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Educational accessory kit

In the educational accessory kit, you will fnd almost all accessories that you

need or start your Electrochemical measurement. Educational accessory kit

contains our items. To start your measurement, you need only to complete with

reerence electrode and a potentiostat/galvanostat.

1. P!" Electrode polishing kit is a polishing kit to reresh the working

electrode surace or #$/%low cell.

&. $#!" $oltammetry cells consist o our kinds o product' Platinum

counter electrode, (ample vials )* pcs+, Teon cap and -as purging

tue.

". Platinum working electrode is a conventional electrode, which has

hydrogen adsorption wave, used or &0& and oides detection.

2. -lassy caron working electrode is chemically stale electrode

despite its relatively large over!potentials to oygen and hydrogenevolutions.

Catalog No. Description

A-000011 Educational accessory kit

http://www.bio-logic.info/potentiostat/products.html

http://www.bio-logic.info/potentiostat/products.html

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Contents

A-002012 GCE Glassy carbon electrode OD: 6.0 mm; ID: 3.0 mm

A-002013 PE Platin!m electrode OD: 6.0 mm; ID: ".6 mm

A-011975 P#$3 Electrode Polis%ing &it

A-002232 'C$3 'oltammetry cell

Optional items


A-012167 (E$") *il+er $ sil+er c%loride re,erence electrode

A-012171 (E$- Non /!eo!s re,erence electrode

A-012108 (E$P' Preser+ati+e +ial ,or (e,erence electrode

A-001209 Cell %older ,or 0 m1 +ial

Cell vials

$arious shapes and si3es o P45E6 glass cell vials are availale or users7

purposes. Please e reerred to their capacity as well.

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Catalog No. Description*ample

'ol!me2!antity pplication

A-001056 *ample +ial 0 m1 "0 pcs 'C$ 'C$3 'C$4 *'C$3 5C

A-011504 *ample +ial 4 m1 "0 pcs 'C$

A-001051 7ater 8ac&eted Glass cell 0 m1 " pc 'C$ 'C$3 'C$4 *'C$3 5C

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A-001195 "00 m1 Glass cell +ial "00 m1 " pc 8ulk Electrolysis cell

A-001194 7ater 8ac&eted Glass cell 9,or b!l& "00 m1 " pc 8ulk Electrolysis cell



A-012062 *ample +ial ,or ((DE$3 60 m1 " pc ((DE$3

A-012018 7ater 8ac&eted Cell +ial 60 m1 " pc ((DE$3



A-012061 Glassare 0 m1 " pc (DE$ ((DE$3

A-009987 7ater 8ac&eted Cell +ial 0 m1 " pc (DE$

http://www.bio-logic.info/potentiostat/glassware_cells.html#Bulk_Electrolysis_Cell




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Accessories




VC-2 Voltammetry Cell

#ounter electrode o $oltammetry cell or $#!& is echangeale. Teon!coated

cell cap e9uips removale teon!coated working electrode holder. (ample holder

or the measurement with a small volume )1:: ! &:: 礚+ is availale as an

optional component.

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#omponents o $#!&/$#!" cell can e provided separately. In that case, each

sample vial ):1:"2"+ includes 1: pieces per the sales unit.


A-001052 VC-2 Voltammetry cell

Contents

A-001056 *ample +ial 90 m1 - pcs

A-002222 Pt co!nter electrode ,or 'C$ cell

A-009028 e,lon cap ,or 'C$

A-010537 P!rging t!be


$oltammetry cells consist o 2 kinds o products ! platinum counter electrode,

sample vials, teon cap and gas purging tue.

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Contents


A-002233 4 cm Platin!m co!nter electrode ,or 'C$3 cell

A-009035 e,lon cap ,or 'C$3



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#apale or measuring o 1 ! " m; o sample volume using electrodes with < mm

o the diameter. %urnished holder prevents the vial rom spilling.



Contents


A-011226 e,lon cap ,or 'C$

A-011227 Cell %older ,or 'C$



#omponents o $#!2 cell can e provided separately. In that case, each sample

vial ):11=">+ includes 1: pieces per the sales unit.

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$oltammetry cells consist o 2 kinds o products ! platinum counter electrode,

sample vials, teon cap and gas purging tue.

#omponents o $#!> cell can e provided separately. In this case, each samplevial )::1:><+ includes 1: pieces per the sales unit.



Contents


A-002233 Pt co!nter electrode ,or 'C$3 cell 4 cm Pt

A-011885 e,lon cap ,or 'C$4


SVC-3 Oxygen-ree Voltammetry Cell

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8y using this cell, researchers can run eperiments ree rom gasifcationed

steam. ?lso, researchers can get rid o inuence o oygen in the cell y

uling nitrogen gas. This eatures are well suited or measurements y ultra

weak current. (ample volume' >!1: m;.

