dehydration class lecture

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    Dehydration (Drying)

    Drying of foods is an important food processing operation

    used to preserve foods.

    The distinguishing features between drying and

    concentration are the final level of water and nature of theproduct.

    Concentration leaves a liquid food

    Whereas drying typically produces product with water

    content sufficiently low to give solid food.

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    Reasonsfor drying foods

    Drying is used to remove water from foods for two reasons:

    to prevent (or inhibit) micro-organisms and hence preserve the

    food.

    to reduce the weight and bulk of food for cheaper transport and

    storage.

    Historically, there was a need to preserve foods for longer times

    so that food was available during times of limited food production or

    availability.

    Hunters needed a technique to preserve meat for more than a few

    days to ensure a continuous food supply. In the same manner, we

    have techniques that allow us to preserve foods as they are harvested,

    so that we can enjoy them at later times.

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    One of the easiest ways to preserve foods is to remove water,

    since

    microorganisms need water to survive and grow. many chemical reactions require water to proceed.

    Early hunters dried their meat to help maintain a more continuous

    food supply.

    Nowadays, we dry foods for the same reason: to provide a

    continuous supply of foods that we can enjoy at any time.

    Other reasons for drying foods

    Removal of water leaves a product reduced in weight and oftenin bulk. This reduces shipping costs and makes the food supply

    more economical. Dried foods also provide convenience. Dried

    convenience foods may be used for special expedition--type

    (military) foods where weight is a major concern.

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    There are many methods and technologies by which we can

    dehydrate foods.

    We must first understand the nature of water in food products to

    appreciate (realize fully) the difficulties in producing high-

    quality dried products.

    Removal of water from foods is not a difficult task. However,removing the water in such a way that the product regains its

    initial form when rehydrated is not so easy.

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    EFFECTSOF DRYINGON PRODUCT

    QUALITY

    After dehydrating the food cannot reach the original quality.

    There is always some change that gives a loss of quality in the

    product.

    The goal is to minimize these changes, while optimizing process

    efficiency and minimizing costs.

    Several types of changes can occur during drying.

    Two main problems are

    loss and change of flavors, and

    change in physical qualities of dried products.

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    Effect on flavor

    One problem with dried foods is that the flavor of therehydrated product is not the same as that of the original.

    During drying, flavor compounds that are typically more

    volatile than water are removed in the drying process.

    The physical forces that cause water molecules to be removed

    from the food during drying also cause volatile compounds

    (alcohols, aldehydes, ketones, etc.) to be removed.

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    burnt flavor

    Dried products have less of these volatile flavoring compounds

    than the original starting material.

    In addition, the rates of chemical reactions are enhanced at the

    elevated temp., and many of these reactions generate undesired

    flavor compounds.

    For example, the browning reaction (between reducing sugars

    and proteins) is enhanced and generates a burnt flavor.

    (reconstituted milk from a dried powder)

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    Browning

    Other chemical reactions may also take place during drying.

    Browning occurs in many foods which results in color changes.

    Protein denaturation can occur during drying, which causes

    increased viscosity

    Thermal degradation of vitamins and proteins may also

    influence the nutritional status of dried products.

    The extent of these changes depends on the nature of the drying

    process. Some types of dryers produce products having superior

    properties on reconstitution. The instant coffee spray-dried andfreeze-dried is different. Since freeze-drying does not involve a

    vapor-liquid interface, the volatile flavor and aroma compounds

    are not lost during drying, and freeze-dried products have higher

    quality.

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    Dehydrating FruitsAnd Vegetables

    Dehydration of fruit and vegetables is one of the oldest forms of

    food preservation techniques and consists primarily of

    establishments engaged in sun drying or artificially dehydrating

    fruits and vegetables.

    By reducing both the weight and volume of the final productdehydration of fruits and vegetables lowers:

    o the cost of packaging

    o storing, and

    o transportation

    Process Description

    Dried or dehydrated fruits and vegetables can be produced by a

    variety of processes.

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    These processes differ primarily

    by the type of drying method used, which depends on the type of

    food.

    by the type of characteristics of the final product.

