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CMP for TSV’s Robert L. Rhoades, Ph.D. Presentation for AVS Joint Meeting June 2011

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Page 1: CMP for TSV’scmpconsulting.org/wa_files/2011_6rhoades.pdf• TSV’s can be filled with any of several conductive materials. –Most common options are copper and polysilicon. –Final

CMP for TSV’s

Robert L. Rhoades, Ph.D.

Presentation for AVS Joint Meeting

June 2011

Page 2: CMP for TSV’scmpconsulting.org/wa_files/2011_6rhoades.pdf• TSV’s can be filled with any of several conductive materials. –Most common options are copper and polysilicon. –Final

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Background

TSV Technology and Market Dynamics

CMP Processing for TSV’s (Examples)

Challenges and Issues

Summary

Outline

Page 3: CMP for TSV’scmpconsulting.org/wa_files/2011_6rhoades.pdf• TSV’s can be filled with any of several conductive materials. –Most common options are copper and polysilicon. –Final

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Background

• Two-dimensional device scaling is increasingly difficult and fast

approaching fundamental limits of physics.

• 3D integration also faces substantial process and design issues, but

various approaches are now gaining traction as viable paths to

achieve many of the same performance improvements previously

pursued mostly through device shrinks.

• Timing for mainstream adoption of 3D is now. Several memory

intensive applications have already been on the market for a few

years, a few MEMS-based modules are also available, and stacked

logic+memory modules are being launched.

• One of the key technologies to enable 3D structures is TSV’s.

Page 4: CMP for TSV’scmpconsulting.org/wa_files/2011_6rhoades.pdf• TSV’s can be filled with any of several conductive materials. –Most common options are copper and polysilicon. –Final

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CMP Applications

CMOS New Apps Substrate/Epi

Glass (oxide) Doped Oxides GaAs

Tungsten Nitrides GaN

Copper NiFe & NiFeCo InP

Shallow Trench Noble Metals CdTe & HgCdTe

Polysilicon Al & Stainless Ge and SiGe

Low k Polymers SiC

Cap Ultra Low k Ultra Thin Wafers Diamond & DLC

Metal Gates Direct Wafer Bond Si & Reclaim

Gate Insulators Through Si Vias SOI

High k Dielectrics 3-D Packaging Quartz

Ir & Pt Electrodes MEMS Titanium

Magnetics Nanodevices

Integrated Optics

2009 - Qty ≥ 36

As CMP applications continue to multiply …

optimized consumables, processes and

methods must be developed with lowest

possible risk and cost

1995 - Qty ≤ 2

CMOS

Glass (oxide)

Tungsten

2001 - Qty ≤ 5

CMOS

Glass (oxide)

Tungsten

Copper

Shallow Trench

Polysilicon

Page 5: CMP for TSV’scmpconsulting.org/wa_files/2011_6rhoades.pdf• TSV’s can be filled with any of several conductive materials. –Most common options are copper and polysilicon. –Final

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3D Packaging Apps

Source: Yole Development 2007

Page 6: CMP for TSV’scmpconsulting.org/wa_files/2011_6rhoades.pdf• TSV’s can be filled with any of several conductive materials. –Most common options are copper and polysilicon. –Final

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3D Scenerios

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Page 7: CMP for TSV’scmpconsulting.org/wa_files/2011_6rhoades.pdf• TSV’s can be filled with any of several conductive materials. –Most common options are copper and polysilicon. –Final

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Market Trend

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Source: TechSearch International

Page 8: CMP for TSV’scmpconsulting.org/wa_files/2011_6rhoades.pdf• TSV’s can be filled with any of several conductive materials. –Most common options are copper and polysilicon. –Final

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Role of CMP

• CMP is used in a damascene architecture to fabricate at least one side,

often both sides, of most TSV’s

• TSV’s can be filled with any of several conductive materials.

– Most common options are copper and polysilicon.

– Final choice depends on dimensions, operating voltage and current,

frequency, plus other integration factors.

