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    PRODUCTION OF 100,000 TONNE PER ANNUM OF 2-ETHYLHEXYL ACRYLATEMECHANICAL AND CHEMICAL DESIGN 5

    CHAPTER 5

    HEAT EXCHANGER

    5.1 INTRODUCTION

    Heat exchangers are found in most chemical system. Sinnot (1999) reported that heat

    exchanger is a device that is used to transfer thermal energy between two or more fluids at

    different temperatures and in thermal contact (Sinnot, 1999).

    Some of more common applications are found in heating, cooling, evaporation or

    condensation, control process liquid and etc. Direct and indirect transfers are two ways of

    heat being transferred by heat exchanger. In direct contact type of heat exchanger or

    recuperators, the fluid does not mix because it was separated by the walls. It contrasts with

    indirect contact of heat exchanger or simply regenerator where heat exchange is done via

    energy storage and rejection trough the exchanger surface. In designing heat exchanger,

    there are several criteria that to be taking into consideration. The details such as the type of

    fluid and phase will be the major factor in choosing the type of heat exchanger.

    5.1.1 Types of heat exchangers

    The term of exchanger absolutely applies to all types of equipment in which heat

    exchange specifically to donate equipment in which heat is exchanged between two

    process streams. For example if exchanger in which a process fluid is heated or cooled by

    a plant service stream is referred to as heaters and coolers, if the process stream is

    vaporize, the exchanger is called vaporizers.

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    The types of heat exchanger used in chemical process and allied industry are listed below:

    Table 5.1: Heat exchanger type

    No. Types Functions

    1. Double pipe heat exchanger The simplest type. Use for heating and cooling.

    2. Shell and tube heat exchanger Used for all application.

    3. Plate exchanger Use for heating and cooling.

    4. Plate-fin exchanger Use for heating and cooling.

    5. Spiral heat exchanger Use for heating and cooling.

    6. Air cooled Cooler and condenser.

    7. Direct contact Cooling and quenching.

    8. Agitated vessels Use for heating and cooling.

    9. Fired heaters Use for heating and cooling.

    (Sinnot, 1999)

    5.1.2 Shell and Tube exchangers: Construction details

    The shell and tube exchanger is the most common type of heat transfer equipment used in

    chemical and allied industries. The advantages of this type are:

    I. The configuration gives a large surface area in a small volume

    II. Good mechanical layout: a good shape for pressure operation

    III. Uses well-established fabrication techniques

    IV. Can be constructed from a wide range of materials

    V. Easily cleaned

    VI. Well established design procedures.

    In manufacturing industry, the application of heat exchanger is used for the process of

    system to derive the final product. The selection of heat exchanger is very important in

    order to achieve 3Ps which are people, profit and planet. The safety of people or workers,

    safe environment and earn profit with recycle back waste of heat in the process. In order to

    select an appropriate heat exchanger, one would firstly consider the design limitations for

    each heat exchanger type. Although cost is often the first criterion evaluated.

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    The simplest and cheapest heat exchanger is the fixed tube sheet design. The main

    advantages are the bundle cannot be removed for cleaning and there is no provision for

    differential expansion of shell and tubes. The U-tube requires only one tube sheet and is

    cheaper than the floating-head types. This type is widely used but limited in use to relative

    cleans fluids as the tube and budles are difficult to clean.

    The exchanger with floating head is more versatile than fixed head and U-tube

    exchangers. They are suitable for high temperature differentials and easier to clean and

    also can be used for fouling liquids.

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    Table 5.2: Selection of heat exchanger

    Type designation Significant feature Application best suited limitations

    Fixed tube sheet Both tube sheets fixed to shell Condenser; liquid-liquid; gas-

    gas; liquid-gas, cooling and

    heating, horizontal or vertical,

    reboiling.

    Temperature difference at

    extremes of about 200F

    Floating head or tubesheet (removable and

    nonremovable bundles)

    One tube sheet floats inshell or with shell, tube bundle

    may or may not be removable

    from shell, but back cover can

    be removed to expose tube

    ends.

