dear timothy farrell: 1700 elm street - suite 200 november ... · #=cp# certifications pace project...
TRANSCRIPT
#=CL#
November 04, 2016
LIMS USE: FR - TIMOTHY FARRELLLIMS OBJECT ID: 10366725
10366725Project:Pace Project No.:
RE:
Timothy FarrellMinerva CSD1466 County Route 29Olmstedville, NY 12857
Minerva Central
Dear Timothy Farrell:Enclosed are the analytical results for sample(s) received by the laboratory on October 17, 2016.The results relate only to the samples included in this report. Results reported herein conform to themost current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,where applicable, unless otherwise noted in the body of the report.
Samples, in the electronic data deliverable (EDD) that accompanied this report, were flagged yellowif they exceeded the NYSDOH 15 ppb action level.
The space designated for the sampler on the chain of custody (COC) indicates if these sampleswere collected by Pace Analytical or were collected by the school district and just relinquished toPace Analytical.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Amanda [email protected] Manager
Enclosures
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC1700 Elm Street - Suite 200
Minneapolis, MN 55414(612)607-1700
Page 1 of 21
#=CP#
CERTIFICATIONS
Pace Project No.:Project:
10366725Minerva Central
Minnesota Certification IDs1700 Elm Street SE Suite 200, Minneapolis, MN 55414Alaska Certification UST-107525 N 8th Street, Salina, KS 67401A2LA Certification #: 2926.01Alaska Certification #: UST-078Alaska Certification #MN00064Alabama Certification #40770Arizona Certification #: AZ-0014Arkansas Certification #: 88-0680California Certification #: 01155CAColorado Certification #PaceConnecticut Certification #: PH-0256EPA Region 8 Certification #: 8TMS-LFlorida/NELAP Certification #: E87605Guam Certification #:14-008rGeorgia Certification #: 959Georgia EPD #: PaceIdaho Certification #: MN00064Hawaii Certification #MN00064Illinois Certification #: 200011Indiana Certification#C-MN-01Iowa Certification #: 368Kansas Certification #: E-10167Kentucky Dept of Envi. Protection - DW #90062Kentucky Dept of Envi. Protection - WW #:90062Louisiana DEQ Certification #: 3086Louisiana DHH #: LA140001Maine Certification #: 2013011Maryland Certification #: 322
Michigan DEPH Certification #: 9909Minnesota Certification #: 027-053-137Mississippi Certification #: PaceMontana Certification #: MT0092Nevada Certification #: MN_00064Nebraska Certification #: PaceNew Jersey Certification #: MN-002New York Certification #: 11647North Carolina Certification #: 530North Carolina State Public Health #: 27700North Dakota Certification #: R-036Ohio EPA #: 4150Ohio VAP Certification #: CL101Oklahoma Certification #: 9507Oregon Certification #: MN200001Oregon Certification #: MN300001Pennsylvania Certification #: 68-00563Puerto Rico CertificationSaipan (CNMI) #:MP0003South Carolina #:74003001Texas Certification #: T104704192Tennessee Certification #: 02818Utah Certification #: MN000642013-4Virginia DGS Certification #: 251Virginia/VELAP Certification #: PaceWashington Certification #: C486West Virginia Certification #: 382West Virginia DHHR #:9952CWisconsin Certification #: 999407970
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC1700 Elm Street - Suite 200
Minneapolis, MN 55414(612)607-1700
Page 2 of 21