    In general, dried or dehydrated fruits and vegetables undergo the

    following process steps:

    o Predrying treatments, such as size selection, peeling, and colorpreservation

    o Drying or dehydration, using natural or artificial methods; and

    o Postdehydration treatments, such as sweating, inspection, and

    packaging. I. Predrying Treatments

    Predrying treatments prepare the raw product for drying or

    dehydration and include raw product (a) preparation and (b) color

    preservation.

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    (a) Raw product preparation includes

    o selection and sorting

    ow

    ashing

    o peeling (some fruits and vegetables)

    o cutting into the appropriate form, and

    o blanching (for some fruits and most vegetables)

    Fruits and vegetables are selected; sorted according to size,maturity, and soundness; and then washed to remove dust, dirt, insect

    matter, mold spores, plant parts, and other material that might

    contaminate or affect the color, aroma, or flavor of the fruit or

    vegetable. Peeling or removal of any undesirable parts follows washing. The

    raw product can be peeled

    o by hand (generally not used in the United States due to high labor

    costs)

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    o with lye or alkali solution

    o with dry caustic and mild abrasion

    o with steam pressureo with high-pressure washers, or

    o with flame peelers

    For fruits, only apples, pears, bananas, and pineapples are usually

    peeled before dehydration.

    Vegetables normally peeled include beets, carrots, parsnips,

    potatoes, onions, and garlic.

    Prunes and grapes are dipped in an alkali solution to remove the

    natural waxy surface coating which enhances the drying process.

    Next, the product is cut into the appropriate shape or form (i. e.,

    halves, wedges, slices, cubes, nuggets, etc.), although some items,

    such as cherries and corn, may by-pass this operation.

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    Flame peeling: A flame peeler utilizes a conveyor belt to transport

    and rotate the material through a furnace heated to temperature

    above 1000 C. The skin (root hairs) is burned off and then removed

    by high-pressure water sprays. Flame peeling is used, for example,

    for peeling onions.

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    Some fruits and vegetables are blanched by immersion in hot water

    (95 to 100 C [203 to 212 F]) or exposure to steam.

    (b) Color preservation The final step in the predehydration treatment is color preservation,

    also known as sulfuring.

    The majority of fruits are treated with sulfur dioxide (SO2) for its

    antioxidant and preservative effects.

    The presence of SO2 is very effective in retarding the browning of

    fruits, which occurs when the enzymes are not inactivated by the

    sufficiently high heat normally used in drying.

    In addition to preventing browning, SO2 treatment reduces the

    destruction ofcarotene and ascorbic acid, which are the important

    nutrients for fruits.

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    Sulfuring dried fruits must be closely controlled so that enough

    sulfur is present to maintain the physical and nutritional properties of

    the product throughout its expected shelf life, but not so large that itadversely affects flavor.

    Some fruits, such as apples, are treated with solutions of sulfite

    (sodium sulfite and sodium bisulfite in approximately equal

    proportions) before dehydration.Although dried fruits commonly use SO2 gas to prevent browning,

    this treatment is not practical for vegetables.

    Most vegetables (potatoes, cabbage, and carrots) are treated with

    sulfite solutions to retard enzymatic browning.

    In addition to color preservation, the presence of a small amount of

    sulfite in blanched, cut vegetables improves storage stability and

    makes it possible to increase the drying temperature during

    dehydration,

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    thus decreasing drying time and increasing the drier capacity without

    exceeding the tolerance for heat damage.

    II. Drying or dehydration

    Drying or dehydration is the removal of the majority of water

    contained in the fruit or vegetable and is the primary stage in the

    production of dehydrated fruits and vegetables.

    Several drying methods are commercially available and the

    selection of the optimal method is determined by:

    o Quality requirements

    o Raw material characteristics, ando Economic factors

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    There are three types of drying processes:

    Sun and solar drying

    Atmospheric dehydration including:

    Stationary or batch processes (kiln, tower, and cabinet driers) and

    Continuous processes (tunnel, continuous belt, belt-trough,

    fluidized-bed, explosion puffing*, foam-mat*, spray, drum, and

    microwave heated driers) and

    Subatmospheric dehydration (vacuum shelf, vacuum belt,

    vacuum drum, and freeze driers)

    Sun and solar drying

    Sun drying (used almost exclusively for fruit) and solar drying

    (used for fruit and vegetables) of foods use the power of the sun to

    remove the moisture from the product.

