NAME

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MOHAMM

05th Septem

Agra, U.P

Indian

Professor

Department

Aligarh Mu

Aligarh-202

Street No. 6

School, New

+91-571-27

+91-983743

+91-571-27

shakir078@

1977

1979

1981

1983

Vitae

MAD SHAK

mber 1957

t of Chemist

uslim Univer

2002 (India)

6, Iqra Colon

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70315 (Off.)

30035 (Mob

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EMPLOYMENT HISTORY-TOTAL UNIVERSITY SERVICE:

2010-Contd. Professor Aligarh Muslim University, Aligarh

2007-2010 Professor King Khalid University, Abha (KSA)

2001-2007 Professor Aligarh Muslim University, Aligarh

1999-2001 Reader Aligarh Muslim University, Aligarh

1997-1999 Professor Addis Ababa University, (UNDP Program)

1993-1997 Reader Aligarh Muslim University, Aligarh.

1988-1993 Senior Lecturer Aligarh Muslim University, Aligarh

1983-1988 Lecturer Aligarh Muslim University, Aligarh

TEACHING EXPERIENCE:

31 years experience at under-graduate (UG) and post- graduate (PG) levels. Taught

Courses of Inorganic Chemistry including Organometalic Chemistry, Spectroscopic

Techniques for structural elucidation of Inorganic compounds, Inorganic reaction

mechanism, photo inorganic Chemistry etc. both at national and international levels.

AREA OF RESEARCH INTEREST:

Synthesis and characterization and applications of multi-dentate macrocyclic ligands and

their mononuclear, binuclear and bis-macrocyclic complexes with variety of transition

metals and non- metals.

Non-aqueous solution chemistry-synthetic applications of chlorosulphonic acid solvent

system: Synthesis and characterization of novel mono-, bis-, tris and tetrakis- metal and

non-metal chlorosulphates and stabilization of illusive partially charged cationic species.

Architecture, synthesis, characterization and applications of supramolecular structures

through self-assembly processes.

Design, synthesis and physico-chemical studies and DNA binding and anti-microbial

applications on novel Schiff base ligands and their transition metal complexes.

Synthesis and characterization of novel metal organic framework and their physic-

chemical studies.

Synthesis, characterization, application of novel Nanomaterials and Nanocomposites.

STUDY/FOREIGN VISITS:

Visited Ain Shams University, Cairo (Egypt) during 1992.

Visiting Scientist, Institute fur Anorganische Chemie der Universitat, Gottingen (FRG)

under (DAAD) May-July, 1993

Visited, Institute fur Anorganische Chemie, RWTH Aachen university of Technology

(FRG) during 1997.

Visiting scientist, Anorganische Chemie, Universat des Sarlandes, Saarbrucken (FRG)

under Deutscher Academischer Austauschdienst (DAAD) July-Sept. 1998.

Visiting Professor, Materials Science, Toyohashi University of technology Toyohashi,

(JAPAN) Sponsored by Daiko foundation, June-Nov, 2000.

Visiting Professor, Chemistry Department, King Saud University, Riyadh, K.S.A., June

3-10, 2011.

Visiting Professor, Chemistry Department, College of Science, King Saud University,

Riyadh, K.S.A., February 15-23, 2013.

Visiting Professor under Visiting Professor Program to Chemistry Department, College

of Science, King Saud University, K.S.A. during June 2013-May 2014.

Visited Las Vegas and New York, U.S.A. during October, 5-13, 2013.

ADMINISTRATIVE RESPONSIBILITIES AT THE UNIVERSITY LEVEL

Chairman, Department of Chemistry, A.M.U., Aligarh- 17.05.2014-03.08.2014.

Coordinator, Centre of Professional Courses, A.M.U., Aligarh since 2011-Contd.

(Running 28 Post-Graduate Diploma Courses, Diploma and Certificate Courses in

Paramedical Sciences, Commerce, Fine Arts, Agriculture, Applied Science, Computer,

Food Technology etc.).

Provost of Hall of Residence having 750 student resident members and 70 non-teaching

staff from Feb.2011 - Jun.2012, Aligarh Muslim University, Aligarh.

Pro-proctor for number of years to manage the law and order situation on the campus.

Warden In-charge in the corporate life of university to facilitate the library, food and

sports amenities to the students for 6 years.

ACADEMIC RESPONSIBILITIES EXECUTED:

Organizing secretary, National Conference held in Department of Chemistry, A.M.U.

Aligarh during 2-3 march, 2012.

Joint organizing secretary, International Conference held in the Department of

Chemistry, A.M.U. Aligarh during 5-6 march 2011.

Promoted scientific education to school and college teachers through various training

programs conducted by center of promotion of Science A.M.U. Aligarh and NGOs.

Reviewer to a number of national and international journals especially of Pergamon

Elsevier and Royal Chemical Society, Taylor Francis, A.C.S etc.

Organized and delivered lectures in number of refresher courses and orientation programs

conducted by Academic Staff College, A.M.U. Aligarh.

Expert Member in Selection Boards for different universities and other National Bodies

like UPSC, JPSC, NCERT, PSC, MHRD (Commonwealth) etc.

Member of NAAC committee of A.M.U. Aligarh.

MEMBERSHIP OF UNIVERSITY BODIES:

Member of Indian council of chemists.

Member of Indian science congress.

Life Member of Indian national science academy.

Member of number of committees at university level such as syllabus revision,

infrastructure development, instrumentation etc.

Member of Executive Committee of AMUTA, 1989-1991.

Member of Academic council, A.M.U, Aligarh, 2007-2010.

