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United States Environmental Protection Agency Region VII
300 Minnesota Avenue Kansas City, KS 66101
Date; _ /JUJ.JJ 2015
Subject: Data Disposition/Sample Release for ASR #: 6787
Project ID: TH07PZ01
Project Description: Oak Grove Village well - RA sampling
From: Tonya Howell SUPR/MOKS
To: Alisha Claycamp ENSV/CARB
I have received and reviewed the Transmittal of Sample Analysis Results for the above-referenced Analytical Services Request(ASR) and have indicated my findings below by checking~6TTe of the boxes for Data Disposition.
I understand all samples will be disposed upon receipt of this form, unless samoles are requested to be held. If I do not return this form all samples will be disposed of on AUG L U ^"13
• "RELEASED" - Read-only to all Region 7 employees and contractors that have R7LIMS "Customer" account. All Samples may be disposed of upon receipt of this form if not requested to be held.
• "Project Manager Accessible" - Available on the LAN in R7LIMS for my use only. All Samples may be disposed of upon receipt of this form if not requested to be held.
• "Archived" - THIS DATA IS OF A SENSITIVE NATURE. Any future reports must be requested through the laboratory. All samples may be disposed of upon receipt of the form if not requested to be held.
• Hold Samples - I have determined that the samples need to be held until —— after which time they will be disposed of in accordance with applicable regulations. The reason for the hold is:
• Samples are associated with a legal proceeding.
• Question/Concern with data - possible reanalysis requested.
O Other:
01 ? Z-
cruoi
40496152
Superfund
3.
J
SOP No. 2410.1G
Attachment 2
LABORATORY CUSTOMER SATISFACTION SURVEY
Thanks for using our services. It would help us in serving you better if you took a minute to complete this survey.
Return the completed survey to Alisha Claycamp, ENST/LTAB.
Name:
Division/Branch/Section:
ASR Number: _ Date:
Was your data received in a timely manner:
Was data usable for its intended purpose:
Communication with Laboratory staff:
Comments:
JUL 2 0 2015 ptr. isl 2
2
nd -> rd ,« ill J 4
1 Late
Little Value
1 Poor
3 30-day
(Standard)
3 Meets Needs
3 Averaee
4 5 Received
Early
4 5 Exceeds
Expectations
4 5 Clear &
Informative
Code: !L
JUL 2 0 2015
United States Environmental Protection Agency — Region 7
300 Minnesota Avenue Kansas City, KS 66101
Date: jyj_ 2 0 2015 Subject: Transmittal of Sample Analysis Results for ASR #: 6787
Project ID: TH07PZ01
Project Description: Oak Grove Village well - RA sampling
From: Margaret E.W. St. Germain, Chief m / Laboratory Technology & Analysis Branch) Environmental Sciences & Technology Division
To: Tonya Howell —••— SUPR/MOKS
Enclosed are the analytical data for the above-referenced Analytical Services Request (ASR) and Project. The Regional Laboratory has reviewed and verified the results in accordance with procedures described in our Quality Manual (QM). In addition to all of the analytical results, this transmittal contains pertinent information that may have influenced the reported results and documents any deviations from the established requirements of the QM.
Please contact us within 14 days of receipt of this package if you determine there is a need for any changes. Please complete the enclosed Customer Satisfaction Survey and Data Disposition/Sample Release memo for this ASR as soon as possible. The process of disposing of the samples for this ASR will be initiated 30 days from the date of this transmittal unless an alternate release date is specified on the Data Disposition/Sample Release memo.
If you have any questions or concerns relating to this data package, contact our customer service line at 913-551-5295.
Enclosures
cc: Analytical Data File.
Page 1 of 12
ASR Number: 6787 Summary of Project Information > i
07/20/2015
Tonya Howell Org: SUPR/MOKS Phone: 913-551-7589
TH07PZ01
Oak Grove Village well - RA sampling
Oak Grove State: Missouri Program: Superfund
OAK GROVE VILLAGE WELL - OAK GROVE VILLAGE Site ID: 07PZ Site OU: 01 WELL GPRA-.RRC: 303DD2 Site Characterization •' :•
To determine the nature and extent of VOC contamination in air from an undefined TCE plume & determine if VOC concentrations in cave air are increasing or decreasing.
Explanation of Codes, Units and Qualifiers used on this report
Sample QC Codes: QC Codes identify the type of Units: Specific units in which results are sample for quality control purpose. reported.
= Field Sample ug/m3 = Micrograms per Cubic Meter FD = Field Duplicate
Data Qualifiers: Specific codes used in conjunction with data values to provide additional information on the quality of reported results, or used to explain the absence of a specific value.
(Blank)= Values have been reviewed and found acceptable for use. U = The analyte was not detected at or above the reporting limit.
