delphi, facility investigation report, appendix f, section 2 · american environmental -. testing...
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American Environmental Testing Laboratory Inc. 2834 a2908 Nor111 Nacxni Slreer. Rul-hank, CA 91504 *L)OHS NO: L541,LACSDNO: 10181 Tci: (888) 288-AETI, * (818) 845-8200 - Fax: (818) 845-8840 . wwwaet lab . % % G E ~ D
OCT 1 O 2009
H a l e y & A l d r i c h N u m b e r of P a g e s 2 aley & H h ; In$. I
500 S o u t h K r a e m e r B l v d . S u i t e 370 D a t e R e c e i v e d 10/04/2005 !
I B r e a , CA 92821-6723
T e l e p h o n e : (714) 985-3434 A t t e n t i o n : Tom T a t n a l l
D a t e R e p o r t e d 10/05/2005
P r o j e c t I D : 3 2 4 8 6 - 0 0 0 p ro jec t ~ a m e : De lph i S y s r e m Corp.
S i t e : 1201 N . Magnolia Avenue Anaheim, CA 92801
Enclosed please find results of analyses of 2 solid waste sampies which were analyzed as specified on the attached
chain of custody. If there are any questions, please do not hesitate to cal.1.
Checked By: Approved By: - ~eL-.~~2 ~ ~~~~~-
Cyrus Razmara, Ph. D.
Laboratory Director
Chain of Custody Record
C!!enl
Haley & Aldrich Adbiess
500 S. Kraeiner Blvd., Suite 370
g ~ o o . ~ a z a : d I : ~SRI.? i i l j9si ~ ~ o r s 0 0 3 O ~ l n k - o n n
P~OJUC: hfansgcr
Tom Tatnall TeIc~hnnn h'!,mbnr (Area Code)
(714) 985-3434 Cify Slsfe
Brea CA
f l ~ n t : ; - n TI C C c t O D S ~ O S ~ ~ : By Lab O ~ r r k r i l . For ?!on!hs
Z;pCodc
92821
L n b o r ~ t o y Namr
AETL
Lab-mlor) ,*riil:csr 9 7 ~ I ~ p b o n ~ N,,rnhc~ 2834 Naomi St., Burbank CA 91504 Tel: (818) 845.szoo
Pro)c(! N n n ~ and Locanon (.Sl?!e)
Delphi, Anaheim CA
Is& biz, c>"h.
Confrn~l'P!>rrba~e Order/?l,o:~ NP
I ~ r s Around Trne Reglared
m2.4 Hours f l 48Hours f l 7 U a y s 3 7 ~ Days f l 2 r Days ~ 0 f , ? . - r s
Sire Conlacr LiibConlar! Anaiysrs (Attach list if more space is needed) T. Tatiiall Jim 1,in
C?<rlerW+:~~b;!l
M;tinx Containers
QC Rrqi~irsmcn!.? (Speaiy!
Date
10i4/2005 -
Lab N~rnllcr
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HA-000009
Page 1 of 1
Sample / 0. No and Description (Containers for each sample may be conihin on one line)
GS0028SSJOO-01
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Date 2 Time 3 $
10i412005
101412005
08 35 1 08'20 1
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Chain of Custody Record
Ors:.?P'~ ?<9,->h+r
HA-000009 Llntr
101412005
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Comments
f RocnivcriBy
2. Recrivcd By
3 R m c t u ~ d B y
Pr"!?ct ~ , ~ * . + : ~ ~ ~ ~
Tom Tatnal l
Tine
iime
Time
I RolnqtirshPd By
2 Religplshed By
3 RoDnni~rsiicdBy
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Date
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American Environmental -. Testing Laboratory Inc. 2814 a 2 9 0 8 Norill Naoiiii Strcct, Bur-bank, CA 91504. DOHS NO: 1541.12ACSDNO: 10181 Tci : (888) 288-AETI, . (818) 845-8200 Fax: (818) 845-8840 . www.astIab.com
ANALYTICAL RESULTS
rea. ('I\ 02X1l-6723 I hone: (7 14)985-3434
Attn: Tom Talllall
Site
' 1201 N Magnolia Abenue
, Aiiaheim, CA 92801
Page 2 I'rojecl ID 32486-000 GTL Job Number Submztted Cl~ent
Project Na111c Delpbl System Corp. - 348:3 - 10/04/2005 HGK , -1 -
Method: (6010B,LEAD), Lead, ICP QC Batch No: 100405
QUA&ITY CONTROL REPORT
QC Batch No: 100405 Sample Spiked: MA5994 QC Prepared: 1010412005 QC Analyzed: 1010412005 Units: mglKg
QC Batch No: 100405 Sample Spiked: MA5994 QC Prepared: 1010412005 QC Analyzed: 1010412005 Units: mgiKg
American Environmental Testing Laboratory Inc. 28348~2908 North Naomi Street, Burbank, CA 91504.DOHS NO: 1541,IACSIlNO: 10181 Tel: (888) 288-AETL. (818) 845-8200 * Fax: (818) 845-8840 - www.aetlab.com
Data Qualifiers and Descriptors
Data Qualifer:
In the QC section, sample results have bee11 taken directly from the ICP reading. No preparatioil factor lias been applied.
A~xalyte was present in the Method Blank.
Result is from a dlluted analys~s.
Result is beyond calibration limits and is estimated.
Analysis was performed over the allowed holding time due to circumsia~~ces which were beyond laboratory control.
Analyte was detected . However, the analyte co~lcentration is an estimated value, which is between the Method Detection Limit (MDJ.) and the Practical Quantitation Limit (PQL).
Matrix spilce recovery is outside co~~t ro l limits due to matrix interference. Laboratory Coiltrol Sample recovery was acceptable.
Sui-rogate recovery is outside control limits due to n ~ a t r ~ x interference
The analysis ofthe sample required a dilution such that the surrogate concentration was diluted below the method acceptance criteria.
Results represent LCS and LCSD data
%Limi: Perce~ii acceptable limits
%REC: Percent recovery.
C0n.L: Acceptable Control Limits
Conce: Added colicelitration to the sample.
I.CS. Laboratoiy Control Sample
MDI,: Metl~od Detection Limit is a statistically derived number which is specific for each inst~unlent, each method, and each conipound. It indicates a distinctively detectable quantity wit11 99% probability.
MS: Matiix Spikc
MS Dli: Matrix Spike Duplicate
American Environmental Testing Laboratory Inc. 2834 &2908 Noi-tli Naoini Street, Burbank, CA 91504 .DOIFIS NO: 1541,LACSDNO: 10181 Tcl: (888) 288-AETL - (818) 845-8200 -Fax: (818) 845-8840 - www.aetIab.com
Data Qualifiers and Descriptors
ND: Analyte was not detected in the san~ple at or above MDL.
1'QL: Practical Quantitation Limit or ML (Minimum Lcvel as per RWQCB) is the rniliimu~n co~ice~itration that can be quantified with move tila11 99% confidence. Talcing into account all aspects of the elrtire analytical i~~stru~nei~tatioli and practice.
Recov: Recovered conceiitration ill the sample.
RPD: Relative Perce~it Difference
American Environmental Testing Laboratory Inc. ,- ?- .:,.* .v.-
2834 a2908 Nortli Naoini Street. Rurbaok, CA 91504 -DOHS NO: L S ~ I . I . A C S ~ E L ~ - . . . ; ,:lD Tei: (888) 288-AETI.. (818) 845-8200. Fax: (818) 845-8840. www.ac t i ab .com
QCV 1 0 2005
O r d e r e d B y
H a l e y & A l d r x c 500 Sou th Krae
~ r e a , CA 92821-6723
Te lephone : (714) 985-3434 A t t e n t i o n : Tom T a t n a l l
P r o j e c t I D : 3 2 4 8 6 - 0 0 0 p r o j e c t prame: Delphi S y s t e m Carp.