• Vias can be completely filled or left partially hollow

– Post-CMP cleaning is a major concern with hollow vias

Page 9: CMP for TSV’scmpconsulting.org/wa_files/2011_6rhoades.pdf• TSV’s can be filled with any of several conductive materials. –Most common options are copper and polysilicon. –Final

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Typical TSV Flow

Wafer Grind

Etch

(optional)

CMP

Stack

Grind

Thickness

Etch

Thickness

Polish

Thickness

SPC

Thickness

Control

Surface and

Topography

Parameters

Pattern/etch/fill

(front side)

Part of device

fabrication

Page 10: CMP for TSV’scmpconsulting.org/wa_files/2011_6rhoades.pdf• TSV’s can be filled with any of several conductive materials. –Most common options are copper and polysilicon. –Final

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TSV Fill Materials

TSV Fill

Material

Deposition

Thickness

Demonstrated CMP

Polish Rate

Dishing / Recess

(Angstroms)

Copper 5 kA – 60 µm 1 kA/min – 8 µm/min 10 A – 0.3 µm

Polysilicon 4 kA – 30 kA 2 kA/min – 15 kA/min 300 – 1200 Ang

Tungsten 3 kA – 9 kA 3 kA;/min – 8 kA/min 150 – 300 Ang

NiFe or NiFeCo 1.5 µm – 8 µm 3 kA/min – 7 kA/min 600 – 4000 Ang

Pt 1.5 µm – 5 µm 1.5 kA/min – 5 kA/min 100 – 800 Ang

Page 11: CMP for TSV’scmpconsulting.org/wa_files/2011_6rhoades.pdf• TSV’s can be filled with any of several conductive materials. –Most common options are copper and polysilicon. –Final

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Copper Vias

Source: IBM

• The most common via fill material

• Typical via sizes 5–100 µm and plating

thicknesses 3–40 um

• Cu recess below 0.4 um achieved for

multiple trials

• Leverages CMOS interconnect

technology (somewhat) but requires

substantial reoptimization

Flat across

Feature

2nd Example: Cu (stop on TEOS)

• Intended integration = Direct Wafer Bonding

• Goal of <200 A total topography

POST-CMP TOPOGRAPHY ACHIEVED

70-90 Angstroms

Page 12: CMP for TSV’scmpconsulting.org/wa_files/2011_6rhoades.pdf• TSV’s can be filled with any of several conductive materials. –Most common options are copper and polysilicon. –Final

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Tungsten Vias

• Technology adapted from proven CMOS device integrations

• Typical via sizes are sub-micron but vias can be ganged in parallel for higher current

• Small via size required to avoid thick depositions of CVD tungsten (typically high tensile stress)

• TSV thickness also limited by aspect ratio

Edge

Center

Page 13: CMP for TSV’scmpconsulting.org/wa_files/2011_6rhoades.pdf• TSV’s can be filled with any of several conductive materials. –Most common options are copper and polysilicon. –Final

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Pt Vias

• Some devices require high temperature processes,

such as annealing of piezoelectric layers

– RF switches, cantilever sensors, and acoustic transducers

• Fabricating TSV’s prior to MEMS (via-first approach)

requires materials that can withstand high annealing

temperatures needed for piezoelectric films (>600oC)

• Platinum is a potential candidate, but fabrication

techniques for Pt vias are not yet mature

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Page 14: CMP for TSV’scmpconsulting.org/wa_files/2011_6rhoades.pdf• TSV’s can be filled with any of several conductive materials. –Most common options are copper and polysilicon. –Final

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Process Flow (partial)

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+V+V

1.Etch vias

in SOI

substrate3-7 mm dia.

5 mm depth

2.Oxidize

silicon

(1 mm);

sputter

Ti/Pt seed (0.7 mm)

3.Deposit

resist

plating

template (3.5 mm)

4.Plate Pt

to fill vias;

remove

resist

5.CMP Pt

over-

burden,

stopping

on SiO2

6.Evaporate

electrodes,

spin coat

PZT (1mm),

anneal (700oC)

Page 15: CMP for TSV’scmpconsulting.org/wa_files/2011_6rhoades.pdf• TSV’s can be filled with any of several conductive materials. –Most common options are copper and polysilicon. –Final

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CMP Slurry Screening

• CMP screening experiments

to determine removal rates

• Process targets:

• Pt (RR > 2000 Ang/min)

• Ti (RR > 2000 Ang/min)

• SiO2 (High selectivity)

• Good surface quality

• Slurry C met required

performance and was used

for further work

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SlurryPt Rate

(A/min)