Project Manager:
Project ID:
Project Desc:
Location:
Site Name:
Purpose:
Page 2 of 12
ASR Number: 6787
Project ID: TH07PZ01
Sample Information Summary
Project Desc: Oak Grove Village well - RA sampling
07/20/2015
Sample QC External Start Start End End Receipt No Code Matrix Location Description Sample No Date Time Date Time Date
1 - Air Gift shop (Jewelry counter) 06/22/2015 13:33 06/23/2015 12:02 06/26/2015
1 - FD Air Gift shop (Jewelry counter) 06/22/2015 13:30 06/23/2015 12:01 06/26/2015
2 - Air Ballroom 06/22/2015 13:38 06/23/2015 __1Jj43 06/26/2015
3 - _ Air Loot Rock 06/22/2015 12:15 06/23/2015 11:30 06/26/2015
4 - _ Air Site Bll 06/22/2015 12:00 06/23/2015 11:13 06/26/2015
5 - Air Lassie 06/22/2015 12:07 06/23/2015 11:06 06/26/2015
6 - _ Air Jungle Room 06/22/2015 11:35 06/23/2015 11:00 06/26/2015
7 - Air Theater 06/22/2015 13:45 06/23/2015 11:37 06/26/2015
8 - _ Air Gazebo 06/22/2015 13:12 06/23/2015 12:39 06/26/2015
9 - _ Air Conference (in slot) 06/22/2015 14:05 06/23/2015 11:56 06/26/2015
10 - _ Air Bat cave (left wing) 06/22/2015 14:35 06/23/2015 11:10 06/26/2015
12 - Air Jungle Room 06/24/2015 15:57 06/25/2015 13:40 06/26/2015
13 - Air Ballroom stage 06/24/2015 16:21 06/25/2015 14:02 06/26/2015
14 - Air Gift shop 06/24/2015 16:30 06/25/2015 13:57 06/26/2015
14 - FD Air Gift shop 06/24/2015 16:31 06/25/2015 13:58 06/26/2015
15 - Air Conference room (left vent) 06/24/2015 16:40 06/25/2015 14:17 06/26/2015
Page 3 of 12
ASR Number: 6787 RLAB Approved Analysis Comments 07/20/2015
Project ID: TH07PZ01 Project Desc Oak Grove Village well - RA sampling
Analysis Comments About Results For This Analysis
1 VOCs in Air at Ambient Levels by GC/MS
Lab: RASP Contract Lab (Out-Source)
Method: Similar to EPA Region 7 RLAB Method 3230.4G (see comments)
Samples: 1- 1-FD 2- 3- 4- 5- 6-7- 8- 9- 10-_ 12- 13- 14-14-FD 15-
Comments: The pressure of the sample canisters was checked prior to analysis. The pressures ranged from 6.9 to 14.7 psia. Sample 6787-14FD was received at 6.9 and required pressurization for analysis which resulted in an initial dilution.
!
Page 4 of 12
ASR Number: 6787 RLAB Approved Sample Analysis Results 07/20/2015
Project ID: TH07PZ01 Project Desc: Oak Grove Village well - RA sampling
analysis/ Analyte Units 1- 1-FD 2- 3-
VOCs in Air at Ambient Levels by GC/MS Acetone ug/m3 22.7 12.1 16 5.95 U
Benzene ug/m3 0.31 U 0.31 U 0.31 U 0.31 U
Bromodichloromethane ug/m3 3.35 U 3.35 U 3.35 U 3.35 U
Bromoform ug/m3 5.17 U 5.17 U 5.17 U 5.17 U
Bromomethane ug/m3 1.94 U 1.94 U 1.94 U 1.94 U
2-Butanone ug/m3 3.18 1.47 U 1.62 1.47 U Carbon Disulfide ug/m3 1.56 U 1.56 U 1.56 U 1.56 U Carbon Tetrachloride ug/m3 0.41 U 0.41 U 0.41 U 0.41 U
Chlorobenzene ug/m3 2.3 U 2.3 U- 2.3 U 2.3 U
Chloroethane ug/m3 1.32 U 1.32 U 1.32 U 1.32 U
Chloroform ug/m3 2.44 U 2.44 U 2.44 U 2.44 U
Chloromethane ug/m3 1.03 U 1.03 U 1.03 U 1.03 U
Dibromochloromethane ug/m3 4.26 U 4.26 U 4.26 U 4.26 U 1,2-Dibromoethane ug/m3 3.84 U 3.84 U ~3T84 U 3.84 U
1,2-Dichlorobenzene ug/m3 3 U 3 U 3 U 3 U
1,3-Dichlorobenzene ug/m3 3 U 3 U 3 U 3 U
Dichlorodifluoromethane ug/m3 3.76 3.51 3.16 4.15 1,1-Dichloroethane ug/m3 2.02 U 2.02 U 2.02 U 2.02 U
1,2-Dichloroethane ug/m3 0.324 0.324 0.19 U 0.19 U
1,1-Dichloroethene ug/m3 1.98 U 1.98 U 1.98 U 1.98 U
cis-l,2-Dichloroethene ug/m3 1.98 U 1.98 U 1.98 U 1.98 U
trans-l,2-Dichloroethene ug/m3 1.98 U 1.98 U 1.98 U 1.98 U
1,2-Dichloropropane ug/m3 2.31 U 2.31 U 2.31 U 2.31 U
cis-l,3-Dichloropropene ug/m3 2.27 U 2.27 U 2.27 U 2.27 U
trans-1,3-Dichloropropene ug/m3 2.27 U 2.27 U 2.27 U 2.27 U
Ethyl Benzene ug/m3 2.17 U 2.17 U 2.17 U 2.17 U
Heptane ug/m3 2.05 U 2.05 U 2.05 U 2.05 U
Hexachlorobutadiene ug/m3 5.33 U 5.33 U 5.33 U 5.33 U
Hexane ug/m3 1.76 U 1.76 U 1.76 U 1.76 U
2-Hexanone ug/m3 2.05 U 2.05 U 2.05 U 2.05 U
Isopropylbenzene ug/m3 2.46 U 2.46 U 2.46 U 2.46 U
Methylene Chloride ug/m3 8.7 U 8.7 U 8.7 U 8.7 U
4-Methyl-2-Pentanone ug/m3 2.05 U 2.05 U Jh05 U 2.05 U