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A-010914 VC-3 !"y#en-$ree Voltammetry cell

Contents


A-002233 4 cm Platin!m co!nter electrode ,or 'C$3 cell

A-011811 e,lon cap ,or *'C$3


SVC-3C Oxygen-ree Voltammetry cell - or application at lo!

temperature

8y using ($#!"# oygen!ree $oltammetry cell, researchers can get rid o

inuence o oygen in the cell y uling nitrogen gas, and also run theeperiments at low temperatures.

%eatures'

%or low temperature measurements, three special precautions are needed'

1. %luctuation o temperature!dependent reerence electrode potential.

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&. Increase o the solution resistance due to a decrease o supporting electrolyte

salt soluility.

". Incorporation o steam condensation.

@sing ($#!"# $oltammetry #ell'1. 5eerence electrode is set away y using sample holder.

&. Aicro electrode is used or measurement in high resistivity solution.

". #ell is closed.

Catalo#

%o&'escri(tion

A-012013 *'C$3C O<ygen$,ree 'oltammetry cell

Contents

e,lon cap ,or *'C$3C

*ample +ial ml 93 pcs


A-012177 *ample %older dia = mm 9 pcs

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Optional items

A-002005 5PE 5icro Platin!m electrode OD: mm ID: "0 >m

A-002006 5?E 5icro Gold electrode OD: mm ID: "0 >m

A-002007 5CE 5icro Carbon ,iber electrode OD: mm ID: - >m


Eample o the ($#!"# $oltammetry #ell application at low temperature

($#!"# 0ygen!ree $oltammetry #ell was tested at !2:癈, y Bepartment o

#hemistry, -raduate (chool o (cience, 0saka @niversity.

(chematic diagram o the eperimental cooling process

(chematic diagram o the Tetrathiaulvalene 0/5ed reaction o 1 mA

Tetrathiaulvalene in #3#C as an electrolyte solution..

:.1 A Tetrautylammonium Perchlorate, using -lassy caron electrode )0B' <

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mm, IB' 1 mm+ and 5E!* Con ?9ueous reerence electrode, with a scan rate o

1:: m$/s.

:.::1 A Tetrautylammonium

Perchlorate, using APTE Aicro Platinum electrode )0B' 2 mm, IB' 1: 祄+ and 5E!

* Con ?9ueous reerence electrode, with a scan rate o >: m$/s.

"icro volume cell

A#? Aicro cell re9uires only >:!&:: 礚 o analyst. This is an advantage or the

researchers who need to study a small volume o sample. @sers can select their

appropriate working electrodes rom our various #$ electrodes.

Dow To @se

1. Prepare supporting electrolyte in a cell vial and sample in the

sample holder. 8e sure to e9uali3e their electrolyte concentration.

&. Place a counter electrode in the cell vial. Fhen organic solvent is

used, it should e put inside the sample holder to avoid I5 drop at

the $ycor glass rit. In that case, please choose " mm diameter o

#$ electrodes.

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". Insert Teon tue into the cell or the sample holder, purge C& gas to

eliminate oygen.

D5eminder

• To lower electric resistance, please soak the $ycor rit o sampleholder into supporting electrolyte solution at least or one hour prior

to use. These rits need to e kept immersed in solution all o time.

• I otained data is shited, I5 drop may e caused. In that case,

please increase the supporting electrolyte as much as fve times or

add approimately :.> A o Ca#l.

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A-011520 )CA )icro cell kit

Contents

A-001052 'C$ 'oltammetry cell

A-012177 *ample %older dia = mm 9 pcs

#ulk electrolysis cell

This product is utili3ed or complete electrolysis. ?s mentioned elow, caron

working electrode is a reticulated orm that provides with suGcient surace area

to gain the rate in electrolysis. The water Hacketed cell can e purchased

separately. Platinum mesh electrode is also availale as a custom order. The

platinum counter electrode e9uips a separating chamer. The progress o an

electrolysis can e investigated y inserting additional indicator electrode

)re9uired to e prepared y users themselves+. That insertion re9uires a port

plug when the indicator electrode is not used.

(uitale or'

• uantitation o mass transer o the electron per molecule

• Aeasuring the asolute 9uantity o the analyte

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• Electrolytic synthesis o new materials )generally in 9uantity o

milligram+

• etc.


A-001197 *ulk Electrolysis Cell

Contents

A-001195 "00 m1 Glass cell

A-010530 Poro!s carbon electrode

A-002234 Platin!m co!nter electrode 3 cm

A-001198 1id ,or co!nter electrode

A-001196 C%amber ,or co!nter electrode

A-001236 O$ring ,or co!nter electrode

A-009131 Port pl!g

A-000178 *tirrer bar

A-001199 e,lon Cap 9,or b!l&

A-010537 Gas p!rging t!be

Optional components

Catalog No. Description *i@e

A-002250 Platin!m ga!@e electrode A0 mes% 4 < 34 mm

A-002251 Gold ga!@e electrode "00 mes% 4 < 34 mm

A-001194 7ater 8ac&eted Glass cell 9,or b!l&

Cell vials king si$e %& '(

ing si3e cell vials with and without doule Hacket are availale. The inner

diameter is J: mm. The availale volume is 1 ;.