S i t e : 1201 N . Magnolia Avenue
Anaheim. CA 92801
Enc losed p l e a s e f i n d r e s u l t s of a n a l y s e s of 1 s o l i d was te
sample which was ana lyzed as s p e c i f i e d on t h e a t t a c h e d c h a i n of c u s t o d y . I f t h e r e a r e any q u e s t i o n s , p l e a s e do n o t h e s i t a t e
t o c a l l .
Checked By: LL Approved B y : - - -J - --
Cyrus Razmara, Ph . D .
L a b o r a t o r y D l r e c t o r
Chain of Custody Record
@24 Hours OSK Flours D 7Da.v~ I 4 D,?:/.v 0 2 1 Days g131heis ~ ~-p I
Cusfodv V\il,mbi.r
HA-00001 0
JNon-Haraid O F I ~ ~ F ~ B O~.4rn lnllagt nPo,son 9 WL~nknnldo
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10~412005
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Labsralon. N 3 m ~
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Haley & Aldrich Prc+rf h l s n a g ~ r
Tom 'I'atnall
Tom Amtin6 i'lmp 4ng;rirrd QC f?cgt,:r?rnrrtr (Speriw!
Chain of Cusfody Record
Haley & Aldrich I Ton1 Tatnall ( AETL 1 101412005 / HA-00001 0 i 1 I I
Address
O N O ~ - H ~ L ; ~ ~ ~ 0 ~ ~ a ~ r n z n i c nsk~r, irri!ant O ~ o i s o n B MUnknnrvn nRe!um TI ciienr O u ~ s p o s a i wy Lab D i i T h i w For hqonths
Tum Arnord Ttmp Rsqasrcrl
0 2 4 Houe 0 4 8 Hours fi7 Days I4 Days n21 Days (70lhcn_____
1. Rs!rnq:,t$hni! By
2 Relrnovrshed By
QC Fiequrrcncn!~ (SpNrfyl
3 R~,in~i!rsnedBy
8 . Rnceivcd By
2 Rrccivrd By
Date
Date
C o m m ~ o l s I
Tcme
T m e
Date
Dale
Dale
Time
Ttme
Time 3 Rci-rivrd 13y Dele Tlmr
American Environmental Testing Laboratory Inc. 2834 &2908 Noriii Naomi Stl-cet, Burbank, CA 91504. DOHS NO: 1541.12AACSDNO: 10181 Tc l : (888) 2 8 8 - A E T L . (81 8) 845-8200 Fax: (818) 845-8840 - www.aeL1ab.com
ANALYTICAL RESULTS
Site
Anaheim, CA 92801
re;,, ('A 92821.0723
Telephone: (714)985-3434 Attn: Toin Tatnall
Page: 2 Project ID: 32486-000 Project Name: D e l p h i System Gorp.
Method: (6010R,LEAD), Lead, ICP QC Batch No: 100405
QC Batch No: 100405 Sample Spiked: MA5994 QC Prepared: 10/04/2005 QC Analyzed: 10104/2005 Units: rngiKg
QC Batch No: 100405 Sample Spiked: MA5994 QC Prepared: 1010412005 QC Analyzed: 1010412005 Units: mglKg
American Environmental Testing Laboratory Inc. 2814&2908 North Naorni Strect, Bui-bank. CA 91504.DOHS NO: 1541.I.ACSDNO: 10181 Tel: (888) 288-AETIL . (8 18) 845-8200. Fax: (8 18) 845-8840 www.aetlab.com
Data Qualifiers and Descriptors
Datr~ Qunlifer:
*. I11 thc QC section, saniple results have been taken d~rectly from tile ICP reading No preparation factor has been applied
Ailalyte was present in the Method Blank
llesult is from a diluted analysis
Result is beyolid calibration limits and is estimated
A~lalysis was performed over the allowed holding time due to circumsta~lces which were beyond laboratory control.
Aiialyte was detected . However, the analyte conce~ltratioi~ is an esti~naled value, which is between the Method Detectio~l Limit (MDL) and the Practical Quaniitation Limit (PQL).
Matrix spike vecovery is outside control liniiis due to inatrix interference. Laboratory Co11t1-ol Sa~nple recovery was acceptable.
Surrogate rccovery is outside control limits due to matrix interference.
The analysis of the sanlple 1-equired a dilution such that the surrogate coi~centration was diluted below tbe method acceptance criteria.
Results represent LCS and LCSD data
%Lirni: Percent acceptable limits.
%REC: Percent recovery.
C0n.L: Acceptable Coi~trol Limits
Conce- Added concentration to liie saliiple.
LCS: Laboratory Cons-01 Sa~nple
MDL: Method Detection Li~nit is a statistically derived ilumber which is specific for each instrument, each method, and each co~npound. It indicates a distinctively detectable quailtity with 99% probability.
MS: Matrix Spike
MS UU: Matrix Spike Duplicate
American Environmental Testing Laboratory Inc. 2814 &2908 North Naomi Strcet, Burhank, CA 91504 .DOHS NO: I541.1,ACSDNO: 10181 Tcl: (888) 288-AETL * (818) 845-8200. Fan: (818) 845-8840. www.act lah.com
Data Qualifiers and Descriptors
ND: Analyte was not detected in the sample at or above MDL
PQI.: Practical Quantitation Limit 01. MI, (Minimum Level as per RWQCB) is the minimum conceneaiion that call be quantified with nmore than 99% confidence. Talcing into account all aspects of the entire analytical instrumentation and practice.
Recov. Recovered concentration In the sample
RIJD: Relative Percent Difference
American Environmental Testing Laboratorv Inc. 2834 8~2908 Nortli Naomi Street, Burbank, CA 91504 -DOITS NO: 1541,1,ACSDNO: 10181 Tel: (888) 288-AETL. (8 18) 845-8200. Fax: (818) 845-8840. w w w . a e t l a b R E c E I v E D
OCT B 8 200.5
T e l e p h o n e : ( 7 1 4 ) 9 8 5 - 3 4 3 4 A t t e n t i o n : Tom T a t n a l l
Job N u m b e r Order Dace C l r e n r
P r o j e c t I D : 32486-000 P r o j e c t Name: Delphi S y s t e n Corp.
S i t e : 1 2 0 1 N . Magnolia Avenue
Anaheim, CA 92801.
Enclosed p l e a s e f i n d r e s u l t s of a n a l y s e s of 13 s o l i d w a s t e samples which were a n a l y z e d a s s p e c i f i e d on t h e a t t a c h e d c h a i n of cus tody . I f t h e r e a r e any q u e s t i o n s , p l e a s e do n o t h e s i t a c e t o c a l l .
Cnecked By: --
Cyrus Razmara, Ph.D. Laborazory I l l r e c t o r
Chain of Cusfody Record
c!isi~& Ntrrnbcr
MA-Q00013
f l~on-wazarr i flfnmrnalrrc f l s k n lrrrrenr Q m s n n B U~lkno%,n
D a A
101712005
O ~ c t t i r n To Ckn t a ~ ; i s p o s a l R y i a b D ~ r r h i i e For hlnnlhs
Lnbomfori. h'srns
AETL
cnenf
Haley 8L Aldrich Projsc: smr#;>Qcr
Tom TatnaIl
T:,m Crnrlnd Time Roquimd
B 2 n Hoiirs 0 4 8 l i o i i r i O 7 ~ a y s O 14 Days 0 2 ; Days f l ~ f h e r s - . - ~ .
QC R o q t r n ~ r n o ~ ? ~ (SpcciWj
Chain of Custody Record
O ~ o n - ~ ? i ; r d B~lamrnablr n ~ k r n !m:airl O?o,soo R m ~ ~ n r ? o w n n~et:,n To C!~a?l ~ ~ s p o s a ~ s ; ' :ab O~rc?rve For
C1,enl
Haley & Aldrich
Turn k o i m d T;nn 9~.~t,imd
0 2 4 Hours 0 4 8 Vours 2 7 Days 3 i 4 Days n 2 ! Days jl?!ners ___.....-p- ~
Safe
10171zoo5
OC Rcqlijrrmrnfs :Sprri?~>
P,~roii, llt,.mb~r
HA-00001 4 P r p c t Manager
Tom Tatnall Lahoralnry Y.7mo
AETL
American -. Environmental Testing Laboratory Inc. 2814 &2908 NortB Naomi Street, Burbank. CA 91504. DOHS NO: 1541,LACSUNO: 10181 Tcl: (888) 2 8 8 - A W L . (818) 845-8200. Fax: (818) 845-8840. www.actlab.com
ANALYTICAL RESULTS Ordered By S i t e
0 South I<racmar Rlvd.
Attn: Tom Tatnall
Page: 2
Project ID: 32486-030 Project Name: 3elphi System Corp.