Naphthalene ug/m3 2.62 U 2.62 U 2.62 U 2.62 U
Styrene ug/m3 4.22 3.11 2.13 U 2.13 U 1,1,2,2-Tetrachloroethane ug/m3 3.43 U 3.43 U 3.43 U 3.43 U
Tetrachloroethene ug/m3 1.49 1.42 1.22 1.36
Toluene ug/m3 1.88 U 1.88 U 1.88 U 1.88 U
1,2,4-Trichlorobenzene ug/m3 3.71 U 3.71 U 3.71 U 3.71 U
1,1,1 -Tri chloroethane ug/m3 2.73 U 2.73 U 2.73 U 2.73 U
1,1,2-Trichloroethane ug/m3 0.23 U 0.23 U 0.23 U 0.23 U
Trichloroethene ug/m3 100 95.7 127 114
Trichlorofluoromethane ug/m3 49.3 46.4 59.4 73.8
1,1,2 -Tri ch 1 o rotrif 1 u oroeth a ne ug/m3 3.83 U 3.83 U 3.83 U 3.83 U
1,2,4-Trimethylbenzene ug/m3 2.46 U 2.46 U 2.46 U 2.46 U
Page 5 of 12
ASR Number: 6787
Project ID: TH07PZ01
Analysis/ Analyte
1,3,5-Trimethylbenzene Vinyl Chloride m and/or p-Xylene o-Xylene
RLAB Approved Sample Analysis Results 07/20/2015
Project Desc: Oak Grove Village well - RA sampling
Units 1- 1-FD 2- 3-
ug/m3 ug/m3 ug/m3 ug/m3
2.46 U 0.16 U 4.34 U 2.17 U
2.46 U
0.16 U
4.34 U
2.17 U
2.46 U
0.16 U
4.34 U
2.17 U
2.46 U
0.16 U
4.34 U
2.17 U
Page 6 of 12
J »
ASR Number: 6787 RLAB Approved Sample Analysis Results 07/20/2015
Project ID: TH07PZ01 Project Desc: Oak Grove Village well - RA sampling
analysis/ Analyte Units 4- 5- 6- 7-
VOCs in Air at Ambient Levels by GC/MS Acetone ug/m3 12.2 5.95 U 5.95 U 12.5
Benzene ug/m3 0.31 U 0.31 U 0.31 U 0.31 U
Bromodichloromethane ug/m3 3.35 U . 3.35 U —3^35 U 3.35 U
Bromoform ug/m3 5.17 U 5.17 U 5.17 U 5.17 U
Bromomethane ug/m3 1.94 U 1.94 U 1.94 U 1.94 U
2-Butanone ug/m3 1.47 U 1.47 U 1.47 U 1.47 U Carbon Disulfide ug/m3 1.56 U 1.56 U 1.56 U 1.56 U
Carbon Tetrachloride ug/m3 0.41 U 0.41 U 0.41 U 0.41 U
Chlorobenzene ug/m3 2.3 U 2.3 U 2.3 U 2.3 U
Chloroethane ug/m3 1.32 U 1.32 U 1.32 U 1.32 U
Chloroform ug/m3 2.44 U 2.44 U 2.44 U 2.44 U
Chloromethane ug/m3 1.03 U 1.03 U 1.03 U 1.03 U
Dibromochloromethane ug/m3 4.26 U 4.26 U 4.26 U 4.26 U
1,2-Dibromoethane ug/m3 3.84 U 3.84 U 3.84 U 3.84 U
1,2-Dichlorobenzene ug/m3 3 U 3 U 3 U 3 U
1,3-Dichlorobenzene ug/m3 3 U 3 U 3 U 3 U
Dichlorodifluoromethane ug/m3 5.83 4.15 5.14 2.47 1,1-Dichloroethane ug/m3 2.02 U 2.02 U 2.02 U 2.02 U 1,2-Dichloroethane ug/m3 0.19 U 0.19 U 0.19 U 0.19 U
1,1-Dichloroethene ug/m3 1.98 U 1.98 U 1.98 U 1.98 U
cis-l,2-Dichloroethene ug/m3 1.98 U 1.98 U 1.98 U 1.98 U
trans-1,2-Dichloroethene ug/m3 1.98 U 1.98 U 1.98 U 1.98 U 1,2-Dichloropropane ug/m3 2.31 U 2.31 U _2>31 U 2.31 U
cis-l,3-Dichloropropene ug/m3 2.27 U 2.27 U 2.27 U 2.27 U
trans- 1,3-Dichloropropene ug/m3 2.27 U 2.27 U 2.27 U . 2.27 U
Ethyl Benzene ug/m3 2.17 U 2.17 U 2.17 U 2.17 U
Heptane ug/m3 2.05 U 2.05 U 2.05 U 2.05 U
Hexachlorobutadiene ug/m3 5.33 U 5.33 U 5.33 U 5.33 U
Hexane ug/m3 1.76 U 1.76 U 1.76 U 1.76 U
2-Hexanone ug/m3 2.05 U 2.05 U 2.05 U 2.05 U
Isopropylbenzene ug/m3 2.46 U 2.46 U 2.46 U 2.46 U
Methylene Chloride ug/m3 8.7 U 8.7 U 8.7 U 55.6
4-Methyl-2-Pentanone ug/m3 2.05 U 2.05 U 2.05 U 2.05 U
Naphthalene ug/m3 2.62 U 2.62 U 2.62 U 2.62 U
Styrene ug/m3 2.13 U 2.13 U 2.13 U 2.13 U
1,1,2,2-Tetrachloroethane ug/m3 3.43 U 3.43 U 3.43 U 3.43 U
Tetrachloroethene ug/m3 1.63 1.42 1.63 0.41 U
Toluene ug/m3 1.88 U 1.88 U 1.88 U 1.88 U
1,2,4-Trichlorobenzene ug/m3 3.71 U 3.71 U 3.71 U 3.71 U
1,1,1-Trichloroethane ug/m3 2.73 U 2.73 U 2.73 U 2.73 U
1,1,2-Trichloroethane ug/m3 0.23 U 0.23 U 0.23 U 0.23 U
Trichloroethene ug/m3 130 120 147 (
0.43 U
Trichlorofluoromethane ug/m3 92.4 76.9 —7-^9 2.81 U
1,1/2-Trichlorotrifluoroethane ug/m3 4.9 3.91 3.83 U 3.83 U
1,2,4-Trimethylbenzene ug/m3 2.46 U 2.46 U 2.46 U 2.46 U
Page 7 of 12
ASR Number: 6787
Project ID: TH07PZ01
RLAB Approved Sample Analysis Results
Project Desc: Oak Grove Village well - RA sampling
07/20/2015
Analysis/ Analyte Units 4- 5- 6- 7-
1,3,5-Trimethyl benzene ug/m3 2.46 U 2.46 U 2.46 U 2.46 U Vinyl Chloride ug/m3 0.16 U 0.16 U 0.16 U 0.16 U rn and/or p-Xylene ug/m3 4.34 U 4.34 U 4.34 U 4.34 U o-Xylene ug/m3 2.17 U 2.17 U 2.17 U 2.17 U
Page 8 of 12
ASR Number: 6787 RLAB Approved Sample Analysis Results
