delphi, facility investigation report, appendix c, section 31 · attention: tom tatnall oct 1 %...

51
American Environmental Testing Laboratory -- Inc. 2834 8~2908 North Naomi Street. Burhank, CA 91504. DOHS NO: 1541,LACSDNO: 1018i Tcl: (888) 288-AETL ' (818) 845-8200 - Fax: (818) 845-8840 ' www.aetiah.corn Ordered BY - Haley L Aldrlch Number of Pages 48 50G Souzli Kraemer Blvd. Sulre 370 Date Recelved 10/05/2005 Brea, CA 92821-6723 MECEWrED Date Reported 10/11/2005 Telephone: (714) 985-3434 A t t e n t i o n : Tom T a t n a l l OCT 1 % 2003 Project ID: 32486-000 Project Name: Delshi System Corp. Site: 1201 N. Magnolia Avenue Anaheim, CA 92801 Enclosed please find results of analyses of 2 water and 2 soil samples which were analyzed as specified on the attached chain of custody. If there are any questions, please do not hesitate to call. Checked By: -- Approved By: 9-9 Cyrus Razmara, Ph. D. Laboratory Director

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American Environmental Testing Laboratory -- Inc. 2834 8 ~ 2 9 0 8 North Naomi Street. Burhank, CA 91504. DOHS NO: 1541,LACSDNO: 1018i Tcl : (888) 2 8 8 - A E T L ' (818) 845-8200 - Fax: (818) 845-8840 ' www.aet iah.corn

Ordered BY - Haley L A l d r l c h Number o f Pages 48

50G Souzli K r a e m e r Blvd. S u l r e 370 Date R e c e l v e d 1 0 / 0 5 / 2 0 0 5

B r e a , CA 92821-6723 MECEWrED D a t e R e p o r t e d 1 0 / 1 1 / 2 0 0 5

Te lephone : (714) 985-3434

A t t e n t i o n : Tom T a t n a l l OCT 1 % 2003

P r o j e c t I D : 32486-000 P r o j e c t Name: Delshi System Corp.

S i t e : 1201 N . Magnolia Avenue Anaheim, CA 92801

Enclosed please find results of analyses of 2 water and 2 soil samples which were analyzed as specified on the attached chain of custody. If there are any questions, please do not hesitate to call.

Checked By: -- Approved By: 9-9

Cyrus Razmara, Ph. D. Laboratory Director

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American -. Environmental Testing Laboratory -- Inc. 2834 &21)08 North Naomi Strect. Burbank, CA 9l504.DOIiS NO: 1541,LACSDNO: I0181 Te l : (888) 2 8 8 - A W L - (818) 845-8200 . Fax: (818) 845-8840 - www.ae t Iab .com

ANALYTICAL RESULTS Ordered By S i t e

Telephone : (714)985-3434 Aitn: Tom Tatnall

Page: 2 - Pro 'ec t ID: 32486-000

Method: (8260B), Volatile Organic Compounds by GC/MS (SW846) QC Batch No: 100605

1 - D a t e Prepared -. .. --

Preparation Method-. - ~- 1 . r ~ ~ A m 2 l ~ v ~ e A

/ ".yl,ll" .... -~

I M a t r ~ x - . ~ ~- A o i l i I s o , ! . . .. ... . .. .

ug/Kg_- uglI<g ug/Kg Uirits - .. ~ .~~~ , - . . .- . --

, -" .... .. . --~. .. *-. -

I Bromobeiircne .. . (I'henyl bromide) ~~-

ND ! Bro~nochloronlcthaiic Hromodichloroincthane I 5 . 0 . --

Bromofonn (Tribroniometl~ane) ---- - bi-omomcihsne(~-de) .... ..

ND - ~ ~ ~ - - ~ ---

iiBuly1benzene . 5 . 0 sec-Bulylbcnrenc ... . .. .. - . .....

I -",.Riit\,ll,m~,en~ ND I I l i - Carbon Disulfide

.-

, ~- ~~.~ .. . ...

: ~ h i o i o n ~ c l h a n e ( M ~ l h ~ i . chloride) -~ .,.. 1 1 5 i 2-Chlorotoiuene 5 . 0 1 0 . 0 ND -. . ... .

ND

I - I ,2-~ibromo-3-chloio~~~~a11e (DBCP) 25 50 ND ND ,--~~--~ ~ ~- ND

'' I - ' ND L ~-~~ ~ ~

.. .. . ,

1,2-Dibromoethane (EDB) iDibro~nomctlrane I I,2-Diclilorobenze1,c ---pp-

I ,3-llichlorobenzcnc ... -~ ~~

....... -.

2834 &2908 North Naoini Slrcei, Busbank, CA 91504 .DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETI.. (818) 845-8200. Fax: (818) 845-8840 www.aellab.com

Page: 3

Pro'ect ID: 32486-000 m Cor .

Method: (8260B), Volatile Organic Compounds by GCIMS (SW846) QC Batch No: 100605

ND , I _ _ - p _ _ - . , , , . ~ ~ ~ . ~~ .~

1,1,2,2-Tstracl1loroetll~ne 1 5 . 0 ND i N D b~~- . . -. . . -

5 . 0 10.0 ND ND ND Tetrachloroethe~le I

~ ~~, ~ , - ppp-

'l'oluene (Methyl benzene) L..~ 1 0 . 0 ND ! ND ND

I . ..

--+ ND ND 8 ND

American Environmental Testing Laboratory Inc. 2814 &2908 North Naoini Sti-~el, Burbank, CA 91504 -DOHS NO: 1541,LACSDNO: 10181 Tci: (888) 288-AETI.. (818) 845-8200 * Fax: (818) 845-8840. www.aer lah .co~n

ANALYTICAL RESULTS

Page: 4

Project ID: 3 2 4 8 6 - 0 0 0 Pro'ect Name: Delahi S s t e m Cor .