Method: (8082), Polychlorillated Bipheilyls (PCBs) by GC
. .
American Environmental Testing Laboratory Inc. 2834a2908 North Naomi Strezt, Burbank, CA 91504 .DOfIS NO: 1541,I,ACSDNO: 10181 Tei: (888) 288-AETL * (818) 845-8200 - F e x : (818) 845-8840. www.aetIab.com
-- ANALYTICAL RESULTS
S i t e
500 South Icracmer Blvd.
Attn: Torn Tatnali
Page: 3
Project ID: 32486-000 Project Name: Delphi System Corp . .
Method: (8082), Polychlorinated Biphenyls (PCBs) by GC QC Batch No: 101005
Aroclor-1221 (PCB-1221) Aroclor-1232 (PCB-1232)
I Arocior- 1242 (PCB- 1242)
American Environmental Testing Laboratory Inc. 2834 a2908 Norlli Naomi Street, Burbank, CA 91504. DOHS NO: 1541,LACSDNO: 10181 l'ei: (888) 288-AETI, . (818) 845-8200. Fax: (818) 845-8840. www.aellah.corn
ANALYTICAL RESULTS
500 South Krae~ner Rlvd.
Telephone: (714)985-3434 Attn: Tom 'Satnail
Page: 4
Prqject ID: 3 2 4 8 6 - 0 0 0 Project Name: Delphi S y s t e m Corp.
Method: (8082), Polychlorinated Biphenyls (PCBs) by GC QC Batch No: 101005
late barnplea I U / U I / Z U U ~
Ge Prepared -- -. separation ~~ Method . -- .
Date A~~alyred --~~ ~~ ~. . Matrix
2.00 1 ND
American Environmental .. Testing Laboratory ..- Inc. 28348~2908 North Naomi Stl-ezt,Burbank, CA 91504.DOHS NO: 154I.LACSD.UO: 1018I TeI: (888) 288-AETI,. (818) 845-8200. Fax: (818) 845-8840. www.ac t l ab .com
ANALYTICAL RESU1,TS
00 South Icraemer Blvd.
Telephone: (714)985-3434 Alti~: Tom Tatnall
Page: 5
Project ID: 32486-030 Project Narne: Delphi System Corp.
Method: (8082), Polychlorinated Biphenyls (PCBs) by (iC QC Batch No: 101005
-- Date Samoied
American Environmental Testing Laboratory Inc. 2814 &2908 Nost11 Naolni Street, Burbanii, CA 91504 'UOHS NO: 1541.1,ACSDNO: 10181 Tci: (888) 288-AETL . (818) 845.8200 * Fax: (818) 845-8840. www.actSab.com
ANALYTICAL RESULTS
Attn: Tom Tatnall
Page: 6
Project ID: 32486-000 Project Name: Deiphi System Corp.
Method: (8082), Polychlorinated Biphenyls (PCBs) by GC QC Batch No: 101005
~. .~ .... .
American Environmental Testing Laboratory Inc. 2834 &2908 North Naolni Strcct, Burbank, CA 91504 vDOI1S NO: 1541,LACSDNO: I O I X I 'Tel: (888) 288-AETl, . (818) 845-8200 - Fax: (818) 845-8840 . www.ac t lab .com
ANALYTICAL RESULTS
Telephone: (714)985-3434 Attn: Tom Tatnall
Page: 7
Project ID: 3 2 4 8 6 - 0 0 0 Project Name: Delphi System Corp.
Method: (8082), Polychloriilated Biphenyls (PCBs) by GC QC Batch No: 101005
American Environmental Testing Laboratory Inc. 2834 8~2908 North Naorni Street, Burbank, CA '91504 * DOHS NO: 1541,IACSDNO: 10181 Tcl: (888) 288-AETl_. (818) 845-8200 ' Fax: (818) 845-8840 * www.aetlab.co~n
ANALYTICAL RESIJLTS Ordered By
Haley & Ald~~ch a 500 South Icraemer Blvd
Telephone: (714)985-3434 Atin: Tom Tatnall
Page: 8
Project ID: 32486-000 Proiect Name: D e i ~ n l Svstem Corp
MUL -.
S i t e
American Environmental Testing Laboratory Inc. - 2814 8~2908 North Naomi Street, Uurbank, CA 91504' DOHS NO: 1541,I.ACSDNO: 10181 Tel: (888) 288-AETL ' (818) 845-8200 Fax: (818) 845-8840 - www.aetlab.corn
ANALYTICAL RESULTS Ordered B y
! Haley & ~ldricl l 5 0 0 South I<raemer Blvd.
Telephone: (714)985-3434 Attn: Tom Tatllall
Page: 9
Project ID: 3 2 4 8 6 - 0 0 0 Pro'ect Name: Deiahi S s t e m Carp.
Method: (8082), Polychloriilated Biphenyls (PCBs) by GC QC Batch No: 101005
'2005 Solid Waste Solid Waste
American Environmental Testing Laboratory Inc. 28348~2908 Nonh Nao~ni Street, Burbanli, CA 91504. DOHS NO: 1541,LACSDNO: lOl8I Tel: (888) 288-AETL. (818) 845-8200 * Fan: (818) 845-8840 www.aetlab.com
ANALYTICAL RESULTS Ordered B y
I Halev & Aldr~cli 500 South Krae~ner Blvd
Site
Telephone: (7 14)985-3434 Ann, Torn Tatnall
Page: 1 0
Project ID: 32486-000 Pro'ect Name: D e l p h i System C o r p .
Method: (8082), Polychlorinated Biphenyls (PCBs) by GC QC Batch No: 101005
1 Our Lab 1.D.
aste
A,",,",. ,,,, ,. ,,,-, ,,., -~ ~ ~ ~ . . ,. . . . .- - f '--- Arocior-1232 (PCB-1232) 4.00 ' 10 : ND ND ND
~ i 0 ~ ~ ~ 1 2 4 2 ) I 4.00 10 I ND - Aroclor-1248 (PCB-] 248) 4.00 10 53.8 60.8 ! 47.3
American Environmental Testing Laboratory Inc. 28148~2908 North Naomi Strcet.Bur-bank, CA 91504 .DOHS NO: 1541,I.ACSI>NO: 10181 Tci: (888) 288-AETL. (818) 845-8200 Fax: (818) 845-8840. www.actlab.co~n
ANALYTICAL RESULTS Ordered By Si te
Tclephonc: (714)985-3434 Atto: Tom Tatnail
Page: 11
Project ID: 32486-000 Project Natne: celphl systerr Corp.
AETL Job N u h e r S u b m l i l c e d C l l e n t
Method: (8082), Polychlorillated Biphenyls (PCBs) by GC QC Batch No: 101005
I (Jnits
American Environmental Testing Laboratory Inc. 2834 8~2908 North Nz~onri Strcet, Burbailk, CA 91504 0DOHS NO: 1541,LACSDNO: IOiXi Tel: (888) 288-AETI. (818) 845-8200 'Fax: (818) 845-8840. www.actlab.com
Ordered Bv ANALYTICAL RESULTS
Site -
500 South Kraetiler Blvd.
Telephone: (714)985-3434 Attn: Tom Talnall
Page: 12
Project ID: 32485-000 Pro'ect Naine: Del h i S stem Coru.
Method: (6010B/7000CAM), CAM Title 22 Metals (SW-846)
~. .
Lead .