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Cell +ial " 1 and optional al!mini!m %older

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Do!ble Bac&et cell +ial " 1


E+-C-001 Cell +ial " 1 diameter: =0 mm dept%: "30 mm

E+-C-019 l!min!m %older ,or cell +ial " 1

E+-C-002 Do!ble Bac&et cell +ial " 1

Corrosion cell kits

8io!;ogic proposes two corrosion kits' a standard one and a complete one. The

main diKerences eing that the complete kit includes a doule Hacket cell vial,

the sample holder and a telescopic stand.

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Boule Hacket corrosion cell


E+-C!,,-1 *tandard corrosion cell &it

Contents

E+-C-001 Cell +ial " 1

E+-C-003 e,lon cap

E+-C-004 e,lon ring 9*ilicone encaps!lated "0 cm diameter

E+-C-005 Cell collar it% clamp

E+-C-009 Grap%ite co!nter electrode rods 9 pieces

E+-C-016 P!rge !be

E+-C-017 )ridge t!be ,or A mm diameter re,erence electrode

,-,-110 *at!rated calomel re,erence electrode 9A mm

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,-A94+111 Cable connection ,or scre cap electrode

,-31)012 " mm OD conical rings ,or A mm OD electrodes 9 pieces

Options

E+-C-019 l!min!m %older ,or cell +ial " 1

E+-C-008 )ridge t!be ,or 6 mm diameter re,erence electrode

E+-C-014 Pt"00 probe 9indicate connector type

E+-C-015 5agnetic stirrer it% emperat!re control

E+-C-018 l!min!m base %older ,or magnetic stirrer

#omplete corrosion cell kit details


E+-C!,,-2 Complete corrosion cell &it

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Contents

E+-C-002 Do!ble Bac&et cell " 1

E+-C-003 e,lon cap

E+-C-004 e,lon ring 9*ilicone encaps!lated "0 cm diameter

E+-C-005 Cell collar it% clamp

E+-C-006 Do!ble P!rge !be

E+-C-009 Grap%ite co!nter electrode rods 9 pieces

E+-C-011 Do!ble n!t 4 mm and " mm diameter

E+-C-012 elescopic cell stand

E+-C-013 *ample %older " cm,ont

E+-C-017 )ridge t!be ,or A mm diameter re,erence electrode

,-,-110 *at!rated calomel re,erence electrode 9A mm

,-A94+111 Cable connection ,or scre cap electrode

,-31)012 " mm OD conical rings ,or A mm OD electrodes 9 pieces

Options

E+-C-008 )ridge t!be ,or 6 mm diameter re,erence electrode

E+-C-014 Pt"00 probe 9indicate connector type

E+-C-015 5agnetic stirrer it% emperat!re control


Corrosion )at cell and galvanic cell kit

This %lat #ell kit is dedicated to study at sampleLs corrosion with a surace area

o 1 or 1: cmM immersed inside corrosive environment. To ft in the cell, the

thickness o the sample has to e inerior to 1 cm. This cell is easy to use and

operates with a small sample volume )&>: m;+.

This corrosion cell is modular and can e modifed in order to carry!out galvanic

coupling or electrochemical noise )Nero 5esistance ?mmeter, N5?+

investigations etween two diKerent or same samples )the surace area o the

samples can e 1 or 1: cmM+. This specifc cell confguration can e uilt with

the galvanic option.

5egarding Electrochemical Coise investigation, note dedicated Electrochemical

Coise ?nalysis tool is included in E#!;a O sotware. To get a complete galvanic

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cell kit, the reerences E;!%;?T and :J&!%;?T/1 should e purchased or the 1

cmM confguration and E;!%;?T!& and :J&!%;?T/1: or the 1: cmM confguration.


E+-.+A/ Corrosion ,lat cell &it ,or sample o, " cmF

Contents

E+-.+A/-3 Corrosion ,lat cell " cmF it% do!ble Bac&et 940 m1 incl!ding E1$H$00

A-002056 (E$)

A-702439 Pt mes% co!nter electrode 94 mm ire A0 mes% Hlat cell design


E+-.+A/-2 Corrosion ,lat cell &it ,or sample o, "0 cmF

Contents

E+-.+A/-4 Corrosion ,lat cell "0 cmF it% do!ble Bac&et 940 m1 incl!ding E1$H$00

A-002056 (E$)

A-702439 Pt mes% co!nter electrode 94 mm ire A0 mes% Hlat cell design

Options

E+-.-002 Glass part ,or ,lat cell 940 m1

E+-.-004 )ridge t!be ,or 6 mm diameter re,erence electrode Hlat cell design

092-.+A/1 *ample %older o, " cmF ,or gal+anic cell

092-.+A/10 *ample %older o, "0 cmF ,or gal+anic cell

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Analytical cell kit

Two analytical kits are availale. The standard one does not include the

telescopic stand and doule Hacket cell.