Project ID: TH07PZ01 Project Desc: Oak Grove Village well - RA sampling
07/20/2015
analysis/ Analyte Units 8- 9- 10- 12-
VOCs in Air at Ambient Levels by GC/MS Acetone ug/m3 7.88 5.95 U 5.95 U 5.95 U
Benzene ug/m3 0.31 U 0.31 U 0.31 U 0.31 U
Bromodichloromethane ug/m3 3.35 U 3.35 U 3.35 U 3.35 U
Bromoform ug/m3 5.17 U 5.17 U 5.17 U 5.17 U
Bromomethane ug/m3 1.94 U 1.94 U 1.94 U 1.94 U
2-Butanone ug/m3 1.47 U 1.47 U 1.47 U 1.47 U
Carbon Disulfide ug/m3 1.56 U 1.56 U 1.56 U 1.56 U
Carbon Tetrachloride ug/m3 0.44 0.41 U 0.41 U 0.41 U
Chlorobenzene ug/m3 2.3 U 2.3 U 2.3 U 2.3 U
Chloroethane ug/m3 1.32 U 1.32 U 1.32 U 1.32 U
Chloroform ug/m3 2.44 U 2.44 U 2.44 U 2.44 U
Chloromethane ug/m3 1.03 U 1.03 U 1.03 U 1.03 U
Dibromochloromethane ug/m3 4.26 U 4.26 U -4726 U 4.26 U
1,2-Dibromoethane ug/m3 3.84 U 3.84 U 3.84 U 3.84 U
1,2-Dichlorobenzene ug/m3 3 U 3 U 3 U 3 U
1,3-Dichlorobenzene ug/m3 3 U 3 U 3 U 3 U
Dichlorodifluoromethane ug/m3 2.87 5.19 2.47 U 5.78
1,1-Dichloroethane ug/m3 2.02 U 2.02 U 2.02 U 2.02 U
1,2-Dichloroethane ug/m3 0.19 U 0.19 U 0.19 U 0.19 U
1,1-Dichloroethene ug/m3 1.98 U 1.98 U 1.98 U 1.98 U
cis-l,2-Dichloroethene ug/m3 1.98 U 1.98 U 1.98 U 1.98 U
trans- 1,2-Dichloroethene ug/m3 1.98 U 1.98 U 1.98 U 1.98 U
1,2-Dichloropropane ug/m3 2.31 U 2.31 U 2.31 U 2.31 U
cis-l,3-Dichloropropene ug/m3 2.27 U 2.27 U 2.27 U 2.27 U
trans-l,3-Dichloropropene ug/m3 2.27 U 2.27 U 2.27 U 2.27 U
Ethyl Benzene ug/m3 2.17 U 2.17 U 2.17 U 2.17 U
Heptane ug/m3 2.05 U 2.05 U 2.05 U 2.05 U
Hexachlorobutadiene ug/m3 5.33 U 5.33 U 5.33 U 5.33 U
Hexane ug/m3 1.76 U 1.76 U 1.76 U 1.76 U
2-Hexanone ug/m3 2.05 U 2.05 U 2.05 U 2.05 U
Isopropylbenzene ug/m3 2.46 U 2.46 U 2.46 U 2.46 U
Methylene Chloride ug/m3 8.82 8.7 U 8.7 U 8.7 U
4-Methyl-2-Pentanone ug/m3 2.05 U 2.05 U ~2"05 U 2.05 U
Naphthalene ug/m3 2.62 U 2.62 U 2.62 U 2.62 U
Styrene ug/m3 2.13 U 2.13 U 2.13 U 2.13 U
1,1,2,2-Tetrachloroethane ug/m3 3.43 U 3.43 U 3.43 U 3.43 U
Tetrachloroethene ug/m3 0.41 U 1.49 0.41 U 2.17
Toluene ug/m3 1.88 U 1.88 U 1.88 U 1.88 U
1,2,4-Trichlorobenzene ug/m3 3.71 U 3.71 U 3.71 U 3.71 U
1,14-Trichloroethane ug/m3 2.73 U 2.73 U 2.73 U 2.73 U
1,1,2-Trichloroethane ug/m3 • 0.23 U 0.23 U 0.23 U 0.23 U
Trichloroethene ug/m3 0.43 U 125 0.43 U 137
Trichlorofluoromethane ug/m3 2.81 U 76.5 2.81 U 99.4
1,1/2-Trichlorotrifluoroethane ug/m3 3.83 U 3.83 U 3.83 U 4.29
1,2,4-Trimethylbenzene ug/m3 2.46 U 2.46 U 2.46 U 2.46 U
Page 9 of 12
ASR Number: 6787
Project ID: TH07PZ01
Analysis/ Analyte
RLAB Approved Sample Analysis Results
Project Desc: Oak Grove Village well - RA sampling
Units 8- 9-
07/20/2015
10- 12-
1,3,5-Trimethylj3£nzene Vinyl Chloride m and/or p-Xylene
o-Xylene
ug/m3 ug/m3 ug/m3 ug/m3
2.46 U
0.16 U
4.34 U
2.17 U
2.46 U
0.16 U
4.34 U
2.17 U
2.46 U
0.16 U
4.34 U
2.17 U
2.46 U 0.16 U 4.34 U 2.17 U
Page 10 of 12
ASR Number: 6787 RLAB Approved Sample Analysis Results
Project ID: TH07PZ01 Project Desc: Oak Grove Village well - RA sampling
07/20/2015
Analysis/ Analyte
1 VOCs in Air at Ambient Levels by GC/MS Acetone
Benzene
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone Carbon Disulfide Carbon Tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
Dibromochloromethane 1,2-Dibromoethane
1.2-Dichlorobenzene
1.3-Dichlorobenzene
Dichlorodifluoromethane
1.1-Dichloroethane
1.2-Dichloroethane
1.1-Dichloroethene
cis-l,2-Dichloroethene
trans-1,2-Dichloroethene 1.2-Dichloropropane
cis-l,3-Dichloropropene
trans-l,3-Dichloropropene
Ethyl Benzene
Heptane
Hexachlorobutadiene
Hexane
2-Hexanone
Isopropylbenzene
Methylene Chloride
4-Methyl-2-Pentanone Naphthalene
Styrene
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,4-Trichlorobenzene
1.1.1-Trichloroethane
1.1.2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,1,2-Trichlorotrifluoroethane
1,2,4-Trimethyl benzene
Units 13- 14- 14-FD 15-
ug/m3 5.95 U 12.7 11.9 U 7.84
ug/m3 0.31 U 0.31 U 0.62 U 0.31 U
ug/m3 3.35 U 3.35 U 6.7 U 3.35 U
ug/m3 5.17 U 5.17 U 10.3 U 5.17 U
ug/m3 1.94 U 1.94 U 3.88 U 1.94 U
