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Depositional and Dewatering Behaviour of Uranium Mill Tailings A Thesis Submitted to the Faculty of Graduate Studies and Research In Partial Fulfillment of the Requirements For the Degree of Master of Applied Science in Environmental Systems Engineering University of Regina By Md. Imteaz Ferdoush Bhuiyan Regina, Saskatchewan August, 2014 Copyright 2014: Md. Imteaz Ferdoush Bhuiyan

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Page 1: Depositional and Dewatering Behaviour of Uranium Mill Tailings A …ourspace.uregina.ca/bitstream/handle/10294/5813/Bhuiyan_MdImtea… · final void ratio (ef) from 8 to 4 (30%

Depositional and Dewatering Behaviour of Uranium Mill Tailings

A Thesis

Submitted to the Faculty of Graduate Studies and Research

In Partial Fulfillment of the Requirements

For the Degree of

Master of Applied Science

in

Environmental Systems Engineering

University of Regina

By

Md. Imteaz Ferdoush Bhuiyan

Regina, Saskatchewan

August, 2014

Copyright 2014: Md. Imteaz Ferdoush Bhuiyan

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UNIVERSITY OF REGINA

FACULTY OF GRADUATE STUDIES AND RESEARCH

SUPERVISORY AND EXAMINING COMMITTEE

Md. Imteaz Ferdoush Bhuiyan, candidate for the degree of Master of Applied Science in Environmental Systems Engineering, has presented a thesis titled, Depositional and Dewatering Behaviour of Uranium Mill Tailings, in an oral examination held on August 1, 2014. The following committee members have found the thesis acceptable in form and content, and that the candidate demonstrated satisfactory knowledge of the subject material. External Examiner: Dr. Hussameldin Ibrahim, Industrial Systems Engineering

Supervisor: Dr. Shahid Azam, Environmental Systems Engineering

Committee Member: *Dr. Tsun Wai Kelvin Ng, Environmental Systems Engineering

Committee Member: Dr. Ezeddin Shirif, Petroleum Systems Engineering

Chair of Defense: Dr. Shelagh Campbell, Faculty of Business Administration *Not present at defense

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ABSTRACT

The Key Lake operation in Saskatchewan, Canada, is the largest uranium mill in the

world. This mill process generates tailings that are deposited into an onsite storage area

called the Deilmann Tailings Management Facility (DTMF). An effective tailings

management scheme requires a clear understanding of slurry behaviour throughout the

life-cycle, starting from production thorough the deposition to dewatering in the storage

facility. The main objective of this research was to investigate the depositional and

dewatering behaviour of uranium mill tailings (4%, 5%, and 6% mill tailings) from the

Key Lake operation under laboratory and field conditions. All of the samples exhibited

the same trend for yield strength development during the tests for rheological properties.

A negligible strength (0.4 kPa) was found to have at 60% solids content (s) followed by a

rapid increase thereafter. The settling and segregation tests were performed under

different initial solids contents (si). The 4% mill tailings exhibited a lower rate and total

amount of settlement than 5% and 6% mill tailings in the settling tests. The initial

hydraulic conductivity (ki) decreased by two orders of magnitude (10-2 m/s to 10-4 m/s)

with a decrease in initial void ratio (ei) from 16 to 4 (15% < si < 40%) and a decrease in

final void ratio (ef) from 8 to 4 (30% < si < 45%) such that 4% mill tailings showed one

order of magnitude lower values than the 5% and 6% mill tailings. The corresponding

settling potential (SP) decreased ten times (50% to 5%) for 4% mill tailings and four

times (60% to 15%) for 5% and 6% mill tailings. The effective stress (σ') increased from

80 Pa to 260 Pa in the settling tests. The average solids content after settling was 35%

(20% < s < 42%) for 4% mill tailings, 40% (15% < s < 60%) for 5% mill tailings, and

39% (18% < s < 54%) for 6% mill tailings with a corresponding normalized solids

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content deviation of ±3%, ±8%, ±6%, respectively. The 4% tailings were less prone to

segregation when compared with 5% and 6% tailings. Nevertheless, all materials were

essentially non-segregating at 40% initial solids content. The large strain consolidation

tests were conducted by using a customized and fabricated consolidation test system.

During the tests, the total strains were 31% to 42% for all investigated mill tailings in an

effective stress range of 0.3 kPa to 8 kPa. The change in void ratio was higher for 4%

mill tailings (Δe = 2.5) than 5% and 6% mill tailings (Δe = 1.3 to 1.7). The lowest

measurable effective stress was 0.3 kPa for all investigated mill tailings. The void ratios

were found to be 3.8, 3.1, and 3.4 at σ' of 1 kPa and further reduced to 3.3, 2.8, and 3.1 at

σ' of 8 kPa for 4%, 5%, and 6% mill tailings. The k values showed an initial scatter

before attaining a steady value and were found to range from 10-7 m/s to 10-8 m/s. The test

results provided the volume compressibility and hydraulic conductivity relationships for

current (4%) and future (5% and 6%) mill tailings. The large strain consolidation

behaviour in the DTMF was investigated by analyzing survey data from 1996 to 2008,

laboratory testing of the current (4%) mill tailings, and history matching of the deposited

tailings using numerical modeling. The numerical modeling results closely approximated

the consolidated tailings elevations and effective profiles in the DTMF over the period of

1996 to 2008. The field effective stress values correlated quite well with the modeling

results thereby validating the predictions. Overall, the results indicate that the effective

stress increased from 0 kPa at the surface to the following values at the DTMF bottom:

200 kPa in 1999, 530 kPa in 2005, and 680 kPa in 2008.

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ACKNOWLEDGEMENTS

I would like to acknowledge and express my profound gratitude to my supervisor,

mentor, and coach, Dr. Shahid Azam, for his persistent guidance, support, and

encouragement throughout my graduate studies at the University of Regina. Without his

constructive criticism and timely suggestions, this endeavour would not have been

successful. I am very thankful to him for the academic training and industrial research

opportunity from which I have gained professional knowledge to advance my career.

My sincere thanks to Cameco Corporation, Canada, for providing materials and

financial assistance. I am grateful to Dr. Patrick Landine and Dr. Jeff Warner from

Cameco Corporation for their suggestions on this work from an industrial perspective.

Thanks are also given to the Natural Sciences and Engineering Research Council and the

Faculty of Graduate Studies and Research for additional financial supports and to the

University of Regina for providing computing and research facilities.

I feel very much indebted to my parents, Abdul Awal Bhuiyan and Ferdoushi

Awal, for their boundless love and blessings. Without their greatest motivation and

encouragement, it would have been impossible for me to complete this research.

Additionally, I am very thankful to all my fellow colleagues and friends for their

generous help and encouragement throughout the coursework and this research. Special

thanks to my sisters Sayeda Fatema and Tahmina Chowdhury and my friend Shifullah

Md Khaled for their inspiration during this journey.

Finally I wish to thank my best friend and my Asma Chowdhury who has

provided me with continual encouragement, support, patience, and love, enabling me to

complete my graduate work. Without you, I would be lost.

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POST DEFFENCE ACKNOWLEDGEMENTS

The time and inputs of Dr. Hussameldin Ibrahim (external examiner) from the Faculty of

Engineering and Applied Science, Dr. Kelvin Ng (supervisory committee member) and

Dr. Ezeddin Shirif (supervisory committee member) from the Faculty of Engineering and

Applied Science, and Dr. Shelagh Campbell (thesis defense chair) from the Faculty of

Business Administration are appreciated for serving on my thesis committee.

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TABLE OF CONTENTS

ACKNOWLEDGEMENTS ............................................................................................ iv

POST DEFFENCE ACKNOWLEDGEMENTS ........................................................... v

TABLE OF CONTENTS ................................................................................................ vi

LIST OF FIGURES ......................................................................................................... ix

LIST OF ABBREVIATIONS ......................................................................................... xi

CHAPTER 1 ...................................................................................................................... 1

INTRODUCTION .......................................................................................................... 1

1.1 Problem Statement .................................................................................................... 1

1.2 Research Objective ................................................................................................... 3

1.3 Thesis Outline ........................................................................................................... 3

CHAPTER 2 ...................................................................................................................... 4

LITERATURE REVIEW ............................................................................................... 4

2.1 General ...................................................................................................................... 4

2.2 Industrial Practice ..................................................................................................... 6

2.2.1 Mining operation ................................................................................................ 6

2.2.2 Tailings production ............................................................................................ 8

2.2.4 Tailings Segregation ........................................................................................ 14

2.2.5 Tailings Dewatering ......................................................................................... 15

2.3 Rheology ................................................................................................................. 16

2.4 Segregation ............................................................................................................. 17

2.5 Dewatering .............................................................................................................. 21

2.5.1 Self-Weight Settling......................................................................................... 21

2.5.2 Large Strain Consolidation .............................................................................. 22

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CHAPTER 3 .................................................................................................................... 26

RESEARCH METHODOLOGY.................................................................................. 26

3.1 General .................................................................................................................... 26

3.2 Uranium Mill Tailings ............................................................................................ 26

3.2.1 Material Properties ........................................................................................... 26

3.2.2 Safety protocol ................................................................................................. 27

3.3 Laboratory Investigation ......................................................................................... 28

3.3.1 Rheological Test .............................................................................................. 28

3.3.2 Settling Test ..................................................................................................... 28

3.3.3 Segregation Test............................................................................................... 30

3.3.4 Large Strain Consolidation Test ...................................................................... 31

3.3.4.1 Fabrication of Apparatus........................................................................... 31

3.3.4.1 Consolidation Test .................................................................................... 37

3.4 Numerical Modeling ............................................................................................... 38

CHAPTER 4 .................................................................................................................... 43

RESULTS AND DISCUSSION ................................................................................... 43

4.1 General .................................................................................................................... 43

4.2 Depositional Behaviour .......................................................................................... 43

4.2.1 Rheological Properties ..................................................................................... 43

4.2.2 Initial Hydraulic Conductivity ......................................................................... 45

4.2.3 Settling Potential .............................................................................................. 48

4.2.4 Effective Stress ................................................................................................ 48

4.2.5 Segregation Behaviour ..................................................................................... 50

4.3 Dewatering behaviour ............................................................................................. 55

4.3.1 Large Strain Consolidation .............................................................................. 55

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4.3.2 Volume Compressibility and Hydraulic Conductivity Relationships .............. 59

4.4 Consolidation Behaviour in the DTMF .................................................................. 61

4.4.1 Tailings Deposition .......................................................................................... 61

4.4.2 Numerical Modeling Results ........................................................................... 64

CHAPTER 5 .................................................................................................................... 68

CONCLUSIONS AND RECOMMENDATIONS ....................................................... 68

5.1 Conclusions ............................................................................................................. 68

5.2 Recommendations ................................................................................................... 70

REFERENCES ................................................................................................................ 71

APPENDIX A .................................................................................................................. 83

APPENDIX B ................................................................................................................ 102

APPENDIX C ................................................................................................................ 121

APPENDIX D ................................................................................................................ 140

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LIST OF FIGURES

Figure 2.1: Uranium mining in Saskatchewan.................................................................... 5

Figure 2.2: Simplified flowchart of uranium mining operation.......................................... 7

Figure 2.3: Schematic of uranium mill tailings production.............................................. 10

Figure 2.4: The pervious surround concept in tailings disposal facility........................... 13

Figure 2.5: Typical Segregation process in the settling column and tailings disposal

facility............................................................................................................................... 19

Figure 3.1: Schematic of the large strain consolidation test system................................. 32

Figure 3.2: Calibration of devices used for the consolidation test................................ 36

Figure 3.3: Numerical modeling scheme.......................................................................... 39

Figure 4.1: Yield stress versus solids content for the investigated mill tailings............... 44

Figure 4.2: Initial hydraulic conductivity with respect to the following: (a) initial void

ratio (b) initial solids content (c) final void ratio (d) final solids content......................... 46

Figure 4.3: Settling potential with respect to the following: (a) initial void ratio (b) initial

solids content (c) final void ratio (d) final solids content................................................. 47

Figure 4.4: Final effective stress with respect to the following: (a) initial void ratio (b)

initial solids content (c) final void ratio (d) final solids content....................................... 49

Figure 4.5: Solids content versus normalized solids content deviation............................ 51

Figure 4.6: Fines content versus normalized solids content deviation..............................53

Figure 4.7: Initial solids content versus segregation......................................................... 54

Figure 4.8: Settling curves: (i) Interface height (ii) void ratio and (iii) solids content

versus elapsed time during large strain consolidation test for (a) 4% (b) 5%, and (c) 6%

mill tailings....................................................................................................................... 56

Figure 4.9: Hydraulic conductivity versus time data in large strain settling test.............. 58

Figure 4.10: Volume compressibility and hydraulic conductivity relationship................ 60

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Figure 4.11: Schematic of DTMF (a) Plan (b) Section A-A' (c) Section B-B' of

consolidated tailings elevations; and (c) Section B-B' of consolidated tailings

elevations.......................................................................................................................... 62

Figure 4.12: Historical tailings elevation in the DTMF from 1996 through

2008.................................................................................................................................. 63

Figure 4.13: History matching of tailings elevation in the DTMF from 1996 through

2008................................................................................................................................... 65

Figure 4.14: Effective stress profiles in the DTMF: (a) 1999 borehole investigations; (b)

2004/05 borehole investigations; and (c) 2008 borehole

investigations.................................................................................................................... 66

Figure D1: Grain size distribution curves of 4%, 5% and 6% mill tailings (GSD test data

reported by Khaled (2012), reproduced with permission from the author).................... 139

Figure D2: Determination of initial hydraulic conductivity from settling test (data

reported by Khaled (2012), reproduced with permission from the author).................... 140

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LIST OF ABBREVIATIONS

AGTMF: Above Ground Tailings Management Facility

BaCl2: Barium Chloride

CCD: Counter Current Decantation

cv : Coefficient of Consolidation

DTMF: Deilmann Tailings Management Facility

DS: Degree of Saturation

e: Void Ratio

��∗: Void Ratio at Fluid Limit

ef : Final Void Ratio

ei : Initial Void Ratio

∆e: Difference of Initial and Final Void Ratio

f: Fines Content

Gs: Specific gravity of solids

GSD: Grain Size Distribution

h: Height of the Slurry Sediment

h1: Initial Hydraulic Head

h2: Final hydraulic head

hi / ht: Normalized Height of the Slurry

k: Hydraulic Conductivity

ki : Initial Hydraulic Conductivity

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masl: Meters above Sea Level

(NH4)2SO4: Ammonium Sulphate

pH: Measure of Acidity or Alkalinity

r2: Coefficient of Determination

S: Segregation

s: Solids Content

si : Initial Solids Content

Savg: Average Solids Content of the sediment

Sd: Solids Content Deviation

u: Pore Pressure

U3O8: Yellowcake/ Triuranium Octoxide

Vs : Settling Velocity

w: Gravimetric Water Content

WNA: World Nuclear Association

σ': Effective Stress

T: Time Factor

τy: Yield Stress

�s: Unit Weight of Solids

�w: Unit weight of Water

ζ : Consolidation Ratio

: Relative Degree of Compression

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CHAPTER 1

INTRODUCTION

1.1 Problem Statement

The Key Lake operation in Saskatchewan, Canada, is the largest uranium mill in the

world (Cameco, 2012), producing 13% of the world’s uranium (World Nuclear

Association, 2012). The Key Lake site receives high grade ores (up to 21% U3O8 in 2010,

as reported by Yun et al. (2011)) from McArthur River, which are diluted to a nominal

4% grade using Deilmann special waste, Gaertner special waste, and mineralized waste

from McArthur prior to milling. Currently, Cameco is assessing the feasibility of milling

higher grade of ore up to 6% U3O8. Mill tailings refer to the solid waste materials that

result from the processing of the uranium ore. The tailings management is an essential

activity related to ore processing at the Key Lake operation since the storage capacity of a

tailings management facility depends on the dewatering behaviour of the deposited

material (Ito and Azam, 2013).

The geotechnical investigations on depositional and dewatering behaviour of

uranium tailings are hardly observed in the literature. Previous geotechnical

investigations on uranium tailings include the following: liquefaction assessment of

tailings embankment at Elliot Lake, Ontario (Matyas et al., 1984), tailings consolidation

at Thuringia, Germany (Wales et al., 2000), historical tailings performance at Key Lake,

Saskatchewan (Azam et al., 2014), and a summary of experience with containment

facility design in Saskatchewan (Mittal and Landine, 2013). Most such studies have

focused on tailings behaviour in the containment facilities. An efficient containment

design requires a clear understanding of slurry behaviour throughout the tailings life-

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cycle starting from tailings production thorough the deposition to dewatering in the

containment facilities. Rheological properties are important in optimizing slurry transport

through pipes to the disposal areas. In Key Lake operations, tailings are pumped from the

mill to a thickener (achieves a solids content of 35% to 40%), and subsequently deposited

from the thickener underflow to the containment facility, called the Deilmann Tailings

Management Facility (DTMF). Post-deposition, tailings segregate due to preferential

settling of coarse particles with respect to the fines. This process affects the rate and

amount of tailings dewatering, thereby influencing the storage capacity of the

containment facility. Furthermore, the segregated tailings can produce zones of higher

and lower hydraulic conductivity, which could result in higher fluxes through the slurries

after closure of tailings management facility.

The DTMF is currently approved to store tailings up to a consolidated elevation

of 466 masl. According to Cameco (2010a), the total volume of sediments was estimated

to be 6.66 × 106 m3 in the DTMF. Based on current production plans, additional tailings

storage capacity is required to support a continued operation of the mill. An

environmental assessment is currently being conducted by Cameco to evaluate the

potential impact and feasibility of raising the final elevation of consolidated tailings to

505 masl. In order to ensure the efficient use of storage facility for different production

and mining schedules, a clear understanding of the tailings dewatering behaviour is

required for the current mill tailings (4%) and future (5% and 6%) mill tailings.

Therefore, there is a need to investigate the tailings dewatering behaviour and assess the

historical dewatering performance in the DTMF.

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1.2 Research Objective

The main objective of this study was to investigate the depositional and dewatering

behaviour of current (4%) and future (5% and 6%) mill tailings. The specified objectives

are as follows:

To investigate the depositional behaviour of uranium mill tailings by laboratory

tests (rheological, settling, and segregation).

To examine the dewatering behaviour (volume compressibility, hydraulic

conductivity, and numerical modeling of consolidation) of uranium mill tailings

in the Deilmann Tailings Management Facility (DTMF).

1.3 Thesis Outline

This thesis is comprised of five chapters. A brief description of each chapter is outlined

as follows: Chapter 1 provides an introduction to the research and establishes the need,

and research objectives of this work. Chapter 2 presents the literature review related to

industrial operation of uranium mining, theoretical background of depositional and

dewatering behaviour, and a review of tailings production and disposal practices. The

geotechnical issues, challenges of tailings management in finite storage capacity are

highlighted. Chapter 3 outlines the research methodology of this work. The laboratory

investigation methods, fabrication of large strain consolidation test system, and the

numerical modeling procedure were discussed in this chapter. Chapter 4 presents the

results and discussion of laboratory investigations and the results of numerical modeling

for consolidation behaviour in the DTMF. Chapter 5 summarizes the main conclusions

obtained from this research and provides recommendations for future work. This is

followed by a list of references and appendices.

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CHAPTER 2

LITERATURE REVIEW

2.1 General

In the 1950s, the emergence of civil nuclear power reactors demonstrated an enormous

potential of nuclear fission for generating electricity. From a small beginning in 1951,

when four light-bulbs were lit with nuclear electricity, the nuclear power industry

currently supplies about 11% of global electricity from 437 nuclear power reactors world-

wide (WNA, 2013; Cameco, 2014). There was a big gap between the world uranium

supply and reactor requirements since 1990s. The world total uranium production was

about 30,000 tonnes in 1995 (50% of global demand), which was found about twice as

58,394 tonnes in 2012 (WNA, 2013). Many companies over the globe are currently

extending their mill facilities and opening up of new mine sites due to this increasing

demand for uranium.

Canada is a major mineral producer, and mining is a major contributor to the

country's economy. Canada produced 15% of world total production in 2012, and most

uranium is generated from mines in northern Saskatchewan. McArthur River, the world's

largest mine was the source of 7,520 tonnes of uranium, processed at the Key Lake mill

facility in northern Saskatchewan (WNA, 2013). The Athabasca basin in northern

Saskatchewan, Canada, (shown in Figure 2.1), has the world's richest uranium ore

reserve. The ore grades (about 16%) at this deposit are 100 times higher than the world

average (Cameco, 2014). Recently, a new uranium mine has begun operation at Cigar

Lake in Canada, due to an increasing uranium requirement over the world.

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Figure 2.1: Uranium mining in SaskatchewanResearch and Response Applications (TERRA) laboratory,

Uranium mining in Saskatchewan (Data source: TerraServer, The Environmental Research and Response Applications (TERRA) laboratory, University of Regina)

5

The Environmental University of Regina)

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2.2 Industrial Practice

2.2.1 Mining operation

Uranium mining uses the same processes used to mine many other metals such as copper,

gold, or nickel, etc. Figure 2.2 shows a simplified flow chart of uranium ore processing

from mining to the production of concentrate (U3O8). Mining process is done in one of

the three ways depending on ore deposit type. Open pit and underground mining are the

conventional uranium mining methods. Open pit mining is used for relatively shallow

deposits, generally less than 100 metres deep. It is generally not economical to use the

open pit mining to extract uranium from an ore body located more than 100 meters below

the surface. Underground mining methods are used in this case however the ore deposit

grade should be higher on this method. In-situ leach method is used for uranium deposits

located below the water table in a confined aquifer. This process dissolves the uranium

while still underground and then pumps a uranium-bearing solution to the surface for

milling. For example, the high grade ore deposits in McArthur River are located between

400 and 600 metres below the surface and underground mining method is used for this

mining operation (Cameco, 2014). The conventional mining and in-situ leach mining

methods produced 49% and 44% of world uranium production respectively and

remaining amount is produced by-product (WNA, 2013).

After mined out the uranium deposits, ores are processed in the mill facility. The

Key Lake mill process is a typical example of uranium milling operation. This mill

receives ore from on site deposits and from McArthur River mine. The process comprised

of the following components: crushing and grinding, sulphuric acid leaching, counter

current decantation, solvent extraction, yellowcake precipitation, and product

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Figure 2.2: Simplified flowchart of uranium mining operation (after WNA, 2013)

Open pit mining

Undergorundmining

Crushing &grinding

Leaching

Seperate solidsTailings production

& disposal

Extract U in liquor

Recyclebarren liquor

PrecipitateUranium

Separate solids

Recyclebarren liquor

Drying

Uranium oxide concentrate U3O8 (yellowcake)

Conains approximately 85% by weight of uranium

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crystallization. In the first stage, large chunks of Key Lake special waste rock are crushed

and blended with mineralized wastes from McArthur River using mill process water. The

resulting slurry is mixed with the high grade McArthur River ore slurry and Falcon

concentrator rejects. The Falcon concentrator separates uranium-rich materials from

concrete-rich materials contained in the mineralized waste rock from McArthur River.

The uranium-rich materials are fed to the mill along with the ore whereas the rejects are

mixed with the tailings (Cameco 2010a). Through a combination of atmospheric and

pressure leaching process using sulphuric acid, the uranium is dissolved, along with other

metals and salts. The slurry is then transferred to the counter current decantation circuit.

This circuit completes the leaching process and separates the barren solids from the

uranium bearing solution through a series of thickeners (circular vessels with inverted

conical bases). The wash solution is gradually impregnated with uranium as it flows

downstream. The pregnant solution is clarified by passing through sand filters, that is fed

to the solvent extraction circuit for purification and concentration through selective

extraction from the pregnant liquor. Uranium is then stripped off the aqueous solution

using (NH4)2SO4 and the loaded strip solution is precipitated as yellowcake. This material

is converted to uranium oxide concentrate (U3O8) by heating to 800oC in the calcining

circuit and the product is put in drums for shipment. The uranium oxide concentrate

(U3O8) contains approximately 85% by weight of uranium.

2.2.2 Tailings production

The uranium content of the ore is often between only 0.1% and 0.2% (WISE Uranium,

2014). Therefore, the amount of tailings generated is nearly the same as that of the ore

milled. At a grade of 0.1% uranium, 99.9% of the material is left over. A large amount of

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tailings produced from uranium milling process and these tailings are generally

engineered on-site (thickening using polymers, pH adjustment using BaCl2) before

depositing into the disposal facility.

Figure 2.3 is a simplified schematic of the tailings production process in the Key

Lake mill facility. Refer back to the Key Lake mining operation on previous section, the

slurry (leach residue) from the counter current decantation (CCD) circuit, the underflow

streams from bulk neutralization thickeners, and underflow solids from clarifier tank after

pH adjustment, are fed to a mix box (tailings feed box). The bulk neutralization process

consists of a series of four neutralization pachucas (high narrow tank with air agitation)

followed by a molybdenum/selenium removal thickener. The pH adjustment is done

using two small air-agitated tanks and a clarifier tank. The tailings neutralization section

consists of a small splitter tailings feed box and two large agitated tailings holding tanks

connected to the tailings pumps. The combined slurry flows to the two tailings holding

tanks where it is adjusted to a pH of 10.5 to 11.0 using lime (Shaw et al., 2011) and such

that the elevated pH values were used to raffinate and precipitate minerals present in

tailings (Mahoney et al., 2006). The slurry is then pumped to a 30 m diameter thickener

where it achieves a solids content of 35 to 40%. Depending on a varieties of factors (such

as mineralogy, extraction process, degree of grinding, specific gravity, and grain size

distribution), tailings are thickened at different solids content prior to disposal in order to

get better performance in the disposal facility (Palkovits, 2007).

2.2.3 Tailings Disposal

Tailings usually exhibit non-Newtonian behaviour, which requires an understanding of

the rheological behaviour in order to economically pump the material from the thickener

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Figure 2.3: Schematic of uranium mill tailings production

Molybdenum and Selenium Thickener

Underflow

Lamela ThickenerUnderflow

Clarifier Tank Underflow

Counter Current Decantation Underflow

Tailings Feed Box

Barium Chloride (BaCl2)

Tailings Tanks

Tailings Thickener(35-40% Solids)

Lime

Slurry

Slurry Slurry

Slurry

Deilmann Tailings Management Facility ( DTMF )

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to the disposal (Sofra and Boger, 2002). The rheological behaviour of various tailings is

not unique in mining different industry (Boger, 2013; Mihireitu, 2009). Depending on

rheological behaviour, tailings are thickened at an optimal solids content so that it can be

pumped or transposed in a financially viable way (Boger et. al, 2002). The rheological

properties of the slurry can also be engineered to deposit tailings without segregation and

to increase consolidation of the overall slurry by storing the fine particles in the voids of

the larger grains (Talmon et. al, 2014). Tailings in slurry form are usually pumped from

mill and disposed to containment facility using either subaqueous or sub-aerial

techniques. Sub-aerial deposition is a technique to disposed tailings above the water line

or on the ground. This method is generally exercised at tailings facilities that have

multiple outlets or points of discharge. The frequency of discharge point rotation and the

number of deposition zones is dependent on the climate, production rate of tailings,

drying characteristics of tailings and the shape of disposal facility (Gipson 1998).

Subaqueous deposition is a method tailings disposal under water and recommended for

those tailings having potential of producing acid by oxidizing (Tremblay, 1998). This

method is also used for uranium tailings to reduced radon exposure from the tailings

surface (Mittal and Landine, 2013).

In milling process at Key Lake, the thickener underflow (final tailings) is

transferred using positive displacement pumps to the disposal facility. There are two

Gould’s SRL heavy duty slurry pumps are used under the thickener for pumping tailings

to the spigots in the disposal facility. The pipe distance from the thickener to the

discharge point for each active spigot is about 2 kilometres. Tailings are being deposited

using a single tremie pipeline and tailings deposition barge at end of each spigot. The end

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of the pipe is submerged about 2 m below of the tailings surface to prevent free fall of

thickened tailings (Mittal and Landine, 2013).

In the 1950s and 1960s, the tailings management practices were found to be

consisted of finding the cheapest way of taking the waste away from mill to the most

convenient topographic depression (Landine and Moldovan, 2010). For example,

uranium tailings were being deposited to Fookes Lake adjacent to the Beaverlodge mill in

northern Saskatchewan during this period. This was not an unique case, similar

depositional practices were observed in many sites over the world in 1950s. Because of

environmental concerns about these sediments in the water and other issues, tailings

storage areas or ponds began to be constructed, which were bounded by impoundments or

dams. The practice of above ground tailings management facility (AGTMF) was started

during 1970s. This types of tailings management facility usually involve the construction

of engineered earthen dams at the ends of a valley created by two parallel ridges. The

decant water from tailings is treated with chemical solutions and sand filtering system

prior to discharge to the environment. Modern tailings management facility includes an

advancement of storage technology with the development of the pervious surround

concept. Many facilities are storing tailings in a mined out pit by engineered with the

pervious surround which allows for enhanced consolidation during operation, as well as

effective control of contaminant migration (Landine and Moldovan, 2010).

