ANALYTICAL REPORT
Job Number: 680-56861-1
Job Description: Hattiesburg Sludge Total APR 2010
For:Ashland Inc.
500 Hercules RoadWilmington, DE 19894
Attention: Nancy Berrios
_____________________________________________
Approved for release.Lidya GuliziaProject Manager I5/11/2010 4:12 PM
Lidya GuliziaProject Manager I
[email protected]/11/2010
cc: Craig Derouen
The test results in this report meet NELAP requirements for parameters for which accreditation is required or available.Any exceptions to the NELAP requirements are noted. Results pertain only to samples listed in this report. This reportmay not be reproduced, except in full, without the written approval of the laboratory. Questions should be directed to theperson who signed this report.
Savannah Certifications and ID #s: A2LA: 0399.01; AL: 41450; ARDEQ: 88-0692; ARDOH; AZ: AZ0741; CA: 03217CA;CO; CT: PH0161; DE; FL: E87052; GA: 803; Guam; HI; IL: 200022; IN; IA: 353; KS: E-10322; KY EPPC: 90084; KYUST; LA DEQ: 30690; LA DHH: LA080008; ME: 2008022; MD: 250; MA: M-GA006; MI: 9925; MS; NFESC: 249; NV:GA00006; NJ: GA769; NM; NY: 10842; NC DWQ: 269; NC DHHS: 13701; PA: 68-00474; PR: GA00006; RI: LAO00244;SC: 98001001; TN: TN0296; TX: T104704185; USEPA: GA00006; VT: VT-87052; VA: 00302; WA; WV DEP: 094; WVDHHR: 9950 C; WI DNR: 999819810; WY/EPAR8: 8TMS-Q
TestAmerica Laboratories, Inc.
TestAmerica Savannah 5102 LaRoche Avenue, Savannah, GA 31404
Tel (912) 354-7858 Fax (912) 352-0165 www.testamericainc.com
Page 1 of 238
Job Narrative
680-56861-1
Receipt
Pre-preserved vials for volatiles analysis were not submitted for sample IBS-5-NS (680-56861-7). The volatiles analysis was perfomed on
a subsample taken from the bulk sample container.
All other samples were received in good condition within temperature requirements.
GC/MS VOA
Method(s) 8260B: A full list spike was utilized for this method. Due to the large number of spiked analytes, there is a high probability that
one or more analytes will recover outside acceptance limits. The laboratory's SOP allows for four analytes to recover outside criteria for
this method when a full list spike is utilized. The LCS/LCSD associated with batch 166185 had one analyte outside control limits;
therefore, re-analysis was not performed. These results have been reported and qualified.
Method(s) 8260B: The continuing calibration verification (CCV) for pentachloroethane recovered above the upper control limit. The
samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been reported.
Method(s) 8260B: The trip blank associated with these samples contained a detection above the method detection limit (MDL) for the
following analyte: acetone.
Method(s) 8260B: The field blank associated with these samples contained a detection above the reporting limit (RL) for toluene and a
detection above the method detection limit (MDL) for 2-butanone, acetone, ethylbenzene, and xylenes. The field blank was re-analyzed
with concurring results; the first set of data has been reported.
Method(s) 8260B: The rinse blank associated with these samples contained a detection above the reporting limit (RL) for toluene and a
detection above the method detection limit (MDL) for 2-butanone and acetone. The rinse blank was re-analyzed with concurring results;
the first set of data has been reported.
Method(s) 8260B: Due to the level of dilution required for the following sample(s), surrogate recoveries are not reported: IBS-1-LS
(680-56861-1), IBS-3-NS (680-56861-2), IBS-3-US (680-56861-6), IBS-4-NS (680-56861-4), IBS-6-NS (680-56861-10), IBS-6-US
(680-56861-13), IBS-7-LS (680-56861-15), IBS-7-US (680-56861-16), IBS-4-US (680-56861-9), IBS-1-US (680-56861-20), IBS-2-LS
(680-56861-22), IBS-2-NS (680-56861-21), IBS-2-US (680-56861-23), IBS-5-LS (680-56861-8), IBS-5-US (680-56861-12), IBS-7-NS
(680-56861-14), IBS-8-US (680-56861-19), IBS-3-LS (680-56861-3), IBS-4-LS (680-56861-5), IBS-6-LS (680-56861-11), IBS-8-LS
(680-56861-18).