ug/m3 1.47 U 1.56 2.94 U 1.47 U
ug/m3 1.56 U 1.56 U 3.12 U 1.56 U
ug/m3 0.41 U 0.41 U 0.82 U 0.41 U
ug/m3 2.3 U 2.3 U 4.6 U 2.3 U
ug/m3 1.32 U 1.32 U 2.64 U 1.32 U
ug/m3 2.44 U 2.44 U 4.88 U 2.44 U
ug/m3 1.03 U 1.03 U 2.06 U 1.03 U
ug/m3 4.26 U 4.26 U 8.52 U 4.26 U
ug/m3 3.84 U 3.84 U ~/T68 U 3.84 U
ug/m3 3 U 3 U 6 U 3 U ug/m3 3 U 3 U 6 U 3 U
ug/m3 2.67 2.47 U 2.47 U 5.54
ug/m3 2.02 U 2.02 U 4.04 U 2.02 U
ug/m3 0.19 U 0.283 0.38 U 0.19 U
ug/m3 1.98 U 1.98 U 3.96 U 1.98 U
ug/m3 1.98 U 1.98 U 3.96 U 1.98 U ug/m3 1.98 U 1.98 U 3.96 U 1.98 U
ug/m3 2.31 U 2.31 U 4.62 U 2.31 U
ug/m3 2.27 U 2.27 U 4.54 U 2.27 U
ug/m3 2.27 U 2.27 U 4.54 U 2.27 U
ug/m3 2.17 U 2.17 U 4.34 U 2.17 U
ug/m3 2.05 U 2.05 U 4.1 U 2.05 U ug/m3 5.33 U 5.33 U 10.7 U 5.33 U
ug/m3 1.76 1.76 U 3.52 U 1.76 U
ug/m3 2.05 U 2.05 U 4.1 U 2.05 U
ug/m3 2.46 U 2.46 U 4.92 U 2.46 U
ug/m3 11.4 64.2 17.4 U • 8.7 U
ug/m3 2.05 U 2.05 U 4.1 U 2.05 U ug/m3 i.'j ug/m3 2.62 U 2.62 U 5.24 U 2.62 U
ug/m3 2.13 U 2.98 4.26 U 2.13 U
ug/m3 3.43 U 3.43 U 6.86 U 3.43 U
ug/m3 0.475 0.475 0.82 U 2.03 ug/m3 1.88 U 1.88 3.76 U 1.88 U
ug/m3 3.71 U 3.71 U 7.42 U 3.71 U
ug/m3 2.73 U 2.73 U 5.46 U 2.73 U
ug/m3 0.23 U 0.23 U 0.46 U 0.23 U ug/m3 24 8.11 9.78 142
ug/m3 13.5 5.22 3.09 93.2 ug/m3 3.83 U 3.83 U 7.66 U 4.14
ug/m3 2.46 U 2.46 U 4.92 U 2.46 U
Page 11 of 12
ASR Number: 6787
Project ID: TH07PZ01
Analysis/ Analyte
1,3,5-Trimethylbenzene Vinyl Chloride m and/or p-Xylene o-Xylene
RLAB Approved Sample Analysis Results 07/20/2015
Project Desc: Oak Grove Village well - RA sampling
Units 13- 14- 14-FD 15-
ug/m3
ug/m3
ug/m3
ug/m3
2.46 U 0.16 U 4.34 U 2.17 U
2.46 U
0.16 U
4.34 U
2.17 U
4.92 U
0.32 U
8.68 U
4.34 U
2.46 U 0.16 U 4.34 U 2.17 U
Page 12 of 12
CHAIN OF CUSTODY RECORD ENVIRONMENTAL PROTECTION AGENCY REGION VII
ACTIVITY LEADER(Print) TonvjOi Hou>3gA\
NAME OF SURVEY OR ACTIVITY DATE OF COLLEJ tt 5® DAY NTH YEAR
CONTENTS OF SHIPMENT
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MI
SAMPLE NUMBER
/~ 1 ^ TYPE OF CONTAINERS SAMPLED MEDIA RECEIVING LABORATORY REMARKS/OTHER INFORMATION (condition of samples upon receipt. fc other sample numbers, etc )
SAMPLE NUMBER
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VOA SET (2 VIALS EA)
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RECEIVING LABORATORY REMARKS/OTHER INFORMATION (condition of samples upon receipt. fc other sample numbers, etc )
SAMPLE NUMBER
NUMBERS OF CONTAINERS PER SAMPLE NUMBER ? o l/l sedime
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RECEIVING LABORATORY REMARKS/OTHER INFORMATION (condition of samples upon receipt. fc other sample numbers, etc )
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DESCRIPTION OF SHIPMENT MODE OF SHIPMENT
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F t E LAMQ uATh E A M P L E R)
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DATE
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TIME
mt
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REASON FOR CHANGE OF CUSTODY S b t p L f C o A j u t Y A t ^ E s
RELINQUISHED BY
^ J ~1 SEALED UNSEALED Of
DATE
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TIME
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RECEIVED BY
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REASON FOR CHANGE OF CUSTODY
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[SEALED UNSEALEDp
REASON FOR /CHANGE OF CUSTODY
7-EPA-9262(Revised 5/85) 'U.S. GPO: 2002-755-917M0053
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 6787 Sample Number: 1 QC Code: Matrix: Air Tag ID: 6787-1-
Project ID: TH07PZ01 Project Manager: Tonya Howell Project Desc: Oak Grove Village well - RA sampling
City: Oak Grove State: Missouri Program: Superfund
Site Name: OAK GROVE VILLAGE WELL - OAK GROVE VILLAGE WELL Site ID: 07PZ' Site OU: 01
Location Desc:
Expected Cone:
Latitude:
Longitude:
^ f n irW)
External Sample Number:
(or Circle One: Low Medium High) Date
Sample Collection: Start: (n /££}/ I S