. . .. Silvzl-
Thallium
j Vanadium 5.0 , ND
IZinc ~~~ , . -
American Environmental - Testing Laboratory Inc. 2834 &2908 North Naomi Sireei, Burbaiik, C A 91504 'DOHS NO: 1541,LACSDNO: I O I X i Tel: (888) 288-AETL - (818) 845-8200 - Fax: (818) 845-8840. www.actiab.com
ANALYTICAL RESULTS O r d e r e d By Site
Telephone: (714)985-3434 Attn: Ton] Tatr~all
Page: 13
Project ID: 3 2 4 8 6 - 0 0 0 Pro'ect Name:
Method: (6010B/7000CAM), CAM Title 22 Metals (SW-846) QC Batch No: 101005
- . .. . . . .- ' 1. 3 2 5
- ;Beryllium i ND
I 1.3 2.5 ND ND ND .- -- ND
2.5 8 5.0 1 14.3 4 . 1 0 ~ I -- 9.55
-. .~ A
Cobalt 2.5 1 5.0 / T N D 2.505 1 ~~ -.4 --AP .- d-~~~~.. .. .. 8
I Copper 5.0 13.9 , 13.0 8.65 1 !. - - 2.5 .~. -- 14.5/1275-- -
1,cad 39.4 78.5 122 ! ..
Mercury (By 121'4 7471) 0.1 0.2 ND ND ND
Molybdenum 1 2.5 ' 5.0 ! ND ND ND -p
hickel ! 2.5 5.0 6.10 I 4.255 ! 8.25 4.853 4.705 -: ~. -- -- .-
Silver I 2.5 5.0 ND ND
Thalliu~n 1 . 0 5 ; - - .~ ~
1 Vanadium 2.5 5.0 22.3 i 13.9 . 15.2
2.5 1 5.0 1 19.8 ! 34.9 t 26.4 i 38.4 i 16.2
American Environmental Testing Laboratory Inc. 2834 8~29118 North Naomi Street, Burhank, CA 91504 .IlOHS NO: 1541,LACSDNO: 10181 Tcl : (888) 2 8 8 - A E T L - (818) 845-8200 Fax: (818) 845-8840 www.actlsb.com
ANALYTICAL RESULTS Ordered By
I Hale) & Aldrlch
S i t e
Telephone: (714)985-3434 Atbl: Tom Tatnall
Page: 1 4
Project ID: 32486-000 Pro'ect Name: Del h i S stem Corp.
Method: (601 0B/7000CAM), CAM Title 22 Metals (SW-846) QC Batch No: 101005
... .
.~. . Mercury (By EPA 7471)__ i ---
'l'hallium ~ n n a d i u m
lZinc ~
American Environmental .. Testing Laboratory Inc. 2834 a2908 North Naomi Street,Burbank, CA 91504.DOHS NO: 1541.LACSDNO: I0181 Tel: (888) 288-AETL (818) 845-8200 - Fax: (818) 845-8840 - www.ae t l ah .com
ANALYTICAL RESULTS
Teleplrone: (714)985-3434 Attn: Tom Tatnall
Page: 15 Project ID: 32486-000
pro'ect Name: Delphi System Corp.
Method. (6010B/7000CAM), CAM Titlc 22 Metals (SW-846) Q m L I E CXJNTROL REPOR'J
QC Batch No: 101005 Sample Spiked: 34849.01 QC Prepared: 1011012005 QC Analyzed: 1011012005 Units: mglKg
- . sample , MS '~-Ms-.' DUP RPD MSIMSD , MS RPD
I
REC % 1 %limit 1 %Limit 1
--~ 2.22 I O ~ ~ - - ~ . O O ; I.1s r I.0o 2.22 107
. - - .. .. -. . - Beryllium ND , 1.00 I 0.89 89 1 1.00 ! 0.89 89, <1 80-120 1 <I5 - I
b~ad i i~ iom .- . ND 1 1.00 1 0.91 92 1.1 b0-120 ' <I5 , Chromium <1 , 80-120 <15
. o.
'- 1.00 ) 1.01 95 1.00 1.011 95
I <1 1 80-120
-. Copper . . ~1 0.153 . 1- 1.00, 11.8 103 1.06 ~ 1 . 103 <I 80-120 4 s .. .-
I i end ND 1.00 1 0.94 94 I 1.00 1 0.93 ' 93 1 1.1 1 80-120 <15 1 , ---"
Mercury (By EPA 7471) ~~ 0.01 1.1 , 80-1201 <15 ! p i iy i ideoum ~~~~ ;. 2.49 104 .,-~ k1;rirrl 1.00 I 2--~-'-7 , 80-120 i <15 ~ ..u..u. -.~. I Selenium I ND 1.00 -- SiI,rrr ND I 1.00 I
QC Batch No: 101005 Sample Spiked: 34849.01 QC Prepared: 1011012005 QC Anaiyzed: 1011012005 Units: rnglKg
~ - ,
Arsenic .. . Barium - .. ~~. - -, . Beryllium
Cadmium
, ~ ,- ~. I I ,-UA 1.02 1 102 I 80-120 1 I I
American Environmental Testing Laboratory ---- Inc. 2834 &2908 Nol-ih Naomi Street. Burbank, CA 91504. DOHS NO: 1541.LACSDNO: 10181 Tel : (888) 288-AETL. (818) 845-8200 ' Fax: (818) 845-8840 . www.actlab.corn
ANALYTICAL E S U L T S Page: 1 6 Pro'ect ID: 32486-000
Method: (6010B/7000CAM), CAM Title 22 Metals (SW-846)
QC Batch No: 101005 Sample Spiked: 34849.01 QC Prepared: 1011012005 QC Analyzed: 1011012005 Units: mglKg
Seleniu~n
Vanadium L~-~ ~ ~ I ! 7inr
American Environmental Testing Laboratory Inc. 2834 &2908 Nol-lh Naolni Street, Burbank, CA 91504 .DOHS NO: 1541,LACSDNO: 10181 Tcl: (888) 2 8 8 - A E T L - (818) 845-8200 Fax: (818) 8 4 5 - 8 8 4 0 . www.aetlab.corn
ANALYTICAL RESULTS
S i t e
Telephone: (714)985-3434 Atb: Toill Tatnall
Page: 1 7 Project ID: 32486-000
. Delphi System Corp.
Method: (8082), Polychlorinated Biphenyls (PCBs) by GC
QC Batch No: 101005 Sample Spiked: 101005 QC Prepared: I011012005 QC Analyzed: 1011012005 Units: mglKg
~p~~ .- - M S ~ MSI
Recov , % REC i 500.00' 100 500.
. 1- i
QC Batch No: 101005 Sample Spiked: 101005 QC Prepared: 1011012005 QC Analyzed: 1011012005 Units: mgiKg
( . - , .- . , - - - . - - - - -~ ~,
LCS LCS LCS LCSILCSD~ i i Concen i Recov 1 % REC : % Limit 1 i i . 1 . - - --
SOO.OO ' 470 00 94 j 75-125 1- j I.. I 1 . r : . I - . I
American Environmental Testing Laboratory Inc. - 2834 8~2908 Norlli Naomi SLreel,Rurbank. CA 91504 .DOHS NO: 1541.1dACSDNO: lO181 Tel: (888) 288-AETL. (818) 845-8200. Fax: (818) 845-8840 ' www.aetIab.com
Data Qualifiers and Descriptors
Data Quali3er:
* In the QC section, sample results have been taken dnectly froin the ICP reading No preparation factor has been appiled
B: Analyte was present in the Method Blank.
D: Result is from a diluted analysis.
E : Result is beyond calibration limits and is estimated.
H : Analysis was performed over the allowed holding time due to circumstances which werc beyond laboratory c011trol.
3: Analyte was detected. However, the analyte con cent ratio^^ is an estimated value, which is between the Method Detection Liinit (MDL) and the Practical Quantitation Limit (PQL).
M : Matrix spike recovery is outside control limits due to matrix interference. 1,aboratory Control Sample recovery was acceptable.