Ti Rate

(A/min)

Tox Rate

(A/min)

Selectivity

(Pt:Ti)

Selectivity

(Ti:Oxide)

A 12 8 <1 1.5 > 8

B 104 1461 195 0.1 7.5

C 2980 3955 132 0.8 30.0

D 436 2108 777 0.2 2.7

0

1000

2000

3000

4000

5000

Slu

rry A

Slu

rry B

Slu

rry C

Slu

rry D

Rem

oval R

ate

(A

ng

/min

)

Pt Rate Ti Rate Oxide Rate

Page 16: CMP for TSV’scmpconsulting.org/wa_files/2011_6rhoades.pdf• TSV’s can be filled with any of several conductive materials. –Most common options are copper and polysilicon. –Final

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Pt Vias

• Electroplated

Pt for via fill

• Tolerates high

temperatures

up to 700oC

16

Photoresist template

Pt plating overburden

Pt plating overburden

resist

etched viaPlated Pt

Ti/Pt seedSiO2

SiO2

Plated Pt

Ti

Silicon

Additional evap Ti

adhesion layer

Via top view (SEM)Via top view

Pt

TiSiO2

Pre-CMP

Post-CMP

Page 17: CMP for TSV’scmpconsulting.org/wa_files/2011_6rhoades.pdf• TSV’s can be filled with any of several conductive materials. –Most common options are copper and polysilicon. –Final

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TSV Improvements

Needed

• Design rule consistency / standardization

• Incoming variation at CMP

• Uniformity

• Selectivity control

• Plug recess/protrusion

• Throughput

• Repeatability

• Cost per unit operation (slurry, pad life, etc.)

Page 18: CMP for TSV’scmpconsulting.org/wa_files/2011_6rhoades.pdf• TSV’s can be filled with any of several conductive materials. –Most common options are copper and polysilicon. –Final

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Design Rules

• Via size

– Determines etch aspect ratio and plating thickness

– Electrical requirements drive minimum size

• Via spacing / pattern density

– Wide variation causes CMP local uniformity issues

– High density of vias weakens mechanical strength

• Feature offsets and tolerances

– Direct impact on die-to-die or wfr-to-wfr alignments

• Via recess and allowed variation

– Design specs must be kept realistic with process capability

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Page 19: CMP for TSV’scmpconsulting.org/wa_files/2011_6rhoades.pdf• TSV’s can be filled with any of several conductive materials. –Most common options are copper and polysilicon. –Final

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Incoming Variation

• Plating thickness variation

– Especially for thicker depositions above 20um

• Etch depth variation

– Range of TSV exposure from opposite side

• TTV from grind or other thinning process

– Determines range of Si to be removed to expose

TSV’s and/or amount of protrusion after exposure

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Page 20: CMP for TSV’scmpconsulting.org/wa_files/2011_6rhoades.pdf• TSV’s can be filled with any of several conductive materials. –Most common options are copper and polysilicon. –Final

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CMP Variation

• Familiar Sources

– Slurry (pH, particles, etc.)

– Pads

– Conditioning disks

– Wear during pad life

– Test wafer vs product wafer

• Less obvious

– Contamination

– Distribution system

– Pumps & filters

– Slurry dispense location

– Source of H2O2

– Head rebuild technique

– DI water temperature

– Metrology instability (Are you

chasing a ghost?)

– Bake/anneal sensitivity

– Barrier metal grain structure

– Pattern density / layout

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Others?

Page 21: CMP for TSV’scmpconsulting.org/wa_files/2011_6rhoades.pdf• TSV’s can be filled with any of several conductive materials. –Most common options are copper and polysilicon. –Final

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CMP Uniformity

• Clearing behavior at CMP driven by 2 factors:

CMP uniformity and deposition uniformity

• TSV is not generally as sensitive as interconnect … but

– Effects are exaggerated with very thick depositions and long

polish times (compared to interconnect)

– Customers prefer older/cheaper equipment in packaging area

which may not have as much control as fab tools

• Selectivity can absorb some variation, but often not

sufficient to make the process robust

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Page 22: CMP for TSV’scmpconsulting.org/wa_files/2011_6rhoades.pdf• TSV’s can be filled with any of several conductive materials. –Most common options are copper and polysilicon. –Final

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Selectivity Control

• Integration determines what materials are being

polished and what are stop layers

– Barrier metal is not universal

– Stop layer options: Barrier, oxide, Si, other?