Figure 2.4 shows a schematic diagram of the in-pit pervious surround concept.

The Deilmann Tailings Management Facility (DTMF) is an example of modern tailings

management facility which represents a refinement of the in-pit pervious surround

concept. The DTMF is engineered from a mined out pit called Deilmann pit. This facility

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Figure 2.4: The pervious surround concept in tailings disposal facility. (Modified after Landine and Moldovan, 2010)

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started receiving tailings from Key Lake operation since 1996. The pond is 1300 meters

long, 600 meters wide and 170 meters deep. It receives tailings at a rate ranging between

1500 m3/day and 2400 m3/day. The facility was initially designed for sub-aerial tailings

deposition followed by a switch to sub-aqueous deposition in 1999. Azam et al. (2014)

provided a chronological summery of tailings deposition and management in the DTMF.

The sub-aqueous deposition in the facility provided a benefit of preventing ice formation

and resulted reduced water treatment (Landine and Moldovan, 2010). The lower portions

of the facility include an engineered side-drain and bottom-drain system to facilitate the

collection of consolidation water via the raise well and the peripheral dewatering system.

2.2.4 Tailings Segregation

The tailings characteristics have influence in their behaviour after they are discharged to

the storage facility. Generally, segregation occurs after deposition of tailings as coarse

size particles settle out leaving fines on the top. The degree of this segregation essentially

depends on the grain size distribution of the tailings and the solids content of the slurry

(Vick, 1990). Segregation was also reported as a function of initial condition of slurry,

that is increasing the solids content by densification, or increasing the fines content

through enrichment of fines tailings, would change a segregating mixture to a non-

segregating one (Azam and Scott, 2005; Matthews et al., 2002). Azam (2003) found that

the initial solids content lower than 15% results segregation in laterite slurries. The

tailings is transported by pipeline to tailings management facility where it segregates

upon disposal, separation of some or all fractions of the coarse solids (Caughill et al.,

1993). The segregation of tailings upon disposal hinders consolidation process and

subsequently affects the proper use of storage facility and reclamation of land etc. When

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dispersed fine size particles are present in a tailings stream, the very slow settling and

consolidation of fine‐graded mine tailings presents a serious issues with the storage

capacity and potential reclamation of settling ponds (Talmon et al., 2014).

During the deposition of tailings, segregation can occur depending on grain size

distribution of the materials. Van Kesteren et al. (2007) reported that the acceleration in

the vertical section of the deposition system is required to control to minimize

segregation of slurries containing cohesive fines and sand. They further reported that the

slurry deposition can be controlled by a multiple tremie or diffuser system by increasing

the friction in the vertical pipe section. Costello et al. (2008) showed segregation distance

was found to be dropped from 25 meters to 10 meters by using multiple tremie or diffuser

system for uranium mine tailings in McClean Lake, Canada.

2.2.5 Tailings Dewatering

In the modern practice of tailings management, tailings dewatering is the most important

issue in the mining industry in terms of impoundment capacity, land reclamation, water

recovery, and reuse. Dewatering behaviour of tailings largely depends on material grain

sizes. Coarse particles (sand, silt) dewaters quickly due to the inert nature whereas fine

particles takes considerable amount of time to release water due their chemically active

nature. There is also an extreme need to recycle and reuse the decant water in the mill

process from the tailings storage facilities in the arid and semi-arid regions due to the

scarcity of water. The poor dewatering characteristics of tailings will result a shortage of

storage capacity and subsequently reduce the life of milling operations, or increase the

land use by creating the need of a new facility. In the several mining industries, it takes a

long time for dewatering because of having substantial amount of fine particles in the

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tailings. Therefore, many advanced technologies have been developed and implemented

in uranium, gold, oil sand, and other mining industry for tailings dewatering (Taylor,

2007; Ritcey, 2005; Mikula et al., 2008; Mpofu et al., 2003). The widely used

technologies are as follows: thickened tailings disposal, centrifuged technology, polymer

added disposal, and thin-lift drying etc.

2.3 Rheology

An essential depositional requirement for delivering tailings to the disposal point is

having a sufficient yield stress (τy), that can carry the largest particles by ensuring a

homogeneous suspension where segregation does not occur. The relationship between

solids content and yield stress should be determined in the first instance to indicate the

minimum solids content necessary to obtain the required yield stress in tailings

depositional scheme (Boger et al., 2002). It was observed in the study for non-Newtonian

fluid mechanics that, the significant presence of fine particles contributes to the

rheological characteristics in a suspension system (Valentik and Whitmore, 1965; Ansley

and Smith, 1967).

Tailings disposal scheme should have some rheological properties that are stable,

easily transportable and yielding low volume at storage. So yield stress measurement has

become significant in evaluating the geotechnical suitability of tailings deposits. In the

observation of flow characteristics effect on segregation behaviour, the vane shear

method was generally used to calculate the yield stress of tailings. The four bladed vane

technique is generally used for yield stress measurement in the high stress range

(Mihireitu, 2009) whereas rheometer can be used in the low stress range (Boger, 2013).

The vane, attached to a torsion measuring head, is carefully inserted into the test material

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and rotated at a low speed where the torque as a function of time is measured. The

maximum torque (Tm) is related to the yield stress (τy). Denoting the diameter of the vane

by Dv and the aspect ratio of the vane cylinder by H/Dv, the maximum torque can be

written by the following equation:

(2.1)

Mihiretu (2009) examined the solids content level at which the rheological

properties of fines play a significant role. His experimental results indicated that the

composition of the fines play a major role in the phenomena of segregation and clay

particles are the main contributors for the rheological behaviours and the yield stress.

Since yield stress is strongly dependent on solids content, the vane shear test data were

usually used to observe the relationship of yield stress with different solid content. There

are different ways in which yield stress is correlated to the solid content of the slurry. For

the experimental work, the yield stress is conveniently plotted as a function of the solid

content (s) of the slurry, the above relation can be rewritten in terms of solid content,

specific gravity (Gs) and a fitting parameter (A) as follows (Mihiretu, 2009):

(2.2)

2.4 Segregation

Segregation is the affinity of solid fractions (or part of it) to settle by creating a

concentration gradient within the mass (Suthaker, 1995). Solids tend to segregate by

virtue of differences in the size, shape, density, and other properties of particles.

Segregation is a common problem with a wide significance and it has been a matter of

�� = �

2 �� �

��+

1

3� ��

�� = � �� (�� − 1)

� + ��(1 − �)�

23−�

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18

interest to physicists, geologist, engineers, and industrial communities. The studies of

segregation are associated with different problems as sedimentation, consolidation,

fluidization, erosion, and mass transport. The tailings stream is transported by pipeline to

the tailings pond, where upon disposal the coarse particles settle out leaving the fines on

top of the pond. Such deposition results in segregation of the tailings. The major

problems associated with a segregating type of tailings are as followings: high operating

and monitoring cost, large storage volume, liquefaction susceptibility, low strength,

toxicity and high environmental risks, slow consolidation rate, less quantity of water to

recycle, and difficulty in land reclamation (Mihiretu, 2009). Therefore, the handling of

mine waste requires an optimal tailings disposal scheme. Currently, the production of non

segregating tailings is being considered as a solution to either the existing tailings

management challenges or future planning.

One may define the term segregation as a tendency for certain sizes or

components with similar properties to preferentially collect in one or another physical

zone of collective (de Silva et al., 1999). The segregation phenomena occurs or not in a

tailings containment depends on particle shape and size distribution, initial solid content,

and flow characteristics of tailings. Figure 2.5 shows a typical segregation process during

self-weight settling. During self-weight settling where two distinct particle sizes of equal

density are involved, it will results in four zones. From top to bottom these zones are:

clear liquid, suspension of smaller particle size only, suspension of both particle sizes,

and the sediment (Mirza and Richardson 1979). In this process the particle attractive

forces are at a minimum, and the particles tend to be dispersed.

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Figure 2.5: Typical Segregation process in the (a) settling column (b) tailings disposal facility.

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Segregation characteristics depend largely on the amount of fine particles present

in tailings. The relatively coarse particles tend to settle, but the fines remain suspended in

the slurry when deposited. Coarser grain particles (size greater than 0.075 mm) settle

with minimum to no segregation, unlike finer grain particles (size smaller than 0.075

mm), which undergo substantial segregation during self-weight settling process

(Dimitrova, 2011). The segregation is highly affected by the solids content in the

deposition of tailings; lower solids content generally exhibits a higher segregation (Major

2003). At higher solids content segregation is increasingly suppressed and eventually

inhibited due to a combination of grain-fluid coupling and particle interlocking (Lockett

and Al-Habbooby, 1974; Davies and Kaye, 1971). At low solids content, particle

interactions are negligible and the effect of fluid counter flow enhances segregation of

particles. Mihiretu (2009) examined the segregation phenomena theoretically and

experimentally with emphasis on identifying the effect of grain size composition. He

found that the segregating nature of slurry can be predicted based on the observation of

rheological responses in addition to grain size distribution and initial conditions.

It is important to define the degree of segregation or segregation index in a

depositional scheme of tailings management. Several attempts was taken on this regard to

quantify the segregation of tailings. To explain segregation behaviour, a quantitative

index, called segregation index, was introduced by different researchers (Suthaker, 1995;

Tang, 1997, Chalaturnyk and Scott, 2001; Azam, 2003). Denoting the average solids

content and height of slurry at time t by Savg and H, the initial solids content by So and the

initial height of slurry by Ho, this segregation index (Is) is calculated after self-weight

settling test and can be defined by the following equation:

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(2.3)

Mihiretu (2009) proposed an another method to define Segregation Index (SI),

which can be written by correlating with the solid content Si of sample section height of

Hi, as the following equation:

(2.4)

A simplified form of the above equations with similar basis (that is, solids content

deviation and layer-wise heights) was used later in this study to define segregation.

2.5 Dewatering

Dewatering is the water recovery from tailings which can also be said as the solid-liquid

separation. To understand tailings dewatering, it is fundamental to have a clear idea about

the self-weight settling behaviour, consolidation behaviour, and the factors affecting

dewatering.

2.5.1 Self-Weight Settling

Self-weight settling of tailings is a complex phenomenon which involves three different

phases: initial flocculation, sedimentation, and consolidation (Imai, 1981). These phases

stages are either inter-related or can be happened simultaneously. A typical self-weight

settling process of tailings in a settling column can be described by using Figure 2.5.

Initially, flocculation is occurred which ceases quickly as the slurry settles with a rapid

decrease in the interface height. This occurrence provides a clear water-solid interface

line. As slurry starts to settle, void ratio decreases gradually and solids content of slurry

�� = � �1

2 �

��

����− 1� ��

���

�+1

− ��

���

�−1

�� ∗ 100%

�=1

�� = �∑ ����� − ���� �

2

∑ ��

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increases at the bottom. The process continues until a soil like structure, sediment is

formed. Once, the particles start transmitting effective stress due to inter granular contact,

consolidation takes place and the behaviour is governed by consolidation theory

(Terzaghi et al., 1996). Jeeravipoolvarn (2010) reported that sedimentation and

consolidation can be identified by absence or presence of effective stress. Self-weight

settling ends after certain period of time until no further change is observed in interface

height. After self-weight settling, a clear water layer exists at top and sediment with a

measurable effective stress exists at the bottom.

2.5.2 Large Strain Consolidation

It has been recognized that the major assumptions in classical small strain theory are

highly restrictive for analysis of slurry type materials during consolidation. Terzaghi

(1925) develop the first approach to define the 1D consolidation. This theory is the most

widely used for consolidation analysis despite of having the well-known limitations. The

major assumptions of this approach are: strains are relatively small and the material

properties remain constant throughout the consolidation process. The major limitation of

this approach was explaining volume change behaviour of tailings, since tailings exhibit

significant changes in void ratios during changes in the applied stress. To distinguish the

application between small strain and large strain theory is essential for assessing tailings

consolidation behaviours. The large strain theory should be considered for tailings

deposition for a thickness higher than 30 meters in the containment facility (Schiffman et

al., 1988). Besson et al. (2010) reported that there is a disappearance of classical small

strain hypothesis to the large strain phenomena at a strain of about 10% or higher when

materials are in compression (such as consolidation).

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The theory of slurry consolidation was originally develop by McNabb (1960) and

later expanded by Gibson et al. (1967) in material coordinate system as follows:

���

��− 1�

�� �

����

��

��+ �

�� (���) ���

�� ��

��� +

��

��= 0 (2.5)

Here, �s and �w are unit weight of solids and fluid (water). The hydraulic conductivity,

void ratio and effective stress are denoted by k, e and σ' respectively. After this theory,

several formulations of the finite strain consolidation theory have been observed in the

literature of geotechnical engineering, but all the formulations are based on same

fundamental principles. Berry and Poskitt (1972) modified the theory which considered

the effect of secondary compression. Monte and Krizek (1976) incorporated the initial

“stress-free” state using finite element approach. Schiffman (1980) updated the theories

by using Lagrangian coordinates so that the variation throughout the soil depth can be

taken into the account. Huerta et al. (1988) developed a one-dimensional mathematical

model with large strain theory to solve seepage induced consolidation phenomena.

Table 2.1 shows a chronological summery for the development of consolidation

theory. The solution of large strain consolidation theory became more important for

practical use as the problem of mine tailings disposal required more exact analyses.

Poskitt (1969) solved the nonlinear large strain consolidation equation by Perturbation

method using a power series. Cargill (1984) developed graphical solution charts based on

linearization and normalization of Gibson et al. (1967) theory. Mikasa and Takada (1986)

developed three different approaches: a standard method with a primary consolidation

ratio correction, a method for finite strain in which coefficient of consolidation (Cv) is

constant, and a method for finite strain with a variable Cv. McVay et al. (1986) compared

the experimental and theoretical prediction of consolidation of soft soil and revealed

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Table 2.1: Chronological summery for the development of consolidation theory

Assumption/Significance Solution/Equation

Terzaghi (1925) The first approach to define consolidation. Strains are small and the material properties remain constant.

��

��= ��

���

���

McNabb (1960) This theory is a landmark in slurry consolidation theory because of the inherent allowance for large deformations.

��

�� = -

�� �

��(���) ���

���

Mikasa (1965) Considered the self weight of the deposit, variable permeability and compressibility.

Gibson et al. (1967) This first derived equation without the limitation of the infinitesimal strain in the normal consolidation theory.

���

��− 1�

�� �

����

��

��+ �

� (�)

�� (���) ���

�� ��

��� +

��

��= 0

Poskitt (1969) Nonlinear large strain consolidation equation was solved by perturbation method.

Monte and Krizek

(1976) Developed large strain consolidation theory that considers the initial, “stress-free” state.

�� �

����∗

��� �

��� �

���

��+

������

����∗ �� +

�� �

����∗�

Schiffman (1980) A new approach which considers the variation throughout the soil depth.

�� �

�� ���

��� ±

���

�(�����)

�� (����)� =

��

����

���

��

Cargill (1984) Prediction of consolidation of soft soil. Graphical solution charts based on Gibson et al. (1967)

McVay et al. (1986) Compared the experimental and theoretical prediction of consolidation of soft soil.

Semi-empirical and analytical solution

Huerta et al. (1988) 1D model with large strain theory to solve seepage induced consolidation phenomena.

Kiousis et al. (1988) A computational model based on advanced elasto-plastic large strain deformation.

Analytical solution approach using the finite element method.

Yao et al. (2002) Numerical solution for consolidation of soft soils by two time-dependent non-linear partial differential equations.

(1 − ��)�

���

����

��

��−

���

�(����)

��(���)

���

��

��

��� =

����

��

��

Morris (2002) The settlement estimation for unconsolidated soil based on Gibson et al. (1967) and Cargill (1984).

Analytical solutions and solution charts

Fox and Qiu (2004) Developed a piecewise-linear model for compressibility of the pore fluid in addition to the consolidation.

Numerical solution

Jeeravipoolvarn et al. (2008)

Numerical solution using three approaches: pre-consolidation, creep compression and layering consolidation.

���

��(�)

��(���)�

��

��+

��(�)

��(���)

���

��� + �. �. �. exp[−�. ���]. ��(���) ��

��= 0

��

�� = �2

��0 ���

��

��0�

�� �(1 + ��)

��

��� =

��

��

��

��=

���

�� (1 + �)�

��

��

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25

nonlinear approach is more realistic than linear attempts. Somogyi (1980) proposed the

power law function for volume compressibility (e-σ') and hydraulic conductivity (k-e)

relationships with four fitting parameters (A, B, C, D) by the following equations:

e = Aσ' B (2.6)

k = Ce D (2.7)

Later Liu and Znidarcic (1991) proposed an extended power law for one

dimensional compression behaviour. This void ratio and effective stress relationship

encountered the deficiency of defining void ratio at low effective stress or any effective

stresses. Fox and Berles (1997) developed a piecewise-linear model which is numerical

attempt based on constitutive relationship of the soil. This model offered a relatively

simple technique to apply and modify with the different initial and boundary conditions.

The major concerns with the tailings consolidation test are the apparatus must be

capable of accommodating large strains (Gan et al., 2011) and have the ability to apply

low loads at early stages to represent operating condition of tailings disposal facilities

(Qiu and Sego, 2001). Upon completion of the consolidation test and hydraulic

conductivity measurement, the compressibility and hydraulic conductivity relationships

are generally determined using the test results. These correlations are the essential

constitutive relationships for predicting the long-term behaviour by numerical modeling.

The consolidation theory has been implemented to a number of numerical

computer programs that are used to solve various consolidation behaviours, such as:

CONDES (Yao and Znidarcic, 1997) and FSCONSOL (GWP Software, 1999). These

programs typically used to calculate the tailings settlements and the capacity of tailing

storage facilities (Geier et al., 2011; Gjerapic et al., 2008).

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26

CHAPTER 3

RESEARCH METHODOLOGY

3.1 General

This chapter presents the research methodology of this study. A comprehensive research

investigation program was developed to understand the depositional and dewatering

behaviour of current (4%) and future uranium mill tailings (5% and 6%). First, the

materials are described including the safety protocol maintained in the laboratory

throughout the research program. Next, the complete laboratory investigation program

has been provided followed by the detailed descriptions of the various tests conducted in

this research. These descriptions include tests for rheological properties, self-weight

settling, grain size distribution, segregation, and large strain consolidation. Finally, a

detail description is provided for numerical modeling of tailings consolidation behaviour.

3.2 Uranium Mill Tailings

3.2.1 Material Properties

The Key Lake Operation of Cameco Corporation, Canada, provided the uranium mill

tailings samples, containing Falcon concentrator rejects at 1:1 ratio. Khaled (2012)

reported the index properties of these three types of tailings (4%, 5% and 6% mill

tailings). The specific gravity (Gs) was measured according to ASTM 854-10 and the

grain size distribution (GSD) was determined according to ASTM D422-63 (2007) using

wet sieving followed by hydrometer analyses on material finer than 0.075 mm. The grain

size distribution curves (Appendix D) were plotted by fitting the GSD test data with the

unimodal (4%) and bimodal (5% and 6%) fit (Fredlund et al., 2000). The unimodal fit

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was found to best describe (r2 = 0.994) the grain size distribution of the current (4%) mill

tailings whereas the bimodal fits were found to best describe (r2 = 0.994) the grain size

distribution of the future (5% and 6%) mill tailings. The GSD curves were used to

characterize the index properties of materials, and further used to interpret the

depositional and dewatering behaviours. Hydrometer data were analyzed to determine the

amount of fines present in the materials, defined as fines content (f) in this study.

3.2.2 Safety protocol

The mill tailings samples for this investigation program were received in a 20 L plastic

pail and was stored in a radioactive shielded sealed box. Using a specialized heat-paneled

vehicle that precluded the effect of freezing, the sample was shipped from the mill to the

Radioactive Tailings Research Laboratory at the University of Regina where these were

stored at 22oC. All of the laboratory tests were performed in this research facility which

licensed by Canadian Nuclear Safety Commission (CNSC). The safety protocol was

maintained by performing weekly wipe test using a scintillation counter, regular radiation

detection survey using a Geiger counter and maintaining radiation inventories of

radioactive substances. These safety practices were maintained in accordance with the

radiation safety policy of the University and CNSC regulations and the safety protocol

was regularly monitored by the Radiation Safety Officer (RSO). During the investigation

program, it was ensured that all legislative requirements are met for the safe use, storage,

transfer, and disposal of radiation and radioactive materials by using the ALARA

principle (as low as reasonably achievable). After the completion of laboratory

investigation program, the used samples were shipped back to the mill for disposal into

the tailings storage facility.

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3.3 Laboratory Investigation

3.3.1 Rheological Test

The yield stress was measured at various solids content in accordance with ASTM

D4648-10 using the vane shear apparatus comprising a 12.7 mm blade height and 12.7

mm diameter (1:1 vane blade). The slurry was placed in the cylindrical mould. The vane,

attached to the upper shaft of apparatus, was lowered by rotating the drive wheel and

pushed into the slurry sample up to a depth equal to the height of the vane. The vane

blade was rotated at a rate of 2 rpm. The resistance offered by the soil to the rotating

blade was measured and used to calculate the yield stress (τy). The applied torque

(product of the maximum angular rotation of the torsion springs and the calibration factor

of the spring) was divided by the vane dimension constant to determine the yield stress.

The gravimetric water content (w) was measured after each of the above tests according

to ASTM D2216-10 using representative samples from the cylindrical mould. Slurry

samples were initially oven dried overnight at 105ºC to evaporate the bulk of the tailings

water. Thereafter, several hours of additional oven drying (at a lower temperature of

60ºC) was carried out until the weight stabilized, to obtain completely dry samples

(Cameco, 2010b). The low temperature was used to prevent the removal of structural

water from gypsum (present in the tailings), thereby ensuring an accurate determination

of gravimetric water content.

3.3.2 Settling Test

Settling tests were conducted using 85 mm diameter graduated cylinders. The initial

sample height was also set at 85 mm in order to make the height to diameter ratio of 1.0

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to minimize wall effects (Azam et al., 2005). The top of the graduated cylinder was

covered with a plastic wrap to prevent evaporation. Prior to each test, the initial solids

content was adjusted by adding the decant water. The estimated solid content was

confirmed by taking a representative sample from the graduated cylinder and measuring

the water content. A clear solid-liquid interface movement (brown mud line observed

through a white background screen) was monitored at regular intervals of time until no

further change was observed. These data were confirmed by taking photographs using a

digital camera with macro lenses of up to six times magnification. After test completion,

the recorded data were plotted as interface height versus time (Appendix D). The slope of

the initial straight-line portion of the settling curve was used to determine the initial

hydraulic conductivity (ki), based on a method described by Pane and Schiffman, (1997).

Using the settling velocity (Vs) of the solid-liquid interface, the initial void ratio (ei) and

the unit weights of soil solids (γs), and water (γw), ki was determined as follows (Pane and

Schiffman, 1997):

ki = [{γwVs (1 + ei)} / (γs – γw)] (3.1)

The settling potential (SP) was calculated using ei and the difference between the

initial and the final void ratio (∆e) as follows (Azam, 2012):

SP = (100 ∆e) / (1 + ei) (3.2)

Using the final void ratio (ef), unit weight of water (γw), height of the slurry

sediment (h), and specific gravity (Gs), the effective stress (σ') at the end of the self-

weight settling test was calculated according to the following equation (Holtz et al.,

2010):

σ' = {(Gs – 1) / (1 + ef)}γw h (3.3)

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The settling tests were conducted at two initial solids contents (si = 15% and

20%) in this study. The settling tests data (as reported by Khaled, 2012) of these

materials for higher initial solids content (≥ 25%) were also used to determine the initial

hydraulic conductivity and settling potential of tailings.

3.3.3 Segregation Test

Upon the completion of the self-weight settling test, water above the sediment was

removed and the sediment was divided into six equal layers for water content

measurement. The water content data were converted to solids content (s) using the

following equation:

s = 1 / (1 + w) (3.4)

The normalized solids content deviation (Sd) was calculated using the solids

content of a given layer (Si) and the average solids content (Savg) of the sediment along

with a normalized height (hi / ht), where hi denoted the individual layer height and ht was

the total sediment height. Using a similar rationale as described earlier (in relation to

Eqns. 2.3 and 2.4), the following equation was used to quantify segregation:

Sd (%) = (Si – Savg) hi / ht (3.5)

To obtain an absolute value for each initial condition (si), segregation (S) was

defined in this study as the square root of the average of the squares of normalized solids

content deviation in each layer. This can be expressed by the following equation:

S (%) = [1/n {(Sd1)2 + (Sd2)

2 + (Sd3)2+ (Sd4)

2 + (Sd5)2+ (Sd6)

2}] 0.5 (3.6)

To account for the limited amount of materials in each layer the grain size

distribution tests were done by combining two consecutive layers using the previously

mentioned procedure. The fines contents (f) obtained from the test results were used to

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investigate segregation behaviour. The GSD tests were conducted for three different

layers at the each of two initial solids contents (si = 15% and 20%) in this study upon

completion of the settling tests. The GSD test data (as reported by Khaled, 2012) for

higher initial solids content (≥ 25%) were also analyzed to calculate the amount fines

content (f) presents in the 4%, 5% and 6% mill tailings.

3.3.4 Large Strain Consolidation Test

The large strain consolidation test is generally used for materials showing at least 10%

volumetric deformation (Besson et al., 2010) and the test results are applicable to the

containment facilities of at least 30 meters of height (Schiffman et al., 1988). The test

apparatus must be capable of accommodating large strains (Gan et al., 2011) and should

allow the application of low loads which pertains to the early stages of tailings disposal

(Qiu and Sego, 2001). Therefore, there was a need to design and fabricate a consolidation

test apparatus to investigate the large strain consolidation behaviour of uranium tailings,

3.3.4.1 Fabrication of Apparatus

Figure 3.1 shows a schematic of the large strain consolidation test system that was

designed, fabricated, and used in the Radioactive Tailings Research Laboratory at the

University of Regina. The primary components of this apparatus were as follows:

consolidometer cell, top plate, hydraulic conductivity measurement system, and data

acquisition. All the materials used in components of the apparatus were selected based on

required strength, chemical/corrosion resistance, and durability criteria that were

identified during the conceptual design phase.

(a) Consolidometer Cell: The consolidometer cell (100 mm diameter and 200 mm high),

was fabricated from acrylic sheet (Plexiglas®) to allow visual inspection of solid-liquid

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Figure 3.1: Schematic of the large strain consolidation test system

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interface change and also to avoid corrosion problems during long-term testing (30 to 40

days). The cost effectiveness and ease of machining the Plexiglas® compared to stainless

steel was also an important reason to choose this material. The cell (200 mm high) was

made from a 1000 mm long Plexiglas® tube and was graduated using a measuring scale

with 1 mm marks. The cell was designed for a slurry sample with an initial size of 100

mm diameter and 100 mm high such that it accommodated the expected large vertical

strains. The additional height in the cell served as a guide cylinder for the loading piston

to travel through as a result of vertical deformation during testing. The cell was fixed

with a base plate (length 152.4 mm, width 152.4 mm, and thickness of 36 mm), that was

also made from the Plexiglas®. The base plate was indented with radial and

circumferential grooves (5 mm diameter) that reported to an outlet that allowed drainage

through the bottom. A porous plate (96 mm diameter and 7.35 mm thickness) along with

a geotextile (2.80 mm thickness) was placed at the cell bottom to preclude fines

migration. The valve at the base plate was closed off for during load application and

opened during hydraulic conductivity measurement. The porous plate was waxed in the

peripheral area to preclude the fines escape through the sides.

(b) Top Plate: The top plate consists of a loading piston with piston shaft, a bubble level

vial, a linear strain gauge, and a porous plate along with a geotextile. Different

alternatives were evaluated for the vertical loading arrangement during the design phase.

Because of the large expected deformations, a lever systems loading could lead to

eccentric or uneven loading. Therefore, a vertical loading arrangement was chosen that

included a loading piston with piston shaft and a bubble level vial. The exclusion of

eccentricity and uneven loading were confirmed by monitoring the level using bubble

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vial attached to the loading shaft. Therefore, this arrangement ensured that regardless of

the strain level, the load will remain constant and vertical throughout the test. A linear

strain gauge with measuring range of 0.4 inch (10.16 mm) and 0.0001 inch (0.0025 mm)

graduation was used to measure the vertical displacement of the consolidating sample.