Method(s) 8260B: Surrogate recovery for the following sample(s) was outside control limits: IBS-5-NS (680-56861-7). Re-extraction
and/or re-analysis was performed with concurring results. The original analysis has been reported.
No other analytical or quality issues were noted.
GC/MS Semi VOA
Method(s) 3546: Many of the project samples would not concentrate to the desired final volume of 1.0 ml. Samples were concentrated to
various final volumes from 5.0 ml to 20 mls and 1.0 ml was delivered to the analysis group for analysis.
Method(s) 8270C: A full list spike was utilized for this method. Due to the large number of spiked analytes, there is a high probability that
one or more analytes will recover outside acceptance limits. The laboratory's SOP allows for 4 analytes to recover outside criteria for this
method when a full list spike is utilized. The LCSD associated with batch 166243 had 3 analytes outside control limits; therefore,
re-extraction/re-analysis was not performed. These results have been reported and qualified.
Method(s) 8270C: The laboratory control sample (LCS) for batch 166243 exceeded control limits for the following analyte(s):
1,4-Napthoquinone, 1-Napthylamine, alpha,alpha-dimethylphenethylamine, famphur, methyl methansulfonate,
o,o,-triethyphosphorothioate has been identified as a poor performing analyte when analyzed using this method; therefore,
re-extraction/re-analysis was not performed. These results have been reported and qualified.
Method(s) 8270C: A full list spike was utilized for this method. Due to the large number of spiked analytes, there is a high probability that
one or more analytes will recover outside acceptance limits. The laboratory's SOP allows for 4 analytes to recover outside criteria for this
method when a full list spike is utilized. The LCS associated with batch 166243 had 3 analytes outside control limits; therefore,
re-extraction/re-analysis was not performed. These results have been reported and qualified.
Method(s) 8270C: The laboratory control sample (LCS) for batch 166243 exceeded control limits for the following analyte(s):
1-napthylamine, alpha,alpha, dimethylphenthylamine, methapyri;ene, methyl methansulfonate, o,o,o-triethylosphorothioate has been
identified as a poor performing analyte when analyzed using this method; therefore, re-extraction/re-analysis was not performed. These
results have been reported and qualified.
Method(s) 8270C: The following samples were diluted due to the nature of the sample matrix: IBS-1-LS (680-56861-1), IBS-3-LS
(680-56861-3), IBS-3-NS (680-56861-2), IBS-3-US (680-56861-6), IBS-4-LS (680-56861-5), IBS-4-US (680-56861-9), IBS-5-NS
Page 2 of 238
(680-56861-7), IBS-2-US (680-56861-23), IBS-1-US (680-56861-20), IBS-4-NS (680-56861-4), IBS-5-US (680-56861-12), IBS-6-LS
(680-56861-11), IBS-6-NS (680-56861-10), IBS-6-US (680-56861-13), IBS-7-LS (680-56861-15), IBS-7-NS (680-56861-14), IBS-7-US
(680-56861-16), IBS-8-LS (680-56861-18), IBS-8-NS (680-56861-17), IBS-8-US (680-56861-19), IBS-2-LS (680-56861-22, IBS-2-NS
(680-56861-21) and the associated MS/MSD samples (680-56861-21 MS and 680-56861-21 MSD). As such, surrogate recoveries are
not reported, and elevated reporting limits (RLs) are provided.
Method(s) 8270C: Sample IBS-4-NS (680-56861-4) was diluted due to the abundance of target analytes. As such, surrogate recoveries
are not reported, and elevated reporting limits (RLs) are provided.
Method(s) 8270C: The laboratory control sample (LCS) for batch 166147 exceeded control limits for the following analytes that have been
identified as poor performer. The following analytes have been identified, in the reference method and/or via historical data, to be poor
and/or erratic performers: Famphur, 1,4-Napthaquinone, Methane sulfonate, Benzaldehyde, 1-naphthylamine, 2-naphthylamine,
p-Dimethylamino azobenzene, p-phenylenediamine, a,a-dimethylphenethylamine, Methapyriline, 2-picoline (2-methylpyridine),
3,3’-dimethylbenzidine, 3,3’-dichlorobenzidine, Benzidine, Benzaldehyde, Benzoic acid, Dinoseb, Hexachlorophene,
Hexachlorocyclopentadiene, o,o,o-triethylphosphoro-thioate.
