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Cristalografia de raios-X

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Cristalografia de raios-X

Como obter “bons” cristais?

Page 5: Cristalografia de raios-X - Unicampleandro.iqm.unicamp.br/leandro/shtml/didatico/qg107/cristalizacao.pdf · The green solution was kept at room temperature for three days to get crystals

Con

cent

raçã

o da

esp

écie

inte

ress

Agente precipitante

CossolventeTemperatura

Precipitação

Solução

Nucleação

Page 6: Cristalografia de raios-X - Unicampleandro.iqm.unicamp.br/leandro/shtml/didatico/qg107/cristalizacao.pdf · The green solution was kept at room temperature for three days to get crystals

Page 7: Cristalografia de raios-X - Unicampleandro.iqm.unicamp.br/leandro/shtml/didatico/qg107/cristalizacao.pdf · The green solution was kept at room temperature for three days to get crystals

The green solution was kept at room temperature for three days to get crystals.

Physica B: Condensed Matter

Volume 407, Issue 21, 1 November 2012, Pages 4208–4213

http://www.sciencedirect.com/science/journal/09214526

http://www.sciencedirect.com/science/journal/09214526/407/21

Page 8: Cristalografia de raios-X - Unicampleandro.iqm.unicamp.br/leandro/shtml/didatico/qg107/cristalizacao.pdf · The green solution was kept at room temperature for three days to get crystals

Materiais:

Ferrioxalato de potássioÁgua, EtanolTubos de ensaioAquecimento/resfriamento

Objetivo:

Obter os melhores cristais.

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