Once again, a porous plate along with a geotextile were placed on the top of the sample to

preclude fines migration during upward drainage. The combined weight of this

arrangement (loading piston, piston shaft, porous plate, and geotextile) ensured the

application of the low initial stress (1 kPa) on the sample (sample calculation of

consolidation loading is provided in the Appendix D9). The loading piston was also

equipped with a plastic container (50 mm diameter) at the bottom to provide a provision

of adjusting small loads. A number of small lead pellets (3.6 mm diameter and weight of

0.25 gm) were placed in the plastic container to achieve desired loading condition at the

early stages of loading.

(c) Hydraulic Conductivity Measurement System: A falling head test arrangement was

used for the measurement of hydraulic conductivity. The arrangement comprised of a 25

mL graduated burette with 0.2 mL graduations, a connectivity tube, the top and bottom

cell outlets, and an outflow beaker. The burette, fixed to a retort stand with a clamp, was

connected to the bottom outlet of the cell through a connectivity tube. To expel any

trapped air bubbles from the tube, a suction was applied on the connectivity tube to get

the water flowing before connecting to the outlet. The bottom outlet was opened to allow

upward drainage through porous stones and that established a falling head condition in

the graduated burette. The top outlet was opened during hydraulic conductivity

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measurements to maintain a constant water level in the sample. The overflow of water

was collected in the outflow beaker.

(d) Data Acquisition: A linear strain gauge measured the vertical displacement of the top

plate due to load application and it was connected to the data acquisition system in the

computer. The data acquisition system enabled the data to be acquired and viewed within

a spreadsheet application during the test. The settlement data were also cross-referenced

by visual inspection of the soil-liquid interface changes during the test and also by taking

photographs using a digital camera at regular time interval (each 1 min up to 10 min and

every 10 min thereafter). A digital single-lens reflex (SLR) camera, Nikon D300S, was

used for this purpose. The exposure time, length of time the camera's shutter was open

when taking a photograph, was 1/60 sec, with a focal length of 34 mm. The output

images were in 2136 pixels in width and 3216 pixels in height with 300 dpi resolution.

(e) Calibration: The individual components of the consolidation test apparatus were

calibrated. Figure 3.2 gives the calibration of graduated burette, linear strain gauge, and

digital camera. The volumetric burette (25 mL graduated burette) was calibrated by

allowing flow of water from it to a 200 mL beaker and weighing the water in the beaker.

The actual volume of water was measured using the volume to weight conversion factor

for water (1 mL = 0.9982 gm at 20oC ± 2oC). Likewise, the strain gauge was calibrated

using the vane shear apparatus (described earlier in rheological test). The apparatus has

an upper shaft that can be lowered by 12.7 mm (vane height) by applying six revolution

though a drive wheel. The gauge was attached to the driver wheel and different

revolutions were applied to calibrate the gauge. Finally, the digital camera was calibrated

with the visual observations of solid-liquid interface.

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Figure 3.2: Calibration of individual components of the consolidation test

90 92 94 96 98 100Visual Reading of Interface Height (mm)

90

92

94

96

98

100

Cam

era

Rea

din

g (m

m)

0 1 2 3 4Angular Displacement (revolutions)

0

2

4

6

8

10

Dia

l G

auge

Rea

ding

(m

m)

0 5 10 15 20 25Measured Volume (mL)

0

5

10

15

20

25

Bur

ette

Rea

din

g (m

L)

a) BuretteY = 1.038 X + 0.1797R2 = 0.999

b) Linear Strain GaugeY = 1.999 X + 1.569R2 = 0.999

c) CameraY = 0.956 X + 0.429R2 = 0.992

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3.3.4.1 Consolidation Test

The uranium mill tailing samples at an initial solids content of 35% (±2%) was poured in

the 100 mm diameter graduated Plexiglas cylinder up to a height of 100 mm. The 35%

(±2%) initial solids content is associated with a non-segregating slurry and the height to

diameter ratio was 1.0 at the starting of test that minimizes the wall effects (Khaled and

Azam, 2014). The degree of saturation (DS = 100%) for investigated tailings were

confirmed (calculation provided in the Appendix D8) by using its relationship with the

specific gravity (Gs), void ratio (e), and water content as follows (Holtz et al., 2010):

DS× e = w×Gs (3.7)

The slurry was initially allowed to settle under self weight. Thereafter, the

sediment was incrementally loaded in the effective stress range of 1 kPa to 8 kPa, thereby

capturing the behaviour of freshly deposited tailings. As described earlier, a linear strain

gauge was used to monitor the vertical deformations and the data were collected using a

data acquisition system. The change of solid-liquid interface was also recorded at equal

time intervals by using a digital camera with macro lenses for a image magnification of

up to six times (Azam, 2011). The captured image files were processed and cross-

referenced with the with the strain data. The entire test data were plotted with respect to

time in the form of interface height, void ratio and solids content.

The hydraulic conductivity was determined using the falling head method after

each load increment by allowing upward drainage. The porous plates and geotextiles

above and below the sample ensured an evenly distributed applied load and precluded

fines migration during hydraulic conductivity measurement (Suthaker and Scott, 1996).

The hydraulic gradient was kept lower than the critical gradient (0.3 to 0.4) to prevent

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sample boiling and to prevent any volume change during hydraulic conductivity

measurement. A constant water level was maintained in the cell by continuously

collecting the decant water in an outflow beaker. Denoting the burette cross-sectional

area by a (m2), sample length by L (m), sample cross-sectional area by A (m2), the initial

hydraulic head by h1 (m), the final head after time t (s) by h2 (m), the hydraulic

conductivity (k, m/s) was measured according to the following equation (Holtz et al.,

2010):

k = (aL/At) ln (h1/h2) (3.8)

3.4 Numerical Modeling

The large strain consolidation test results were converted to constitutive relationships

describing the consolidation process. The extended power law function was selected

because it captures slurry behaviour under initial conditions, that is, at low effective

stresses. Denoting the effective stress by σ' (kPa), void ratio by e, the fit parameters by A

(kPa-1), B (dimensionless) and Z (kPa), volume compressibility was expressed using the

following equation (Liu and Znidarcic, 1991):

e = A(σ' + Z)B (3.9)

Denoting the two empirical parameters by C (m/s) and D (dimensionless), the

power law function (Somogyi, 1980) was used for hydraulic conductivity relationship as

follows:

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Figure 3.3: Numerical modeling scheme

Volume Compressibility

Hydraulic Conductivity

Index Properties

Material Properties

Initial Condition

Stage Filling Data Processing

Boundery Conditions

Modeling Scheme

Modeling Program

Settlement-TimeCurve

Effective Stress Profile

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k = CeD (3.10)

Figure 3.2 describes the consolidation modeling process. The one-dimensional

finite difference modeling program, CONDES, was used utilizing the large strain

consolidation theory (Gibson et al., 1967). The program required five input parameters

related to tailings properties as mentioned in equation (3.8) and (3.9), and the initial

conditions of the materials. Denoting the specific gravity of tailings by Gs, Lagrangian

coordinate system by a (positive upward), unit weight of pore fluid by γw (kN/m3), the

program solves the governing equation, a non-linear second order partial differential

equation that formulated for one dimensional compression as follows:

(1 − ��)�

���

����

��

��−

���

�(����)

��(���)

���

��

��

��� =

����

��

�� (3.11)

A detail formulation of the governing equation were given by Yao et al. (2002).

From the field application of consolidation processes, the Dirichlet boundary condition

(stress type) can be imposed for the governing equation of one-dimensional compression.

The Dirichilet type boundary condition is also referred to as the stress type or first

boundary condition (Cheng and Cheng, 2005) because it is a stress-related boundary

condition. The stresses on the boundary will be converted into void ratios (e) using the

volume compressibility relationship, equation (3.10). The program uses a mixed form of

central and forward difference methods with an implicit time integration scheme for the

numerical solution of the governing equation (Yao and Znidarcic, 1997). The implicit

scheme solves the governing equation involving both the current state of the system and

the subsequent state of the system. This scheme is numerically very stable and takes

much less computational time for multiple time steps. The program employs an uniform

mesh for the spatial discretization and automatically generates a non-uniform mesh for

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certain cases when a finer mesh is required. The CONDES is capable of simulating

various boundary conditions (pervious at the bottom) and staged filling sequences

(Gjerapic et al., 2009), which are the major reasons for choosing this program for

numerical analyses of consolidation behaviour in the DTMF.

The historical multi-stage filling data from 1996 to 2008 were provided to the

program in terms of depositional height of tailings in the DTMF. A series of tailings

investigation programs were conducted in the DTMF by Cameco in 1999, 2004/05, and

2008/09. Based on these investigation program, the incremental tailings heights were

determined from volume-area measurements using discharge rates (m3/day), operating

durations (days) and the variable width (m) at different height (m) of the facility. These

heights were corrected to account for the volume of sloughed sand in 2001 and 2005. The

program outputs were obtained in the form a continuous settlement-time curve as well as

the effective stress profile at each selected time.

The assumptions of the modeling program were as follows (Yao and Znidarcic,

1997): (i) the soil is fully saturated throughout the consolidation process; (ii) the soil is

homogeneous; (iii) water flow is vertical that resulted from vertical deformation during

one-dimensional compression; (iv) creep is negligible; (v) water and solid are

incompressible and their properties are constant; and (vi) Darcy’s law and with the

conservation of mass are applicable.

The limitations of modeling program were as follows: The program was unable to

incorporate the spatial variability of tailings in the storage facility, that is, different soil

properties in different layer. Likewise, the program was unable to incorporate a pre-

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existing soil layer of prior to filling and, as such, a zero initial height was provided at the

beginning of stage filling process. Furthermore, the program considered a self-adjusting

boundary for bottom drainage. However, it was incapable to accommodate a sidewall

drainage system like the drainage system present in the DTMF. Finally, the convergence

problem could occur in the program if the number of iterations is greater than 600 (that

is, the analysis converges either at a very slow rate or does not converge at all). However,

it did not occur in this study. This numerical problem was overcome by providing

appropriate material characteristics and boundary conditions.

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CHAPTER 4

RESULTS AND DISCUSSION

4.1 General

This chapter outlines the laboratory test data, analysis of laboratory tests results, and

numerical modeling results. First, the tests data for yield stress, initial hydraulic

conductivity, settling potential, and segregation are presented. Next, laboratory test data

for dewatering behaviour are presented in terms of compressibility and hydraulic

conductivity during the tests. The volume compressibility and hydraulic conductivity

relationships are presented using the test results. Finally, the analysis of historical

consolidation behaviour in the DTMF is presented and matched with the results of

numerical modeling.

4.2 Depositional Behaviour

4.2.1 Rheological Properties

Figure 4.1 plots the yield stress versus solid content for 4%, 5% mill tailings sample. All

samples followed a similar trend, that is, a negligible strength up to s = 60% followed by

a rapid increase thereafter. This is attributed to similar particle shape originated identical

tailings production processes. Based on grain size distribution analysis, all sample were

characterized as sandy silts and classified as SM according to the Unified Soil

Classification System (USCS). The 4% mill tailings were found as well graded with 29%

material finer than 0.075 mm whereas the 5% and 6% mill tailings were observed as gap-

graded with 50% fines. The effect of different grain size distributions was insignificant

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Figure 4.1: Yield stress versus solids content for the investigated mill tailings

20 30 40 50 60 70 80Solids Content (%)

0

2

4

6

8

10

Yie

ld s

tres

s (k

Pa)

4% Mill Tailings

5% Mill Tailings

6% Mill Tailings

Oil Sand Tailings(Mihiretu, 2009)

Nickel Tailings(Boger, 2013)

Clay Tailings(Boger, 2013)

This Study

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and the inflexion point occurred at τy = 0.4 kPa. This is similar to other types of tailings

(from clay, nickel, and oil sand processing) where the inflexion point occurs at a yield

stress between 0.2-0.4 kPa (Boger, 2013; Mihiretu, 2009). The variation in inflexion

point for solids content ranging from 20% to 55%, depends on grain size distribution,

clay type and water chemistry (Sobkowicz and Morgenstern, 2009). The relatively higher

solids content at the inflexion point for Uranium tailings is attributed to the nature of the

investigated material. The rheological properties of mine tailings varies within and

among industries, dependent on particle size distribution and colloid-liquid interaction

(Boger, 2013; Mihiretu, 2009). On the other hand, increasing the fraction of silt and sand

size particles shifts the curve towards the right, that is, the yield stress occurs at higher

solids content due to the electrochemically inactive nature of the soil particles. In general,

clayey materials developed yield stress at lower solids content and vice versa. This is

because the presence of higher amounts of clay size along with their electrochemically

active nature increases solid-liquid interactions in slurries at low solids content.

4.2.2 Initial Hydraulic Conductivity

Figure 4.2 plots ki (rate of dewatering) with respect to the following: initial void ratio,

initial solids content (si), final void ratio, and final solids content (sf). The initial test

conditions were used to highlight their effect on slurry dewatering, whereas the final test

conditions were used to identify the range of dewatering achieved during the self weight

settling tests. Separate correlations (with r2 > 0.8) were found to describe the behaviour of

uranium tailings: one for 4% mill tailings and one for 5% and 6% mill tailings together.

The ki decreased by two orders of magnitude (10-2 m/s to 10-4 m/s) with a decrease in ei

from 16 to 4 (15% < si < 40%) and a decrease in ef from 8 to 4 (30% < si < 45%) such

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46

Figure 4.2 : Initial hydraulic conductivity with respect to the following: (a) initial void ratio (b) initial solids content (c) final void ratio (d) final solids content

0 4 8 12 16Initial Void Ratio

10-5

10-4

10-3

10-2

10-1

Init

ial

Hyd

rual

ic C

ond

ucti

vity

(m

/s)

ln ki = 0.44 ei - 9.9

r2 = 0.88

ln ki = 0.58 ei - 12.0

r2 = 0.90

0 10 20 30 40 50Initial Solids Content (%)

10-5

10-4

10-3

10-2

10-1

Init

ial

Hyd

rual

ic C

ondu

ctiv

ity

(m/s

)

0 4 8 12 16Final Void Ratio

10-5

10-4

10-3

10-2

10-1

Init

ial

Hyd

rual

ic C

ondu

ctiv

ity

(m/s

)

0 10 20 30 40 50Final Solids Content (%)

10-5

10-4

10-3

10-2

10-1

Init

ial

Hyd

rual

ic C

ond

ucti

vity

(m

/s)

(a) (b)

(d)(c)

ln ki = -0.26 si + 0.1

r2 = 0.89

ln ki = -0.21 si - 0.4

r2 = 0.97

ln ki = 1.82 ef - 14.6

r2 = 0.95

ln ki = 1.73 ef - 16.9

r2 = 0.87

ln ki = -0.41 sf + 6.80

r2 = 0.82

ln ki = -0.36 sf + 7.5

r2 = 0.96

4% Mill Tailings 5% Mill Tailings 6% Mill Tailings Best Fit

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47

Figure 4.3: Settling potential with respect to the following: (a) initial void ratio (b) initial solids content (c) final void ratio (d) final solids content

0 4 8 12 16Initial Void Ratio

0

20

40

60

Set

tlin

g P

ote

nti

al (

%)

SP = 3.64 ei + 3.4r2 = 0.95

SP = 3.75 ei - 8.14

r2 = 0.98

0 10 20 30 40 50Initial Solids Content (%)

0

20

40

60

Set

tlin

g P

ote

ntia

l (%

)

SP = -1.65 si + 79.7

r2 = 0.98

SP = 3.75 si - 8.14r2 = 0.98

(a) (b)

0 4 8 12 16Final Void Ratio

0

20

40

60

Set

tlin

g P

ote

ntia

l (%

)

SP = 14.30 ef - 32.3

r2 = 0.95

SP = 11.27 ef - 40.0r2 = 0.97

0 10 20 30 40 50Final Solids Content (%)

0

20

40

60

Set

tlin

g P

ote

ntia

l (%

) SP = -2.80 sf + 140.0

r2 = 0.94

SP = -2.70 sf + 114.4

r2 = 0.91

(c) (d)

4% Mill Tailings 5% Mill Tailings 6% Mill Tailings Best Fit

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48

that about one order of magnitude lower values were observed for 4% mill tailings when

compared with 5% and 6% tailings. Overall, the decrease in hydraulic conductivity

during hindered sedimentation (settling of a 3-D network of soil particles with no

effective stress (Pane and Schiffman, 1997)) is attributed to a decrease in total pore space,

an increase in dead end pores, and an increase in tortuousity (Suthaker and Scott, 1996).

4.2.3 Settling Potential

Figure 4.3 is a series of plots of SP (amount of dewatering) with respect to the above

mentioned parameters. Separate linear correlations (r2 > 0.95) were found to best describe

the behaviour of uranium tailings: one for 4% mill tailings and one for 5% and 6% mill

tailings together. For the above mentioned ranges of void ratios and solids contents given

in Figure 4.3, SP decreased ten times (50% to 5%) for 4% mill tailings and four times

(60% to 15%) for 5% and 6% mill tailings. The above reasons governing the rate of fluid

flowing through the tailings also affect the amount of fluid migrated through the tailings.

This means that the rate and amount of dewatering are directly proportional for the

investigated uranium tailings. This is similar to the behaviour of tailings from residual

laterite ores, as reported by Azam (2012).

4.2.4 Effective Stress

Figure 4.4 plots the final effective stress versus the above mentioned parameters. A single

fit was found to best describe σ' variation with respect to the initial conditions whereas

separate correlations (one for 4% and another for 5 and 6% combined) were found for

final conditions. As expected, the compressibility relationships (effective stress versus

void ratio) were found to be non-linear whereas the slurry concentration relationships

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49

Figure 4.4: Final effective stress with respect to the following: (a) initial void ratio (b) initial solids content (c) final void ratio (d) final solids content

0 10 20 30 40 50Initial Solids Content (%)

100

200

300

Fin

al E

ffec

tive

Str

ess

(Pa)

0 10 20 30 40 50Final Solids Content (%)

100

200

300

Fin

al E

ffec

tive

Str

ess

(Pa)

r2 = 0.99

'f = 12.18 sf - 244.6

'f = 12.82 sf - 325.7r2 = 0.97

'f = 7.42 si - 43.2

r2 = 0.98

0 4 8 12 16Final Void Ratio

0

100

200

300

Fin

al E

ffec

tiv

e S

tres

s (P

a)

ln 'f = -1.94 ln ef + 7.9r2 = 0.97

ln 'f = -1.74 ln ef + 8.0

r2 = 0.97

0 4 8 12 16Initial Void Ratio

0

100

200

300

Fin

al E

ffec

tiv

e S

tres

s (P

a)

ln 'f = -0.92 ln ei + 6.9

r2 = 0.94

(a) (b)

(c) (d)

4% Mill Tailings 5% Mill Tailings 6% Mill Tailings Best Fit

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50

(effective stress versus solids content) were found to be linear. The r2 values were close to

0.9 for all of the correlations. The final effective stress increased from 80 Pa to 260 Pa

with a decrease in ei from 16 to 4 (solids content increased from 15% to 40%) and a

decrease of ef from 8 to 4 (solids content increased from 30% to 45%). The presence of

measurable effective stress change over a wide range of void ratio confirms the large

strain consolidation behaviour of the slurry where the effective stress is transmitted

through inter-granular contact (Terzaghi et al., 1996).

4.2.5 Segregation Behaviour

Figure 4.5 plots solids content versus normalized solids content deviation from the

average. The average solids content after settling was found to be 35% (20% < s < 42%)

for 4% mill tailings, 40% (15% < s < 60%) for 5% mill tailings and 39% (18% < s <

54%) for 6% mill tailings with a corresponding normalized deviation of ±3%, ±8%, ±6%,

respectively. The above narrow ranges for 4% tailings mean low segregation and the

reverse is true for the other two mill tailings. This is because of the well graded grain size

distribution of the 4% mill tailings compared to the gap graded nature of 5% and 6% mill

tailings. Mihiretu (2009) reported significant segregation of sand grains from fines in

gap-graded oil sand tailings. From a practical standpoint (operational control and facility

planning), the ±2% solids content deviation is considered as acceptable based on

historical DTMF performance (Azam et al., 2014). This means that the 4% mill tailings

can be deposited at an si of as low as 25%, while the 5% and 6% mill tailings would

require an si higher than 30%. Furthermore, the low solids content along with the

negative values of normalized solids content deviation characterized the top layers of the

slurry and the opposite parameters characterized the bottom layers of the slurry. The

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51

Figure 4.5: Solids content versus normalized solids content deviation

4% Mill Tailingssi = 15.1%

si = 20.2%

si = 26.0%

si = 30.3%

si = 35.9%

si = 40.0%

10

20

30

40

50

60

70

Sol

ids

Con

ten

t (%

)

5% Mill Tailingssi = 15.2%

si = 20.4%

si = 25.0%

si = 30.1%

si = 36.1%

si = 41.8%

10

20

30

40

50

60

70

So

lids

Con

tent

(%

)

10/70

6% Mill Tailingssi = 15.2%

si = 20.0%

si = 25.5%

si = 30.0%

si = 35.0%

si = 40.1%

-10 -8 -6 -4 -2 0 2 4 6 8 10

Normalized Solids Content Deviation (%)

10

20

30

40

50

60

70

So

lid

s C

onte

nt (

%)

10/70

Best Fit

Best Fit

Best Fit

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52

leaner (low initial solids content) mixtures exhibited a wider range of solids content

deviation when compared with thicker (high initial solids content) mixtures. The

increased segregation in the leaner mixtures is attributed to the absence of a three

dimensional particle network during the settling process (Shimoska et al., 2013). This

was also observed during the laboratory experimentation in the form of preferential

particle settling. Regardless of the ore grade, segregation was found to decease as si

increased, that is, most data for high si values tended to zero normalized solids content

deviation.

Figure 4.6 shows fines content versus normalized solids content deviation. The

average fines content was found to be 42% (35% < f < 42%) for 4% mill tailings, 56%

(23% < f < 95%) for 5% mill tailings and 56% (26% < f < 95%) for 6% mill tailings with

a corresponding normalized deviation of ±3%, ±8%, ±6%, respectively. The high fines

content along with negative values of normalized solids content deviation are found in

the top layers of slurry (because of preferential settling of the coarse grains) while low

fines content and positive deviations are found in the bottom layers. Again, the narrow

ranges for 4% indicate low segregation over a wider range of si, while the 5% and 6%

mill tailings show increasing segregation as si decreases. The lower segregation range for

4% mill tailings is attributed to the well graded nature despite its low fines content (29%)

whereas the higher segregation of the other two slurries (5% and 6%) were observed due

to the gap graded nature despite their higher fines content (49%).

Figure 4.7 correlates segregation with the initial solids content. Separate linear

correlations were found for 4% mill tailings (r2 = 0.97) and for 5% and 6% mill tailings

together (r2 = 0.9). As expected, segregation was found to decrease with increasing initial

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53

Figure 4.6: Fines content versus normalized solids content deviation

-10 -8 -6 -4 -2 0 2 4 6 8 10

Normalized Solids Content Deviation (%)

20

40

60

80

100

Fin

es C

onte

nt

(%) 6% Mill Tailings

si = 15.2%

si = 20.0%

si = 25.5%

si = 30.0%

si = 35.0%

si = 40.1%

20

40

60

80

100

Fin

es C

ont

ent

(%) 4% Mill Tailings

si = 15.1%

si = 20.2%

si = 26.0%

si = 30.30%

si = 35.90%

si = 40.0%

20

40

60

80

100

Fin

es C

onte

nt (

%) 5% Mill Tailings

si = 15.2%

si = 20.4%

si = 25.0%

si = 30.1%

si = 36.1%

si = 41.8%

20/100

20/100

Best Fit

Best Fit

Best Fit

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54

Figure 4.7: Initial solids content versus segregation

0 1 2 3 4Segregation (%)

10

20

30

40

50

Init

ial

Sol

ids

Con

tent

(%

) 4% Mill Tailings

5% Mill Tailings

6% Mill Tailings

si = -7.53 S - 40.3

r 2 = 0.90

si = -21.42 S + 41.0

r2 = 0.97

Best fit

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55

solids content. The two curves merged at 40% initial solids content where segregation

was negligible. The steeper slope for 4% mill tailings (narrower segregation range)

means that segregation of this material is less susceptible to changes in initial solids

content, whereas the flatter slope for the 5% and 6% mill tailings (wider range of

segregation) indicates that segregation in these materials is more sensitive to the initial

solids content. From an operational perspective, this figure indicates that high grade mill

tailings have less room for error during slurry preparation, which is, achieving the desired

initial solids content.

4.3 Dewatering behaviour

4.3.1 Large Strain Consolidation

Figure 4.8 plots the large strain consolidation test results in the form of interface height,

void ratio and solids content versus elapsed time. In 4% mill tailings, the interface height

changed from 10 cm to 8.4 cm due to self-weight consolidation and the height was

further reduced to 5.8 cm due to applied loads (up to σ' of 8 kPa) during large strain

consolidation tests. The total strain was calculated using the ratio of height change to the

initial height and found to be 42% for 4% mill tailings. The interface height changed to

7.6 cm and 8.0 cm during self-weight consolidation whereas the final height was found to

be 6.2 cm and 6.9 cm for 5% and 6% mill tailings. The total strains were calculated as

38% and 31% respectively. A similar height reduction under comparable effective stress

was observed by Pedroni and Aubertin (2013) for fine silty sludge. Similar interface

change behaviour was observed during consolidation test of treated oil sand tailings

(Moore et al, 2013) and laterite slurries (Azam et al., 2005) but a higher stain were

observed in laterite slurry due to having a lower initial solids content.

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56

Figure 4.8: Settling curves: (i) interface height (ii) void ratio and (iii) solids content versus elapsed time during large strain consolidation test for (a) 4% (b) 5% and (c) 6% mill tailings.

5

6

7

8

9

10

11In

terf

ace

heig

ht (

cm)

2

3

4

5

6

Voi

d R

atio

0.1 1 10 100 1000 10000

Elapsed Time (min)

30

35

40

45

50

55

Sol

ids

Con

ten

t (%

)

0.1 1 10 100 1000 10000

Elapsed Time (min)

0.1 1 10 100 1000 10000

Elapsed Time (min)

5/6

2/55

104

/0.1

Self-Weight 1 kPa 2 kPa 4 kPa 8 kPa

(a) 4% Mill Tailings (b) 5% Mill Tailings (c) 6% Mill Tailings

(i) (i)(i)

(ii) (ii)(ii)

(iii) (iii)(iii)

104

/0.1104

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57

The void ratio versus time curves can be characterized by two conditions: self-

weight and large strain consolidation test curves. The slurry settled from a void ratio of

5.8 to 4.8 under self-weight and void ratio further reduced to 3.3 at σ' = 8 kPa for 4% mill

tailings. The corresponding void ratio change was observed from 4.5 to 3.4 and 4.6 to 3.6

during self-weight consolidation whereas it further reduced to a final void ratio of 2.8 and

3.1 for 5% and 6% mill tailings. Tailings behaviour is often influenced by self-weight

settling for low initial solids contents. But it is not the case for higher solids content,

which attain sufficient consistency for preventing relative movement between different

size particles Geier et al. (2011). The solids content increased from 31.9% to 36.4% due

to self-weight and to 45.5% final solids content for 4% mill tailings. The corresponding

solids contents were found to be 37.8% to 44.4% and 37.5% to 43% due to self-weight

and to 49.3% and 46.8% final solids content for 5% and 6% mill tailings after the tests.

Figure 4.9 gives the hydraulic conductivity data measured after each load

increment in the large strain consolidation test for (a) 4% mill tailings (b) 5% mill tailings

and (c) 6% mill tailings on a semi logarithmic scale. Under each load increment, the data

showed an initial scatter before attaining a steady state value. This is attributed to

equilibration of inertia with the hydraulic gradient required to move water through the

soil and redistribution of pore sizes during this process. The range of scatter decreased

with higher loads because of a reduced capacity of the tailings to undergo further pore

sizes changes. The k values for the all investigated tailings were found to be ranging from

10-7 to 10-8 m/s. The 4% mill tailings shows a higher range of k values when compared

with 5% and 6% mill tailings. The steady state k values were obtained after about 30 min

for all mill tailings and were used in subsequent analyses.