    High temperature differentials,above about 200F. Extremes;

    dirty fluids requiring cleaning of

    inside as well as outside of shell,

    horizontal or vertical.

    Internal gaskets offer dangerof leaking. Corrosiveness of

    fluids on shell side floating

    parts. Usually confined to

    horizontal units.

    u-tube, u-bundle Only one tube sheet required.

    Tubes bent in U-shape.

    Bundle is removable.

    High temperature differentials

    which might require provision for

    expansion in fixed tube units.

    Clean service or easily cleaned

    conditions

    on both tube side and shell side.

    Horizontal or vertical

    Bends must be carefully

    made or mechanical damage

    and danger of rupture can

    result. Tube side velocities

    can cause erosion of inside

    of bends. Fluid should be

    free of suspended particles.

    Kettle Tube bundle removable as U-

    type or floating head. Shell

    enlarged to allow boiling and

    vapor disengaging.

    Boiling fluid on shell side, as

    refrigerant, or process fluid being

    vaporized. Chilling or cooling of

    tube side fluid in refrigerant

    evaporation on shell side.

    For horizontal installation.

    Physically large for other

    applications.

    Source: Rules of Thumbs for chemical engineer, Carl Branan, 2002.

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    5.2 BASIC DESIGN PROCEDURES

    5.2.1 Design Criteria for process heat exchanger

    The criteria that a process heat exchanger must satisfy are easily enough stated

    if we confine ourselves to a certain process. The criteria include:

    1) The heat exchanger must meet the process requirements. This means

    that it must effect the desired change in thermal condition of the process

    stream within the allowable pressure drops. At the same time, it must

    continue doing this until the next scheduled shut down for maintenance.

    2) The heat exchanger must withstand the service conditions of the

    environment of the plant which includes the mechanical stresses of

    installation, start-up, shutdown, normal operation, emergencies and

    maintenance. Besides, the heat exchanger must also resist corrosion by

    the environment, processes and streams. This is mainly a matter of

    choosing materials of construction, but mechanical design does have

    some effect.

    3) The heat exchanger must be maintainable, which usually implies

    choosing a configuration that permits cleaning and replacement. In order

    to do this, the limitations is the positioning the exchanger and providing

    clear space around it. Replacement usually involves tubes and other

    components that may be especially vulnerable to corrosion, erosion, or

    vibration.

    4) The cost of the heat exchanger should be consistent with requirements.

    Meaning of the cost here implement to the cost of installation. Operation

    cost and cost of lost production due to exchanger malfunction or

    unavailable should be considered earlier in the design.

    5) The limitations of the heat exchanger. Limitations are on length,

    diameter, weight and tube specifications due to plant requirements and

    process flow.

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    Figure 5.1 shows the general outlines of the design procedures.

    Step 1

    Specification

    define duty

    Step 2

    Collect physical

    properties

    Step 3

    Assume value of

    overall coefficient

    Uo, ass

    Step 4Decide no of shell

    and tube passes

    calculate Tlm,

    correction factor

    and Tm

    Step 5

    Determine heat

    transfer area

    required

    Step 6

    Decide tube, tube

    size, material

    assign fluid to shell

    or tube side

    Step 7

    Calculate no of

    tubes

    Step 8

    Calculate shell

    diameter

    Step 9

    Estimate tube-side

    heat transfer

    coefficient

    Step 10

    Decide baffle

    spacing and

    estimate shell-side

    heat transfer

    coeffcient

    Step 11

    Calculate overall

    heat transfer

    coefficient

    including fouling

    0 < Uo, cal Uo, ass < 30%

    Uo, ass

    Set Uo, ass = Uo,

    calc

    Step 12

    Estimate tube and

    shell side pressure

    drops

    Pressure drop within

    specification ?

    If yes

    Step 13

    Estimation cost of

    heat exchanger

    Can design be

    optimized to reduce

    cost ??

    If yes

    Accpet design

    If No

    Figure 5.1: Design procedure of heat exchanger (Sinnot, 1999).

