American Environmental ~~ Testing .. . Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (818) 845-8200 Fax: (818) 845-8840 www.aetlab.com
Ordered By
Number of Pages 13 - Suite 370 Date Received 08/01/2006
Date Reported 08/04/2006
Telephone: (714) 985-3434 Job Number Order Date Client
Attention: Tom Tatnall 38375 1 08/01/2006 1 H &A
Project ID: 32486-007 Project Name: Delphi System Corp.
Site : 1201 N. Magnolia Avenue Anaheim, CA 92801
Enclosed please find results of analyses of 1 water and 11 solid waste samples which were analyzed as specified on the attached chain of custody. If there are any questions, please do not hesitate to call.
Checked By: PA . .-
Approved By:
Cyrus Razmara, Ph. D. Laboratory Director
American Environmental Testing Laboratory Inc. 2834 & 2908 North Naomi Street, Burbank, CA 9 1504 DOHS NO: 1541, LACSD NO: 10181 Tel: (888) 288-AETL (818) 845-8200 Fax: (818) 845-8840 www.aet1ab.com
CHAIN OF CUSTODY RECORD NO 427'09
TABLE Summary of Aqueous Analytical Results for Polychlorinated Biphenyls (PCBs) by GC
1201 N. Magnolia Avenue Anaheim, CA 92801
Polychlorinated Biphenyls (PCBs) by GC. Method: 8082
Sample Date
Laboratory Job Number
Aroclor-1016 (PCB-1016) ug/L
Aroclor-1221 (PCB-1 221 ) ug/L
Aroclor-1232 (PCB-1 232) uglL
Aroclor-1242 (PCB-1 242) ug/L
Aroclor-I 248 (PCB-1 248) ug1L
Aroclor-I254 (PCB-1254) uglL
Aroclor-1260 (PCB-1260) uglL
Aroclor-I 262 (PCB-1262) uglL
Aroclor-1268 (PCB-1 268) ug/L
1) "ND<Xn INDICATES CONSTITUENT(S) NOT DETECTED AT OR ABOVE METHOD DETECTION LIMIT.
2) "J" INDICATES ANALYTE WAS DETECTED. HOWEVER, ANALYTE CONCENTRATION IS AN ESTIMATED VALUE WHICH IS BETWEEN
THE METHOD DETECTION LIMIT (MDL) AND THE PRACTICAL QUANTITATION LIMIT(PQL).
3) "D" INDICATES THE SAMPLE WAS DILUTED TO BRING THE ANALYTE CONCENTRATION WITHIN CALIBRATION RANGE.
File: AQ-8082.~1~
TABLE Summary of Solid Waste Analytical Results for Polychlorinated Biphenyls (PCBs) by GC
1201 N. Magnolia Avenue Anaheim, CA 92801
Polychlorinated Biphenyls (PCBs) by GC. Method: (8082)
Sample Date
Laboratory Job Number
Aroclor-1016 (PCB-1 01 6) udKg
Aroclor-1221 (PCB-1 221) uglKg
Aroclor-1232 (PCB-1 232) uglKg
Aroclor-1242 (PCB-1 242) %\Kg
Aroclor-I 248 (PCB-1 248) uglKg
Aroclor-1254 (PCB-1254) udKg
Aroclor-I 260 (PCB-1260) udKg
Aroclor-I 262 (PCB-1 262) usn<S
Aroclor-I 268 (PCB-1268) udKg
1) "ND<X" INDICATES CONSTITUENT(S) NOT DETECTED AT OR ABOVE METHOD DETECTION LIMIT.
2) "J" INDICATES ANALYTE WAS DETECTED. HOWEVER, ANALYTE CONCENTRATION IS AN ESTIMATED VALUE WHICH IS BETWEEN
THE METHOD DETECTION LIMIT (MDL) AND THE PRACTICAL QUANTITATION LIMIT(PQL).
3) "D" INDICATES THE SAMPLE WAS DILUTED TO BRING THE ANALYTE CONCENTRATION WITHIN CALIBRATION RANGE.
File: SW-8082.~1~
American Environmental Testing Laboratory Inc. 2834 & 2908 North Naomi Street, Burbank, CA 9 1504 DOHS NO: 1541, LACSD NO: 10181 Tel: (888) 288-AETL (8 18) 845-8200 Fax: (81 8 ) 845-8840 www.aetlab.com
ANALYTICAL RESULTS
Ordered By --
/ Haley & Aldrich 7 ; 500 South Kraemer Blvd. i
1 g:, z 1 9 2 8 2 1-6723
Site
Anaheim, CA 92801
Telephone: (714)985-3434 Attn: Tom Tatnall
Pane: 2
Method: (8082), Polychlorinated Biphenyls (PCBs) by GC QC Batch No: 080206
"
Clienq -- H&A , -- L
Project ID: 32486-007 Project Name: Delphi System Corp .
/ Our Lab I.D. Client Sample I.D.
Date Sampled
1 Matrix 1 1 Solid Waste / Solid Waste Solid Waste Solid Waste I Solid Waste 1
AETL Job Number 38375
MethodBlank
08/01/2006 08/01/2006 ~08/01/2006 /08/01/2006
Submitted 0 8 / 0 1 / 2 0 0 6
Date Pre~ared 08/02/2006 108/02/2006 08/02/2006 08/02/2006 /08/02/2006
3 5 5 0 ~ 1 3 5 5 0 ~ Preparation Method
38375.0% CSO257-CC-0
oo-ol
3 5 5 0 ~
Date Analvzed
Units Dilution Factor Analy te s MDL
Aroclor-1232 (PCB-1232) Aroclor-1242 (PCB-1242) Aroclor- 1248 (PCB- 1248) Aroclor- 1254 (PCB- 1254) Aroclor-1260 (PCB-1260) Aroclor- 1262 (PCB-1262)
Aroclor- 1268 (PCB- 1268)
38375.02 CSO258-CC-0
00-01
08/02/2006 /08/02/2006 08/02/2006 08/02/2006 08/02/2006
PQL
50.0
50.0
Aroclor- 10 16 (PCB- 10 16)
Our Lab I.D. Surrogate s I%~ec.~imit
38375.03 / 38375.04 CSO259-CC-01 CSO260-CC-0
oo-ol I o ~ - ~ l i
3 5 5 0 ~
25.0
25.0
25.0
25.0
25.0
25.0
25.0
25.0
3 5 5 0 ~
1 R e s u l t s
ND
ND Aroclor- 122 1 (PCB- 122 1) 1 25.0
% R e c .
50.0
50.0
50.0
50.0
50.0
50.0
50.0
1 R e s u l t s
ND
ND
38375.01 % R e c .
ND
ND
ND
ND
ND
ND
ND
% K g 1
R e s u l t s ND
ND
38375.02 1 38375.03 % R e c . 1 % R e c .
ND
ND
12 9
ND
ND
ND
ND
38375.04 1 % R e c . 1
ugKg 1
R e s u l t s ND
ND
@Kg 1
Results
ND
ND
ND
ND
ND
ND
ND
ND
ND
I N D ND I ND
288
ND
ND
ND
ND
, 64.0
ND
ND
m i ND i
American Environmental Testing Laboratory Inc. 2834 & 2908 North Naomi Street, Burbank, CA 91504 -DOHS NO: 1541, LACSDNO: 10181 Tel: (888) 288-AETL (8 18) 845-8200 Fax: (8 18) 845-8840 www.aetlab.com
ANALYTICAL RESULTS
O r d e r e d By Haiey & Aldrich 500 South Kraemer Blvd. Suite 370
i Brea, CA 9282 1-6723
S i t e
Anaheim, CA 9280 1
Telephone: (714)985-3434 Attn : Tom Tatnall
Paae: 3
Method : (8082), Polychlorinated Biphenyls (PCBs) by GC QC Batch No: 080206
L,
Project ID: 32486-007 Project Name: Delphi System Corp .
Our Lab I.D. Client Sample I.D.
Date Sampled Date Pre~ared
1 Matrix 1 I Solid Waste Solid Waste / I 1 1
- Client 1
- - H&A 1
AETL Job Number 38375
38375.05 CSO261-CC-0
00-01
1 ~ r e ~ a r a t i b n Method 3 5 5 0 ~ 3 5 5 0 ~
Submitted 0 8 / 0 1 / 2 0 0 6
08/02/2006
I Date Analyzed
38375.06 CSO262-CC-0
00-01 08/01/200608/01/2006
08/02/2006
108/02/2006 08/02/2006
Dilution Factor Analytes MDL
Aroclor- 10 16 (PCB- 10 16) 1 25.0
Aroclor-122 1 (PCB-122 1) 1 25.0
1
I I
Aroclor-1232 (PCB-1232)
Aroclor- 1242 (PCB- 1242)
Aroclor-1248 (PCB-1248)
1 Aroclor-1268 (PCB- 1268) I -- ~
PQL
50.0
50.0
Aroclor- 1254 (PCB- 1254)
Aroclor- 1260 (PCB- 1260)
Aroclor-1262 (PCB-1262)
25.0
25.0
25.0
1 Results
ND
ND
25.0
25.0
25.0
/Our Lab I.D. /Surrogates ]%~ec.~imib
1 Results
ND
ND
50.0
50.0
50.0
50.0
50.0
50.0
38375.05 % Rec.
