ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica Sacramento880 Riverside ParkwayWest Sacramento, CA 95605Tel: (916)373-5600
TestAmerica Job ID: 320-4071-1Client Project/Site: Stringfellow Acid Project
For:CH2M Hill Constructors, Inc.3 Hutton Centre DriveSuite 200Santa Ana, California 92707
Attn: Emily Keene
Authorized for release by:10/8/2013 5:44:30 PM
Jill Kellmann, Project Manager II(916)[email protected]
This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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SDMS DOCID#1142010
Table of Contents
Client: CH2M Hill Constructors, Inc.Project/Site: Stringfellow Acid Project
TestAmerica Job ID: 320-4071-1
Page 2 of 43TestAmerica Sacramento
10/8/2013
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
Isotope Dilution Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 24
Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 37
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 38
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 39
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 40
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 42
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Definitions/GlossaryTestAmerica Job ID: 320-4071-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Qualifiers
GC/MS VOA
Qualifier Description
H Sample was prepped or analyzed beyond the specified holding time
Qualifier
GC Semi VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
HPLC/IC
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
LCMS
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤ Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TestAmerica Sacramento
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Case NarrativeClient: CH2M Hill Constructors, Inc. TestAmerica Job ID: 320-4071-1
Project/Site: Stringfellow Acid Project
Job ID: 320-4071-1
Laboratory: TestAmerica Sacramento
Narrative
Job Narrative
320-4071-1
Receipt
The samples were received on 9/14/2013 9:10 AM; the samples arrived in good condition, properly preserved and, where required, on ice.
The temperatures of the 2 coolers at receipt time were 3.7º C and 3.8º C.
GC/MS VOA - GRO
The associated sample in batch 25193 was received with the encore container improperly set. As a result, the cap of the encore came off
during transit, and the sample was lost. As a result, two low level encores were prepared and no medium level encores were preserved.
The following samples were prepared outside of preparation holding time: EPAZ5MW5S00 (320-4071-1), EPAZ5MW9S00 (320-4071-3),
EPAZ5S15S00 (320-4071-4), EPAZ5S15S03 (320-4071-5), EPAZ5S16S00 (320-4071-6), EPAZ5S16S03 (320-4071-7), EPAZ5S16S13
(320-4071-8), EPAZ5S17S00 (320-4071-9), EPAZ5S18S00 (320-4071-10). The samples were received on a Saturday with no advance
notice of delivery.
No other analytical or quality issues were noted.
GC/MS Semi VOA - Method NDMA
The matrix spike / matrix spike duplicate (MS/MSD) recoveries for prep batch 25607 (analytical batch 25889) were outside control limits.
The associated laboratory control sample (LCS) recovery met acceptance criteria.
The matrix spike / matrix spike duplicate (MS/MSD) percent recoveries and percent RPD for prep batch 25404 (analytical batch 26498)
were outside control limits. No action was taken, as the percent recovery values were acceptable in the laboratory control sample (LCS).
No other analytical or quality issues were noted.
HPLC - Method 7199
The sample matrix has been determined to be reductive in natures. (320-4069-3 MSI), EPAZ5S102S51 (320-4069-3), EPAZ5S102S51
(320-4069-3 MS), EPAZ5S102S51 (320-4069-3 MSD), EPAZ5S15S00 (320-4071-4), EPAZ5S17S00 (320-4071-9).
No other analytical or quality issues were noted.
GC Semi VOA
No analytical or quality issues were noted.
LCMS - Method 6850
The matrix spike duplicate (MSD) recovery for batch 26394 was outside control limits due to a high level of target analyte present int the
parent sample. The associated laboratory control sample (LCS) recovery met acceptance criteria.
The results for sample EPAZ5MW5S00 (320-4071-1) were reported from the analysis of a diluted extract due to high concentration of the
target analyte in the analysis of the undiluted extract. The dilution factor was applied to the labeled internal standard area counts and
these area counts were within acceptance limits
Due to the high concentration of Perchlorate in the parent sample, the recoveries in the matrix spike / matrix spike duplicate (MS/MSD) for
batch 26394 are over the calibration range of the instrument and flagged with the "E" qualifier. The MS/MSD were not diluted and
re-analysed. The associated laboratory control sample (LCS) met acceptance criteria.
No analytical or quality issues were noted.
General Chemistry
No analytical or quality issues were noted.
Organic Prep
No analytical or quality issues were noted.
TestAmerica SacramentoPage 4 of 43 10/8/2013
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Case NarrativeClient: CH2M Hill Constructors, Inc. TestAmerica Job ID: 320-4071-1
Project/Site: Stringfellow Acid Project
Job ID: 320-4071-1 (Continued)
Laboratory: TestAmerica Sacramento (Continued)
I certify that this data package is in compliance with the terms and conditions of the contract and Statement of Work both technically and for
completeness, for other than the condition(s) detailed above. Release of the data contained in this hardcopy data package and in the
computer-readable data submitted has been authorized by the Quality Assurance Manager or his/her designee, as verified by the following
signature.
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Detection SummaryTestAmerica Job ID: 320-4071-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Client Sample ID: EPAZ5MW5S00 Lab Sample ID: 320-4071-1
☼Diesel Range Organics (C10-C24)
RL
0.99 mg/Kg
MDL
0.30
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA112 8015B
☼Fluoride 2.5 mg/Kg0.30 Soluble11.4 J 9056
☼Nitrate 0.25 mg/Kg0.11 Soluble149 9056
☼Sulfate 10 mg/Kg0.48 Soluble2360 9056
☼Perchlorate - DL 50 ug/Kg2.6 Total/NA10290 6850
pH 0.100 SU0.100 Soluble17.92 9045C
Oxidation Reduction Potential 0.10 millivolts0.10 Soluble1460 SM 2580B
Client Sample ID: EPAZ5MW5S3 Lab Sample ID: 320-4071-2
No Detections.
Client Sample ID: EPAZ5MW9S00 Lab Sample ID: 320-4071-3
☼Diesel Range Organics (C10-C24)
RL
1.0 mg/Kg
MDL
0.30
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA15.0 8015B
☼Fluoride 2.5 mg/Kg0.30 Soluble11.6 J 9056
☼Nitrate 0.25 mg/Kg0.11 Soluble19.9 9056
☼Sulfate 5.1 mg/Kg0.24 Soluble1150 9056
☼Perchlorate - RA 5.0 ug/Kg0.26 Total/NA128 6850
pH 0.100 SU0.100 Soluble110.3 9045C
Oxidation Reduction Potential 0.10 millivolts0.10 Soluble1330 SM 2580B
Client Sample ID: EPAZ5S15S00 Lab Sample ID: 320-4071-4
☼Diesel Range Organics (C10-C24)
RL
0.99 mg/Kg
MDL
0.30
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA113 8015B
☼Fluoride 2.5 mg/Kg0.30 Soluble12.5 9056
☼Nitrate 0.25 mg/Kg0.11 Soluble16.1 9056
☼Sulfate 5.0 mg/Kg0.24 Soluble117 9056
☼Perchlorate - RA 5.0 ug/Kg0.26 Total/NA14.2 J 6850
pH 0.100 SU0.100 Soluble17.37 9045C
Oxidation Reduction Potential 0.10 millivolts0.10 Soluble1400 SM 2580B
Client Sample ID: EPAZ5S15S03 Lab Sample ID: 320-4071-5
☼Diesel Range Organics (C10-C24)
RL
1.0 mg/Kg
MDL
0.31
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.80 8015B
☼Fluoride 2.5 mg/Kg0.31 Soluble11.0 J 9056
☼Nitrate 0.25 mg/Kg0.11 Soluble10.54 9056
☼Sulfate 5.1 mg/Kg0.24 Soluble11.1 J 9056
pH 0.100 SU0.100 Soluble17.78 9045C
Oxidation Reduction Potential 0.10 millivolts0.10 Soluble1490 SM 2580B
Client Sample ID: EPAZ5S16S00 Lab Sample ID: 320-4071-6
☼Diesel Range Organics (C10-C24)
RL
0.99 mg/Kg
MDL
0.30
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA16.8 8015B
☼Fluoride 2.4 mg/Kg0.29 Soluble11.2 J 9056
☼Nitrate 0.24 mg/Kg0.11 Soluble122 9056
☼Sulfate 4.9 mg/Kg0.23 Soluble16.5 9056
TestAmerica Sacramento
This Detection Summary does not include radiochemical test results.
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Detection SummaryTestAmerica Job ID: 320-4071-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Client Sample ID: EPAZ5S16S00 (Continued) Lab Sample ID: 320-4071-6
☼Perchlorate
RL
5.0 ug/Kg
MDL
0.26
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J2.4 6850
pH 0.100 SU0.100 Soluble16.70 9045C
Oxidation Reduction Potential 0.10 millivolts0.10 Soluble1500 SM 2580B
Client Sample ID: EPAZ5S16S03 Lab Sample ID: 320-4071-7
☼Diesel Range Organics (C10-C24)
RL
1.0 mg/Kg
MDL
0.30
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA11.1 8015B
☼Fluoride 2.6 mg/Kg0.31 Soluble11.3 J 9056
☼Nitrate 0.26 mg/Kg0.11 Soluble11.3 9056
☼Sulfate 5.1 mg/Kg0.25 Soluble12.6 J 9056
☼Perchlorate 4.9 ug/Kg0.26 Total/NA10.27 J 6850
pH 0.100 SU0.100 Soluble18.13 9045C
Oxidation Reduction Potential 0.10 millivolts0.10 Soluble1470 SM 2580B
Client Sample ID: EPAZ5S16S13 Lab Sample ID: 320-4071-8
☼Diesel Range Organics (C10-C24)
RL
1.0 mg/Kg
MDL
0.31
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA11.2 8015B
☼Fluoride 2.5 mg/Kg0.30 Soluble11.3 J 9056
☼Nitrate 0.25 mg/Kg0.11 Soluble11.4 9056
☼Sulfate 5.1 mg/Kg0.24 Soluble13.8 J 9056
pH 0.100 SU0.100 Soluble18.03 9045C
Oxidation Reduction Potential 0.10 millivolts0.10 Soluble1480 SM 2580B
Client Sample ID: EPAZ5S17S00 Lab Sample ID: 320-4071-9
☼Diesel Range Organics (C10-C24)
RL
0.99 mg/Kg
MDL
0.30
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA13.4 8015B
☼Fluoride 2.5 mg/Kg0.30 Soluble11.3 J 9056
☼Nitrate 0.49 mg/Kg0.22 Soluble251 9056
☼Sulfate 4.9 mg/Kg0.24 Soluble115 9056
☼Perchlorate 5.0 ug/Kg0.26 Total/NA13.8 J 6850
pH 0.100 SU0.100 Soluble16.18 9045C
Oxidation Reduction Potential 0.10 millivolts0.10 Soluble1510 SM 2580B
Client Sample ID: EPAZ5S18S00 Lab Sample ID: 320-4071-10
☼Diesel Range Organics (C10-C24)
RL
1.0 mg/Kg
MDL
0.31
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.92 8015B
☼Fluoride 2.5 mg/Kg0.30 Soluble10.86 J 9056
☼Nitrate 0.25 mg/Kg0.11 Soluble13.9 9056
☼Sulfate 5.0 mg/Kg0.24 Soluble17.6 9056
☼Perchlorate 4.8 ug/Kg0.25 Total/NA10.99 J 6850
pH 0.100 SU0.100 Soluble16.66 9045C
Oxidation Reduction Potential 0.10 millivolts0.10 Soluble1520 SM 2580B
TestAmerica Sacramento
This Detection Summary does not include radiochemical test results.