#=SS#
SAMPLE SUMMARY
Pace Project No.:Project:
10366725Minerva Central
Lab ID Sample ID Matrix Date Collected Date Received
10366725001 MCS018 Water 09/27/16 07:35 10/17/16 09:45
10366725002 MCS019 Water 09/27/16 07:10 10/17/16 09:45
10366725003 MCS020 Water 09/27/16 07:10 10/17/16 09:45
10366725004 MCS021 Water 09/27/16 07:25 10/17/16 09:45
10366725005 MCS022 Water 09/27/16 07:30 10/17/16 09:45
10366725006 MCS023 Water 09/27/16 07:30 10/17/16 09:45
10366725007 MCS024 Water 09/27/16 07:30 10/17/16 09:45
10366725008 MCS025 Water 09/27/16 07:28 10/17/16 09:45
10366725009 MCS026 Water 09/27/16 07:25 10/17/16 09:45
10366725010 MCS027 Water 09/27/16 07:05 10/17/16 09:45
10366725011 MCS028 Water 09/27/16 07:05 10/17/16 09:45
10366725012 MCS029 Water 09/27/16 07:00 10/17/16 09:45
10366725013 MCS030 Water 09/27/16 06:50 10/17/16 09:45
10366725014 MCS031 Water 09/27/16 06:50 10/17/16 09:45
10366725015 MCS032 Water 09/27/16 06:50 10/17/16 09:45
10366725016 MCS033 Water 09/27/16 06:50 10/17/16 09:45
10366725017 MCS034 Water 09/27/16 06:50 10/17/16 09:45
10366725018 MCS035 Water 09/27/16 06:55 10/17/16 09:45
10366725019 MCS036 Water 09/27/16 06:55 10/17/16 09:45
10366725020 MCS040 Water 09/27/16 07:20 10/17/16 09:45
10366725021 MCS041 Water 09/27/16 07:20 10/17/16 09:45
10366725022 MCS042 Water 09/27/16 07:25 10/17/16 09:45
10366725023 MCS043 Water 09/27/16 07:25 10/17/16 09:45
10366725024 MCS044 Water 09/27/16 07:10 10/17/16 09:45
10366725025 MCS045 Water 09/27/16 07:10 10/17/16 09:45
10366725026 MCS047 Water 09/27/16 07:13 10/17/16 09:45
10366725027 MCS048 Water 09/27/16 07:13 10/17/16 09:45
10366725028 MCS049 Water 09/27/16 07:13 10/17/16 09:45
10366725029 MCS050 Water 09/27/16 07:15 10/17/16 09:45
10366725030 MCS051 Water 09/27/16 07:35 10/17/16 09:45
10366725031 MCS052 Water 09/27/16 07:35 10/17/16 09:45
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC1700 Elm Street - Suite 200
Minneapolis, MN 55414(612)607-1700
Page 3 of 21
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:Project:
10366725Minerva Central
Lab ID Sample ID MethodAnalytesReported LaboratoryAnalysts
10366725001 MCS018 EPA 200.8 1 PASI-MRJS
10366725002 MCS019 EPA 200.8 1 PASI-MRJS
10366725003 MCS020 EPA 200.8 1 PASI-MRJS
10366725004 MCS021 EPA 200.8 1 PASI-MRJS
10366725005 MCS022 EPA 200.8 1 PASI-MRJS
10366725006 MCS023 EPA 200.8 1 PASI-MRJS
10366725007 MCS024 EPA 200.8 1 PASI-MRJS
10366725008 MCS025 EPA 200.8 1 PASI-MRJS
10366725009 MCS026 EPA 200.8 1 PASI-MRJS
10366725010 MCS027 EPA 200.8 1 PASI-MRJS
10366725011 MCS028 EPA 200.8 1 PASI-MRJS
10366725012 MCS029 EPA 200.8 1 PASI-MRJS
10366725013 MCS030 EPA 200.8 1 PASI-MRJS
10366725014 MCS031 EPA 200.8 1 PASI-MRJS
10366725015 MCS032 EPA 200.8 1 PASI-MTT3
10366725016 MCS033 EPA 200.8 1 PASI-MRJS
10366725017 MCS034 EPA 200.8 1 PASI-MAJM
10366725018 MCS035 EPA 200.8 1 PASI-MRJS
10366725019 MCS036 EPA 200.8 1 PASI-MRJS
10366725020 MCS040 EPA 200.8 1 PASI-MRJS
10366725021 MCS041 EPA 200.8 1 PASI-MWBS
10366725022 MCS042 EPA 200.8 1 PASI-MWBS
10366725023 MCS043 EPA 200.8 1 PASI-MWBS
10366725024 MCS044 EPA 200.8 1 PASI-MWBS
10366725025 MCS045 EPA 200.8 1 PASI-MWBS
10366725026 MCS047 EPA 200.8 1 PASI-MWBS
10366725027 MCS048 EPA 200.8 1 PASI-MWBS
10366725028 MCS049 EPA 200.8 1 PASI-MWBS
10366725029 MCS050 EPA 200.8 1 PASI-MWBS
10366725030 MCS051 EPA 200.8 1 PASI-MWBS