SG: SUI-rogate recovery is outside control liinits due to mawix interference
SS: The analysis of the sample required a dilution such that the surrogate concentration was diluted below the method acceptance criteria.
X : Results represent LCS and LCSD data.
Definition:
%Limi: Percent acceptable limits.
%REC: Percent recovery.
C0n.L: Acceptable Control Limits
Conce: Added concentration to the sample
LCS: 1,aboratory Control Sample
MDL: Method Detection Limit is a statistically derived number which is specific for each instrument, each method, and each compound. It indicates a distinctively detectable quantity with 99% probability.
MS: Matrix Spike
MS DU: Matrix Spike Duplicate
American Environmental Testing Laboratory Inc. 2834&2908 North Naolni SL~.eer, Burbank, CA 91504 .DOHS NO: 1541,LACSDNO: 10181 Tel : (888) 288-AETL - (818) 845-8200 ' Fax: (818) 845-8840 f www.ae l lab .com
Data Qualifiers and Descriptors
ND: Analyte was not detected in the sample at or above MDI
PQL: Practical Qua~ltitation Limit or MI. (Minimum Level as per RWQCR) is the mini~nun~ concentration that can be quantified with more than 99% confidence. Taking into acco~ult all aspects of the entire analytical instrumentation and practice.
Recov: Recovered concentratioil in the sample.
RPD: Relative Percent Difference
American Environmental Testing Laboratory Inc. 2834 &2908 Norrlr Nao~rii Sti-ccl, Burbank, CA 91504 *DOIIS NO: I ~ ~ I , L A c s I I ~ ~ @ ~ ~ ~ Tel: (888) 288-AETL * (818) 845-8200 - Fax: (818) 845-8840 www.aetlah.corn
OCT 1 8 2003
Ordered B y -
H a l e y & A l d r l c h Number of P a g e s 3 500 Souct, Kraemcr B l v d . S u l r e 370 D a t e R e c e l v e d 1 0 / 1 0 / 2 0 0 5
B r e a , CA 92821-6723 Dace R e p o r t e d 1 0 / 1 2 / 2 0 0 5
T e l e p h o n e : ( 7 1 4 ) 9 8 5 - 3 4 3 4 A t t e n t i o n : Tom T a t n a l l
P r o j e c t I D : 32486-002 P r o j e c t Name: Del.phi System Corp .
S i t e : 1201 N . Magnolia Avenue
Acaheim, CA 92801
Enclosed p l e a s e f i n d r e s u l t s of a n a l y s e s o f 1 s o l i d waste sample which was a n a l y z e d a s s p e c i f i e d on t h e a t t a c h e d c h a i n of cus tody . I f t h e r e a r e any q u e s t i o n s , p l e a s e do n o t h e s i t a t e
t o c a l i .
Approved By: - 4-- -
Cyrus Razmara, 2h.D.
Labora to ry E l r e c t o r
American Environmental Testing Laboratory Pnc. --
2834 North Nao~ni Street Burbank, CA 91504 * DOHS NO: 1541. LACSD NO: 10181 Tel: (888) 288-AETL (818) 845-8200 * Fax: (818) 845-8840
CHAIN OF CUSTODY RECORD +. 1
$ q !.j p ;? % .: u * 5 .> 1. V"'
Chain of Custody Record
Cfknl
Haley & Aldrich
Address
500 S. Kraemer Blvd., Suite 370
0 ~ 0 ~ ~ u a ~ a i d nni?nin;.ibii. D ~ k , n irngnt O ~ a r s o n 8 WUPWOW~
Lahcrirory Namc
AETL
i n h o r n f ~ ~ Address R ToiCphOne N N N N ~ Z Z 2834 Naami St., BurbankCA91504 Tel: (818)
845-8200
Pmo,w;rl MensG<:i
Tom 'I'atnalt Telrphonr Niirnbrr lrlren Code)
(7 14) 935-1434
L3~cnirr. ?o c18nnr W~isposai ey L L ~ brlrchlvo FL - b~rnt"s
Da!e
1011 01200s
! .?b Mtilmlhor
Cu~iwJy Nc,mh~r
HA-000023
Page 1 of I Z~pCpCnde
92821 C ~ t y
Brea
Turn Aioi~nd Trmo Rrqcrred
~ Y I W ~ S 3 4 8 H m 0 7 ~ a y s n 14 Days 3 2 1 Days ~Ofhcrs.. ,,
Spcca! insmreoris/connjt~nnn ct niircar
Prqccl hr8!ume and Lwa t r~n :SlnlS)
Delphi, Anaheim CA
Slate
CA
Cornrnm!~
06 R+qoirnnonli (Sp~dyJ
mrafrcri Months longer than I rnoolfi!
Anniysls (Affach lisf if more space is needed) S ~ t e Contact
T. Tatnall
I . Received By
2. RerrwsdBy
3. neccived ey
nrne
Time
Time
f Reimq~ishadBy
2 Re1,fi~nguaned By
3 Rcitnrju!shed By
%' 8 2
LahC001,~~l
Jim Lin
Dare
Dale
Date
Cnr~:e;nN,?ybr!l
Preservatives Conta iners
C~nlraci~Pi.ihhaso OniedCuofe h'o
Dat?
nalc
~ s r o
Matr~x
i rmc
Irma
lime
[A tee may be nseased if snvplos ar?
Samp le / D. No, and Descr ip t ion
(Containers for each sample may be cornbin on one line)
CSOOI 6~CC..OOO_OI
2
~ w s i h f e Hazard ldentrtrcatrmn
Date
1011 012005
4
Srlmpm
Time
1245
3
Drcposai
X
t
J
x l
American Environmental Testing Laboratory Inc. .-
2834 8~2908 Nnilh Nao~ni Street. Rurbank, CA 91504 * DOI-IS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL. (818) 845-8200. Fax: (818) 845-8840 - www.actIab.com
ANALYTICAI, RESULTS
S i t e
Telephone: (714)985-3434 Attn: Tom Tatilall
Page: 2 32486-002
. , - r.
Method: (8082), Polychlorinated Biphenyls (PCBs) by GC QC Batch No: 101005
American Environmental Testing Laboratory Inc. 28348~2908 iVo1.1h Naonii Strcel, Rurbank, CA 91504 .DOHS NO: 1541,LACSDNO: 10181 Tcl: (888) 288-AETI.. (818) 845-8200 Fax: (818) 845-8840 * www.acilab.com
Ordered Bv
ANALYTICAL RESULTS
Site
Telephone (714)985-3434 ~ t t n l Tom Tatnall
Method. (8082), Polychlorinated Biphenyls (PCBs) by GC QlJALITY CONTROL REPORT
QC Batch No: 101005 Sample Spiked: 101005 QC Prepared: 1011012005 QC Analyzed: 1011112005 Units: mglKg
QC Batch No: 101005 Sample Spiked: 101005 QC Prepared: 1011012005 QC Analyzed: 1011112005 Units: mglKg
American -. Environmental Testing Laboratory Inc. 28348~2908 Noi.ih Naolni Street. Burbank, CA 91504 .I)OHS NO: IS4I.LACSDNO: 10181 Tcl: (888) 288-AETL - (818) 845-8200 - Fax: (818) 845-8840 * www.aetlab.corn
Data Qualifiers and Descriptors
Data Qualifier:
In the QC section, sample results have been taken directly from the ICP reading. No preparation factor has been applied.
SG:
Analyte was present in the Method Blank.
Result is from a diluted analysis
Result is beyond calibration limits and is estimated.
Analysis was performed over the allowed holding time due to circumstances which were beyond laboratory control.
Analyte was detected. However, the analyte concel~tration is an estimated value, which is between the Method Detection Limit (MDL) and the Practical Quantitation Limit (PQL).
Matrix spike recovery is outside control limits due to matrix interference. Laboratory Control Sa~nple recovexy was acceptable.
Surrogate recovery is outside control limits due to matrix interference
S8: The analysis of the sample required a dilution such that the surrogate concenaatioil was diluted below the method acceptance criteria.
