column tray and packing design - university of oklahoma 1-2013/column... · 2013-10-03 · che 4253...
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DISTILLATION/ABSORPTION COLUMN TRAY DESIGN
ChE 4253 - Design IChE 4253 - Design I
Trays types
Sieve Valve Bubble cap
Enhance Deck (Sulzer)
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DISTILLATION/ABSORPTION COLUMN TRAY DESIGN
ChE 4253 - Design IChE 4253 - Design I
Operational limits for trays.
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DISTILLATION/ABSORPTION COLUMN TRAY DESIGN
ChE 4253 - Design IChE 4253 - Design I
Design Point
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DISTILLATION/ABSORPTION COLUMN TRAY DESIGN
ChE 4253 - Design IChE 4253 - Design I
Diameter first. Design for velocity. Flooding velocity given by (are you surprised?)
AN
Use ~80% of flooding velocity. Diameter is a function of the NET area AN
Fair correlation
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DISTILLATION/ABSORPTION COLUMN TRAY DESIGN
ChE 4253 - Design IChE 4253 - Design I
Tray Spacing: Large if froth is expected, also allow space for crawling (12” to 24”).
Downcomer area: Fluid velocity larger than ascending bubbles (minimum width: 5”) Range of velocities= 0.1-0.7 ft/sec. Residence time criteria (3-5 sec) . Downcomerflooding should be avoided.
Hole diameter: 3/16 to ¼ in.
Total Hole Area: Such that the velocity through the holes does not form jets)
Number of Holes: Hole area/Total hole area
Height of weir: Francis formula
Pressure drop: to be watched. Do not want it to be too large (5-10”). Typical value ~0.1 psi
Efficiency: Murphy & Point Efficiency. There are correlations. In the absence of data look for similar mixtures.
2
0.905( ) 0.785( )All holes
holes
A hole diameterK K equilateral triangular pitch K rectangular pitchA hole pitch
− ⎛ ⎞−= = =⎜ ⎟−⎝ ⎠
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DISTILLATION/ABSORPTION PACKED COLUMN DESIGN
ChE 4253 - Design IChE 4253 - Design I
Packed Towers
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DISTILLATION/ABSORPTION COLUMN TRAY DESIGN
ChE 4253 - Design IChE 4253 - Design I
Random Packing
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DISTILLATION/ABSORPTION COLUMN TRAY DESIGN
ChE 4253 - Design IChE 4253 - Design I
Structured Packing Flexipack (Koch)
Sulzer
Ceramic
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DISTILLATION/ABSORPTION COLUMN TRAY DESIGN
ChE 4253 - Design IChE 4253 - Design I
Packing Height: Number of equilibrium stages x HETP (Height Equivalent to a Theoretical Plate)
HETP: Typically a function of gas rate (ft/sec) and the packing, as well as the mixture.
Packing Diameter: Similar graph to Fair’s graph