Member of Committee of Faculty of Science for three terms of two years each.

Member of A.M.U, Court, 2011-2012.

Member of Academic council, A.M.U, Aligarh during 2013-2016

RESEARCH PROJECTS:

Completed three major research projects (2-CSIR and 1-UGC) as Principal Investigator.

Co-I investigator in one research project funded by KACST, Saudi Arabia 2009-2010.

SCHOLARSHIPS AND FELLOWSHIPS:

Post-Graduate merit Scholarship, faculty of science, A.M.U, Aligarh (1977-1979).

Junior research fellowship, council of scientific and industrial research (CSIR) New

Delhi, 1980-1982.

Senior research fellowship, council of scientific and industrial research (CSIR) New

Delhi, 1982-1983.

RESEARCH ACHEIVEMENTS:

Two students received young scientist under DST fast track scheme.

h-index-20, and 1205 citations for 107 publications (Thomson Reuters)

h-index-18, i-10 index 32 and 993 citations (Google Scholar)

A number of our publications have been selected amongst top 20 articles by www.

Biomed Lib.Com website dealing with “who is publishing in my Domain”.

a) RESEARCH PAPERS PUBLISHED:

Number of research publications in Journals of international repute : 112

b) RESEARCH SUPERVISION:

Ph.D. Thesis supervised: 16

M.Phil Dissertations Supervised: 05

M.Tech and M.Sc. Dissertations Supervised: 03

c) CONFERENCES ATTENTED:

International: 05

National: 08

d) BOOKS WRITTEN:

The chemistry of synthetic zeolites (Published by AMU Division), 2003.

Fundamental of Organometalic chemistry (introduction. Reactivity, structure,

bonding and applications, (under preparation).

RESEARCH PUBLICATIONS:

1. Electrical Conductivity, Isothermal Stability, and Ammonia-Sensing Performance of Newly Synthesized and Characterized Organic-Inorganic Polycarbazole−Titanium Dioxide Nanocomposite Mohammad Shakir, Noor-e-Iram, Mohd Shoeb Khan, Saud Ibrahim Al-Resayes, Asif Ali Khanand Umair Baig Ind. Eng. Chem. Res. 2014, 53, 8035−8044.

2. Synthesis, Spectroscopic characterization and in vitro antimicrobial studies of Schiff base ligand, H2L derived from glyoxalic acid and 1,8-diaminonaphthalene and its Co(II),Ni(II),Cu(II)andZn(II)complexes. S.I.Al-Resayes,M.Shakir,N.Shahid,M.Azam,A.U.Khan, Arabian Journal of Chemistry, DOI: 10.1016/j.arabjc.2011.11.004

3. Novel Pd(II)-Salen complexes showing high in vitro anti-proliferavative effects against human hepatoma cancer by modulating specific regulatory genes. Mohammad Azam, Z. Hussain, I. Ward, S. I. Al-Resayes, M. S. Khan, Mohammad Shakir, T-Kruszynska, R. Kruszynski Dalton Trans., 41, 2012, 10854-10864.

4. A novel Ru(II) complex derived from hydroxydiamine as a potential antitumor agent; synthesis and structural characterization. M. Azam, I. Ward, S. I. Al-Resayes, Mohammad Shakir, A. Ahmad, F. H Sarkar Inorg. Chem. Commun., 20, 2012, 252-258.

5. Synthesis, Physico-chemical studies and Antioxidant activities of Transition Metal Complexes with a permidine ligand. Mohammad Azam, I.Ward, S. I. Al-Resayes, M.Zahin, I.Ahmad, Mohammad Shakir, Z. Anorg. Allg. Chem., 638, 2012, 1-7.

6. Synthesis, Spectroscopic characterization and biological activities of N4O2 Schiff base ligand and its metal complexes of Co(II), Ni(II), Cu(II) and Zn(II). S. I. Al-Resayes, Mohammad Shakir, Ambreen Abbasi, Kr.M.Y.Amin, A.Lateef. Spectrochemica Acta 93, 2012, 86-94.

7. Synthesis, Spectroscopic characterization, DNA interaction and antibacterial study of metal complexes of tetraazamacrocyclic Schiff base. Mohammad Shakir, S.Khanam, F.Firdaus, A.Latif, M. Aatif, S. I. Al-Resayes. Spectrochemica Acta 93, 2012, 354-362

8. Template synthesis and spectroscopic characterization of Novel 16- membered [N]

Schiff base macrocyclic complexes of Co(II), Ni(II), Cu(II) and Zn(II). Mohammad Shakir, Sadiqa Khanam, Mohammad Azam, M.Aatif, Dr.Farha Firdaus. Journal of Coordination Chemistry, 64, 2011, 3158-3168.

9. Sphericals Nanoparticles (SNPs)NiO; Synthesis, characterization and optical properties. A.Kalam, A. S. Al-Shiri, M. Shakir, A. A. El. Bindary, El. Sayed S Yousef, G. Du. Synth. React. Inorg. Met-Org. nano-met.Chem., 41 2011, 1324-1330.

10. Synthesis, Spectroscopic characterization and in vitro anti microbial studies of Schiff base ligand, H2L derived from glyoxalic acid and 1,8- diaminonaphthalene and its Co(II), Ni(II), Cu(II) and Zn(II) complexes. S. I. Al-Resayes, Mohammad Shakir, N. Shahid, Mohammad Azam, A.U Khan. Arabian.J.Chem., Accepted 2011, Available online.