X : Results represent LCS and LCSD data
Definition:
%Limi: Percent acceptable limits
%RE(:: Percent recovery.
Con.1.: Acceptable Control Limits
Conce: Added concentration to the sample
LCS: Laboratory Colltrol Sanlple
MDL: Method Detection Limit is a statistically derived number which is specific for each instrument, each method, and each coinpound. It indicates a distinctively detectable quantity with 99% probability.
MS: Matrix Spike
MS DU: Matrix Spike Duplicate
American Environmental Testing Laboratory Inc. -- - 28348~2908 North Naolni Strcet, Burbank. CA 91504 .DOHS NO: 1541. LACSDNO: 10181 Tcl: (888) 288-AETL - (818) 845-8200 - Fax: (818) 845-8840 * www.aetlab.com
Data Qualifiers and Descriptors
ND: Analyte was not detected ill the sample at or above MDL.
PQL: Practical Quantitation Limit or ML (Minimum Level as per RWQCB) is the minimum concentration that can be quautified with more &an 99% confidence. Taking into account a!! aspects of the entire analytical illstrumentation and practice.
Recov: Recovered concentration in the sample.
RPD: Relative Percent Difference
American Environmental Testing .- Laboratory Inc. 2834&2908 North Nanmi Strecl, Burhank. CA 91504 -DOHS NO: 1541,LACSD E E ~ ~ D Tel: (888) 288-AETL - (818) 845-8200 9 Fax: (818) 845-8840. www.aet
OCT 2 8 2005
Ordered B
Telephone: (714)985-3434 Attention: Tom Tatnall
Project ID: 32485-000 Project Name: Delphi Syster. COrp.
Site: 1201 N. Magnolia Avenue
Anaheim, CA 92801
Enclosed p l e a s e f i n d r e s u l t s of a n a l y s e s of 2 s o l i d was te samples which were ana lyzed a s s p e c i f i e d on t h e a t t a c h e d c h a i n of c u s t o d y . I f t h e r e a r e any q u e s t i o n s , p l e a s e do n o t h e s i t a t e t o c a l l .
Approved By: -"-3 EE~~w~??Lrp-~~~=~~= ~ .
Cyrus Kazmara, Ph .D.
L a b o r a t o r y D i r e c t o r
Chain of Custody Record
American Environmental Testing Laboratory Inc. 2834 &2908 North Nao~ni Street. Burhank. CA 9 1504- DOHS NO: 1541,1AACSDNO: 10181 Tcl: (888) 288-AETT_.. (818) 845-8200. Pax: (818) 845-8840 - www.aet1ah.com
ANALYTICAL RESULTS Site
00 South I<raemer Bivd.
I
Attn: Tom Tatna i l
Page : 2
Project ID: 32485-000 Project N a m e : Delphi S y s t e m Corp.
Method: (M8015G), TPH as Gasoline and Light Hydrocarbons Using GCIFID QC Batch No: 102005
Y %..I YY ...,,.l" ~- .... ...
; Date Prepared ......
American Environmental Testing Laboratory Inc. 2814 & 2908 North Naorni Strezt, Burbant. CA 91504 - DOHS NO: l541,LACSDrUO: lOl8l Tel : (888) 288-AETL. (818) 845-8200. Fax: (818) 845-8840. wwwazt lab .com
ANALYTICAL RESULTS
Attn: Tom Tat~iall
Page: 3
Project ID: 32486-003 Prqject Name: Delphi System Corp.
American Environmental Testing Laboratory Inc. 2834 8~2908 North Naomi Street. Burhank. CA 91504.I)OHS NO: 1541,LACSDNO: 10181 721: (888) 288-AETL. (818) 845-8200. Fax : (818) 845-8840 - www.actlah.com
ANALYTICAL RESULTS Ordered By
't-idle! & Aldrlch >00 South IKraemer Blvd -iulir 570 Urea CA 92821-6723
Telephone (714)985-3434 A t t ~ l Tom Tatnall
S i t e , . ~~~~. ~~ .. . . ~ . ~~~~~~~~~~~
I201 N. Magnolia Avenue 'Anaheim, CA 92801 I
Page: 4
Project ID: 3 2 4 8 6 - 0 0 0 Project Name: Delphi Sys t em Corp.
~ - -~ ~
Method: (8082), Polychlorinated Biphenyls (PCBs) by GC QC Batch No: 102005
D a t e Prepared IV/LU, L U I - 1. Preparation Methodp-' 1 3 5 5 0 ~ I 3:
b a t e ~ n a l ~ z e d :10/20/2005 ;10/2(
Matrix : .. . .--.---
1~~~ - .. Date Sampled ---
i Date Prepared
American Environmental .- Testing Laboratory Inc. 2834&2908 North Naoini Street, Burbank, CA 91504 .DOHS NO: 1541.1,ACSDNO: 10181 Te l : (888) 288-ACTL . (818) 845-8200. Fax: (818) 845-8840 - www.uet1i1b.com
ANALYTICAL IiESULTS Ordered B y
Haley & Aldrich 1 930 - Soiith Kraemer Blvd Sure 370
I Rrea, CA 9282 1-6723
S i t e
1201 N Magnoha Avenue I Anaheim, CA 9280 1
Telephone: (7 14)985-3434 Attti: Tom Tatnall
Page: 5
Project ID: 32486-000 Project Name: De lph i System Corp.
Method: (8270C), Semivolatile Organic Compounds by GCIMS (SW-846) QC Batch No: 102005
-- Matrix -- Units
Anthracene Azobeiizene Rn,,.riAin,. , , . .. , , , , .' , , , > -~ HenZo(a)imthracene
-- - , Benzo(k)fluoranlhene
,-
~ i s ( 2 - ~ i i l o l - ~ t b o x ~ ) m ~ t h a i 1 e
12-Chloropheiiol 4-Cliiorophmyi pl~eny i ether -
-- iUi-n-odyi phtlialale (Dioctyi estcr) I 0.25 0.50 . ~~~ ~p~ . .~ ~ ~p~- . ,- ~ ~~
American Environmental Testing Laboratory Inc. 2814 8 ~ 2 9 0 8 North Naomi Street. Durbank, CA 91504 -DOHS NO: 1541,L.ACSDNO. 10181 Te l : (888) 288-AETL . (818) 845-8200 Fax: ( 8 1 8 ) 845-8840 www.aet1ab.com
ANALYTICAL RESULTS
Paee: 6 - Project ID: 32486-000 Project Name: Delphi System Corp.
Method: (8270C), Semivolatile Organic Compounds by GC/MS (SW-846) QC Batch No: 102005
I i I 00.01 00.01 - -- .. .__ 1 0 / 1 9 / 2 0 0 5 / 2 0 0 5 1 I...
005 i0/20/2005 ! ~~...
B I 3550% 1 I -- i 005 110/21/2005 I 1
- -. Date Sampled -
' I ) a l e P I e p a i e d I - Preparat~on Method - Date Analyzed -- Matr~x
10/21/2005
Solid Waste
I- 10/21/2
Solid W --
I Dilution Factor
L-P-
llibcnzofuran 'I;:;:~;;;;;;~;:: .- 1,4-Dichlorobenzene . . .
3,3'-llichlorobenzidi~ie -- 2;4-Diclilorophcnol - .- --
Dietliyi phthaidte (Diethyl ester) 1 . . Dirnctliyl phtlialate (Dime
~. i 2,4-Dimelliylphenol 4,6-Diiiitro-2-methyIphend
2.4-Dinitrophmol 1- 2,4-Dinitrotoluenc
~ D i ! ~ i t r o t o l u c n e (2,6-DNT) I 0.25 vl~-- ND
- 10.25 - 0.50 - --
ND I l'luoranthcne .- -A . -, iIiinrei,,r 1 0.25 0.50 1 ND ND 7 7
..... " I-I." ~- --+ ~~
2-~itroaniiine i 0.25 0.50 -. . . . - i- ND I N D T ND I
?-Nitroaniline I .. / N D ,--. - ND ~. , 14-Nitroaniline 0.50 ND ND I ND -. -, - 1 :
0'25 1 0.50
.. ! 4 Nitrobenzene (NR) 0.25 ND ND I m t ~.., I ~.hlii,.,,,,hi.~.ni I 0.25 I 0.50 I ND ND ND
American Environmental Testing Laboratory Inc. 2834&2908 North Naomi Strecl. Burbank. CA 91504 .DOHS NO: 1141,LACSDNO. 10181 Tei: (888) 288-AETL. (818) 845-8200 * Fax: ($18) 845-8840 - www.azrlab.com
ANALYTICAL RESIJLTS
Page: 7
Project ID: 3 2 4 8 6 - 0 0 0 Project Name: D e l p h i System Corp .