ND
ND
28.3J
38375.06 % Rec.
ND
ND
ND
ND
ND
ND
ND
ND
ND
O r d e r e d By [%ley& Aldrich 500 South Kraemer Blvd. Suite 370 Brea. CA 9282 1-6723
American Environmental Testing Laboratory Inc. -- - -- - - - - - . ppp
2834 & 2908 North Naomi Street, Burbank, CA 91504 DOHS NO: 1541, LACSDNO: 10181 Tel: (888) 288-AETL (818) 845-8200 Fax: (818) 845-8840 www.aetlab.com
ANALYTICAL RESULTS
S i t e --
120 1 N. Magnolia Avenue Anaheim, CA 9280 1
Telephone: (7 14)985-3434 Attn: Tom Tatnall
Method: (8082), Polychlorinated Biphenyls (PCBs) by GC QC Batch No: 080306
Page: 4
/ Method ~lankl 38375.07 / 1 / o u r Lab I.D. I
1 Client Sample I.D.
Client H &A
Project ID: 32486-007 Project Name: Delphi S y s t e m Corp.
AETZ Job Number 38375
- Submitted 08/01/2006
Anal ytes MDL
1 Aroclor- 1242 (PCB- 1242)
/ Aroclor-1248 (PCB-1248)
Aroclor-1254 (PCB-1254)
PQL
50.0
50.0
50.0
Aroclor- 10 16 (PCB- 10 16) Aroclor- 1221 (PCB-1221)
Aroclor- 1232 (PCB-1232)
25.0
25.0
25.0
25.0
25.0
25.0
---
1
Results
ND
ND
ND
-- Our Lab I.D.
50.0
50.0
50.0
% Rec.
94
Surrogates
Results
ND
ND
ND
%Rec.Limit
I
I
ND
ND
ND
38375.07 % Rec.
98 Tetrachloro-m-xylene 1 30-150 /
--
ND
286
ND 1
American Environmental Testing Laboratory Inc. --- - - - -- .- - --
2834 & 2908 North Naomi Street, Burbank, CA 9 1504 DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (8 18) 845-8200 Fax: (8 18) 845-8840 www.aetlab.com
ANALYTICAL RESULTS
Ordered By Ull.7 & Aldrith 500 South Kraemer Blvd. Suite 370 Brea, CA 9282 1-6723
Telephone: (714)985-3434 Attn: Tom Tatnall
Page: 5 Project ID: 32486-007 Project Name: Delphi Sys tem Corp .
Site
1201 N. Magnolia Avenue Anaheim, CA 9280 1
/ AETL Job Number / Submitted I ~1Kt-1
Method: (8082), Polychlorinated Biphenyls (PCBs) by GC QC Batch No: 080206
--
Our Lab I.D. Client Sample I.D.
I
Date Sampled Date Prepared Pre~aration Method
Matrix 1 1 Solid Waste / Solid Waste I Solid Waste Solid Waste / I
38375.11 CSO267-CC-0
I I 1 I
1 Units 1 I ugKg / u d K g / ugKg ugfKg 1 1
I
I
38375.08 CSO264-CC-0
08/02/2006
3550B
Date Analyzed
I Dilution Factor 1 / 1 1 1 1 1 / 1 / ~ n a l ~ t e s MDL PQL ( Results I Results I Results 1 Results / I
I
I 00-0 1
108/02/2006 /08/02/2006 j08/02/2006 /08/02/2006 1
38375.09 CSO26.5-CC-0
08 /0 l /200608/0 l /2006
08/02/2006
3550B
- 38375.10
CSO266-CC-0
00-01
/ rocl lor- 10 16 (PCB- 10 16)
00-01 1 00-01 08/01/2006
08/02/2006
3550B
/ Aroclor-1232 (PCB-1232)
Aroclor- 1242 (PCB- 1242)
Aroclor-1248 (PCB-1248)
1 Aroclor- 1268 (PCB-1268) / 25.0 50.0 I ND ND ND 1 ND 1 1
25.0
/ Aroclor-1254 (PCB-1254)
1 Aroclor- 1260 (PCB- 1260) 25.0 50.0 ND ND ND ND
08/01/2006
08/02/2006
3550B
ND
25.0
25.0
25.0
Aroclor- 1262 (PCB-1262)
I I I
I
50.0
ND
Our Lab I.D. Surrogates I%~ec.~imib
1 Aroclor- 122 1 (PCB-1 22 1) 1 25.0 1 50.0 ND ND
50.0
50.0
50.0
25.0
ND
1 38375.08 1 %Rec.
ND
ND
36.95
50.0
ND
38375.09 1 38375.10 %Rec. / % R e c .
ND
ND
32.05
ND
38375.11 1 %Rec. 1
ND
ND
ND
44 .6J
ND
ND
ND
ND
475
I
ND ND
American .. -. . . Environmental - - Testing Laboratory Inc. .......--pp..-p--.- ~p
2834 8~2908 North Naomi Street, Burbank. CA 91 504 *DOHS NO: 1541, LACSD NO: 10181 T e l : (888) 288-AETL (818) 845-8200 Fax: (818) 845-8840 www.aetlab.com
- ANALYTICAL RESULTS
Ordered By
500 South Kraemer Blvd. Suite 370
Telephone: (714) 985-3434 Attn : Tom Tatnall
Page 6 Project ID: 32486-007 Project Name: Delphi System Corp.
S i t e
120 1 N. Magnolia Avenue Anaheim, CA 9280 1
AETL Job Number 1 Submitted / Client
38375 1 08/01/2006 / H&A
- - , " "
Analytes Arsenic ' , I 1"" " ' . . I
tr.
Methods of Analvses 1 1601 OBSCAN)
Date Prepared Date Analyzed
\ - - - - - - z
08/02/2006
08/02/2006 Matrix QC Batch Number
- - Lab ID I Sample ID Sampled
- - Results
Method Detection Limit Practical Quantitation Limit
, Dilution Factor
Units i mg/Kg
Solid Waste
080206-1
- - 0.5
5.0
1
--
I
38375.11 1~~0267-CC-000-01
N/AI Method Blank .--,
08/01/2006
l I -.
3.905
ND .. -
American Environmental - Testing Laboratory -- -- Inc. 2834 & 2908 North Naomi Street, Burbank, CA 9 1504 DOHS NO. 1541, LACSD NO: 10181 Tel: (888) 288-AETL (8 18) 845-8200 Fax: (81 8) 845-8840 www.aetlab.com
ANALYTICAL RESULTS O r d e r e d By
Haley & Aldrich 500 South Kraemer Blvd. Suite 370
Telephone: (714)985-3434 Attn: Tom Tatnall
Page: 7
Project ID: 32486-007 Project Name: Delphi System Corp
S i t e
Anaheim, CA 92801
AETL Job Number 1 Submitted 1 Client 38375 1 0 8 / 0 1 / 2 0 0 6 1 H&A
Method: 8082, Polychlorinated Biphenyls (PCBs) by GC - - -
QC Batch No: 080206
Our Lab I.D. Method Blank 38375.12 Client Sample I.D. EB-080106
Date Sampled 08/01/2006
Date Prepared 08/02/2006 08/02/2006
Preparation Method 3510~ 3 5 1 0 ~
Date Analyzed 08/04/2006 08/04/2006
Matrix Units Dilution Factor
Aroclor-1232 (PCB-1232) 1 1.0
Aroclor- 1242 (PCB- 12421 1.0
PQL 5.0
10.0
Analytes
Aroclor- 10 16 (PCB- 10 16)
Aroclor-122 1 (PCB-1221)
MDL 1.0
2.0
5.0
5.0
Aroclor- 1248 (PCB- 1248) 1 1.0
I Aroclor- 1262 (PCB- 1262)
Aroclor- 1268 (PCB- 1268) - -- -. -- ---
Aqueous
ug/L 1
Results
ND
ND
5.0
5.0
5.0
Aroclor-1254 (PCB-1254)
Aqueous
ug/L 1
Results
ND
ND
ND
ND
1.0
1.0
1.0
ND
ND
ND
ND
ND Aroclor- 1260 (PCB- 1260) 1 1.0
ND
ND
ND
5.0
5.0
Our Lab I.D. Method Blank % Rec.