End: &J2&W
Time(24 hr)
I3-:3S
Laboratory Analyses: Container Preservative
1 - 6 L i t e r C a n i s t e r N o n e
Holding Time Analysis 60 Days 1 VOCs in Air at Ambient Levels by GC/MS
Sample Comments:
(N/A) VQCOMVA Wc
T)(L()VSC|
-5.5 L 150
Sample Collected By: USGS
1 of 1
Sample Collection Field Sheet US EPA Region 7 0
Kansas City, KS y/
d / 1-fD ASR Number: 6787 Sample Number: 23$ QC CodeuM-P Matrix: Air Tag ID: 6787-Z&-
Project ID: TH07PZ01 Project Desc: Oak Grove Village well - RA samf
City: Oak Grove Program: Superfund
Site Name: OAK GROVE VILLAGE WEL/- OAK GROVE VILLAGE WELL Site ID: 07PZ Site OU: 01
oject Manager: Tonya Howell
State: Missouri
Location Desc:
Expected Cone:
Latitude:
Longitude:
External Sample Number:
Circle One: Low Medium High) Date
Sample Collection: Start: (p /oQV 15
End: (p &V 15
Time(24 hr)
Laboratory Analyses: Container / Preservative
1 - 6 L i t e r C a n i s t e r / N o n e
Holding Time Analysis 60 Days 1 VOCs in Air at Ambient Levels by GC/MS
Sample Coiyiments:
(N/A)
C) -0
Vis&k -SlAO
EWxV -50
c m * - 5 i Q i
: fVRDL I M5
Py&d Trieste.
Sample Collected By: U5GS
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 6787 Sample Number: 2 QC Code: Matrix: Air Tag ID: 6787-2-_
Project ID: TH07PZ01 Project Manager: Tonya Howell Project Desc: Oak Grove Village well - RA sampling
City: Oak Grove State: Missouri Program: Superfund
Site Name: OAK GROVE VILLAGE WELL - OAK GROVE VILLAGE WELL Site ID: 07PZ Site OU: 01
Location Desc:
Expected Cone:
Latitude:
Longitude:
External Sample Number:
(or Circle One: Low Medium High) Date
Sample Collection: Start: fc \S End: Ib D9>! \S
Time(24 hr)
Laboratory Analyses: Container Preservative
1 - 6 Liter Canister None Holding Time Analysis
60 Days 1 VOCs in Air at Ambient Levels by GC/MS
Sample Comments:
(N/A)
-Iv\\\TaV 6 o
oairv# 59H?
rUcjf RROL J5 5
Sample Collected By: USGS
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 6787 Sample Number: 3 QC Code: Matrix: Air Tag ID: 6787-3-_
Project ID: TH07PZ01 Project Manager: Tonya Howell Project Desc: Oak Grove Village well - RA sampling
City: Oak Grove State: Missouri Program: Superfund
Site Name: OAK GROVE VILLAGE WELL - OAK GROVE VILLAGE WELL Site ID: 07PZ Site OU: 01
Location Desc:
Expected Cone:
Latitude:
Longitude:
Inn! External Sample Number:
(or Circle One: Low Medium High) Date Time(24 hr)
Sample Collection: Start: Ql/22/IS UriJj?
End: (gj&t\5 LL:_2D
Laboratory Analyses: Container Preservative
1 - 6 L i t e r C a n i s t e r N o n e
Holding Time Analysis
60 Days 1 VOCs in Air at Ambient Levels by GC/MS
Sample Comments:
(N/A)
-0
fYkU-
Sample Collected By: USGS
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 6787 Sample Number: 4 QC Code: Matrix: Air Tag ID: 6787-4-_
Project ID: TH07PZ01 Project Manager: Tonya Howell Project Desc: Oak Grove Village well - RA sampling
City: Oak Grove State: Missouri Program: Superfund
Site Name: OAK GROVE VILLAGE WELL - OAK GROVE VILLAGE WELL Site ID: 07PZ Site OU: 01
Location Desc: SvVQ
Expected Cone:
Latitude:
Longitude:
External Sample Number:
(or Circle One: Low Medium High) Date
Sample Collection: Start: (b_/22/J5
End: Co \ S
Time(24 hr)
I z . o o
U_:_L3
Laboratory Analyses: Container Preservative
1 - 6 L i t e r C a n i s t e r N o n e Holding Time Analysis
60 Days 1 VOCs in Air at Ambient Levels by GC/MS
Sample Comments:
(N/A)
*Xw\V\<x\ '• 0
car# iu4q
Rec^t (\«.t>L 1%
- ' i - D
Sample Collected By: USGS
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 6787 Sample Number: 5 QC Code: Matrix: Air Tag ID: 6787-5-
Project ID: TH07PZ01 Project Manager: Tonya Howell Project Desc: Oak Grove Village well - RA sampling
City: Oak Grove State: Missouri Program: Superfund
Site Name: OAK GROVE VILLAGE WELL - OAK GROVE VILLAGE WELL Site ID: 07PZ Site OU: 01
Location Desc:
Expected Cone:
Latitude:
Longitude:
External Sample Number:
(or Circle One: Low Medium High) Date
Sample Collection: Start: (b /Q£t/&5
End: £l/23/L5
Time(24 hr)
U_:Q4?