11. Synthesis, Spectroscopic characterization and In-vitro antimicrobial Screening of 16-Membered tetraazamacrocyclic Schiff base and its complexes with Co(II), Ni(II), Cu(II) and Zn(II) ions. Mohammad Shakir, Sadiqa Khanam, Mohammad Azam, A.U Khan, Farha Firdaus. Synth. React. Inorg.Met.-org. nano-met. Chem., 41, 2011, 979-986.

12. Template synthesis and physic chemical studies of 14- membered functionalized pendant arm Schiff base Macrocyclic Complexes of Co(II), Ni(II), Cu(II) and Zn(II); DNA binding studies on Co(II) complexes. Mohammad Shakir, Mohammad Azam, Sultana Naseem, Asad U.Khan. Synth. React. Inorg.Met.-org. nano-met. Chem., 41, 2011, 1056-1062.

13. Synthesis, Spectroscopic characterization and comparative DNA binding studies of Schiff base complexes derived from 1- leucine and glyoxal. Mohammad Shakir, Nida Shahid, Naushaba Sami, Mohammad Azam and Asad U.Khan. Spectrochemica Acta Part A, 82, 2011, 31-36.

14. Synthesis, Spectroscopic and electrochemical studies of N, N-bis[(E)-2-thienylmethylidene]- 1,8- napthalenediamine and its Co(II) complexes; DNA Cleavage and generation of superoxide anion. Mohammad Shakir, Mohammad Azam, M. F. Ullah and S.M Hadi. Journal of Photochemistry and Photobiology B: Biology, 104, 2011, 449-456

15. Synthesis, Spectroscopic studies and crystal structure of the Schiff base ligand L derived from condensation of 2-thiophenecarboxaldehyde and 3,3- diaminobenzidene and its complexes with Co(II), Ni(II), Cu(II), Cd(II) and Hg(II). Comparative DNA binding studies of L and its Co (II), Ni (II) and Cu (II) complexes. Mohammad Shakir, Ambreen Abbasi, Mohammad Azam and Asad U.Khan. Spectrochemica Acta Part A, 79, 2011, 1866-1875.

16. Synthesis and Spectroscopic studies on Schiff base ligand derived from condensation of 2-furaldehyde and 3,3-diaminobenzidine, L and its complexes with Co(II) , Ni(II), Cu(II) and Zn(II): Comperative DNA binding studies of L and its complexes with Co(II), Ni(II), Cu(II) and Zn(II); Comperative DNA binding studies of L and its Cu(II) and Zn(II) co mplexes. M. Shakir ,A.Abbasi, A.U Khan. S.N Khan. Spectrochemica Acta Part A: 78, 2011, 2-35

17. Synthesis, physic-chemical and antimicrobial screening studies of Co(II), Ni(II), Cu(II) and Zn(II) with 18-membered schiff base octaazamacrocyclic ligand. Tahir Ali Kha, Siltana Naseem, Rafat Hajra and Mohammad Shakir. Synth.React.Inorg.Met.-org. nano-met. Chem., 40, 2010, 861-868.

18. Synthesis, Spectroscopic, thermal and antimicrobial studies of tetradentate 12 1nd 14-membered Schiff base ligands and theit compleses with Fe(II), Co(II), and Cu(II), Metal Ions. F.Firdaus, K.Fatma, M. Shakir. J.Coord.Chem., 63, 2010, 3956-3968.

19. Synthesis and Spectral characterization of 14 and 16-membered tetraazamacrocyclic Schiff base ligands and their transition metal complexes and a comperative study of interaction of calf thymus DNA with copper (II) complexes. T.A.Khan, S.Naseem, A.U .Khan, M. Shakir. Spectrochemica Acta Part A, 73, 2009, 622-629.

20. Metal ion controlled synthesis of 16 and 18-membered binuclear octaazamacrocyclic complexes with Co(II), Ni(II), Cu(II) and Zn(II) : A comperative spectroscopic approach to DNA binding to Co(II), complex. F.Firdaus, K.Fatma, A.U .Khan. M. Shakir. J. Serb.Chem. Soc., 74, 2009, 939-951.

21. Synthesis and Spectroscopic studies on complexes N,N-bis-(2-pyridinecarboxaldimine)-1,8-diaminonaphthalene(L): DNA binding studies on copper(II) complex.

Mohammad Shakir, Mohammad Azam, Shama Parveen, Asad Ullah Khan and F. Firdaus. Spectrochemica Acta Part A, 71, 2009, 1851-1856.

22. Template synthesis and physico-chemical characterization of 14- membered tetraimine macrocyclic complexes, [MLX2] [M= Co(II) , Ni(II), Cu(II) and Zn(II)]. DNA binding study on [CoLCl2] complex. F.Firdaus, K.Fatma, M. Azam, Shahper N.Khan, Asad U.Khan and M. Shakir. Spectrochemica Acta Part A, 72, 2009, 591-596.

23. Template synthesis and physico-chemical syudies of 14-membered hexaazamacrocyclic complexs with Co(II) , Ni(II), Cu(II) and Zn(II): A comperative spectroscopic approach of DNA binding with Cu(II) and Ni(II) complexes. F.Firdaus, K.Fatma, M. Azam, S. N.Khan, Asad U.Khan and M. Shakir. Transition Met.Chem, 33, 2008, 467-473.

24. Synthesis and Spectral studies of 12-membered tetraimine macrocyclic ligand and its complexes. Mohammad Shakir, Shakira Khatoon, Shama Parveen and Yasser Azim. Transition Met.Chem., 32, 2007, 42-46.

25. Metal-ion directed synthesis of binuclear octaazamacrocclic complexes of manganese (II), cobalt (II), nickel (II), copper (II), and zinc (II) and their physicochemical studies. T.A.Khan, Sultana Naseem, Yasser Azim, Shama Parveen and Mohammad Shakir. Trans. Met. Chem. 32, 2007, 706-710.