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Client Sample ResultsTestAmerica Job ID: 320-4071-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Lab Sample ID: 320-4071-1Client Sample ID: EPAZ5MW5S00Matrix: SolidDate Collected: 09/13/13 00:00
Percent Solids: 99.6Date Received: 09/14/13 09:10
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MSRL MDL
Gasoline Range Organics (GRO)
-C7-C12
ND H 0.48 0.048 mg/Kg ☼ 09/16/13 10:11 09/17/13 15:05 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromofluorobenzene (Surr) 103 70 - 131 09/16/13 10:11 09/17/13 15:05 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8015B - Diesel Range Organics (DRO) (GC)RL MDL
Diesel Range Organics (C10-C24) 12 0.99 0.30 mg/Kg ☼ 09/18/13 09:44 09/30/13 17:02 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
o-Terphenyl (Surr) 108 63 - 141 09/18/13 09:44 09/30/13 17:02 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 7199 - Chromium, Hexavalent (IC)RL MDL
Cr (VI) ND 0.80 0.15 mg/Kg ☼ 09/19/13 13:40 09/20/13 21:44 10
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 9056 - Anions, Ion Chromatography - SolubleRL MDL
Fluoride 1.4 J 2.5 0.30 mg/Kg ☼ 10/01/13 19:46 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.25 0.11 mg/Kg 10/01/13 19:46 1☼Nitrate 49
10 0.48 mg/Kg 10/02/13 16:12 2☼Sulfate 360
Method: 6850 - Perchlorate by LC/MS or LC/MS/MS - DLRL MDL
Perchlorate 290 50 2.6 ug/Kg ☼ 10/01/13 08:31 10/07/13 14:02 10
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 8321A - Benzene Sulfonic Acids (LCMS)RL MDL
p-CBSA ND 9.9 0.87 ug/Kg ☼ 09/26/13 07:18 09/28/13 08:08 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromobenzenesulfonic Acid 87 70 - 130 09/26/13 07:18 09/28/13 08:08 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: GCMSMS_NDMA - Nitrosamines by Isotope Dilution and GC/CI/MS/MSRL MDL
N-Nitrosodimethylamine ND 5.2 0.79 ug/Kg ☼ 09/18/13 09:28 10/02/13 04:04 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
N-Nitrosodimethylamine-d6 67 50 - 150 09/18/13 09:28 10/02/13 04:04 1
Isotope Dilution Dil FacAnalyzedPreparedQualifier Limits%Recovery
General Chemistry - SolubleRL MDL
pH 7.92 0.100 0.100 SU 09/20/13 14:30 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.10 0.10 millivolts 09/20/13 12:08 1Oxidation Reduction Potential 460
Lab Sample ID: 320-4071-2Client Sample ID: EPAZ5MW5S3Matrix: WaterDate Collected: 09/13/13 13:30
Date Received: 09/14/13 09:10
Method: 6850 - Perchlorate by LC/MS or LC/MS/MSRL MDL
Perchlorate ND 0.50 0.082 ug/L 09/30/13 09:37 10/02/13 21:06 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
TestAmerica Sacramento
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Client Sample ResultsTestAmerica Job ID: 320-4071-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Lab Sample ID: 320-4071-2Client Sample ID: EPAZ5MW5S3Matrix: WaterDate Collected: 09/13/13 13:30
Date Received: 09/14/13 09:10
Method: GCMSMS_NDMA - Nitrosamines by Isotope Dilution and GC/CI/MS/MSRL MDL
N-Nitrosodimethylamine ND 1.9 0.37 ng/L 09/20/13 09:28 09/24/13 20:12 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
N-Nitrosodimethylamine-d6 34 25 - 150 09/20/13 09:28 09/24/13 20:12 1
Isotope Dilution Dil FacAnalyzedPreparedQualifier Limits%Recovery
Lab Sample ID: 320-4071-3Client Sample ID: EPAZ5MW9S00Matrix: SolidDate Collected: 09/13/13 10:30
Percent Solids: 98.2Date Received: 09/14/13 09:10
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MSRL MDL
Gasoline Range Organics (GRO)
-C7-C12
ND H 0.54 0.054 mg/Kg ☼ 09/16/13 10:11 09/17/13 15:28 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromofluorobenzene (Surr) 103 70 - 131 09/16/13 10:11 09/17/13 15:28 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8015B - Diesel Range Organics (DRO) (GC)RL MDL
Diesel Range Organics (C10-C24) 5.0 1.0 0.30 mg/Kg ☼ 09/18/13 09:44 09/30/13 17:33 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
o-Terphenyl (Surr) 103 63 - 141 09/18/13 09:44 09/30/13 17:33 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 7199 - Chromium, Hexavalent (IC)RL MDL
Cr (VI) ND 0.81 0.15 mg/Kg ☼ 09/19/13 13:40 09/20/13 21:57 10
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 9056 - Anions, Ion Chromatography - SolubleRL MDL
Fluoride 1.6 J 2.5 0.30 mg/Kg ☼ 10/01/13 19:58 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.25 0.11 mg/Kg 10/01/13 19:58 1☼Nitrate 9.9
5.1 0.24 mg/Kg 10/01/13 19:58 1☼Sulfate 150
Method: 6850 - Perchlorate by LC/MS or LC/MS/MS - RARL MDL
Perchlorate 28 5.0 0.26 ug/Kg ☼ 10/01/13 08:31 10/07/13 14:19 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 8321A - Benzene Sulfonic Acids (LCMS)RL MDL
p-CBSA ND 10 0.89 ug/Kg ☼ 09/26/13 07:18 09/28/13 08:26 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromobenzenesulfonic Acid 97 70 - 130 09/26/13 07:18 09/28/13 08:26 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: GCMSMS_NDMA - Nitrosamines by Isotope Dilution and GC/CI/MS/MSRL MDL
N-Nitrosodimethylamine ND 4.9 0.74 ug/Kg ☼ 09/18/13 09:28 10/02/13 04:41 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
N-Nitrosodimethylamine-d6 60 50 - 150 09/18/13 09:28 10/02/13 04:41 1
Isotope Dilution Dil FacAnalyzedPreparedQualifier Limits%Recovery
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Client Sample ResultsTestAmerica Job ID: 320-4071-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Lab Sample ID: 320-4071-3Client Sample ID: EPAZ5MW9S00Matrix: SolidDate Collected: 09/13/13 10:30
Date Received: 09/14/13 09:10
General Chemistry - SolubleRL MDL
pH 10.3 0.100 0.100 SU 09/20/13 14:45 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.10 0.10 millivolts 09/20/13 12:08 1Oxidation Reduction Potential 330
Lab Sample ID: 320-4071-4Client Sample ID: EPAZ5S15S00Matrix: SolidDate Collected: 09/13/13 08:54
Percent Solids: 99.3Date Received: 09/14/13 09:10
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MSRL MDL
Gasoline Range Organics (GRO)
-C7-C12
ND H 0.56 0.056 mg/Kg ☼ 09/16/13 10:11 09/17/13 15:51 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromofluorobenzene (Surr) 100 70 - 131 09/16/13 10:11 09/17/13 15:51 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8015B - Diesel Range Organics (DRO) (GC)RL MDL
Diesel Range Organics (C10-C24) 13 0.99 0.30 mg/Kg ☼ 09/18/13 09:44 09/30/13 18:03 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
o-Terphenyl (Surr) 115 63 - 141 09/18/13 09:44 09/30/13 18:03 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 7199 - Chromium, Hexavalent (IC)RL MDL
Cr (VI) ND 0.81 0.15 mg/Kg ☼ 09/19/13 13:40 09/20/13 22:10 10
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 9056 - Anions, Ion Chromatography - SolubleRL MDL
Fluoride 2.5 2.5 0.30 mg/Kg ☼ 10/01/13 20:09 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.25 0.11 mg/Kg 10/01/13 20:09 1☼Nitrate 6.1
5.0 0.24 mg/Kg 10/01/13 20:09 1☼Sulfate 17
Method: 6850 - Perchlorate by LC/MS or LC/MS/MS - RARL MDL
Perchlorate 4.2 J 5.0 0.26 ug/Kg ☼ 10/01/13 08:31 10/07/13 14:35 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 8321A - Benzene Sulfonic Acids (LCMS)RL MDL
p-CBSA ND 10 0.88 ug/Kg ☼ 09/26/13 07:18 09/28/13 08:45 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromobenzenesulfonic Acid 85 70 - 130 09/26/13 07:18 09/28/13 08:45 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: GCMSMS_NDMA - Nitrosamines by Isotope Dilution and GC/CI/MS/MSRL MDL
N-Nitrosodimethylamine ND 5.2 0.79 ug/Kg ☼ 09/18/13 09:28 10/02/13 07:07 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
N-Nitrosodimethylamine-d6 72 50 - 150 09/18/13 09:28 10/02/13 07:07 1
Isotope Dilution Dil FacAnalyzedPreparedQualifier Limits%Recovery
General Chemistry - SolubleRL MDL
pH 7.37 0.100 0.100 SU 09/20/13 14:30 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
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Client Sample ResultsTestAmerica Job ID: 320-4071-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Lab Sample ID: 320-4071-4Client Sample ID: EPAZ5S15S00Matrix: SolidDate Collected: 09/13/13 08:54
Date Received: 09/14/13 09:10
General Chemistry - Soluble (Continued)RL MDL
Oxidation Reduction Potential 400 0.10 0.10 millivolts 09/20/13 12:08 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Lab Sample ID: 320-4071-5Client Sample ID: EPAZ5S15S03Matrix: SolidDate Collected: 09/13/13 09:25
Percent Solids: 95.6Date Received: 09/14/13 09:10
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MSRL MDL
Gasoline Range Organics (GRO)
-C7-C12
ND H 0.51 0.051 mg/Kg ☼ 09/16/13 10:11 09/17/13 16:15 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromofluorobenzene (Surr) 103 70 - 131 09/16/13 10:11 09/17/13 16:15 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8015B - Diesel Range Organics (DRO) (GC)RL MDL
Diesel Range Organics (C10-C24) 0.80 J 1.0 0.31 mg/Kg ☼ 09/18/13 09:44 09/30/13 18:33 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
o-Terphenyl (Surr) 96 63 - 141 09/18/13 09:44 09/30/13 18:33 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 7199 - Chromium, Hexavalent (IC)RL MDL
Cr (VI) ND 0.83 0.16 mg/Kg ☼ 09/19/13 13:40 09/20/13 22:22 10
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 9056 - Anions, Ion Chromatography - SolubleRL MDL
Fluoride 1.0 J 2.5 0.31 mg/Kg ☼ 10/01/13 20:21 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.25 0.11 mg/Kg 10/01/13 20:21 1☼Nitrate 0.54
5.1 0.24 mg/Kg 10/01/13 20:21 1☼Sulfate 1.1 J
Method: 6850 - Perchlorate by LC/MS or LC/MS/MSRL MDL
Perchlorate ND 5.2 0.27 ug/Kg ☼ 10/01/13 08:31 10/03/13 20:52 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 8321A - Benzene Sulfonic Acids (LCMS)RL MDL
p-CBSA ND 10 0.91 ug/Kg ☼ 09/26/13 07:18 09/28/13 09:04 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromobenzenesulfonic Acid 96 70 - 130 09/26/13 07:18 09/28/13 09:04 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: GCMSMS_NDMA - Nitrosamines by Isotope Dilution and GC/CI/MS/MSRL MDL
N-Nitrosodimethylamine ND 5.6 0.85 ug/Kg ☼ 09/18/13 09:28 10/02/13 07:44 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
N-Nitrosodimethylamine-d6 90 50 - 150 09/18/13 09:28 10/02/13 07:44 1
Isotope Dilution Dil FacAnalyzedPreparedQualifier Limits%Recovery
General Chemistry - SolubleRL MDL
pH 7.78 0.100 0.100 SU 09/20/13 14:30 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.10 0.10 millivolts 09/20/13 12:08 1Oxidation Reduction Potential 490
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Client Sample ResultsTestAmerica Job ID: 320-4071-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Lab Sample ID: 320-4071-6Client Sample ID: EPAZ5S16S00Matrix: SolidDate Collected: 09/13/13 07:45