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Boule Hacket analytical cell.


E+-E+EC/,!-1 *tandard analytical cell &it A0 m1

Contents

E+-A-001 Cell glass A0 m1

E+-A-003 e,lon co+er 4 %oles

E+-A-004 e,lon ring 9*ilicone encaps!lated "0 cm diameter

E+-A-005 Cell collar it% clamp ,or analytical cell

E+-A-008 )ridge t!be ,or 6 mm diameter re,erence electrode

E+-A-009 Pt Co!nter electrode

E+-A-016 P!rge t!be

A-002056 (E$) calomel re,erence electrode

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Options

E+-A-017 )ridge t!be ,or A mm diameter re,erence electrode

#omplet analytical cell kit details


E+-E+EC/,!-2 Complete analytical cell &it A0 m1

Contents

E+-A-002 Do!ble 8ac&et cell glass A0 m1

E+-A-003 e,lon Cap co+er 4 %oles

E+-A-004 e,lon ring 9*ilicone encaps!lated "0 cm diameter

E+-A-005 Cell collar it% clamp ,or analytical cell

E+-A-006 Do!ble P!rge !be

E+-A-008 )ridge t!be ,or 6 mm diameter re,erence electrode

E+-A-009 Pt Co!nter electrode

E+-A-011 Do!ble n!t ,or cell stand

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E+-A-012 elescopic cell stand

A-002056 (E$) calomel re,erence electrode

Options

E+-A-016 P!rge !be ,or analytical cell

E+-A-017 )ridge t!be ,or A mm diameter re,erence electrode

Corrosion * analytical kits accessories

?long with corrosion and analytical kits, several accessories can e used to hold

the cell or the sample. ? magnetic stirrer is provided with a PT1:: proe. ? wide

range o purge and ridge tues is also proposed depending on the cell si3e andon the reerence electrode used.

(tand, holder and stirrer

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Telescopic cell stand with optional doule nut and doule Hacket corrosion cell

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P"00 temperat!re probe Corrosion sample %older


E+-C-011 Do!ble n!t 94 mm and " mm diameter ,or telescopic stand

E+-C-012 elescopic cell stand 9pro+ided it%o!t corrosion cell clamp and n!t

E+-C-013 *ample %older "cm,or corrosion cell

E+-C-014 P"00 probe $ re/!ires E1$C$0"4

E+-C-015A 5agnetic stirrer %eater $ 0 ' $ it%o!t P"00 probe

E+-C-015* 5agnetic stirrer %eater $ ""0 ' $ it%o!t P"00 probe

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Purge and ridge tues

Purge tues

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8ridge tues


E+-A-006 Do!ble p!rge t!be ,or analytical cell

E+-C-006 Do!ble p!rge t!be ,or corrosion cell

E+-C-016 P!rge !be ,or corrosion cell

E+-A-016 P!rge !be ,or analytical cell

E+-C-008 )ridge t!be ,or 6 mm diameter re,erence electrode ,or corrosion cell

E+-C-017 )ridge t!be ,or A mm diameter re,erence electrode ,or corrosion cell

E+-A-008 )ridge t!be ,or 6 mm diameter re,erence electrode ,or analytical cell

E+-A-017 )ridge t!be ,or A mm diameter re,erence electrode ,or analytical cell

+late material evaluating cell

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%is /!ite %andy cell is de+eloped in order to e+al!ate plate

material s!c% as metal semi$cond!cting plate etc. In

e+al!ation a sample plate is sandic%ed beteen cell bloc&s.

Catalog No. Description 2!antity

A-011951 Plate 5aterial E+al!ating Cell "

Contents

e,lon Cell J)odyK "

e,lon Cell J)aseK "

O$ring "

*cre 0 mm

P!rging t!be " m "

A-002222 Pt co!nter electrode ,or 'C$ cell "

,Optional +roduct .eerence Electrode

@sers can select a reerence electrode separately or this cell rom'


A-012167 (E$") *il+er$*il+er c%loride re,erence electrode


A-002058 (E$"C *il+er*il+er C%loride (e,erence Electrode 9*at!rated #Cl

A-002056 (E$) Calomel (e,erence Electrode

A-002057 (E$C (e,erence Electrode

A-011503 (E$6L (e,erence Electrode #it a+ailable in al&aline sol!tion

D ow to (et @p

1. Place a plate sample on a lower side teon lock o the cell.

?pplicale plate dimensions' F' 1:!&: mm, T' " mm

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&. Put another teon lock on the sample, and drive two screws evenly

to f the plate. ;i9uid contact area depends on inner diameter o

the 0!ring. Beliver approimately 1 m; o electrolyte ater fing the

plate.