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    In explosion puffing the partially dried (15 to 35 wt.-% moisture)

    vegetable pieces are conveyed into a puffing chamber (gun: the

    chamber has a quick opening lid) which is brought to a predetermined

    pressure. When the water contained within the pieces is heated above

    its atmospheric boiling point in the gun, pressure builds up and when

    the pieces are instantly discharged, the flushing of water vapors from

    within each piece creates a porous structure. The porous structure

    permits much faster dehydration and rapid rehydration of the dried

    product.

    Carrot and potato cubes made by this method rehydrate in 5-6 min.

    by simmering in water as against 30-60 min. for conventionally air

    dried product.

    (Used for rice and wheat breakfast cereals)

    Explosion puffing*

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    Foam-mat drying*

    Concentrated liquids have be dried by heated air on conveyor driers,

    using a technique known as foam mate drying. The liquid is made into

    a foam, by the addition of a small amount, 1% or less, of a foaming

    agent, such as soya protein, albumin, fatty acid ester of sucrose and

    glycerol monostearate, and the incorporation of air or other gases by

    injection or mixing. The foam is spread in thin layers or strips on a

    wire mesh belt and conveyed through the drier.

    relatively rapid drying can be achieved, of the order of 1 hour in air

    at 100 C, yielding a porous dry product with good rehydration

    properties.

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    Microwave heating occurs between 300 MHz and 300 GHz

    (wavelength 1mm to 1m).

    Microwave heating of a substance by electromagnetic energy

    operating in that frequency range.

    Microwaves themselves do not represent heat but absorbed energy

    is converted into heat inside the product.

    The heating of foods by microwave energy is accomplished both

    by the absorption of microwave energy by dipole water molecules

    and ionic components (often salt) of food.

    As the energy enters the foods, dipolar water molecules try to

    align in the electric field orientation. They oscillate around their

    axis, generating heat within the food, resulting in dehydration.

    Microwave Drying

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    When ionized compounds are subjected to a microwave field, they

    randomly collide with non-ionized groups in an electric field. The

    kinetic energy of these ions is transmitted into heat during thecollisions.

    The depth of the material and type of material being exposed also

    affects penetration.

    The waves bounce from wall to wall, until the product absorbs

    eventually all of the energy. In this manner, the drying rate is

    increased greatly. This type of heating is highly efficient; and power

    utilization efficiencies are generally greater than 70 %.

    Important commercial aspects include the ability to maintain

    color and quality of the natural food. This has been found prevalent

    in potato chips.

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    Sun drying of fruit crops is limited to climates with hot sun and dry

    atmosphere, and to certain fruits, such as prunes, grapes, dates, figs,

    apricots, and pears.

    These crops are processed in substantial quantities without much

    technical aid by simply spreading the fruit on the ground, racks,

    trays, or roofs and exposing them to the sun until dry.

    Advantages of this process are its simplicity and its small capital

    investment.

    Disadvantages include complete dependence on the elements and

    moisture levels no lower than 15 to 20 percent (corresponding to a

    limited shelf life).

    Solar drying utilizes black-painted trays, solar trays, collectors,

    and mirrors to increase solar energy and accelerate drying.

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    Atmospheric dehydration

    Atmospheric forced-air driers artificially dry fruits and vegetables

    o by passing heated air with controlled relative humidity over thefood to be dried, or

    o by passing the food to be dried through the heated air, and is the

    most widely used method of fruit and vegetable dehydration.

    Various devices are used to control air circulation and

    recirculation.

    o Stationary or batch processes include kiln, tower (or stack), and

    cabinet driers.

    o Continuous processes are used mainly for vegetable dehydration

    and include tunnel, continuous belt, belt trough, fluidized-bed,

    explosion puffing, foam-mat, spray, drum, and microwave-heated

    driers.