Percent Solids: 99.1Date Received: 09/14/13 09:10
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MSRL MDL
Gasoline Range Organics (GRO)
-C7-C12
ND H 0.72 0.072 mg/Kg ☼ 09/16/13 10:11 09/17/13 16:38 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromofluorobenzene (Surr) 101 70 - 131 09/16/13 10:11 09/17/13 16:38 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8015B - Diesel Range Organics (DRO) (GC)RL MDL
Diesel Range Organics (C10-C24) 6.8 0.99 0.30 mg/Kg ☼ 09/18/13 09:44 09/30/13 20:35 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
o-Terphenyl (Surr) 127 63 - 141 09/18/13 09:44 09/30/13 20:35 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 7199 - Chromium, Hexavalent (IC)RL MDL
Cr (VI) ND 0.80 0.15 mg/Kg ☼ 09/19/13 13:40 09/20/13 23:00 10
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 9056 - Anions, Ion Chromatography - SolubleRL MDL
Fluoride 1.2 J 2.4 0.29 mg/Kg ☼ 10/01/13 20:32 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.24 0.11 mg/Kg 10/01/13 20:32 1☼Nitrate 22
4.9 0.23 mg/Kg 10/01/13 20:32 1☼Sulfate 6.5
Method: 6850 - Perchlorate by LC/MS or LC/MS/MSRL MDL
Perchlorate 2.4 J 5.0 0.26 ug/Kg ☼ 10/01/13 08:31 10/03/13 21:09 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 8321A - Benzene Sulfonic Acids (LCMS)RL MDL
p-CBSA ND 10 0.89 ug/Kg ☼ 09/26/13 07:18 09/28/13 09:22 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromobenzenesulfonic Acid 102 70 - 130 09/26/13 07:18 09/28/13 09:22 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: GCMSMS_NDMA - Nitrosamines by Isotope Dilution and GC/CI/MS/MSRL MDL
N-Nitrosodimethylamine ND 5.0 0.77 ug/Kg ☼ 09/18/13 09:28 10/02/13 08:20 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
N-Nitrosodimethylamine-d6 72 50 - 150 09/18/13 09:28 10/02/13 08:20 1
Isotope Dilution Dil FacAnalyzedPreparedQualifier Limits%Recovery
General Chemistry - SolubleRL MDL
pH 6.70 0.100 0.100 SU 09/20/13 14:30 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.10 0.10 millivolts 09/20/13 12:08 1Oxidation Reduction Potential 500
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Client Sample ResultsTestAmerica Job ID: 320-4071-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Lab Sample ID: 320-4071-7Client Sample ID: EPAZ5S16S03Matrix: SolidDate Collected: 09/13/13 08:50
Percent Solids: 96.5Date Received: 09/14/13 09:10
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MSRL MDL
Gasoline Range Organics (GRO)
-C7-C12
ND H 0.51 0.051 mg/Kg ☼ 09/16/13 10:11 09/17/13 17:01 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromofluorobenzene (Surr) 102 70 - 131 09/16/13 10:11 09/17/13 17:01 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8015B - Diesel Range Organics (DRO) (GC)RL MDL
Diesel Range Organics (C10-C24) 1.1 1.0 0.30 mg/Kg ☼ 09/18/13 09:44 09/30/13 21:06 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
o-Terphenyl (Surr) 101 63 - 141 09/18/13 09:44 09/30/13 21:06 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 7199 - Chromium, Hexavalent (IC)RL MDL
Cr (VI) ND 0.83 0.16 mg/Kg ☼ 09/19/13 13:40 09/20/13 23:13 10
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 9056 - Anions, Ion Chromatography - SolubleRL MDL
Fluoride 1.3 J 2.6 0.31 mg/Kg ☼ 10/01/13 20:44 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.26 0.11 mg/Kg 10/01/13 20:44 1☼Nitrate 1.3
5.1 0.25 mg/Kg 10/01/13 20:44 1☼Sulfate 2.6 J
Method: 6850 - Perchlorate by LC/MS or LC/MS/MSRL MDL
Perchlorate 0.27 J 4.9 0.26 ug/Kg ☼ 10/01/13 08:31 10/03/13 21:26 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 8321A - Benzene Sulfonic Acids (LCMS)RL MDL
p-CBSA ND 10 0.91 ug/Kg ☼ 09/26/13 07:18 09/28/13 09:41 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromobenzenesulfonic Acid 103 70 - 130 09/26/13 07:18 09/28/13 09:41 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: GCMSMS_NDMA - Nitrosamines by Isotope Dilution and GC/CI/MS/MSRL MDL
N-Nitrosodimethylamine ND 5.1 0.77 ug/Kg ☼ 09/18/13 09:28 10/02/13 08:57 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
N-Nitrosodimethylamine-d6 79 50 - 150 09/18/13 09:28 10/02/13 08:57 1
Isotope Dilution Dil FacAnalyzedPreparedQualifier Limits%Recovery
General Chemistry - SolubleRL MDL
pH 8.13 0.100 0.100 SU 09/20/13 14:30 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.10 0.10 millivolts 09/20/13 12:08 1Oxidation Reduction Potential 470
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Client Sample ResultsTestAmerica Job ID: 320-4071-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Lab Sample ID: 320-4071-8Client Sample ID: EPAZ5S16S13Matrix: SolidDate Collected: 09/13/13 09:10
Percent Solids: 97.4Date Received: 09/14/13 09:10
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MSRL MDL
Gasoline Range Organics (GRO)
-C7-C12
ND H 0.51 0.051 mg/Kg ☼ 09/16/13 10:11 09/17/13 18:34 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromofluorobenzene (Surr) 102 70 - 131 09/16/13 10:11 09/17/13 18:34 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8015B - Diesel Range Organics (DRO) (GC)RL MDL
Diesel Range Organics (C10-C24) 1.2 1.0 0.31 mg/Kg ☼ 09/18/13 09:44 09/30/13 21:36 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
o-Terphenyl (Surr) 106 63 - 141 09/18/13 09:44 09/30/13 21:36 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 7199 - Chromium, Hexavalent (IC)RL MDL
Cr (VI) ND 0.82 0.15 mg/Kg ☼ 09/19/13 13:40 09/20/13 23:26 10
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 9056 - Anions, Ion Chromatography - SolubleRL MDL
Fluoride 1.3 J 2.5 0.30 mg/Kg ☼ 10/01/13 20:55 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.25 0.11 mg/Kg 10/01/13 20:55 1☼Nitrate 1.4
5.1 0.24 mg/Kg 10/01/13 20:55 1☼Sulfate 3.8 J
Method: 6850 - Perchlorate by LC/MS or LC/MS/MSRL MDL
Perchlorate ND 5.2 0.27 ug/Kg ☼ 10/01/13 08:31 10/03/13 21:42 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 8321A - Benzene Sulfonic Acids (LCMS)RL MDL
p-CBSA ND 10 0.90 ug/Kg ☼ 09/26/13 07:18 09/28/13 09:59 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromobenzenesulfonic Acid 102 70 - 130 09/26/13 07:18 09/28/13 09:59 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: GCMSMS_NDMA - Nitrosamines by Isotope Dilution and GC/CI/MS/MSRL MDL
N-Nitrosodimethylamine ND 4.8 0.72 ug/Kg ☼ 09/18/13 09:28 10/02/13 09:33 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
N-Nitrosodimethylamine-d6 71 50 - 150 09/18/13 09:28 10/02/13 09:33 1
Isotope Dilution Dil FacAnalyzedPreparedQualifier Limits%Recovery
General Chemistry - SolubleRL MDL
pH 8.03 0.100 0.100 SU 09/20/13 14:30 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.10 0.10 millivolts 09/20/13 12:08 1Oxidation Reduction Potential 480
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Client Sample ResultsTestAmerica Job ID: 320-4071-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Lab Sample ID: 320-4071-9Client Sample ID: EPAZ5S17S00Matrix: SolidDate Collected: 09/13/13 07:50
Percent Solids: 99.8Date Received: 09/14/13 09:10
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MSRL MDL
Gasoline Range Organics (GRO)
-C7-C12
ND H 0.63 0.063 mg/Kg ☼ 09/16/13 10:11 09/17/13 18:58 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromofluorobenzene (Surr) 100 70 - 131 09/16/13 10:11 09/17/13 18:58 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8015B - Diesel Range Organics (DRO) (GC)RL MDL
Diesel Range Organics (C10-C24) 3.4 0.99 0.30 mg/Kg ☼ 09/18/13 09:44 09/30/13 22:07 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
o-Terphenyl (Surr) 115 63 - 141 09/18/13 09:44 09/30/13 22:07 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 7199 - Chromium, Hexavalent (IC)RL MDL
Cr (VI) ND 0.81 0.15 mg/Kg ☼ 09/19/13 13:40 09/20/13 23:38 10
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 9056 - Anions, Ion Chromatography - SolubleRL MDL
Fluoride 1.3 J 2.5 0.30 mg/Kg ☼ 10/01/13 21:07 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.49 0.22 mg/Kg 10/02/13 16:23 2☼Nitrate 51
4.9 0.24 mg/Kg 10/01/13 21:07 1☼Sulfate 15
Method: 6850 - Perchlorate by LC/MS or LC/MS/MSRL MDL
Perchlorate 3.8 J 5.0 0.26 ug/Kg ☼ 10/01/13 08:31 10/03/13 21:59 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 8321A - Benzene Sulfonic Acids (LCMS)RL MDL
p-CBSA ND 10 0.88 ug/Kg ☼ 09/26/13 07:18 09/28/13 10:18 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromobenzenesulfonic Acid 99 70 - 130 09/26/13 07:18 09/28/13 10:18 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: GCMSMS_NDMA - Nitrosamines by Isotope Dilution and GC/CI/MS/MSRL MDL
N-Nitrosodimethylamine ND 5.2 0.79 ug/Kg ☼ 09/18/13 09:28 10/02/13 10:09 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
N-Nitrosodimethylamine-d6 77 50 - 150 09/18/13 09:28 10/02/13 10:09 1
Isotope Dilution Dil FacAnalyzedPreparedQualifier Limits%Recovery
General Chemistry - SolubleRL MDL
pH 6.18 0.100 0.100 SU 09/20/13 14:30 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.10 0.10 millivolts 09/20/13 12:08 1Oxidation Reduction Potential 510
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Client Sample ResultsTestAmerica Job ID: 320-4071-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Lab Sample ID: 320-4071-10Client Sample ID: EPAZ5S18S00Matrix: SolidDate Collected: 09/13/13 00:00
Percent Solids: 98.9Date Received: 09/14/13 09:10
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MSRL MDL
Gasoline Range Organics (GRO)
-C7-C12
ND H 0.57 0.057 mg/Kg ☼ 09/16/13 10:11 09/17/13 19:21 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromofluorobenzene (Surr) 101 70 - 131 09/16/13 10:11 09/17/13 19:21 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 8015B - Diesel Range Organics (DRO) (GC)RL MDL
Diesel Range Organics (C10-C24) 0.92 J 1.0 0.31 mg/Kg ☼ 09/18/13 09:44 09/30/13 22:37 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
o-Terphenyl (Surr) 103 63 - 141 09/18/13 09:44 09/30/13 22:37 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: 7199 - Chromium, Hexavalent (IC)RL MDL
Cr (VI) ND 0.81 0.15 mg/Kg ☼ 09/19/13 13:40 09/20/13 23:51 10
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 9056 - Anions, Ion Chromatography - SolubleRL MDL
Fluoride 0.86 J 2.5 0.30 mg/Kg ☼ 10/01/13 21:18 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.25 0.11 mg/Kg 10/01/13 21:18 1☼Nitrate 3.9
5.0 0.24 mg/Kg 10/01/13 21:18 1☼Sulfate 7.6
Method: 6850 - Perchlorate by LC/MS or LC/MS/MSRL MDL
Perchlorate 0.99 J 4.8 0.25 ug/Kg ☼ 10/01/13 08:31 10/03/13 22:16 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Method: 8321A - Benzene Sulfonic Acids (LCMS)RL MDL
p-CBSA ND 10 0.88 ug/Kg ☼ 09/26/13 07:18 09/28/13 10:36 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