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    5.2.2 Fluid allocation factor

    Table 5.3: Fluid allocation

    Factor Fluid allocation

    Corrosion The more corrosive fluid should be allocated to the tube side

    Fouling The fluid that has the greatest tendency to foul the heat transfer

    surfaces should be place in tube

    Fluid temperature If the temperature is high enough to require the use of special

    alloy, placing the higher temperature fluid in the tubes

    Operating pressure The higher pressure stream should be allocated to the tube

    side

    Viscosity A higher heat-transfer coefficient will be obtained by allocating

    the more viscous material to the shell side.

    (Sinnot, 1999)

    5.3 CHEMICAL DESIGN OF HEAT EXCHANGER

    5.3.1 Step 1: Specification

    The product, 2 ethylhexyl acrylate 12430 kg/hr, leaves at top of distillation column at

    119.7C and is to be cooled to 30C by exchange with water at 20C.

    Chilled

    water inlet,

    20C

    water

    outlet, 35C

    2-ethylhexyl

    acrylate at inlet,

    119.7 C

    2-ethylhexyl

    acrylate at outlet,

    30CE-107

    S25S24

    The heat load was 2.989 x 106kJ/hr or 830.278 kW

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    Cooling water balance

    Table 5.4: Fouling factor

    Fluid Coefficient (W/m2.C) Factor (resistance)

    (m2C/W)

    Cooling water (towers) 3000 - 60000 0.00030.00017

    Organic liquids 5000 0.0002

    (Sinnot, 1999)

    5.3.2 Step 2: Physical properties

    Table 5.5: Properties at tube side (Chilled water)

    Properties Inlet Mean Outlet Unit

    Temperature 20 27.5 35 C

    spec heat 4.044 4.0415 4.039 kJ/kgC

    thermal conductivity 0.611 0.6213 0.6315 W/mC

    density 1007 1001.45 995.9 kg/m3

    viscosity 0.8904 0.7719 0.6514 cP

    Flow rate 49320 49320 49320 kg/hr

    Table 5.6: Properties at shell side (2-ethylhexylacrylate)

    Inlet Mean Outlet Unit

    Temperature 119.7 74.85 30 C

    spec heat 2.966 2.8335 2.701 kJ/kg C

    thermal conductivity 9.903 x 10-2 0.1069 0.1147 W/m C

    density 792.7 833.55 871.4 kg/m3

    viscosity 0.394 0.8565 1.319 cP

    Flow rate 12430 12430 12430 kg/hr

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    5.3.3 Step 3: Overall coefficient

    According to typical overall coefficient as shown in Table 5.7, the overall coefficient will

    be in the range 250 to 750 W/m2C. So, first trial starts with 500 W/m2C.

    Table 5.7: Typical overall coefficient

    Shell and Tube heat exchangers

    Hot fluid Cold fluid U (W/m2C)

    Coolers

    Organic Water 250 - 750

    Light oils Water 350 - 900

    Heavy oils Water 60 - 300

    Gases Water 20 - 300

    Organic Brine 150 - 500

    (Sinnot, 1999)

    5.3.4 Step 4: Exchanger Type and Dimensions

    An even number of tube passes is usually the preferred arrangement, at these positions

    the inlet and outlets nozzles at the same end of heat exchanger which simplifies the

    pipe work.

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    Figure 5.2: Heat exchanger

    Start with one shell pass and two tube passes.

    Where

    Assumptions:

    I. No change in specific heat

    II. The overall heat transfer coefficient is constant

    III. No heat losses

    Shell

    Tubes

    T2

    T1

    t2

    t1

    Temperature

    Heat transfer

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    True temperature difference by applying correction factor to allow for the departure from

    counter current flow:

    Where Ftis temperature correction factor

    Two dimensionless temperature ratios:

    R = equal to the shell-side fluid flow rate times the fluid mean specific heat devided by

    the tube side fluid flow rate times the tube-side fluid specific heat.