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    Tunnel driers are the most flexible, efficient, and widely used

    dehydration system available commercially.

    Subatmospheric dehydrationSubatmospheric (or vacuum) dehydration occurs at low air

    pressures and includes vacuum shelf, vacuum drum, vacuum belt, and

    freeze driers.

    The main purpose of vacuum drying is to enable the removal of

    moisture at less than the boiling point under ambient conditions.

    Because of the high installation and operating costs of vacuum

    driers, this process is used for drying raw material that may

    deteriorate as a result of oxidation or may be modified chemically as

    a result of exposure to air at elevated temperatures.

    There are two categories of vacuum driers:

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    In the first category, moisture in the food is evaporated from the

    liquid to the vapor stage, and includes vacuum shelf, vacuum drum,

    and vacuum belt driers.

    In the second category of vacuum driers, the moisture of the food

    is removed from the product by sublimination, which is converting

    ice directly into water vapor.

    The advantages of freeze drying are

    o High flavor retention

    o Maximum retention of nutritional value

    o Minimal damage to the product texture and structure

    o Little change in product shape and color, and

    o A finished product with an open structure that allows fast and

    complete rehydration

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    Disadvantages include

    o High capital investment,

    o High processing costs, and

    o Need for special packing to avoid oxidation and moisture gain in

    the finished product.

    III. Postdehydration treatments

    Treatments of the dehydrated product vary according to the type of

    fruit or vegetable and the intended use of the product.

    These treatments may include

    Sweating

    Screening

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    Inspection,

    Instantization treatments, and

    Packaging.

    Sweating involves holding the dehydrated product in bins or

    boxes to equalize the moisture content.

    Screening removes dehydrated pieces of unwanted size, usually

    called "fines".

    Inspection: The dried product is inspected to remove foreign

    materials, discolored pieces, or other imperfections such as skin,

    carpel, or stem particles.

    Instantization treatments are used to improve the rehydration

    rate of the low-moisture product.

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    Packaging is common to most all dehydrated products and has a

    great deal of influence on the shelf life of the dried product.

    Packaging of dehydrated fruits and vegetables must Protect the product against moisture, light, air, dust, microflora,

    foreign odor, insects, and rodents

    Provide strength and stability to maintain original product size,

    shape, and appearance throughout storage, handling, and marketing Consist of materials that are approved for contact with food. Cost

    is also an important factor in packaging.

    Package types include cans, plastic bags, drums, bins, and cartons,

    and depend on the end-use of the product.

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    Water activity

    Water activity (aw

    ) is defined as the ratio of the vapor pressure

    of water measured at the food surface (Pw) to the saturation

    vapor pressure of pure water at the same temperature (Pw)

    oP

    P

    a!

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    Water activity

    For a cup of water, the vapor pressureover the surface is measured as thesaturation vapor pressure, and aw is 1.

    When there are solutes in the water suchas sugars, salts, etc. the vapor pressureover the water surface is lower than thesaturation vapor pressure, and aw is

    reduced to some value less than 1. Thereduction in water activity depends on thetype of solutes present and their levels.

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    Water Activity

    For food products, the water activity is

    generally less than 1. aw is related to the

    moisture content of the food, the types and

    concentrations of different solutes, and the

    structure or physical characteristics of the food.

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    DRYING METHODS

    1.DirectContact Dryers

    Sun Dryer/Bin Dryer/Kiln Dryer/ Tray or Cabinet Dryer/Tunnel Dryer/Belt or Conveyor Dryer/

    Fluidized Bed Dryer/Rotary Air Dryer/Spray Dryer. 2.IndirectContact Dryers

    Drum Dryer

    3.Infrared or Dielectric Dryers

    Infrared Dryers/Microwave Dryers.

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    Tray or Cabinet Dryer

    The food product placed in a pan is placed

    inside a drying chamber with hot air blowing

    across the product until drying is complete.

    Some of the hot air used for drying may be

    recirculated through the dryer to conserve

    energy However, increased relative humidity

    of the recirculated air decreases dryerefficiency.