4-Bromobenzenesulfonic Acid 104 70 - 130 09/26/13 07:18 09/28/13 10:36 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Method: GCMSMS_NDMA - Nitrosamines by Isotope Dilution and GC/CI/MS/MSRL MDL
N-Nitrosodimethylamine ND 4.9 0.74 ug/Kg ☼ 09/18/13 09:28 10/02/13 10:46 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
N-Nitrosodimethylamine-d6 79 50 - 150 09/18/13 09:28 10/02/13 10:46 1
Isotope Dilution Dil FacAnalyzedPreparedQualifier Limits%Recovery
General Chemistry - SolubleRL MDL
pH 6.66 0.100 0.100 SU 09/20/13 14:30 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
0.10 0.10 millivolts 09/20/13 12:08 1Oxidation Reduction Potential 520
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Surrogate SummaryTestAmerica Job ID: 320-4071-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MSPrep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (70-131)
BFB
103320-4071-1
Percent Surrogate Recovery (Acceptance Limits)
EPAZ5MW5S00
103320-4071-3 EPAZ5MW9S00
100320-4071-4 EPAZ5S15S00
103320-4071-5 EPAZ5S15S03
101320-4071-6 EPAZ5S16S00
102320-4071-7 EPAZ5S16S03
102320-4071-8 EPAZ5S16S13
100320-4071-9 EPAZ5S17S00
101320-4071-10 EPAZ5S18S00
104LCS 320-25274/7 Lab Control Sample
104MB 320-25274/11 Method Blank
Surrogate Legend
BFB = 4-Bromofluorobenzene (Surr)
Method: 8015B - Diesel Range Organics (DRO) (GC)Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (63-141)
OTPH1
108320-4071-1
Percent Surrogate Recovery (Acceptance Limits)
EPAZ5MW5S00
103320-4071-3 EPAZ5MW9S00
115320-4071-4 EPAZ5S15S00
96320-4071-5 EPAZ5S15S03
127320-4071-6 EPAZ5S16S00
101320-4071-7 EPAZ5S16S03
106320-4071-8 EPAZ5S16S13
115320-4071-9 EPAZ5S17S00
103320-4071-10 EPAZ5S18S00
101LCS 320-25407/2-A Lab Control Sample
97MB 320-25407/1-A Method Blank
Surrogate Legend
OTPH = o-Terphenyl (Surr)
Method: 8321A - Benzene Sulfonic Acids (LCMS)Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (70-130)
4-Bromobenzenesulfonic Acid
87320-4071-1
Percent Surrogate Recovery (Acceptance Limits)
EPAZ5MW5S00
97320-4071-3 EPAZ5MW9S00
85320-4071-4 EPAZ5S15S00
96320-4071-5 EPAZ5S15S03
102320-4071-6 EPAZ5S16S00
103320-4071-7 EPAZ5S16S03
102320-4071-8 EPAZ5S16S13
99320-4071-9 EPAZ5S17S00
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Surrogate SummaryTestAmerica Job ID: 320-4071-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Method: 8321A - Benzene Sulfonic Acids (LCMS) (Continued)Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (70-130)
4-Bromobenzenesulfonic Acid
104320-4071-10
Percent Surrogate Recovery (Acceptance Limits)
EPAZ5S18S00
100LCS 320-26024/2-A Lab Control Sample
122MB 320-26024/1-A Method Blank
Surrogate Legend
4-Bromobenzenesulfonic Acid = 4-Bromobenzenesulfonic Acid
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Isotope Dilution SummaryTestAmerica Job ID: 320-4071-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Method: GCMSMS_NDMA - Nitrosamines by Isotope Dilution and GC/CI/MS/MSPrep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (50-150)
NDMA
67320-4071-1
Percent Isotope Dilution Recovery (Acceptance Limits)
EPAZ5MW5S00
60320-4071-3 EPAZ5MW9S00
72320-4071-4 EPAZ5S15S00
90320-4071-5 EPAZ5S15S03
72320-4071-6 EPAZ5S16S00
79320-4071-7 EPAZ5S16S03
71320-4071-8 EPAZ5S16S13
77320-4071-9 EPAZ5S17S00
79320-4071-10 EPAZ5S18S00
78LCS 320-25404/2-A Lab Control Sample
96MB 320-25404/1-A Method Blank
Surrogate Legend
NDMA = N-Nitrosodimethylamine-d6
Method: GCMSMS_NDMA - Nitrosamines by Isotope Dilution and GC/CI/MS/MSPrep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (25-150)
NDMA
34320-4071-2
Percent Isotope Dilution Recovery (Acceptance Limits)
EPAZ5MW5S3
49LCS 320-25607/2-A Lab Control Sample
43MB 320-25607/1-A Method Blank
Surrogate Legend
NDMA = N-Nitrosodimethylamine-d6
TestAmerica Sacramento
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QC Sample ResultsTestAmerica Job ID: 320-4071-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MS
Client Sample ID: Method BlankLab Sample ID: MB 320-25274/11
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 25274
RL MDL
Gasoline Range Organics (GRO)
-C7-C12
ND 0.50 0.050 mg/Kg 09/17/13 13:08 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
4-Bromofluorobenzene (Surr) 104 70 - 131 09/17/13 13:08 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 320-25274/7
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 25274
Gasoline Range Organics (GRO)
-C7-C12
1.00 0.919 mg/Kg 92 79 - 123
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
4-Bromofluorobenzene (Surr) 70 - 131
Surrogate
104
LCS LCS
Qualifier Limits%Recovery
Method: 8015B - Diesel Range Organics (DRO) (GC)
Client Sample ID: Method BlankLab Sample ID: MB 320-25407/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 26290 Prep Batch: 25407
RL MDL
Diesel Range Organics (C10-C24) ND 1.0 0.30 mg/Kg 09/18/13 09:44 09/30/13 11:58 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
o-Terphenyl (Surr) 97 63 - 141 09/30/13 11:58 1
MB MB
Surrogate
09/18/13 09:44
Dil FacPrepared AnalyzedQualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 320-25407/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 26290 Prep Batch: 25407
Diesel Range Organics
(C10-C24)
10.0 9.92 mg/Kg 99 67 - 113
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
o-Terphenyl (Surr) 63 - 141
Surrogate
101
LCS LCS
Qualifier Limits%Recovery
TestAmerica Sacramento
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QC Sample ResultsTestAmerica Job ID: 320-4071-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Method: 7199 - Chromium, Hexavalent (IC)
Client Sample ID: Method BlankLab Sample ID: MB 440-132189/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 132325 Prep Batch: 132189
RL MDL
Cr (VI) ND 0.80 0.15 mg/Kg 09/19/13 13:40 09/20/13 08:41 10
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 440-132189/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 132325 Prep Batch: 132189
Cr (VI) 15.9 12.0 mg/Kg 76 65 - 110
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Method: 9056 - Anions, Ion Chromatography
Client Sample ID: Method BlankLab Sample ID: MB 320-26456/1-A
Matrix: Solid Prep Type: Soluble
Analysis Batch: 26521
RL MDL
Fluoride ND 2.5 0.30 mg/Kg 10/01/13 17:17 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.245.0 mg/Kg 10/01/13 17:17 1Sulfate
Client Sample ID: Lab Control SampleLab Sample ID: LCS 320-26456/2-A
Matrix: Solid Prep Type: Soluble
Analysis Batch: 26521
Fluoride 25.0 26.8 mg/Kg 107 85 - 115
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Sulfate 25.0 27.9 mg/Kg 112 85 - 115
Client Sample ID: Method BlankLab Sample ID: MB 320-26456/1-A
Matrix: Solid Prep Type: Soluble
Analysis Batch: 26522
RL MDL
Nitrate ND 0.25 0.11 mg/Kg 10/01/13 17:17 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 320-26456/2-A
Matrix: Solid Prep Type: Soluble
Analysis Batch: 26522
Nitrate 5.00 5.34 mg/Kg 107 85 - 115
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Method: 6850 - Perchlorate by LC/MS or LC/MS/MS
Client Sample ID: Method BlankLab Sample ID: MB 320-26279/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 26429 Prep Batch: 26279
RL MDL
Perchlorate ND 0.50 0.082 ug/L 09/30/13 09:37 10/02/13 19:25 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
TestAmerica Sacramento
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QC Sample ResultsTestAmerica Job ID: 320-4071-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Method: 6850 - Perchlorate by LC/MS or LC/MS/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 320-26279/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 26429 Prep Batch: 26279
Perchlorate 5.00 5.11 ug/L 102 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Method BlankLab Sample ID: MB 320-26394/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 26675 Prep Batch: 26394
RL MDL
Perchlorate ND 5.0 0.26 ug/Kg 10/01/13 08:31 10/03/13 18:55 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 320-26394/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 26675 Prep Batch: 26394
Perchlorate 50.0 53.0 ug/Kg 106 80 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
Method: 8321A - Benzene Sulfonic Acids (LCMS)
Client Sample ID: Method BlankLab Sample ID: MB 320-26024/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 26161 Prep Batch: 26024
RL MDL
p-CBSA ND 10 0.88 ug/Kg 09/26/13 07:18 09/28/13 04:44 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
4-Bromobenzenesulfonic Acid 122 70 - 130 09/28/13 04:44 1
MB MB
Surrogate
09/26/13 07:18
Dil FacPrepared AnalyzedQualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 320-26024/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 26161 Prep Batch: 26024
p-CBSA 50.0 56.9 ug/Kg 114 70 - 130
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
4-Bromobenzenesulfonic Acid 70 - 130
Surrogate
100
LCS LCS
Qualifier Limits%Recovery
Method: GCMSMS_NDMA - Nitrosamines by Isotope Dilution and GC/CI/MS/MS
Client Sample ID: Method BlankLab Sample ID: MB 320-25404/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 26498 Prep Batch: 25404
RL MDL
N-Nitrosodimethylamine ND 5.0 0.76 ug/Kg 09/18/13 09:28 10/01/13 22:02 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
TestAmerica Sacramento
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QC Sample ResultsTestAmerica Job ID: 320-4071-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Method: GCMSMS_NDMA - Nitrosamines by Isotope Dilution and GC/CI/MS/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 320-25404/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 26498 Prep Batch: 25404
N-Nitrosodimethylamine-d6 96 50 - 150 10/01/13 22:02 1
MB MB
Isotope Dilution
09/18/13 09:28
Dil FacPrepared AnalyzedQualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 320-25404/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 26498 Prep Batch: 25404
N-Nitrosodimethylamine 5.00 5.86 ug/Kg 117 70 - 130
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
N-Nitrosodimethylamine-d6 50 - 150
Isotope Dilution
78
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Method BlankLab Sample ID: MB 320-25607/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 25889 Prep Batch: 25607
RL MDL
N-Nitrosodimethylamine ND 2.0 0.39 ng/L 09/20/13 09:28 09/24/13 18:23 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
N-Nitrosodimethylamine-d6 43 25 - 150 09/24/13 18:23 1
MB MB
Isotope Dilution
09/20/13 09:28
Dil FacPrepared AnalyzedQualifier Limits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 320-25607/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 26020 Prep Batch: 25607
N-Nitrosodimethylamine 20.0 26.0 ng/L 130 58 - 150
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec.