Method(s) 8270C: Matrix spikes for batch 166138 could not be recovered due to sample matrix interferences which required sample
dilution. The associated laboratory control sample (LCS) met acceptance criteria.
Method(s) 8270C: The laboratory control sample (LCS) for batch 166138 exceeded control limits for one or more of analytes identified as
poor performers. The following analytes have been identified, in the reference method and/or via historical data, to be poor and/or erratic
performers: Famphur, 1,4-Napthaquinone, Methane sulfonate, Benzaldehyde, 1-naphthylamine, 2-naphthylamine, p-Dimethylamino
azobenzene, p-phenylenediamine, a,a-dimethylphenethylamine, Methapyriline, 2-picoline (2-methylpyridine), 3,3’-dimethylbenzidine,
3,3’-dichlorobenzidine, Benzidine, Benzaldehyde, Benzoic acid, Dinoseb, Hexachlorophene, Hexachlorocyclopentadiene,
o,o,o-triethylphosphoro-thioate. Re-extraction was not performed.
No other analytical or quality issues were noted.
Metals
No analytical or quality issues were noted.
General Chemistry
No analytical or quality issues were noted.
VOA Prep
Method(s) 5035: The pre-preserved volatile sample vials submitted for the following sample(s) contained significantly less than 5 grams:
IBS-1-LS (680-56861-1), IBS-4-LS (680-56861-5), IBS-8-US (680-56861-19). Reporting limits in these samples have been elevated
based on the analysis weight.
No other analytical or quality issues were noted.
Comments
No additional comments.
Page 3 of 238
METHOD SUMMARY
Job Number: 680-56861-1Client: Ashland Inc.
Preparation MethodMethodLab LocationDescription
Matrix: Solid
SW846 8260BVolatile Organic Compounds (GC/MS) TAL SAV
SW846 5030ATAL SAVPurge and Trap
SW846 5035TAL SAVClosed System Purge and Trap
SW846 8270CSemivolatile Compounds by Gas Chromatography/Mass
Spectrometry (GC/MS)
TAL SAV
SW846 3546TAL SAVMicrowave Extraction
SW846 6010BMetals (ICP) TAL SAV
SW846 3050BTAL SAVPreparation, Metals
SW846 7471AMercury (CVAA) TAL SAV
SW846 7471ATAL SAVPreparation, Mercury
Matrix: Water
SW846 8260BVolatile Organic Compounds (GC/MS) TAL SAV
SW846 5030BTAL SAVPurge and Trap
SW846 8270CSemivolatile Compounds by Gas Chromatography/Mass
Spectrometry (GC/MS)
TAL SAV
SW846 3520CTAL SAVLiquid-Liquid Extraction (Continuous)
SW846 6010BMetals (ICP) TAL SAV
SW846 3010ATAL SAVPreparation, Total Metals
SW846 7470AMercury (CVAA) TAL SAV
SW846 7470ATAL SAVPreparation, Mercury
Lab References:
TAL SAV = TestAmerica Savannah
Method References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
TestAmerica Savannah
Page 4 of 238
METHOD / ANALYST SUMMARY
Client: Ashland Inc. Job Number: 680-56861-1
Method Analyst Analyst ID
Lanier, Carolyn CLSW846 8260B
Sokolin, Eleina ESSW846 8260B
Haynes, Carion CRHSW846 8270C
Bland, Brian BCBSW846 6010B
Eaton, Cliff CESW846 7470A
Eaton, Cliff CESW846 7471A
TestAmerica Savannah
Page 5 of 238
SAMPLE SUMMARY
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample IDLab Sample ID Client Matrix
Date/Time
Sampled
Date/Time
Received
04/14/2010 0950 04/17/2010 1045IBS-1-LS680-56861-1 Solid
04/14/2010 1245 04/17/2010 1045IBS-3-NS680-56861-2 Solid
04/14/2010 1255 04/17/2010 1045IBS-3-LS680-56861-3 Solid
04/14/2010 1715 04/17/2010 1045IBS-4-NS680-56861-4 Solid
04/14/2010 1735 04/17/2010 1045IBS-4-LS680-56861-5 Solid
04/15/2010 0845 04/17/2010 1045IBS-3-US680-56861-6 Solid
04/15/2010 0950 04/17/2010 1045IBS-5-NS680-56861-7 Solid
04/15/2010 1005 04/17/2010 1045IBS-5-LS680-56861-8 Solid
04/15/2010 1100 04/17/2010 1045IBS-4-US680-56861-9 Solid
04/15/2010 1105 04/17/2010 1045IBS-6-NS680-56861-10 Solid