26. Synthesis and physico-chemical syudies on complexes of 1,2-diaminophenyl-N,N-bis-(2-pyridinecarboxaldimine),(L): A spectroscopic approach on binding of DNA with the copper complex. Mohammad Shakir, Mohammad Azam, Yasser Azim, Shama Parveen and A.U. Khan. Polyhedron, 26, 2007, 5513-5518.

27. Synthesis and characterization of complexes of Co(II) , Ni(II), Cu(II) and Zn(II) with 12 membered Schiff bases ucing powe ligands and the study of their antimicrobial and reducing power. M.Shakir, Y.Azim, H.T.N. Chishti and S.Parveen Spectrochemica Acta Part A., 2006, 65, 490-496.

28. Synthesis, physic-chemical and antimicrobial screening studies on 14 an 16 membered hexaazamacrocyclic complexes bearing pendant amine groups.

M.Shakir, Y.Azim, H.T.N. Chishti, N.Begum, P.Chingsubam and M.Y Siddiqui J.Braz.Chem. Soc., 25, 2006, 272-278.

29. Cation supported self- assembly of coordination polymers, [(H2en) (ntpMCl2)] n ( M =

Zn(II) , Cd(II) and Hg (II) involving tripodal acid, ntp. X-ray crystal structure and binding studies on zinc helicate. M.Shakir, S. Parveen, P. Chingsubam, Katsuyuki Aoki, S.N. Khan and A.U.Khan. Polyhedron 25, (2006), 2929-2934.

30. Metal ion-directed synthesis of 16- membered tetraazamacrocyclic complexes and their physico-chemical studies. M.Shakir, H.T.N Chishti and P. Chingsubam, Spectrochimica Acta A, (2005), 64, 512- 517.

31. Binuclear octaazamacrocyclic complexes of Co(II) , Ni(II), Cu(II) and Zn(II) derived from tris (aminoethyl) amine and 1,3 dibromopropane; synthesis and characterization. M.Shakir, P. Chingsubam, H.T.N Chishti. Polish J. Chem., (2005), 79, 1731-1738.

32. Synthesis and spectral studies on 16- membered diamidediimine tetrazamacrocyclic complexes of [ MLCl] Cl [ M= Mn (II), Fe(II), Co(II), Ni(II), Cu(II) and Zn(II)]. M. Shakir and S. Khatoon. Polish J. Chem., (2005), 79, 1627-1633.

33. Metal directed synthesis of Hexaazamacrocyclic complexes of Co(II) , Ni(II), Cu(II) and Zn(II) and their physic-chemical studies. M. Shakir, Y. Azim, H.T.N. Chishti and P. Chingsubam. Polish J. Chem., (2005), 79, 1115-1121.

34. Template Synthesis of 20-membered Decaazamacrocyclic complexes of Mn (II), Co(II) , Ni (II), Cu(II) and Zn(II) and their characterization. T.A. Khan, S. Tabassum, M. Shakir and S. Parveen. Synth.React.Inorg.Met.-org. nano-met. Chem., 2005, 35, 119-125.

35. Metal ion- directed synthesis of 12 and 14 membered tetraazamacrocyclic complexes and their physic-chemical studies. T.A. Khan , S.S. Ghani, M. Shakir and S. Tabassum Synth. React. Inorg. Met.-Org . Nano-met Chem. (2005), 35, 1-5

36. Synthesis and physico-chemical studies on 18-memebered octaazamacrocyclic complexes of Mn(II), Co(II) , Ni(II), Cu(II) and Zn(II) ions. T.A. Khan , Shabana tabassum , Yasser Azim and M. Shakir Synth. React. Inorg. Met.-Org . Nano-met Chem. 34, (2004), 1305-1318.

37. Mononuclear complexes of magnase (II), iron(II), cobalt(II), nickel(II), copper(II) and zinc(II) with 4-amino-3,5-bis(pyridin-2-yl)-1,2,4-triazole and tris (2- aminoethyl)amine:

crystal structure of [Ni(tren)(abpt)](NO3)2(H2O)2.25.

M. Shakir, S. Parveen, N. Begum and P. Chingsubam. Transition Met. Chem., (2004), 29, 196-199

38. Synthesis and physico-chemical studies on 20-membered decaazamacrocyclic complexes of Mn (II), Fe(II), Co(II), Ni(II), Cu(II), and Zn(II) derived from 1,6- diacetylpyridine dihydrazone. M. Shakir, P. Chingsubam, H. T. N. Chishti, Y. Azim and N. Begum Indian J. Chem., (2004), 43A, 556-561.

39. Synthesis and characterization of hexaazamacrocylic complexes with Co(II), Ni(II), Cu(II) and Zn(II) derived from pthalaldehyde and 2,6 diaminopyridine. M. Shakir, H. T. N. Chishti, Y. Azim, and N. Begum. Synth. React. Inorg. Met.-Org . Nano-met Chem. (2004), 809-818.

40. Interaction of manganese(II), iron(II), cobalt(II), nickel(II), copper(II) and zinc(II) with acetalhydrazine, formed in situ; first crystal structure of tris (acetalhydrazine) nickel(II) perchlorate. M. Shakir, S. Parbeen, N.Begum, Y. Azim Trans. Met. Chem. 2004, 29, 916-920.