Method: (8260B), Volatile Organic Compounds by GCIMS (SW846) QC Batch No: 100605

American Environmental Testing Laboratory Inc. .-

28348~2908 North Naomi Strset,Burbank,CA 91504.DOHS NO: 1541,IXSDNO: 10181 Ts l : (888) 288-AETL. (818) 845-8200 - F a x : (818) 845-8840 - www.aet lab.com

ANALYTICAL RESULTS

Telephone: (714)985-3434 Attn: Tom Tatnall

Page: 5

Pro'ect ID: 32486-303 ern Cor .

Method: (M801 SG), TPH as Gasoline and Light tIydrocarhons Using GCIFID QC Batch No: 100605

- . Soil I Soil

American Environmental -. Testing Laboratory Inc. 2834&2908 North Naomi Street. Buubank, CA 95504 .DOHS NO: 1541,LACSDNO: 10181 Tcl: (888) 2 8 8 - A W L - (818) 845-8200. Fax: (818) 845-8840 * www.aeclah.com

ANALYTICAL RESULTS

0 South Kraemel- Blvd.

Telephone: (714)985-3434 Ann: Tom Tatilail

Page: 6

Project ID: 3 2 4 8 6 - 0 0 0 L ame: Project li Delphi System Corp.

Method: (MSOlSD), TPII as Diesel and Heavy Hydrocarbons Using GCIFIU)

American Environmental Testing Laboratory Inc. 2834&290X Norlli Naomi Street, BUI-bank, CA 91504 -DOHS NO: 1541,LACSDNO: 10181 Tcl: (888) 288-AETL - (818) 845-8200. Fax: (818) 845-8840. www.acilab.com

-

Ordered By - i-ialey & Aldrich 500 South Kraen~el Blvd

ANALYTICAL RESULTS Site

Telephone: (71 4)985-3434 Attn: Toin Tatnail

Page 7

Project 1I) 32486-000 1 AETL Job Number Submitted Cl~ent I'roject Name. aelphl System Corp. 34830 i i0/05/20C5 I h&A i

Method (M8015D), TPH as Diesel and Heavy Hydrocarbons Using GCIFID QC Batch No 100605

Dale Sampled I- ... . I Date Prepared -~

I Preparation Method - Datc A~ialyzed 1.. ___- - Matrix

Dilution Factor

American Environmental Testing Laboratory Inc. 2834 &2908 North Naonii Street, Burbank, CA 91504.DOHS NO: 1541,LACSIlNO: 10lXl Ycl: (888) 288-AETL (818) 845-8200 - Fan: (818) 845-8840. www.aet1ab.com

ANALYTICAL RESULTS O r d e r e d By Site

Telephone: (714)985-3434 Attn: Toin Tatnail

Page: 8

Project ID: 32486-000 I'roject Name: Delphi System Corp.

~ ~~- ~~~~ ~ ~p~ ~~ ~ . ~ ~

Method: (M8015D), TPH as Diesel and Heavy Hydrocarbons Using GCIFID

American Environmental Testing .. Laboratory Inc. 2814 8.2908 North Naomi Street. Burbank. CA 91504 * DOHS NO: 1541,LACSDNO: 10181

. ,

. ~ ~~~

, Tcl: (888) 2 8 8 - A W L e (818)845-8200 Fax: (818) 845-8840. www.aerlab.com

Ordered Bv

ANALYTICAL RESULTS Site

Telephone: (71 4)985-3434 Attn: Torn Tatnall

Page: 9

Pro'ect ID: 3 2 4 8 6 - 0 0 0

Method: (83 lo), Polynuclear Aromatic IIydrocarbons (SW-846)

American Environmental Testing Laboratory Inc. 28148~2908 North Naoini Streel, Burbank, CA 91504 .DOHS NO: 154I,LACSL>NO: 1OlXi Tel: (888) 288-AETL . (818) 845-8200. Fax: (818) 845-8840. www.aeilah.com

ANALYTICAL RESULTS

Page: 10

Project ID: 32486-000 Pro'ect Name:

Method: 183101. Po!vnuclear Aromatic Svdrocarbons (SW-846)

American Environmental Testing Laboratory Inc. 2834&2908 North Naomi Street, Rul-bank, CA 91504 -DOHS NO: 1541,LACSDNO: 10181 Tel : (888) 288-AETL (818) 845-8200 Fax: (818) 845-8840 - www.aztlab.corn

ANALYTICAL RESULTS Ordered By

Hdfey gL Aldrrch

i O O South I<raenier Rlvd

S i t e

Telephone: (7 14)985-3434 Attn: Tom Tatna l l

Page: 11

Projec t ID: 3 2 4 8 6 - 0 0 0 Pro jec t Name: Del.pi-i System Corp.

Method: (8270C), Semivolatile Organic Compounds by GCIMS (SW-846) QC Batch No: 100605

Benzyl rZ1col1ol

IBis(2-Chloroethoxy) . .- Bis(2-ChloroethyI)e1l1cr Bis(2-chioroisopropyl) ether

Bis(2-elhylhexyi) plitbalate 4-Brornophenyi phenyl ether Butvi benzvl ohilialate

~ - ~~~.

-- 2-Chloronapiilhaiene ~~ -

2-Chiorophenol

4-Chlorophenyi plieiiyl ~ the , - ."'

..... ~ -

Chryscnc I L~ . . .. . :

0.50 ND 1 Di-11-butvl vhihalale

American Environmental Testing Laboratory ..... Inc. 2834 &2908 Nortli Naoini Street, Burbank, CA 91504 .DOHS NO: 1541.LACSDNO: 10181 Tel: (888) 288-AETL 0 (818) 845-8200 Fax: 1818) 845-8840 www.acllab.com

ANALYTICAL RESULTS

Page: 1 2

Prqject ID: 32486-000 Project Name: Delphi System C o r p .