108
Surrogates
I Tetrachloro-m-xylene --
ND
ND
38375.12 % Rec,
9 1
% R e c .Limit
30-150
ND
ND - -
American Environmental Testing Laboratory Inc. -- - - -- - - --
2834 & 2908 North N a o m ~ Street, Burbank, CA 9 1504 DOHS NO. 1541, LACSD NO. 10181 Tel. (888) 288-AETL (818) 845-8200 Fax (818) 845-8840 www.aetlab.com
ANALYTICAL RESULTS
S i t e
120 1 N. Magnolia Avenue Anaheim, CA 92 80 1
--
T e l e p h o n e : (714) 985-3434 A t t n : Tom T a t n a l l
P a g e 8 C l i e n t
H &A P r o j e c t I D : 32486-007
P r o j e c t Name: Delphi S y s t e m Corp.
AETL Job Number 3 8 3 7 5
S u b m i t t e d - 0 8 / 0 1 / 2 0 0 6
American -- Environmental -- - Testing -- Laboratory Inc. 2834 &2908 North N a o m ~ Street, Burbank, CA 91504 DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (818) 845-8200 Fax: (818) 845-8840 www.aetlab.com
ANALYTICAL RESULTS
Ordered By k a F & Aldrich / 500 South Kraemer Blvd. ! Suite 370 I Brea, CA 9282 1-6723
S i t e
Magnolia Avenue Anaheim, CA 9280 1
Telephone: (714)985-3434 Attn: Tom Tatnall
QUALITY CONTROL REPORT
Page: 9
QC Batch No: 080106 Sample Spiked: 38354.08 QC Prepared: 08/01/2006 QC Analyzed: 08/01/2006 Units: mglL
- --- -- .- -
/ Sample I MS I MS 1 MS 1 MS DUP MS DUP / MS DUP RPD 1 M S I M ~ ~
Client -.
H &A Project ID: 32486-007 ProjectName: Delphi S y s t e m Corp.
Method: 60 1 OBSCAN, Total Arsenic
QC Batch No: 080106 Sample Spiked: 38354.08 QC Prepared: 08/01/2006 QC Analyzed: 08/01/2006 Units: mglL
aETL Job Number 38375
-
Analytes
I Arsenic
Submitted 08/01/2006
Result
0.007
Concen
1.00
-- --
LCSILCSD
% Limit Analytes
I
Recov
0 .91
I
LCS
Concen
80-120 -
Arsenic - - - - - -
% REC
90
LCS
Recov
1.00
LCS
% REC
Concen
1.00
0.85
Recov
0.92
85
% REC
91
%
1.1
% Limit
80-120
% Limit
(15 /
American Environmental Testing Laboratory Inc. - -. .. .-
2834 &2908 North Naomi Street, Burbank, CA 91 504 DOHS NO: 1541, LACSD NO: 10181 Tel: (888) 288-AETL (818) 845-8200 Fax: (818) 845-8840 www.aetlab.com
ANALYTICAL RESULTS
Ordered B y -.
Haley & Aldrich 500 South Kraemer Blvd. Suite 370 Brea. CA 92821-6723
Site
120 1 N. Mkgnolia Avenue Anaheim, CA 92801
Telephone: (714)985-3434 Attn: Tom Tatnall
Method: 8082, Polychlorinated Biphenyls (PCBs) by GC QUALITY CONTROL REPORT
Page: 10
QC Batch No: 080206 Sample Spiked: 080206 QC Prepared: 08/02/2006 QC Analyzed: 08/04/2006 Units: uglL
Project ID: 32486-007 Project Name: Delphi S y s t e m Corp.
I 1 Sample MS 1 MS MS 1 MS DUP 1 MS DUP MS DUP RPD MSIMSD MS RPD 1
QC Batch No: 080206 Sample Spiked: 080206 QC Prepared: 08/02/2006 QC Analyzed: 08/04/2006 Units: uglL
C l i e n t ; H&A i
AETL Job Number 38375
Analytes
Aroclor- 1260 (PCB- 1260) -- -
Submitted 08 /01 /2006
Analytes / Concen Recov % REC 1 % Limit I 1 1 I I 1 !
Result
0 . 0
1
Concen
2.50
LCSILCSD T L C S 1 LCS I
! I I I I I I i I I 1
LCS
I Aroclor-1260 (PCB- 1260) --
Recov
2 .53
2.50 --
% REC
101
2.03
Concen
2.50
81
Recov
2 .70
75-125
% REC
108
%
6 . 7
% Limit
75-125
% Limit
<20
American Environmental Testing Laboratory Inc. -- - - - p~
2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (8 18) 845-8200 Fax: (818) 845-8840 www.aetlab.com
ANALYTICAL RESULTS
O r d e r e d By paley & Aldrich 500 South Kraemer Blvd. Suite 370 Brea. CA 9282 1-6723
S i t e -
1201 N. Magnolia Avenue Anaheim, CA 9280 1
Telephone: (7 14)985-3434 Attn: Tom Tatnall
QC Batch No: 080206-1 Sample Spiked: 38375.01 QC Prepared: 08/02/2006 QC Analyzed: 08/02/2006 Units: mglKg
Page: 11
QC Batch No: 080206-1 Sample Spiked: 38375.01 QC Prepared: 08/02/2006 QC Analyzed: 08/02/2006 Units: mglKg
client-- H &A
--
Project ID: 32486-007 Project Name: Delphi System Corp.
Analytes
Arsenic
Method: (60 1 OBSCAN), Arsenic by ICP QUALITY CONTROL REPORT
AETL Job ~ilmber 38375
Sample
Result
0.062
7 Analytes
Arsenic
-submitted 08/01/2006
MS
Concen
1.00
LCS
Concen
1.00
MS
Recov
1.07
LCS
Recov
1.01
MS
% REC
101
LCS
% REC
101
LCSILCSD
% Limit
80-120
MS DUP
Concen
1.00
MS DUP
Recov
1.06
MSDUP
% REC
100
RPD
%
<1
MSIMSD
% Limit
80-120
MS RPD
% Limit
<15
2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (8 18) 845-8200 Fax: (8 18) 845-8840 www.aetlab.com
ANALYTICAL RESULTS
O r d e r e d B y
500 South Kraemer Blvd.
Brea. CA 9282 1-6723
S i t e
Anaheim, CA 9280 1
Telephone: (714)985-3434 Attn: Tom Tatnall
Method: (8082), Polychlorinated Biphenyls (PCBs) by GC QUALITY CONTROL REPORT
Page: 12
QC Batch No: 080206 Sample Spiked: 080206 QC Prepared: 08/02/2006 QC Analyzed: 08/02/2006 Units: uglKg
I I Sample MS / MS MS MS DUP 1 MS DUP MS DUP 1 RPD MSlMSD 1 MS RPD 1
Submitted 1 Client
08/01/2006 L-_ H&A , Project ID: 32486-007 Project Name: Delphi S y s t e m Corp.
- AETL J O ~ Number
38375
QC Batch No: 080206 Sample Spiked: 080206 QC Prepared: 08/02/2006 QC Analyzed: 08/02/2006 Units: ug/Kg
Analytes / Result Concen
500.00 Aroclor-1260 (PCB-1260) - -.
0.0
--
1
Recov
440.00
I
LCSILCSD
% Limit
50-150
Analytes
Aroclor- 1260 (PCB-1260)
% REC
88
LCS
Concen
500.00
Concen
500.00
LCS
Recov
495.00
Recov
500.00
LCS
% REC
99
% REC
100
%
12.8
% Limit
50-150
% Limit
<50
Ordered Bv
American Environmental --- - Testing -- Laboratory Inc. 2834 8~2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (8 18) 845-8200 Fax: (8 18) 845-8840 www.aetlab.com
ANALYTICAL RESULTS
I Haley & Aldrich 1 500 South Kraemer Blvd. Suite 370
Telephone: (714)985-3434 Attn: Tom Tatnall
S i t e
120 1 N. Magnolia Avenue Anaheim, CA 9280 1 1
Method: (8082), Polychlorinated Biphenyls (PCBs) by GC
Page: 13
QUALITY CONTROL REPORT
QC Batch No: 080306 Sample Spiked: 080306 QC Prepared: 08/03/2006 QC Analyzed: 08/03/2006 Units: uglKg
Client - 1 H&A 1 '
Submitted 08/01/2006
Project ID: 32486-007 Project Name: Delphi System Corp.