Method: (8270C), Seinivolatile Organic Compounds by GCIMS (SW-846) QC Batch No: 102005
..
N-nitrosodiplieiiylan~i~ -- Peniachlorophenol
I'yrcnc
.
American Environmental Testing Laboratory Inc. 2814 &2908 North Nziomi Street, Burbank, CA 91504 -DOHS NO: l541,LACSDNO: 10181 Tel: (888) 288-AET1.v (818) 845-8200. Fax: (818) 845-8840 - www.aet lab.com
ANALYTICAL RESULTS
Ordered By Halev & Aldrich
Si t e
' 1201 N Magnolia Avenue 00 South I<rae~iizr Blvd.
Telephone: (714)985-3434 Attn: Toin Taliiall
Page: 8 32486-000
,-
Method: (8082), Polychlorinated Biphenyls (PCBs) by GC QUALITY CONTROL REPORT -
QC Batch No: 102005 Sample Spiked: 102005 QC Prepared: 10120/2005 QC Analyzed: 1012012005 Units: rnglKg
QC Batch No: 102005 Sample Spiked: 102005 QC Prepared: 10120/2005 QC Analyzed: 1012012005 Units: rnglKg
American - Environmental -. Testing Laboratory Inc. 2834 8 ~ 2 9 0 8 North Naoini Street, Burbank, CA 91504 .DOHS NO: 1541,I.ACSDNQ 10181 Tel: ( 8 8 8 ) 288-AETI. . (818) 8 4 5 - 8 2 0 0 - F a x : ( 8 1 8 ) 845-8840 * www.aet Iab .com
- AKALYTICAL RESULTS
Attn: Tom Tatnall
Site
11201 N Magnoha Avenue Anaheim, CA 92801
Page: 9 32486-000
Method (8270C), Semivolatile Organic Compounds by GCIMS (SW-846) QUALITY CONTROL REPORT
QC Batch No: 102005 Sample Spiked: 102005 QC Prepared: 1012012005 QC Analyzed: 1012112005 Units: mglKg
QC Batch No: 102005 Sample Spiked: 102005 QC Prepared: 1012012005 QC Analyzed: 1012112005 Units: mglKg
Recov % REC % Limit
100.00 110.00 i 11
American Environmental Testing Laboratory Inc. 2834 a2908 Nori l l Nao~n i Street, Bu~.hank, CA 91 504. DONS NO: 1541,I,ACSDNO: 10181 Tel : (888) 288-AETT.. (818) 845-8200 * Pax: (818) 845-8840 0 www.actiab.corn
ANALYTICAI, RESULTS
Ordered By I l ialey & Aldtich 500 South Icraerne~ B l vd
i Su~te 370 'Brra, C A 92821 -6723
Telepllo~ie (714)985-3434 Attn Tom Talnall
Si te
Page: 10 Project ID: 3 2 4 8 6 - 0 0 0 project Name: Deighi System Corp.
Method: (M8015D), TPH as Diesel and I-Ieavy Hydrocarbolls Using GCIFIU
QC Batch No: 102005 Sample Spiked: 34988.02 QC Prepared: 10/20/2005 QC Analyzed: 1012012005 Units: mglKg
QC Batch No: 102005 Sample Spiked: 34988.02 QC Prepared: 1012012005 QC Analyzed: 10/20/2005 Units: mglKg
American -. Environmental Testing Laboratory Inc. 2834&2908 Noi-ti1 Nao~ni Slieer,Rui-hank, CA 91504.DOHS NO: l541,LACSDNO: 10181 Tcl: (888) 288-AETL ' (818) 845-8200 ' F a x : (818) 845-8840 ' www.aetlab.com
AKALYTICAL RESULTS
Telephone: (714)985-3434
Attn: Tom Tali~all
Site r 1201 Pi Magnolra Avenue 1 Anahelm, CA 9280 1
Page: 11 Project ID: 3 2 4 8 6 - 0 0 0
pro'eclName: Delphi System Corp.
Method: (M8015G), TPH as Gasoline and Light IIydrocarbons Using GCIFID QUALITY CONTROL REPORT
QC Batch No: 102005 Sample Spiked: 102005 QC Prepared: 1012012005 QC Analyzed: 1012012005 Units: mglKg
QC Batch No: 102005 Sample Spiked: 102005 QC Prepared: 1012012005 QC Analyzed: 1012012005 Units: mglKg
American Environmental Testing Laboratory Inc. 2834 &2908 North Naorni Strecl. Burbank, CA 91504.DOHS NO: 1541,I~ACSDNO: 10181 Tcl: (888) 288-AET12 * (818) 845-8200 - Fax: (818) 845-8840. www.aetIab.com
Data Qualifiers and 1)escriptors
Data Qualifier:
*.
B:
D:
E :
H:
J:
M:
S6:
S8:
X :
In the QC section, sample results have been taken directly from the ICP reading. No preparation factor has bee11 applied.
Analyte was present in the Method Blank.
Result is from a diluted analysis.
Result is beyond calibration limits and is estimated.
Analysis was performed over the allowed holding time due to circumstances which were beyond laboratory control.
Analyte was detected . However, the analyte collcentration is an estimated value, which is between t11e Method Detection Limit (MDL) and the Practical Quantitation Limit (PQL).
Matrix spike recovery is outside control limits due to matrix interference. 1,ahoratory Control Sample recovery was acceptable.
Surrogate recovery is outside control limits due to matrix interference.
The ailalysis of the sample required a dilution such that the surrogate conceniration was diluted below the method acceptance criteria.
I<esults represent LCS and LCSD data.
%Limi: Percent acceptable limits.
%REC: Percent recovery.
Con.L: Acceptable Control Limits
Conce: Added concentration to the sample
LCS: Laboratory Control Sample
MDl.,: Method Detection Limit is a statistically derived number which is specific for each instrument, each method, and each compound. It indicates a distinctively detectable quantity with 99% probability.
MS: Matiix Spike
MS Dli: Matl-ix Spike Duplicate
American Environmental Testing Laboratory Inc. 2834 &2908 Norti, Naorni Strcel. Burbank, CA 91504 'DOHS NO: 1541,I.ACSDNO: 10181 Tel: (888) 288-AETL - 1818) 845-8200 . Fax: (818) 845-8840 www.aetlab.com
Data Qualifiers and Descriptors
ND : Ailalyte was not detected in the sample at or above MDL
PQL: Practical Qua~~titation Limit or ML (Minimum Level as pcr RWQCB) is the minimum co~lcentration that can
be quantified with Inore than 99% confidence. Taking into account all aspects of the entire analytical i~~strumentation and practice.
Recov: Recovered concentration in the sample.
RPD: Relative Percent Difference
American Environmental Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (8 18) 845-8200 Fax: (8 18) 845-8840 www.aetlab.com a
To: Tom Tatnall
From: Dr. Cyrus Razmara, AETL
Date: November 16, 2005
Subiect: Correction of Qualifier for Surrogates
RECEIVED
NOV 2 1 2009
Haley & Aldrich, Inc.
This package contains revised final report pages. These pages should replace previously released data for the AETL job number listed below. For your reference, a copy of the Chain-of-Custody form that lists the job number and your project information is attached. If you have any questions, please contact me. Thank you.