10366725031 MCS052 EPA 200.8 1 PASI-MWBS
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC1700 Elm Street - Suite 200
Minneapolis, MN 55414(612)607-1700
Page 4 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:Project:
10366725Minerva Central
Sample: MCS018 Lab ID: 10366725001 Collected: 09/27/16 07:35 Received: 10/17/16 09:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 12.6 ug/L 10/28/16 23:03 7439-92-10.10 1
Sample: MCS019 Lab ID: 10366725002 Collected: 09/27/16 07:10 Received: 10/17/16 09:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 2.3 ug/L 10/28/16 23:21 7439-92-10.10 1
Sample: MCS020 Lab ID: 10366725003 Collected: 09/27/16 07:10 Received: 10/17/16 09:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 2.2 ug/L 10/28/16 23:24 7439-92-10.10 1
Sample: MCS021 Lab ID: 10366725004 Collected: 09/27/16 07:25 Received: 10/17/16 09:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 4.6 ug/L 10/28/16 23:27 7439-92-10.10 1
Sample: MCS022 Lab ID: 10366725005 Collected: 09/27/16 07:30 Received: 10/17/16 09:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 1.5 ug/L 10/28/16 23:30 7439-92-10.10 1
Sample: MCS023 Lab ID: 10366725006 Collected: 09/27/16 07:30 Received: 10/17/16 09:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 3.6 ug/L 10/28/16 23:33 7439-92-10.10 1
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2016 01:17 PM
Pace Analytical Services, LLC1700 Elm Street - Suite 200
Minneapolis, MN 55414(612)607-1700
Page 5 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:Project:
10366725Minerva Central
Sample: MCS024 Lab ID: 10366725007 Collected: 09/27/16 07:30 Received: 10/17/16 09:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 2.7 ug/L 10/28/16 23:36 7439-92-10.10 1
Sample: MCS025 Lab ID: 10366725008 Collected: 09/27/16 07:28 Received: 10/17/16 09:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 3.3 ug/L 10/28/16 23:39 7439-92-10.10 1
Sample: MCS026 Lab ID: 10366725009 Collected: 09/27/16 07:25 Received: 10/17/16 09:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.72 ug/L 10/28/16 23:42 7439-92-10.10 1
Sample: MCS027 Lab ID: 10366725010 Collected: 09/27/16 07:05 Received: 10/17/16 09:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.90 ug/L 10/28/16 23:51 7439-92-10.10 1
Sample: MCS028 Lab ID: 10366725011 Collected: 09/27/16 07:05 Received: 10/17/16 09:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 4.4 ug/L 10/28/16 23:54 7439-92-10.10 1
Sample: MCS029 Lab ID: 10366725012 Collected: 09/27/16 07:00 Received: 10/17/16 09:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 2.7 ug/L 10/28/16 23:57 7439-92-10.10 1
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2016 01:17 PM
Pace Analytical Services, LLC1700 Elm Street - Suite 200
Minneapolis, MN 55414(612)607-1700
Page 6 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:Project:
10366725Minerva Central
Sample: MCS030 Lab ID: 10366725013 Collected: 09/27/16 06:50 Received: 10/17/16 09:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 179 ug/L 10/29/16 00:00 7439-92-10.10 1
Sample: MCS031 Lab ID: 10366725014 Collected: 09/27/16 06:50 Received: 10/17/16 09:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 367 ug/L 10/29/16 00:03 7439-92-10.10 1
Sample: MCS032 Lab ID: 10366725015 Collected: 09/27/16 06:50 Received: 10/17/16 09:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 1380 ug/L 10/31/16 15:44 7439-92-11.0 10