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58

Figure 4.9: Hydraulic conductivity versus time data in large strain settling test

0 20 40 60Elapsed Time (min)

(c) 6% Mill TailingsSelf Weight

1 kPa

2 kPa

4 kPa

8 kPa

0 20 40 60Elapsed Time (min)

(b) 5% Mill TailingsSelf Weight

1 kPa

2 kPa

4 kPa

8 kPa

0 20 40 60Elapsed Time (min)

10-8

10-7

10-6

Hyd

raul

ic C

ondu

ctiv

ity

(m/s

)

(a) 4% Mill TailingsSelf Weight

1 kPa

2 kPa

4 kPa

8 kPa

60/0 60/0

k = 6.1×10-7 m/s

k = 1.3×10-7 m/s

k = 1.5×10-7 m/s

k = 4.3×10-8 m/s

k = 4.7×10-7 m/s

k = 8.9×10-8 m/s

k = 1.5×10-7 m/s

k = 1.9×10-7 m/s

k = 2.7×10-7 m/s

k = 5.0×10-8 m/s

k = 5.7×10-8 m/s

k = 7.9×10-8 m/sk = 1.1×10-7 m/s

k = 1.9×10-7 m/s

k = 2.7×10-7 m/s

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59

4.3.2 Volume Compressibility and Hydraulic Conductivity Relationships

Figure 4.10 plots the volume compressibility and hydraulic conductivity relationships for

the investigated mill tailings. The compressibility curve was fitted to the extended power

law function. The lowest measurable effective stress was approximately 0.3 kPa for all

tailings at void ratio e = 4.8, 3.4 and 3.6 for 4%, 5% and 6% mill tailings respectively.

The void ratio at the effective stress of 1 kPa was found to be 3.8, 3.1 and 3.4

respectively. A similar range of value of void ratio (e = 2.6 to 4.6) was also reported by

Mittal and Landine (2013) for the various uranium tailings from Northern Saskatchewan.

With comparatively higher change in void ratio (from e = 4.8 to 3.3), the 4% mill tailings

was observed to have higher compressibility behaviour. A relative small change in void

ratio (Δe = 0.5 ~ 0.6) was observed for both 5% and 6% mill tailings. This is attributed to

the higher amount of silt size materials presence, gap graded nature of particle

distribution and the initial conditions for 5% and 6% mill tailings.

The curve of hydraulic conductivity relationship was fitted with the conventional

power law function. The hydraulic conductivity at the end of self-weight consolidation

was measured to be 6.1×10-7 m/s at e = 4.8 for 4% mill tailings. During load-induced

consolidation (e = 4.8 to e = 3.3), hydraulic conductivity varied from 2.6×10-7 m/s to

1.7×10-7 m/s. At the end of self-weight consolidation, The hydraulic conductivity was

measured to be 1.5×10-7 m/s and 4.6×10-7 m/s at e = 3.4 and 3.6 for 5% and 6% mill

tailings respectively. During load-induced consolidation (e = 3.4 to e = 2.8 and e = 3.6 to

3.1), hydraulic conductivity decreased from 7.9×10-8 m/s to 4.4×10-8 m/s and 2.7×10-8 to

8.9×10-8. The lower k values of 5% and 6% mill tailings are attributed to higher water

retention capability that, in turn, is derived from the presence of higher amount of silt size

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60

Figure 4.10: Volume compressibility and hydraulic conductivity relationship.

2.5 3 3.5 4 4.5 5

Void Ratio

10-8

10-7

10-6

Hyd

rauli

c C

ondu

ctiv

ity

(m/s

)

4% : k = 1.16 x 10-9 e4.0

5% : k = 5.92 x 10-11 e6.4

6% : k = 1.74 x 10-13 e-11.5

0.1

1

10

Eff

ecti

ve S

tres

s (k

Pa)

4% : e = 3.9 ( '+0.03)-0.10

5% : e = 3.2 ( '+0.01)-0.06

6% : e = 3.5 ( '+0.01) -0.05

10-6/0.1

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61

materials in the slurry. Mittal and Landine (2013) reported a similar range of value of k

(10-7 to 10-8 m/s) for the various uranium tailings from Northern Saskatchewan. The

observed compressibility and hydraulic conductivity relationships provided the essential

constitutive relationships for predicting and managing long-term performance of uranium

tailings in containment facility.

4.4 Consolidation Behaviour in the DTMF

4.4.1 Tailings Deposition

Figure 4.11 shows the schematics of the DTMF. All of the coordinates are based on the

Key Lake mine grid system, whereas the elevations are referenced to the geodetic datum.

The pit boundary (crest line) is based on the aerial photographic survey data of 2005

(Cameco 2005), whereas the actual tailings surface in 2005 and the average tailings

surface in 2008 were derived from bathymetric surface surveys (Cameco 2009). From

1996 to 1999, tailings were deposited in the East Cell while ore was still being mined

from the west part of the pit. A series of field investigation programs were conducted

during 1999, 2004/05 and 2008. Borehole locations for these programs are shown on

figures. The annual consolidated tailings elevations (1996 through 2008), given in

sections A-A' and B-B', are based on monthly topographical surveys (1996-1999) and

annual bathymetric surface surveys (1999-2008). The entire DTMF geometry is not given

in section A-A' because of negligible tailings amount in the West Cell. The average

consolidated tailings surface in the East Cell was 450 masl, as recorded in 2008. The

facility was initially operated in sub-aerial deposition mode and was then switched to

sub-aqueous deposition in December 1998 to prevent ice formation (Landine and

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62

Figure 4.11: Schematic of DTMF: (a) Plan view; (b) Section A-A' of consolidated tailings elevations; and (c) Section B-B' of consolidated tailings elevations

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63

Figure 4.12: Historical tailings elevation in the DTMF from 1996 through 2008

May-95 May-00 May-05 May-10

Time

350

375

400

425

450

475

Tai

ling

s E

lev

atio

n (m

asl) Field Data Depositional Stages

Sand Sloughing

Subaerial Discharge

Subaqueous Discharge

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64

Moldovan, 2010). Slope instability developed in October 2001 when the water level rose

above the lower-most level of the outwash sand in the West Cell. Sloughing continued in

a series of events up to May 2005, when further water level rise was halted. With a

maximum thickness of up to 40 m (from 410 masl to 450 masl), the sloughed sands are

shown as a wedge in section A-A' and as a 10 m layer in section B-B'.

Figure 4.12 gives the consolidated tailings elevation in the DTMF from 1996

through 2008. The average cumulative surface height shows four distinct stages: (i) rapid

increase of 13 m/year in the first three years due to a smaller base area; (ii) steady height

increase of 2.5 m/year over the next four years due to the gradual increase in surface area;

(iii) relatively large height increase of about 7 m/year in the next three years due to sand

sloughing displacing the tailings; and (iv) a steady height increase of 3 m/year over the

next three years due production increase. The average consolidated tailings elevation in

the containment facility increased from 376 masl to 451 masl during 1996 to 2008.

4.4.2 Numerical Modeling Results

Figure 4.10 provided the required input for numerical modeling of consolidation

behaviour that is, the volume compressibility and hydraulic conductivity parameters (A =

3.9 kPa-1, B = -0.10, C = 1.2×10-9 m/s, D = 4.0 and Z = 0.03 kPa) for current (4%) mill

tailings. The history matching of settlement-time curve in the DTMF from 1996 to 2008

for investigated mill tailings was presented in Figure 4.13. The consolidated heights

closely matched the model predictions.

Figure 4.14 presents observed and modelled effective stress profiles in the DTMF.

Generally, the model results matched quite well with the average values reported by

Azam et al. (2014) as well as with measured values (Cameco, 2005). The predictions of

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Figure 4.13: History matching of tailings elevation in the DTMF from 1996 through 2008

May-95 May-00 May-05 May-10

Time

350

375

400

425

450

475

Tai

lin

gs E

leva

tion

(m

asl) Field Data Model Prediction

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Figure 4.14: Effective stress profiles in the DTMF: (a) 1999 borehole investigations; (b) 2004/05 borehole investigations; and (c) 2008 borehole investigations.

350

375

400

425

450

475

Tai

ling

s E

leva

tion

(m

asl)

350

375

400

425

450

475

Tai

ling

s E

leva

tion

(m

asl)

0 100 200 300 400 500 600 700

Effective Stress (kPa)

350

375

400

425

450

475

Tai

ling

s E

leva

tion

(m

asl)

350/475

350/475

ModeledE8E2

E6E2 Piezocone E6 Piezocone

ModeledE12E3

E9

ModeledE8E2

E6

(a)

(b)

(c)

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1999 exhibited the best match when compared with the average effective stress (albeit the

latter were linear) because of the small size of the DTMF ensuing similar depositional

history in all three borehole locations (E3, E9, and E12). The 2004/05 and the 2008

predictions clearly exhibited the nonlinear behaviour of the deposited tailings. The

variations of the modeling results (pertaining to the entire DTMF) from the average

effective stresses are attributed to the dissimilar depositional histories in the various

areas. The effect of sand sloughing is visible in boreholes E2 in the form of two different

slopes whereas the higher tailings deposition towards the east area after sand sloughing is

evident at location E8. The intermediate borehole location E6 was closest to the overall

conditions in the DTMF up to about 400 masl. At the DTMF bottom, the model was

corrected for the volume of sand sloughed thereby predicting higher effective stresses.

The measured effective stress (piezocone values in 2004/05) correlated quite well with

the modeling results thereby validating the predictions. This is attributed to the silty sand

nature of the investigated tailings that showed a significant amount of dewatering takes

place at low effective stresses (42% at σ' = 8 kPa), as depicted in Figure 4.8. Overall, the

model results indicate that the effective stress increased from 0 kPa at the surface to the

following values at the DTMF bottom: 200 kPa in 1999, 530 kPa in 2005, and 680 kPa in

2008 along with a vertical hydraulic conductivity in the order of 10-8 m/s.

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CHAPTER 5

CONCLUSIONS AND RECOMMENDATIONS

5.1 Conclusions

Knowledge of depositional and dewatering behaviour of tailings is fundamental to

efficient tailings management. A detailed laboratory investigation and geotechnical

analysis were conducted to understand these behaviours of uranium mill tailings from

Key Lake, Saskatchewan, Canada. The main conclusions of this research are summarized

as follows:

All of the samples exhibited the same trend for yield strength development. A

negligible strength was found to have at 60% solids content followed by a rapid

increase thereafter. The inflexion point occurred at a yield stress of 0.4 kPa.

The 4% mill tailings exhibited a lower rate and total amount of settlement than 5%

and 6% mill tailings. The ki decreased by two orders of magnitude (10-2 m/s to 10-4

m/s) with a decrease in ei from 16 to 4 (15% < si < 40%) and a decrease in ef from 8 to

4 (30% < si < 45%) such that 4% mill tailings showed one order of magnitude lower

values than the 5% and 6% mill tailings. The corresponding SP decreased ten times

(50% to 5%) with increasing si for 4% mill tailings and four times (60% to 15%) for

5% and 6% mill tailings. The effective stress increased from 80 Pa to 260 Pa in the

self-weight settling tests.

The 4% tailings were less segregating when compared with 5% and 6% tailings. The

average solids content after settling was 35% (20% < s < 42%) for 4% mill tailings,

40% (15% < s < 60%) for 5% mill tailings and 39% (18% < s < 54%) for 6% mill

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tailings with a corresponding normalized solids content deviation of ±3%, ±8%, ±6%,

respectively. Considering that ±2% solids content deviation is acceptable, the 4% mill

tailings can be deposited at an si of as low as 25%, while the 5% and 6% mill tailings

would require an si higher than 30%. Furthermore, the high grade mill tailings have

less room for error during slurry preparation.

The large strain consolidation tests were conducted by using a customized and

fabricated consolidation test system. During the consolidation tests (σ' = 0.3 kPa to 8

kPa), the tailings settled from a void ratio of ei = 5.8 to ef = 3.3 for 4% mill tailings

and the initial void ratio reduced from 4.5 to 2.8 and 4.6 to 3.1 for 5% and 6% mill

tailings. With an si of 31.9%, 4% mill tailings achieved an sf of 45.5% after the

consolidation tests. The solids content increased from 37.8% to 49.3% and 37.5% to

46.8 for 5% and 6% mill tailings. The k values showed an initial scatter before

attaining a steady value under each load increment for all investigated mill tailings.

The test results provided the volume compressibility and hydraulic conductivity

relationships for current (4%) and future (5% and 6%) mill tailings. The lowest

measurable effective stress was approximately 0.3 kPa for all mill tailings. The 4%

mill tailings was observed to have higher change in void ratio (Δe = 1.5) compared to

small change in void ratio (Δe = 0.5~0.6) in both 5% and 6% mill tailings. The k

varied from 6.0×10-7 m/s to 1.0×10-7 m/s for 4% mill tailings, whereas for 5% and 6%

mill k varied from 4.7×10-7 to 4.4×10-8 m/s.

The large strain consolidation behaviour in the DTMF was investigated by analyzing

survey data from 1996 to 2008, laboratory testing of the current (4%) mill tailings,

and history matching of the deposited tailings using numerical modeling.

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The average consolidated tailings height in the DTMF has four distinct stages from

1996 to 2008: (i) rapid increase of 13 m/year in the first three years, (ii) steady height

increase of 2.5 m/year over the next four years, (iii) relatively large height increase of

about 7 m/year in the next three years, and (iv) a steady height increase of 3 m/year

over the next three years.

The numerical modeling results closely approximated the consolidated tailings

elevations and effective stresses in the DTMF over the period of 1996 to 2008. The

measured effective stresses values correlated quite well with the modeling results

thereby validating the predictions. Overall, the results indicate that the effective stress

increased from 0 kPa at the surface to the following values at the DTMF bottom: 200

kPa in 1999, 530 kPa in 2005, and 680 kPa in 2008.

5.2 Recommendations

The future recommendations are as follows:

Rheological properties of uranium tailings should be further investigated by

conducting laboratory tests for the determination of viscosity and yield stress at

different shear rates in order to assess the optimum depositional conditions.

Shear induced segregation behaviour should be examined for uranium tailings

depositional scheme with a single tremie to achieve a non-segregation condition.

The developed volume compressibility and hydraulic conductivity relationship for

uranium tailings should be calibrated at higher consolidation loads in large scale tests.

A consolidation model that accommodates the multi-layer slurries with different

compressibility and hydraulic conductivity during multi-stage pond filling will further

explain the dewatering behaviour of uranium mill tailings.

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APPENDIX A

Laboratory test data of 4% mill tailings sample

Table A1: Vane shear test data of 4% mill tailings sample

Test No

Max. Angular Rotation

(Deg)

Height, H (mm)

Width, D (mm)

Vane Constant, K (mm3)

Spring No

Calibration factor

(N-mm/Deg)

Torque, M

(N-mm)

Yield stress

τ (kPa)

Weight (gm)

Water content, w (%)

Solid content,

s (%)

Can Can + wet

slurry

Can + Dry

slurry

1 0 12.7 12.7 4290.12 1 0.89 0.00 0.00 15.54 28.04 17.52 531.31 15.84

2 0 12.7 12.7 4290.12 1 0.89 0.00 0.00 15.52 26.34 17.78 378.76 20.89

3 0 12.7 12.7 4290.12 1 0.89 0.00 0.00 15.54 27.54 18.62 289.61 25.67

4 0 12.7 12.7 4290.12 1 0.89 0.00 0.00 15.49 40.92 23.26 227.28 30.55

5 0 12.7 12.7 4290.12 1 0.89 0.00 0.00 15.53 34.53 21.77 204.49 32.84

6 0 12.7 12.7 4290.12 1 0.89 0.00 0.00 15.54 26.78 19.55 180.30 35.68

7 0 12.7 12.7 4290.12 1 0.89 0.00 0.00 15.56 25.04 19.16 163.33 37.97

8 0 12.7 12.7 4290.12 1 0.89 0.00 0.00 31.94 80.50 51.98 142.32 41.27

9 0 12.7 12.7 4290.12 1 0.89 0.00 0.00 31.8 89.67 57.26 127.30 44.00

10 1 12.7 12.7 4290.12 2 1.71 1.71 0.40 31.95 83.27 60.87 77.46 56.35

11 6 12.7 12.7 4290.12 2 1.71 10.26 2.39 32.07 77.97 62.67 50.00 66.67

12 5 12.7 12.7 4290.12 3 2.61 13.05 3.04 31.52 65.06 54.09 48.60 67.29

13 6 12.7 12.7 4290.12 3 2.61 15.66 3.65 32.03 71.17 59.28 43.63 69.62

14 33 12.7 12.7 4290.12 3 2.61 86.13 20.08 31.54 74.2 62.51 37.75 72.60

15 42 12.7 12.7 4290.12 3 2.61 109.62 25.55 31.8 48.7 44.28 35.42 73.85

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Table A2: Self-weight settling test data of 4% mill tailings sample

Test condition si = 20.2% si = 15.1%

Elapsed time (min) Interface height (cm) Interface height (cm)

0.1 8.50 8.50

1 8.45 8.40

2 8.40 7.70

3 8.40 7.40

4 8.35 7.20

5 8.35 7.00

6 8.30 6.80

7 8.25 6.60

8 8.25 6.40

9 8.20 6.30

10 8.20 6.25

20 7.80 5.65

30 7.50 5.30

40 7.30 5.10

50 7.15 4.90

60 7.00 4.75

70 6.85 4.60

80 6.70 4.50

90 6.60 4.40

100 6.50 4.35

200 5.90 4.30

300 5.40 4.25

400 5.20 4.20

500 5.10 4.20

1000 5.10 4.20

1200 5.10 4.20

1440 5.10 4.20

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Table A3: Segregation test data of 4% mill tailings sample (si = 20.2%)

Layer depth (cm) Weight (g) w (%) s (%)

From To can + wet can + dry can water solid

5.10 4.25 80.87 41.05 31.88 39.82 9.17 4.34 18.72

4.25 3.40 96.86 49.38 31.73 47.48 17.65 2.69 27.10

3.40 2.55 90.25 49.14 31.95 41.11 17.19 2.39 29.49

2.55 1.70 97.44 52.07 31.90 45.37 20.17 2.25 30.78

1.70 0.85 94.65 52.31 32.04 42.34 20.27 2.09 32.38

0.85 0.00 66.22 44.87 31.64 21.35 13.23 1.61 38.26

Table A4: Segregation test data of 4% mill tailings sample (si = 15.1%)

Layer depth (cm) Weight (g) w (%) s (%)

From To can + wet can + dry can water solid

4.20 3.50 92.69 41.20 31.72 51.49 9.48 5.43 15.55

3.50 2.80 82.03 43.96 31.81 38.07 12.15 3.13 24.19

2.80 2.10 72.85 43.22 31.92 29.63 11.30 2.62 27.61

2.10 1.40 73.92 44.59 32.09 29.33 12.50 2.35 29.88

1.40 0.70 77.88 46.83 31.71 31.05 15.12 2.05 32.75

0.70 0.00 72.13 48.59 32.91 23.54 15.68 1.50 39.98

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Table A5: Grain size analysis (sieve and hydrometer) of 4% mill tailings sample at si = 20.2% (top layer)

Sieve# Tare Dry mass % retained Cumulative % Passing

4 92.62 92.62 0.00 0.00 0.00 100.00

10 92.62 92.62 0.00 0.00 0.00 100.00

18 92.62 92.62 0.00 0.00 0.00 100.00

40 96.84 97.14 0.30 1.08 1.08 98.92

70 106.02 111.10 5.08 18.31 19.39 80.61

100 87.55 90.77 3.22 11.61 31.00 69.00

140 116.92 119.73 2.81 10.13 41.13 58.87

200 92.72 94.79 2.07 7.46 48.59 51.41

pan 473.03 487.29 14.26

Elapsed Hydrometer Temp Ct Corr. Hyd. Hyd. Corr. only Eff. Depth

Adjusted Diameter Percentage

Time (min) Reading (C)

Reading for meniscus L (cm) L/t K % Finer % Finer (mm) of Fine

0

0.5 19 18 -0.35 13.65 20 13.018 26.036 0.0138 71.04475 36.5212 0.070415 100

1 17 18 -0.35 11.65 18 13.3462 13.3462 0.0138 60.63526 31.17011 0.050415 85.34799

2 15 18 -0.35 9.65 16 13.6744 6.8372 0.0138 50.22577 25.81902 0.036084 70.69597

4 14 18 -0.35 8.65 15 13.8385 3.459625 0.0138 45.02103 23.14347 0.025668 63.36996

8 12 18 -0.35 6.65 13 14.1667 1.770838 0.0138 34.61154 17.79238 0.018364 48.71795

15 10 18 -0.35 4.65 11 14.4949 0.966327 0.0138 24.20206 12.44129 0.013566 34.06593

30 9 18 -0.35 3.65 10 14.659 0.488633 0.0138 18.99731 9.765742 0.009647 26.73993

60 8 18 -0.35 2.65 9 14.8231 0.247052 0.0138 13.79257 7.090196 0.006859 19.41392

120 8 18 -0.35 2.65 9 14.8231 0.123526 0.0138 13.79257 7.090196 0.00485 19.41392

240 8 18 -0.35 2.65 9 14.8231 0.061763 0.0138 13.79257 7.090196 0.00343 19.41392

480 8 18 -0.35 2.65 9 14.8231 0.030881 0.0138 13.79257 7.090196 0.002425 19.41392

1440 8 18 -0.35 2.65 9 14.8231 0.010294 0.0138 13.79257 7.090196 0.0014 19.41392

2880 8 18 -0.35 2.65 9 14.8231 0.005147 0.0138 13.79257 7.090196 0.00099 19.41392

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Table A6: Grain size analysis (sieve and hydrometer) of 4% mill tailings sample at si = 20.2% (mid layer)

Sieve# Tare Dry mass % retained Cumulative % Passing

4 92.62 92.62 0.00 0.00 0.00 100.00

10 92.62 92.62 0.00 0.00 0.00 100.00

18 92.62 92.62 0.00 0.00 0.00 100.00

40 96.84 97.51 0.67 1.75 1.75 98.25

70 106.02 114.39 8.37 21.91 23.66 76.34

100 87.54 92.39 4.85 12.70 36.36 63.64

140 116.89 120.72 3.83 10.03 46.39 53.61

200 92.72 95.54 2.82 7.38 53.77 46.23

pan 473.00 490.66 17.66

Elapsed Hydrometer Temp Ct Corr. Hyd. Hyd. Corr. only Eff. Depth

Adjusted Diameter Percentage

Time (min) Reading (C)

Reading for meniscus L (cm) L/t K % Finer % Finer (mm) of Fine

0

0.5 19 18 -0.35 13.65 20 13.018 26.036 0.0138 71.04475 32.84425 0.070415 100

1 17 18 -0.35 11.65 18 13.3462 13.3462 0.0138 60.63526 28.0319 0.050415 85.34799

2 16 18 -0.35 10.65 17 13.5103 6.75515 0.0138 55.43052 25.62573 0.035867 78.02198

4 15 18 -0.35 9.65 16 13.6744 3.4186 0.0138 50.22577 23.21956 0.025515 70.69597

8 14 18 -0.35 8.65 15 13.8385 1.729813 0.0138 45.02103 20.81339 0.01815 63.36996

15 12 18 -0.35 6.65 13 14.1667 0.944447 0.0138 34.61154 16.00104 0.013411 48.71795

30 10 18 -0.35 4.65 11 14.4949 0.483163 0.0138 24.20206 11.1887 0.009592 34.06593

60 9 18 -0.35 3.65 10 14.659 0.244317 0.0138 18.99731 8.782527 0.006821 26.73993

120 8 18 -0.35 2.65 9 14.8231 0.123526 0.0138 13.79257 6.376356 0.00485 19.41392

240 8 18 -0.35 2.65 9 14.8231 0.061763 0.0138 13.79257 6.376356 0.00343 19.41392

480 8 18 -0.35 2.65 9 14.8231 0.030881 0.0138 13.79257 6.376356 0.002425 19.41392

1440 8 18 -0.35 2.65 9 14.8231 0.010294 0.0138 13.79257 6.376356 0.0014 19.41392

2880 8 18 -0.35 2.65 9 14.8231 0.005147 0.0138 13.79257 6.376356 0.00099 19.41392

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Table A7: Grain size analysis (sieve and hydrometer) of 4% mill tailings sample at si = 20.2% (bottom layer)

Sieve# Tare Dry mass % retained Cumulative % Passing

4 92.62 92.62 0.00 0.00 0.00 100.00

10 92.62 92.62 0.00 0.00 0.00 100.00

18 92.62 92.62 0.00 0.00 0.00 100.00

40 96.85 97.76 0.91 2.65 2.65 97.35

70 106.02 114.80 8.78 25.53 28.18 71.82

100 87.52 92.04 4.52 13.14 41.32 58.68

140 116.88 120.00 3.12 9.07 50.39 49.61

200 92.71 95.08 2.37 6.89 57.28 42.72

pan 473.01 487.70 14.69

Elapsed Hydrometer Temp Ct Corr. Hyd. Hyd. Corr. only Eff. Depth

Adjusted Diameter Percentage

Time (min) Reading (C)

Reading for meniscus L (cm) L/t K % Finer % Finer (mm) of Fine

0

0.5 22 14 -1.35 15.65 23 12.5257 25.0514 0.0138 81.45423 34.79391 0.069071 100

1 20 13 -1.6 13.4 21 12.8539 12.8539 0.0138 69.74356 29.79159 0.049476 85.623

2 18 12 -1.85 11.15 19 13.1821 6.59105 0.0138 58.03289 24.78927 0.035429 71.24601

4 17 11 -2.1 9.9 18 13.3462 3.33655 0.0138 51.52696 22.01021 0.025207 63.25879

8 13 10 -2.35 5.65 14 14.0026 1.750325 0.0138 29.4068 12.56138 0.018257 36.10224

15 11 10 -2.35 3.65 12 14.3308 0.955387 0.0138 18.99731 8.114874 0.013489 23.32268

30 10 10 -2.35 2.65 11 14.4949 0.483163 0.0138 13.79257 5.891621 0.009592 16.93291

60 9 10 -2.35 1.65 10 14.659 0.244317 0.0138 8.587826 3.668368 0.006821 10.54313

120 8 9 -2.6 0.4 9 14.8231 0.123526 0.0138 2.081897 0.889301 0.00485 2.555911

240 8 9 -2.6 0.4 9 14.8231 0.061763 0.0138 2.081897 0.889301 0.00343 2.555911

480 8 9 -2.6 0.4 9 14.8231 0.030881 0.0138 2.081897 0.889301 0.002425 2.555911

1440 8 9 -2.6 0.4 9 14.8231 0.010294 0.0138 2.081897 0.889301 0.0014 2.555911

2880 8 9 -2.6 0.4 9 14.8231 0.005147 0.0138 2.081897 0.889301 0.00099 2.555911

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Table A8: Grain size analysis (sieve and hydrometer) of 4% mill tailings sample at si = 15.1% (top layer)

Sieve# Tare Dry mass % retained Cumulative % Passing

4 92.62 92.62 0.00 0.00 0.00 100.00

10 92.62 92.62 0.00 0.00 0.00 100.00

18 92.62 92.62 0.00 0.00 0.00 100.00

40 96.83 96.89 0.06 0.27 0.27 99.73

70 106.04 108.58 2.54 11.38 11.65 88.35

100 87.54 89.95 2.41 10.80 22.45 77.55

140 116.89 119.03 2.14 9.59 32.03 67.97

200 92.68 94.40 1.72 7.71 39.74 60.26

pan 473.02 486.47 13.45

Elapsed Hydrometer Temp Ct Corr. Hyd. Hyd. Corr. only Eff. Depth

Adjusted Diameter Percentage

Time (min) Reading (C)

Reading for meniscus L (cm) L/t K % Finer % Finer (mm) of Fine

0

0.5 19 18 -0.35 13.65 20 13.018 26.036 0.0138 71.04475 42.81146 0.070415 100

1 17 18 -0.35 11.65 18 13.3462 13.3462 0.0138 60.63526 36.53872 0.050415 85.34799

2 16.5 18 -0.35 11.15 17.5 13.42825 6.714125 0.0138 58.03289 34.97053 0.035758 81.68498

4 15 18 -0.35 9.65 16 13.6744 3.4186 0.0138 50.22577 30.26598 0.025515 70.69597

8 14 18 -0.35 8.65 15 13.8385 1.729813 0.0138 45.02103 27.12961 0.01815 63.36996

15 13 18 -0.35 7.65 14 14.0026 0.933507 0.0138 39.81629 23.99324 0.013333 56.04396

30 12 18 -0.35 6.65 13 14.1667 0.472223 0.0138 34.61154 20.85687 0.009483 48.71795

60 11 18 -0.35 5.65 12 14.3308 0.238847 0.0138 29.4068 17.7205 0.006744 41.39194

120 10 18 -0.35 4.65 11 14.4949 0.120791 0.0138 24.20206 14.58412 0.004796 34.06593

240 10 18 -0.35 4.65 11 14.4949 0.060395 0.0138 24.20206 14.58412 0.003391 34.06593

480 10 18 -0.35 4.65 11 14.4949 0.030198 0.0138 24.20206 14.58412 0.002398 34.06593