• Selectivity is mostly driven by the slurry

• Custom formulations can be finely optimized, but

tunability allows broader industry solutions

• Each change in integration can have a huge impact on

CMP constraints for selectivity

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Page 23: CMP for TSV’scmpconsulting.org/wa_files/2011_6rhoades.pdf• TSV’s can be filled with any of several conductive materials. –Most common options are copper and polysilicon. –Final

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Recess/Protrusion

• Factors that drive recess/protrusion

– Selectivity among exposed materials

– Material integrity of core portion of TSV

– Overpolish time required to clear all areas of wafer

• Balance is required

– Too much recess Open contacts

– Too much protrusion Mechanical stress or poor bonding

in some integrations (not as critical for solder bumps)

• Overly tight constraints can easily lead to excess

development costs and difficulty meeting timelines

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Page 24: CMP for TSV’scmpconsulting.org/wa_files/2011_6rhoades.pdf• TSV’s can be filled with any of several conductive materials. –Most common options are copper and polysilicon. –Final

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Throughput

• Most TSV processes involve very thick films

– Leads to long polish times at CMP

• Suppliers are focused on high rate Cu slurries

– First generation about 1-1.5 um/min

– Second generation claiming 3-4 um/min

– Via recess can be a challenge at very high rates

• Multi-wafer tools can be an advantage

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Page 25: CMP for TSV’scmpconsulting.org/wa_files/2011_6rhoades.pdf• TSV’s can be filled with any of several conductive materials. –Most common options are copper and polysilicon. –Final

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Repeatability

• Critical in HVM

– Often overlooked or downplayed in development

• High rate slurries tend to be more vulnerable to

contaminants, mix ratios, etc.

• Endpoint can help absorb variations, but has a

few quirks as well

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Page 26: CMP for TSV’scmpconsulting.org/wa_files/2011_6rhoades.pdf• TSV’s can be filled with any of several conductive materials. –Most common options are copper and polysilicon. –Final

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Cost Factors

• Development Cost Factors

– Materials choices and availability

– Number of design cycles

– Speed of implementation

• Manufacturing Cost Factors

– Direct Consumables: Pads, slurries, pad life, etc.

– Plating thickness

– Throughput (drives # of tools and capital cost)

– Yield and scrap rate

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Page 27: CMP for TSV’scmpconsulting.org/wa_files/2011_6rhoades.pdf• TSV’s can be filled with any of several conductive materials. –Most common options are copper and polysilicon. –Final

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Development Costs

• Classic engineering tradeoff:

Speed, Low Cost, or Quality

(choose 2)

• Short product life means shorter

timeline for next gen

• Development $$ have to be

amortized over product life

Actions being taken by manufacturers to control development costs:

Extreme prioritization and minimize cycles of learning

Push early screening and optimization down to suppliers

Outsource non-critical functions or bring in outside resources

Alliances and consortia to share next gen development costs

Page 28: CMP for TSV’scmpconsulting.org/wa_files/2011_6rhoades.pdf• TSV’s can be filled with any of several conductive materials. –Most common options are copper and polysilicon. –Final

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Summary

• Through Silicon Via Technology (TSV)

– Enabling many 3D integrations and growing rapidly

– Most TSV flows rely on CMP at least once, often twice

• Areas Needing Improvement

– Design rule consistency / standardization

– Incoming variation at CMP

– Uniformity

– Selectivity control

– Plug recess/protrusion

– Throughput

– Repeatability

– Cost per unit operation (slurry, pad life, etc.)

Page 29: CMP for TSV’scmpconsulting.org/wa_files/2011_6rhoades.pdf• TSV’s can be filled with any of several conductive materials. –Most common options are copper and polysilicon. –Final

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THANK YOU !

• Many thanks to the following:

– Dorota Temple and Dean Malta of RTI, Inc. for Pt data

– Other customers who gave permission to use images and data

– Terry Pfau, Paul Lenkersdorfer, & Donna Grannis of Entrepix

• For additional information, please contact:

Robert L. Rhoades, Ph.D.

Entrepix, Inc.

Chief Technology Officer

+1.602.426.8668

[email protected]

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