Method: (8270C), Se~llivolatile Organic Compounds by GCIMS (SW-846) QC Batch No: 100605

American Environmental -- Testing Laboratory Inc. 2834 8~2908 Nortli Naoini Street, Burhank, CA 91504 'DOHS NO: l541,1,ACSDNO: 1018i Tcl: (888) 288-AETL * (818) 845-8200. Fax: (818) 845-8840. www.aetlab.com

ANALYTICAL RESULTS

Page: 13

Project ID: 32486-000 Project Name: Delphi Sys t em Carp.

Method: (8270C), Semivolatile Organic Compounds by GCIMS (SW-846) QC Batch No: 100605

American Environmental Testing Laboratory Inc. 28348~2908 North Naoini Street, Burbank. CA 91504 *DOHS NO: 1541,LACSDNO: I0!8! Tel: (888) 288-AETL. (818) 845-8200. Fax: (818) 845-8840 www.aet lab.com

ANALYTICAL RESULTS Ordered By

T e l e p h o n e : (71 4)985-3434 Ann: Tom Tatnall

Page: 1 4

Pro'ect ID: 32486-000 . .

Method: (8270C), Semivolatile Organic Compounds by GCIMS (SW-846) QC Batch No: 100605

Date Sampled Date Prepared -

Units .. -

B e i ~ ~ y l Alcoho! 2 .50 I 5 I ND I 1 2 .50 1 5 3

~~ ~,~~~ . ... . 4- - . .. . 2 .50 I 5 1 ND

~. - - ~ ~ ~ ~ ~ ~ . . . .

4-Bromoulienv! u11envl ether 1 2 .50 1

American Environmental ... Testing Laboratory Inc. 2834 8~2908 North Neomi Streci,Burbank, CA 91504 .DOHS NO: 1541,LACSUNO: 10181 Tcl: (888) 288-AETL - (818) 845-8200. Fax: (8 18) 845.8840 . www.aet lab.com

ANALYTICAL RESULTS

Page: 1 5

Project ID: 3 2 4 8 6 - 0 0 0 Pro'ect Name: Deluhi Svsrern C a r .

Method: (8270C), Semivolatile Organic Compounds by GC/MS (SW-846) QC Batch No: 100605

Date Prepared I ....... . ~ U / U ~ / Z U U ~ 1 I-'reparation Method I - - 3550B ---- -. .. 1 n3+- A ~ ~ I . , ~ O A 10/10/2005 I

lNaphtlialene ..

2-Nitroaniliiie 3-Nitroaniline

......... . -.-

4-Nilruiiniline - - - - ...........

ilrobenzene (ND) ......... .-

American Environmental Testing Laboratory Inc. 2834 &2908 Nortli Naolni Slreet,Rurbank, CA 91504 'DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL. (818) 845-8200 Q Fax: (818) 845-8840 - www.aetlab.com

ANALYTICAL RESULTS

Page: 1 6

Project ID: 32486-000 Pro'ect Name: Del h i S stem Corp.

Method: (8270C), Semivolatile Organic Compounds by GCIMS (SW-846) QC Batch No: 100605

American Environmental Testing Laboratory Inc. 28148~2908 North Naorni Sircet, Burbank. CA 91504 *DOHS NO: 154I,LACSDNO: 10181 Tcl: (888) 288-AETI, . (818) 845-8200 - Fan: (818) 845-8840. www.aet1ab.com

ANALYTICAL RESULTS Ordered By

I Haley & Aldr~cli

Telcphone: (714)985-3434 Attn: Tom Tatnall

Page: 1 7 - Project ID: 32486-000 Proiect Name: D e l p h ~ Svstem Corp

S i t e

American Environmental Testing .- Laboratory Tnc. 2834 a2908 North Yaon~i Street, Burbank, CA 9 I504 - DOHS NO: 1541, LACSDNO: I0181 Tel: (888) 288-AETI.. (818) 845-8200. Fax: (818) 845-8840. www.acrlab.com

ANALYTICAL RESULTS

Page: 18

Project ID: 32486-000 project Name: Delphi System Corp.

Method: (8270C); Semivolatile Organic Compouilds by GUMS (SW-846) QC Batch No: 100605

~. I Date Sampled - _.. _-A- i

Dale Prepared Preparation Method . .- .-- -. .. Date Al~alyzed ~~. . .~

,---_i : Matrix

.. . ~ ~ - ~ ~ ~ llexachlorocyclopentadie~~e 0 . 2 5 0 .50 ND

o , i .&..-.,. -

Hcxachloroethane 0.50 ' ND . -~~ ..,.. ~~

Indeii0(1,2,3-cd)~~rrei1e 7 0.25 0 .50 ND .- . lsophoronc 0 . 2 5 0 . 5 0 ND I I

1 2-Metlivl~~anhthaleile 0 . 2 5 0 .50 ! ND

American Environmental Testing Laboratory Inc. 2834 &2908 Norrli Naomi Street. Burbank, CA 91504 .DOHS NO: 1541,LACSDNO: 10181 Tcl: (888) 2 8 8 - A E T L ' (818) 845-8200 ' Fax : (818) 845-8840 www.ae t l ab .com

ANALYTICAL RESULTS

Page 1 9

Pro'ect ID: 32486-000

Method: (8270C), Selnivolatile Organic Compounds by GCIMS (SW-846) QC Batch No: 100605

1 Date Prepared ~~. ~~~... . ~ 1 Prepalation Method - Date Analyzed

American Environmental Testing Laboratory Inc. 2834 8~2908 North Naomi Street, Rurbank. CA 9 1504. DOHS NO: 1541, LACSDNO: 10181 Tel: (888) 288-AETL . (818) 845-8200 Fax: (818) 845-8840 * www.aet lab.com

ANALYTICAL

-00 South Kraemer Blvd

S i t e

'Telephone: (7 14)985-3434 Atln: Tom Tatnall

Page: 2 0

Project ID: 3 2 4 8 6 - 0 0 0 Project Name: D e l p h i S y s t e m C o r p .