Limits
N-Nitrosodimethylamine-d6 25 - 150
Isotope Dilution
49
LCS LCS
Qualifier Limits%Recovery
Method: 9045C - pH
Client Sample ID: EPAZ5MW5S00Lab Sample ID: 320-4071-1 DU
Matrix: Solid Prep Type: Soluble
Analysis Batch: 132475
pH 7.92 7.940 SU 0.3 2
Analyte
DU DU
DUnitResult Qualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Method: SM 2580B - Reduction-Oxidation (REDOX) Potential
Client Sample ID: EPAZ5MW5S00Lab Sample ID: 320-4071-1 DU
Matrix: Solid Prep Type: Soluble
Analysis Batch: 132478
Oxidation Reduction Potential 460 454 millivolts 0.9 5
Analyte
DU DU
DUnitResult Qualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
TestAmerica Sacramento
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QC Association SummaryTestAmerica Job ID: 320-4071-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
GC/MS VOA
Prep Batch: 25193
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 5035320-4071-1 EPAZ5MW5S00 Total/NA
Solid 5035320-4071-3 EPAZ5MW9S00 Total/NA
Solid 5035320-4071-4 EPAZ5S15S00 Total/NA
Solid 5035320-4071-5 EPAZ5S15S03 Total/NA
Solid 5035320-4071-6 EPAZ5S16S00 Total/NA
Solid 5035320-4071-7 EPAZ5S16S03 Total/NA
Solid 5035320-4071-8 EPAZ5S16S13 Total/NA
Solid 5035320-4071-9 EPAZ5S17S00 Total/NA
Solid 5035320-4071-10 EPAZ5S18S00 Total/NA
Analysis Batch: 25274
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8260B/CA_LUFT
MS
25193320-4071-1 EPAZ5MW5S00 Total/NA
Solid 8260B/CA_LUFT
MS
25193320-4071-3 EPAZ5MW9S00 Total/NA
Solid 8260B/CA_LUFT
MS
25193320-4071-4 EPAZ5S15S00 Total/NA
Solid 8260B/CA_LUFT
MS
25193320-4071-5 EPAZ5S15S03 Total/NA
Solid 8260B/CA_LUFT
MS
25193320-4071-6 EPAZ5S16S00 Total/NA
Solid 8260B/CA_LUFT
MS
25193320-4071-7 EPAZ5S16S03 Total/NA
Solid 8260B/CA_LUFT
MS
25193320-4071-8 EPAZ5S16S13 Total/NA
Solid 8260B/CA_LUFT
MS
25193320-4071-9 EPAZ5S17S00 Total/NA
Solid 8260B/CA_LUFT
MS
25193320-4071-10 EPAZ5S18S00 Total/NA
Solid 8260B/CA_LUFT
MS
LCS 320-25274/7 Lab Control Sample Total/NA
Solid 8260B/CA_LUFT
MS
MB 320-25274/11 Method Blank Total/NA
GC Semi VOA
Prep Batch: 25407
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3550B320-4071-1 EPAZ5MW5S00 Total/NA
Solid 3550B320-4071-3 EPAZ5MW9S00 Total/NA
Solid 3550B320-4071-4 EPAZ5S15S00 Total/NA
Solid 3550B320-4071-5 EPAZ5S15S03 Total/NA
Solid 3550B320-4071-6 EPAZ5S16S00 Total/NA
Solid 3550B320-4071-7 EPAZ5S16S03 Total/NA
Solid 3550B320-4071-8 EPAZ5S16S13 Total/NA
Solid 3550B320-4071-9 EPAZ5S17S00 Total/NA
Solid 3550B320-4071-10 EPAZ5S18S00 Total/NA
Solid 3550BLCS 320-25407/2-A Lab Control Sample Total/NA
Solid 3550BMB 320-25407/1-A Method Blank Total/NA
TestAmerica Sacramento
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QC Association SummaryTestAmerica Job ID: 320-4071-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
GC Semi VOA (Continued)
Analysis Batch: 26290
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8015B 25407320-4071-1 EPAZ5MW5S00 Total/NA
Solid 8015B 25407320-4071-3 EPAZ5MW9S00 Total/NA
Solid 8015B 25407320-4071-4 EPAZ5S15S00 Total/NA
Solid 8015B 25407320-4071-5 EPAZ5S15S03 Total/NA
Solid 8015B 25407320-4071-6 EPAZ5S16S00 Total/NA
Solid 8015B 25407320-4071-7 EPAZ5S16S03 Total/NA
Solid 8015B 25407320-4071-8 EPAZ5S16S13 Total/NA
Solid 8015B 25407320-4071-9 EPAZ5S17S00 Total/NA
Solid 8015B 25407320-4071-10 EPAZ5S18S00 Total/NA
Solid 8015B 25407LCS 320-25407/2-A Lab Control Sample Total/NA
Solid 8015B 25407MB 320-25407/1-A Method Blank Total/NA
HPLC/IC
Leach Batch: 26456
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid DI Leach320-4071-1 EPAZ5MW5S00 Soluble
Solid DI Leach320-4071-3 EPAZ5MW9S00 Soluble
Solid DI Leach320-4071-4 EPAZ5S15S00 Soluble
Solid DI Leach320-4071-5 EPAZ5S15S03 Soluble
Solid DI Leach320-4071-6 EPAZ5S16S00 Soluble
Solid DI Leach320-4071-7 EPAZ5S16S03 Soluble
Solid DI Leach320-4071-8 EPAZ5S16S13 Soluble
Solid DI Leach320-4071-9 EPAZ5S17S00 Soluble
Solid DI Leach320-4071-10 EPAZ5S18S00 Soluble
Solid DI LeachLCS 320-26456/2-A Lab Control Sample Soluble
Solid DI LeachMB 320-26456/1-A Method Blank Soluble
Analysis Batch: 26521
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 9056 26456320-4071-1 EPAZ5MW5S00 Soluble
Solid 9056 26456320-4071-3 EPAZ5MW9S00 Soluble
Solid 9056 26456320-4071-4 EPAZ5S15S00 Soluble
Solid 9056 26456320-4071-5 EPAZ5S15S03 Soluble
Solid 9056 26456320-4071-6 EPAZ5S16S00 Soluble
Solid 9056 26456320-4071-7 EPAZ5S16S03 Soluble
Solid 9056 26456320-4071-8 EPAZ5S16S13 Soluble
Solid 9056 26456320-4071-9 EPAZ5S17S00 Soluble
Solid 9056 26456320-4071-10 EPAZ5S18S00 Soluble
Solid 9056 26456LCS 320-26456/2-A Lab Control Sample Soluble
Solid 9056 26456MB 320-26456/1-A Method Blank Soluble
Analysis Batch: 26522
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 9056 26456320-4071-1 EPAZ5MW5S00 Soluble
Solid 9056 26456320-4071-3 EPAZ5MW9S00 Soluble
Solid 9056 26456320-4071-4 EPAZ5S15S00 Soluble
Solid 9056 26456320-4071-5 EPAZ5S15S03 Soluble
Solid 9056 26456320-4071-6 EPAZ5S16S00 Soluble
Solid 9056 26456320-4071-7 EPAZ5S16S03 Soluble
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QC Association SummaryTestAmerica Job ID: 320-4071-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
HPLC/IC (Continued)
Analysis Batch: 26522 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 9056 26456320-4071-8 EPAZ5S16S13 Soluble
Solid 9056 26456320-4071-10 EPAZ5S18S00 Soluble
Solid 9056 26456LCS 320-26456/2-A Lab Control Sample Soluble
Solid 9056 26456MB 320-26456/1-A Method Blank Soluble
Analysis Batch: 26942
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 9056 26456320-4071-1 EPAZ5MW5S00 Soluble
Analysis Batch: 26943
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 9056 26456320-4071-9 EPAZ5S17S00 Soluble
Prep Batch: 132189
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3060A320-4071-1 EPAZ5MW5S00 Total/NA
Solid 3060A320-4071-3 EPAZ5MW9S00 Total/NA
Solid 3060A320-4071-4 EPAZ5S15S00 Total/NA
Solid 3060A320-4071-5 EPAZ5S15S03 Total/NA
Solid 3060A320-4071-6 EPAZ5S16S00 Total/NA
Solid 3060A320-4071-7 EPAZ5S16S03 Total/NA
Solid 3060A320-4071-8 EPAZ5S16S13 Total/NA
Solid 3060A320-4071-9 EPAZ5S17S00 Total/NA
Solid 3060A320-4071-10 EPAZ5S18S00 Total/NA
Solid 3060ALCS 440-132189/2-A Lab Control Sample Total/NA
Solid 3060AMB 440-132189/1-A Method Blank Total/NA
Analysis Batch: 132325
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 7199 132189320-4071-1 EPAZ5MW5S00 Total/NA
Solid 7199 132189320-4071-3 EPAZ5MW9S00 Total/NA
Solid 7199 132189320-4071-4 EPAZ5S15S00 Total/NA
Solid 7199 132189320-4071-5 EPAZ5S15S03 Total/NA
Solid 7199 132189320-4071-6 EPAZ5S16S00 Total/NA
Solid 7199 132189320-4071-7 EPAZ5S16S03 Total/NA
Solid 7199 132189320-4071-8 EPAZ5S16S13 Total/NA
Solid 7199 132189320-4071-9 EPAZ5S17S00 Total/NA
Solid 7199 132189320-4071-10 EPAZ5S18S00 Total/NA
Solid 7199 132189LCS 440-132189/2-A Lab Control Sample Total/NA
Solid 7199 132189MB 440-132189/1-A Method Blank Total/NA
LCMS
Prep Batch: 25404
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3550B320-4071-1 EPAZ5MW5S00 Total/NA
Solid 3550B320-4071-3 EPAZ5MW9S00 Total/NA
Solid 3550B320-4071-4 EPAZ5S15S00 Total/NA
Solid 3550B320-4071-5 EPAZ5S15S03 Total/NA
Solid 3550B320-4071-6 EPAZ5S16S00 Total/NA
TestAmerica Sacramento
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QC Association SummaryTestAmerica Job ID: 320-4071-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
LCMS (Continued)
Prep Batch: 25404 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3550B320-4071-7 EPAZ5S16S03 Total/NA
Solid 3550B320-4071-8 EPAZ5S16S13 Total/NA
Solid 3550B320-4071-9 EPAZ5S17S00 Total/NA
Solid 3550B320-4071-10 EPAZ5S18S00 Total/NA
Solid 3550BLCS 320-25404/2-A Lab Control Sample Total/NA
Solid 3550BMB 320-25404/1-A Method Blank Total/NA
Prep Batch: 25607
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3510C320-4071-2 EPAZ5MW5S3 Total/NA
Water 3510CLCS 320-25607/2-A Lab Control Sample Total/NA
Water 3510CMB 320-25607/1-A Method Blank Total/NA
Analysis Batch: 25889
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water GCMSMS_NDM
A
25607320-4071-2 EPAZ5MW5S3 Total/NA
Water GCMSMS_NDM
A
25607MB 320-25607/1-A Method Blank Total/NA
Analysis Batch: 26020
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water GCMSMS_NDM
A
25607LCS 320-25607/2-A Lab Control Sample Total/NA
Prep Batch: 26024
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid SHAKE320-4071-1 EPAZ5MW5S00 Total/NA
Solid SHAKE320-4071-3 EPAZ5MW9S00 Total/NA
Solid SHAKE320-4071-4 EPAZ5S15S00 Total/NA
Solid SHAKE320-4071-5 EPAZ5S15S03 Total/NA
Solid SHAKE320-4071-6 EPAZ5S16S00 Total/NA
Solid SHAKE320-4071-7 EPAZ5S16S03 Total/NA
Solid SHAKE320-4071-8 EPAZ5S16S13 Total/NA
Solid SHAKE320-4071-9 EPAZ5S17S00 Total/NA
Solid SHAKE320-4071-10 EPAZ5S18S00 Total/NA
Solid SHAKELCS 320-26024/2-A Lab Control Sample Total/NA
Solid SHAKEMB 320-26024/1-A Method Blank Total/NA
Analysis Batch: 26161
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8321A 26024320-4071-1 EPAZ5MW5S00 Total/NA
Solid 8321A 26024320-4071-3 EPAZ5MW9S00 Total/NA
Solid 8321A 26024320-4071-4 EPAZ5S15S00 Total/NA