1440 10 18 -0.35 4.65 11 14.4949 0.010066 0.0138 24.20206 14.58412 0.001385 34.06593

2880 10 18 -0.35 4.65 11 14.4949 0.005033 0.0138 24.20206 14.58412 0.000979 34.06593

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Table A9: Grain size analysis (sieve and hydrometer) of 4% mill tailings sample at si = 15.1% (mid layer)

Sieve# Tare Dry mass % retained Cumulative % Passing

4 92.62 92.62 0.00 0.00 0.00 100.00

10 92.62 92.62 0.00 0.00 0.00 100.00

18 92.62 92.62 0.00 0.00 0.00 100.00

40 96.84 97.04 0.20 0.81 0.81 99.19

70 106.03 111.10 5.07 20.61 21.42 78.58

100 87.55 90.55 3.00 12.20 33.62 66.38

140 116.90 119.42 2.52 10.24 43.86 56.14

200 92.71 94.39 1.68 6.83 50.69 49.31

pan 473.02 485.15 12.13

Elapsed Hydrometer Temp Ct Corr. Hyd. Hyd. Corr. only Eff. Depth

Adjusted Diameter Percentage

Time (min) Reading (C)

Reading for meniscus L (cm) L/t K % Finer % Finer (mm) of Fine

0

0.5 20 18 -0.35 14.65 21 12.8539 25.7078 0.0138 76.24949 37.59782 0.06997 100

1 18 18 -0.35 12.65 19 13.1821 13.1821 0.0138 65.84 32.46501 0.050104 86.34812

2 17 18 -0.35 11.65 18 13.3462 6.6731 0.0138 60.63526 29.89861 0.035649 79.52218

4 16 18 -0.35 10.65 17 13.5103 3.377575 0.0138 55.43052 27.3322 0.025362 72.69625

8 15 18 -0.35 9.65 16 13.6744 1.7093 0.0138 50.22577 24.7658 0.018042 65.87031

15 14 18 -0.35 8.65 15 13.8385 0.922567 0.0138 45.02103 22.19939 0.013255 59.04437

30 12 18 -0.35 6.65 13 14.1667 0.472223 0.0138 34.61154 17.06659 0.009483 45.39249

60 10 18 -0.35 4.65 11 14.4949 0.241582 0.0138 24.20206 11.93378 0.006783 31.74061

120 9 18 -0.35 3.65 10 14.659 0.122158 0.0138 18.99731 9.367374 0.004823 24.91468

240 9 18 -0.35 3.65 10 14.659 0.061079 0.0138 18.99731 9.367374 0.003411 24.91468

480 9 18 -0.35 3.65 10 14.659 0.03054 0.0138 18.99731 9.367374 0.002412 24.91468

1440 9 18 -0.35 3.65 10 14.659 0.01018 0.0138 18.99731 9.367374 0.001392 24.91468

2880 9 18 -0.35 3.65 10 14.659 0.00509 0.0138 18.99731 9.367374 0.000985 24.91468

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Table A10: Grain size analysis (sieve and hydrometer) of 4% mill tailings sample at si = 15.1% (bottom layer)

Sieve# Tare Dry mass % retained Cumulative % Passing

4 92.62 92.62 0.00 0.00 0.00 100.00

10 92.62 92.62 0.00 0.00 0.00 100.00

18 92.62 92.62 0.00 0.00 0.00 100.00

40 96.84 98.13 1.29 3.98 3.98 96.02

70 106.02 116.11 10.09 31.10 35.08 64.92

100 87.53 91.82 4.29 13.22 48.30 51.70

140 116.90 119.69 2.79 8.60 56.91 43.09

200 92.69 94.61 1.92 5.92 62.82 37.18

pan 472.97 485.03 12.06

Elapsed Hydrometer Temp Ct Corr. Hyd. Hyd. Corr. only Eff. Depth

Adjusted Diameter Percentage

Time (min) Reading (C)

Reading for meniscus L (cm) L/t K % Finer % Finer (mm) of Fine

0

0.5 22 14 -1.35 15.65 23 12.5257 25.0514 0.0138 81.45423 30.28169 0.069071 100

1 20 13 -1.6 13.4 21 12.8539 12.8539 0.0138 69.74356 25.92809 0.049476 85.623

2 18 12 -1.85 11.15 19 13.1821 6.59105 0.0138 58.03289 21.5745 0.035429 71.24601

4 16 11 -2.1 8.9 17 13.5103 3.377575 0.0138 46.32222 17.2209 0.025362 56.86901

8 14 10 -2.35 6.65 15 13.8385 1.729813 0.0138 34.61154 12.8673 0.01815 42.49201

15 13 10 -2.35 5.65 14 14.0026 0.933507 0.0138 29.4068 10.93237 0.013333 36.10224

30 12 10 -2.35 4.65 13 14.1667 0.472223 0.0138 24.20206 8.997435 0.009483 29.71246

60 11 10 -2.35 3.65 12 14.3308 0.238847 0.0138 18.99731 7.062503 0.006744 23.32268

120 10 9 -2.6 2.4 11 14.4949 0.120791 0.0138 12.49138 4.643838 0.004796 15.33546

240 10 9 -2.6 2.4 11 14.4949 0.060395 0.0138 12.49138 4.643838 0.003391 15.33546

480 10 9 -2.6 2.4 11 14.4949 0.030198 0.0138 12.49138 4.643838 0.002398 15.33546

1440 10 9 -2.6 2.4 11 14.4949 0.010066 0.0138 12.49138 4.643838 0.001385 15.33546

2880 10 9 -2.6 2.4 11 14.4949 0.005033 0.0138 12.49138 4.643838 0.000979 15.33546

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Table A11: Consolidation test data of 4% mill tailings sample (self-weight)

Elapsed Time (min) Interface height (cm) Solids content (%) Void Ratio

0.1 10.00 31.94 5.75

1 10.00 32.42 5.75

2 9.95 32.53 5.72

3 9.95 32.53 5.72

4 9.90 32.64 5.70

5 9.90 32.64 5.70

6 9.90 32.64 5.70

7 9.85 32.75 5.67

8 9.85 32.75 5.67

9 9.80 32.86 5.64

10 9.80 32.86 5.64

20 9.75 32.98 5.61

30 9.70 33.09 5.58

40 9.65 33.21 5.55

50 9.60 33.32 5.52

60 9.55 33.44 5.49

70 9.50 33.55 5.47

80 9.40 33.79 5.41

90 9.35 33.91 5.38

100 9.25 34.15 5.32

200 8.9 35.02 5.12

300 8.7 35.54 5.01

400 8.6 35.81 4.95

500 8.5 36.08 4.89

1000 8.4 36.35 4.83

1200 8.4 36.35 4.83

1440 8.4 36.35 4.83

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Table A12: Consolidation test data of 4% mill tailings sample (σ' = 1.03 kPa)

Elapsed Time (min) Interface height (cm) Solids content (%) Void Ratio

0.1 8.40 36.35 4.83

1 8.30 36.64 4.77

2 8.20 36.92 4.72

3 8.10 37.21 4.66

4 8.00 37.50 4.60

5 7.90 37.80 4.54

6 7.80 38.10 4.49

7 7.70 38.40 4.43

8 7.60 38.71 4.37

9 7.55 38.87 4.34

10 7.50 39.02 4.31

20 7.20 40.00 4.14

30 7.00 40.68 4.03

40 6.85 41.20 3.94

50 6.75 41.56 3.88

60 6.70 41.74 3.85

70 6.70 41.74 3.85

80 6.70 41.74 3.85

90 6.70 41.74 3.85

100 6.70 41.74 3.85

200 6.65 41.92 3.82

300 6.65 41.92 3.82

400 6.6 42.11 3.80

500 6.6 42.11 3.80

1000 6.6 42.11 3.80

1200 6.6 42.11 3.80

1440 6.6 42.11 3.80

2880 6.6 42.11 3.80

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Table A13: Consolidation test data of 4% mill tailings sample (σ' = 2.01 kPa)

Elapsed Time (min) Interface height (cm) Solids content (%) Void Ratio

0.1 6.60 42.11 3.80

1 6.52 42.36 3.76

2 6.50 42.45 3.74

3 6.48 42.54 3.73

4 6.46 42.59 3.72

5 6.44 42.66 3.71

6 6.43 42.71 3.70

7 6.42 42.76 3.69

8 6.41 42.80 3.69

9 6.39 42.85 3.68

10 6.38 42.89 3.68

20 6.30 43.21 3.63

30 6.25 43.41 3.60

40 6.22 43.53 3.58

50 6.20 43.61 3.57

60 6.19 43.65 3.56

70 6.18 43.69 3.56

80 6.17 43.71 3.55

90 6.17 43.73 3.55

100 6.17 43.74 3.55

200 6.14 43.83 3.54

300 6.13 43.87 3.53

400 6.13 43.89 3.53

500 6.12 43.91 3.52

1000 6.11 43.95 3.52

1200 6.11 43.96 3.52

1440 6.11 43.98 3.52

2880 6.10 44.01 3.51

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Table A14: Consolidation test data of 4% mill tailings sample (σ' = 4.03 kPa)

Elapsed Time (min) Interface height (cm) Solids content (%) Void Ratio

0.1 6.10 44.01 3.51

1 6.09 44.04 3.51

2 6.09 44.06 3.50

3 6.09 44.07 3.50

4 6.08 44.08 3.50

5 6.08 44.08 3.50

6 6.08 44.11 3.50

7 6.07 44.13 3.49

8 6.06 44.16 3.49

9 6.06 44.16 3.49

10 6.06 44.17 3.49

20 6.04 44.24 3.48

30 6.03 44.29 3.47

40 6.02 44.33 3.47

50 6.01 44.36 3.46

60 6.01 44.38 3.46

70 6.00 44.40 3.46

80 6.00 44.42 3.45

90 5.99 44.44 3.45

100 5.99 44.46 3.45

200 5.97 44.55 3.44

300 5.96 44.58 3.43

400 5.95 44.61 3.43

500 5.95 44.62 3.42

1000 5.94 44.68 3.42

1200 5.94 44.69 3.42

1440 5.93 44.70 3.41

2880 5.93 44.72 3.41

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Table A15: Consolidation test data of 4% mill tailings sample (σ' = 8.33 kPa)

Elapsed Time (min) Interface height (cm) Solids content (%) Void Ratio

0.1 5.93 44.72 3.41

1 5.92 44.79 3.40

2 5.91 44.82 3.40

3 5.90 44.85 3.39

4 5.89 44.88 3.39

5 5.89 44.89 3.39

6 5.89 44.90 3.39

7 5.89 44.91 3.39

8 5.88 44.92 3.38

9 5.88 44.93 3.38

10 5.88 44.94 3.38

20 5.87 44.99 3.37

30 5.85 45.06 3.37

40 5.84 45.08 3.36

50 5.84 45.09 3.36

60 5.84 45.11 3.36

70 5.84 45.11 3.36

80 5.83 45.13 3.36

90 5.83 45.14 3.35

100 5.83 45.15 3.35

200 5.82 45.18 3.35

300 5.78 45.35 3.33

400 5.78 45.37 3.32

500 5.78 45.37 3.32

1000 5.77 45.41 3.32

1200 5.76 45.42 3.32

1440 5.76 45.44 3.31

2880 5.76 45.46 3.31

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Table A16: Hydraulic conductivity test data of 4% mill tailings sample (self-weight)

Elapsed time

Sample height (cm)

a (sq.cm)

A (sq.cm)

Initial head at burette, h1 (cm)

Initial time,

t1 (sec)

Final head at burette, h2 (cm)

Final time,

t2 (sec)

Hydraulic Conductivity

(m/Sec)

0 8.4 1.5 78.54 - - - - -

1 8.4 1.5 78.54 51.3 0 49.7 60 8.47×10-07

2 8.4 1.5 78.54 49.7 60 48.2 120 8.01×10-07

3 8.4 1.5 78.54 48.2 120 46.8 180 7.88×10-07

4 8.4 1.5 78.54 46.8 180 45.6 240 6.94×10-07

5 8.4 1.5 78.54 45.6 240 44.6 300 6.32×10-07

6 8.4 1.5 78.54 44.6 300 43.4 360 7.30×10-07

7 8.4 1.5 78.54 43.4 360 42.4 420 6.24×10-07

8 8.4 1.5 78.54 42.4 420 41.4 480 6.17×10-07

9 8.4 1.5 78.54 41.4 480 40.4 540 6.76×10-07

10 8.4 1.5 78.54 40.4 540 39.4 600 6.25×10-07

12 8.4 1.5 78.54 39.4 600 37.4 720 6.96×10-07

14 8.4 1.5 78.54 37.4 720 35.8 840 5.84×10-07

16 8.4 1.5 78.54 35.8 840 34.2 960 6.11×10-07

18 8.4 1.5 78.54 34.2 960 32.6 1080 6.67×10-07

20 8.4 1.5 78.54 32.6 1080 30.9 1200 7.02×10-07

22 8.4 1.5 78.54 30.9 1200 29.5 1320 6.20×10-07

24 8.4 1.5 78.54 29.5 1320 28.1 1440 6.50×10-07

26 8.4 1.5 78.54 28.1 1440 26.7 1560 6.83×10-07

28 8.4 1.5 78.54 26.7 1560 25.5 1680 6.15×10-07

30 8.4 1.5 78.54 25.5 1680 24.4 1800 6.08×10-07

35 8.4 1.5 78.54 24.4 1800 21.7 2100 6.12×10-07

40 8.4 1.5 78.54 21.7 2100 19.4 2400 6.07×10-07

45 8.4 1.5 78.54 19.4 2400 17.3 2700 6.13×10-07

50 8.4 1.5 78.54 17.3 2700 15.4 3000 6.11×10-07

55 8.4 1.5 78.54 15.4 3000 13.8 3300 6.11×10-07

60 8.4 1.5 78.54 13.8 3300 12.3 3600 6.11×10-07

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Table A17: Hydraulic conductivity test data of 4% mill tailings sample (σ' = 1.03 kPa)

Elapsed time

Sample height (cm)

a (sq.cm)

A (sq.cm)

Initial head at burette, h1 (cm)

Initial time,

t1 (sec)

Final head at burette, h2 (cm)

Final time,

t2 (sec)

Hydraulic Conductivity

(m/Sec)

0 6.6 1.5 78.54 - - - - -

1 6.6 1.5 78.54 51.3 0 50.1 60 4.97×10-07

2 6.6 1.5 78.54 50.1 60 49.4 120 2.81×10-07

3 6.6 1.5 78.54 49.4 120 48.8 180 2.85×10-07

4 6.6 1.5 78.54 48.8 180 48.2 240 2.60×10-07

5 6.6 1.5 78.54 48.2 240 47.6 300 2.34×10-07

6 6.6 1.5 78.54 47.6 300 47.1 360 2.37×10-07

7 6.6 1.5 78.54 47.1 360 46.4 420 2.99×10-07

8 6.6 1.5 78.54 46.4 420 45.9 480 2.43×10-07

9 6.6 1.5 78.54 45.9 480 45.3 540 2.76×10-07

10 6.6 1.5 78.54 45.3 540 44.7 600 2.80×10-07

12 6.6 1.5 78.54 44.7 600 43.6 720 2.54×10-07

14 6.6 1.5 78.54 43.6 720 42.4 840 2.93×10-07

16 6.6 1.5 78.54 42.4 840 41.5 960 2.34×10-07

18 6.6 1.5 78.54 41.5 960 40.4 1080 2.74×10-07

20 6.6 1.5 78.54 40.4 1080 39.3 1200 2.99×10-07

22 6.6 1.5 78.54 39.3 1200 38.3 1320 2.71×10-07

24 6.6 1.5 78.54 38.3 1320 37.4 1440 2.40×10-07

26 6.6 1.5 78.54 37.4 1440 36.4 1560 2.84×10-07

28 6.6 1.5 78.54 36.4 1560 35.6 1680 2.33×10-07

30 6.6 1.5 78.54 35.6 1680 34.7 1800 2.69×10-07

35 6.6 1.5 78.54 34.7 1800 32.6 2100 2.71×10-07

40 6.6 1.5 78.54 32.6 2100 30.5 2400 2.71×10-07

45 6.6 1.5 78.54 30.5 2400 28.6 2700 2.70×10-07

50 6.6 1.5 78.54 28.6 2700 26.8 3000 2.73×10-07

55 6.6 1.5 78.54 26.8 3000 25.2 3300 2.69×10-07

60 6.6 1.5 78.54 25.2 3300 23.6 3600 2.70×10-07

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Table A18: Hydraulic conductivity test data of 4% mill tailings sample (σ' = 2.01 kPa)

Elapsed time

Sample height (cm)

a (sq.cm)

A (sq.cm)

Initial head at burette, h1 (cm)

Initial time,

t1 (sec)

Final head at burette, h2 (cm)

Final time,

t2 (sec)

Hydraulic Conductivity

(m/Sec)

0 6.1 1.5 78.54 - - - - -

1 6.1 1.5 78.54 51.2 0.0 50.5 60 2.54×10-07

2 6.1 1.5 78.54 50.5 60.0 50.0 120 2.06×10-07

3 6.1 1.5 78.54 50.0 120.0 49.5 180 1.82×10-07

4 6.1 1.5 78.54 49.5 180.0 49.0 240 2.10×10-07

5 6.1 1.5 78.54 49.0 240.0 48.6 300 1.59×10-07

6 6.1 1.5 78.54 48.6 300.0 48.1 360 1.87×10-07

7 6.1 1.5 78.54 48.1 360.0 47.7 420 1.62×10-07

8 6.1 1.5 78.54 47.7 420.0 47.3 480 1.91×10-07

9 6.1 1.5 78.54 47.3 480.0 46.9 540 1.65×10-07

10 6.1 1.5 78.54 46.9 540.0 46.5 600 1.66×10-07

12 6.1 1.5 78.54 46.5 600.0 45.7 720 1.69×10-07

14 6.1 1.5 78.54 45.7 720.0 45.0 840 1.50×10-07

16 6.1 1.5 78.54 45.0 840.0 44.2 960 1.67×10-07

18 6.1 1.5 78.54 44.2 960.0 43.5 1080 1.48×10-07

20 6.1 1.5 78.54 43.5 1080.0 42.8 1200 1.65×10-07

22 6.1 1.5 78.54 42.8 1200.0 42.0 1320 1.83×10-07

24 6.1 1.5 78.54 42.0 1320.0 41.3 1440 1.71×10-07

26 6.1 1.5 78.54 41.3 1440.0 40.6 1560 1.58×10-07

28 6.1 1.5 78.54 40.6 1560.0 39.9 1680 1.77×10-07

30 6.1 1.5 78.54 39.9 1680.0 39.1 1800 1.89×10-07

35 6.1 1.5 78.54 39.1 1800.0 37.3 2100 1.86×10-07

40 6.1 1.5 78.54 37.3 2100.0 35.5 2400 1.85×10-07

45 6.1 1.5 78.54 35.5 2400.0 33.9 2700 1.87×10-07

50 6.1 1.5 78.54 33.9 2700.0 32.3 3000 1.88×10-07

55 6.1 1.5 78.54 32.3 3000.0 30.7 3300 1.89×10-07

60 6.1 1.5 78.54 30.7 3300.0 29.3 3600 1.86×10-07

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Table A19: Hydraulic conductivity test data of 4% mill tailings sample (σ' = 4.03 kPa)

Elapsed time

Sample height (cm)

a (sq.cm)

A (sq.cm)

Initial head at burette, h1 (cm)

Initial time,

t1 (sec)

Final head at burette, h2 (cm)

Final time,

t2 (sec)

Hydraulic Conductivity

(m/Sec)

0 5.9 1.5 78.54 - - - - -

1 5.9 1.5 78.54 51.2 0.0 50.6 60 2.21×10-07

2 5.9 1.5 78.54 50.6 60.0 50.3 120 1.24×10-07

3 5.9 1.5 78.54 50.3 120.0 49.9 180 1.25×10-07

4 5.9 1.5 78.54 49.9 180.0 49.5 240 1.51×10-07

5 5.9 1.5 78.54 49.5 240.0 49.2 300 1.27×10-07

6 5.9 1.5 78.54 49.2 300.0 48.8 360 1.40×10-07

7 5.9 1.5 78.54 48.8 360.0 48.5 420 1.16×10-07

8 5.9 1.5 78.54 48.5 420.0 48.2 480 1.29×10-07

9 5.9 1.5 78.54 48.2 480.0 47.9 540 1.30×10-07

10 5.9 1.5 78.54 47.9 540.0 47.5 600 1.31×10-07

12 5.9 1.5 78.54 47.5 600.0 46.8 720 1.46×10-07

14 5.9 1.5 78.54 46.8 720.0 46.2 840 1.21×10-07

16 5.9 1.5 78.54 46.2 840.0 45.5 960 1.50×10-07

18 5.9 1.5 78.54 45.5 960.0 44.8 1080 1.39×10-07

20 5.9 1.5 78.54 44.8 1080.0 44.1 1200 1.55×10-07

22 5.9 1.5 78.54 44.1 1200.0 43.4 1320 1.43×10-07

24 5.9 1.5 78.54 43.4 1320.0 42.8 1440 1.31×10-07

26 5.9 1.5 78.54 42.8 1440.0 42.1 1560 1.55×10-07

28 5.9 1.5 78.54 42.1 1560.0 41.5 1680 1.42×10-07

30 5.9 1.5 78.54 41.5 1680.0 40.8 1800 1.52×10-07

35 5.9 1.5 78.54 40.8 1800.0 39.2 2100 1.50×10-07

40 5.9 1.5 78.54 39.2 2100.0 37.7 2400 1.50×10-07

45 5.9 1.5 78.54 37.7 2400.0 36.2 2700 1.53×10-07

50 5.9 1.5 78.54 36.2 2700.0 34.7 3000 1.52×10-07

55 5.9 1.5 78.54 34.7 3000.0 33.3 3300 1.55×10-07

60 5.9 1.5 78.54 33.3 3300.0 32.0 3600 1.53×10-07

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Table A20: Hydraulic conductivity test data of 4% mill tailings sample (σ' = 8.33 kPa)

Elapsed time

Sample height (cm)

a (sq.cm)

A (sq.cm)

Initial head at burette, h1 (cm)

Initial time,

t1 (sec)

Final head at burette, h2 (cm)

Final time,

t2 (sec)

Hydraulic Conductivity

(m/Sec)

0 5.6 1.5 78.54 - - - - -

1 5.6 1.5 78.54 51.2 0.0 50.7 60 1.63×10-07

2 5.6 1.5 78.54 50.7 60.0 50.4 120 1.18×10-07

3 5.6 1.5 78.54 50.4 120.0 50.1 180 1.18×10-07

4 5.6 1.5 78.54 50.1 180.0 49.7 240 1.31×10-07

5 5.6 1.5 78.54 49.7 240.0 49.4 300 1.08×10-07

6 5.6 1.5 78.54 49.4 300.0 49.1 360 1.21×10-07

7 5.6 1.5 78.54 49.1 360.0 48.7 420 1.22×10-07

8 5.6 1.5 78.54 48.7 420.0 48.4 480 1.10×10-07

9 5.6 1.5 78.54 48.4 480.0 48.1 540 1.35×10-07

10 5.6 1.5 78.54 48.1 540.0 47.7 600 1.24×10-07

12 5.6 1.5 78.54 47.7 600.0 47.0 720 1.32×10-07

14 5.6 1.5 78.54 47.0 720.0 46.3 840 1.34×10-07

16 5.6 1.5 78.54 46.3 840.0 45.7 960 1.29×10-07

18 5.6 1.5 78.54 45.7 960.0 45.0 1080 1.31×10-07

20 5.6 1.5 78.54 45.0 1080.0 44.4 1200 1.20×10-07

22 5.6 1.5 78.54 44.4 1200.0 43.7 1320 1.35×10-07

24 5.6 1.5 78.54 43.7 1320.0 43.1 1440 1.23×10-07

26 5.6 1.5 78.54 43.1 1440.0 42.5 1560 1.39×10-07

28 5.6 1.5 78.54 42.5 1560.0 41.9 1680 1.27×10-07

30 5.6 1.5 78.54 41.9 1680.0 41.3 1800 1.29×10-07

35 5.6 1.5 78.54 41.3 1800.0 39.8 2100 1.29×10-07

40 5.6 1.5 78.54 39.8 2100.0 38.4 2400 1.28×10-07

45 5.6 1.5 78.54 38.4 2400.0 37.1 2700 1.26×10-07

50 5.6 1.5 78.54 37.1 2700.0 35.8 3000 1.27×10-07

55 5.6 1.5 78.54 35.8 3000.0 34.5 3300 1.25×10-07

60 5.6 1.5 78.54 34.5 3300.0 33.3 3600 1.26×10-07

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APPENDIX B

Laboratory test data of 5% mill tailings sample

Table B1: Vane shear test data of 5% mill tailings sample

Test No

Max. Angular Rotation

(Deg)

Height, H (mm)

Width, D (mm)

Vane Constant, K (mm3)

Spring No

Calibration factor

(N-mm/Deg)

Torque, M

(N-mm)

Yield stress

τ (kPa)

Weight (gm)

Water content, w (%)

Solid content,

s (%)

Can Can + wet

slurry

Can + Dry

slurry

1 0 12.7 12.7 4290.12 1 0.89 0.00 0.00 15.84 15.54 28.04 17.52 531.31

2 0 12.7 12.7 4290.12 1 0.89 0.00 0.00 20.89 15.52 26.34 17.78 378.76

3 0 12.7 12.7 4290.12 1 0.89 0.00 0.00 25.67 15.54 27.54 18.62 289.61

4 0 12.7 12.7 4290.12 1 0.89 0.00 0.00 30.55 15.49 40.92 23.26 227.28

5 0 12.7 12.7 4290.12 1 0.89 0.00 0.00 32.84 15.53 34.53 21.77 204.49

6 0 12.7 12.7 4290.12 1 0.89 0.00 0.00 35.68 15.54 26.78 19.55 180.30

7 0 12.7 12.7 4290.12 1 0.89 0.00 0.00 37.97 15.56 25.04 19.16 163.33

8 0.2 12.7 12.7 4290.12 2 1.71 0.34 0.08 40.18 15.55 42.93 26.55 148.91

9 0.3 12.7 12.7 4290.12 2 1.71 0.51 0.12 51.86 15.48 51.96 34.40 92.81

10 0.5 12.7 12.7 4290.12 2 1.71 0.86 0.20 53.61 15.52 59.54 39.12 86.53

11 1 12.7 12.7 4290.12 2 1.71 1.71 0.40 59.82 15.48 63.96 44.48 67.17

12 1.5 12.7 12.7 4290.12 2 1.71 2.57 0.60 62.60 15.54 64.20 46.00 59.75

13 6 12.7 12.7 4290.12 2 1.71 10.26 2.39 69.57 15.52 56.73 44.19 43.74

14 18.5 12.7 12.7 4290.12 2 1.71 31.64 7.37 70.83 15.54 62.61 48.88 41.18

15 22 12.7 12.7 4290.12 2 1.71 37.62 8.77 72.27 15.54 49.47 40.06 38.38

16 29 12.7 12.7 4290.12 2 1.71 49.59 11.56 74.68 15.52 47.12 39.12 33.90

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Table B2: Self-weight settling test data of 5% mill tailings sample

Test condition si = 20.4% si = 15.2%

Elapsed time (min) Interface height (cm) Interface height (cm)

0.1 8.50 8.50

1 8.30 8.20

2 8.10 7.90

3 7.90 7.60

4 7.70 7.30

5 7.55 7.10

6 7.40 6.90

7 7.25 6.70

8 7.10 6.50

9 7.00 6.35

10 6.90 6.20

20 5.50 4.60

30 5.25 4.20

40 5.10 4.00

50 4.95 3.80

60 4.80 3.70

70 4.70 3.60

80 4.65 3.50

90 4.60 3.45

100 4.55 3.40

200 4.50 3.35

300 4.40 3.30

400 4.40 3.25

500 4.40 3.25

1000 4.40 3.25

1200 4.40 3.25

1440 4.40 3.25

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Table B3: Segregation test data of 5% mill tailings sample (si = 20.4%)

Layer depth (cm) Weight (g) w (%) s (%)

From To can + wet can + dry can water solid

4.40 3.67 87.78 39.71 31.88 48.07 7.83 6.14 14.01

3.67 2.93 92.20 46.93 31.73 45.27 15.20 2.98 25.14

2.93 2.20 78.40 45.95 31.96 32.45 13.99 2.32 30.12

2.20 1.47 85.23 50.81 31.90 34.42 18.91 1.82 35.46

1.47 0.73 78.50 53.07 32.06 25.43 21.01 1.21 45.24

0.73 0.00 89.82 71.56 31.64 18.26 39.92 0.46 68.61

Table B4: Segregation test data of 5% mill tailings sample (si = 15.2%)