Method: (8082), Polychlorinated Biphenyls (PCBs) by GC QC Batch No: 100605

I ! . ... ~~~~ ~~~ . ~ .

:dale Sa~npled -- .- Date Prepared --. . .

1 Preparation ~ e i h o d -~ 3 5 5 0 ~ 35508 . .-

p2!!te.,!!!~al~zed . . . . I Matrix

~~. 1 Units -.

8 Surrogates

28348~2908 Norrli Nao~ni Street, Burbank, CA 91504 'DOHS NO: 1541.I~ACSDNO: 10181 f f Tcl: (888) 288-AETL. (XIS) 845-8200 - Fax: (818) 845-8840 * www.actlab.com

S i t e

outh Kraemer Blvd.

Telephone: (714)985-3434 Attn: Tom Tat~iall

Page: 2 1

Project ID: 3 2 4 8 6 - 0 0 0 Project Narne: Delphi System Corp.

Method: (6010B/7000CAM), CAM Title 22 Metals (SW-846)

# 01-01 02-01

Units -~

I Cadmium .. ~

Ciiroiniu~n --.-

Cobalt

5 : 10

Thalliunr

7 - Z inc

American Environmental .. Testing Laboratory Inc. 2834 8~2908 Nortli Naolni Sweet. Burbank, CA 91504 .DOHS NO: 1541.1,ACSDNO: 10181 Tcl: (888) 288-AETI_.. (818) 845-8200. Fax: (818) 845-8840. www.act1ab.com

ANALYTICAL RESULTS Ordered B y

I Halei & Aldrich

Site

Telephone: (7 14)985-3434 Attn: Tom Tatnall

*

Pro'ect ID: 3 2 4 8 6 - 0 0 0

Method: 8260B, Volatile Organic Compo~mds by GCIMS (SW846)

.

... . - Matrix

.

scc-Butylbenzcne

.~~ Carbon tetrachloride -~

Chlorohcnzei~e ~~ ---- ~4

ibromomcthane -~

Dichloiobenzene

American Environmental Testing ... Laboratory Inc. 2834&2908 North Naoini Slreet, Rurhnnk, CA 91504 .DOI-IS NO: l511,LACSDNO: 10181 Tel : (888) 288-AETL . (818) 845-8200 - Fax: (818) 845-8840. www.aet lab.com

ANALYTICAL RESULTS

Page: 2 3

Pro'ect ID: 32486-000 i stem Cor .

Method: 8260B, Volatile Organic Compounds by GCIMS (SW846) QC Batch No: 100605

Preparation Method --- ~~

Date Allalyred -~ Matrix

I , I-Dichioroethene ~~ ~.. . ~-

1,2-Dichioropropane .. 1,3-Dic11ioropropa11r

1, 1-Dicliloropropene

l&chiorohutadicne

1 , I, i ,2-Teirachloroetlianc .- 1 ,--- !,1,2,2-'~etrachloroethanc 'Tctrachloroeli~enc p~

1,l.I-Tricllloroetha~~e - ... . 1;1 ,2-'I'richloroctha~~

, , f .~. ,2,3-Trichloroprop&~e . -- ~

American -. Environmental .. Testing Laboratory .. Inc. 2834 &2908 North Naomi Strcct, Burbank. CA 91504 .DOHS NO: lS41,LACSDNO: 10181 Tel: (888) 288-AETI. - (818) 845-8200. Fax: (818) 845-8840 ' www.aetlah.com

ANALYTICAL RESULTS

Page: 2 4

Project ID: 3 2 4 8 6 - 0 0 0 Project Name: Delphi System Carp.

..........

Method: 8260B, Volatile Organic Co~npoullds by GC/MS (SW846) QC Batch No: 100605

American Environmental Testing Laboratory Inc. 2814 &2908 Nortli Naomi Street, Burbank, CA 91504 - DOHS NO: 1541;LACSDNO: I0181 Tel: (888) 288-AETL (818) 845-8200 - Fax: (818) 845-8840 - www.actleb.com

ANALYTICAL RESULTS

00 South I<raemcr Rlvd.

Telephone: (714)985-3434 Altn: Tom Tatnall

Page: 2 5

Pro,ject ID: 3 2 4 8 6 - 0 0 0 Project Name: Delphi S y s t e m Corp.

Method: M8015G, TPH as Gasoline and Light Hydrocarbons Using GCIFID QC Batch No: 100605

American Environmental Testing Laboratory .... Inc. 2834 8~2908 North Naonii Strect, Burbank, CA 91504 .DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL. (818) 845-8200. Fax: (818) 845-8840. www.acllab.com

ANALYTICAI, RESULTS Ordered By Site

Telephone: (714)985-3434 Attn: Tom Tatnall

Page: 26

Prqject ID: 3 2 4 8 6 - 0 0 0 Project Narne: Delphj. System Corp.

~~ --

~

Date Prepared ~~.

Preparation Method ,. . ..

~,. . .. ..

American Environmental Testing Laboratory Inc. 2834 &2908 Norlir Naolili Strecl, Burbank, CA Y 1504 - DOHS NO: 1541.LACSDNO: 10181 Tel: (888) 288-AETL. (818) 845-8200. Fax: (818) 845-8840. www.aclIab.com

ANALYTICAL RESULTS Ordered By

Halcy & A l d l ~ h 500 South Krdzlllel Blvd I

S i t e

Telephone: (714)985-3434

Attu: Tom T a t ~ i a l l

Page: 2 7 - Pro 'ec t ID: 32486-000

Method: 83 10, Polynuclear Aromatic I-lydrocarbons (SW-846) QC Batch No: 101005

ate Analyzed -

1 Matrix -- 10,

Aqueous

Preparation Melliod ~ -p-~~~ p~

~...