    S = measure of the temperature efficiency of the exchanger

    Based on figure 12.19 0.98An economic exchanger design cannot normally achieved if the correction factor falls

    below about 0.75

    5.3.5 Step 5: Heat transfer area

    5.3.6 Step 6: Layout and Tube size

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    A shell-and-tube type heat exchanger is recommended because it is a versatile

    exchanger often used in similar applications. The main factors prompting this decision

    are the large surface area provided in a small volume, a good shape for higher

    pressure operations, and the ease of cleaning. The final factor is that design and

    fabrication methods are well established. This enables the design specification to be as

    close to the optimum as is practical.

    A floating head-type shell-and-tube heat exchanger is recommended for this

    application because of the need to provide capacity for thermal expansion of the tube

    bundle. The floating head also enables easy withdrawal of the tube bundle for cleaning

    purposes. This factor may be very advantageous, not because the streams are

    subjected to fouling, but because of the possibility high boiling residues carryover from

    the reactor will be deposited on the walls of the tubes.

    Finally, a split-ring heat exchanger is selected. This split-flange design reduces

    the large clearances for efficiency and ease of cleaning.

    Table 5.8: Design specification

    Material Stainless Steel

    Length of tube, Lt(m) 4.2672

    Outer diameter, Dto, (m) 0.01905

    Inner diameter, Dti, (m) 0.01575

    Material thermal conductivity,(W/m.K) 16

    Pitch, Pt =1.25Dto(m) 0.02381

    (Christie, 1993)

    5.3.7 Step 7: Number of Tubes

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    Equation 5.11

    5.3.8 Step 8: Bundle and Shell Diameter

    Where

    Db= bundle diameter

    Dto= tube outside diameter

    Table 5.9: Constant for use in equation 5.14

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    Triangular pitch, pt= 1.25 Dto

    number of passes 1 2 4 6 8

    K1 0.319 0.249 0.175 0.0743 0.0365

    n1 2.142 2.207 2.285 2.499 2.675(Sinnot, 1999)

    Tube pinch = 1.25Dto

    Shell bundle clearance, Figure 12.12 is 58 mm

    The shell inside diameter, Ds= Db+ 58

    Ds= 386 + 58Ds= 444 mm = 0.44m

    5.3.9 Step 9: Tube side heat transfer coefficient

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    5.3.10 Step 10: Shell side heat transfer coefficient

    0.249 2.207 Shell bundle clearance, Figure 12.12 is 58 mm, (Sinnott and Towler 2009).

    The shell inside diameter, Ds= Db+ 58

    Ds= 386 + 58

    Ds= 444 mm = 0.444m

    As a first trial, take baffle spacing = Ds/2, this spacing should give good heat transfer

    without too high a pressure drop.

    Baffle spacing Lb= 222

    Number of baffle = Nb +1 = L/Lb

    Nb = 18 baffles

    Cross flow Asfor the hypothetical row of tubes at the shell equator:

    Where

    Pt= tube pitch

    lb= baffle spacing

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    Calculate the shell side equivalent diameter (hydraulic diameter)

    Use baffle with a 25% cut which should give a reasonable heat transfer coefficient

    without too large pressure drop.

    From figure 12.29, By neglecting viscosity correction, 5.3.11 Step 11: Overall Coefficient

    Where

    Uo= Overall Coefficient, W/m2C

    hs = Shell side coefficient, W/m2C

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    hi= tube side coefficient, W/m2C

    hod = shell fouling factor, W/m2C

    hid= tube fouling factor, W/m2C

    kw= thermal conductivity of the tube wall material, W/m2C

    Percent error:

    The value falls within the range, thus it is acceptable

    5.3.12 Step 12: Pressure Drop

    5.3.12.1Tube-side pressure drop

    * +

    Where

    Np= number of tube-side passes

    Ut= tube-side velocity, m/s

    L = length of tube.