41. Synthesis and physic-chemical studies on a 15 membered Hexaazamacrocyclic ligands derived from hydrazine and its complexes with Co(II), Ni(II), Cu(II) and Zn(II). M. Shakir, S. Parbeen, N.Begum, P. Chingsubam. and S.Tabassum. Synth. React. Inorg. Met.-Org. Nano-met Chem. (2004), 34,1135-1148.

42. Metal Ion Directed Synthesis of 20-membered Octaaza Macrocyclic Complexes of Co(II), Ni(II), Cu(II), And Zn(II) and their physicochemical properties. M. Shakir, P. Chingsubam, Y. Azim and S. Parbeen Synth. React. Inorg. Met.-Org . Nano-met Chem. (2004), 34,847-858.

43. Metal Ion Promoted Synthesis of Hexaaza [17] paracyclophane Derived from Terephthalaldehyde involving Co(II), Ni(II), Cu(II) and Zn(II) and their physico-

chemical studies. M. Shakir, N.Begum, S. Parbeen and Y. Azim Synth. React. Inorg. Met.-Org . Chem. (2004), 34, 797-808.

44. Synthesis of 14-membered pentaazabis (macrocyclic) complexes of Co(II), Ni(II), Cu(II) and Zn(II) linked via hydrazine and their physico-chemical studies. M. Shakir, N.Begum, S. Parbeen and Y. Azim Synth. React. Inorg. Met.-Org. Chem. (2003), 33, 1367-1379.

45. Synthesis and physico-chemical studies on 14-16 membered Octaazamacrocyclic complexes derived from hydrazine with Co(II), Ni(II), Cu(II) and Zn(II). M. Shakir, H. T. N. Chishti, Y. Azim, P. Chingsubam and Y. Siddiqi. Synth. React. Inorg. Met.-Org . Chem. (2003), 33, 1569-1583.

46. Mononuclear complexes of 4-amino-3,5-bis(pyridin-2-yl)-1,2,4-triazole containing

tripodal tris(3-aminopropyl)amine: Crystal structure of [Ni(trpn)(abpt)](ClO4)2.

M. Shakir, N.Begum, S. Parbeen and Y. Azim Polyhedron, 2003, 22 , 3181-3186.

47. Metal complexes of 22-membered mononuclear tetraimine tetramidemacrocycles ; Synthesis and characterization. T.A. Khan, S.S. Hasan, A.K.Mohammed, K.S. Islam and M. Shakir. Synth. React. Inorg. Met.-Org. Chem. (2000), 30, 815.

48. Metal-ion directed synthesis of 14-16 membered tetraamine macrocylic complexes. A.K. Mohammed, K.S. Islam, S.S. Hasan and M. Shakir. Transition Met. Chem. (1999), 24, 198-201.

49. Macrocyclic complexes of polyazaunits with divalent transition metals. M. Shakir, K.S. Islam, A.K. Mohammed and S.S. Hasan. Transition Met. Chem. (1999), 24, 577.

50. Template synthesis and spectroscopic studies of 13-membered oxotetraazamacrocyclic complexes. T.A. Khan, S.S.Hasan, A.K. Mohammed and M. Shakir. Indian J. Chem. (1998), 37A, 1123.

51. Synthesis and spectroscopic studies of octaazamacrocyclic complexes. S.S. Hasan, N. Jahan, T.A. Khan, A.K. Mohammed and M. Shakir Synth. React. Inorg. Met.-Org. Chem., (1998), 28, 153.

52. Synthesis of imidazolato and 2-methylimidazolato derivatives of Te (IV).

M. Shakir, K.S. Islam, S.S.Hasan. N.Jahan. Phosphorus, Sulfur, Silicon Relat. Elem. (1998), 136-138, 603-606.

53. Synthesis and Characterization of Organotellurium (IV) chlorosulfates. A.K.Mohammad and M. Shakir Phosphorus, Sulfur, Silicon Relat. Elem. (1998), 136-138, 553-556.

54. Nineteen -membered pentaazamacrocyclic complexes bearing tetraamide groups. O.S.M. Nasman, R.M. Barak, A.A. Khaldi, I.Elnahhal, S.P. Varkey and M. Shakir Transition Met. Chem. (1997), 22, 272-276.

55. Synthesis and Characterization of bis (macrocyclic) complexes based on the 13membered pentaaza unit. T.A. Khan, M.A. Rather, N. Jahan, S.P. Varkey and M.Shakir Synth. React. Inorg. Met.-Org. Chem., (1997), 27, 843.

56. Tetraamide macrocyclic complexes of transition metals derived from hydrazine. M. Shakir, K.S. Islam, A.K. Mohammed and N. Jahan. Transition Met. Chem. (1997), 22, 1989

57. Template synthesis and spectroscopic studies of highly conjugated tetraiminetetraamide macrocyclic complexes from 1, 2-diphenylethane- 1,2- dionedihydrazone. T.A. Khan, S.S. Hasan, S.P. Varkey, M. A. Rather, N. Jahan and M. Shakir. Transition Met. Chem., (1997), 22, 4.

58. Transition Metal Complexes 13-14 membered tetrazamacrocycles : Synthesis and characterization M. Shakir, O.S.M. Nasman, A.K. Mohammed and S.P. Varkey. Polyhedron. (1996), 15, 1283-1287.

59. Synthesis and Physico-chemical studies on the coordinating behaviour of chlorosulphate ion

in metal tris (Chlorosulphates). M (SO3Cl)3 [M = Cr, Mn, Fe], and their complexes. M. Shakir, F. Firdaus and P.S. Hameed. Synth. React. Inorg. Met.-Org. Chem., (1996), 697-720.

60. Binucleating N6 22-membered macrocyclic transition metal complexes: Synthesis and Characterization. M.Shakir, Omar S.M. Nasman and S.P. Varkey.