Sample: MCS033 Lab ID: 10366725016 Collected: 09/27/16 06:50 Received: 10/17/16 09:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 202 ug/L 10/29/16 00:09 7439-92-10.10 1
Sample: MCS034 Lab ID: 10366725017 Collected: 09/27/16 06:50 Received: 10/17/16 09:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8 Preparation Method: EPA 200.8200.8 MET ICPMS
Lead 1270 ug/L 11/02/16 16:20 7439-92-110/31/16 11:091.0 10
Sample: MCS035 Lab ID: 10366725018 Collected: 09/27/16 06:55 Received: 10/17/16 09:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 72.2 ug/L 10/29/16 00:12 7439-92-10.10 1
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2016 01:17 PM
Pace Analytical Services, LLC1700 Elm Street - Suite 200
Minneapolis, MN 55414(612)607-1700
Page 7 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:Project:
10366725Minerva Central
Sample: MCS036 Lab ID: 10366725019 Collected: 09/27/16 06:55 Received: 10/17/16 09:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 13.2 ug/L 10/29/16 00:15 7439-92-10.10 1
Sample: MCS040 Lab ID: 10366725020 Collected: 09/27/16 07:20 Received: 10/17/16 09:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 5.5 ug/L 10/29/16 00:18 7439-92-10.10 1
Sample: MCS041 Lab ID: 10366725021 Collected: 09/27/16 07:20 Received: 10/17/16 09:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 17.4 ug/L 11/04/16 12:12 7439-92-10.10 1
Sample: MCS042 Lab ID: 10366725022 Collected: 09/27/16 07:25 Received: 10/17/16 09:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 8.0 ug/L 11/04/16 12:16 7439-92-10.10 1
Sample: MCS043 Lab ID: 10366725023 Collected: 09/27/16 07:25 Received: 10/17/16 09:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 2.6 ug/L 11/04/16 12:17 7439-92-10.10 1
Sample: MCS044 Lab ID: 10366725024 Collected: 09/27/16 07:10 Received: 10/17/16 09:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 21.7 ug/L 11/04/16 12:18 7439-92-10.10 1
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2016 01:17 PM
Pace Analytical Services, LLC1700 Elm Street - Suite 200
Minneapolis, MN 55414(612)607-1700
Page 8 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:Project:
10366725Minerva Central
Sample: MCS045 Lab ID: 10366725025 Collected: 09/27/16 07:10 Received: 10/17/16 09:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 2.3 ug/L 11/04/16 12:19 7439-92-10.10 1
Sample: MCS047 Lab ID: 10366725026 Collected: 09/27/16 07:13 Received: 10/17/16 09:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 3.1 ug/L 11/04/16 12:23 7439-92-10.10 1
Sample: MCS048 Lab ID: 10366725027 Collected: 09/27/16 07:13 Received: 10/17/16 09:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 4.4 ug/L 11/04/16 12:24 7439-92-10.10 1
Sample: MCS049 Lab ID: 10366725028 Collected: 09/27/16 07:13 Received: 10/17/16 09:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 3.9 ug/L 11/04/16 12:25 7439-92-10.10 1
Sample: MCS050 Lab ID: 10366725029 Collected: 09/27/16 07:15 Received: 10/17/16 09:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 0.75 ug/L 11/04/16 12:26 7439-92-10.10 1
Sample: MCS051 Lab ID: 10366725030 Collected: 09/27/16 07:35 Received: 10/17/16 09:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 4.8 ug/L 11/04/16 12:27 7439-92-10.10 1