". ?ttach a Pt counter electrode and a reerence electrode to the cell

y setting them onto a cell cap. Fe would recommend you to twist

up the Pt part appropriately i the counter electrode is longer.

/lo! cell

0orking Electrodes or /lo! Cell

0ur Forking electrodes or ow cell are mounted on locks o PEE. This resin

protects the electrodes rom eternal noise and allows researchers to utili3e

them regardless the content o moile phase o P;# ecause o their hard,

organic solvent!resistance. -lassy caron is usually chosen or the redo

reaction study on li9uid chromatography. Platinum, -old, #aron paste and

Cickel electrodes are utili3ed or special purposes.

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%eatures

• 8ecome stale immediately

• @sale with acid, alkaline, and organic solvents

• Easy maintenance o Forking electrodes y wipe with acetone

• Forking electrodes can e rereshed using P!" cell Polishing it

• #an e used as chemically modifed electrodes or io!sensors

Cross /lo! Cell - Structure

#ross %low #ell is capale o 9uantitation at the level o 1:

-15

mol y the owrate' 1 m;/min ! 1:: 礚/min.

%eatures

• Betection electrode or P;#

• Electrode or ow inHection

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• Electrode or io!sensor development

Catalog No. Description pplication

A-002456 Cross ,lo cell 9Glassy Carbon 7or&ing electrode: GC dia. 3 mm < 9d!al type

A-002457 Cross ,lo cell 9Platin!m 7or&ing electrode: Pt dia. 3 mm < 9d!al type

A-012122 Cross ,lo cell 9Gold 7or&ing electrode: ! dia. 3 mm < 9d!al type

Contents

Item 5aterial 2!antity

7or&ing Electrode ,or cross ,lo cell "

(e,erence Electrode 9(E$3' *il+er$sil+er c%loride (e,erence electrode *cre type PO5 M" "

Cross Hlo cell bloc& PEE# M "

Hlo cell base bloc& PO5 "

*cre ,or base bloc& *?* M3

Hlo cell arm *?*

*cre ,or arm *?*

7or&ing Electrode connector brass "

Land scre ,or clamp *?* "

*tainless plate ,or clamp *?* "

Clamped plate *?* "

e,lon t!be EHE30 cm

A0 cm

*ilicon t!be *i cm

A cm

*tainless pipe 4 cm *?* "

G$45 e,lon Gas&et 9Cross Hlo HEP "

Dynaseal PEE# ,ingertig%t PEE# 3

Q1 Polyacetal resin Q& Polyether!ether!ketone Q" (tainless @sed (teel

Cross /lo! Cell - 0orking Electrode

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.adial /lo! cell

5adial %low #ell is developed or microore chromatography. Its detecting

eGciency will improve when ow rate is 1: 礚/min or lower. This ow cell

consists o thin layer electrode and symmetric design.

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Catalog No. Description pplication

A-003456 (adial ,lo cell 9Glassy Carbon 7or&ing electrode: GC dia. 6 mm 9single type

A-003457 (adial ,lo cell 9Platin!m 7or&ing electrode: Pt dia. 3 mm 9single type

A-011236 (adial ,lo cell 9Gold 7or&ing electrode: ! dia. 3 mm 9single type

Contents

Item 5aterial 2!antity

7or&ing Electrode ,or (adial ,lo cell "

(e,erence Electrode 9(E$3' *il+er$sil+er c%loride (e,erence electrode *cre type PO5 "

(adial Hlo cell bloc& PEE# "

Hlo cell base bloc& PO5 "

*cre ,or base bloc& *?*

Hlo cell arm *?*

*cre ,or arm *?*

Land scre ,or clamp *?* "

*tainless plate ,or clamp *?* "

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Clamped plate *?* "

e,lon t!be EHE30 cm

A0 cm

*ilicon t!be *i cm

A cm

*tainless pipe 4 cm *?* "

G$45( e,lon Gas&et 9(adial Hlo HEP "