American - Environmental Testing Laboratory Inc. 2834&2908 North Naorni Street, Burbank, CA 91504 *DOHS NO: 1541,LACSJ)NO: 10181 'Tel: (888) 288-AETL. (818) 845-8200 * Fax: (818) 845-8840 - www.aet lab.com

ANALYTICAL RESULTS Ordered By Site

'Teleplione: (714)985-3434 Attn: 'Tom Tatnall

Page: 2 8 -

Pro'ect ID: 3 2 4 8 6 - 0 0 0

Method: 8270C, Semivolatile Organic Compouids by GCIMS (SW-846) QC Batch No: 101005

- .

Benzo(a)pyrene

Bcnzo(b)fluora~ilheile 13enzo(g,h,i)peryiene

-~ Bis(2-clilosoisopropyl) cther Bis(2-elhyllicxyl) ikhalats

14-Bromophenyl phenyi etlrcr ;Bol>'i benzyl p h i l i a l ~ t ~

;b-~1~i~~~-3-~~th~1~hiF~1 ~ ..

4-Chioroaniline . .

Chrysene . iDi-11-butyl phthalate

-~ .. .- [l)i-n-octyl phlhalaie (l>ioctyI ~sic?)

J)ibenzo(a;h)anthracene -~-~pp~-~~~

American Environmental Testing Laboratory Inc. 2814 &2908 North Naorni Street, Burbank, CA 9 1504. DOHS NO: 1541,lACSDNO: 10181 Tcl: (888) 288-AETL. (818) 845-8200 . Fax: (818) 845-8840 - www.actiab.com

ANALYTICAL RESULTS

Page: 29

Pro'ect ID: 32486-000

Method: 8270C, Semivolatile Organic Compounds by GCIMS (SW-846) QC Batch No: 101005

American Environmental ..... Testing ... Laboratory ... Inc. 2814 8 ~ 2 9 0 8 North Naorni Street, Bul.bai~k, CA 91504 .DOHS NO: 1541,LACSDNO: 10181 Tel : (888) 288-AET1,. (818) 845-8200 - Fax: (818) 845-8840 - w w w . a e t l a b . c o ~ ~ ~

ANALYTICAL RESULTS

Page: 30

Pro'ect ID: 3 2 4 8 6 - 0 0 0

Method: 8270C, Semivolatile Organic Coinpounds by GCIMS (SW-846) QC Batch No: 101005