Polyhedron, (1996), 15, 309-314.

61. Synthesis and electrochemical studies of a new series of pendant armed hexaazamacrocyclic transition metal complexes. M. Shakir, A.K. Mohamed, S.P. Varkey and Z.A. Siddiqi Transition Met. Chem., (1996), 21, 162-165

62. Incorporation of peptide bonds in the synthesis of polyazamacrocyclic complexes. T.A. Khan, S.S. Hasan, S.P. Varkey, M.A. Rather and M. Shakir. Transition Met. Chem., (1996), 21,283-286.

63. Synthesis and Characterization of cobalt(II), nickel(II), copper(II) and zinc(II) complexes

of N5, 17-18 membered pentaazamacrocycles with N5 donor atoms. M. Shakir, O.S.M. Nasman, A.K. Mohamed and S.P. Varkey. Indian J. Chem., (1996), 35A, 710-713.

64. Self condensation reaction of o-aminobenzoic acid in presence of metal ions. M. Shakir, O.S.M. Nasman, A.K. Mohammed and S.P. Varkey. Polyhedron, (1996), 15, 2869-2874.

65. Cobalt (II), Nickel (II), Copper (II) and Zinc (II) complexes of 14-16 membered tetraazamacrocycles bearing diamide groups : Synthesis and Characterization. M. Shakir, O.S.M. Nasman, A.K. Mohammed and S.P. Varkey. Synth. React. Inorg. Met.-Org. Chem., (1996),26, 1035-1052.

66. Organotin transition metal complexes of 18-memberde binuclear hexaazamacrocycles: synthesis and characterization. M. Shakir, O.S.M. Nasman, A.K. Mohammed and S.P. Varkey. Synth. React. Inorg. Met.-Org. Chem., (1996),26, 509-528.

67. Synthesis and structural studies of bis (macrocyclic) metal (II) complexes based on 14-18 membered pentaaza unit. M. Shakir, A.K. Mohammed, S.P. Varkey and O.S.M. Nasman. Indian J. Chem., (1996), 35A, 671-676.

68. Studies on the interaction of Iron (II), Nickel (II), Copper (II) and Zn(II) with tetraazamacrocycles. M. Shakir, S.P. Varkey , O.S.M. Nasman Indian J. Chem., (1996), 35A, 671-676.

69. Synthesis and characterization of 14-16 membered tetraazamacrocyclic transition metal complexes bearing diamide groups. M. Shakir, A.K. Mohammed, O.S.M. Nasman. and S.P. Varkey Synth. React. Inorg. Met.-Org. Chem., (1996),26, 855-870.

70. Spectroscopic studies of heterobimetallic adducts of tin with Mn (II), Co(II), Ni(II), Cu(II) and Zn(II). T.A. Khan, M.A.Rather, S.P. Varkey, M. Shakir. Main Group Met. Chem., (1996), 19, 225-230.

71. Transition metal complexes of 16-18 membered tertaaazamacrocycles bearing polyamides groups. M. Shakir, A.K. Mohammed, O.S.M. Nasman. Polyhedron, 1996, 15, 3487-3492.

72. Template Synthesis and Characterization of Rh(III), Ir(III) and Pt(II)Tetraazamacrocyclic complexes. M. Shakir, A.K. Mohammed, O.S.M. Nasman. and S.P. Varkey Synth. React. Inorg. Met. -Org. Chem., (1995), 25, 1617-1684.

73. A new synthetic route for the preparation of tetraazamacrocycles and their transition metal complexes. M. Shakir and S.P. Varkey Polyhedron, 1996, 15, 1117-1127.

74. Preparation and Structural characterization of 14-16 membered pendant arm macrocyclic complexesoftransitionmetalions. M.Shakir,A.K.Mohammed,O.S.M.Nasman,S.PVarkey.AndZ.ASiddiqui Polyhedron, 1995, 14, 1277-1282.

75. Transition metal complexes of 20-22 membered octaazamacrocycles : Synthesis and characterization M.Shakir,A.K.Mohammed,S.PVarkey,O.S.M.Nasman,Z.ASiddiqui Polyhedron, 1995, 14, 1277-1282.

76. Organo tellurium (IV) derivatives: Synthesis and characterization of metal dialkyl tetrakis(chlorosulphato)tellurate(IV).M2[R2Te(SO3Cl)4](M=Na,K)andSn[R2Te(SO3Cl)4] (R=CH3,C2H5,n-C3H7,n-C4H9). M.Shakir,P.S.Hameed,F.FirdausandS.P.Varkey.

Polyhedron, 1995, 14, 1289-1294.

77. Synthesis of novel 16-18 membered tetraazamacrocycles and their Cu(II), Co(II) and Ni(II)complexes M.Shakir,S.P.Varkey Indian J. Chem. (1995), 34A, 355-359

78. Synthesis and characterization of 5,12- dioxa-7,14-dimethyl-1,4,8,11- tetraazacyclotetradeca-1,8-diene and its metal complexes with chromium (II), manganese, iron(II), nickel (II)and zinc(II)metalions. M.Shakir,S.P.VarkeyandT.AKhan Indian J. Chem., (1995), 34A, 72-75.

79. Ethylenediamine complexes of transition metal bis (Chlorosulfates). M.Shakir,F.FirdausandP.S.Hameed. Transition Met. Chem., (1995), 20, 34-37.