QC Batch No: 080306 Sample Spiked: 080306 QC Prepared: 08/03/2006 QC Analyzed: 08/03/2006 Units: uglKg
AETL Job Number 38375
Analytes
Aroclor- 1260 (PCB- 1260) - --
I
I 1 Analytes
LCS LCS LCS LCSILCSD
Concen Recov % REC % Limit
Sample
Result
0.0
MS
Concen
500.00
MS
Recov
450.00
MS
% REC
90
MS DUP
Concen
500.00
MS DUP
Recov
520.00
MSDUP
% REC
104
RPD
%
14.4
MSIMSD
% Limit
50-150
MS RPD
% Limit
<50 , _--A
American - Environmental Testing - Laboratory Inc. 2834 & 2908 North Naomi Street, Burbank, CA 9 1504 -DOHS NO: 1541, LACSD NO. 10181 Tel: (888) 288-AETL (818) 845-8200 Fax: (818) 845-8840 www.aetlab.com
Data Qualifiers and Descriptors
Data Qualifier:
*. In the QC section, sample results have been taken directly from the ICP reading. No preparation factor has been applied.
Analyte was present in the Method Blank.
Result is from a diluted analysis.
Result is beyond calibration limits and is estimated.
Analysis was performed over the allowed holding time due to circumstances which were beyond laboratory control.
Analyte was detected . However, the analyte concentration is an estimated value, which is between the Method Detection Limit (MDL) and the Practical Quantitation Limit (PQL).
Matrix spike recovery is outside control limits due to matrix interference. Laboratory Control Sample recovery was acceptable.
Surrogate recovery is outside control limits due to matrix interference.
The analysis of the sample required a dilution such that the surrogate concentration was diluted below the method acceptance criteria.
Results represent LCS and LCSD data.
Definition :
%Limi: Percent acceptable limits.
%REC : Percent recovery.
C0n.L: Acceptable Control Limits
Conce: Added concentration to the sample.
LCS: Laboratory Control Sample
MDL: Method Detection Limit is a statistically derived number which is specific for each instrument, each method, and each compound. It indicates a distinctively detectable quantity with 99% probability.
MS: Matrix Spike
MS DU: Matrix Spike Duplicate
American Environmental Testing Laboratory Inc. -- ~ -~ -- ~ -- ~ - ~ - - -.
2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO. 10181 Tel: (888) 288-AETL (818) 845-8200 Fax: (818) 845-8840 www.aetlab.com
Data Qualifiers and Descriptors
ND : Analyte was not detected in the sample at or above MDL.
PQL: Practical Quantitation Limit or ML (Minimum Level as per RWQCB) is the minimum concentration that can be quantified with more than 99% confidence. Taking into account all aspects of the entire analytical instrumentation and practice.
Recov: Recovered concentration in the sample.
RPD : Relative Percent Difference
American Environmental Testing -- - Laboratory -. Inc. pp -p -
2834 & 2908 North N a o m ~ Street, Burbank, CA 91504 -DOHS NO. 1541, LACSD NO. 10181 Tel. (888) 288-AETL (818) 845-8200 Fax. (818) 845-8840 www.aetlab.
Telephone: (714) 985-3434 Attention: Tom Tatnall
Ordered By H-
Job Number Order Date Client
38386 1 08/02/2006 1 H &A
Haley & Aldrich 500 South Kraemer Blvd. Suite 370
Brea, CA 92821-6723
Project ID: 32486-007 Project Name: Delphi System Corp.
Site : 1201 N. Magnolia Avenue Anaheim, CA 92801
Number of Pages 12 ch, Iflc. Date Received 08/02/2006
Date Reported 08/07/2006
Enclosed please find results of analyses of 1 water and 11 solid waste samples which were analyzed as specified on the attached chain of custody. If there are any questions, please do not hesitate to call.
Checked By: Approved By:
Cyrus Razmara, Ph. D. Laboratory Director
CHAIN OF CUSTODY RECORD N? 43951
TABLE Summary of Aqueous Analytical Results for Polychlorinated Biphenyls (PCBs) by GC
1201 N. Magnolia Avenue Anaheim, CA 92801
Polychlorinated Biphenyls (PCBs) by GC. Method: 8082
1) "ND<X" INDICATES CONSTITUENT(S) NOT DETECTED AT OR ABOVE METHOD DETECTION LIMIT.
2) "J" INDICATES ANALYTE WAS DETECTED. HOWEVER, ANALYTE CONCENTRATION IS AN ESTIMATED VALUE WHICH IS BETWEEN
THE METHOD DETECTION LIMIT (MDL) AND THE PRACTICAL QUANTITATION LIMIT(PQL).
3) "D" INDICATES THE SAMPLE WAS DILUTED TO BRING THE ANALYTE CONCENTRATION WITHIN CALIBRATION RANGE.
File: AQ-8082.~1~
TABLE Summary of Solid Waste Analytical Results for Arsenic by ICP
1201 N. Magnolia Avenue Anaheim, CA 92801
Arsenic by ICP. Method: (6010BSCAN)
1) "ND<X" INDICATES CONSTITUENT(S) NOT DETECTED AT OR ABOVE METHOD DETECTION LIMIT.
2) "J" INDICATES ANALYTE WAS DETECTED. HOWEVER. ANALYTE CONCENTRATION IS AN ESTIMATED VALUE WHICH IS BETWEEN
THE METHOD DETECTION LIMIT (MDL) AND THE PRACTICAL QUANTITATION LIMIT(PQL).
3) "D" INDICATES THE SAMPLE WAS DILUTED TO BRING THE ANALYTE CONCENTRATION WITHIN CALIBRATION RANGE.
Sample Date
Laboratory Job Number
Arsenic
File: SW-6010BSCAN.xls
5.0 5.0 500 mg/Kg
8/2/2006
38386
2.305
- 8/2/2006
38386
3.655
8/2/2006
38386
16.4
8/2/2006
38386
4.60J
8/2/2006
38386
4.20J
8/2/2006
38386
14.9
8/2/2006
38386
4.60J
8/2/2006
38386
24.5
8/2/2606
38386
4.305
TABLE Summary of Solid Waste Analytical Results for Polychlorinated Biphenyls (PCBs) by GC
1201 N. Magnolia Avenue Anaheim, CA 92801
Polychlorinated Biphenyls (PCBs) by GC. Method: (8082)
Sample Date
Laboratory Job Number
Aroclor-1016 (PCB-1016) udKg
Aroclor-1221 (PCB-? 221 ) -
udKg
Aroclor-1232 (PCB-1232) udKg
Aroclor-1242 (PCB-1242) ug/Kg
Aroclor-1248 (PCB-1 248) ug/Kg
Aroclor-1254 (PCB-1 254) ug/Kg
Aroclor-1260 (PCB-1260) ug/Kg
Aroclor-1262 (PCB-1 262) ug/Kg
Aroclor-1268 (PCB-1 268) udKg
1) "NDcX" INDICATES CONSTITUENT(S) NOT DETECTED AT OR ABOVE METHOD DETECTION LIMIT.
2) "J" INDICATES ANALYTE WAS DETECTED. HOWEVER, ANALYTE CONCENTRATION IS AN ESTIMATED VALUE WHICH IS BETWEEN
THE METHOD DETECTION LIMIT (MDL) AND THE PRACTICAL QUANTITATION LIMIT(PQL).
3) "D" INDICATES THE SAMPLE WAS DILUTED TO BRING THE ANALYTE CONCENTRATION WITHIN CALIBRATION RANGE.
File: SW-8082.~1~
. . . .- - .- .- -
American Environmental .- - Testing -- - Laboratory -. Inc. 2834 &2908 North N a o m ~ Street, Burbank, CA 91504 =DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (8 18) 845-8200 Fax: (81 8) 845-8840 www.aetlab.com
ANALYTICAL RESULTS
Ordered By
Anaheim, CA 9280 1 Suite 370
Telephone: (714)985-3434 Attn : Tom Tatnall
Page: 2 Client
H&A I Project ID: 32486-007 Project Name: Delphi System Corp .
Our Lab I.D.
Method: (8082), Polychlorinated Biphenyls (PCBs) by GC QC Batch No: 080306
i
% Rec.
94
Surrogates
1 Tetrachloro-m-xylene 4-
AETL Job Number 38386
% R e c . Limit 30-150
Submitted
08/02/2006
38386.01 % Rec.
7 9
38386.02 % Rec.
8 4
38386.03 % Rec.
8 7
38386.04 % Rec.