Layer depth (cm) Weight (g) w (%) s (%)

From To can + wet can + dry can water solid

3.25 2.708 76.92 37.55 31.92 39.37 5.63 6.99 12.51

2.71 2.168 67.35 38.38 31.88 28.97 6.50 4.46 18.33

2.17 1.628 62.98 39.53 31.98 23.45 7.55 3.11 24.35

1.63 1.088 64.09 40.19 31.96 23.90 8.23 2.90 25.61

1.09 0.548 74.94 49.47 32.10 25.47 17.37 1.47 40.55

0.55 0.008 69.95 62.02 31.70 7.93 30.32 0.26 79.27

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Table B5: Grain size analysis (sieve and hydrometer) of 5% mill tailings sample at si = 20.4% (top layer)

Sieve# Tare Dry mass % retained Cumulative % Passing

4 92.62 92.62 0.00 0.00 0.00 100.00

10 105.57 105.57 0.00 0.00 0.00 100.00

18 421.04 421.04 0.00 0.00 0.00 100.00

40 371.66 371.71 0.05 0.22 0.22 99.78

70 361.74 362.45 0.71 3.10 3.32 96.68

100 350.26 350.85 0.59 2.58 5.90 94.10

140 344.86 345.68 0.82 3.58 9.48 90.52

200 326.20 327.70 1.50 6.56 16.04 83.96

pan 369.75 388.96 19.21

Elapsed Hydrometer Temp Ct Corr. Hyd. Hyd. Corr. only Eff. Depth

Adjusted Diameter Percentage

Time (min) Reading (C)

Reading for meniscus L (cm) L/t K % Finer % Finer (mm) of Fine

0

0.5 22.0 18 -0.35 16.7 23.0 12.5 25.0514 0.0138 86.66 72.76 0.0691 100.00

1 21.0 18 -0.35 15.7 22.0 12.7 12.6898 0.0138 81.45 68.39 0.0492 93.99

2 20.0 18 -0.35 14.7 21.0 12.9 6.4270 0.0138 76.25 64.02 0.0350 87.99

4 20.0 18 -0.35 14.7 21.0 12.9 3.2135 0.0138 76.25 64.02 0.0247 87.99

8 19.0 18 -0.35 13.7 20.0 13.0 1.6273 0.0138 71.04 59.65 0.0176 81.98

15 17.0 18 -0.35 11.7 18.0 13.3 0.8897 0.0138 60.64 50.91 0.0130 69.97

30 16.0 18 -0.35 10.7 17.0 13.5 0.4503 0.0138 55.43 46.54 0.0093 63.96

60 15.0 18 -0.35 9.7 16.0 13.7 0.2279 0.0138 50.23 42.17 0.0066 57.96

120 15.0 18 -0.35 9.7 16.0 13.7 0.1140 0.0138 50.23 42.17 0.0047 57.96

240 14.0 18 -0.35 8.7 15.0 13.8 0.0577 0.0138 45.02 37.80 0.0033 51.95

480 10.0 18 -0.35 4.7 11.0 14.5 0.0302 0.0138 24.20 20.32 0.0024 27.93

1440 10.0 18 -0.35 4.7 11.0 14.5 0.0101 0.0138 24.20 20.32 0.0014 27.93

2880 10.0 18 -0.35 4.7 11.0 14.5 0.0050 0.0138 24.20 20.32 0.0010 27.93

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Table B6: Grain size analysis (sieve and hydrometer) of 5% mill tailings sample at si = 20.4% (mid layer)

Sieve# Tare Dry mass % retained Cumulative % Passing

4 92.62 92.62 0.00 0.00 0.00 100.00

10 105.57 105.57 0.00 0.00 0.00 100.00

18 421.04 421.04 0.00 0.00 0.00 100.00

40 371.66 371.71 0.05 0.15 0.15 99.85

70 361.74 362.61 0.87 2.61 2.76 97.24

100 350.26 352.80 2.54 7.63 10.39 89.61

140 344.86 350.31 5.45 16.36 26.75 73.25

200 326.20 329.78 3.58 10.75 37.50 62.50

pan 369.75 390.57 20.82

Elapsed Hydrometer Temp Ct Corr. Hyd. Hyd. Corr. only Eff. Depth

Adjusted Diameter Percentage

Time (min) Reading (C)

Reading for meniscus L (cm) L/t K % Finer % Finer (mm) of Fine

0

0.5 24.0 18 -0.35 18.7 21.0 12.9 25.7078 0.0138 97.07 60.67 0.0700 100.00

1 22.0 18 -0.35 16.7 20.0 13.0 13.0180 0.0138 86.66 54.17 0.0498 89.28

2 20.0 18 -0.35 14.7 19.0 13.2 6.5911 0.0138 76.25 47.66 0.0354 78.55

4 19.0 18 -0.35 13.7 18.0 13.3 3.3366 0.0138 71.04 44.41 0.0252 73.19

8 17.0 18 -0.35 11.7 17.0 13.5 1.6888 0.0138 60.64 37.90 0.0179 62.47

15 16.0 18 -0.35 10.7 16.0 13.7 0.9116 0.0138 55.43 34.65 0.0132 57.10

30 15.0 18 -0.35 9.7 15.0 13.8 0.4613 0.0138 50.23 31.39 0.0094 51.74

60 13.0 18 -0.35 7.7 14.0 14.0 0.2334 0.0138 39.82 24.89 0.0067 41.02

120 11.0 18 -0.35 5.7 13.0 14.2 0.1181 0.0138 29.41 18.38 0.0047 30.29

240 10.0 18 -0.35 4.7 12.0 14.3 0.0597 0.0138 24.20 15.13 0.0034 24.93

480 10.0 18 -0.35 4.7 11.0 14.5 0.0302 0.0138 24.20 15.13 0.0024 24.93

1440 10.0 18 -0.35 4.7 11.0 14.5 0.0101 0.0138 24.20 15.13 0.0014 24.93

2880 10.0 18 -0.35 4.7 11.0 14.5 0.0050 0.0138 24.20 15.13 0.0010 24.93

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Table B7: Grain size analysis (sieve and hydrometer) of 5% mill tailings sample at si = 20.4% (bottom layer)

Sieve# Tare Dry mass % retained Cumulative % Passing 4 92.62 92.62 0.00 0.00 0.00 100.00

10 105.57 105.57 0.00 0.00 0.00 100.00

18 421.04 421.04 0.00 0.00 0.00 100.00

40 371.66 373.46 1.80 2.92 2.92 97.08

70 361.74 384.23 22.49 36.53 39.45 60.55

100 350.26 361.15 10.89 17.69 57.14 42.86

140 344.86 352.35 7.49 12.17 69.30 30.70

200 326.20 330.57 4.37 7.10 76.40 23.60

pan 369.75 384.28 14.53

Elapsed Hydrometer Temp Ct Corr. Hyd. Hyd. Corr. only Eff. Depth

Adjusted Diameter Percentage

Time (min) Reading (C)

Reading for meniscus L (cm) L/t K % Finer % Finer (mm) of Fine

0

0.5 22.0 18 -0.35 16.7 23.0 12.5 25.0514 0.0138 86.66 20.45 0.0691 100.00

1 20.0 18 -0.35 14.7 21.0 12.9 12.8539 0.0138 76.25 17.99 0.0495 87.99

2 19.0 18 -0.35 13.7 20.0 13.0 6.5090 0.0138 71.04 16.77 0.0352 81.98

4 17.0 18 -0.35 11.7 18.0 13.3 3.3366 0.0138 60.64 14.31 0.0252 69.97

8 15.0 18 -0.35 9.7 16.0 13.7 1.7093 0.0138 50.23 11.85 0.0180 57.96

15 14.0 18 -0.35 8.7 15.0 13.8 0.9226 0.0138 45.02 10.62 0.0133 51.95

30 13.0 18 -0.35 7.7 14.0 14.0 0.4668 0.0138 39.82 9.40 0.0094 45.95

60 12.0 18 -0.35 6.7 13.0 14.2 0.2361 0.0138 34.61 8.17 0.0067 39.94

120 11.0 18 -0.35 5.7 12.0 14.3 0.1194 0.0138 29.41 6.94 0.0048 33.93

240 10.0 18 -0.35 4.7 11.0 14.5 0.0604 0.0138 24.20 5.71 0.0034 27.93

480 10.0 18 -0.35 4.7 11.0 14.5 0.0302 0.0138 24.20 5.71 0.0024 27.93

1440 10.0 18 -0.35 4.7 11.0 14.5 0.0101 0.0138 24.20 5.71 0.0014 27.93

2880 10.0 18 -0.35 4.7 11.0 14.5 0.0050 0.0138 24.20 5.71 0.0010 27.93

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Table B8: Grain size analysis (sieve and hydrometer) of 5% mill tailings sample at si = 15.2% (top layer)

Sieve# Tare Dry mass % retained Cumulative % Passing

4 92.62 92.62 0.00 0.00 0.00 100.00

10 92.62 92.62 0.00 0.00 0.00 100.00

18 92.62 92.62 0.00 0.00 0.00 100.00

40 96.85 96.87 0.02 0.15 0.15 99.85

70 106.02 106.11 0.09 0.69 0.84 99.16

100 87.50 87.61 0.11 0.84 1.68 98.32

140 116.90 116.97 0.07 0.53 2.21 97.79

200 92.72 93.08 0.36 2.75 4.96 95.04

pan 473.05 485.50 12.45

Elapsed Hydrometer Temp Ct Corr. Hyd. Hyd. Corr. only Eff. Depth

Adjusted Diameter Percentage

Time (min) Reading (C)

Reading for meniscus L (cm) L/t K % Finer % Finer (mm) of Fine

0

0.5 20.0 18 -0.35 14.7 21.0 12.9 25.7078 0.0138 76.25 72.47 0.0700 100.00

1 18.0 18 -0.35 12.7 19.0 13.2 13.1821 0.0138 65.84 62.57 0.0501 86.35

2 17.0 18 -0.35 11.7 18.0 13.3 6.6731 0.0138 60.64 57.63 0.0356 79.52

4 16.0 18 -0.35 10.7 17.0 13.5 3.3776 0.0138 55.43 52.68 0.0254 72.70

8 14.0 18 -0.35 8.7 15.0 13.8 1.7298 0.0138 45.02 42.79 0.0182 59.04

15 13.0 18 -0.35 7.7 14.0 14.0 0.9335 0.0138 39.82 37.84 0.0133 52.22

30 12.0 18 -0.35 6.7 13.0 14.2 0.4722 0.0138 34.61 32.89 0.0095 45.39

60 11.0 18 -0.35 5.7 12.0 14.3 0.2388 0.0138 29.41 27.95 0.0067 38.57

120 10.0 18 -0.35 4.7 11.0 14.5 0.1208 0.0138 24.20 23.00 0.0048 31.74

240 10.0 18 -0.35 4.7 11.0 14.5 0.0604 0.0138 24.20 23.00 0.0034 31.74

480 10.0 18 -0.35 4.7 11.0 14.5 0.0302 0.0138 24.20 23.00 0.0024 31.74

1440 10.0 18 -0.35 4.7 11.0 14.5 0.0101 0.0138 24.20 23.00 0.0014 31.74

2880 10.0 18 -0.35 4.7 11.0 14.5 0.0050 0.0138 24.20 23.00 0.0010 31.74

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Table B9: Grain size analysis (sieve and hydrometer) of 5% mill tailings sample at si = 15.2% (mid layer)

Sieve# Tare Dry mass % retained Cumulative % Passing

4 92.62 92.62 0.00 0.00 0.00 100.00

10 92.62 92.62 0.00 0.00 0.00 100.00

18 92.62 92.62 0.00 0.00 0.00 100.00

40 96.85 96.87 0.02 0.12 0.12 99.88

70 106.02 106.27 0.25 1.51 1.63 98.37

100 87.50 87.83 0.33 1.99 3.62 96.38

140 116.90 117.45 0.55 3.32 6.94 93.06

200 92.72 94.05 1.33 8.03 14.98 85.02

pan 473.00 487.08 14.08

Elapsed Hydrometer Temp Ct Corr. Hyd. Hyd. Corr. only Eff. Depth

Adjusted Diameter Percentage

Time (min) Reading (C)

Reading for meniscus L (cm) L/t K % Finer % Finer (mm) of Fine

0

0.5 21.0 18 -0.35 15.7 22.0 12.7 25.3796 0.0138 81.45 69.26 0.0695 100.00

1 19.0 18 -0.35 13.7 20.0 13.0 13.0180 0.0138 71.04 60.41 0.0498 87.22

2 17.0 18 -0.35 11.7 18.0 13.3 6.6731 0.0138 60.64 51.55 0.0356 74.44

4 16.0 18 -0.35 10.7 17.0 13.5 3.3776 0.0138 55.43 47.13 0.0254 68.05

8 14.0 18 -0.35 8.7 15.0 13.8 1.7298 0.0138 45.02 38.28 0.0182 55.27

15 13.0 18 -0.35 7.7 14.0 14.0 0.9335 0.0138 39.82 33.85 0.0133 48.88

30 12.0 18 -0.35 6.7 13.0 14.2 0.4722 0.0138 34.61 29.43 0.0095 42.49

60 11.0 18 -0.35 5.7 12.0 14.3 0.2388 0.0138 29.41 25.00 0.0067 36.10

120 10.0 18 -0.35 4.7 11.0 14.5 0.1208 0.0138 24.20 20.58 0.0048 29.71

240 9.0 18 -0.35 3.7 10.0 14.7 0.0611 0.0138 19.00 16.15 0.0034 23.32

480 9.0 18 -0.35 3.7 10.0 14.7 0.0305 0.0138 19.00 16.15 0.0024 23.32

1440 9.0 18 -0.35 3.7 10.0 14.7 0.0102 0.0138 19.00 16.15 0.0014 23.32

2880 9.0 18 -0.35 3.7 10.0 14.7 0.0051 0.0138 19.00 16.15 0.0010 23.32

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Table B10: Grain size analysis (sieve and hydrometer) of 5% mill tailings sample at si = 15.2% (bottom layer)

Sieve# Tare Dry mass % retained Cumulative % Passing

4 92.62 92.62 0.00 0.00 0.00 100.00

10 92.62 92.62 0.00 0.00 0.00 100.00

18 92.62 92.62 0.00 0.00 0.00 100.00

40 96.83 98.21 1.38 3.62 3.62 96.38

70 106.05 112.68 6.63 17.37 20.99 79.01

100 87.54 95.87 8.33 21.83 42.82 57.18

140 116.90 124.04 7.14 18.71 61.53 38.47

200 92.70 96.98 4.28 11.22 72.75 27.25

pan 473.01 483.41 10.40

Elapsed Hydrometer Temp Ct Corr. Hyd. Hyd. Corr. only Eff. Depth

Adjusted Diameter Percentage

Time (min) Reading (C)

Reading for meniscus L (cm) L/t K % Finer % Finer (mm) of Fine

0

0.5 22.0 14 -1.35 15.7 23.0 12.5 25.0514 0.0138 81.45 22.20 0.0691 100.00

1 20.0 13 -1.60 13.4 21.0 12.9 12.8539 0.0138 69.74 19.01 0.0495 85.62

2 18.0 12 -1.85 11.2 19.0 13.2 6.5911 0.0138 58.03 15.82 0.0354 71.25

4 17.0 11 -2.10 9.9 18.0 13.3 3.3366 0.0138 51.53 14.04 0.0252 63.26

8 16.0 10 -2.35 8.7 17.0 13.5 1.6888 0.0138 45.02 12.27 0.0179 55.27

15 15.0 10 -2.35 7.7 16.0 13.7 0.9116 0.0138 39.82 10.85 0.0132 48.88

30 13.0 10 -2.35 5.7 14.0 14.0 0.4668 0.0138 29.41 8.01 0.0094 36.10

60 12.0 10 -2.35 4.7 13.0 14.2 0.2361 0.0138 24.20 6.60 0.0067 29.71

120 11.0 9 -2.60 3.4 12.0 14.3 0.1194 0.0138 17.70 4.82 0.0048 21.73

240 10.0 9 -2.60 2.4 11.0 14.5 0.0604 0.0138 12.49 3.40 0.0034 15.34

480 10.0 9 -2.60 2.4 11.0 14.5 0.0302 0.0138 12.49 3.40 0.0024 15.34

1440 10.0 9 -2.60 2.4 11.0 14.5 0.0101 0.0138 12.49 3.40 0.0014 15.34

2880 10.0 9 -2.60 2.4 11.0 14.5 0.0050 0.0138 12.49 3.40 0.0010 15.34

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Table B11: Consolidation test data of 5% mill tailings sample (self-weight)

Elapsed Time (min) Interface height (cm) Solids content (%) Void Ratio

0.1 10.00 37.80 4.54

1 9.85 38.16 4.47

2 9.80 38.28 4.45

3 9.80 38.28 4.45

4 9.75 38.40 4.43

5 9.75 38.40 4.43

6 9.75 38.40 4.43

7 9.70 38.52 4.41

8 9.70 38.52 4.41

9 9.70 38.52 4.41

10 9.70 38.52 4.41

20 9.60 38.76 4.36

30 9.50 39.01 4.31

40 9.45 39.14 4.29

50 9.35 39.39 4.25

60 9.30 39.52 4.22

70 9.20 39.78 4.18

80 9.15 39.91 4.16

90 9.05 40.17 4.11

100 9.00 40.31 4.09

200 8.3 42.27 3.77

300 7.90 43.48 3.59

400 7.75 43.95 3.52

500 7.70 44.11 3.50

1000 7.6 44.43 3.45

1200 7.6 44.43 3.45

1440 7.6 44.43 3.45

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Table B12: Consolidation test data of 5% mill tailings sample (σ' = 1.05 kPa)

Elapsed Time (min) Interface height (cm) Solids content (%) Void Ratio

0.1 7.60 44.98 3.45

1 7.60 44.45 3.45

2 7.59 44.46 3.45

3 7.59 44.48 3.45

4 7.57 44.53 3.44

5 7.55 44.61 3.43

6 7.54 44.64 3.42

7 7.53 44.67 3.42

8 7.52 44.71 3.41

9 7.50 44.77 3.40

10 7.49 44.82 3.40

20 7.37 45.21 3.34

30 7.28 45.50 3.31

40 7.21 45.75 3.27

50 7.15 45.94 3.25

60 7.10 46.13 3.22

70 7.06 46.27 3.20

80 7.02 46.40 3.19

90 6.99 46.52 3.17

100 6.96 46.63 3.16

200 6.81 47.17 3.09

300 6.78 47.27 3.08

400 6.77 47.32 3.07

500 6.76 47.35 3.07

1000 6.74 47.41 3.06

1200 6.74 47.41 3.06

1440 6.74 47.42 3.06

2880 6.73 47.45 3.06

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Table B13: Consolidation test data of 5% mill tailings sample (σ' = 2.14 kPa)

Elapsed Time (min) Interface height (cm) Solids content (%) Void Ratio

0.1 6.73 47.45 3.06

1 6.72 47.47 3.05

2 6.72 47.49 3.05

3 6.71 47.51 3.05

4 6.70 47.53 3.05

5 6.70 47.55 3.04

6 6.70 47.56 3.04

7 6.69 47.58 3.04

8 6.69 47.59 3.04

9 6.68 47.61 3.04

10 6.68 47.61 3.04

20 6.65 47.72 3.02

30 6.63 47.80 3.01

40 6.62 47.86 3.01

50 6.60 47.91 3.00

60 6.59 47.95 3.00

70 6.58 47.98 2.99

80 6.58 48.01 2.99

90 6.57 48.03 2.99

100 6.57 48.04 2.98

200 6.55 48.13 2.97

300 6.54 48.15 2.97

400 6.54 48.17 2.97

500 6.53 48.18 2.97

1000 6.52 48.22 2.96

1200 6.52 48.22 2.96

1440 6.52 48.23 2.96

2880 6.52 48.24 2.96

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Table B14: Consolidation test data of 5% mill tailings sample (σ' = 4.17 kPa)

Elapsed Time (min) Interface height (cm) Solids content (%) Void Ratio

0.1 6.52 48.24 2.96

1 6.52 48.22 2.96

2 6.51 48.28 2.96

3 6.50 48.30 2.95

4 6.50 48.31 2.95

5 6.50 48.33 2.95

6 6.49 48.34 2.95

7 6.49 48.35 2.95

8 6.49 48.35 2.95

9 6.49 48.35 2.95

10 6.49 48.36 2.95

20 6.47 48.43 2.94

30 6.45 48.49 2.93

40 6.44 48.53 2.93

50 6.43 48.57 2.92

60 6.43 48.59 2.92

70 6.42 48.62 2.92

80 6.42 48.64 2.91

90 6.41 48.65 2.91

100 6.41 48.67 2.91

200 6.39 48.75 2.90

300 6.38 48.78 2.90

400 6.38 48.79 2.90

500 6.37 48.81 2.90

1000 6.37 48.84 2.89

1200 6.36 48.85 2.89

1440 6.36 48.85 2.89

2880 6.35 48.88 2.89

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Table B15: Consolidation test data of 5% mill tailings sample (σ' = 8.55 kPa)

Elapsed Time (min) Interface height (cm) Solids content (%) Void Ratio

0.1 6.36 48.88 2.89

1 6.34 48.90 2.88

2 6.33 48.93 2.88

3 6.33 48.95 2.88

4 6.32 48.97 2.88

5 6.32 48.99 2.87

6 6.31 49.01 2.87

7 6.31 49.03 2.87

8 6.31 49.04 2.87

9 6.30 49.05 2.87

10 6.30 49.07 2.86

20 6.29 49.09 2.86

30 6.29 49.10 2.86

40 6.29 49.11 2.86

50 6.28 49.14 2.86

60 6.28 49.16 2.85

70 6.27 49.18 2.85

80 6.27 49.19 2.85

90 6.27 49.20 2.85

100 6.27 49.20 2.85

200 6.25 49.25 2.84

300 6.25 49.28 2.84

400 6.24 49.29 2.84

500 6.24 49.30 2.84

1000 6.24 49.32 2.84

1200 6.23 49.33 2.83

1440 6.23 49.34 2.83

2880 6.23 49.34 2.83

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Table B16: Hydraulic conductivity test data of 5% mill tailings sample (self-weight)

Elapsed time

Sample height (cm)

a (sq.cm)

A (sq.cm)

Initial head at burette, h1 (cm)

Initial time,

t1 (sec)

Final head at burette, h2 (cm)

Final time,

t2 (sec)

Hydraulic Conductivity

(m/Sec)

0 7.6 1.5 78.54 - - - - -

1 7.6 1.5 78.54 51.3 0 50.6 60 3.16×10-07

2 7.6 1.5 78.54 50.6 60 50.0 120 2.88×10-07

3 7.6 1.5 78.54 50.0 120 49.5 180 2.59×10-07

4 7.6 1.5 78.54 49.5 180 49.1 240 1.96×10-07

5 7.6 1.5 78.54 49.1 240 48.8 300 1.65×10-07

6 7.6 1.5 78.54 48.8 300 48.4 360 1.99×10-07

7 7.6 1.5 78.54 48.4 360 47.9 420 2.35×10-07

8 7.6 1.5 78.54 47.9 420 47.6 480 1.69×10-07

9 7.6 1.5 78.54 47.6 480 47.2 540 2.04×10-07

10 7.6 1.5 78.54 47.2 540 46.8 600 1.89×10-07

12 7.6 1.5 78.54 46.8 600 46.2 720 1.47×10-07

14 7.6 1.5 78.54 46.2 720 45.6 840 1.76×10-07

16 7.6 1.5 78.54 45.6 840 45.0 960 1.51×10-07

18 7.6 1.5 78.54 45.0 960 44.3 1080 1.81×10-07

20 7.6 1.5 78.54 44.3 1080 43.8 1200 1.56×10-07

22 7.6 1.5 78.54 43.8 1200 43.2 1320 1.67×10-07

24 7.6 1.5 78.54 43.2 1320 42.6 1440 1.50×10-07

26 7.6 1.5 78.54 42.6 1440 42.0 1560 1.71×10-07

28 7.6 1.5 78.54 42.0 1560 41.5 1680 1.54×10-07

30 7.6 1.5 78.54 41.5 1680 41.0 1800 1.50×10-07

35 7.6 1.5 78.54 41.0 1800 39.7 2100 1.50×10-07

40 7.6 1.5 78.54 39.7 2100 38.5 2400 1.50×10-07

45 7.6 1.5 78.54 38.5 2400 37.3 2700 1.50×10-07

50 7.6 1.5 78.54 37.3 2700 36.1 3000 1.50×10-07

55 7.6 1.5 78.54 36.1 3000 35.0 3300 1.50×10-07

60 7.6 1.5 78.54 35.0 3300 33.9 3600 1.50×10-07

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Table B17: Hydraulic conductivity test data of 5% mill tailings sample (σ' = 1.05 kPa)

Elapsed time

Sample height (cm)

a (sq.cm)

A (sq.cm)

Initial head at burette, h1 (cm)

Initial time,

t1 (sec)

Final head at burette, h2 (cm)

Final time,

t2 (sec)

Hydraulic Conductivity

(m/Sec)

0 6.7 1.5 78.54 - - - - -

1 6.7 1.5 78.54 51.3 0 50.9 60 1.68×10-07

2 6.7 1.5 78.54 50.9 60 50.7 120 8.43×10-08

3 6.7 1.5 78.54 50.7 120 50.5 180 8.47×10-08

4 6.7 1.5 78.54 50.5 180 50.3 240 7.08×10-08

5 6.7 1.5 78.54 50.3 240 50.1 300 8.53×10-08

6 6.7 1.5 78.54 50.1 300 50.0 360 7.13×10-08

7 6.7 1.5 78.54 50.0 360 49.8 420 8.59×10-08

8 6.7 1.5 78.54 49.8 420 49.6 480 7.19×10-08

9 6.7 1.5 78.54 49.6 480 49.4 540 7.21×10-08

10 6.7 1.5 78.54 49.4 540 49.2 600 8.68×10-08

12 6.7 1.5 78.54 49.2 600 48.9 720 6.55×10-08

14 6.7 1.5 78.54 48.9 720 48.6 840 8.06×10-08

16 6.7 1.5 78.54 48.6 840 48.3 960 6.64×10-08

18 6.7 1.5 78.54 48.3 960 47.9 1080 8.17×10-08

20 6.7 1.5 78.54 47.9 1080 47.6 1200 7.48×10-08

22 6.7 1.5 78.54 47.6 1200 47.2 1320 8.29×10-08

24 6.7 1.5 78.54 47.2 1320 46.9 1440 7.59×10-08

26 6.7 1.5 78.54 46.9 1440 46.5 1560 7.65×10-08

28 6.7 1.5 78.54 46.5 1560 46.2 1680 7.70×10-08

30 6.7 1.5 78.54 46.2 1680 45.9 1800 7.91×10-08

35 6.7 1.5 78.54 45.9 1800 45.0 2100 7.86×10-08

40 6.7 1.5 78.54 45.0 2100 44.2 2400 7.81×10-08

45 6.7 1.5 78.54 44.2 2400 43.4 2700 7.82×10-08

50 6.7 1.5 78.54 43.4 2700 42.6 3000 7.90×10-08

55 6.7 1.5 78.54 42.6 3000 41.8 3300 7.98×10-08

60 6.7 1.5 78.54 41.8 3300 41.1 3600 7.92×10-08

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Table B18: Hydraulic conductivity test data of 5% mill tailings sample (σ' = 2.14 kPa)

Elapsed time

Sample height (cm)

a (sq.cm)

A (sq.cm)

Initial head at burette, h1 (cm)

Initial time,

t1 (sec)

Final head at burette, h2 (cm)

Final time,

t2 (sec)

Hydraulic Conductivity

(m/Sec)