Solid 8321A 26024320-4071-5 EPAZ5S15S03 Total/NA
Solid 8321A 26024320-4071-6 EPAZ5S16S00 Total/NA
Solid 8321A 26024320-4071-7 EPAZ5S16S03 Total/NA
Solid 8321A 26024320-4071-8 EPAZ5S16S13 Total/NA
Solid 8321A 26024320-4071-9 EPAZ5S17S00 Total/NA
Solid 8321A 26024320-4071-10 EPAZ5S18S00 Total/NA
Solid 8321A 26024LCS 320-26024/2-A Lab Control Sample Total/NA
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QC Association SummaryTestAmerica Job ID: 320-4071-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
LCMS (Continued)
Analysis Batch: 26161 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8321A 26024MB 320-26024/1-A Method Blank Total/NA
Prep Batch: 26279
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water Filtration320-4071-2 EPAZ5MW5S3 Total/NA
Water FiltrationLCS 320-26279/2-A Lab Control Sample Total/NA
Water FiltrationMB 320-26279/1-A Method Blank Total/NA
Prep Batch: 26394
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid SHAKE320-4071-1 EPAZ5MW5S00 Total/NA
Solid SHAKE320-4071-1 - DL EPAZ5MW5S00 Total/NA
Solid SHAKE320-4071-3 EPAZ5MW9S00 Total/NA
Solid SHAKE320-4071-3 - RA EPAZ5MW9S00 Total/NA
Solid SHAKE320-4071-4 EPAZ5S15S00 Total/NA
Solid SHAKE320-4071-4 - RA EPAZ5S15S00 Total/NA
Solid SHAKE320-4071-5 EPAZ5S15S03 Total/NA
Solid SHAKE320-4071-6 EPAZ5S16S00 Total/NA
Solid SHAKE320-4071-7 EPAZ5S16S03 Total/NA
Solid SHAKE320-4071-8 EPAZ5S16S13 Total/NA
Solid SHAKE320-4071-9 EPAZ5S17S00 Total/NA
Solid SHAKE320-4071-10 EPAZ5S18S00 Total/NA
Solid SHAKELCS 320-26394/2-A Lab Control Sample Total/NA
Solid SHAKEMB 320-26394/1-A Method Blank Total/NA
Analysis Batch: 26429
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6850 26279320-4071-2 EPAZ5MW5S3 Total/NA
Water 6850 26279LCS 320-26279/2-A Lab Control Sample Total/NA
Water 6850 26279MB 320-26279/1-A Method Blank Total/NA
Analysis Batch: 26498
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid GCMSMS_NDM
A
25404320-4071-1 EPAZ5MW5S00 Total/NA
Solid GCMSMS_NDM
A
25404320-4071-3 EPAZ5MW9S00 Total/NA
Solid GCMSMS_NDM
A
25404320-4071-4 EPAZ5S15S00 Total/NA
Solid GCMSMS_NDM
A
25404320-4071-5 EPAZ5S15S03 Total/NA
Solid GCMSMS_NDM
A
25404320-4071-6 EPAZ5S16S00 Total/NA
Solid GCMSMS_NDM
A
25404320-4071-7 EPAZ5S16S03 Total/NA
Solid GCMSMS_NDM
A
25404320-4071-8 EPAZ5S16S13 Total/NA
Solid GCMSMS_NDM
A
25404320-4071-9 EPAZ5S17S00 Total/NA
Solid GCMSMS_NDM
A
25404320-4071-10 EPAZ5S18S00 Total/NA
Solid GCMSMS_NDM
A
25404LCS 320-25404/2-A Lab Control Sample Total/NA
TestAmerica Sacramento
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QC Association SummaryTestAmerica Job ID: 320-4071-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
LCMS (Continued)
Analysis Batch: 26498 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid GCMSMS_NDM
A
25404MB 320-25404/1-A Method Blank Total/NA
Analysis Batch: 26675
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 6850 26394320-4071-1 EPAZ5MW5S00 Total/NA
Solid 6850 26394320-4071-3 EPAZ5MW9S00 Total/NA
Solid 6850 26394320-4071-4 EPAZ5S15S00 Total/NA
Solid 6850 26394320-4071-5 EPAZ5S15S03 Total/NA
Solid 6850 26394320-4071-6 EPAZ5S16S00 Total/NA
Solid 6850 26394320-4071-7 EPAZ5S16S03 Total/NA
Solid 6850 26394320-4071-8 EPAZ5S16S13 Total/NA
Solid 6850 26394320-4071-9 EPAZ5S17S00 Total/NA
Solid 6850 26394320-4071-10 EPAZ5S18S00 Total/NA
Solid 6850 26394LCS 320-26394/2-A Lab Control Sample Total/NA
Solid 6850 26394MB 320-26394/1-A Method Blank Total/NA
Analysis Batch: 26877
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 6850 26394320-4071-1 - DL EPAZ5MW5S00 Total/NA
Solid 6850 26394320-4071-3 - RA EPAZ5MW9S00 Total/NA
Solid 6850 26394320-4071-4 - RA EPAZ5S15S00 Total/NA
General Chemistry
Analysis Batch: 26014
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid D 2216320-4071-1 EPAZ5MW5S00 Total/NA
Solid D 2216320-4071-3 EPAZ5MW9S00 Total/NA
Solid D 2216320-4071-4 EPAZ5S15S00 Total/NA
Solid D 2216320-4071-5 EPAZ5S15S03 Total/NA
Solid D 2216320-4071-6 EPAZ5S16S00 Total/NA
Solid D 2216320-4071-7 EPAZ5S16S03 Total/NA
Solid D 2216320-4071-8 EPAZ5S16S13 Total/NA
Solid D 2216320-4071-9 EPAZ5S17S00 Total/NA
Solid D 2216320-4071-10 EPAZ5S18S00 Total/NA
Solid D 2216320-4071-10 DU EPAZ5S18S00 Total/NA
Leach Batch: 132365
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid DI Leach320-4071-1 EPAZ5MW5S00 Soluble
Solid DI Leach320-4071-1 DU EPAZ5MW5S00 Soluble
Solid DI Leach320-4071-3 EPAZ5MW9S00 Soluble
Solid DI Leach320-4071-4 EPAZ5S15S00 Soluble
Solid DI Leach320-4071-5 EPAZ5S15S03 Soluble
Solid DI Leach320-4071-6 EPAZ5S16S00 Soluble
Solid DI Leach320-4071-7 EPAZ5S16S03 Soluble
Solid DI Leach320-4071-8 EPAZ5S16S13 Soluble
Solid DI Leach320-4071-9 EPAZ5S17S00 Soluble
Solid DI Leach320-4071-10 EPAZ5S18S00 Soluble
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QC Association SummaryTestAmerica Job ID: 320-4071-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
General Chemistry (Continued)
Analysis Batch: 132475
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 9045C 132365320-4071-1 EPAZ5MW5S00 Soluble
Solid 9045C 132365320-4071-1 DU EPAZ5MW5S00 Soluble
Solid 9045C 132365320-4071-3 EPAZ5MW9S00 Soluble
Solid 9045C 132365320-4071-4 EPAZ5S15S00 Soluble
Solid 9045C 132365320-4071-5 EPAZ5S15S03 Soluble
Solid 9045C 132365320-4071-6 EPAZ5S16S00 Soluble
Solid 9045C 132365320-4071-7 EPAZ5S16S03 Soluble
Solid 9045C 132365320-4071-8 EPAZ5S16S13 Soluble
Solid 9045C 132365320-4071-9 EPAZ5S17S00 Soluble
Solid 9045C 132365320-4071-10 EPAZ5S18S00 Soluble
Analysis Batch: 132478
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid SM 2580B 132365320-4071-1 EPAZ5MW5S00 Soluble
Solid SM 2580B 132365320-4071-1 DU EPAZ5MW5S00 Soluble
Solid SM 2580B 132365320-4071-3 EPAZ5MW9S00 Soluble
Solid SM 2580B 132365320-4071-4 EPAZ5S15S00 Soluble
Solid SM 2580B 132365320-4071-5 EPAZ5S15S03 Soluble
Solid SM 2580B 132365320-4071-6 EPAZ5S16S00 Soluble
Solid SM 2580B 132365320-4071-7 EPAZ5S16S03 Soluble
Solid SM 2580B 132365320-4071-8 EPAZ5S16S13 Soluble
Solid SM 2580B 132365320-4071-9 EPAZ5S17S00 Soluble
Solid SM 2580B 132365320-4071-10 EPAZ5S18S00 Soluble
TestAmerica Sacramento
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Lab ChronicleClient: CH2M Hill Constructors, Inc. TestAmerica Job ID: 320-4071-1
Project/Site: Stringfellow Acid Project
Client Sample ID: EPAZ5MW5S00 Lab Sample ID: 320-4071-1Matrix: SolidDate Collected: 09/13/13 00:00
Percent Solids: 99.6Date Received: 09/14/13 09:10
Prep 5035 MEO09/16/13 10:11 TAL SAC25193
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.2 g 5 mL
Analysis 8260B/CA_LUFTM
S
1 25274 09/17/13 15:05 MEO TAL SACTotal/NA
Prep 3550B 25407 09/18/13 09:44 ALH TAL SACTotal/NA 30.55 g 3 mL
Analysis 8015B 1 26290 09/30/13 17:02 UFB TAL SACTotal/NA
Leach DI Leach 26456 10/01/13 12:38 LW1 TAL SACSoluble 10.04 g 50 mL
Analysis 9056 1 26521 10/01/13 19:46 LW1 TAL SACSoluble 5 mL
Analysis 9056 1 26522 10/01/13 19:46 LW1 TAL SACSoluble 5 mL
Analysis 9056 2 26942 10/02/13 16:12 LW1 TAL SACSoluble 5 mL
Prep 3060A 132189 09/19/13 13:40 RW TAL IRVTotal/NA 1.26 g 50 mL
Analysis 7199 10 132325 09/20/13 21:44 QPD TAL IRVTotal/NA
Prep SHAKE 26024 09/26/13 07:18 HJA TAL SACTotal/NA 10.17 g 100 mL
Analysis 8321A 1 26161 09/28/13 08:08 NSS TAL SACTotal/NA
Prep 3550B 25404 09/18/13 09:28 ALH TAL SACTotal/NA 9.62 g .5 mL
Analysis GCMSMS_NDMA 1 26498 10/02/13 04:04 VMN TAL SACTotal/NA
Prep SHAKE 26394 10/01/13 08:31 HJA TAL SACTotal/NA 3.04 g 10.00 mL
Analysis 6850 1 26675 10/03/13 20:02 NSS TAL SACTotal/NA
Prep SHAKE DL 26394 10/01/13 08:31 HJA TAL SACTotal/NA 3.04 g 10.00 mL
Analysis 6850 DL 10 26877 10/07/13 14:02 NSS TAL SACTotal/NA
Analysis D 2216 1 26014 09/25/13 15:35 JCB TAL SACTotal/NA
Analysis 9045C 1 132475 09/20/13 14:30 NT TAL IRVSoluble 20 mL
Leach DI Leach 132365 09/20/13 08:40 NT TAL IRVSoluble 19.91 g 20 mL
Analysis SM 2580B 1 132478 09/20/13 12:08 NT TAL IRVSoluble 20 mL
Client Sample ID: EPAZ5MW5S3 Lab Sample ID: 320-4071-2Matrix: WaterDate Collected: 09/13/13 13:30
Date Received: 09/14/13 09:10
Prep 3510C NGK09/20/13 09:28 TAL SAC25607
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 1048.1 mL 0.5 mL
Analysis GCMSMS_NDMA 1 25889 09/24/13 20:12 VMN TAL SACTotal/NA
Prep Filtration 26279 09/30/13 09:37 HJA TAL SACTotal/NA 4.00 mL 4.00 mL
Analysis 6850 1 26429 10/02/13 21:06 NSS TAL SACTotal/NA
Client Sample ID: EPAZ5MW9S00 Lab Sample ID: 320-4071-3Matrix: SolidDate Collected: 09/13/13 10:30
Percent Solids: 98.2Date Received: 09/14/13 09:10
Prep 5035 MEO09/16/13 10:11 TAL SAC25193
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.68 g 5 mL
Analysis 8260B/CA_LUFTM
S
1 25274 09/17/13 15:28 MEO TAL SACTotal/NA
Prep 3550B 25407 09/18/13 09:44 ALH TAL SACTotal/NA 30.61 g 3 mL
TestAmerica Sacramento
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Lab ChronicleClient: CH2M Hill Constructors, Inc. TestAmerica Job ID: 320-4071-1
Project/Site: Stringfellow Acid Project
Client Sample ID: EPAZ5MW9S00 Lab Sample ID: 320-4071-3Matrix: SolidDate Collected: 09/13/13 10:30
Percent Solids: 98.2Date Received: 09/14/13 09:10
Analysis 8015B UFB09/30/13 17:331 TAL SAC26290