9 6
American - Environmental . - -. -- - --- Testing Laboratory - -- Inc. 2834 8 ~ 2 9 0 8 North Naom~ Street, Burbank, CA 91504*DOHS NO. 1541,LACSDNO: 10181 Tel: (888) 288-AETL (818) 845-8200 Fax: (8 18) 845-8840 www.aetlab.com
ANALYTICAL RESULTS
Ordered By
500 South Kraemer Blvd. Suite 370
Telephone: (714)985-3434 Attn: Tom Tatnall
S i t e
Anaheim, CA 9280 1
Method: (8082), Polychlorinated Biphenyls (PCBs) by GC QC Batch No: 080306
Page: 3
H &A Project ID: 32486-007 Project Name: Delphi System C o r p .
38386.09 CSO276-CC-0
Aroclor- 1248 (PCB- 1248)
Aroclor-1254 (PCB-1254)
Aroclor-1260 (PCB-1260)
AETL Job Number 38386
Aroclor- 1262 (PCB- 1262)
Aroclor-1268 (PCB-1268)
- Submitted 08/02/2006
38386.07 CSO274-CC-0
38386.06 CSO273-CC-0
- - - Our Lab I.D. Client Sample I.D.
25.0
25.0
25.0
/ Our Lab I.D. Surrogates / % ~ e c . ~ i r n i b
- 38386.08
CSO275-CC-0 38386.05
CSO272-CC-0
25.0
25.0
50.0
50.0
50.0
38386.05 % Rec.
50.0
50.0
107
ND
ND
38386.06 % Rec.
ND
ND
ND
ND
ND
38386.07 % Rec.
ND
ND
ND
ND
ND
38386.08 % Rec.
ND
ND
38386.09 ' % Rec.
ND
ND
ND
42.05
ND
ND
ND
ND
ND
ND
American Environmental - - --. . - - Testing Laboratory Inc. - -- -- -- -- - -- . . --
2834 & 2908 North Naomi Street, Burbank, CA 91 504 *DOHS NO: 1541, LACSD NO: 10181 Tel: (888) 288-AETL (818) 845-8200 Fax: (818) 845-8840 www.aetlab.com
ANALYTICAL RESULTS
O r d e r e d By 1 Haley & Aldrich 500 South Kraemer Blvd. Suite 370 Brea, CA 9282 1-6723
Telephone: (714)985-3434 Attn: Tom Tatnall
Page: 4 Project ID: 32486-007 Project Name: Delphi Sys tem Corp.
S i t e
1201 N. Magnolia Avenue Anaheim, CA 92801
Method: (8082), Polychlorinated Biphenyls (PCBs) by GC QC Batch No: 080306
AETL Job Number ( Submitted 38386 1 08/02/2006
Client H &A
Our Lab LD. i Client Sample I.D.
38386.10 CSO277-CC-0
Date Sampled Date Prepared Pre~aration Method
08/02/2006
08/03/2006
3 5 5 0 ~
Date Analyzed Matrix
08/04/2006
Solid Waste
Analytes MDL
Aroclor- 1232 (PCB- 1232)
Aroclor-1242 (PCB-1242)
, Aroclor-1248 (PCB-1248)
1 Aroclor- 1268 (PCB-1268) 1 500 / 1000 1 ND 1 1 I 1 1
i
PQL
1000
1000
Aroclor- 10 16 (PCB- 10 16)
Results
ND
ND
500
500
500
500
I Aroclor-1254 (PCB-1254)
Aroclor-1260 (PCB-1260)
Aroclor- 1262 (PCB- 1262)
Aroclor- 122 1 (PCB- 122 1) 1 500
1000
1000
1000
500
500
500
1000
1000 ----
1000
ND
ND
ND
38386.10 % Rec.
Our Lab I.D. , Surrogates
ND
ND
% R e c . L i m i t i
I
I
23,400
Ordered BY
American Environmental - -- - Testing Laboratory - - Inc. 2834 &2908 North N a o m ~ Street, Burbank, CA 91504 DOHS NO. 1541,LACSDNO: 10181 Tel: (888) 288-AETL (8 18) 845-8200 Fax: (81 8) 845-8840 www.aetlab.com
ANALYTICAL RESULTS
S i t e
1500 South Kraemer Blvd. I Suite 370 ~ r e a . CA 92821-6723
1201 N, Magnolia Avenue Anaheim, CA 9280 1
Telephone: (714)985-3434 Attn: Tom Tatnall
Pane: 5
Method: (8082), Polychlorinated Biphenyls (PCBs) by GC QC Batch No: 080306
- a -
Client -
H &A Project ID: 32486-007 Project Name: Delphi System Corp.
- - Our Lab I.D. Client Sample I.D.
38386.11 CSO278-CC-0
00-01
Date Sampled Date Prepared Preparation Method Date Analyzed Matrix Units
- AETL Job Number
38386
I Dilution Factor / ~ n a l ~ t e s MDL PQL
/ rocl lor- 10 16 (PCB- 10 16) 1 25.0 50.0
Submitted
08/02/2006
08/02/2006
08/03/2006
3550B
08/04/2006
Solid Waste
udKn 1
Results
ND
Aroclor- 122 1 (PCB- 122 1) 25.0 50.0
Aroclor-1232 (PCB-1232) 25.0 50.0
Aroclor- 1242 (PCB-1242) 25.0 50.0
Aroclor- 1248 (PCB-1248) 25.0 50.0
Aroclor- 1254 (PCB- 1254) 25.0 50.0
Aroclor- 1260 (PCB-1260) 25.0 50.0
ND
ND
ND
167
ND
ND
Aroclor-1262 (PCB-1262) 25.0 50.0
Aroclor- 1268 (PCB- 1268) 25.0 50.0
I
ND
ND
Our Lab I.D. Surrogates % R e c . Limib Tetrachloro-m-xvlene 1 30-150
I
38386.11 % Rec.
98
American Environmental Testing Laboratory Inc. - - pppp -- - - - - - - -
2834 &2908 North Naom~ Street, Burbank, CA 91504 DOHS NO 1541,LACSDNO 10181 Tel (888) 288-AETL (8 18) 845-8200 Fax. (8 18) 845-8840 www.aetlab.com
ANALYTICAL RESULTS
Ordered By
Haley & Aldrich 500 South Kraemer Blvd.
/ Suite 370 I Brea, CA 92821-6723
Attn :
I Telephone: (714) 985-3434
Tom Tatnall
Page 6 Project ID: 32486-007 Project Name: Delphi System Corp.
Site
Anaheim, CA 9280 1
AETL Job Number Submitted Client 38386 08/02/2006 H&A
- .
Analytes Arsenic 62-32 *;n ""'q-' ' <y " "" ' <I%
i i ,> -i-
Methods of Analyses (601 OBSCAN) I
1 Date Prewared I I I !
08/02/2006 ! Date Analyzed 08/02/2006
Matrix Solid Waste
OC Batch Number 080206-2 ! -
/Units mg/Kg
Method Detection Limit 0.5 Practical Quantitation Limit 5.0
1 Dilution Factor I I
1
N / A ~ z h o d Blank 1 / I ND / I !
American Environmental - - - - Testing - - Laboratory Inc. 2834 &2908 North Naom~ Street, Burbank, CA 91504 DOHS NO. 1541,LACSDNO. 10181 Tel. (888) 288-AETL (818) 845-8200 Fax. (818) 845-8840 www.aetlab.com
ANALYTICAL RESULTS Ordered B y
500 South Kraemer Blvd. Suite 370 Brea, CA 9282 1-6723
Telephone: (7 14)985-3434 Attn: Tom Tatnall
S i t e 120 1 N. Magnolia Avenue Anaheim, CA 92801
Page: 7
Project ID: 32486-007 AETL Job Number Submitted Client Project Name: D e l p h i S y s t e m C o r p . 3 8 3 8 6 0 8 / 0 2 / 2 0 0 6 H &A
Method: 8082, Polychlorinated Biphenyls (PCBs) by GC QC Batch No: 080206
Our Lab I.D. Method Blank 38386.12 Client Sample I.D. EB-080206
Date Sampled 08/02/2006
Date Pre~ared 08/02/2006 08/02/2006
1 Preparation Method 3510~ 3510~
1 Date Analyzed 08/04/2006 08/04/2006
i Matrix Aqueous Aqueous
I Units I I ug/L I ug/L I I I i I
- - 1 Dilution Factor 1 1 Analytes MDL PQL Results Results
I
Aroclor- 122 1 (PCB- 122 1) 2.0 10.0 ND ND 1 i
Aroclor- 1232 (PCB- 1232) 1.0 5.0 ND ND i
Aroclor- 1242 (PCB- 1242) 1.0 5.0 ND ND
Aroclor- 1248 (PCB- 1248) 1.0 5.0 ND ND I
Aroclor-1260 (PCB-] 260) 1.0 5.0 ND ND
Aroclor- 1262 (PCB- 1262) 1.0 5.0 ND ND
Aroclor- 1268 (PCB- 1268) 1.0 5.0 ND ND
Our Lab I.D. Method Blank 38386.12 / Surrogates %Rec.Limib % Rec. % Rec. 1 Tetrachloro-m-xvlene 1 30-150 108 77 1
American Environmental Testing Laboratory Inc. - --- -- - pp - -- - pppp - -
2834 &2908 North Naom~ Street, Burbdnk, CA 91504 -DOHS NO. 1541,LACSDNO: 10181 Tel: (888) 288-AETL (818) 845-8200 F a x (818) 845-8840 www.aet lab.com
ANALYTICAL RESULTS
Ordered By . - .-
Haley & Aldrich South Kraemer BLvd.