80. Synthesis and characterization of adduct of dichlorosulphato bis (1-3 propylenediamine) metal(II) complexes with dialkyl tin chlorides. M.Shakir,S.Hameed,F.FirdausandS.P.Varkey. Polyhedron, 1994, 20, 142-143

81. Synthesis and characterization of organotin (IV) chlorosulfates Li2[R2Sn(SO3Cl)4],

Ba[R2Sn(SO3Cl)4]andSn[R2Sn(SO3Cl)4](R=CH3,C2H5,C3H7,C4H9). M.Shakir,S.Hameed,F.FirdausandS.P.Varkey. Polyhedron, (1994), 13, 2953-2956.

82. Syntheticapproachestoinorganicringsystems. M.Shakir,H.WRoeskey. Phosphorus, Sulfur, Silicon Relat. Elem. (1994), 93, 13-38.

83. Synthesis and characterization of binuclear transition metal macrocyclic complexes of 23, 24-dioxo-3, 7, 14, 18- tetraaza cycloeicosa-1, 2, 7, 9, 11, 13, 18, 20-octaene. M.ShakirandS.P.Varkey Proc. Nat. Acid.Scie(India), 1994, 64A, 183-188.

84. Synthesis and characterization of complexes of diamines with transition

metal bis(Chlorosulphates),M(SO3Cl)2 [M=Cr, Mn, Fe, Co, Ni].

M.Shakir,P.S.Hameed,F.FirdausandS.P.Varkey Synth. React. Inorg. Met. -Org. Chem., (1994), 24, 1733-1744.

85. Six-coordinate dinuclear hexaazamacrocyclic complexes of nickel(II), copper(II) and Zinc(II)withtetraamidegroupligand. M.Shakir,S.P.Varkeyand Transition Met. Chem., (1994), 19, 606-610.

86. Template synthesis of Fe(II), Co(II), Cu(II) and Zn(II) complexes of diamidediimine macrocycles. M.Shakir,S.P.Varkey,F.FirdausandP.S.Hameed Polyhedron, (1994), 13, 2319-2325

87. Synthesis and Spectral Studies of binuclear transition metal complexes of diamidediimine-hexaazamacrocycles. M.Shakir,S.P.Varkey,F.FirdausandP.S.Hameed Polyhedron, (1994), 13, 1355-1361.

88. Binuclear transition metal complexes of schiff base macrocycles containing the furanmoiety. M.Shakir,S.P.VarkeyandD.Kumar Synth. React. Inorg. Met. -Org. Chem., (1994), 24, 941-952.

89. Synthesis and characterization of metal mono (chlorosulphates).

M(SO3Cl)(M=Ag(I) and Hg(I) and their complexes with organic donor bases M.Shakir,S.P.Varkey,F.FirdausandP.S.Hameed Synth. React. Inorg. Met. -Org. Chem., (1994), 24, 1647-1660.

90. Synthesis and characterization of Cr(II), Mn(II), Fe(II), Co(II), Ni(II), Cu(II), Zn(II) and Hg(II) complexes of N, N' diphenyl hydrazine and their triphenylphosphine derivatives M.Shakir,S.P.VarkeyandD.Kumar Indian J. Chem. (1994), 33A, 426-428

91. Synthesis and structural characterization of cobalt (II), nickel (II) and copper (II) complexes of 18-membered mixed donor macrocycles. M.Shakir, S.P.Varkey Polyhedron, (1994), 13, 791-797.

92. Divalent cobalt, nickel, copper and zinc complexes of tetraazamacrocycles bearing polyamide group: Synthesis and characterization. M.Shakir, S.P.Varkey and P.S. Hameed

Polyhedron, (1993), 12, 2775-2780.

93. Synthesis and characterization of Cobalt (II), Nickel (II) and copper (II) complexes of dithiadiaza macrocycles. M.Shakir, S.P. Varkey and P.S. Hameed. J.Chem. Res.(S), 1993,11, 442-43; (M), 2964-2985.

94. Solvolysis in chlorosulphuric acid: Preparation and characterization of K[Hg(SO3Cl)n],

(NH4)2Zn(SO3Cl)nCl4-n]UO2[Zn(SO3Cl)nCH3COO)4-n]K3[Cr(SO3Cl6],K3

[Cr(SO3Cl2)(CO4)2],K3[Cr(SO3Cl)4(C2O4)andNa3[Co(SO3Cl (ONO)6] n = 1,2,3,4,5). M.Shakir,F.FirdausandP.S.Hameed Transition Met. Chem., (1993), 18, 391-395.

95. 3,4-dicyano-5aminopyrazole complexes of anhydrous divalent transition metal chlorides andtheirtriphenylphosphinederivatives. M.Shakir,S.P.VarkeyandD.Kumar. Transition Met. Chem. (1993), 18, 107-109

96. 3-Mercapto-1,2-Propanediol and its 1-methoxy and 1-ethoxy derivatives, HSCH2CH(OH)CH2OR

’ (R

’=H, CH3, C2H5), as uninegative bidentate bridging ligands:

Synthesis and characterization of dimeric complexes with cobalt, copper and silver M.Shakir,S.P.VarkeyandD.Kumar Polyhedron, 1992, 11, 283-2836

97. Diethyl telluride as a ligand : Synthesis and physico-chemical studies on its complexes

with transition metal bis (chlorosulphates) M(SO3Cl)2 [M- Cr, Mn, Fe, Co, Ni, Cu]. M.Shakir,F.FirdausandP.S.Hameed Transition Met. Chem., (1992), 22, 1087-1096.

98. Transition metal complexes of 1, 2- dihapto-4- cyano-5-aminopyrazolide ion. M.Shakir,D.KumarandZ.A.Siddiqi. Transition Met. Chem. (1991), 16, 631-633.