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2016 01:17 PM
Pace Analytical Services, LLC1700 Elm Street - Suite 200
Minneapolis, MN 55414(612)607-1700
Page 9 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:Project:
10366725Minerva Central
Sample: MCS052 Lab ID: 10366725031 Collected: 09/27/16 07:35 Received: 10/17/16 09:45 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 200.8200.8 MET ICPMS, DW
Lead 8.5 ug/L 11/04/16 12:28 7439-92-10.10 1
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2016 01:17 PM
Pace Analytical Services, LLC1700 Elm Street - Suite 200
Minneapolis, MN 55414(612)607-1700
Page 10 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:Project:
10366725Minerva Central
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:QC Batch Method:
Analysis Method:Analysis Description:
442355EPA 200.8
EPA 200.8ICPMS Metals, Drinking Water
Associated Lab Samples: 10366725001, 10366725002, 10366725003, 10366725004, 10366725005, 10366725006, 10366725007,10366725008, 10366725009, 10366725010, 10366725011, 10366725012, 10366725013, 10366725014,10366725015, 10366725016, 10366725018, 10366725019, 10366725020
Parameter UnitsBlankResult
ReportingLimit Qualifiers
METHOD BLANK: 2410054Associated Lab Samples: 10366725001, 10366725002, 10366725003, 10366725004, 10366725005, 10366725006, 10366725007,
10366725008, 10366725009, 10366725010, 10366725011, 10366725012, 10366725013, 10366725014,10366725015, 10366725016, 10366725018, 10366725019, 10366725020
Matrix: Water
Analyzed
Lead ug/L ND 0.10 10/28/16 22:39
Parameter UnitsLCS
Result% RecLimits Qualifiers% RecConc.
2410055LABORATORY CONTROL SAMPLE:LCSSpike
Lead ug/L 110100 110 85-115
Parameter UnitsMS
Result% RecLimits Qual% RecConc.
2413799MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpikeResult
10366725001
2413800
MSDResult
MSD% Rec RPD RPD
MaxMSDMSSpikeConc.
Lead ug/L 100 101 70-130104 3 2010012.6 114 117
Parameter UnitsMS
Result% RecLimits Qualifiers% RecConc.
2413801MATRIX SPIKE SAMPLE:MSSpike
Result10366725020
Lead ug/L 108100 103 70-1305.5
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2016 01:17 PM
Pace Analytical Services, LLC1700 Elm Street - Suite 200
Minneapolis, MN 55414(612)607-1700
Page 11 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:Project:
10366725Minerva Central
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:QC Batch Method:
Analysis Method:Analysis Description:
442364EPA 200.8
EPA 200.8ICPMS Metals, Drinking Water
Associated Lab Samples: 10366725021, 10366725022, 10366725023, 10366725024, 10366725025, 10366725026, 10366725027,10366725028, 10366725029, 10366725030, 10366725031
Parameter UnitsBlankResult
ReportingLimit Qualifiers
METHOD BLANK: 2410092Associated Lab Samples: 10366725021, 10366725022, 10366725023, 10366725024, 10366725025, 10366725026, 10366725027,
10366725028, 10366725029, 10366725030, 10366725031
Matrix: Water
Analyzed
Lead ug/L ND 0.10 11/04/16 12:09
Parameter UnitsLCS
Result% RecLimits Qualifiers% RecConc.
2410093LABORATORY CONTROL SAMPLE:LCSSpike
Lead ug/L 105100 105 85-115
Parameter UnitsMS
Result% RecLimits Qual% RecConc.
2431439MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpikeResult
10366725021
2431440
MSDResult
MSD% Rec RPD RPD
MaxMSDMSSpikeConc.
Lead ug/L 100 105 70-130102 3 2010017.4 123 119
Parameter UnitsMS
Result% RecLimits Qualifiers% RecConc.