/ Suite 370 / Brea, CA 92821-6723 Telephone: (714) 985-3434
Attn : Tom Tatnall
Page 8 Project ID: 32486-007 Project Name: Delphi System Corp.
Site
120 1 N. Magnolia Avenue Anaheim, CA 92801
AETL Job Number Submitted I Client 38386 / 08/02/2006 / H&A
ilution Factor
Units Method Detection Limit Practical Quantitation Limit
mglL i 0.05
0.10 i , I
American Environmental Testing Laboratory Inc. -- - - - - - -- - - --- -- -- -- pp - -
2834 &2908 North Naom~ Street, Burbank, CA 91504-DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL ( 8 18) 845-8200 Fax: (8 18) 845-8840 www.aetlab.com
ANALYTICAL RESULTS
O r d e r e d By
500 South Kraemer Blvd. Suite 370
Telephone: (714)985-3434 Attn: Tom Tatnall
S i t e
120 1 N. Magnolia Avenue Anaheim, CA 9280 1
Pane: 9
Method: 60 1 OBSCAN, Total Arsenic
"
QUALITY CONTROL REPORT
QC Batch No: 080306 Sample Spiked: 38392.01 QC Prepared: 08/03/2006 QC Analyzed: 08/03/2006 Units: mglL
Submitted
08/02/2006 Project ID: 32486-007 Project Name: Delphi SYS t em Corp .
Sample MS MS 1 MS 1 MS DUP MS DUP I MS DUP RPD 1 MSlMSD I MS RT
- AETL Job Number
38386
/ Analytes / Result I Concen Recov / % REC I Concen Recov / % REC % % Limit / % Limit 1
QC Batch No: 080306 Sample Spiked: 38392.01 QC Prepared: 08/03/2006 QC Analyzed: 08/03/2006 Units: mglL
- .
LCSILCSD
% Lim~t
80-120
Analytes
Arsenic --
LCS
Concen
1.00
LCS
Recov
0.98
LCS
% REC
98
O r d e r e d Bv
American Environmental Testing --- Laboratory -- Inc. 2834 & 2908 North Naom~ Street, Burbank, CA 91504 *DOHS NO 1541, LACSDNO. 10181 Tel: (888) 288-AETL (8 18) 845-8200 Fax. (8 18) 845-8840 www.aetlab.com
ANALYTICAL RESULTS
1 Haley & Aldrich 1 500 South Kraemer Blvd. Suite 370 Brea. CA 9282 1-6723
S i t e
1201 N. Magnolia Avenue Anaheim, CA 9280 1
Telephone: (714)985-3434 Attn: Tom Tatnall
Page: 10
Method: 8082, Polychlorinated Biphenyls (PCBs) by GC QUALITY CONTROL REPORT
-
QC Batch No: 080206 Sample Spiked: 080206 QC Prepared: 08/02/2006 QC Analyzed: 08/04/2006 Units: uglL
Client H &A
--A
Project ID: 32486-007 Project Name: Delphi System Corp .
QC Batch No: 080206 Sample Spiked: 080206 QC Prepared: 08/02/2006 QC Analyzed: 08/04/2006 Units: uglL
Analytes
Aroclor- 1260 (PCB- 1260) - - - - - .. - -. -
LCS LCS LCS LCSILCSD
Analytes Concen Recov % REC % Limit
2.50 2.03 81 75-125
AETL Job Number 38386
Submitted 08/02/2006
Sample
Result
0.0
MS
Concen
2.50
MS
Recov
2.53
MS
% REC
101
MSDUP
Concen
2.50
MS DUP
Recov
2.70
MSDUP
% REC
108
RPD
%
6.7
MSIMSD
% Limit
75-125
MSRPD
% Limit
<20
American Environmental - Testing Laboratory Inc. - -- -- - - -. --- -- .. -
2834 8 ~ 2 9 0 8 North N a o m ~ Street, Burbank, CA 91504-DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (8 18) 845-8200 Fax: (81 8) 845-8840 www.aetlab.com
ANALYTICAL RESULTS
Ordered By
500 South Kraemer Blvd. Suite 370 1 Brea, CA 92821-6723
Telephone: (714)985-3434 Attn: Tom Tatnall
Page: 11 Project ID: 32486-007 Prni~rt Name. D e l ~ h i Svs tem Corr,.
S i t e --
1201 N. Magnolia Avenue Anaheim, CA 92801
AETL Job umber / Submitted 1 Client 38386 1 08/02/2006 1 H &A
Method: (6010BSCAN), Arsenic by ICP QUALITY CONTROL REPORT
QC Batch No: 080206-2 Sample Spiked: 38386.04 QC Prepared: 08/02/2006 QC Analyzed: 08/02/2006 Units: mglKg
QC Batch No: 080206-2 Sample Spiked: 38386.04 QC Prepared: 08/02/2006 QC Analyzed: 08/02/2006 Units: mglKg
I I Analytes
Arsenic
Sample
Result
0.092
1
MS
Concen
1.00
LCSILCSD
% Limit
80-120
--
Analytes
Arsenic
MS
Recov
1.06
LCS
Concen
1.00
MS
% REC
97
LCS
Recov
1.06
LCS
% REC
106
MS DUP
Concen
1.00
MS DUP
Recov
1.08
MSDUP
% REC
9 9
RPD
%
2.0
MSIMSD
% Limit
80-120
MSRPD
% Limit
4 5 _1
American Environmental Testing Laboratory Inc. - - - . .-A - - -- . . - - - -
2834 8 ~ 2 9 0 8 North N a o m ~ Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (81 8) 845-8200 Fax: ( 8 18) 845-8840 www.aetlab.com
ANALYTICAL RESULTS
Ordered By
Anaheim, CA 92801
Telephone: (714)985-3434 Attn: Tom Tatnall
Page: 1 2 Client
H&A - -. 1 Project ID: 32486-007 ProjectName: Delphi System Corp.
AETL Job Number 38386
Method: (8082), Polychlorinated Biphenyls (PCBs) by GC QUALITY CONTROL REPORT
QC Batch No: 080306 Sample Spiked: 080306 QC Prepared: 08/03/2006 QC Analyzed: 08/03/2006 Units: uglKg
Submitted 08/02/2006
MSIMSD
% Lim~t
75-125
Analytes
Aroclor-1260 (PCB-1260)
M S ~ % Limit
<20
MSDUP
% REC
104
QC Batch No: 080306 Sample Spiked: 080306 QC Prepared: 08/03/2006 QC Analyzed: 08/03/2006 Units: uglKg
RPD
%
14.4
Sample
Result
0 .0
Analytes
Aroclor- 1260 (PCB- 1260) - -
MS
Concen
500 .00
LCS
Concen
500.00
MS
Recov
450 . O O
LCS
Recov
545.00
MS
% REC
90
LCS
% REC
109
LCSILCSD
% Limit
75-125
MSDUP
Concen
500.00
MS DUP
Recov
520.00
American Environmental ~ .--- - - Testing ~ p p ~ Laboratory Inc. 2834 8 ~ 2 9 0 8 North Naomi Street, Burbank, CA 91 504*DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (81 8) 845-8200 Fax: (8 18) 845-8840 www.aetlab.com
Data Qualifiers and Descriptors
Data Qualifier:
*. In the QC section, sample results have been taken directly from the ICP reading. No preparation factor has been applied.
Analyte was present in the Method Blank.
Result is from a diluted analysis.
Result is beyond calibration limits and is estimated.
Analysis was performed over the allowed holding time due to circumstances which were beyond laboratory control.
Analyte was detected . However, the analyte concentration is an estimated value, which is between the Method Detection Limit (MDL) and the Practical Quantitation Limit (PQL).
Matrix spike recovery is outside control limits due to matrix interference. Laboratory Control Sample recovery was acceptable.
Surrogate recovery is outside control limits due to matrix interference.
The analysis of the sample required a dilution such that the surrogate concentration was diluted below the method acceptance criteria.
Results represent LCS and LCSD data.
%Limi: Percent acceptable limits.
%REC: Percent recovery.