Matrix ~. ~ ~~

Units

~~~~ . ,4,5-Trichloi-ophr~loi

~ ~

American Environmental Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504. DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (818) 845-8200. Fax: (818) 845-8840 www.actlab.com

Ordered Bv

ANALYTICAL RESULTS Site

Telephone: (714)985-3434 Attn: Torn Tatilall

Page: 31

Project ID: 3 2 4 8 6 - 0 0 0 Project Name: Delphi S y s tern C o r p .

. Aroclor-1260 (PCD-1260) . -

Arocior-1262 ( P C B : S ~ ~ ~ )

American - Environmental Testing Laboratory Tnc. 2834 &2908 North Naorni Street, Burbank. CA 91504 .DOHS NO: 1541,LACSDRO: 10181 Tcl: (888) 288-AETI,. (818) 845-8200. Fax: (818) 845-8840 - \vww.aetlab.com

ANALYTICAL RESULTS Ordered By

Haley 8r Ald~ lch

5 0 0 South Kraemer Blvd

Site

Telephone: (71 4)985-3434 Attn: Tom Tatnall

Page: 32 - I'ro'ect ID: 3 2 4 8 6 - 0 0 0

Method: 6010/7000CAM, CAM Title 22 Metals (SW-846) QC Batch No: 100705

Thallium

.. 'Tin,.

American Environmental .. Testing Laboratory Inc. 2814 &2908 North Naomi Strcct. Rurhank, CA 91504 *DOHS NO: 1541,I,ACSDNO: 10181 'Scl: (888) 288-AETL - (818) 845-8200 F a x : (818) 845-8840. w w w . a c t l a b . c o m

ANALYTICAL RESULTS

Telephone: (714)985-3434 Attit: Tom Tat11a11

Page: 3 3 Project ID: 3 2 4 8 6 - 0 0 0

E e l hi S s t e m C o r .

Metl~od: 601 017000CAM, CAM Title 22 Metals (SW-846)

QUALIECONTROL REPORT

QC Batch No: 100705 Sample Spiked: 34830.04 QC Prepared: 10/07/2005 QC Analyzed: 10/0712005 Units: mg/L

i 7--

MSDUP RPD MSiMSD

a % REC I % %Limit o !mi

- - ... . Copper Lead ND 1.00 <15

- - - ~

Mercury (By EPA 7470) ND p~~-~--~- ~ . . .. . Molvbdeiium ND

QC Batch No: 100705 Sample Spiked: 34830.04 QC Prepared: 10/07/2005 QC Analyzed: 10107i2005 Units: mgiL

..

Cadiiiiiim .. Chromium

....- Copper .~ I r a i l 1.00 0.92

American - Environmental .- Testing Laboratory Tnc. 2834 ti2908 North Nnomi Stieet,Huubaok, CA 91504.DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL - (818) 845-8200 a Fax: (818) 845-8840 a www.aeLiah.com

ANALYTICAL RESULTS Page: 34 Project ID: 3 2 4 8 6 - 0 0 0 pro'ectName: Delphi System C o r p .

Method: 6010/7000CAM, CAM Title 22 Metals (SW-846)

QC Batch No: 100705 Sample Spiked: 34830.04 QC Prepared: 1010712005 QC Analyzed: 1010712005 Units: mglL

. . Silver

~~ - l'hallium

Vanadium 7inr

American Environmental Testing Laboratory Inc. 2814 &2908 North Nao~ni Street, Bul.hank. CA 91504 .DOI-1S NO: 1541.1,ACSDNO: 10181 Tel: ( 8 8 8 ) 288-AETL ' (818) 8 4 5 - 8 2 0 0 . Fax: (818) 845-8840 - www.aetlab.com

-

ANALYTICAL RESULTS

S i t e

Telephone: (714)985-3434 Altn: Tom Tatnall

Paae: 35 - Pro'ect ID: 3 2 4 8 6 - 0 0 0

Method: 8082, Polychloriilated Biphenyls (PCBs) by GC Q U L I T Y CONTROL REPORT

QC Batch No: 101005 Sample Spiked: 101005 QC Prepared: 10110/2005 QCAnalyzed: 10/10/2005 Units: uglL

~GF~Ms DUP MS

Concen Recov %

2.50i 2.95, 118

QC Batch No: 101005 Sample Spiked: 101005 QC Prepared: 1Ol1012005 QCAnalyzed: 10110/2005 Units: ugiL

American Environmental .- Testing Laboratory Inc. 2834 &2908 North Naorni Street, Burbank, CA 91504 .DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL. (818) 845-8200. Fax: (818) 845-8840 www.aet lah.com

-

ANALYTICAL RESULTS

Page: 36 P1.o'ect ID: 32486-000

Method: 8260B, Volatile Organic Compounds by GCIMS (SW846) Q U L I T Y CONTROL REPORT

QC Batch No: 100605 Sample Spiked: 100605 QC Prepared: 1010612005 QC Analyzed: 1010612005 Units: uglL

QC Batch No: 100605 Sample Spiked: 100605 QC Prepared: 1010612005 QC Analyzed: 1010612005 Units: uglL

Anlllerican -. Environnlllental Testing - Laboratory Inc. 2834&2908 North Naoini Strcct, Burbank, CA 91504.DOHS NO: 1541,LACSDNO: I O I X I Tel : (888) 288-AETI.. (818) 845-8200 - Fax: (818) 845-8840 * www.aetIab.com

- ANALYTICAL RESIJLTS

Teleplione: (714)985-3434 Attn: Tom Tatnall

Page: 37 Project ID: 3 2 4 8 6 - 0 0 0

prqjectName: Delphi Sys tem Corp. ~ ~~

S i t e

Method: 8270'2, Semivolatile Organic Compounds by GCIMS (SW-846)

QC Batch No: 101005 Sample Spiked: 101005 QC Prepared: 1011012005 QC Analyzed: 1011012005 Units: uglL

QC Batch No: 101005 Sample Spiked: 101005 QC Prepared: 1011012005 QC Analyzed: 1011012005 Units: uglL

I -. 4-~111oro-3-n1etl~$~hcnol .. . ... p~ ~ ...... ~ ~ ~ . -

2-Chlorophcnol

1,4-Dichlorobsnze~1c

12,4-~initrot61"% 7--. ~~~.~ j N-Nitroso-Di-n-propylaniinc

American Environmental Testing Laboratory Inc. 28348~2908 North Naomi Street, Burbaiik, CA 91504 .DOHS NO: 1541,1AACSDNO: 10181 Tel: (888) 288-AETL - (81 8 ) 845-8200 Fax : (818) 845-8840 * www.acl1ab.com

ANALYTICAL RESULTS

Ordered By Haley & Aldr~ch

Site

'Ielephone (714)985-3434 Attn Tom Tatnall

Page: 3 8 Pro'ect ID: 32486-000

r .

Method: 83 10, Polyiluclear Aromatic Hydrocarbons (SW-846) QUALITY CONTROL REPORT

QC Batch No: 101005 Sample Spiked: 101005 QC Prepared: 1011012005 QC Analyzed: 1011012005 Units: uglL

QC Batch No: 101005 Sample Spiked: 101005 PC Prepared: 1011012005 QC Analyzed: 1011012005 Units: uglL

. .. . .

i:iuorciic ~-