04/15/2010 1110 04/17/2010 1045IBS-6-LS680-56861-11 Solid
04/15/2010 1145 04/17/2010 1045IBS-5-US680-56861-12 Solid
04/15/2010 1415 04/17/2010 1045IBS-6-US680-56861-13 Solid
04/15/2010 1505 04/17/2010 1045IBS-7-NS680-56861-14 Solid
04/15/2010 1520 04/17/2010 1045IBS-7-LS680-56861-15 Solid
04/15/2010 1525 04/17/2010 1045IBS-7-US680-56861-16 Solid
04/15/2010 1600 04/17/2010 1045IBS-8-NS680-56861-17 Solid
04/15/2010 1615 04/17/2010 1045IBS-8-LS680-56861-18 Solid
04/15/2010 1620 04/17/2010 1045IBS-8-US680-56861-19 Solid
04/15/2010 1700 04/17/2010 1045IBS-1-US680-56861-20 Solid
04/16/2010 0840 04/17/2010 1045IBS-2-NS680-56861-21 Solid
04/16/2010 0850 04/17/2010 1045IBS-2-LS680-56861-22 Solid
04/16/2010 0930 04/17/2010 1045IBS-2-US680-56861-23 Solid
04/15/2010 1735 04/17/2010 1045FB-1680-56861-24FB Water
04/16/2010 0945 04/17/2010 1045FB-2680-56861-25FB Water
04/14/2010 0000 04/17/2010 1045TB-1680-56861-26TB Water
04/15/2010 0000 04/17/2010 1045TB-2680-56861-27TB Water
04/16/2010 1000 04/17/2010 1045RB-1680-56861-28RB Water
TestAmerica Savannah
Page 6 of 238
SAMPLE RESULTS
TestAmerica Savannah
Page 7 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-1-LS
Client Matrix: % Moisture: 53.4
680-56861-1
Solid
Date Sampled: 04/14/2010 0950
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/25/2010 1854
1000000
8260B Analysis Batch: 680-166686
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0466.d
2.8 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
190000000 U 19000000042000000Acetone
770000000 U 770000000160000000Acetonitrile
380000000 U 38000000092000000Acrolein
380000000 U 380000000130000000Acrylonitrile
19000000 U 190000002800000Benzene
19000000 U 190000005700000Bromoform
19000000 U 190000005700000Bromomethane
96000000 U 9600000092000002-Butanone (MEK)
19000000 U 190000004200000Carbon disulfide
19000000 U 190000003200000Carbon tetrachloride
19000000 U 190000003700000Chlorobenzene
19000000 U 1900000080000002-Chloro-1,3-butadiene
19000000 U 190000006500000Chlorodibromomethane
19000000 U 1900000010000000Chloroethane
19000000 U 190000004200000Chloroform
19000000 U 190000003800000Chloromethane
19000000 U 1900000084000003-Chloro-1-propene
19000000 U 190000003200000cis-1,3-Dichloropropene
38000000 U 38000000170000001,2-Dibromo-3-Chloropropane
19000000 U 190000006500000Dibromomethane
19000000 U 190000003700000Dichlorobromomethane
19000000 U 190000003600000Dichlorodifluoromethane
19000000 U 1900000042000001,1-Dichloroethane
19000000 U 1900000042000001,2-Dichloroethane
19000000 U 1900000057000001,1-Dichloroethene
19000000 U 1900000033000001,2-Dichloropropane
19000000 U 190000005000000Ethylbenzene
19000000 U 190000005700000Ethylene Dibromide
19000000 U 1900000013000000Ethyl methacrylate
96000000 U 96000000130000002-Hexanone
19000000 U 190000006900000Iodomethane
770000000 U 770000000200000000Isobutyl alcohol
380000000 U 38000000088000000Methacrylonitrile
19000000 U 190000003800000Methylene Chloride
38000000 U 3800000017000000Methyl methacrylate
96000000 U 96000000160000004-Methyl-2-pentanone (MIBK)
96000000 U 9600000024000000Pentachloroethane
380000000 U 380000000100000000Propionitrile
19000000 U 190000003600000Styrene
19000000 U 1900000092000001,1,1,2-Tetrachloroethane
19000000 U 1900000061000001,1,2,2-Tetrachloroethane
19000000 U 190000007300000Tetrachloroethene
160000000 190000003200000Toluene
38000000 U 3800000011000000trans-1,4-Dichloro-2-butene
19000000 U 190000002400000trans-1,2-Dichloroethene
19000000 U 190000003300000trans-1,3-Dichloropropene
TestAmerica Savannah Page 8 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-1-LS