Dynaseal PEE# ,ingertig%t PEE# 3

Electrodes and Accessories or /lo! Cell 1it

?pplication o Electrodes

• -#' commonly used or measurement o 5edo ehavior

• P%#' commonly used or measurement o 5edo ehavior

• ?u' measurement o thiol!related compounds with amalgamate

electrode

• Pt' measurement o hydrogen peroide and oidi3ed sustance

• ?g' measurement o cyano!sulfde

• #P' derivati3ationed electrode y flling compound o caron paste,

en3yme and chemical sustance into it

• Ci' amino acids measurement y chemical derivati3ation

ype Catalog No. Item Description

Cross

Hlo

A-001000 Glassy Carbon Electrode ,or cross ,lo cell

dia. 3 mm < 9d!al type

*i@e: 4 < 4 mm

A-001002 Gold Electrode ,or cross ,lo cell

A-001012 Platin!m Electrode ,or cross ,lo cell

A-001008 *il+er Electrode ,or cross ,lo cell

A-001004 Carbon Paste Electrode ,or cross ,lo cell

A-001009 Nic&el Electrode ,or cross ,lo cell

A-001046 G$5 e,lon Gas&et 9 pcs Hilm t%ic&ness: "祄

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A-001047 G$45 e,lon Gas&et 9 pcs Hilm t%ic&ness: 4祄

A-001048 G$65 e,lon Gas&et 9 pcs Hilm t%ic&ness: 40祄

A-001049 G$A5 e,lon Gas&et 9 pcs Hilm t%ic&ness: "4祄

A-001092 G$""5 *ilicon Gas&et 9 pcs Hilm t%ic&ness: 400祄

A-001093 G$"5 *ilicon Gas&et 9 pcs Hilm t%ic&ness: "000祄

A-001032 Cross Hlo cell bloc& 5aterial: PEE#

(adial

Hlo

A-001016 Glassy Carbon electrode ,or (adial ,lo cell diam. 6 mm 9single type

*i@e: 4 < 4 mmA-010941 Copper electrode ,or radial ,lo cell

A-009908 Platin!m electrode ,or radial ,lo cell

diam. 3 mm 9single type

*i@e: 4 < 4 mm

A-011155 Gold Electrode ,or radial ,lo cell

A-000999 PHCE Carbon electrode ,or radial ,lo cell

A-010251 Carbon Paste Electrode ,or radial ,lo cell

A-001146 G$5( e,lon Gas&et 9 pcs Hilm t%ic&ness: "祄

A-001147 G$45( e,lon Gas&et 9 pcs Hilm t%ic&ness: 4祄

A-001148 G$65( e,lon Gas&et 9 pcs Hilm t%ic&ness: 40祄

A-001031 (adial Hlo cell bloc& 5aterial: PEE#

Cross(adial

A-012169 (E$3' ggCl (e,erence electrode scre type *i@e: dia. "0 < A mm

A-001531 ""6 PEE# t!beID: 0.4 mm

1engt%: 3.0 m

A-004130 Dynaseal PEE# ,ingertig%t 9"0 pcs*cre ,or pipe connecting

integrated ""6

Spectroelectrocemical cell

(pectroelectrochemistry )(E#+ is aimed at the investigation o electrochemical

reaction mechanism and the interace structure etween electrolyte solution

and electrode. 5emarkale progress in this feld and related technology enales

(E# to e applied in wide areas. Cowadays, the relation etween asorance

and potential or reversile or 9uasi!reversile system is theoretically

elucidated, on which asis the analysis o electrochemical characteristics

ecomes possile or the system otherwise diGcult with only the result o

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voltammogram. Typical eample is redo en3yme cytochrome c and methylene!

lue

• 5eal!time monitoring o chromatic change y red!o reaction

• ?nalysis o the charge transer at the electrode/li9uid surace

• (pectrometric measurement o near/surace o electrodes

• ?soring spectrum o the product and intermediate

• ParametersR concentration, diKusion coeGcient and lie time

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A-011240 EC-C /in +ayer uart lass (ectroelectrocemical cell it

Components

A-011498 *EC$C Pt Ga!@e or&ing electrode

A-011499 *EC$C Pt co!nter electrode

A-011500 *EC$C %in 1ayer 2!art@ Glass cell 1ig%t pass lengt%: " mm

A-011501 *EC$C e,lon Cap


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Hront +ie *ide +ie

.eerence Electrode or SEC-C

5eerence Electrode can e chosen optionally rom elow'


A-012167 (E$") *il+er$*il+er c%loride re,erence electrode1engt%:

A0.0 mmOD: 6.0 mm

A-012171 (E$- Non /!eo!s re,erence electrode 9gg 1engt%: OD: 6.0 mm

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A-012167 (E$") *il+er$*il+er c%loride re,erence electrode1engt%:

A0.0 mmOD: 6.0 mm

A0.0 mm

0orking Electrode or SEC-C


A-012017 *EC$C ! Ga!@e or&ing electrode

A-011498 *EC$C Pt Ga!@e or&ing electrode

Spectroelectrocemical cell %5 mm optical pat lengt(

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Thin ;ayer uart3 -lass (pectroelectrochemical cell it

The :.> mm optical path length version (E#!# Thin ;ayer uart3 -lass

(pectroelectrochemical cell it is a new option or your spectroelectrochemicalmeasurement. The advantage o this new optical path length cell is that, with a

:.> mm optical path length, you could reduce the electrolysis time, compared

with the time necessary when you carried the electrolysis reaction with 1.: mm

optical path length 9uart3 cell.