C0n.L: Acceptable Control Limits
Conce: Added concentration to the sample.
LCS: Laboratory Control Sample
MDL: Method Detection Limit is a statistically derived number which is specific for each instrument, each method, and each compound. It indicates a distinctively detectable quantity with 99% probability.
MS: Matrix Spike
MS DU: Matrix Spike Duplicate
American -- Environmental - Testing - Laboratory Inc. 2834 & 2908 North Naom~ Street, Burbank, CA 9 1504 DOHS NO: 1541, LACSD NO: 10181 Tel: (888) 288-AETL (8 18) 845-8200 Fax: (81 8) 845-8840 www.aetlab.com
Data Qualifiers and Descriptors
ND: Analyte was not detected in the sample at or above MDL.
PQL: Practical Quantitation Limit or ML (Minimum Level as per RWQCB) is the minimum concentration that can be quantified with more than 99% confidence. Taking into account all aspects of the entire analytical instrumentation and practice.
Recov: Recovered concentration in the sample.
RPD: Relative Percent Difference
Enclosed please find results of analyses of 1 water and 13 solid waste samples which were analyzed as specified on the attached chain of custody. If there are any questions, please do not hesitate to call.
TABLE Summary of Aqueous Analytical Results for Polychlorinated Biphenyls (PCBs) by GC
1201 N. Magnolia Ave. Anaheim, CA 92801
Polychlorinated Biphenyls (PCBs) by GC. Method: 8082
Sample Date 912612006
Laboratory Job Number 39098
Aroclor-1016 (PCB-1016) ug/L ND<l 0
~ r o c l o ~ 2 2 1 (PCB-1221 ) uglL ND<2 0 -- - -
Aroclor-1232 (PCB-1232) uglL NDc1 0
rocl lor-1 242 (PCB-1242) uglL ND<1 0
Aroclor-1248 (PCB-7248) u g l ~ ~ D c i 0
Aroclor-1254 (PCB-1254) ug/L ND<l 0
~roclor-~260<P~~-1260) ug1L ND<1 0
~rockr-1262 (PCB-1262) -
uglL NDc1 0 - --- -- -
Aroclor-1268 (PCB-1268) uglL ND<1 0 - -
1) "ND<X INDICATES CONSTITUENT(S) NOT DETECTED AT OR ABOVE METHOD DETECTION LIMIT.
2) "J" INDICATES ANALYTE WAS DETECTED. HOWEVER, ANALYTE CONCENTRATION IS AN ESTIMATED VALUE WHICH IS BETWEEN
THE METHOD DETECTION LIMIT (MDL) AND THE PRACTICAL QUANTITATION LIMIT(PQL).
3) "D" INDICATES THE SAMPLE WAS DILUTED TO BRING THE ANALYTE CONCENTRATION WITHIN CALIBRATION RANGE.
File: AQ-8082.~1~
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American Environmental Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank. CA 91504*DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (81 8) 845-8200 Fax: (818) 845-8840 www.aetlab.com
-
ANALYTICAL RESULTS
O r d e r e d By S i t e
Haley & Aldrich 500 South Kraemer Blvd. Suite 370 Brea, CA 9282 1-6723 I Telephone: (714) 985-3434 Attn: Tom Tatnall
Page 2 Project ID: 32486-007 Project Name: Delphi System Corp.
39098.09 39098.1 0 39098.1 1 39098.12 39098.13
NIA
CSO287-CC-000-01 CSO288-CC-000-01 CSO289-CC-000-01 CSO290-CC-000-01
CS0291 -CC-000-01 Method Blank
09/26/2006 09/26/2006 09/26/2006 0912612006
09/26/2006 I I
3.905
20.3
17.4
3.105
5.05
ND
Ordered By
American Environmental Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (8 18) 845-8200 Fax: (81 8 ) 845-8840 www.aetlab.com
ANALYTICAL RESULTS
Haley & Aldrich 500 South Kraemer Blvd. Suite 370 Brea, CA 9282 1-6723 1
S i t e
Telephone: (714)985-3434 Attn: Tom Tatnall
Page: 3
Method: (8082), Polychlorinated Biphenyls (PCBs) by GC QC Batch No: 092706
Project ID: 32486-007 Project Name: Delphi System Corp .
, ,&ETZ1' Sob; ,Nq#bW 39098
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CS028 1-CC-0 ir,&s*o4 i : CSO282-CC-0
American Environmental Testing Laboratory Inc. 2834 8 ~ 2 9 0 8 North Naomi Street, Burbank. CA 91504 DOHS NO: 1541,LACSDNO. 10181 Tel: (888) 288-AETL (81 8) 845-8200 Fax: (81 8 ) 845-8840 www.aetlab.com
ANALYTICAL RESULTS
Telephone: (7 14)985-3434 Attn: Tom Tatnall
S i t e
Page: 4
Method: (8082), Polychlorinated Biphenyls (PCBs) by GC QC Batch No: 092706
&ur L S ~ -' i'i I I
Client Sample I.D. CSO283-CC-0 CSO285-CC-0 CSO284-CC-0 CSO286-CC-0 A$M$r CSO287-CC-0
American Environmental Testing Laboratory Inc. 2834 8 ~ 2 9 0 8 North Naomi Street, Burbank, CA 91504*DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (818) 845-8200 Fax: (818) 845-8840 www.aetlab.com
ANALYTICAL RESULTS
Ordered Bv Site
Telephone: (7 14)985-3434 Attn: Tom Tatnall
Page: 5 Project ID: 32486-007 Proiect Name: Delphi S y s t e m Corp.
''8bb ' N*? 1' ~ S U i t t e ? , - 1 "Client 39098 1 09 /26 /2006 1 H &A
Method: (8082), Polychlorinated Biphenyls (PCBs) by GC QC Batch No: 092706
0"IH ' "XD. .~ 1 ' 1 1 ' $ Client Sample I.D. CSO290-CC-0 CSO291-CC-0 CSO288-CC-0 CSO289-CC-0
American Environmental Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (8 18) 845-8200 Fax: (8 18) 845-8840 www.aetlab.com
ANALYTICAL RESULTS
Telephone: (714)985-3434 Attn: Tom Tatnall
Page: 6 Project ID: 32486-007 Proiect Name: Delphi System Corp .
S i t e
Method: 8082, Polychlorinated Biphenyls (PCBs) by GC QC Batch No: 092706
Ordered Bv
American Environmental Testing Laboratory Inc. 2834 8~2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (818) 845-8200 Fax: (818) 845-8840 www.aetlab.com
ANALYTICAL RESULTS
Telephone: (7 14)985-3434 Attn: Tom Tatnall
Page: 7 Project ID: 32486-007 Project Name: Delphi S y s t e m Corp.
S i t e
Method: 601 OBSCAN, Total Arsenic QUALITY CONTROL REPORT
QC Batch No: 092906 Sample Spiked: 39098.14 QC Prepared: 09/29/2006 QC Analyzed: 09/29/2006 Units: mglL
QC Batch No: 092906 Sample Spiked: 39098.14 QC Prepared: 09/29/2006 QC Analyzed: 09/29/2006 Units: mglL
O r d e r e d By
American Environmental Testing Laboratory Inc. 2834 8~2908 North Naorni Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (818) 845-8200 Fax: (818) 845-8840 www.aetlab.com
ANALYTICAL RESULTS
Telephone: (714)985-3434 Attn: Tom Tatnall
- Project ID: 32486-007 Proiect Name: Delphi Sys tem Corp.
S i t e
Method: 8082, Polychlorinated Biphenyls (PCBs) by GC QUALITY CONTROL REPORT
QC Batch No: 092706 Sample Spiked: 092706 QC Prepared: 09/27/2006 QC Analyzed: 09/28/2006 Units: uglL
QC Batch No: 092706 Sample Spiked: 092706 QC Prepared: 09/27/2006 QC Analyzed: 09/28/2006 Units: uglL
American Environmental Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 -DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (81 8) 845-8200 Fax: (81 8) 845-8840 www.aetlab.com
ANALYTICAL RESULTS
Attn: Tom Tatnall
QC Batch No: 100206 Sample Spiked: 39098.01 QC Prepared: 10102/2006 QC Analyzed: 10/02/2006 Units: mglKg
Page: 9
QC Batch No: 100206 Sample Spiked: 39098.01 QC Prepared: 1010U2006 QC Analyzed: 10lOU2006 Units: mglKg
Project ID: 32486-007 Project Name: Delphi System Corp .