indeno(l,2,1-~d)pyrei1c

American -. Environmental ... -. Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504. DOHS NO: 1541,LACSDNO: 10181 Tcl: (888) 288-AETL (818) 845-8200 Pax: (818) 845-8840. www.act lab.com

ANALYTICAL RESULTS

Telephone: (71 4)985-3434 Attn: Tom Tatnall

Page: 3 9 32486-000

Method: M8015D; TPH as Diesel and Heavy Hydrocarbons Using GCJFID

QUALITY CONTROL RESORT QC Batch No: 100705 Sample Spiked: 34823.05 QC Prepared: 1010712005 QC Analyzed: 1010812005 Units: mglL

QC Batch No: 100705 Sample Spiked: 34823.05 QC Prepared: 1010712005 QC Analyzed: 1010812005 Units: mgiL

American Environmental Testing Laboratory Inc. .-

2834 8~21108 North Naolni Street, Rui-bank, CA 91504 .DOHS NO: 1541.1,ACSDNO: 10IXI Tel : (888) 288-AETL. (818) 845-8200. Fax: (818) 845-8840 * www.aet lab.com

ANALYTICAL RESULTS

Telephone: (7 14)985-3434 Attn: Tom Tatnall

Page: 4 0 Pro'ect ID: 3 2 4 8 6 - 0 0 0

5 ten Cor .

Method: M8015G. TPH as Gasoline and Light Hydrocarbons Uslllg GCIFID QUALITY CONTROL REPOLT

QC Batch No: 100605 Sample Spiked: 100605 QC Prepared: 1010612005 QC Analyzed: 10/06/2005 Units: mglL

QC Batch No: 100605 Sample Spiked: 100605 QC Prepared: 10/06/2005 QC Analyzed: 1010612005 Units: mglL

American -. Environmental - Testing Laboratory Inc. 2814 &2908 North Naomi Street, Burbank, C A 91504 -DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 2 8 8 - A E T L - (818) 845-8200 . Fax: (818) 845-8840 * www.aellab.com

- ANA1,YTICAL RESULTS

S i t e

Telephone: (714)985-3434 Attn: Tom Tatnall

Page: 4 1 Pro'ect lD: 32486-000

Method: (601 OB/7000CAM), CAM Title 22 Metals (SW-846) Q U J l Y C.O~TROL&EiIPORJ

QC Batch No: 100705 Sample Spiked: 34807.01 QC Prepared: 10/07/2005 QC Analyzed: 10/07/2005 Units: mgiKg

Chroiniuin 2.5 80-120

I Cobalt ~.. ... :Copper , ~ . .~ 1,ed

Selenium

~ ~~~-~~~-p .~

QC Batch No: 100705 Sample Spiked: 34807.01 QC Prepared: 10/07/2005 QC Analyzed: 10/07/2005 Units: mgiKg

s LCSILCSD, I

American -- Environmental Testing Laboratory Tnc. 2834 &2908 North Naomi Slreel, Burbank, CA 91504 -DO11S NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL * (818) 845-8200 - Fax: (818) 845-8840 - www.aellab.corn

ANALYTICAL NZSULTS Page: 4 2 Project ID: 32486-000 Pro'ectNalne: Delphi Sys!.ern Corp.

Method: (6010Bl7000CAM)~ CAM Title 22 Metals (SW-846)

QC Batch No: 100705 Sample Spiked: 34807.01 QC Prepared: 1010712005 QC Analyzed: 1010712005 Units: mglKg

- - - - LCS 1 LCS - LCS ,LCSILCSD~

Analytes Concen 1 Recov % REC I % Limit ' I I I I I

~ . . .- .- ~ - 1 ' . . 'd -- i Nickel &... ~~ .. , .-1.00 l.02, 102 80-1201 I Scleniuin i 1.00 1.08 108 80-120 ....- . .

1.00 0 .98 98 , 80-1201*~ Silver

American -. Environmental Testing Laboratory Inc. 2834 &2908 North Naoini Street, Burbank, CA 91504 DOHS NO: 1541,LACSDNO: 10181 'Tei: (888) 288-AETI. - (818) 845-8200 - Fax: (818) 845-8840 - www.aellab.corn

ANALYTICAL RESULTS

Site

500 South l<raeme

Telephone: (714)985-3434 ~ t t i T o m Tatnall

Page: 4 3 Pro'ect ID: 3 2 4 8 6 - 0 0 0

Method: (8082), Polychlorinated Biphenyls (PCBs) by GC Q U L I L I E ~ C O N ' T R O D ~

QC Batch No: 100605 Sample Spiked: 100605 QC Prepared: 1010612005 QC Analyzed: 10106/2005 Units: mglKg

~-

p i e r MS I hilS hilS I MS DUP MS DUP I MS

Result Concen Recov % REC Conren I Remv I.. 0 .0 / 500.00 ' 560.00 ' 112 ' 500.00 , 555.0

, - -- . - i - 1 - l ~ ~ - ~

QC Batch No: 100605 Sample Spiked: 100605 QC Prepared: 1010612005 QC Analyzed: 1010612005 Units: mglKg

Analvtes

LCS LCS ' LCS LCSiLCSD

Concen Recov % REC % Llmit

American .. Environmental Testing ... Laboratory Inc. 28148~2908 North Naomi Sveel. Rurhank, CA 91504 -DOHS NO: 1541,1,ACSDN0: 10181 Tcl: (888) 288-AETL. (818) 845-8200 - Fax: (818) 845-8840 www.aetlab.com

- ANALYTICAL RESULTS

S i t e

Telephone: (714)985-3434 Attn: Toin Tatnall

I: 32486-000 1 AETL JOD N

D e l a h i Svstem CorP. .3483(

QUAL!TYCONTROLREPORT

QC Batch No: 100605 Sample Spiked: 100605 QC Prepared: 10106/2005 QC Analyzed: 1010612005 Units: uglKg

--

ampiel MS I s PS 7 ME I M S D U ~ S DF! RPD

QC Batch No: 100605 Sample Spiked: 100605 QC Prepared: 1010612005 QC Analyzed: 1010612005 Units: uglKg

American Environmental Testing Laboratory Inc. 2834&2908 North Naorni Street, Burhank. CA 91504 .D011S NO: 1541,LACSDNO: 10181 Tel : (888) 288-AETL. (818) 845-8200 . Fax: (818) 845-8840 www.aet lah.com

ANALYTICAL RESU1,TS

Telephone: (7 14)985-3434

S i t e

~ t t i Torn Tatilall

Page: 4 5 32486-300

Method: (8270C), Semivolatile Organic Co~nponnds by GCIMS (SW-846) QUALITY CONTROLREPORT

QC Batch No: I00605 Sample Spiked: 100605 QC Prepared: 1010612005 PC Analyzed: 1011112005 Units: mglKg

~ ~ -. . ~~7~ . ~ ,

ple i MS i MS S DUP MS DUP ' MS DU MSIMSD MS RPD I I

Result ' Concen i Recov oncen ' Recov % REC 1 %Limit % Limit I - - -. ,-

0 . 0 I 1 0 0 . 0 0 I 69 .00 I 6 9 I 1 0 0 . 0 ~ 7 0 . 0 0 7 0 [' 1 . 4 ; 46-118 <20 1

.. . -. .

Plicnol _ -

Pyrenc I 0 . 0 ,-. I .2.4-'~richlorobenzziic I , .- 1 -

