : ---- Issue Date : 05-FEB-2010

Site : YEERONGPILLY




release.

This Certificate of Analysis contains the following information:

l General Comments

l Analytical Results

l Surrogate Control Limits






ISO/IEC 17025.




Nancy Wang Instrument Chemist Organics

Environmental Division Melbourne



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EM1001038


009-173A - REBATCH EB1001008:Project

General Comments






When date(s) and/or time(s) are shown bracketed, these have been assumed by the laboratory for processing purposes. If the sampling time is displayed as 0:00 the information was not provided by client.



^ = This result is computed from individual analyte detections at or above the level of reporting

Key :

EP068: Results need to be scrutinized accordingly as samples were extracted outside the holding time.l

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Analytical Results



EM1001038-005EM1001038-004EM1001038-003EM1001038-002EM1001038-001UnitLORCAS NumberCompound





<0.05<0.05 <0.05 <0.05 <0.05mg/kg0.05319-85-7beta-BHC

<0.05<0.05 <0.05 <0.05 <0.05mg/kg0.0558-89-9gamma-BHC

<0.05<0.05 <0.05 <0.05 <0.05mg/kg0.05319-86-8delta-BHC

<0.05<0.05 <0.05 <0.05 <0.05mg/kg0.0576-44-8Heptachlor

<0.05<0.05 <0.05 <0.05 <0.05mg/kg0.05309-00-2Aldrin





<0.05<0.05 <0.05 <0.05 <0.05mg/kg0.0560-57-1Dieldrin

<0.05<0.05 0.07 0.06 0.12mg/kg0.0572-55-94.4`-DDE

<0.05<0.05 <0.05 <0.05 <0.05mg/kg0.0572-20-8Endrin


<0.05<0.05 <0.05 <0.05 0.50mg/kg0.0572-54-84.4`-DDD



<0.2<0.2 <0.2 <0.2 3.5mg/kg0.250-29-34.4`-DDT




87.961.7 99.4 70.8 69.0%0.121655-73-2Dibromo-DDE


10072.1 116 82.8 80.9%0.178-48-8DEF

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Recovery Limits (%)Sub-Matrix: SOIL

Compound CAS Number Low High


Dibromo-DDE 21655-73-2 49 130


DEF 78-48-8 53 140

False












Site : YEERONGPILLY


Sampler : ---- Issue Date : 05-FEB-2010

:Order number 2465




release.

This Quality Control Report contains the following information:

l Laboratory Duplicate (DUP) Report; Relative Percentage Difference (RPD) and Acceptance Limits

l Method Blank (MB) and Laboratory Control Spike (LCS) Report ; Recovery and Acceptance Limits

l Matrix Spike (MS) Report; Recovery and Acceptance Limits






ISO/IEC 17025.




Nancy Wang Instrument Chemist Organics




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General Comments






Anonymous = Refers to samples which are not specifically part of this work order but formed part of the QC process lot



RPD = Relative Percentage Difference

# = Indicates failed QC

Key :

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EM1001038



Laboratory Duplicate (DUP) Report

The quality control term Laboratory Duplicate refers to a randomly selected intralaboratory split. Laboratory duplicates provide information regarding method precision and sample heterogeneity. The permitted ranges

for the Relative Percent Deviation (RPD) of Laboratory Duplicates are specified in ALS Method QWI -EN/38 and are dependent on the magnitude of results in comparison to the level of reporting: Result < 10 times LOR:-

No Limit; Result between 10 and 20 times LOR:- 0% - 50%; Result > 20 times LOR:- 0% - 20%.



EA055: Moisture Content (QC Lot: 1237631)

EA055-103: Moisture Content (dried @ 103°C) ---- 1.0 % 9.4 9.6 1.9 No LimitAnonymousEM1000947-002

EA055-103: Moisture Content (dried @ 103°C) ---- 1.0 % 10.0 10.6 5.6 0% - 50%AnonymousEM1000947-023

EP068A: Organochlorine Pesticides (OC) (QC Lot: 1237206)

EP068: alpha-BHC 319-84-6 0.05 mg/kg <0.05 <0.05 0.0 No LimitB68-1EM1001038-001











EP068: Dieldrin 60-57-1 0.05 mg/kg <0.05 <0.05 0.0 No Limit










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Method Blank (MB) and Laboratory Control Spike (LCS) Report

The quality control term Method / Laboratory Blank refers to an analyte free matrix to which all reagents are added in the same volumes or proportions as used in standard sample preparation. The purpose of this QC

parameter is to monitor potential laboratory contamination. The quality control term Laboratory Control Sample (LCS) refers to a certified reference material, or a known interference free matrix spiked with target

analytes. The purpose of this QC parameter is to monitor method precision and accuracy independent of sample matrix. Dynamic Recovery Limits are based on statistical evaluation of processed LCS.