Method: (6010BSCAN), Arsenic by ICP QUALITY CONTROL REPORT
AETL 39098 J P - ~
0 9 / 2 6 / 2 0 0 6 1 H &A
American Environmental Testing Laboratory Inc. 2834 & 2908 North Naomi Street, Burbank, CA 91504 DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (8 18) 845-8200 Fax: (8 18) 845-8840 www.aetlab.com
ANALYTICAL RESULTS
O r d e r e d By S i t e
Telephone: (7 14)985-3434 Attn: Tom Tatnall
Page: 10 - Project ID: 32486-007 Project Name: Delphi Sys tem Corp.
Method: (8082), Polychlorinated Biphenyls (PCBs) by GC QUALITY CONTROL REPORT
QC Batch No: 092706 Sample Spiked: 092706 QC Prepared: 09/27/2006 QC Analyzed: 09/28/2006 Units: uglKg
QC Batch No: 092706 Sample Spiked: 092706 QC Prepared: 09/27/2006 QC Analyzed: 09/28/2006 Units: uglKg
American Environmental Testing Laboratory Inc. 2834 & 2908 North Naomi Street, Burbank, CA 9 1504 DOHS NO: 1541, LACSDNO: 10181 Tel: (888) 288-AETL (8 18) 845-8200 Fax: (8 18) 845-8840 www.aetlab.com
Data Qualifiers and Descriptors
Data Qualifier:
Definition:
%Limi:
%REC :
C0n.L:
Conce:
LCS:
MDL:
MS:
MS DU:
In the QC section, sample results have been taken directly from the ICP reading. No preparation factor has been applied.
Analyte was present in the Method Blank.
Result is from a diluted analysis.
Result is beyond calibration limits and is estimated.
Analysis was performed over the allowed holding time due to circumstances which were beyond laboratory control.
Analyte was detected . However, the analyte concentration is an estimated value, which is between the Method Detection Limit (MDL) and the Practical Quantitation Limit (PQL).
Matrix spike recovery is outside control limits due to matrix interference. Laboratory Control Sample recovery was acceptable.
Surrogate recovery is outside control limits due to matrix interference.
The analysis of the sample required a dilution such that the surrogate concentration was diluted below the method acceptance criteria.
Results represent LCS and LCSD data.
Percent acceptable limits.
Percent recovery.
Acceptable Control Limits
Added concentration to the sample.
Laboratory Control Sample
Method Detection Limit is a statistically derived number which is specific for each instrument, each method, and each compound. It indicates a distinctively detectable quantity with 99% probability.
Matrix Spike
Matrix Spike Duplicate
American Environmental Testing - Laboratory Inc. 2834 & 2908 North Naomi Street, Burbank, CA 9 1504 DOHS NO: 1541, LACSD NO: 10181 Tel: (888) 288-AETL (8 18) 845-8200 Fax: (81 8) 845-8840 www.aetlab.com
RECrT"-- ' ~ 3
Ordered B y O C T 1 9 2006
Telephone: (714) 985-3434
Attention: Tom Tatnall
Jag Number Order Date Client 39287 1 10/09/2006 1 H&A
Project ID: 32486-007 Project Name: Delphi System Corp.
Site : 1201 N. Magnolia Ave.
Anaheim, CA 92801
Enclosed please find results of analyses of 13 concrete samples which were analyzed as specified on the attached chain of custody. If there are any questions, please do not hesitate to call.
Checked By: Approved By: v-
Cyrus Razmara, Ph. D.
Laboratory Director
Page 1 0 1 1
Page 1 of 2
Cyrus Razmara
From: Hoggan, Kelly [[email protected]]
Sent: Monday, October 09,2006 11 :51 AM
To: Cyrus Razmara; Jim Lin
Subject: Additional Analysis for Job # 39098
Jim and Cyrus,
Please run lead 6010B on all thirteen concrete matrix samples from Job # 39098 with 3 day TOT. CS0279-SS-000-01 through CS0291~SS~000~01 .
Thanks,
Kelly Hoggan Geologist Haley A. Aldrich, Inc. 500 S. Kraemer Blvd., Suite 370 Brea, CA 92821-6723 Direct Line: 714.984.21 04 Cell: 714.709.3072 Office: 714.985.3434 Fax: 714.985.3433 [email protected] www.HaleyAldrich.com
NOTICE
The information contained in this communication is confidential and privileged proprietary information intended only for the individual or entity to whom it is addressed. Any unauthorized use, distribution, copying or disclosure of this communication is prohibited. If you have received this communication in error, please contact the sender immediately.
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American Environmental Testing Laboratory Inc. 2834 & 2908 North Naomi Street, Burbank, CA 9 1504 *DOHS NO: 1541, LACSDNO: 10181 Tel: (888) 288-AETL (818) 845-8200 Fax: (818) 845-8840 www.aetlab.com
ANALYTICAL RESULTS
Ordered Bv S i t e
500 South Kraemer Blvd. Suite 370
Telephone: (714)985-3434 Attn: Tom Tatnall
- - Q - --
Project ID: 3 2 4 8 6 - 0 0 7 Project Name: Delphi Sys tem Corp.
Method: (601 OB.LEAD), Lead, ICP QC Batch No: 101106
American Environmental Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504 -DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (818) 845-8200 Fax: (818) 845-8840 www.aetlab.com
ANALYTICAL RESULTS
Ordered Bv S i t e
500 South Kraemer Blvd. Suite 370
Telephone: (7 14)985-3434 Attn: Tom Tatnall
Pane: 3 " Project ID: 32486-007 Project Name: Delphi Sys tem Corp.
Method: (60 1 OB.LEAD), Lead, ICP QC Batch No: 101106
American Environmental Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504-DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (818) 845-8200 Fax: (818) 845-8840 www.aetlab.com
ANALYTICAL RESULTS
O r d e r e d Bv Site - - -- - - - -
500 South Kraemer Blvd. Suite 370
Telephone: (714)985-3434 Attn: Tom Tatnall
Page: 4 - Project ID: Proiect Name: Delphi System Corp.
Method: (601 OB.LEAD), Lead, ICP QC Batch No: 101106
American Environmental Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, CA 91504.DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (818) 845-8200 Fax: (818) 845-8840 www.aetlab.com
ANALYTICAL RESULTS Ordered By Site
500 South Kraemer Blvd. Suite 370
Telephone: (7 14)985-3434 Attn: Tom Tatnall
Page: 5
Project ID: 32486-007 Project Name: Delphi Sys tem Corp.
Method: (60 1 OB.LEAD), Lead, ICP QUALITY CONTROL REPORT
QC Batch No: 101106 Sample Spiked: 39287.01 QC Prepared: 10/1112006 QC Analyzed: 10/11/2006
QC Batch No: 101106 Sample Spiked: 39287.01 QC Prepared: 10/11/2006 QC Analyzed: 10/11/2006
American Environmental Testing Laboratory Inc. 2834 &2908 North Naomi Street, Burbank, C A 91504 DOHS NO: 1541,LACSDNO: 10181 Tel : (888) 288-AETL (81 8 ) 845-8200 Fax: (81 8) 845-8840 www.aetlab.com
Data Qualifiers and Descriptors
Data Qualifier:
* : In the QC section, sample results have been taken directly from the ICP reading. No preparation factor has been applied.
Analyte was present in the Method Blank.
Result is from a diluted analysis.
Result is beyond calibration limits and is estimated.
Analysis was performed over the allowed holding time due to circumstances which were beyond laboratory control.
Analyte was detected . However, the analyte concentration is an estimated value, which is between the Method Detection Limit (MDL) and the Practical Quantitation Limit (PQL).
Matrix spike recovery is outside control limits due to matrix interference. Laboratory Control Sample recovery was acceptable.
Surrogate recovery is outside control limits due to matrix interference.
The analysis of the sample required a dilution such that the surrogate concentration was diluted below the method acceptance criteria.
Results represent LCS and LCSD data.
Definition:
%Limi: Percent acceptable limits.
%REC : Percent recovery.
C0n.L: Acceptable Control Limits
Conce: Added concentration to the sample.
LCS: Laboratory Control Sample
MDL: Method Detection Limit is a statistically derived number which is specific for each instrument, each method, and each compound. It indicates a distinctively detectable quantity with 99% probability.
MS: Matrix Spike
MS DU: Matrix Spike Duplicate
American Environmental -- Testing Laboratory Inc. 2834 8~2908 North Naomi Street, Burbank, CA 91504 *DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (818) 845-8200 Fax: (818) 845-8840 www.aetlab.com
Data Qualifiers and Descriptors
ND: Analyte was not detected in the sample at or above MDL.
PQL: Practical Quantitation Limit or ML (Minimum Level as per RWQCB) is the minimum concentration that can be quantified with more than 99% confidence. Taking into account all aspects of the entire analytical instrumentation and practice.
Recov: Recovered concentration in the sample.
RPD: Relative Percent Difference