99. Reactions of tetraiodomercurate anion with HSO3Cl: Synthesis and physico-chemical studies

on M2[Hg (SO3Cl)3 ( M=Cu, K), (Et4N)2 [Hg (SO3Cl)2I2 ] and K2 [Hg(SO3Cl)n4-n (n= 1,2 and3) Z.A.Siddiqi,M.Shakir. Bull. Chem.Soc.(japan), 1991, 64, 3665-3668.

100. Dimethyl telluride as a ligand : synthesis and physico-chemical studies on its complexes with transition metal bis (chlorosulphates) M(SO3Cl)2 [M- Cr, Mn, Fe, Co, Ni, Cu]. M. Shakir, D. Kumar and Z.A. Siddiqi. Transition Met. Chem. 1991, 16, 149-151.

101. Coordinating Behaviour of 4- cyano-5-aminopyrazole Ligand : Synthesis and physico-chemical studies of some transition metal complexes, ML4 Cl2 [M= Fe, Co, Ni, Cu ; L= HCNH2Pz]. M. Shakir, D. Kumar and Z.A. Siddiqi. Synth. React. Inorg. Met.-. Org. Chem., 1990, 20, 1241-1251.

102. Synthesis of Bis (imidazolate) dialkyl tin (IV) and covalent tin (II) imidazolate derivatives. Z.A. Siddiqi, S.N. Qidwai and M. Shakir J.Chem.Research(S), 1990,10,328-329.

103. Synthesis and characterization of the complexes of 5-amino-4- cyanopyrazole with Cr(II), zn(II), cd(II) and Hg(II). M. Shakir, D. Kumar and Z.A. Siddiqi. Indian J. Chem. 1990, 29A, 919-921.

104. Coordination Complexes of labile phosphorous (III) derivatives [RP(NSC)2 (R= CH3), C6H5) with first row transition metals. Z.A. Siddiqi, S.N. Qidwai and M. Shakir Bull. Chem.Soc. Fr., 1990, No. 127, 193-196.

105. Reactivity of N- Trimethyl silyl-imidazole and 2-methyl imidazole: synthesis and physico-chemical studies on transition metal imidazolates and mixed ligand imidazolates. Z.A. Siddiqi, S.N. Qidwai, M. Jaria and M.Shakir. Transition Met. Chem. 1988, 13, 317-320.

106. Reactions of N- Trimethyl silyl-imidazole and 2-methyl imidazole with anhydrous CoCl2 [Co (PPh3)3Cl] and synthesis and physico-chemical studies on two coordinate Co (II) complexes. Z.A. Siddiqi, S.N. Qidwai, M. Jaria and M.Shakir Transition Met. Chem. 1988, 13, 244-246.

107. Redox reactions in HSO3Cl solvent system : Formation of dibromoiodine (III) cation. S. A. A. Zaidi, M. Yamin, M. Shakir and Z.A. Siddiqi. Bull. Chem.Soc. Fr., 1987, 3, 441-44.

108. Triorganotin (IV) halide complexes of tetrakis (nitroindazolyl) borates. S. A. A. Zaidi, S. A. Shaheer and M. Shakir. Indian J. Chem., 1986, 25A, 863-864.

109. Synthesis and characterization of sodium hexakis (chlorosulphato) irridate (IV), Na2[Ir(SO3Cl)6] and sodium tetrakis (chlorosulphato)- palladate(II), Na2 [Pd (SO3Cl)4]. S. A. A. Zaidi, T.A Khan, Z.A. Siddiqi, M. Shakir. Synth. React. Inorg. Met.-. Org. Chem., 1986, 16, 491-497.

110. Synthesis and characterization of Sn(II) and Pb(II) chlorosulphates and their complexes with nitrogen containing donor bases. S. A. A. Zaidi, M. Yamin, M. Shakir and Z.A. Siddiqi. Indian J. Chem., 1985, 24A, 788-789.

111. Synthesis and characterization of selenium and tellurium oxychlorosulphates - oxobis (cholorosulphato) selenium (IV) and tellurium (IV): MO(SO3Cl)2 [M= Se or Te]. S. A. A. Zaidi, S.R.A. Zaidi, M. Shakir, S.A. Shaheer and Z.A. Siddiqi. Synth. React. Inorg. Met.-. Org. Chem., 1985, 4, 449-458.

Communicated Papers:

1. In-vitro DNA binding, molecular docking and antimicrobial studies on newly synthesized poly(o-toluidine)-titanium dioxide nanocomposite Mohammad Shakir, Mohd Shoeb Khan, Saud Ibrahim Al-Resayes,Umair Baig, Parvez Alam, Rizwan Hasan Khan, Mahboob Alam RSC Adv.2014, 4, 39174-39183.

2. Synthesis and characterization of a nano-hydroxyapatite/chitosan/polyethylene glycol nanocomposite for bone tissue engineering Mohammad Shakir, Reshma Jollya, Mohd Shoeb Khana, Noor-E-Irama, Tarun Kumar Sharmab and Saud Ibrahim Al-Resayesc Materials Science and Engineering C

3. Synthesis, structural characterization and antibacterial, antioxidant and anti-biofilm activities of novel Schiff base modulated Co(II), Ni(II), Cu(II) and Zn(II) complexes

Mohammad Shakir, Shumaiya Hanif and Saud I. Al-Resayesb Spectrochimica Acta Part A

4. Synthesis and characterization of Samarium doped ZnO nanoparticles and their

photocatalytic activity under visible light irradiation.  M.Shakira*, M.Faraza and Saud I. Al-Resayesb Industrial and Engineering Chemistry