Sub-Matrix: SOIL Method Blank (MB)

Report

Laboratory Control Spike (LCS) Report

Spike Spike Recovery (%) Recovery Limits (%)

Result Concentration HighLowLCSMethod: Compound CAS Number LOR Unit


EP068: alpha-BHC 319-84-6 0.05 mg/kg <0.05 92.30.25 mg/kg 13047.3

EP068: Hexachlorobenzene (HCB) 118-74-1 0.05 mg/kg <0.05 81.00.25 mg/kg 12845.6

EP068: beta-BHC 319-85-7 0.05 mg/kg <0.05 94.70.25 mg/kg 13055.9

EP068: gamma-BHC 58-89-9 0.05 mg/kg <0.05 92.30.25 mg/kg 12951.1

EP068: delta-BHC 319-86-8 0.05 mg/kg <0.05 91.20.25 mg/kg 12756.1

EP068: Heptachlor 76-44-8 0.05 mg/kg <0.05 98.90.25 mg/kg 12551.6

EP068: Aldrin 309-00-2 0.05 mg/kg <0.05 1080.25 mg/kg 12154.9

EP068: Heptachlor epoxide 1024-57-3 0.05 mg/kg <0.05 96.80.25 mg/kg 12256.9

EP068: trans-Chlordane 5103-74-2 0.05 mg/kg <0.05 96.30.25 mg/kg 12257.9

EP068: alpha-Endosulfan 959-98-8 0.05 mg/kg <0.05 99.60.25 mg/kg 12856.6

EP068: cis-Chlordane 5103-71-9 0.05 mg/kg <0.05 97.10.25 mg/kg 12357.1

EP068: Dieldrin 60-57-1 0.05 mg/kg <0.05 89.60.25 mg/kg 12356

EP068: 4.4`-DDE 72-55-9 0.05 mg/kg <0.05 95.00.25 mg/kg 12558.4

EP068: Endrin 72-20-8 0.05 mg/kg <0.05 98.30.25 mg/kg 12857.9

EP068: beta-Endosulfan 33213-65-9 0.05 mg/kg <0.05 81.20.25 mg/kg 12860.6

EP068: 4.4`-DDD 72-54-8 0.05 mg/kg <0.05 95.30.25 mg/kg 12655.7

EP068: Endrin aldehyde 7421-93-4 0.05 mg/kg <0.05 91.40.25 mg/kg 12347.1

EP068: Endosulfan sulfate 1031-07-8 0.05 mg/kg <0.05 95.30.25 mg/kg 12857.2

EP068: 4.4`-DDT 50-29-3 0.2 mg/kg <0.2 97.90.25 mg/kg 13452.5

EP068: Endrin ketone 53494-70-5 0.05 mg/kg <0.05 95.90.25 mg/kg 12657.7

EP068: Methoxychlor 72-43-5 0.2 mg/kg <0.2 95.80.25 mg/kg 13953.4

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Matrix Spike (MS) Report

The quality control term Matrix Spike (MS) refers to an intralaboratory split sample spiked with a representative set of target analytes. The purpose of this QC parameter is to monitor potential matrix effects on analyte

recoveries. Static Recovery Limits as per laboratory Data Quality Objectives (DQOs). Ideal recovery ranges stated may be waived in the event of sample matrix interference.

Sub-Matrix: SOIL Matrix Spike (MS) Report

Spike Recovery (%) Recovery Limits (%)Spike

HighLowMSConcentrationLaboratory sample ID Client sample ID Method: Compound CAS Number


B68-2EM1001038-002 58-89-9EP068: gamma-BHC 75.50.25 mg/kg 13345

76-44-8EP068: Heptachlor 96.50.25 mg/kg 12840

309-00-2EP068: Aldrin 78.70.25 mg/kg 12645

60-57-1EP068: Dieldrin 88.80.25 mg/kg 12650

72-20-8EP068: Endrin 1020.25 mg/kg 13446

50-29-3EP068: 4.4`-DDT 73.00.25 mg/kg 13535

True












Site : YEERONGPILLY


----:Sampler Issue Date : 05-FEB-2010

:Order number 2465

No. of samples received : 5

Quote number : BN/194/09 No. of samples analysed : 5

This report supersedes any previous report(s) with this reference. Results apply to the sample(s) as submitted. All pages of this report have been checked and approved for release.