0 6.5 1.5 78.54 - - - - -

1 6.5 1.5 78.54 51.2 0.0 50.9 60 1.08×10-07

2 6.5 1.5 78.54 50.9 60.0 50.7 120 8.17×10-08

3 6.5 1.5 78.54 50.7 120.0 50.6 180 6.83×10-08

4 6.5 1.5 78.54 50.6 180.0 50.4 240 6.85×10-08

5 6.5 1.5 78.54 50.4 240.0 50.3 300 5.50×10-08

6 6.5 1.5 78.54 50.3 300.0 50.1 360 5.51×10-08

7 6.5 1.5 78.54 50.1 360.0 50.0 420 5.53×10-08

8 6.5 1.5 78.54 50.0 420.0 49.9 480 5.54×10-08

9 6.5 1.5 78.54 49.9 480.0 49.7 540 5.56×10-08

10 6.5 1.5 78.54 49.7 540.0 49.6 600 5.57×10-08

12 6.5 1.5 78.54 49.6 600.0 49.4 720 4.89×10-08

14 6.5 1.5 78.54 49.4 720.0 49.1 840 6.33×10-08

16 6.5 1.5 78.54 49.1 840.0 48.8 960 5.65×10-08

18 6.5 1.5 78.54 48.8 960.0 48.5 1080 6.40×10-08

20 6.5 1.5 78.54 48.5 1080.0 48.3 1200 5.00×10-08

22 6.5 1.5 78.54 48.3 1200.0 48.0 1320 6.47×10-08

24 6.5 1.5 78.54 48.0 1320.0 47.7 1440 5.06×10-08

26 6.5 1.5 78.54 47.7 1440.0 47.4 1560 6.54×10-08

28 6.5 1.5 78.54 47.4 1560.0 47.2 1680 5.12×10-08

30 6.5 1.5 78.54 47.2 1680.0 46.9 1800 5.73×10-08

35 6.5 1.5 78.54 46.9 1800.0 46.3 2100 5.70×10-08

40 6.5 1.5 78.54 46.3 2100.0 45.7 2400 5.72×10-08

45 6.5 1.5 78.54 45.7 2400.0 45.0 2700 5.80×10-08

50 6.5 1.5 78.54 45.0 2700.0 44.4 3000 5.75×10-08

55 6.5 1.5 78.54 44.4 3000.0 43.8 3300 5.77×10-08

60 6.5 1.5 78.54 43.8 3300.0 43.2 3600 5.73×10-08

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Table B19: Hydraulic conductivity test data of 5% mill tailings sample (σ' = 4.17 kPa)

Elapsed time

Sample height (cm)

a (sq.cm)

A (sq.cm)

Initial head at burette, h1 (cm)

Initial time,

t1 (sec)

Final head at burette, h2 (cm)

Final time,

t2 (sec)

Hydraulic Conductivity

(m/Sec)

0 6.4 1.5 78.54 - - - - -

1 6.4 1.5 78.54 51.2 0.0 51.0 60 9.23×10-08

2 6.4 1.5 78.54 51.0 60.0 50.8 120 6.62×10-08

3 6.4 1.5 78.54 50.8 120.0 50.6 180 6.64×10-08

4 6.4 1.5 78.54 50.6 180.0 50.5 240 6.13×10-08

5 6.4 1.5 78.54 50.5 240.0 50.3 300 5.88×10-08

6 6.4 1.5 78.54 50.3 300.0 50.2 360 5.36×10-08

7 6.4 1.5 78.54 50.2 360.0 50.1 420 5.38×10-08

8 6.4 1.5 78.54 50.1 420.0 49.9 480 5.39×10-08

9 6.4 1.5 78.54 49.9 480.0 49.8 540 5.40×10-08

10 6.4 1.5 78.54 49.8 540.0 49.7 600 5.42×10-08

12 6.4 1.5 78.54 49.7 600.0 49.4 720 5.44×10-08

14 6.4 1.5 78.54 49.4 720.0 49.2 840 4.78×10-08

16 6.4 1.5 78.54 49.2 840.0 48.9 960 4.81×10-08

18 6.4 1.5 78.54 48.9 960.0 48.7 1080 4.14×10-08

20 6.4 1.5 78.54 48.7 1080.0 48.5 1200 4.85×10-08

22 6.4 1.5 78.54 48.5 1200.0 48.3 1320 4.18×10-08

24 6.4 1.5 78.54 48.3 1320.0 48.1 1440 4.89×10-08

26 6.4 1.5 78.54 48.1 1440.0 47.9 1560 4.21×10-08

28 6.4 1.5 78.54 47.9 1560.0 47.6 1680 5.65×10-08

30 6.4 1.5 78.54 47.6 1680.0 47.4 1800 4.97×10-08

35 6.4 1.5 78.54 47.4 1800.0 46.8 2100 4.98×10-08

40 6.4 1.5 78.54 46.8 2100.0 46.2 2400 5.10×10-08

45 6.4 1.5 78.54 46.2 2400.0 45.6 2700 4.99×10-08

50 6.4 1.5 78.54 45.6 2700.0 45.1 3000 5.05×10-08

55 6.4 1.5 78.54 45.1 3000.0 44.5 3300 4.99×10-08

60 6.4 1.5 78.54 44.5 3300.0 44.0 3600 5.00×10-08

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Table B20: Hydraulic conductivity test data of 5% mill tailings sample (σ' = 8.55 kPa)

Elapsed time

Sample height (cm)

a (sq.cm)

A (sq.cm)

Initial head at burette, h1 (cm)

Initial time,

t1 (sec)

Final head at burette, h2 (cm)

Final time,

t2 (sec)

Hydraulic Conductivity

(m/Sec)

0 6.2 1.5 78.54 - - - - -

1 6.2 1.5 78.54 51.2 0.0 51.0 60 7.76×10-08

2 6.2 1.5 78.54 51.0 60.0 50.9 120 5.19×10-08

3 6.2 1.5 78.54 50.9 120.0 50.8 180 3.90×10-08

4 6.2 1.5 78.54 50.8 180.0 50.7 240 3.91×10-08

5 6.2 1.5 78.54 50.7 240.0 50.5 300 5.23×10-08

6 6.2 1.5 78.54 50.5 300.0 50.4 360 3.93×10-08

7 6.2 1.5 78.54 50.4 360.0 50.3 420 3.94×10-08

8 6.2 1.5 78.54 50.3 420.0 50.2 480 5.26×10-08

9 6.2 1.5 78.54 50.2 480.0 50.1 540 3.95×10-08

10 6.2 1.5 78.54 50.1 540.0 50.0 600 4.49×10-08

12 6.2 1.5 78.54 50.0 600.0 49.8 720 3.71×10-08

14 6.2 1.5 78.54 49.8 720.0 49.6 840 4.66×10-08

16 6.2 1.5 78.54 49.6 840.0 49.4 960 3.34×10-08

18 6.2 1.5 78.54 49.4 960.0 49.2 1080 4.02×10-08

20 6.2 1.5 78.54 49.2 1080.0 49.0 1200 4.71×10-08

22 6.2 1.5 78.54 49.0 1200.0 48.8 1320 3.38×10-08

24 6.2 1.5 78.54 48.8 1320.0 48.6 1440 4.07×10-08

26 6.2 1.5 78.54 48.6 1440.0 48.4 1560 3.41×10-08

28 6.2 1.5 78.54 48.4 1560.0 48.2 1680 4.79×10-08

30 6.2 1.5 78.54 48.2 1680.0 48.0 1800 4.12×10-08

35 6.2 1.5 78.54 48.0 1800.0 47.5 2100 4.15×10-08

40 6.2 1.5 78.54 47.5 2100.0 47.0 2400 4.20×10-08

45 6.2 1.5 78.54 47.0 2400.0 46.5 2700 4.24×10-08

50 6.2 1.5 78.54 46.5 2700.0 46.0 3000 4.29×10-08

55 6.2 1.5 78.54 46.0 3000.0 45.5 3300 4.33×10-08

60 6.2 1.5 78.54 45.5 3300.0 45.0 3600 4.38×10-08

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APPENDIX C

Laboratory test data of 6% mill tailings sample

Table C1: Vane shear test data of 6% mill tailings sample

Test No

Max. Angular Rotation

(Deg)

Height, H (mm)

Width, D (mm)

Vane Constant, K (mm3)

Spring No

Calibration factor

(N-mm/Deg)

Torque, M

(N-mm)

Yield stress

τ (kPa)

Weight (gm)

Water content, w (%)

Solid content,

s (%) Can

Can + wet slurry

Can + Dry

slurry

1 0 12.7 12.7 4290.12 1 0.89 0.00 0.00 15.84 15.54 28.04 17.52 531.31

2 0 12.7 12.7 4290.12 1 0.89 0.00 0.00 20.89 15.52 26.34 17.78 378.76

3 0 12.7 12.7 4290.12 1 0.89 0.00 0.00 25.67 15.54 27.54 18.62 289.61

4 0 12.7 12.7 4290.12 1 0.89 0.00 0.00 30.55 15.49 40.92 23.26 227.28

5 0 12.7 12.7 4290.12 1 0.89 0.00 0.00 32.84 15.53 34.53 21.77 204.49

6 0 12.7 12.7 4290.12 1 0.89 0.00 0.00 35.68 15.54 26.78 19.55 180.30

7 0.5 12.7 12.7 4290.12 1 0.89 0.45 0.10 62.21 31.92 85.00 64.94 60.75

8 0 12.7 12.7 4290.12 1 0.89 0.00 0.00 60.89 31.65 79.59 60.84 64.23

9 0 12.7 12.7 4290.12 1 0.89 0.00 0.00 61.99 31.84 95.95 71.58 61.32

10 0 12.7 12.7 4290.12 1 0.89 0.00 0.00 61.01 31.45 87.75 65.80 63.90

11 7 12.7 12.7 4290.12 2 1.71 11.97 2.79 67.22 31.92 77.71 62.70 48.77

12 2.5 12.7 12.7 4290.12 2 1.71 4.28 1.00 62.45 32.02 77.13 60.19 60.13

13 16 12.7 12.7 4290.12 2 1.71 27.36 6.38 70.39 31.5 74.7 61.91 42.06

14 58 12.7 12.7 4290.12 2 1.71 99.18 23.12 72.43 31.87 73.98 62.37 38.07

15 10.5 12.7 12.7 4290.12 2 1.71 17.96 4.19 70.02 31.75 80.89 66.16 42.81

16 8.5 12.7 12.7 4290.12 2 1.71 14.54 3.39 68.27 31.92 75.38 61.59 46.48

17 25.5 12.7 12.7 4290.12 2 1.71 43.61 10.16 71.10 31.49 84.05 68.86 40.65

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Table C2: Self-weight settling test data of 6% mill tailings sample

Test condition si = 20% si = 15.2%

Elapsed time (min) Interface height (cm) Interface height (cm)

0.1 8.50 8.50

1 8.20 8.10

2 8.00 7.85

3 7.70 7.55

4 7.50 7.30

5 7.30 7.10

6 7.10 6.85

7 6.90 6.60

8 6.60 6.35

9 6.30 6.10

10 6.10 5.80

20 5.20 4.70

30 4.90 4.30

40 4.70 4.10

50 4.50 4.00

60 4.45 3.85

70 4.40 3.80

80 4.35 3.70

90 4.35 3.65

100 4.30 3.65

200 4.20 3.60

300 4.10 3.55

400 4.10 3.50

500 4.10 3.50

1000 4.10 3.50

1200 4.10 3.50

1440 4.10 3.50

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Table C3: Segregation test data of 6% mill tailings sample (si = 20%)

Layer depth (cm) Weight (g) w (%) s (%)

From To can + wet can + dry can water solid

4.10 3.42 81.90 39.67 31.85 42.23 7.82 5.40 15.62

3.42 2.73 76.94 42.40 31.73 34.54 10.67 3.24 23.60

2.73 2.05 75.94 45.14 31.93 30.80 13.21 2.33 30.02

2.05 1.37 72.77 45.78 31.87 26.99 13.91 1.94 34.01

1.37 0.68 86.85 53.04 31.64 33.81 21.40 1.58 38.76

0.68 0.00 85.29 65.40 32.04 19.89 33.36 0.60 62.65

Table C4: Segregation test data of 6% mill tailings sample (si = 15.2%)

Layer depth (cm) Weight (g) w (%) s (%)

From To can + wet can + dry can water solid

3.50 2.92 76.61 38.28 31.86 38.33 6.42 5.97 14.35

2.92 2.33 69.00 39.89 31.75 29.11 8.14 3.58 21.85

2.33 1.75 76.12 43.11 31.93 33.01 11.18 2.95 25.30

1.75 1.17 63.36 41.13 31.86 22.23 9.27 2.40 29.43

1.17 0.58 75.40 50.38 32.02 25.02 18.36 1.36 42.32

0.58 0.00 73.56 58.90 31.63 14.66 27.27 0.54 65.04

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Table C5: Grain size analysis (sieve and hydrometer) of 6% mill tailings sample at si = 20.0% (top layer)

Sieve# Tare Dry mass % retained Cumulative % Passing

4 92.62 92.62 0.00 0.00 0.00 100.00

10 92.62 92.62 0.00 0.00 0.00 100.00

18 92.62 92.62 0.00 0.00 0.00 100.00

40 96.83 96.85 0.02 0.10 0.10 99.90

70 106.03 106.06 0.03 0.16 0.26 99.74

100 87.52 87.55 0.03 0.16 0.42 99.58

140 116.90 117.14 0.24 1.25 1.67 98.33

200 92.71 93.32 0.61 3.19 4.86 95.14

pan 126.42 144.64 18.22

Elapsed Hydrometer Temp Ct Corr. Hyd. Hyd. Corr. only Eff. Depth

Adjusted Diameter Percentage

Time (min) Reading (C)

Reading for meniscus L (cm) L/t K % Finer % Finer (mm) of Fine

0

0.5 19.0 18 -0.35 13.7 20.0 13.0 26.0360 0.0138 71.04 67.59 0.0704 100.00

1 17.0 18 -0.35 11.7 18.0 13.3 13.3462 0.0138 60.64 57.69 0.0504 85.35

2 16.0 18 -0.35 10.7 17.0 13.5 6.7552 0.0138 55.43 52.74 0.0359 78.02

4 15.0 18 -0.35 9.7 16.0 13.7 3.4186 0.0138 50.23 47.79 0.0255 70.70

8 13.0 18 -0.35 7.7 14.0 14.0 1.7503 0.0138 39.82 37.88 0.0183 56.04

15 12.0 18 -0.35 6.7 13.0 14.2 0.9444 0.0138 34.61 32.93 0.0134 48.72

30 11.0 18 -0.35 5.7 12.0 14.3 0.4777 0.0138 29.41 27.98 0.0095 41.39

60 10.0 18 -0.35 4.7 11.0 14.5 0.2416 0.0138 24.20 23.03 0.0068 34.07

120 9.0 18 -0.35 3.7 10.0 14.7 0.1222 0.0138 19.00 18.07 0.0048 26.74

240 9.0 18 -0.35 3.7 10.0 14.7 0.0611 0.0138 19.00 18.07 0.0034 26.74

480 9.0 18 -0.35 3.7 10.0 14.7 0.0305 0.0138 19.00 18.07 0.0024 26.74

1440 9.0 18 -0.35 3.7 10.0 14.7 0.0102 0.0138 19.00 18.07 0.0014 26.74

2880 9.0 18 -0.35 3.7 10.0 14.7 0.0051 0.0138 19.00 18.07 0.0010 26.74

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Table C6: Grain size analysis (sieve and hydrometer) of 6% mill tailings sample at si = 20.0% (mid layer)

Sieve# Tare Dry mass % retained Cumulative % Passing

4 92.62 92.62 0.00 0.00 0.00 100.00

10 92.62 92.62 0.00 0.00 0.00 100.00

18 92.62 92.62 0.00 0.00 0.00 100.00

40 96.84 96.87 0.03 0.11 0.11 99.89

70 106.00 106.85 0.85 3.07 3.17 96.83

100 87.48 88.92 1.44 5.19 8.37 91.63

140 116.89 119.32 2.43 8.76 17.13 82.87

200 92.69 95.82 3.13 11.29 28.42 71.58

pan 473.03 492.88 19.85

Elapsed Hydrometer Temp Ct Corr. Hyd. Hyd. Corr. only Eff. Depth

Adjusted Diameter Percentage

Time (min) Reading (C)

Reading for meniscus L (cm) L/t K % Finer % Finer (mm) of Fine

0

0.5 20.0 18 -0.35 14.7 21.0 12.9 25.7078 0.0138 76.25 54.58 0.0700 100.00

1 18.0 18 -0.35 12.7 19.0 13.2 13.1821 0.0138 65.84 47.13 0.0501 86.35

2 17.0 18 -0.35 11.7 18.0 13.3 6.6731 0.0138 60.64 43.40 0.0356 79.52

4 16.0 18 -0.35 10.7 17.0 13.5 3.3776 0.0138 55.43 39.68 0.0254 72.70

8 15.0 18 -0.35 9.7 16.0 13.7 1.7093 0.0138 50.23 35.95 0.0180 65.87

15 13.0 18 -0.35 7.7 14.0 14.0 0.9335 0.0138 39.82 28.50 0.0133 52.22

30 12.0 18 -0.35 6.7 13.0 14.2 0.4722 0.0138 34.61 24.78 0.0095 45.39

60 11.0 18 -0.35 5.7 12.0 14.3 0.2388 0.0138 29.41 21.05 0.0067 38.57

120 10.0 18 -0.35 4.7 11.0 14.5 0.1208 0.0138 24.20 17.32 0.0048 31.74

240 10.0 18 -0.35 4.7 11.0 14.5 0.0604 0.0138 24.20 17.32 0.0034 31.74

480 10.0 18 -0.35 4.7 11.0 14.5 0.0302 0.0138 24.20 17.32 0.0024 31.74

1440 10.0 18 -0.35 4.7 11.0 14.5 0.0101 0.0138 24.20 17.32 0.0014 31.74

2880 10.0 18 -0.35 4.7 11.0 14.5 0.0050 0.0138 24.20 17.32 0.0010 31.74

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Table C7: Grain size analysis (sieve and hydrometer) of 6% mill tailings sample at si = 20.0% (bottom layer)

Sieve# Tare Dry mass % retained Cumulative % Passing

4 92.62 92.62 0.00 0.00 0.00 100.00

10 92.62 92.62 0.00 0.00 0.00 100.00

18 92.62 92.62 0.00 0.00 0.00 100.00

40 96.84 97.41 0.57 1.03 1.03 98.97

70 106.00 120.84 14.84 26.77 27.80 72.20

100 87.48 96.63 9.15 16.51 44.31 55.69

140 116.89 123.81 6.92 12.48 56.79 43.21

200 92.69 97.57 4.88 8.80 65.60 34.40

pan 118.97 138.04 19.07

Elapsed Hydrometer Temp Ct Corr. Hyd. Hyd. Corr. only Eff. Depth

Adjusted Diameter Percentage

Time (min) Reading (C)

Reading for meniscus L (cm) L/t K % Finer % Finer (mm) of Fine

0

0.5 21.0 14 -1.35 14.7 22.0 12.7 25.3796 0.0138 76.25 26.23 0.0695 100.00

1 19.0 13 -1.60 12.4 20.0 13.0 13.0180 0.0138 64.54 22.20 0.0498 84.64

2 18.0 12 -1.85 11.2 19.0 13.2 6.5911 0.0138 58.03 19.97 0.0354 76.11

4 17.0 11 -2.10 9.9 18.0 13.3 3.3366 0.0138 51.53 17.73 0.0252 67.58

8 15.0 10 -2.35 7.7 16.0 13.7 1.7093 0.0138 39.82 13.70 0.0180 52.22

15 14.0 10 -2.35 6.7 15.0 13.8 0.9226 0.0138 34.61 11.91 0.0133 45.39

30 12.0 10 -2.35 4.7 13.0 14.2 0.4722 0.0138 24.20 8.33 0.0095 31.74

60 11.0 10 -2.35 3.7 12.0 14.3 0.2388 0.0138 19.00 6.54 0.0067 24.91

120 11.0 9 -2.60 3.4 12.0 14.3 0.1194 0.0138 17.70 6.09 0.0048 23.21

240 10.0 9 -2.60 2.4 11.0 14.5 0.0604 0.0138 12.49 4.30 0.0034 16.38

480 10.0 9 -2.60 2.4 11.0 14.5 0.0302 0.0138 12.49 4.30 0.0024 16.38

1440 10.0 9 -2.60 2.4 11.0 14.5 0.0101 0.0138 12.49 4.30 0.0014 16.38

2880 10.0 9 -2.60 2.4 11.0 14.5 0.0050 0.0138 12.49 4.30 0.0010 16.38

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Table C8: Grain size analysis (sieve and hydrometer) of 6% mill tailings sample at si = 15.2% (top layer)

Sieve# Tare Dry mass % retained Cumulative % Passing

4 92.62 92.62 0.00 0.00 0.00 100.00

10 92.62 92.62 0.00 0.00 0.00 100.00

18 92.62 92.62 0.00 0.00 0.00 100.00

40 96.86 96.86 0.00 0.00 0.00 100.00

70 106.01 106.02 0.01 0.08 0.08 99.92

100 87.52 87.56 0.04 0.31 0.39 99.61

140 116.92 116.99 0.07 0.55 0.94 99.06

200 92.69 93.13 0.44 3.45 4.39 95.61

pan 473.04 485.23 12.19

Elapsed Hydrometer Temp Ct Corr. Hyd. Hyd. Corr. only Eff. Depth

Adjusted Diameter Percentage

Time (min) Reading (C)

Reading for meniscus L (cm) L/t K % Finer % Finer (mm) of Fine

0

0.5 20.0 18 -0.35 14.7 21.0 12.9 25.7078 0.0138 76.25 72.90 0.0700 100.00

1 18.0 18 -0.35 12.7 19.0 13.2 13.1821 0.0138 65.84 62.95 0.0501 86.35

2 16.0 18 -0.35 10.7 17.0 13.5 6.7552 0.0138 55.43 53.00 0.0359 72.70

4 15.0 18 -0.35 9.7 16.0 13.7 3.4186 0.0138 50.23 48.02 0.0255 65.87

8 13.0 18 -0.35 7.7 14.0 14.0 1.7503 0.0138 39.82 38.07 0.0183 52.22

15 12.0 18 -0.35 6.7 13.0 14.2 0.9444 0.0138 34.61 33.09 0.0134 45.39

30 11.0 18 -0.35 5.7 12.0 14.3 0.4777 0.0138 29.41 28.12 0.0095 38.57

60 10.0 18 -0.35 4.7 11.0 14.5 0.2416 0.0138 24.20 23.14 0.0068 31.74

120 9.0 18 -0.35 3.7 10.0 14.7 0.1222 0.0138 19.00 18.16 0.0048 24.91

240 9.0 18 -0.35 3.7 10.0 14.7 0.0611 0.0138 19.00 18.16 0.0034 24.91

480 9.0 18 -0.35 3.7 10.0 14.7 0.0305 0.0138 19.00 18.16 0.0024 24.91

1440 9.0 18 -0.35 3.7 10.0 14.7 0.0102 0.0138 19.00 18.16 0.0014 24.91

2880 9.0 18 -0.35 3.7 10.0 14.7 0.0051 0.0138 19.00 18.16 0.0010 24.91

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Table C9: Grain size analysis (sieve and hydrometer) of 6% mill tailings sample at si = 15.2% (mid layer)

Sieve# Tare Dry mass % retained Cumulative % Passing

4 92.62 92.62 0.00 0.00 0.00 100.00

10 92.62 92.62 0.00 0.00 0.00 100.00

18 92.62 92.62 0.00 0.00 0.00 100.00

40 96.86 96.89 0.03 0.13 0.13 99.87

70 106.01 106.27 0.26 1.12 1.25 98.75

100 87.52 87.96 0.44 1.90 3.15 96.85

140 116.92 118.59 1.67 7.21 10.37 89.63

200 92.69 94.84 2.15 9.29 19.65 80.35

pan 126.42 145.02 18.60

Elapsed Hydrometer Temp Ct Corr. Hyd. Hyd. Corr. only Eff. Depth

Adjusted Diameter Percentage

Time (min) Reading (C)

Reading for meniscus L (cm) L/t K % Finer % Finer (mm) of Fine

0

0.5 21.0 18 -0.35 15.7 22.0 12.7 25.3796 0.0138 81.45 65.44 0.0695 100.00

1 19.0 18 -0.35 13.7 20.0 13.0 13.0180 0.0138 71.04 57.08 0.0498 87.22

2 18.0 18 -0.35 12.7 19.0 13.2 6.5911 0.0138 65.84 52.90 0.0354 80.83

4 17.0 18 -0.35 11.7 18.0 13.3 3.3366 0.0138 60.64 48.72 0.0252 74.44

8 15.0 18 -0.35 9.7 16.0 13.7 1.7093 0.0138 50.23 40.35 0.0180 61.66

15 14.0 18 -0.35 8.7 15.0 13.8 0.9226 0.0138 45.02 36.17 0.0133 55.27

30 12.0 18 -0.35 6.7 13.0 14.2 0.4722 0.0138 34.61 27.81 0.0095 42.49

60 11.0 18 -0.35 5.7 12.0 14.3 0.2388 0.0138 29.41 23.63 0.0067 36.10

120 10.0 18 -0.35 4.7 11.0 14.5 0.1208 0.0138 24.20 19.45 0.0048 29.71

240 10.0 18 -0.35 4.7 11.0 14.5 0.0604 0.0138 24.20 19.45 0.0034 29.71

480 10.0 18 -0.35 4.7 11.0 14.5 0.0302 0.0138 24.20 19.45 0.0024 29.71

1440 10.0 18 -0.35 4.7 11.0 14.5 0.0101 0.0138 24.20 19.45 0.0014 29.71

2880 10.0 18 -0.35 4.7 11.0 14.5 0.0050 0.0138 24.20 19.45 0.0010 29.71

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Table C10: Grain size analysis (sieve and hydrometer) of 6% mill tailings sample at si = 15.2% (bottom layer)

Sieve# Tare Dry mass % retained Cumulative % Passing

4 92.62 92.62 0.00 0.00 0.00 100.00

10 92.62 92.62 0.00 0.00 0.00 100.00

18 92.62 92.62 0.00 0.00 0.00 100.00

40 96.86 97.50 0.64 1.39 1.39 98.61

70 106.01 119.14 13.13 28.47 29.86 70.14

100 87.52 95.15 7.63 16.54 46.40 53.60

140 116.92 123.72 6.80 14.74 61.14 38.86

200 92.69 98.31 5.62 12.19 73.33 26.67

pan 119.00 131.30 12.30

Elapsed Hydrometer Temp Ct Corr. Hyd. Hyd. Corr. only Eff. Depth

Adjusted Diameter Percentage

Time (min) Reading (C)

Reading for meniscus L (cm) L/t K % Finer % Finer (mm) of Fine

0

0.5 22.0 14 -1.35 15.7 23.0 12.5 25.0514 0.0138 81.45 21.72 0.0691 100.00

1 20.0 13 -1.60 13.4 21.0 12.9 12.8539 0.0138 69.74 18.60 0.0495 85.62

2 19.0 12 -1.85 12.2 20.0 13.0 6.5090 0.0138 63.24 16.87 0.0352 77.64

4 18.0 11 -2.10 10.9 19.0 13.2 3.2955 0.0138 56.73 15.13 0.0251 69.65

8 16.0 10 -2.35 8.7 17.0 13.5 1.6888 0.0138 45.02 12.01 0.0179 55.27

15 14.0 10 -2.35 6.7 15.0 13.8 0.9226 0.0138 34.61 9.23 0.0133 42.49

30 12.0 10 -2.35 4.7 13.0 14.2 0.4722 0.0138 24.20 6.45 0.0095 29.71

60 11.0 10 -2.35 3.7 12.0 14.3 0.2388 0.0138 19.00 5.07 0.0067 23.32

120 10.0 9 -2.60 2.4 11.0 14.5 0.1208 0.0138 12.49 3.33 0.0048 15.34

240 10.0 9 -2.60 2.4 11.0 14.5 0.0604 0.0138 12.49 3.33 0.0034 15.34

480 10.0 9 -2.60 2.4 11.0 14.5 0.0302 0.0138 12.49 3.33 0.0024 15.34

1440 10.0 9 -2.60 2.4 11.0 14.5 0.0101 0.0138 12.49 3.33 0.0014 15.34

2880 10.0 9 -2.60 2.4 11.0 14.5 0.0050 0.0138 12.49 3.33 0.0010 15.34

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Table C11: Consolidation test data of 6% mill tailings sample (self-weight)

Elapsed Time (min) Interface height (cm) Solids content (%) Void Ratio

0.1 10.00 37.50 4.57

1 9.90 37.91 4.52

2 9.85 38.03 4.50

3 9.85 38.03 4.50

4 9.85 38.03 4.50

5 9.80 38.15 4.48

6 9.80 38.15 4.48

7 9.80 38.15 4.48

8 9.80 38.15 4.48

9 9.80 38.15 4.48

10 9.80 38.15 4.48

20 9.70 38.39 4.43

30 9.60 38.63 4.38

40 9.50 38.88 4.34

50 9.40 39.13 4.29

60 9.30 39.39 4.25

70 9.20 39.65 4.20

80 9.10 39.91 4.16

90 9.05 40.04 4.13

100 9.00 40.17 4.11

200 8.35 41.99 3.81

300 8.10 42.73 3.70

400 8.05 42.88 3.68

500 8.00 43.04 3.65

1000 8.00 43.04 3.65

1200 8.00 43.04 3.65

1440 8.00 43.04 3.65

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Table C12: Consolidation test data of 6% mill tailings sample (σ' = 1.08 kPa)