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Leach DI Leach 26456 10/01/13 12:38 LW1 TAL SACSoluble 10.04 g 50 mL
Analysis 9056 1 26521 10/01/13 19:58 LW1 TAL SACSoluble 5 mL
Analysis 9056 1 26522 10/01/13 19:58 LW1 TAL SACSoluble 5 mL
Prep 3060A 132189 09/19/13 13:40 RW TAL IRVTotal/NA 1.26 g 50 mL
Analysis 7199 10 132325 09/20/13 21:57 QPD TAL IRVTotal/NA
Prep SHAKE 26024 09/26/13 07:18 HJA TAL SACTotal/NA 10.02 g 100 mL
Analysis 8321A 1 26161 09/28/13 08:26 NSS TAL SACTotal/NA
Prep 3550B 25404 09/18/13 09:28 ALH TAL SACTotal/NA 10.45 g .5 mL
Analysis GCMSMS_NDMA 1 26498 10/02/13 04:41 VMN TAL SACTotal/NA
Prep SHAKE 26394 10/01/13 08:31 HJA TAL SACTotal/NA 3.08 g 10.00 mL
Analysis 6850 1 26675 10/03/13 20:19 NSS TAL SACTotal/NA
Prep SHAKE RA 26394 10/01/13 08:31 HJA TAL SACTotal/NA 3.08 g 10.00 mL
Analysis 6850 RA 1 26877 10/07/13 14:19 NSS TAL SACTotal/NA
Analysis D 2216 1 26014 09/25/13 15:35 JCB TAL SACTotal/NA
Analysis 9045C 1 132475 09/20/13 14:45 NT TAL IRVSoluble 20 mL
Leach DI Leach 132365 09/20/13 08:40 NT TAL IRVSoluble 20.05 g 20 mL
Analysis SM 2580B 1 132478 09/20/13 12:08 NT TAL IRVSoluble 20 mL
Client Sample ID: EPAZ5S15S00 Lab Sample ID: 320-4071-4Matrix: SolidDate Collected: 09/13/13 08:54
Percent Solids: 99.3Date Received: 09/14/13 09:10
Prep 5035 MEO09/16/13 10:11 TAL SAC25193
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.52 g 5 mL
Analysis 8260B/CA_LUFTM
S
1 25274 09/17/13 15:51 MEO TAL SACTotal/NA
Prep 3550B 25407 09/18/13 09:44 ALH TAL SACTotal/NA 30.38 g 3 mL
Analysis 8015B 1 26290 09/30/13 18:03 UFB TAL SACTotal/NA
Analysis 9056 1 26521 10/01/13 20:09 LW1 TAL SACSoluble 5 mL
Leach DI Leach 26456 10/01/13 12:38 LW1 TAL SACSoluble 10.17 g 50 mL
Analysis 9056 1 26522 10/01/13 20:09 LW1 TAL SACSoluble 5 mL
Prep 3060A 132189 09/19/13 13:40 RW TAL IRVTotal/NA 1.24 g 50 mL
Analysis 7199 10 132325 09/20/13 22:10 QPD TAL IRVTotal/NA
Prep SHAKE 26024 09/26/13 07:18 HJA TAL SACTotal/NA 10.04 g 100 mL
Analysis 8321A 1 26161 09/28/13 08:45 NSS TAL SACTotal/NA
Prep 3550B 25404 09/18/13 09:28 ALH TAL SACTotal/NA 9.67 g .5 mL
Analysis GCMSMS_NDMA 1 26498 10/02/13 07:07 VMN TAL SACTotal/NA
Prep SHAKE 26394 10/01/13 08:31 HJA TAL SACTotal/NA 3.02 g 10.00 mL
Analysis 6850 1 26675 10/03/13 20:36 NSS TAL SACTotal/NA
Prep SHAKE RA 26394 10/01/13 08:31 HJA TAL SACTotal/NA 3.02 g 10.00 mL
Analysis 6850 RA 1 26877 10/07/13 14:35 NSS TAL SACTotal/NA
Analysis D 2216 1 26014 09/25/13 15:35 JCB TAL SACTotal/NA
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Lab ChronicleClient: CH2M Hill Constructors, Inc. TestAmerica Job ID: 320-4071-1
Project/Site: Stringfellow Acid Project
Client Sample ID: EPAZ5S15S00 Lab Sample ID: 320-4071-4Matrix: SolidDate Collected: 09/13/13 08:54
Date Received: 09/14/13 09:10
Analysis 9045C NT09/20/13 14:301 TAL IRV132475
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Soluble 20 mL
Leach DI Leach 132365 09/20/13 08:40 NT TAL IRVSoluble 19.98 g 20 mL
Analysis SM 2580B 1 132478 09/20/13 12:08 NT TAL IRVSoluble 20 mL
Client Sample ID: EPAZ5S15S03 Lab Sample ID: 320-4071-5Matrix: SolidDate Collected: 09/13/13 09:25
Percent Solids: 95.6Date Received: 09/14/13 09:10
Prep 5035 MEO09/16/13 10:11 TAL SAC25193
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.1 g 5 mL
Analysis 8260B/CA_LUFTM
S
1 25274 09/17/13 16:15 MEO TAL SACTotal/NA
Prep 3550B 25407 09/18/13 09:44 ALH TAL SACTotal/NA 30.35 g 3 mL
Analysis 8015B 1 26290 09/30/13 18:33 UFB TAL SACTotal/NA
Analysis 9056 1 26521 10/01/13 20:21 LW1 TAL SACSoluble 5 mL
Leach DI Leach 26456 10/01/13 12:38 LW1 TAL SACSoluble 10.29 g 50 mL
Analysis 9056 1 26522 10/01/13 20:21 LW1 TAL SACSoluble 5 mL
Prep 3060A 132189 09/19/13 13:40 RW TAL IRVTotal/NA 1.26 g 50 mL
Analysis 7199 10 132325 09/20/13 22:22 QPD TAL IRVTotal/NA
Prep SHAKE 26024 09/26/13 07:18 HJA TAL SACTotal/NA 10.14 g 100 mL
Analysis 8321A 1 26161 09/28/13 09:04 NSS TAL SACTotal/NA
Prep 3550B 25404 09/18/13 09:28 ALH TAL SACTotal/NA 9.39 g .5 mL
Analysis GCMSMS_NDMA 1 26498 10/02/13 07:44 VMN TAL SACTotal/NA
Prep SHAKE 26394 10/01/13 08:31 HJA TAL SACTotal/NA 3.04 g 10.00 mL
Analysis 6850 1 26675 10/03/13 20:52 NSS TAL SACTotal/NA
Analysis D 2216 1 26014 09/25/13 15:35 JCB TAL SACTotal/NA
Leach DI Leach 132365 09/20/13 08:40 NT TAL IRVSoluble 20.09 g 20 mL
Analysis 9045C 1 132475 09/20/13 14:30 NT TAL IRVSoluble 20 mL
Analysis SM 2580B 1 132478 09/20/13 12:08 NT TAL IRVSoluble 20 mL
Client Sample ID: EPAZ5S16S00 Lab Sample ID: 320-4071-6Matrix: SolidDate Collected: 09/13/13 07:45
Percent Solids: 99.1Date Received: 09/14/13 09:10
Prep 5035 MEO09/16/13 10:11 TAL SAC25193
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 3.49 g 5 mL
Analysis 8260B/CA_LUFTM
S
1 25274 09/17/13 16:38 MEO TAL SACTotal/NA
Prep 3550B 25407 09/18/13 09:44 ALH TAL SACTotal/NA 30.55 g 3 mL
Analysis 8015B 1 26290 09/30/13 20:35 UFB TAL SACTotal/NA
Analysis 9056 1 26521 10/01/13 20:32 LW1 TAL SACSoluble 5 mL
Leach DI Leach 26456 10/01/13 12:38 LW1 TAL SACSoluble 10.31 g 50 mL
Analysis 9056 1 26522 10/01/13 20:32 LW1 TAL SACSoluble 5 mL
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Lab ChronicleClient: CH2M Hill Constructors, Inc. TestAmerica Job ID: 320-4071-1
Project/Site: Stringfellow Acid Project
Client Sample ID: EPAZ5S16S00 Lab Sample ID: 320-4071-6Matrix: SolidDate Collected: 09/13/13 07:45
Percent Solids: 99.1Date Received: 09/14/13 09:10
Prep 3060A RW09/19/13 13:40 TAL IRV132189
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 1.26 g 50 mL
Analysis 7199 10 132325 09/20/13 23:00 QPD TAL IRVTotal/NA
Prep SHAKE 26024 09/26/13 07:18 HJA TAL SACTotal/NA 10.01 g 100 mL
Analysis 8321A 1 26161 09/28/13 09:22 NSS TAL SACTotal/NA
Prep 3550B 25404 09/18/13 09:28 ALH TAL SACTotal/NA 10.01 g .5 mL
Analysis GCMSMS_NDMA 1 26498 10/02/13 08:20 VMN TAL SACTotal/NA
Prep SHAKE 26394 10/01/13 08:31 HJA TAL SACTotal/NA 3.03 g 10.00 mL
Analysis 6850 1 26675 10/03/13 21:09 NSS TAL SACTotal/NA
Analysis D 2216 1 26014 09/25/13 15:35 JCB TAL SACTotal/NA
Leach DI Leach 132365 09/20/13 08:40 NT TAL IRVSoluble 20.02 g 20 mL
Analysis 9045C 1 132475 09/20/13 14:30 NT TAL IRVSoluble 20 mL
Analysis SM 2580B 1 132478 09/20/13 12:08 NT TAL IRVSoluble 20 mL
Client Sample ID: EPAZ5S16S03 Lab Sample ID: 320-4071-7Matrix: SolidDate Collected: 09/13/13 08:50
Percent Solids: 96.5Date Received: 09/14/13 09:10
Prep 5035 MEO09/16/13 10:11 TAL SAC25193
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.09 g 5 mL
Analysis 8260B/CA_LUFTM
S
1 25274 09/17/13 17:01 MEO TAL SACTotal/NA
Prep 3550B 25407 09/18/13 09:44 ALH TAL SACTotal/NA 30.65 g 3 mL
Analysis 8015B 1 26290 09/30/13 21:06 UFB TAL SACTotal/NA
Analysis 9056 1 26521 10/01/13 20:44 LW1 TAL SACSoluble 5 mL
Leach DI Leach 26456 10/01/13 12:38 LW1 TAL SACSoluble 10.12 g 50 mL
Analysis 9056 1 26522 10/01/13 20:44 LW1 TAL SACSoluble 5 mL
Prep 3060A 132189 09/19/13 13:40 RW TAL IRVTotal/NA 1.25 g 50 mL
Analysis 7199 10 132325 09/20/13 23:13 QPD TAL IRVTotal/NA
Prep SHAKE 26024 09/26/13 07:18 HJA TAL SACTotal/NA 10.07 g 100 mL
Analysis 8321A 1 26161 09/28/13 09:41 NSS TAL SACTotal/NA
Prep 3550B 25404 09/18/13 09:28 ALH TAL SACTotal/NA 10.23 g .5 mL
Analysis GCMSMS_NDMA 1 26498 10/02/13 08:57 VMN TAL SACTotal/NA
Prep SHAKE 26394 10/01/13 08:31 HJA TAL SACTotal/NA 3.15 g 10.00 mL
Analysis 6850 1 26675 10/03/13 21:26 NSS TAL SACTotal/NA
Analysis D 2216 1 26014 09/25/13 15:35 JCB TAL SACTotal/NA
Analysis 9045C 1 132475 09/20/13 14:30 NT TAL IRVSoluble 20 mL
Leach DI Leach 132365 09/20/13 08:40 NT TAL IRVSoluble 20.06 g 20 mL
Analysis SM 2580B 1 132478 09/20/13 12:08 NT TAL IRVSoluble 20 mL
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Lab ChronicleClient: CH2M Hill Constructors, Inc. TestAmerica Job ID: 320-4071-1
Project/Site: Stringfellow Acid Project
Client Sample ID: EPAZ5S16S13 Lab Sample ID: 320-4071-8Matrix: SolidDate Collected: 09/13/13 09:10
Percent Solids: 97.4Date Received: 09/14/13 09:10
Prep 5035 MEO09/16/13 10:11 TAL SAC25193
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.08 g 5 mL
Analysis 8260B/CA_LUFTM
S
1 25274 09/17/13 18:34 MEO TAL SACTotal/NA
Prep 3550B 25407 09/18/13 09:44 ALH TAL SACTotal/NA 29.99 g 3 mL
Analysis 8015B 1 26290 09/30/13 21:36 UFB TAL SACTotal/NA
Analysis 9056 1 26521 10/01/13 20:55 LW1 TAL SACSoluble 5 mL
Leach DI Leach 26456 10/01/13 12:38 LW1 TAL SACSoluble 10.15 g 50 mL
Analysis 9056 1 26522 10/01/13 20:55 LW1 TAL SACSoluble 5 mL
Prep 3060A 132189 09/19/13 13:40 RW TAL IRVTotal/NA 1.25 g 50 mL
Analysis 7199 10 132325 09/20/13 23:26 QPD TAL IRVTotal/NA
Prep SHAKE 26024 09/26/13 07:18 HJA TAL SACTotal/NA 10.05 g 100 mL
Analysis 8321A 1 26161 09/28/13 09:59 NSS TAL SACTotal/NA
Prep 3550B 25404 09/18/13 09:28 ALH TAL SACTotal/NA 10.78 g .5 mL
Analysis GCMSMS_NDMA 1 26498 10/02/13 09:33 VMN TAL SACTotal/NA
Prep SHAKE 26394 10/01/13 08:31 HJA TAL SACTotal/NA 2.99 g 10.00 mL
Analysis 6850 1 26675 10/03/13 21:42 NSS TAL SACTotal/NA
Analysis D 2216 1 26014 09/25/13 15:35 JCB TAL SACTotal/NA
Analysis 9045C 1 132475 09/20/13 14:30 NT TAL IRVSoluble 20 mL