This Interpretive Quality Control Report contains the following information:


l Quality Control Parameter Frequency Compliance


l Summary of Outliers




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Analysis Holding Time Compliance

The following report summarises extraction / preparation and analysis times and compares with recommended holding times. Dates reported represent first date of extraction or analysis and precludes subsequent

dilutions and reruns. Information is also provided re the sample container (preservative) from which the analysis aliquot was taken. Elapsed period to analysis represents number of days from sampling where no

extraction / digestion is involved or period from extraction / digestion where this is present. For composite samples, sampling date is assumed to be that of the oldest sample contributing to the composite. Sample date

for laboratory produced leachates is assumed as the completion date of the leaching process. Outliers for holding time are based on USEPA SW 846, APHA, AS and NEPM (1999). A listing of breaches is provided in

the Summary of Outliers.

Holding times for leachate methods (excluding elutriates) vary according to the analytes being determined on the resulting solution. For non -volatile analytes, the holding time compliance assessment compares the

leach date with the shortest analyte holding time for the equivalent soil method. These soil holding times are: Organics (14 days); Mercury (28 days) & other metals (180 days). A recorded breach therefore does not

guarantee a breach for all non-volatile parameters.

Matrix: SOIL Evaluation: û = Holding time breach ; ü = Within holding time.

AnalysisExtraction / PreparationSample DateMethod

EvaluationDue for analysisDate analysedEvaluationDue for extractionDate extractedContainer / Client Sample ID(s)



26-JAN-2010----B68-1, B68-2,

B76-1, B76-2,

B76-3

03-FEB-2010----19-JAN-2010 ---- û



15-MAR-201002-FEB-2010B68-1, B68-2,

B76-1, B76-2,

B76-3

04-FEB-201003-FEB-201019-JAN-2010 û ü

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Quality Control Parameter Frequency ComplianceThe following report summarises the frequency of laboratory QC samples analysed within the analytical lot(s) in which the submitted sample(s) was(where) processed. Actual rate should be greater than or equal to

the expected rate. A listing of breaches is provided in the Summary of Outliers.

Matrix: SOIL Evaluation: û = Quality Control frequency not within specification ; ü = Quality Control frequency within specification.

Quality Control SpecificationQuality Control Sample Type

ExpectedQC Regular Actual

Rate (%)Quality Control Sample Type CountEvaluationAnalytical Methods Method


NEPM 1999 Schedule B(3) and ALS QCS3 requirement 11.1 10.02 18 üMoisture Content EA055-103




Method Blanks (MB)


Matrix Spikes (MS)

ALS QCS3 requirement 20.0 5.01 5 üPesticides by GCMS EP068

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Brief Method SummariesThe analytical procedures used by the Environmental Division have been developed from established internationally recognized procedures such as those published by the US EPA, APHA, AS and NEPM. In house

developed procedures are employed in the absence of documented standards or by client request. The following report provides brief descriptions of the analytical procedures employed for results reported in the

Certificate of Analysis. Sources from which ALS methods have been developed are provided within the Method Descriptions.

Analytical Methods Method DescriptionsMatrixMethod

A gravimetric procedure based on weight loss over a 12 hour drying period at 103-105 degrees C. This method

is compliant with NEPM (1999) Schedule B(3) (Method 102)

Moisture Content EA055-103 SOIL

(USEPA SW 846 - 8270B) Extracts are analysed by Capillary GC/MS and quantification is by comparison against

an established 5 point calibration curve. This technique is compliant with NEPM (1999) Schedule B(3) (Method

504,505)

Pesticides by GCMS EP068 SOIL

Preparation Methods Method DescriptionsMatrixMethod

In-house, Mechanical agitation (tumbler). 20g of sample, Na2SO4 and surrogate are extracted with 150mL 1:1

DCM/Acetone by end over end tumble. The solvent is decanted, dehydrated and concentrated (by KD) to the

desired volume for analysis.

Tumbler Extraction of Solids (Option A -

Concentrating)

ORG17A SOIL

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Summary of Outliers


The following report highlights outliers flagged in the Quality Control (QC) Report. Surrogate recovery limits are static and based on USEPA SW846 or ALS-QWI/EN/38 (in the absence of specific USEPA limits). This

report displays QC Outliers (breaches) only.