Elapsed Time (min) Interface height (cm) Solids content (%) Void Ratio

0.1 8.00 43.04 3.65

1 8.00 43.06 3.65

2 8.00 43.06 3.65

3 8.00 43.07 3.65

4 8.00 43.07 3.65

5 8.00 43.07 3.65

6 8.00 43.07 3.65

7 8.00 43.07 3.65

8 8.00 43.07 3.65

9 8.00 43.07 3.65

10 8.00 43.07 3.65

20 7.99 43.08 3.65

30 7.97 43.15 3.64

40 7.92 43.29 3.62

50 7.89 43.40 3.60

60 7.86 43.50 3.58

70 7.83 43.59 3.57

80 7.80 43.67 3.56

90 7.79 43.72 3.55

100 7.78 43.75 3.55

200 7.69 44.03 3.51

300 7.66 44.12 3.50

400 7.66 44.14 3.49

500 7.65 44.16 3.49

1000 7.63 44.22 3.48

1200 7.62 44.27 3.47

1440 7.55 44.48 3.44

2880 7.50 44.65 3.42

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Table C13: Consolidation test data of 6% mill tailings sample (σ' = 2.08 kPa)

Elapsed Time (min) Interface height (cm) Solids content (%) Void Ratio

0.1 74.98 7.50 44.65

1 74.97 7.50 44.66

2 74.96 7.50 44.67

3 74.96 7.50 44.67

4 74.96 7.50 44.67

5 74.96 7.50 44.67

6 74.94 7.49 44.67

7 74.92 7.49 44.68

8 74.91 7.49 44.68

9 74.89 7.49 44.69

10 74.86 7.49 44.70

20 74.65 7.47 44.77

30 74.50 7.45 44.82

40 74.40 7.44 44.85

50 74.30 7.43 44.88

60 74.25 7.42 44.90

70 74.20 7.42 44.92

80 74.17 7.42 44.93

90 74.14 7.41 44.94

100 74.13 7.41 44.94

200 74.02 7.40 44.98

300 73.99 7.40 44.99

400 73.97 7.40 45.00

500 73.95 7.40 45.00

1000 73.92 7.39 45.01

1200 73.90 7.39 45.02

1440 73.89 7.39 45.02

2880 73.84 7.38 45.04

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Table C14: Consolidation test data of 6% mill tailings sample (σ' = 4.09 kPa)

Elapsed Time (min) Interface height (cm) Solids content (%) Void Ratio

0.1 7.38 45.04 3.37

1 7.38 45.04 3.37

2 7.37 45.08 3.36

3 7.36 45.12 3.36

4 7.35 45.15 3.35

5 7.33 45.19 3.35

6 7.33 45.22 3.34

7 7.32 45.25 3.34

8 7.31 45.28 3.34

9 7.29 45.33 3.33

10 7.28 45.36 3.32

20 7.22 45.57 3.30

30 7.19 45.69 3.28

40 7.17 45.76 3.27

50 7.15 45.81 3.27

60 7.15 45.84 3.26

70 7.14 45.86 3.26

80 7.13 45.88 3.26

90 7.13 45.88 3.26

100 7.13 45.90 3.25

200 7.12 45.94 3.25

300 7.11 45.95 3.25

400 7.11 45.97 3.24

500 7.11 45.97 3.24

1000 7.11 45.97 3.24

1200 7.11 45.97 3.24

1440 7.11 45.97 3.24

2880 7.11 45.97 3.24

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Table C15: Consolidation test data of 6% mill tailings sample (σ' = 8.25 kPa)

Elapsed Time (min) Interface height (cm) Solids content (%) Void Ratio

0.1 7.11 45.97 3.24

1 7.10 46.01 3.24

2 7.09 46.05 3.23

3 7.07 46.12 3.22

4 7.06 46.15 3.22

5 7.05 46.19 3.22

6 7.05 46.21 3.21

7 7.04 46.24 3.21

8 7.03 46.26 3.21

9 7.03 46.28 3.20

10 7.03 46.27 3.20

20 6.99 46.41 3.19

30 6.97 46.49 3.18

40 6.96 46.52 3.17

50 6.95 46.56 3.17

60 6.94 46.58 3.17

70 6.94 46.59 3.16

80 6.94 46.60 3.16

90 6.93 46.61 3.16

100 6.93 46.62 3.16

200 6.92 46.68 3.15

300 6.91 46.70 3.15

400 6.91 46.72 3.15

500 6.90 46.73 3.15

1000 6.89 46.76 3.14

1200 6.89 46.78 3.14

1440 6.89 46.78 3.14

2880 6.88 46.80 3.14

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Table C16: Hydraulic conductivity test data of 6% mill tailings sample (self-weight)

Elapsed time

Sample height (cm)

a (sq.cm)

A (sq.cm)

Initial head at burette, h1 (cm)

Initial time, t1 (sec)

Final head at burette, h2 (cm)

Final time, t2 (sec)

Hydraulic Conductivity

(m/Sec)

0 8.0 1.5 78.54 - - - - -

1 8.0 1.5 78.54 51.3 0 49.6 60 8.75×10-07

2 8.0 1.5 78.54 49.6 60 48.4 120 6.24×10-07

3 8.0 1.5 78.54 48.4 120 47.4 180 4.96×10-07

4 8.0 1.5 78.54 47.4 180 46.8 240 3.60×10-07

5 8.0 1.5 78.54 46.8 240 45.9 300 4.76×10-07

6 8.0 1.5 78.54 45.9 300 45.2 360 4.10×10-07

7 8.0 1.5 78.54 45.2 360 44.5 420 3.79×10-07

8 8.0 1.5 78.54 44.5 420 43.7 480 4.62×10-07

9 8.0 1.5 78.54 43.7 480 43.0 540 4.31×10-07

10 8.0 1.5 78.54 43.0 540 42.1 600 4.99×10-07

12 8.0 1.5 78.54 42.1 600 40.6 720 4.62×10-07

14 8.0 1.5 78.54 40.6 720 39.3 840 4.25×10-07

16 8.0 1.5 78.54 39.3 840 37.9 960 4.62×10-07

18 8.0 1.5 78.54 37.9 960 36.5 1080 4.91×10-07

20 8.0 1.5 78.54 36.5 1080 35.3 1200 4.14×10-07

22 8.0 1.5 78.54 35.3 1200 34.1 1320 4.40×10-07

24 8.0 1.5 78.54 34.1 1320 32.8 1440 4.82×10-07

26 8.0 1.5 78.54 32.8 1440 31.6 1560 4.74×10-07

28 8.0 1.5 78.54 31.6 1560 30.5 1680 4.78×10-07

30 8.0 1.5 78.54 30.5 1680 29.4 1800 4.68×10-07

35 8.0 1.5 78.54 29.4 1800 26.8 2100 4.72×10-07

40 8.0 1.5 78.54 26.8 2100 24.4 2400 4.71×10-07

45 8.0 1.5 78.54 24.4 2400 22.2 2700 4.74×10-07

50 8.0 1.5 78.54 22.2 2700 20.3 3000 4.72×10-07

55 8.0 1.5 78.54 20.3 3000 18.5 3300 4.74×10-07

60 8.0 1.5 78.54 18.5 3300 16.8 3600 4.72×10-07

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Table C17: Hydraulic conductivity test data of 6% mill tailings sample (σ' = 1.08 kPa)

Elapsed time

Sample height (cm)

a (sq.cm)

A (sq.cm)

Initial head at burette, h1 (cm)

Initial time, t1 (sec)

Final head at burette, h2 (cm)

Final time, t2 (sec)

Hydraulic Conductivity

(m/Sec)

0 7.5 1.5 78.54 - - - - -

1 7.5 1.5 78.54 51.3 0 49.6 60 7.88×10-07

2 7.5 1.5 78.54 49.6 60 48.7 120 4.53×10-07

3 7.5 1.5 78.54 48.7 120 48.1 180 2.96×10-07

4 7.5 1.5 78.54 48.1 180 47.5 240 3.00×10-07

5 7.5 1.5 78.54 47.5 240 47.0 300 2.70×10-07

6 7.5 1.5 78.54 47.0 300 46.5 360 2.38×10-07

7 7.5 1.5 78.54 46.5 360 46.0 420 2.75×10-07

8 7.5 1.5 78.54 46.0 420 45.5 480 2.44×10-07

9 7.5 1.5 78.54 45.5 480 45.0 540 2.81×10-07

10 7.5 1.5 78.54 45.0 540 44.4 600 2.85×10-07

12 7.5 1.5 78.54 44.4 600 43.6 720 2.35×10-07

14 7.5 1.5 78.54 43.6 720 42.6 840 2.77×10-07

16 7.5 1.5 78.54 42.6 840 41.8 960 2.26×10-07

18 7.5 1.5 78.54 41.8 960 41.0 1080 2.31×10-07

20 7.5 1.5 78.54 41.0 1080 40.2 1200 2.35×10-07

22 7.5 1.5 78.54 40.2 1200 39.3 1320 2.60×10-07

24 7.5 1.5 78.54 39.3 1320 38.4 1440 2.87×10-07

26 7.5 1.5 78.54 38.4 1440 37.5 1560 2.73×10-07

28 7.5 1.5 78.54 37.5 1560 36.7 1680 2.57×10-07

30 7.5 1.5 78.54 36.7 1680 35.9 1800 2.74×10-07

35 7.5 1.5 78.54 35.9 1800 33.8 2100 2.79×10-07

40 7.5 1.5 78.54 33.8 2100 32.0 2400 2.71×10-07

45 7.5 1.5 78.54 32.0 2400 30.2 2700 2.71×10-07

50 7.5 1.5 78.54 30.2 2700 28.5 3000 2.71×10-07

55 7.5 1.5 78.54 28.5 3000 27.0 3300 2.70×10-07

60 7.5 1.5 78.54 27.0 3300 25.5 3600 2.73×10-07

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Table C18: Hydraulic conductivity test data of 6% mill tailings sample (σ' = 2.08 kPa)

Elapsed time

Sample height (cm)

a (sq.cm)

A (sq.cm)

Initial head at burette, h1 (cm)

Initial time, t1 (sec)

Final head at burette, h2 (cm)

Final time, t2 (sec)

Hydraulic Conductivity

(m/Sec)

0 7.4 1.5 78.54 - - - - -

1 7.4 1.5 78.54 51.2 0.0 50.5 60 3.39×10-07

2 7.4 1.5 78.54 50.5 60.0 49.9 120 2.50×10-07

3 7.4 1.5 78.54 49.9 120.0 49.5 180 2.21×10-07

4 7.4 1.5 78.54 49.5 180.0 49.1 240 1.91×10-07

5 7.4 1.5 78.54 49.1 240.0 48.6 300 2.24×10-07

6 7.4 1.5 78.54 48.6 300.0 48.2 360 1.94×10-07

7 7.4 1.5 78.54 48.2 360.0 47.9 420 1.63×10-07

8 7.4 1.5 78.54 47.9 420.0 47.5 480 1.97×10-07

9 7.4 1.5 78.54 47.5 480.0 47.0 540 2.32×10-07

10 7.4 1.5 78.54 47.0 540.0 46.6 600 2.01×10-07

12 7.4 1.5 78.54 46.6 600.0 45.9 720 1.86×10-07

14 7.4 1.5 78.54 45.9 720.0 45.1 840 2.07×10-07

16 7.4 1.5 78.54 45.1 840.0 44.5 960 1.57×10-07

18 7.4 1.5 78.54 44.5 960.0 43.8 1080 1.86×10-07

20 7.4 1.5 78.54 43.8 1080.0 43.0 1200 2.08×10-07

22 7.4 1.5 78.54 43.0 1200.0 42.3 1320 1.84×10-07

24 7.4 1.5 78.54 42.3 1320.0 41.6 1440 1.96×10-07

26 7.4 1.5 78.54 41.6 1440.0 40.9 1560 2.18×10-07

28 7.4 1.5 78.54 40.9 1560.0 40.2 1680 1.93×10-07

30 7.4 1.5 78.54 40.2 1680.0 39.5 1800 1.96×10-07

35 7.4 1.5 78.54 39.5 1800.0 38.0 2100 1.90×10-07

40 7.4 1.5 78.54 38.0 2100.0 36.5 2400 1.89×10-07

45 7.4 1.5 78.54 36.5 2400.0 35.0 2700 1.93×10-07

50 7.4 1.5 78.54 35.0 2700.0 33.6 3000 1.96×10-07

55 7.4 1.5 78.54 33.6 3000.0 32.2 3300 1.95×10-07

60 7.4 1.5 78.54 32.2 3300.0 30.9 3600 1.89×10-07

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Table C19: Hydraulic conductivity test data of 6% mill tailings sample (σ' = 4.09 kPa)

Elapsed time

Sample height (cm)

a (sq.cm)

A (sq.cm)

Initial head at burette, h1 (cm)

Initial time, t1 (sec)

Final head at burette, h2 (cm)

Final time, t2 (sec)

Hydraulic Conductivity

(m/Sec)

0 7.1 1.5 78.54 - - - - -

1 7.1 1.5 78.54 51.2 0.0 50.7 60 2.37×10-07

2 7.1 1.5 78.54 50.7 60.0 50.4 120 1.19×10-07

3 7.1 1.5 78.54 50.4 120.0 50.1 180 1.50×10-07

4 7.1 1.5 78.54 50.1 180.0 49.8 240 1.06×10-07

5 7.1 1.5 78.54 49.8 240.0 49.6 300 1.06×10-07

6 7.1 1.5 78.54 49.6 300.0 49.3 360 1.22×10-07

7 7.1 1.5 78.54 49.3 360.0 49.1 420 1.23×10-07

8 7.1 1.5 78.54 49.1 420.0 48.8 480 1.23×10-07

9 7.1 1.5 78.54 48.8 480.0 48.5 540 1.24×10-07

10 7.1 1.5 78.54 48.5 540.0 48.3 600 1.09×10-07

12 7.1 1.5 78.54 48.3 600.0 47.9 720 1.02×10-07

14 7.1 1.5 78.54 47.9 720.0 47.4 840 1.11×10-07

16 7.1 1.5 78.54 47.4 840.0 46.9 960 1.28×10-07

18 7.1 1.5 78.54 46.9 960.0 46.4 1080 1.13×10-07

20 7.1 1.5 78.54 46.4 1080.0 45.9 1200 1.31×10-07

22 7.1 1.5 78.54 45.9 1200.0 45.4 1320 1.16×10-07

24 7.1 1.5 78.54 45.4 1320.0 45.0 1440 1.00×10-07

26 7.1 1.5 78.54 45.0 1440.0 44.5 1560 1.18×10-07

28 7.1 1.5 78.54 44.5 1560.0 44.1 1680 1.11×10-07

30 7.1 1.5 78.54 44.1 1680.0 43.7 1800 1.12×10-07

35 7.1 1.5 78.54 43.7 1800.0 42.6 2100 1.12×10-07

40 7.1 1.5 78.54 42.6 2100.0 41.5 2400 1.15×10-07

45 7.1 1.5 78.54 41.5 2400.0 40.5 2700 1.10×10-07

50 7.1 1.5 78.54 40.5 2700.0 39.5 3000 1.13×10-07

55 7.1 1.5 78.54 39.5 3000.0 38.5 3300 1.16×10-07

60 7.1 1.5 78.54 38.5 3300.0 37.6 3600 1.11×10-07

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Table C20: Hydraulic conductivity test data of 6% mill tailings sample (σ' = 8.25 kPa)

Elapsed time

Sample height (cm)

a (sq.cm)

A (sq.cm)

Initial head at burette, h1 (cm)

Initial time, t1 (sec)

Final head at burette, h2 (cm)

Final time, t2 (sec)

Hydraulic Conductivity

(m/Sec)

0 6.9 1.5 78.54 - - - - -

1 6.9 1.5 78.54 51.2 0.0 50.9 60 1.43×10-07

2 6.9 1.5 78.54 50.9 60.0 50.7 120 8.63×10-08

3 6.9 1.5 78.54 50.7 120.0 50.5 180 8.66×10-08

4 6.9 1.5 78.54 50.5 180.0 50.3 240 8.70×10-08

5 6.9 1.5 78.54 50.3 240.0 50.1 300 8.73×10-08

6 6.9 1.5 78.54 50.1 300.0 49.9 360 8.77×10-08

7 6.9 1.5 78.54 49.9 360.0 49.7 420 8.80×10-08

8 6.9 1.5 78.54 49.7 420.0 49.5 480 8.84×10-08

9 6.9 1.5 78.54 49.5 480.0 49.3 540 8.87×10-08

10 6.9 1.5 78.54 49.3 540.0 49.1 600 8.91×10-08

12 6.9 1.5 78.54 49.1 600.0 48.7 720 8.96×10-08

14 6.9 1.5 78.54 48.7 720.0 48.3 840 9.04×10-08

16 6.9 1.5 78.54 48.3 840.0 47.9 960 9.11×10-08

18 6.9 1.5 78.54 47.9 960.0 47.5 1080 9.19×10-08

20 6.9 1.5 78.54 47.5 1080.0 47.1 1200 7.72×10-08

22 6.9 1.5 78.54 47.1 1200.0 46.8 1320 8.55×10-08

24 6.9 1.5 78.54 46.8 1320.0 46.4 1440 7.83×10-08

26 6.9 1.5 78.54 46.4 1440.0 46.1 1560 8.68×10-08

28 6.9 1.5 78.54 46.1 1560.0 45.7 1680 8.91×10-08

30 6.9 1.5 78.54 45.7 1680.0 45.3 1800 8.98×10-08

35 6.9 1.5 78.54 45.3 1800.0 44.4 2100 8.85×10-08

40 6.9 1.5 78.54 44.4 2100.0 43.5 2400 8.97×10-08

45 6.9 1.5 78.54 43.5 2400.0 42.6 2700 8.95×10-08

50 6.9 1.5 78.54 42.6 2700.0 41.8 3000 9.00×10-08

55 6.9 1.5 78.54 41.8 3000.0 40.9 3300 8.97×10-08

60 6.9 1.5 78.54 40.9 3300.0 40.1 3600 8.94×10-08

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APPENDIX D

Geotechnical index properties, settling test summary, and sample calculation

Table D1: Summary of index properties based on Grain Size Distribution curves (GSD

test data reported by Khaled (2012), reproduced with permission from author)

Sample 4% Mill Tailings 5% Mill Tailings 6% Mill Tailings

Gs 2.70 2.76 2.74

– 0.075 mm, % 29 49 49

– 0.002 mm, % 2 2 3

D10 (mm) 0.029 0.007 0.009

D30 (mm) 0.078 0.029 0.014

D60 (mm) 0.173 0.107 0.121

Cu = (D60/D10) 6.0 15.3 13.4

Cc = {D302/( D60 × D10)} 1.2 1.1 0.2

USCS Soil Classification SM (Silty sands) SM (Silty sands) SM (Silty sands)

Table D2: Settling test summary of 4% mill tailings from this study for si < 25% and

Khaled (2012) for si ≥ 25% (data reproduced with permission from author)

si

(%) Hi

(cm) ei Vs

(cm/s) ki

(cm/s) sf

(%) Hf

(cm) ef SP

(%) σ'f

(Pa)

15.1 8.5 15.52 239×10-3 2.3236 26.47 4.2 7.67 47.52 78.43

20.2 8.5 10.92 30×10-3 1.6766 29.63 5.1 6.55 36.66 109.28

26 8.5 7.86 7×10-3 0.0365 32.16 6.3 5.82 23.02 149.48

30.3 8.5 6.35 4×10-3 0.0173 34.55 7 5.23 15.24 181.91

35.9 8.5 4.93 3×10-3 0.0105 38.5 7.6 4.41 8.77 227.55

40 8.5 4.14 2×10-3 0.006 42.08 7.8 3.8 6.61 263.08

Table D3: Settling test summary of 5% mill tailings from this study for si < 25% and

Khaled (2012) for si ≥ 25% (data reproduced with permission from author)

si

(%) Hi

(cm) ei

Vs

(cm/s2) ki

(cm/s) sf

(%) Hf

(cm) ef

SP (%)

σ'f (Pa)

15.2 8.5 15.52 222×10-3 2.1583 31.75 3.25 5.93 58.05 75.87

20.4 8.5 10.92 155×10-3 1.0873 32.8 4.4 5.65 44.21 107.02

25 8.5 8.28 115×10-3 0.6079 35.71 5.1 4.97 35.67 115.97

30.1 8.5 6.41 18.5×10-3 0.0779 40.4 5.4 4.07 31.58 172.34

36.1 8.5 4.89 8.5×10-3 0.0284 42.87 6.4 3.68 20.54 221.43

41.8 8.5 3.84 5.6×10-3 0.0154 46.58 7 3.16 14.05 272.06

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Table D4: Settling test summary of 6% mill tailings from this study for si < 25% and

Khaled (2012) for si ≥ 25% (data reproduced with permission from author)

si

(%) Hi

(cm) ei

Vs

(cm/s2) ki

(cm/s) sf

(%) Hf

(cm) ef

SP (%)

σ'f (Pa)

15.2 8.5 15.4 241×10-3 2.3260 30.33 3.5 6.34 55.24 77.18

20 8.5 11.04 219×10-3 1.5517 34.14 4.1 5.33 47.43 104.92

25.5 8.5 8.01 85×10-3 0.4401 36.78 5 4.71 36.63 141.77

30 8.5 6.39 19×10-3 0.0807 38.58 5.8 4.36 27.47 175.07

35.1 8.5 5.07 11×10-3 0.0384 41.8 6.4 3.81 20.76 214.87

40.1 8.5 4.09 6×10-3 0.0175 44.49 7.1 3.42 13.16 260.08

Table D5: Layer-wise grain size distribution test summary of 4% mill tailings from this

study for si < 25% and data analyzed after Khaled (2012) for si ≥ 25%

si

(%) Layer

Average solids content savg (%)

Fines content f (%)

Normalized solids content deviation sd (%)

15.1

Top 19.871 60.260 -2.819

Middle 28.745 49.309 0.140

Bottom 36.364 37.176 2.679

20.2

Top 22.909 51.406 -2.181

Middle 30.130 46.230 0.226

Bottom 35.317 42.716 1.955

26

Top 30.457 43.367 -1.460

Middle 35.375 40.110 0.179

Bottom 38.680 36.728 1.281

30.3

Top 32.814 40.130 -0.990

Middle 36.620 37.580 0.278

Bottom 37.919 38.667 0.712

35.9

Top 36.927 41.768 -0.606

Middle 38.985 42.550 0.080

Bottom 40.320 41.908 0.525

40.0

Top 40.208 37.097 -0.313

Middle 40.987 37.511 -0.054

Bottom 42.248 35.949 0.367

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Table D6: Layer-wise grain size distribution test summary of 5% mill tailings from this

study for si < 25% and data analyzed after Khaled (2012) for si ≥ 25%

si

(%) Layer

Average solids content savg (%)

Fines content f (%)

Normalized solids content deviation sd (%)

15.2

Top 15.418 95.038 -6.010

Middle 24.985 85.024 -2.819

Bottom 59.907 27.254 8.829

20.4

Top 19.572 83.960 -5.620

Middle 32.792 62.504 -1.213

Bottom 56.928 23.599 6.832

25.0

Top 19.477 88.676 -5.680

Middle 39.257 56.840 0.913

Bottom 50.820 34.630 4.767

30.1

Top 35.499 55.562 -1.980

Middle 42.138 54.446 0.233

Bottom 46.681 49.144 1.747

36.1

Top 39.925 52.350 -1.790

Middle 45.620 50.120 0.110

Bottom 50.325 44.013 1.680

41.8

Top 46.070 51.160 -0.910

Middle 49.320 49.220 0.170

Bottom 50.960 47.970 0.730

Table D7: Layer-wise grain size distribution test summary of 6% mill tailings from this

study for si < 25% and data analyzed after Khaled (2012) for si ≥ 25%

si

(%) Layer

Average solids content savg (%)

Fines content f (%)

Normalized solids content deviation sd (%)

15.2 Top 18.099 95.608 -4.983

Middle 27.364 80.346 -1.895 Bottom 53.680 26.670 6.877

20.0 Top 19.613 95.144 -4.832

Middle 32.013 71.583 -0.699 Bottom 50.704 34.404 5.531

25.5 Top 24.499 53.800 -4.856

Middle 41.493 49.980 0.829 Bottom 50.994 44.660 4.017

30.0 Top 35.499 53.762 -1.854

Middle 42.138 51.134 0.242 Bottom 46.681 48.281 1.808

35.1 Top 38.754 54.274 -1.317

Middle 43.791 52.432 0.362 Bottom 45.571 45.859 0.955

40.1 Top 42.483 51.157 -0.817

Middle 45.440 49.215 0.169 Bottom 46.880 50.180 0.648

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Figure D1: Grain size distribution curves of 4%, 5% and 6% mill tailings (GSD test data

reported by Khaled (2012), reproduced with permission from the author)

0.0001 0.001 0.01 0.1 1Grain Size (mm)

0

20

40

60

80

100

Per

cen

t F

iner

(%

)

Best Fit: 4% Mill Tailings (This Study)

Best Fit: 5% Mill Tailings (This Study)

Best Fit: 6% Mill Tailings (This Study)

4% Mill Tailings Data (Khaled, 2012)

5% Mill Tailings Data (Khaled, 2012)

6% Mill Tailings Data (Khaled, 2012)

Clay Size (< 0.002 mm) Silt Size Sand Size (>0.075 mm)

r2 = 0.994

r2 = 0.996

r2 = 0.996

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Figure D2: Determination of initial hydraulic conductivity from settling test (data

reported by Khaled (2012), reproduced with permission from the author)

0

3

6

9

Inte

rfac

e H

eigh

t (c

m)

5 % Mill TailingsThis Study

si = 15.2%

si = 20.4%

Khaled (2012)

si = 25.0 %

si = 30.1 %

si = 36.1 %

si = 41.8 %

0 100 200 300 400 500Elapsed Time (min)

0

3

6

9

Inte

rfac

e H

eigh

t (c

m)

6 % Mill TailingsThis Study

15.2%

20.0%

Khaled (2012)

25.5 %

30.0 %

35.1 %

40.1 %

0

3

6

9

Inte

rfac

e H

eigh

t (c

m)

4 % Mill TailingsThis Study

si = 15.1%

si = 20.2%

Khaled (2012)

si = 26.0 %

si = 30.3 %

si = 35.9 %

si = 40.0 %

3/9

3/9

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Table D8: Initial conditions of sample for consolidation tests

Parameters 4% mill tailings 5% mill tailings 6% mill tailings

Water content, w (%) 213.50 164.60 166.70 Void ratio, e 5.75 4.54 4.57 Specific gravity, Gs 2.70 2.76 2.74 Degree of saturation, DS (%) 100 100 100 D9: Sample calculation of consolidation loading for 4% mill tailings

Initial water content, w = 213.50%

Initial solids content, s = (1/1+w) = 31.94%

Specific gravity, Gs = 2.70

Diameter (D) of the sample = 10 cm Height (h) of the sample = 10 cm Area of sample, A = 1/4 (πD2) = 78.54 Sq.cm Volume of sample, V = A h = 785.40 cc Initial solids content, s = 31.94%

Initial weight of slurry, W = 983.09 gm Initial weight of solids Ws = s × W 313.61 gm Initial weight of water Ww = W-Ws 669.49 gm

Unit weight of water, γw = 1 gm/cc Initial unit weight of slurry, γ = W/V 1.25 gm/cc Void ratio, e = {(1+w) Gsγw / γ}- 1 = 5.75

Stress of 1 kPa, σ = 1 kPa Equivalent load required, P = σ / A 7.85 Newton (a) Required mass, m =(P/g) = 0.80 kg g = 9.81; acceleration due to gravity 800.6 gm

Sample height after self weight settling, h1 = 8.4 cm Solids content, s = 36.4% Void ratio, e = 4.83 Unit weight, γ = γw {(Gs+e) / (1+e)} 1.29 gm/cc Effective unit weight, γ' = γ - γw = 0.29 gm/cc Effective unit weight, γ' = 2.86 N per cubic metre

(1) Effective stress after settling, σ' = (γ - γw) h1 0.24 kPa

Load 1: 1 kPa

(2) Loading piston and plastic container = 367 gm (3) Porous stone = 114 gm Equivalent applied stress with self weight (1+2+3) = 0.84 kPa

Additional weight for 1 kPa = (1 - 0.84) × (a) 128 gm