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    Tunnel Dryer

    The food product is loaded onto trays that are

    placed into carts. The carts are input at one end

    of the tunnel dryer and move through to the

    outlet. Air blowing within the tunnel causes

    drying at a specified rate, so that the food

    product reaches the exit on completion of

    drying. (1) cocurrent; (2) countercurrent; or (3)mixed flow,

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    Belt or Conveyor Dryer

    Product may also be moved through a dryer by

    placing it on a belt or conveyor. In order to

    extend the time within a conveyor dryer, a

    series of conveyors may be arranged one

    above the other. In this case, product drops

    from an upper conveyor to a lower conveyor.

    air flow can be through the conveyor andthrough the bed of food product laying on the

    conveyor.

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    Fluidized Bed Dryer

    Air flow through a bed of product is sufficient

    to lift the product. Since there is intimate

    contact between air and product drying rates in

    this type of dryer are quite good. This type of

    dryer is limited to granulated powders, or

    small pieces of product. The air velocity

    depends on particle size, density.

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    Rotary Air Dryer

    These dryers are typically arranged ashorizontal cylinders that rotate along theirmain axis. Wet product enters one end of the

    dryer and moves towards the other end by acombination of gravity and the bafflearrangement within the cylinder. As thecylinder rotates, air forced into the cylinder

    blows across the product as it tumbles, to provide effective contact between air andproduct.

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    SPRAY DRYING

    Atomization

    Air Handling

    Dryer Chamber Powder Separation

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    Atomization

    Atomization produces a cloud of droplets with very

    large surface area for drying.

    High pressure nozzle: droplet size is controlled by

    pressure of the fluid food against the nozzle.

    Centrifugal atomizer: Liquid food is pumped into a

    spinning disk, where it is accelerated by centrifugal

    force and expelled from the ends of the disk-shaped

    atomizer, become a cloud of droplets .

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    Air spray atomization

    with high velocity air

    Centrifugal atomization

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    Air Handling

    Ambient air is taken in through a vent and

    heated prior to circulation into the drying

    chamber. Heating can be accomplished in

    several ways. Air can be passed either through

    steam coils or an electric heater to attain

    elevated temperatures, typically between l50

    and 500.

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    Dryer Chamber

    In the residence time of droplets in the spray dryingchamber, the droplets go from a moisture content inthe range of about 40% to only about 5-10%.

    The food droplets are sprayed at the top of thechamber and fall down to the bottom by gravity. Bothair and food droplets enter the chamber at the top andfall to the bottom of it, where air is separated fromdry powder and the product is removed from thedryer.

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    Product quality of Freeze Drying

    The original structure of the food is

    maintained and flavor retention in is excellent.

    The cost of freeze drying is very high.

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    Steps in Freeze Drying

    Freezing.

    Primary Drying.

    Secondary Drying. Heat and Mass Transfer in Freeze Drying

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    Primary Drying

    Sublimation of ice is accomplished by controlling the

    vacuum level in the freeze dryer and through careful

    heat input. A high vacuum is desired to enhance

    sublimation rate. Introduction of heat is to supply energy to a plate on

    which the food is sitting (conduction heating), while

    also providing a radiation source above the product.

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    Sublimation Front

    The ice recedes into the food product as drying

    occurs. This boundary between frozen and

    dried product is called the sublimation front.

    Heat must be transferred into the product to

    this front to promote sublimation, and water

    vapor must then be removed by mass transfer

    through the dried product

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    Secondary Drying

    Once all the ice is sublimed out of the frozen

    food, the secondary drying process begins.

    Heat is continually added, but at a slower rate

    since moisture loss occurs only by diffusion of

    water molecules out of the freeze--dried matrix.

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    Collapse Behavior

    Rapid heat addition causes the temperature ofthe product to exceed its collapse temperature.product becomes sufficiently flowable that it

    "collapses!' During collapse, the pockets whereice crystals have sublimed disappear as thefood slowly flows into these regions. Thiscauses product to have higher density and

    reduces its ability to be rehydrate.

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    VaporCondensor

    A condenser collects the vapors as they exit

    the freeze dryer to enhance efficiency and

    prevent fouling of the vacuum pump.

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