Laboratory Analyses: Container Preservative
1 - 6 L i t e r C a n i s t e r N o n e
Holding Time Analysis
60 Days 1 VOCs in Air at Ambient Levels by GC/MS
Sample Comments:
(N/A)
VlflLUWW
"TaMOA 0 0
l < \ O
Cfll# 5112.
IKQ# KtO
- 5 - 0
Sample Collected By: USGS
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 6787 Sample Number: 6 QC Code: Matrix: Air Tag ID: 6787-6-
Project ID: TH07PZ01 Project Manager: Tonya Howell Project Desc: Oak Grove Village well - RA sampling
City: Oak Grove State: Missouri Program: Superfund
Site Name: OAK GROVE VILLAGE WELL - OAK GROVE VILLAGE WELL Site ID: 07PZ Site OU: 01
Location Desc:
Expected Cone:
Latitude:
Longitude:
torn
External Sample Number:
(or Circle One: Low Medium High) Date
Sample Collection: Start: (0/2*2/ VS
End:
Time(24 hr)
lL:^5
\!j_QD
Laboratory Analyses: Container Preservative
1 - 6 L i t e r C a n i s t e r N o n e
Holding Time Analysis
60 Days 1 VOCs in Air at Ambient Levels by GC/MS
Sample Comments:
(N/A)
Vonxwx
£^\0\Jy. "3)0 0
<£vm»S - 5 0
cjk\\4 S\%
xm
14%
Sample Collected By: USGS
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 6787 Sample Number: 7 QC Code: Matrix: Air Tag ID: 6787-7-
Project ID: TH07PZ01 Project Manager: Tonya Howell Project Desc: Oak Grove Village well - RA sampling
City: Oak Grove State: Missouri Program: Superfund
Site Name: OAK GROVE VILLAGE WELL - OAK GROVE VILLAGE WELL Site ID: 07PZ Site OU: 01
Location Desc:
Expected Cone:
Latitude:
Longitude:
External Sample Number:
(or Circle One: Low Medium High) Date
Sample Collection: Start: (b fZ2-! \5
End: <b £3/ \5
Time(24 hr)
0_:jU5
IL:_3T-
Laboratory Analyses: Container Preservative
1 - 6 L i t e r C a n i s t e r N o n e
Holding Time Analysis 60 Days 1 VOCs in Air at Ambient Levels by GC/MS
Sample Comments:
(N/A)
TvnASQY - D 0
gola^F 2<3<8(Q
ftdoi 156
"T.0! 0
VaajslX' "1-5
Sample Collected By: USGS
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 6787 Sample Number: 8 QC Code: Matrix: Air Tag ID: 6787-8-
Project ID: TH07PZ01 Project Manager: Tonya Howell Project Desc: Oak Grove Village well - RA sampling
City: Oak Grove State: Missouri Program: Superfund
Site Name: OAK GROVE VILLAGE WELL - OAK GROVE VILLAGE WELL Site ID: 07PZ Site OU: 01
Location Desc:
Expected Cone:
Latitude:
Longitude:
G\<k fcehp
External Sample Number:
(or Circle One: Low Medium High) Date
Sample Collection: Start: Co /2lA,S
End: G /2VIS
Time(24 hr)
i2.: .20
Laboratory Analyses: Container Preservative
1 - 6 L i t e r C a n i s t e r N o n e
Holding Time Analysis
60 Days 1 VOCs in Air at Ambient Levels by GC/MS
Sample Comments:
(N/A)
"Lot\YOi\ ' 0-0
•• - 50 .0
O.O
fttPL \5H
Sample Collected By: USGS
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 6787 Sample Number: 9 QC Code: Matrix: Air Tag ID: 6787-9-_
Project ID: TH07PZ01 Project Manager: Tonya Howell Project Desc: Oak Grove Village well - RA sampling
City: Oak Grove State: Missouri Program: Superfund
Site Name: OAK GROVE VILLAGE WELL - OAK GROVE VILLAGE WELL Site ID: 07PZ Site OU: 01
Location Desc:
Expected Cone:
Latitude:
Longitude:
External Sample Number:
(or Circle One: Low Medium High) Date Time(24 hr)
Sample Collection: Start: (b /22/ \S"
End: U :
Laboratory Analyses: Container Preservative
1 - 6 Liter Canister None
Holding Time Analysis
60 Days 1 VOCs in Air at Ambient Levels by GC/MS
Sample Comments:
(N/A)
TKtVvBiL' 0-0
" M - 0
C(W$f
M£>L 158
• -CoO
Sample Collected By: USGS
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 6787 Sample Number: 10 QC Code: Matrix: Air Tag ID: 6787-10-_
Project ID: JH07PZ01 Project Manager: Tonya Howell Project Desc: Oak Grove Village well - RA sampling
City: Oak Grove State: Missouri Program: Superfund
Site Name: OAK GROVE VILLAGE WELL - OAK GROVE VILLAGE WELL Site ID: 07PZ Site OU: 01
Location Desc:
Expected Cone:
Latitude:
Longitude:
External Sample Number:
(or Circle One: Low Medium High) Date
Sample Collection: Start: _fi>/22/J5
End: fc/2-3/ \f7
Time(24 hr)
\L:JD
Laboratory Analyses: Container Preservative
1 - 6 Liter Canister None
Holding Time Analysis 60 Days 1 VOCs in Air at Ambient Levels by GC/MS
Sample Comments:
(N/A)
M a c vjluwx
~XVMfrq\ : ~\.0
-2>\.0
VayvoS * - \ .*0