    Jf = tube side friction factor, figure 12.24 = 2.7 x 10-3

    Neglect viscosity correction

    [ ] 5.3.12.2Shell-side pressure drop

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    * +

    Jf = shell side friction factor, figure 12.30 = 6 x 10-2

    Neglect viscosity correction

    [ ]

    5.4 MECHANICAL DESIGN FOR HEAT EXCHANGER

    In the mechanical design for heat exchanger subject to internal pressure, several steps

    need to be taken into consideration, the steps involve are:

    1. Design pressure and design temperatures

    2. Material of construction

    3. Design stress

    4. Wall thicknesses

    5. Head and closure thickness

    6. Channel cover thickness

    7. Dead weight load

    8. Vessel support

    9. Nozzle diameter

    10. Baffle heat exchanger

    5.4.1 Design pressure and temperature

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    For vessel under internal pressure, the design pressure is taken as the pressure at

    which 5 to 10% above the normal operating pressure in order to prevent from spurious

    operation of relief valve during minor upsets.

    The strengths of materials decrease with increasing temperature, thus themaximum allowable stress will depend on the material of construction. Under the ASME

    BPV Code, the maximum working temperature at which the maximum allowable stress

    is evaluated should be taken as the maximum working temperature. Take a safety

    factor as 10%.

    For tube side,

    Operating temperature : 30 C

    Design temperature : 30 x 1.1 = 33 C

    For shell side

    Operating temperature : 119.5 C

    Design temperature : 119.5 x 1.1 = 131.45 C

    Table 5.10: Design pressure and temperature for heat exchanger

    Operating Design

    Shell side Tube side Shell side Tube side

    Temperature , C 119.5 35 131.45 38.5

    Take design pressure of 3 bars for both shell and tube heat exchanger because of for

    safety reason and leakage inspection purpose (BASF).

    5.4.2 Material of construction

    Selection of suitable material must take into account the suitability of the material for

    fabrication as well as compatibility of the material with the process environment. A few

    factors that should be considered while choosing the material of construction are:

    Corrosion Resistance

    Operating conditions

    Economic feasibility

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    Suitability for fabrication

    Process safety

    Table 5.11: Material of construction

    Material Advantage Disadvantage

    Carbon Steel Low cost, easy to fabricate, abundant,most common material. Resists mostalkaline environments well.

    Very poor resistance to acids andstronger alkaline streams. Morebrittle than other materials,especially at low temperatures.

    Stainless Steel Relatively low cost, still easy tofabricate. Resist a wider variety ofenvironments than carbon steel.

    Available is many different types.

    No resistance to chlorides andresistance decreases significantlyat higher temperatures.

    254 SMO (Avesta) Moderate cost, still easy to fabricate.Resistance is better over a widerrange of concentrations andtemperatures compared to stainlesssteel.

    Little resistance to chlorides andresistance at higher temperaturescould be improved.

    Titanium Very good resistance to chlorides(widely used in seawaterapplications). Strength allows it to befabricated at smaller thicknesses.

    While the material is moderatelyexpensive, fabrication is difficult.Much of cost will be in weldinglabor.

    Pd stabilizedTitanium

    Superior resistance to chlorides, evenat higher temperatures. Is often usedon sea water application whereTitanium's resistance may not beacceptable.

    Very expensive material andfabrication is again difficult andexpensive.

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    (Source: http://www.cheresources.com/exprules.shtml)

    Vessel and pipes should be made of stainless steel or aluminium. Although 2-ethylhexyl

    acrylate does not corrode carbon steel, there is a risk of contamination if corrosion does

    occur (http://www2.basf.us).

    Table 5.12: Types and characteristics of stainless steel

    Type Characteristics

    304(18/8) Generally used.

    Contains minimum Cr and Ni that give Stable

    austenitic structure.

    Carbon content is low enough for heat treatment

    not to be normally needed with thin sections to

    prevent weld decay.

    304L low carbon version of type 304(

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    sulfuric acid.