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2!art@ cell Pt or&ing electrode

0n the let, :.> mm and 1.: mm optical path length 9uart3 cell are shown. 0n

the right, Pt working electrode with the dimension is shown. %or :.> mm, as or

1.: mm, you should select the working electrode )Pt or ?u+ appropriate or your

research purpose.

Note: There is a specifc working electrode or 0.5 mm optical path length. The

working electrode or 1.0 mm optical path length can not be used in 0.5 mm

optical path length quartz cell.

Comparison o electrolytic speed in unction o optical pat lengt

& mA potassium errocyanide )2D%e)#C+<+ was suHected to an electrolysis

reaction at :.< $ until its staility, and 1 A C0" was used as a reerence. The

oidation reaction was monitored y the comparison o the asorance in

unction o the time at wavelengths o 2&: and ":: nm.

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0.4 mm optical pat% lengt% ".0 mm optical pat% lengt%


A-012604 EC-C05 /in +ayer uart lass (ectroelectrocemical cell it

A-012605 EC-05C /in +ayer uart lass (ectroelectrocemical cell it Au

Common Components

A-012608 *EC$C04 %in 1ayer 2!art@ Glass cell 1ig%t pass lengt%: 0.4 mm

A-012609 *EC$C04 Pt co!nter electrode

A-011501 *EC$C e,lon Cap


7or&ing electrode

A-012606 *EC$C04 Pt Ga!@e or&ing electrode A0 5es%

A-012607 *EC$C04 ! Ga!@e or&ing electrode "00 5es%

Optional items

A-012167 (E$") *il+er$*il+er c%loride re,erence electrode


Spectroelectrocemical )o! cell

?pplications'

• (tudy o charge transer mechanism on the interace etween

electrode and electrolyte.

• (pectroscopy on electrode surace or in the neighorhood.

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• ?sorption spectra o products and intermediates.

• ?nalysis o concentration, diKusion coeGcient, lie time so on.

(chematic view o ow cell )thin layer ow channel, light pass and working

electrode+ is shown elow. Forking electrodes )IT0, platinum mini!grid, and gold

mini!grid+ are replaceale. @$ or visile light is introduced via optical!fer rom

light source and the asored light is transerred into ##B via optical!fer.

Eample o spectrum change during oidation!reduction o errocene y #$ is

shown elow.

Spectroelectrocemical electrodes

(chematic diagram o spectroelectrochemical ow cell

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+t and old mini rid electrode

(tructure o IT0 electrode

Pt mini!grid electrode is made y sputtering on 9uart3 plate as shown in elow

picture.

(i3e is = S&* mm, width o grid line is 1>: m, space etween lines is 1:: 祄.

Cat No. Description

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A-011320 *EC$H *pectroelectroc%emical ,lo cell

Contents

A-011329 *EC$H ,lo cell base

A-011330 *EC$H ,lo cell bloc& 9

A-011331 *EC$H ,lo cell bloc& 9)

A-011495 *EC$H400 e,lon gas&et 9 pcs

A-010562 -$?' ?''I* Collimating 1ens 00$000 nm

------ Dynaseal PEE# ,ingertig%t 93 pcs

------ e,lon t!be 9A0 cm

------ *ilicon t!be 930 cm

------ *tainless t!be OD ""6 940 mm

Optional +roducts

Cat No. Description

A-011810 *EC$H "000祄 probe type o, optical ,iber 1engt%: " m

A-011496 *EC$H Pt grid electrode ,or ,lo cell A < - < " mm

A-011497 *EC$H ! grid electrode ,or ,lo cell A < - < " mm

A-011519 *EC$H IO electrode ,or ,lo cell 9 pcs A < - < " mm

A-012169 (E$3' *il+er$sil+er c%loride (e,erence electrode *cre type "0 < 44 mm

A-012173 (E$-' Non /!eo!s re,erence electrode 9gg *cre type "0 < 44 mm

Sample olders

These products enale to take electrochemical measurement y only &:: 礚 o

the analyte with voltammetry cells. ? vycor glass tip is attached to the end o its

glass tue, and ions transmit reely.

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Catalog No. Description *i@e

A-012177 *ample %older dia =.0 mm 9 pcs OD: = mm ID: - mm 1: 44 mm

A-012176 *ample %older dia 6.0 mm 9 pcs OD: 6 mm ID: mm 1: 44 mm

A-012175 *ample %older dia .4 mm 9 pcs OD: .4 mm ID: mm 1: 0 mm

Vycor glass products

$ycorSglass is porous glass with 2:!&:: Sdiameter o pores. #hemically stale,

operational as high as =:: 癈. ?lso can e cut with a sharp knie.