QC Batch No: 100605 Sample Spiked: 100605 QC Prepared: 1010612005 QC Analyzed: 1011112005 Units: mg1Kg

p~~ - . ~- ~

I ~p~

I- - . .

ics LCS LCS lCCSilCSFJT~ I Concen , Recov % REC j % Limit /

-.- 7 0 3 1 2 3 7

. hioro-3-methylphenol

2-Chloi-ophenol 62 ' 25-102 -. ~~ -~ 1,4-Diciilorobcn~znc I ~ 0 0 . 0 0 I 7 5 . 0 0 282804 1 L~~---.+-

1 2;4-i~initrotoiuene 1 o o . 0 0 85 .00 I - -- I-. I . 1 N-Nitroso-Ui-11-propylamine 1 ~~.. -4- , 1

l'cntaciiiorophenol ---. ~ . - ~ j 1 Plicnol

Pyrcne -p- ~ .. i 1 7 AT~;,.hlninl~rir.rrxie

American Environmental Testing Laboratory Inc. 2834 &21108 North Naomi Street, Rurbank. CA 91504 .DONS NO: 1541.LACSDNO: 10181 Tel: (888) 288-AETL. (8 18) 845-8200 - F a x : (818) 845-8840 www.aellab.com

ANALYTICAL RESIJLTS

Site

Telephorre: (714)985-3434 Attn: Tom Tatnall

Page: 4 6 32486-000

Method: (83 lo), Polynuclear Aromatic Hydrocarbons (SW-846)

QUALITY CONTROL R E P B T

QC Batch No: 101005 Sample Spiked: 101005 QC Prepared: 1011012005 QC Analyzed: 1011012005 Units: mglKg

Analvtes

QC Batch No: 101005 Sample Spiked: 101005 QC Prepared: 1011012005 QC Analyzed: 1011012005 Units: mglKg

American ... Environmental Testing .- Laboratory Inc. 2834&2908 North Naorni St~cci , Uurbank, CA 91504 .DOI-IS NO: 1541,1,ACSDNO: 10181 Tel : (888) 288 -AETL (818) 845-8200 Fax: (818) 845-8840 * www.act1ab.com

ANALYTICAL RESULTS

Telephone: (7 14)985-3434

Site

Attn: Tom Tatnal l

Page: 4 7 32486-300

Method: (M8015D), TPI-I as Diesel and IIeavy Hydrocarbons Using GCIFID QUALITY-CONTROLIEP'RT

QC Batch No: 100605 Sample Spiked: 100605 QC Prepared: I010612005 QC Analyzed: 10/06/2005 Units: mglKg

.- s TS DUFMS D U ~ ~ ~ S D U P ~ 1 MSIMSD MS RPD 1

% REC i O h , o h Limit 1 %:!it 1 84 4 . 9 75-125 <20 ~pp~ I

QC Batch No: 100605 Sample Spiked: 100605 QC Prepared: 1010612005 QC Analyzed: 10106/2005 Units: mglKg

American ... Environmental Testing Laboratory Inc. 2834 6r2908 Yortll Naomi Slrcet, Burbank. CA 91504 .DOHS NO: 1541,LACSDNO: 10181 Tc l : (888) 288 -AETL . (818) 845-8200. Fax: (818) 845-8840. www.ael1ab.corn

ANALYTICAL RESULTS

S i t e

lephone: (714)985-3434 ~ t t n ; Torn Tatnall

Page: 4 8 Pro'ect ID: 32406-030

Method: (M8015G), 'IPH as Gasoline and Light I-Iydrocarbons Using GCIFID

QC Batch No: 100605 Sample Spiked: 100605 QC Prepared: 1010612005 QC Analyzed: 1010612005 Units: mglKg

p~ - ~~p~ -. -~ -

MS 1 MS DUP 1 MS DUP MS DUP RPD MSIMSD MS RPD 1 v ! Oh REG Concen Recov YO RE:. %

% T i t %Limit 3

I 95 / 2.50 2.331 93 I 2.1 , 75 125 , <20 1 I J - L i . - L - 1 . - ! .;

QC Batch No: 100605 Sample Spiked: 100605 QC Prepared: 1010612005 QC Analyzed: 1010612005 Units: mglKg ~-~~ p~~ - i . , - , ~~ - I Ccs LCS ~LCSILCSD! I % REC %Limit i 1 -

84 1 75-125: ! y- I i I

i 1 ~ - ~

! -

American Environmental Testing Laboratory Inc. 2834 8~2908 North Nao~ni Street, Burbank, CA 0 1504. DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL. (818) 845-8200 - Fax: (818) 845-8840. www.aellab.com

Data Qualifiers and Descriptors

Data Qualzyer:

*. In the QC section, sample results have been taken directly froin the ICP reading. No preparation factor lias been applied.

R: Analyte was present in the Method Blank.

D: Result is from a diluted analysis.

E : Result is beyond calibration lilnits and is estimated.

H: Analysis was perfo~med over the allowed holding time due to circumstances which were beyond laboratory control.

J : Analyte was detected. However, the analyte concentration is an estimated value, which is between tlie Method Detection Limit (MDL) and the Practical Quantitation Limit (PQL).

M : Matrix spike recovel-y is outside control limits due to matrix intel-ference. Laboratory Control Sample recovery was acceptable.

S6: Surrogate recovery is outside control limits due to matrix interference.

SX: The analysis of the sample required a dilution such that the surrogate concentration was diluted below the method acceptance criteria.

X : Results represent LCS and I.CSD data

%Limi:

%REC:

C0n.L:

Conce:

LCS:

MDL:

MS:

MS DU:

Percent acceptable limits

Percent recovery.

Acceptable Control Limits

Added concentration to the sample.

Laboratory Control Sample

Method Detectioli Limit is a statistically derived nulnbcr which is specific for each instmment, each method, and each compound. It indicates a distinctively detectablc quantity with 99% probability.

Matrix Spike

Matrix Spike Duplicate

American Environmental Testing Laboratory Inc. 2834 8~2908 North Naomi Street, Biirbank, CA 91504. DOHS NO: 1541,LACSDNO. 10181 Tel: (888) 288-AE'TL. (818) 845-8200. Fax: (818) 845-8840 - www.aetlab.com

Data Qualifiers and Descriptors

ND: Analyte was not detected ill the sample at 01. above MDL

PQL: Practical Quantilation Limit or MI. (Minimum Level as per RWQCB) is the ~nininrum conceiltration that can be quantified with move than 99% confidence. Taking into account all aspects of the entire analytical insiru~nentation and practice.

Recov: Recovered coilcentration in tile sample

W D : Kelat~ve Percent Difference