2431441MATRIX SPIKE SAMPLE:MSSpike
Result10366725031
Lead ug/L 99.9100 91 70-1308.5
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2016 01:17 PM
Pace Analytical Services, LLC1700 Elm Street - Suite 200
Minneapolis, MN 55414(612)607-1700
Page 12 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:Project:
10366725Minerva Central
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:QC Batch Method:
Analysis Method:Analysis Description:
443802EPA 200.8
EPA 200.8200.8 MET
Associated Lab Samples: 10366725017
Parameter UnitsBlankResult
ReportingLimit Qualifiers
METHOD BLANK: 2419974Associated Lab Samples: 10366725017
Matrix: Water
Analyzed
Lead ug/L ND 0.10 11/01/16 17:31
Parameter UnitsLCS
Result% RecLimits Qualifiers% RecConc.
2419975LABORATORY CONTROL SAMPLE:LCSSpike
Lead ug/L 103100 103 85-115
Parameter UnitsMS
Result% RecLimits Qual% RecConc.
2419976MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpikeResult
10366399246
2419977
MSDResult
MSD% Rec RPD RPD
MaxMSDMSSpikeConc.
Lead ug/L M6100 43 70-13044 0 201002100 2140 2140
Parameter UnitsMS
Result% RecLimits Qualifiers% RecConc.
2419978MATRIX SPIKE SAMPLE:MSSpike
Result10366867055
Lead ug/L 108100 99 70-1308.6
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2016 01:17 PM
Pace Analytical Services, LLC1700 Elm Street - Suite 200
Minneapolis, MN 55414(612)607-1700
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#=QL#
QUALIFIERS
Pace Project No.:Project:
10366725Minerva Central
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.ND - Not Detected at or above adjusted reporting limit.J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.MDL - Adjusted Method Detection Limit.PQL - Practical Quantitation Limit.RL - Reporting Limit.S - Surrogate1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte isa combined concentration.Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.LCS(D) - Laboratory Control Sample (Duplicate)MS(D) - Matrix Spike (Duplicate)DUP - Sample DuplicateRPD - Relative Percent DifferenceNC - Not Calculable.SG - Silica Gel - Clean-UpU - Indicates the compound was analyzed for, but not detected.N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - MinneapolisPASI-M
ANALYTE QUALIFIERS
Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.M6
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2016 01:17 PM
Pace Analytical Services, LLC1700 Elm Street - Suite 200
Minneapolis, MN 55414(612)607-1700
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#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:Project:
10366725Minerva Central
Lab ID Sample ID QC Batch Method QC Batch Analytical MethodAnalyticalBatch
10366725001 442355MCS018 EPA 200.810366725002 442355MCS019 EPA 200.810366725003 442355MCS020 EPA 200.810366725004 442355MCS021 EPA 200.810366725005 442355MCS022 EPA 200.810366725006 442355MCS023 EPA 200.810366725007 442355MCS024 EPA 200.810366725008 442355MCS025 EPA 200.810366725009 442355MCS026 EPA 200.810366725010 442355MCS027 EPA 200.810366725011 442355MCS028 EPA 200.810366725012 442355MCS029 EPA 200.810366725013 442355MCS030 EPA 200.810366725014 442355MCS031 EPA 200.810366725015 442355MCS032 EPA 200.810366725016 442355MCS033 EPA 200.810366725018 442355MCS035 EPA 200.810366725019 442355MCS036 EPA 200.810366725020 442355MCS040 EPA 200.8
10366725021 442364MCS041 EPA 200.810366725022 442364MCS042 EPA 200.810366725023 442364MCS043 EPA 200.810366725024 442364MCS044 EPA 200.810366725025 442364MCS045 EPA 200.810366725026 442364MCS047 EPA 200.810366725027 442364MCS048 EPA 200.810366725028 442364MCS049 EPA 200.810366725029 442364MCS050 EPA 200.810366725030 442364MCS051 EPA 200.810366725031 442364MCS052 EPA 200.8
10366725017 443802 444419MCS034 EPA 200.8 EPA 200.8
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2016 01:17 PM
Pace Analytical Services, LLC1700 Elm Street - Suite 200
Minneapolis, MN 55414(612)607-1700
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10/21/16
temp ok
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