    From criteria selection above, it can be concluded that Stainless Steel 316 is the

    best material to be used in designing heat exchanger. Weld decay is the intergranular

    corrosion in chemical plant. This is caused by the precipitation of chromium carbides at

    the grain boundaries in a zone adjacent to the weld. Weld decay can be avoided by

    using low carbon grades (

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    Inner pressure, Pi= 0.3 N/mm2

    Allowable stress, S = 137.6891 N/mm2

    Inner diameter, Di= 15.75 mm

    Joint efficiency, E = 0.85

    0.02 mmCorrosion allowance = 3mmMinimum thickness, t = 3.02 mm, 4.22 mm has chosen as tube thickness (Standard

    size).

    5.4.4.2 Minimum thickness of shell wall

    Where

    Inner pressure, Pi= 0.3 N/mm2

    Allowable stress, S = 112.3163 N/mm2

    Nominal shell diameter, Ds= 444 mm

    Joint efficiency, E = 0.85

    0.7 mmCorrosion allowance = 4mm

    Minimum thickness, t = 4.7 mm, minimum thickness of 5 mm is chosen (Sinnot, 1999).

    5.4.5 Head and closure thickness

    Table 5.13: Choice of closure

    Flat plates and formed

    head

    Cover for manways

    Channel cover for heat exchanger

    Cheapest type

    Limited to low pressure and small- diameter

    vessel

    Torispherical head Most commonly used

    For vessel up to operating pressure of 15 bar

    Ellipsoidal head Most economical closure for pressure above 15

    bar

    Hemispherical head The strongest shape

    For high pressure

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    Price higher than Torispherical head

    From Table 5.13 types of closures, by conducting the process condition and diameter of

    vessel, the most suitable head of closure are Torispherical head.

    5.4.5.1 Torispherical head

    t uat

    Rc= crown radius = 444 mm

    Inner pressure, Pi= 0.3 N/mm2

    Allowable stress, S = 112.3163 N/mm2

    Joint efficiency, E = 0.85

    5.4.6 Channel cover thickness

    Flat plates are used as the closure of heat exchangers. The minimum thickness of the

    channel cover required is calculated as follows:

    t e

    uatBolted cover with a full face gasket, take Cp = 0.4 and D equal to the bolt circle

    diameter. De = Ds

    t

    t= 9.1787mm + 4 mm = 13.1787mm

    5.4.7 Dead weight load

    5.4.7.1 Weight of vessel

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    The calculations weight of a cylindrical vessel with domed ends, and uniform wall

    thickness, can be estimated from the following equation:

    v vmmv mt

    uatWv= total weight of shell

    Cv= 1.08 for vessel with few internal fittings

    Hv= length of cylindrical section = 4.2672m

    g = 9.81m/s2

    t = wall thickness, mm = 5 mm

    Dm= mean diameter = (Ds+ t x 10-3), m = (444 + 5) x 10-3= 0.449 m

    m= density of vessel material, kg/m3

    , stainless steel = 8300 kg/m3

    v ( )

    5.4.7.2 Weight of tubes

    t t( )m uatNt= number of tubes = 190

    Do= outer diameter = 0.01950 m

    Di= inner diameter = 0.01575 m

    m= density of material = 8300 kg/m3

    t

    (

    )

    5.4.7.3 Weight of insulation

    Mineral wool density = 130 kg/m3

    Thickness of insulation = 75 mm

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    Density of insulation = 130 x 2 = 260 kg/m3

    Approximate volume of insulation

    te

    uat

    uat

    V = 0.45 m3

    W = Vg

    W = (130) (9.81) (0.45)

    W = 573.8850 N

    Total weight = vessel weight + tube weight + insulation weight

    Total Weight = + + 573.8850 = 29015.44 N = 27.26 kN

    5.4.8 Vessel support

    The support vessel will depend on the size, shape and weight of the vessel; the design

    temperature and pressure; the vessel location and arrangement and the external and

    internal fittings and attachments. Horizontal vessel normally mounted on two saddle

    support.