Revisions:
AETL Job Number: 34986
For pages 5 to 7
Cyrus RazGra, Ph.D. Laboratory Director
Client
Haley & Aldrich Address
500 S. Kraemer Blvd., Suite 370
m 2 4 ~ o u m 0 4 8 ~ o u r s O 7 ~ a y s 0 1 4 Days 0 2 1 Days nothers
Project Manager
Tom Tatnall Telephone Number (Area Code)
(714) 985-3434 Cay
Brea
o ~ o n - H a w r d O~ lammabk D ~ k i n Irritant t l ~ o b o n B m ~ n k n o w n
I I !page I of I
o ~ e t u r n TO client ~ ~ i s ~ o s a l ~ y Lab O ~ r c h i v e For Months
Laboratory Name
AETL
Laboralw Address 8 Tekphone Number 2834 Naomi St.. Burbank CA 91504 Tel: (am, w.szoo
ho@ Name and L o w t m (Stale)
Delphi, Anaheim CA
State
CA Site Contact
T. Tatnall ZqCode
9282 1
Turn Around Time Required
Date
1011912005
Lab Number
LabContacf
Jim Lin
ContracWmhase Ordermuote No
OC Requiremenls (Specify)
Custody Number
HA-000032
Carrk?rM/ayb~U
3Y984- o l 3\1486- 02,
relamed Months longer Ulan 1 m U 7 )
~2 2
: X
Sample / D. No. and Descnpbon (Containers for eacb sample may be combln on one Ime)
CSOOl7~CC~OOO~Ol
csool8~cc~ooo~ol
Possibk Hazard ldenfdicalan
0 ' 0 '
Analysls (Attach 11st dmore space IS needed)
Matnx
Specml InslNUanslCondilcm of Recerpl
g 2
q k q 4 s a
Q O Z 2 X
X X X
Date
1011 912005
1011 912005
2
Preservabves Containers
Time
12 40
12 45
$ 2
$ 2 1
1
$ 2
E X
5 s
Sample (A fee may be assessed rf samples are
5 c4
8 $
$,
Dsposal
0
x X
2 8 ' 8 8 T 6
American Environmental Testing Laboratory Inc. 2834 & 2908 North Naomi Street, Burbank, CA 91504 DOHS NO: 1541, LACSD NO: 10181 Tel: (888) 288-AETL (818) 845-8200 Fax: (818) 845-8840 www.aetlab.com
ANALYTICAL RESULTS O r d e r e d Bv S i t e
I Waley & Aldrich 500 South Kraemep Blvd. / Suite 370
' Brea, - - CA 92821-6723 - -. - - -
- --
Anaheim, CA 9280 1
- - -. -- - -
Telephone: (71 4)985-3434 Attn: Tom Tatnall
Page: 5
Method: (8270C), Semivolatile Organic Compounds by GCIMS (SW-846) QC Batch No: 102005
/ Client Sample I.D. I I / CSOO17-CC-01 CSOO18-CC-01 1 1
pk"18n't H &A
Project ID: 32486-000 Project Name: Delphi System Corp.
I I
Anw&$tes MDL PQL 1 d s u l ~ s Reqults R e q y k t s 1 Acenaohthene 0 . 2 5 1 0 . 5 0 1 ND ND ND
I ' rar~ $I& ' jtab %yt@@$f& 34986
;'I-=
10/19/2005
Acenaphthylene
Benzidine 0 . 2 5 0 . 5 0 ND ND ND
Benzo(a)anthracene 0 . 2 5 1 0 . 5 0 1 ND ND ND
1 Azobenzene I I I I I I I
0 . 2 5
0 . 2 5 1 0 . 5 0 1 ND
L \-2 , ,. d
Benzo(k)fluoranthene Benzoic Acid Benzvl Alcohol
/ Butyl benzyl phthalate / 0 . 2 5 1 0 . 5 0 1
0 . 5 0
ND
ND
I
I ND ND ND
) ND ND ND
4-Chlorophenyl phenyl ether 0 . 2 5 0 . 5 0 ND ND ND
0 . 2 5 0 . 5 0 ND ND ND
ND Anthracene ND
J ., Bis(2-chloroisopropyl) ether Bis(2-ethylhexyl) phthalate 4-Bromophenyl phenyl ether
1 Di-n-octyl phthalate (Dioctyl ester) 0 . 2 5 0.5C
ND
0 . 2 5 1 0 . 5 0 1 ND
1
ND
ND
ND
0 . 2 5
0 . 2 5
0 . 2 5
0 . 2 5
0 . 2 5
0 . 2 5
ND
0 . 5 0
0 . 5 0
0 . 5 0
. - ND
/ 4-Chloro-3-methvl~henol 0 . 2 5 1 0 . 5 0 1 ND
ND
ND
ND
ND
0 . 5 0
0 . 5 0
0 . 5 0
ND
ND
ND
1.91
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Page: 6
American Environmental Testing Laboratory Inc. 2834 & 2908 North Naomi Street, Burbank, CA 91504 DOHS NO: 1541, LACSD NO: 10181 Tel: (888) 288-AETL (81 8) 845-8200 Fax: (8 18) 845-8840 www.aetlab.com
Project ID: 32486-000 Project Name: Delphi System Corp.
ANALYTICAL RESULTS
I I I
Method: (8270C), Semivolatile Organic Compounds by GCIMS (SW-846) QC Batch No: 102005
- .- -. - , Our Lab I.D. [ ~ e t h o d ~lankf 34986.01- -- 1 - . .. . 34986102 - 1 / Client Sample I.D. 1 1 /CSOO~~-CC-O~CSOO~~-CC-O~ 1 1
1 Matrix I I Solid Waste I Solid Waste / Solid Waste I 1 1
,
Date Sampled Date Prepared Pre~aration Method
Units I mg/Kg I m a g / mgKg I
Dibenzofuran
10/20/2005
3550B
3-Dichlorobenzene ,4-Dichlorobenzene
3,3'-Dichlorobenzidine 2,4-Dichlorophenol Diethyl phthalate (Diethyl ester)
Dilution Factor
0.25
Dimethyl phthalate (Dimethyl ester) 2,4-Dimethy lphenol 4.6-Dinitro-2-methylphenol
10/19/2005
10/20/2005
3550B
1 I 1 I 1 /
1.2-Dichlorobenzene 0.25
0.25
0.25
0.25
0.25
Fluoranthene
10/19/2005
10/20/2005
3 5 5 0 ~
0.50
0.25
0.25
0.25
Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene
0.25 1 0.50 1 ND
0.50
0.50
0.50
0.50
0.50
0.25
I
I
ND
0.50
0.50
0.50
Fluorene 0.25
0.25
0.25
3-Nitroaniline 4-Nitroaniline Nitrobenzene (NB) 4-Nitrophenol
ND
ND
ND
ND
ND
ND
0.50
ND
ND
ND
ND
ND
0.25 1 0.50 1 ND
0.50
0.50
0.50
0.25
0.25
0.25
0.25
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.50
0.50
0.50
0.50
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
American Environmental Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (818) 845-8200 Fax: (818) 845-8840 www.aetlab.com
ANALYTICAL RESULTS
Page: 7
Method: (8270C), Semivolatile Organic Compounds by GCIMS (SW-846) QC Batch No: 102005
Project ID: 32486-000 Project Name: Delphi System Corp.
Units Dilution Factor 1 I 1 I 1 I
d?4e&ibmb Hmi@p=. 34986
Date Sampled Date Prepared Preparation Method Date Analyzed Matrix
- . - I I ,
Analytes MM, PQL 1 Results 1 Results / Results I
1 Pentachlorophenol 1 0.25 / 0.50 / ND I ND / ND I I I
i%&- 10/19/2005
10/20/2005
3 5 5 0 ~
10/21/2005
Solid Waste
H &A
00-01 10/19/2005
10/20/2005
3 5 5 0 ~
10/21/2005
Solid Waste
00-01 10/19/2005
10/20/2005
3 5 5 0 ~
10/21/2005
Solid Waste