5eminder'

4ellowish discoloration indicates the contamination. This is caused y asoring

o organics into their pores rom the air.

Speci6cations

*peci,ic gra+ity Jin dry conditionK ".4

'oid +ol!me A Q

+r. pore diameter 0$00 ,ont

Internal s!r,ace area 40 mg

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Catalog No. Description 2!antity

A-012182 'ycor Glass (od dia .A4<.0 mm 4 pcs

A-012183 Leat s%rin& e,lon t!bing "00 mm "

A-001087'ycor glass t!be

OD: - mm; ID: 4 mm; 1engt%: "0 cm"

+1-3 electrode +olising 1it

Polishing kit to maintain good condition o working electrodes or #$/%low cell.

Catalog!e No. Description

A-011975 -3 Electrode olisin# kit

Contents

$00"040 0.04祄 polis%ing al!mina 90 m1

$0004 "祄 polis%ing diamond 9"0 m1

$00"00 l!mina polis%ing pad 9"0 pcs

$00"0" Diamond polis%ing pad 9"0 pcs

$00= (eplacement glass plate ,or P#$3 9" pc

#ontents o P!" can e provided separately. In that case, each polishing pad )?!

::1:2: ?lumina polishing pad/?!::1:21 Biamond polishing pad+ includes &:

pieces o them per the sales unit.

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7o! to polis te 0orking electrodes8 surace !it +1-3

1. Prepare the glass plate, and put a ew drops o polishing diamond

on diamond polishing pad.

&. old the #$ electrode at right angle to the pad, and polish in acircular motion.

". 5eplace the diamond pad to an alumina polishing pad, put a ew

drops o polishing alumina, and polish the electrode to e mirror

surace. 5inse the electrode surace with distilled water, and fnish

y air drying.

?ttention' Polishing with P!" is the most appropriate way to clean up electrode

surace. Please consult us when other methods are applied.

+olising o +/CE Electrode * +yrolytic rapite Electrode

P%#E electrode can regain its electrochemical sensitivity and reproduciility y

polishing with Emery paper sicU2:::. ?ter the polishing, please clean its

surace with ultrasonic cleaner or 1:!<: seconds )V re9uency' >: k3, output

power' 1:: F+. P%#E electrode is a signifcantly competent electrode. In order to

keep its perormance rom going to e eroded, we recommend re!polishing ater

a certain period o time.

@se o distilled water is re9uired during this procedure. (icU&::: grade emery

paper is used at the preliminary stage only or persistent stain.

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EuroCellTM Corrosion Cell

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The EuroCellTM is a complete, ready-to-run electrochemical cell for corrosion measurements. The sample,usually a cylinder, is secured to a threaded steel rod. The EuroCell will accept any sample that can be drilledand tapped with a 3-48 thread. Its a!ailable in both "#$ an un%ac&eted model and "'$ a %ac&eted !ersion to

control the temperature of the electrochemical e(periment.

The EuroCell was desi)ned for e(periments with electrolyte !olumes from *+-'++ ml. Traditionally, corrosione(periments are performed in a one-liter flas& such as the Multiort Corrosion Cell it, usin) electrolyte!olumes of *+-/++ ml. The practice of usin) lar)e !olumes has e!ol!ed from standardi0ed procedures suchas 12TM * for otentiodynamic 1nodic olari0ation Measurements. The only technical reason to employ hi)helectrolyte !olumes is to minimi0e contamination by the corrosion products.

1 photo of the EuroCell is shown below. There are fi!e ports a '454+ )round-)lass %oint, two 6 1ce-Threds,and two #45'+ )round-)lass %oints. The central '454+ )round )lass %oint supports the cylindrical 7or&in)Electrode "your corrosion sample$ in the 2ample older. The 9eference Electrode :rid)e Tube and theCounter Electrode and the :ubbler are all mounted in the 1ce-Threds, which allow them to be ad%usted!ertically to accommodate a wide ran)e of sample !olumes. The !ertical ad%ustment is also handy to ma&e sureyour 9eference Electrode :rid)e Tube is placed close to the surface of your corrosion sample. The :ubbler iscontained in the #45'+ %oint and has one position for deaeration and another for blan&etin). The standard

Counter Electrode is a )raphite rod. It is also possible to use a platinum counter electrode. 1 brid)e tubecontainin) a platinum counter electrode is a!ailable "art ;o. //+-#/4$ to pre!ent products from the counterelectrode from contactin) products from the wor&in) electrode. 7e included an additional #45'+ port for athermometer or other accessory.

Cylindrical samples for the EuroCell can be fabricated in your lab or, for con!enience, can be purchaseddirectly from Metal 2amples, a commercial supplier of corrosion samples for testin).

Clic& to enlar)e

http://popupwindow%28%27http//aseptec.com.my/popup_image.php?pID=83%27)



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