    Saddles must be designed to withstand the load impose by the weight of the vessel and

    contents. The dimension of typical standard saddle designed are given in table

    Table 5.14: Standard steel saddles (adapted from Bhattacharyya, 1976)

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    (Sinnot, 1999)

    Table 5.15: Saddle support for heat exchanger

    Vesseldiameter

    m

    Weight

    kN

    Dimension , m mm

    V Y C E J G t2 t1 boltdiameter

    boltholes

    0.45 m 27.26 0.37 0.11 0.42 0.18 0.15 0.07 4.6 3.9 15.43 19.29(Sinnot, 1999)

    Figure 5.3: The diagram for saddle support and its dimensions (Sinnot, 1999).

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    5.4.9 Nozzle diameter

    Designing tube side and shell side nozzles heat exchanger is based on TEMA heat

    exchanger standard.

    For carbon steel : Dopt= 293G0.52-0.37 Equation 5.33

    For stainless steel : Dopt= 260G0.52-0.37 Equation 5.34

    Figure 5.4: Typical standard flange design, (BS 4504) (All dimensions mm)

    (Sinnot, 1999)

    5.4.9.1 Tube side nozzle

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    Pipe size at inlet:

    Material of construction : Stainless steel

    Flow rate : 13.7 kg/s

    Density : 1007 kg/m3

    Optimum duct diameter : 260G0.52-0. 37

    : 78.5 mm

    The nearest value for optimum duct diameter is nominal pipe 80mm:

    Pipe size at outlet:

    Material of construction : Stainless steel

    Flow rate : 13.7 kg/s

    Density : 995.9 kg/m3

    Optimum duct diameter : 260G0.52-0. 37

    : 78.84 mm

    The nearest value for optimum duct diameter is nominal pipe 80mm

    5.4.9.2 Shell side nozzle

    Pipe size at inlet:

    Material of construction : Stainless steel

    Flow rate : 3.453 kg/s

    Density : 792.7 kg/m3

    Optimum duct diameter : 260G0.52-0. 37

    : 41.895 mm

    The nearest value for optimum duct diameter is nominal pipe 50 mm

    Pipe size at outlet:

    Material of construction : Stainless steel

    Flow rate : 3.453 kg/s

    Density : 871.4 kg/m3

    Optimum duct diameter : 260G0.52-0. 37

    : 40.45 mm

    The nearest value for optimum duct diameter is nominal pipe 50 mm

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    5.4.10 Baffle heat exchanger

    From chemical design calculation:

    Tube outside diameter , Dto : 0.01905m

    Pitch, Pt : 0.02375m

    Number of tubes : 190

    Bundle diameter, Db : 0.386m

    Shell inside diameter, Ds : 0.444m

    Baffle spacing, Ib : 0.222m

    HC= baffle cut height = Dsx Bc, where Bcis the baffle cut as a fraction, Bc= 0.25

    Hb, = height from the baffle chord to the top of the tube bundle,

    Bb= "bundle cut" = Hb/Db,

    b = angle subtended by the baffle chord, rads,

    Db= bundle diameter.

    Height from the baffle chord to the top of the tube bundle

    uat

    mBundle cut

    uat

    m

    From Figure 5.5, Ra (ratio of the bundle cross-sectional area in the window zone to thetotal bundle cross-sectional area) = 0.15 and b (angle subtended by the baffle chord)

    1.9 rad = 108.86.

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    Figure 5.5: Baffle geometry factor (Sinnot, 1999)

    Number of tubes in window zone Nw= Ntx Ra Equation 5.37

    Nw= 190 x 0.15 = 28.5 = 29 tubes

    For equilateral triangular pitch, pt= 0.87pt

    Pt= 0.87(0.02375) = 0.02066m

    Number of tube rows in window zone, Nwv

    wv pt uat

    Nwv= 3.97 = 4 rows

    Number of tubes in cross flow zone, Nc= Nt2Nw Equation 5.39

    Nc= 132 tubes

    Ratio number of tubes in window zone to total number, Rw

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    w wt

    uatRw= 0.3

    Window zone area: Aw

    w

    a wt

    uat

    w

    Aw= 0.015m

    2

    Number of tube rows in cross flow zone area: Ncv

    b Hb

    t

    Ncv= 10.74 = 11 rows

    Baffle cut height, Hc

    Hc= Dsx Bc Equation 5.43

    Hc= 0.444 x 0.25 = 0.111 m

    Assume tube to baffle clearance, Ct= 0.8 mm and baffle to shell clearance, Cs= 1.6mm