Leach DI Leach 132365 09/20/13 08:40 NT TAL IRVSoluble 20.15 g 20 mL
Analysis SM 2580B 1 132478 09/20/13 12:08 NT TAL IRVSoluble 20 mL
Client Sample ID: EPAZ5S17S00 Lab Sample ID: 320-4071-9Matrix: SolidDate Collected: 09/13/13 07:50
Percent Solids: 99.8Date Received: 09/14/13 09:10
Prep 5035 MEO09/16/13 10:11 TAL SAC25193
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 3.97 g 5 mL
Analysis 8260B/CA_LUFTM
S
1 25274 09/17/13 18:58 MEO TAL SACTotal/NA
Prep 3550B 25407 09/18/13 09:44 ALH TAL SACTotal/NA 30.21 g 3 mL
Analysis 8015B 1 26290 09/30/13 22:07 UFB TAL SACTotal/NA
Leach DI Leach 26456 10/01/13 12:38 LW1 TAL SACSoluble 10.12 g 50 mL
Analysis 9056 1 26521 10/01/13 21:07 LW1 TAL SACSoluble 5 mL
Analysis 9056 2 26943 10/02/13 16:23 LW1 TAL SACSoluble 5 mL
Prep 3060A 132189 09/19/13 13:40 RW TAL IRVTotal/NA 1.24 g 50 mL
Analysis 7199 10 132325 09/20/13 23:38 QPD TAL IRVTotal/NA
Prep SHAKE 26024 09/26/13 07:18 HJA TAL SACTotal/NA 10.05 g 100 mL
Analysis 8321A 1 26161 09/28/13 10:18 NSS TAL SACTotal/NA
Prep 3550B 25404 09/18/13 09:28 ALH TAL SACTotal/NA 9.63 g .5 mL
Analysis GCMSMS_NDMA 1 26498 10/02/13 10:09 VMN TAL SACTotal/NA
Prep SHAKE 26394 10/01/13 08:31 HJA TAL SACTotal/NA 3.01 g 10.00 mL
Analysis 6850 1 26675 10/03/13 21:59 NSS TAL SACTotal/NA
Analysis D 2216 1 26014 09/25/13 15:35 JCB TAL SACTotal/NA
Analysis 9045C 1 132475 09/20/13 14:30 NT TAL IRVSoluble 20 mL
TestAmerica Sacramento
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Lab ChronicleClient: CH2M Hill Constructors, Inc. TestAmerica Job ID: 320-4071-1
Project/Site: Stringfellow Acid Project
Client Sample ID: EPAZ5S17S00 Lab Sample ID: 320-4071-9Matrix: SolidDate Collected: 09/13/13 07:50
Date Received: 09/14/13 09:10
Leach DI Leach NT09/20/13 08:40 TAL IRV132365
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Soluble 19.92 g 20 mL
Analysis SM 2580B 1 132478 09/20/13 12:08 NT TAL IRVSoluble 20 mL
Client Sample ID: EPAZ5S18S00 Lab Sample ID: 320-4071-10Matrix: SolidDate Collected: 09/13/13 00:00
Percent Solids: 98.9Date Received: 09/14/13 09:10
Prep 5035 MEO09/16/13 10:11 TAL SAC25193
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 4.42 g 5 mL
Analysis 8260B/CA_LUFTM
S
1 25274 09/17/13 19:21 MEO TAL SACTotal/NA
Prep 3550B 25407 09/18/13 09:44 ALH TAL SACTotal/NA 29.42 g 3 mL
Analysis 8015B 1 26290 09/30/13 22:37 UFB TAL SACTotal/NA
Analysis 9056 1 26521 10/01/13 21:18 LW1 TAL SACSoluble 5 mL
Leach DI Leach 26456 10/01/13 12:38 LW1 TAL SACSoluble 10.06 g 50 mL
Analysis 9056 1 26522 10/01/13 21:18 LW1 TAL SACSoluble 5 mL
Prep 3060A 132189 09/19/13 13:40 RW TAL IRVTotal/NA 1.25 g 50 mL
Analysis 7199 10 132325 09/20/13 23:51 QPD TAL IRVTotal/NA
Prep SHAKE 26024 09/26/13 07:18 HJA TAL SACTotal/NA 10.09 g 100 mL
Analysis 8321A 1 26161 09/28/13 10:36 NSS TAL SACTotal/NA
Prep 3550B 25404 09/18/13 09:28 ALH TAL SACTotal/NA 10.38 g .5 mL
Analysis GCMSMS_NDMA 1 26498 10/02/13 10:46 VMN TAL SACTotal/NA
Prep SHAKE 26394 10/01/13 08:31 HJA TAL SACTotal/NA 3.17 g 10.00 mL
Analysis 6850 1 26675 10/03/13 22:16 NSS TAL SACTotal/NA
Analysis D 2216 1 26014 09/25/13 15:35 JCB TAL SACTotal/NA
Analysis 9045C 1 132475 09/20/13 14:30 NT TAL IRVSoluble 20 mL
Leach DI Leach 132365 09/20/13 08:40 NT TAL IRVSoluble 20.07 g 20 mL
Analysis SM 2580B 1 132478 09/20/13 12:08 NT TAL IRVSoluble 20 mL
Laboratory References:
TAL IRV = TestAmerica Irvine, 17461 Derian Ave, Suite 100, Irvine, CA 92614-5817, TEL (949)261-1022
TAL SAC = TestAmerica Sacramento, 880 Riverside Parkway, West Sacramento, CA 95605, TEL (916)373-5600
TestAmerica Sacramento
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Certification SummaryClient: CH2M Hill Constructors, Inc. TestAmerica Job ID: 320-4071-1
Project/Site: Stringfellow Acid Project
Laboratory: TestAmerica SacramentoAll certifications held by this laboratory are listed. Not all certifications are applicable to this report.
Authority Program EPA Region Certification ID Expiration Date
A2LA NE-OS-22-13A2LA 01-31-14
A2LA DoD ELAP 2928-01 01-31-14
Alaska (UST) State Program 10 UST-055 12-18-13
Arizona State Program 9 AZ0708 08-11-14
Arkansas DEQ State Program 6 88-0691 06-17-14
California NELAP 9 1119CA 01-31-14
Connecticut State Program 1 PH-0691 06-30-15
Florida NELAP 4 E87570 06-30-14
Guam State Program 9 N/A 08-31-14
Hawaii State Program 9 N/A 01-31-14
Illinois NELAP 5 200060 03-17-14
Kansas NELAP 7 E-10375 10-31-13
Louisiana NELAP 6 30612 06-30-14
Michigan State Program 5 9947 01-31-14
Nebraska State Program 7 NE-OS-22-13 01-31-14
Nevada State Program 9 CA44 07-31-14
New Jersey NELAP 2 CA005 06-30-14
New York NELAP 2 11666 04-01-14
Northern Mariana Islands State Program 9 MP0007 02-01-14
Oregon NELAP 10 CA200005 03-28-14
Pennsylvania NELAP 3 68-01272 03-31-14
South Carolina State Program 4 87014 06-30-14
Texas NELAP 6 T104704399-08-TX 05-31-14
US Fish & Wildlife Federal LE148388-0 12-31-13
USDA Federal P330-11-00436 12-30-14
USEPA UCMR Federal 1 CA00044 11-06-14
Utah NELAP 8 QUAN1 01-31-14
Washington State Program 10 C581 05-05-14
West Virginia State Program 3 9930C 12-31-13
Wyoming State Program 8 8TMS-Q 01-31-14
Laboratory: TestAmerica IrvineAll certifications held by this laboratory are listed. Not all certifications are applicable to this report.
Authority Program EPA Region Certification ID Expiration Date
Alaska CA0153110State Program 06-30-14
Arizona State Program 9 AZ0671 10-13-13
California LA Cty Sanitation Districts 9 10256 01-31-14
California NELAP 9 1108CA 01-31-14
California State Program 9 2706 06-30-14
Guam State Program 9 Cert. No. 12.002r 01-28-14 *
Hawaii State Program 9 N/A 01-31-14
Nevada State Program 9 CA015312007A 07-31-14
New Mexico State Program 6 N/A 01-31-14
Northern Mariana Islands State Program 9 MP0002 01-31-14
Oregon NELAP 10 4005 09-12-14
USDA Federal P330-09-00080 06-06-14
USEPA UCMR Federal 1 CA01531 01-31-15
TestAmerica Sacramento
* Expired certification is currently pending renewal and is considered valid.
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Method SummaryTestAmerica Job ID: 320-4071-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Method Method Description LaboratoryProtocol
SW8468260B/CA_LUFTM
S
Volatile Organic Compounds by GC/MS TAL SAC
SW8468015B Diesel Range Organics (DRO) (GC) TAL SAC
SW8467199 Chromium, Hexavalent (IC) TAL IRV
SW8469056 Anions, Ion Chromatography TAL SAC
EPA6850 Perchlorate by LC/MS or LC/MS/MS TAL SAC
SW8468321A Benzene Sulfonic Acids (LCMS) TAL SAC
TestAmerica SOPGCMSMS_NDMA Nitrosamines by Isotope Dilution and GC/CI/MS/MS TAL SAC
SW8469045C pH TAL IRV
ASTMD 2216 Percent Moisture TAL SAC
SMSM 2580B Reduction-Oxidation (REDOX) Potential TAL IRV
Protocol References:
ASTM = ASTM International
EPA = US Environmental Protection Agency
SM = "Standard Methods For The Examination Of Water And Wastewater",
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
TestAmerica SOP = TestAmerica, Inc., Standard Operating Procedure
Laboratory References:
TAL IRV = TestAmerica Irvine, 17461 Derian Ave, Suite 100, Irvine, CA 92614-5817, TEL (949)261-1022
TAL SAC = TestAmerica Sacramento, 880 Riverside Parkway, West Sacramento, CA 95605, TEL (916)373-5600
TestAmerica Sacramento
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Sample SummaryTestAmerica Job ID: 320-4071-1Client: CH2M Hill Constructors, Inc.
Project/Site: Stringfellow Acid Project
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
320-4071-1 EPAZ5MW5S00 Solid 09/13/13 00:00 09/14/13 09:10
320-4071-2 EPAZ5MW5S3 Water 09/13/13 13:30 09/14/13 09:10
320-4071-3 EPAZ5MW9S00 Solid 09/13/13 10:30 09/14/13 09:10
320-4071-4 EPAZ5S15S00 Solid 09/13/13 08:54 09/14/13 09:10
320-4071-5 EPAZ5S15S03 Solid 09/13/13 09:25 09/14/13 09:10
320-4071-6 EPAZ5S16S00 Solid 09/13/13 07:45 09/14/13 09:10
320-4071-7 EPAZ5S16S03 Solid 09/13/13 08:50 09/14/13 09:10
320-4071-8 EPAZ5S16S13 Solid 09/13/13 09:10 09/14/13 09:10
320-4071-9 EPAZ5S17S00 Solid 09/13/13 07:50 09/14/13 09:10
320-4071-10 EPAZ5S18S00 Solid 09/13/13 00:00 09/14/13 09:10
TestAmerica Sacramento
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Login Sample Receipt Checklist
Client: CH2M Hill Constructors, Inc. Job Number: 320-4071-1
Login Number: 4071
Question Answer Comment
Creator: Hytrek, Cheryl
List Source: TestAmerica Sacramento
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
FalseCOC is filled out with all pertinent information. COC not relinquished.
N/AIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica SacramentoPage 42 of 43 10/8/2013
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Login Sample Receipt Checklist
Client: CH2M Hill Constructors, Inc. Job Number: 320-4071-1
Login Number: 4071
Question Answer Comment
Creator: Sung, Hubert
List Source: TestAmerica Irvine
List Creation: 09/18/13 11:41 AMList Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
N/AIs the Field Sampler's name present on COC? Received project as a subcontract.
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
N/AContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
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