Sample Collected By: USGS
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 6787 Sample Number: 12 QC Code: Matrix: Air Tag ID: 6787-12-_
Project ID: TH07PZ01 Project Manager: Tonya Howell Project Desc: Oak Grove Village well - RA sampling
City: Oak Grove State: Missouri Program: Superfund
Site Name: OAK GROVE VILLAGE WELL - OAK GROVE VILLAGE WELL Site ID: 07PZ Site OU: 01
Location Desc:
Expected Cone:
Latitude:
Longitude:
External Sample Number:
(or Circle One: Low Medium High)
" n k l \ H I U . I
Date
Sample Collection: Start: ftk/34/ IS
End: Ob/2$±5
Time(24 hr)
li:_UO
Laboratory Analyses: Container Preservative
1 - 6 L i t e r C a n i s t e r N o n e
Holding Time Analysis 60 Days 1 VOCs in Air at Ambient Levels by GC/MS
WTf Sample Comments:
(N/A)
~lv\vVvoii. O.O # : \S\
djLplQQ ~ ^)0? ,Q
" — (dy0
Sample Collected By: USGS
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 6787 Sample Number: 13 QC Code: Matrix: Air Tag ID: 6787-13-
Project ID: TH07PZ01 Project Manager: Tonya Howell Project Desc: Oak Grove Village well - RA sampling
City: Oak Grove State: Missouri Program: Superfund
Site Name: OAK GROVE VILLAGE WELL - OAK GROVE VILLAGE WELL Site ID: 07PZ Site OU: 01
f e r l l v ^ Location Desc: ,s^e
Expected Cone:
Latitude:
Longitude:
External Sample Number: 3^^
(or Circle One: Low Medium High) Date
<ea£)^lT*-
Laboratory Analyses: ^Container Preservative
1 - 6 L i t e r C a n i s t e r N o n e
Sample Collection: Start: Ok /Q2M/ 15
End: 6fo/12SM5
Time(24 hr)
iy.:.Q3c
Holding Time
60 Days
Analysis
1 VOCs in Air at Ambient Levels by GC/MS
Sample Comments:
(N/A)
1WVICL\ ~ 10 in $
i j k \ •
/ W p L / s l
I.
Sample Collected By: USGS
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
ASR Number: 6787 Sample Number: 14 QC Code: Matrix: Air Tag ID: 6787-14-
Project ID: TH07PZ01 Project Manager: Tonya Howell Project Desc: Oak Grove Village well - RA sampling
City: Oak Grove State: Missouri Program: Superfund
Site Name: OAK GROVE VILLAGE WELL - OAK GROVE VILLAGE WELL Site ID: 07PZ Site OU: 01
Location Desc: 6\£l Shop
External Sample Number: ft- WnM rt^juJajoR
Expected Cone:
Latitude:
Longitude:
(or Circle One: Low Medium High) Date
Sample Collection: Start: 734/ \5 End: OJh/aViS
Time(24 hr)
l b - . 3 D
IV 5>
Laboratory Analyses: Container Preservative
1 - 6 L i t e r C a n i s t e r None
Holding Time Analysis
60 Days 1 VOCs in Air at Ambient Levels by GC/MS
Sample Comments:
(N/A)
1UYVv^\ % Key
Sample Collected By: USGS
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
Tag ID: 6787^S~_ J* aRD ASR Number: 6787 Sample Number: QC Code: i r j Matrix: Air
Project ID: TH07PZ01 Project Manager: Tonya Howell Project Desc: Oak Grove Village well - RA sampling
City: Oak Grove State: Missouri Program: Superfund
Site Name: OAK GROVE VILLAGE WELL - OAK GROVE VILLAGE WELL Site ID: 07PZ Site OU: 01
G \SX- S h o p Fi ft (WXi ta-U, Location Desc:
Expected Cone:
Latitude:
Longitude:
External Sample Number: ^%2-f) L IH-T ^
(or Circle One: Low Medium High) Date
Sample Collection: Start: Qb 7^4/15
End: (&J25/\S
Time(24 hr)
Laboratory Analyses: Container
1 - 6 L i t e r C a n i s t e r Preservative
None
Holding Time Analysis
60 Days 1 VOCs in Air at Ambient Levels by GC/MS
Sample Comments:
(N/A)
TA'VHgV. 0-b iv\frj
- f m i " . ' l 4 5
C
mjlwv
Sample Collected By: USGS
1 of 1
Sample Collection Field Sheet US EPA Region 7 Kansas City, KS
\5 ASR Number: 6787 Sample Number: ,~3r6T QC Code: Matrix: Air
15 Tag ID: 6787-3r6-_
Project ID: TH07PZ01 Project Manager: Tonya Howell Project Desc: Oak Grove Village well - RA sampling
City: Oak Grove State: Missouri Program: Superfund
Site Name: OAK GROVE VILLAGE WELL - OAK GROVE VILLAGE WELL Site ID: 07PZ Site OU: 01
Clo i d W ve^l~ — ' — —
External Sample Number:
Location Desc: \a\orv
Expected Cone:
Latitude:
Longitude:
(or Circle One: Low Medium High) Date
Sample Collection: Start: Ob /i?M/ IS End: Q&yZ^AS
Time(24 hr)
I4:_y0
Laboratory Analyses: Container
1 - 6 L i t e r C a n i s t e r
Preservative
None
Holding Time Analysis 60 Days 1 VOCs in Air at Ambient Levels by GC/MS
Sample Comments:
(N/A)
TvmVsoA-' 0>D * n\^
fi-wuGL
-j-\ tyA : .M.
Sample Collected By: USGS
1 of 1