    Tube to baffle clearance area, Atb

    Atb= 0.00385 m

    2

    Baffle to shell clearance area, Abs

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    Abs= 0.00156m2

    Baffle cut area, Ab= Ib(DsDb)

    Ab= 0.222(0.4440.386) = 0.0129 m2

    Figure 5.6: Baffle and tube geometry (Sinnot,1999).

    Bundle diameter, Db : 0.386m

    Shell inside diameter, Ds : 0.444m

    Hc = 0.111 m

    b= 108.86

    5.4.11 Summary of mechanical design

    Table 5.16: Mechanical design sheet for heat exchanger

    Heat Exchanger Specification SheetEquipment No

    Description Heat ExchangeDesigned by : Abdul JalilSheet No 1/1

    OPERATING DATASize (m) Type Shell and tube No of Units 1

    Shells per unit 1 HORIZONTAL CONNECTED IN (parallel/series) Parallel

    Surface per Unit 1 Surface per shell 1 No of passes 2

    PERFORMANCE OF ONE UNIT

    SHELL SIDE TUBE SIDE

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    Fluid circulating Stream 25stream 26 Chilled water

    Total fluid entering IN OUT IN OUT

    Vapor (kg/h) n/a n/a n/a n/a

    Liquid (kg/h) 12430 12430 49320 49320

    Density (kg/m3) 833.55 1001.45

    Viscosity liquid (cP) 0.8565 0.7719

    Specific Heat (kJ/kg K) 2.447 4.0415

    Thermal conductivity (W/mK) 0.1253 0.6213

    Temperature (C) 119.7 30 20 35

    Pressure (kPa) 121 489

    Velocity (m/s) 0.72 0.21

    No of passes 1 2

    Fouling resistance (W/m2C) 784.48 3335.296

    Pressure drop, kPa 5.4 8.4

    Heat exchange (kJ/hr) 2.989 x 106

    Material Stainless steel 316

    Insulation Mineral wool 75mm

    Design Pressure (N/mm2) 0.3 0.3

    Design Temperature (C) 131.45 38.5O.D (mm) 449 19.05

    I.D (mm) 444 14.83

    Minimum thickness (mm) 5 4.22

    Length (m) 4.2672

    Pitch (mm) 23.81

    Vessel cover Torispherical head, 5.2393 mm

    Channel cover thickness, mm 13.1787

    Dead weight of vessel (N) 2869.3284

    Weight of tube (N) 23817

    Weight of insulation (N) 573.8850

    Weight of heat exchanger(kN) 27.26No of baffles 18

    Baffle cut 25%

    REFERENCES

    Branan, C. 2002. Rules of Thumb for Chemical Engineer.USA: Elsevier.

    Christie, J. G. 1993. Transport Process and Unit Operations.New York: Prentice Hall.

    Don, W. G. and Perry, R. H. 1997. Perrys Chemical Engineers Handbook . US:

    McGrawHill

    Incropera & Dewitt. 2007. Fundamental of Heat and Mass Transfer. US: McGrawHill

    Publication.

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    Sinnot, R. K. 1999. Chemical Engineering Design. Great Britain: Butterworth

    Heinemann.

    Thakore, S. B. and Bhatt, B. I. 2007. Introduction to Process Engineering and Design.

    India: McGrawHill Publication.

    APPENDIX E

    Table E1: Typical overall coefficient

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    Table E2: Fouling factors (coefficients), typical values

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    Figure E1: Temperature correction factor: one shell pass; two or more even tubepasses

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    Table E3: Conductivity of metals

    Figure E2: Tube-side heat-transfer factor

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    Figure E3: Shell-side heat-transfer factors, segmental baffles