Duplicates, Method Blanks, Laboratory Control Samples and Matrix Spikes

l For all matrices, no Method Blank value outliers occur.

l For all matrices, no Duplicate outliers occur.

l For all matrices, no Laboratory Control outliers occur.

l For all matrices, no Matrix Spike outliers occur.

Regular Sample Surrogates

l For all regular sample matrices, no surrogate recovery outliers occur.

Outliers : Analysis Holding Time Compliance

This report displays Holding Time breaches only. Only the respective Extraction / Preparation and/or Analysis component is/are displayed.

Matrix: SOIL


Date analysedDate extractedContainer / Client Sample ID(s) Days

overdue

Days

overdue

Due for extraction Due for analysis

Method



26-JAN-2010----B68-1, B68-2,

B76-1, B76-2,

B76-3

03-FEB-2010---- ---- 8



----02-FEB-2010B68-1, B68-2,

B76-1, B76-2,

B76-3

----03-FEB-2010 1 ----


The following report highlights breaches in the Frequency of Quality Control Samples.

l No Quality Control Sample Frequency Outliers exist.

0.00

SAMPLE RECEIPT NOTIFICATION (SRN)Comprehensive Report

Work Order : EM1001038




FORTITUDE VALLEY BC QLD,

AUSTRALIA 4006

4 Westall Rd Springvale VIC Australia

3171




::Project 009-173A - REBATCH EB1001008 Page 1 of 2

:Order number 2465

::C-O-C number ---- Quote number EB2009BUTPAR0323 (BN/194/09)

Site : YEERONGPILLY

Sampler : :QC Level---- NEPM 1999 Schedule B(3) and ALS

QCS3 requirement

DatesDate Samples Received : 02-FEB-2010 Issue Date : 02-FEB-2010 16:07

Scheduled Reporting Date: 09-FEB-2010:Client Requested Due Date 09-FEB-2010

Delivery DetailsMode of Delivery Temperature: :Samples on hand ----

No. of coolers/boxes No. of samples received: :N/A 5

Sercurity Seal No. of samples analysed: :Intact. 5

General Comments

This report contains the following information:l

- Sample Container(s)/Preservation Non-Compliances

- Summary of Sample(s) and Requested Analysis

- Requested Deliverables

l Samples received in appropriately pretreated and preserved containers.l Sample(s) have been received within recommended holding timesl Please direct any queries related to sample condition / numbering / breakages to Peter Ravlic.l Analytical work for this work order will be conducted at ALS Melbourne.

l Sample Disposal - Aqueous (14 days), Solid (90 days) from date of completion of work order.




02-FEB-2010 16:07:Issue Date

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Sample Container(s)/Preservation Non-Compliances



Summary of Sample(s) and Requested Analysis

Some items described below may be part of a laboratory

process neccessary for the execution of client requested

tasks. Packages may contain additional analyses, such as

the determination of moisture content and preparation

tasks, that are included in the package.

When date(s) and/or time(s) are shown bracketed, these

have been assumed by the laboratory for processing

purposes. If the sampling time is displayed as 0:00 the

information was not provided by client.

SO

IL -

EA

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EM1001038-001 19-JAN-2010 15:00 B68-1 ü ü

EM1001038-002 19-JAN-2010 15:00 B68-2 ü ü

EM1001038-003 19-JAN-2010 15:00 B76-1 ü ü

EM1001038-004 19-JAN-2010 15:00 B76-2 ü ü

EM1001038-005 19-JAN-2010 15:00 B76-3 ü ü

Matrix: SOIL

Client sample IDLaboratory sample

ID

Client sampling

date / time

Requested Deliverables

MR LUKE AMIES

- *AU Certificate of Analysis - NATA ( COA ) Email [email protected]

- *AU Interpretive QC Report - DEFAULT (Anon QCI Rep) ( QCI ) Email [email protected]

- *AU QC Report - DEFAULT (Anon QC Rep) - NATA ( QC ) Email [email protected]

- A4 - AU Sample Receipt Notification - Environmental ( SRN ) Email [email protected]


- Default - Chain of Custody ( COC ) Email [email protected]

- EDI Format - ENMRG ( ENMRG ) Email [email protected]

- EDI Format - XTab ( XTAB ) Email [email protected]

MS SUE WILLIAMS