Client Matrix: % Moisture: 53.4
680-56861-1
Solid
Date Sampled: 04/14/2010 0950
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/25/2010 1854
1000000
8260B Analysis Batch: 680-166686
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0466.d
2.8 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
19000000 U 1900000023000001,1,1-Trichloroethane
19000000 U 1900000050000001,1,2-Trichloroethane
19000000 U 190000005000000Trichloroethene
19000000 U 190000004600000Trichlorofluoromethane
19000000 U 1900000092000001,2,3-Trichloropropane
38000000 U 380000009600000Vinyl acetate
19000000 U 190000005700000Vinyl chloride
38000000 U 380000004200000Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
0 65 - 124D4-Bromofluorobenzene
0 65 - 124DDibromofluoromethane
0 65 - 132DToluene-d8 (Surr)
TestAmerica Savannah Page 9 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-3-NS
Client Matrix: % Moisture: 21.3
680-56861-2
Solid
Date Sampled: 04/14/2010 1245
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/25/2010 1917
1000
8260B Analysis Batch: 680-166686
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0467.d
5.7 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
56000 U 5600012000Acetone
220000 U 22000046000Acetonitrile
110000 U 11000027000Acrolein
110000 U 11000038000Acrylonitrile
2500 J 5600810Benzene
5600 U 56001700Bromoform
5600 U 56001700Bromomethane
28000 U 2800027002-Butanone (MEK)
5600 U 56001200Carbon disulfide
5600 U 5600930Carbon tetrachloride
5600 U 56001100Chlorobenzene
5600 U 560023002-Chloro-1,3-butadiene
5600 U 56001900Chlorodibromomethane
5600 U 56003000Chloroethane
5600 U 56001200Chloroform
5600 U 56001100Chloromethane
5600 U 560025003-Chloro-1-propene
5600 U 5600930cis-1,3-Dichloropropene
11000 U 1100049001,2-Dibromo-3-Chloropropane
5600 U 56001900Dibromomethane
5600 U 56001100Dichlorobromomethane
5600 U 56001000Dichlorodifluoromethane
5600 U 560012001,1-Dichloroethane
5600 U 560012001,2-Dichloroethane
5600 U 560017001,1-Dichloroethene
5600 U 56009601,2-Dichloropropane
5600 U 56001400Ethylbenzene
5600 U 56001700Ethylene Dibromide
5600 U 56003800Ethyl methacrylate
28000 U 2800037002-Hexanone
5600 U 56002000Iodomethane
220000 U 22000058000Isobutyl alcohol
110000 U 11000026000Methacrylonitrile
5600 U 56001100Methylene Chloride
11000 U 110005000Methyl methacrylate
28000 U 2800047004-Methyl-2-pentanone (MIBK)
28000 U 280007000Pentachloroethane
110000 U 11000029000Propionitrile
5600 U 56001000Styrene
5600 U 560027001,1,1,2-Tetrachloroethane
5600 U 560018001,1,2,2-Tetrachloroethane
5600 U 56002100Tetrachloroethene
190000 5600940Toluene
11000 U 110003200trans-1,4-Dichloro-2-butene
5600 U 5600700trans-1,2-Dichloroethene
5600 U 5600970trans-1,3-Dichloropropene
TestAmerica Savannah Page 10 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-3-NS
Client Matrix: % Moisture: 21.3
680-56861-2
Solid
Date Sampled: 04/14/2010 1245
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/25/2010 1917
1000
8260B Analysis Batch: 680-166686
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0467.d
5.7 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
5600 U 56006601,1,1-Trichloroethane
5600 U 560014001,1,2-Trichloroethane
5600 U 56001400Trichloroethene
5600 U 56001300Trichlorofluoromethane
5600 U 560027001,2,3-Trichloropropane
11000 U 110002800Vinyl acetate
5600 U 56001700Vinyl chloride
11000 U 110001200Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
0 65 - 124D4-Bromofluorobenzene
0 65 - 124DDibromofluoromethane
0 65 - 132DToluene-d8 (Surr)
TestAmerica Savannah Page 11 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-3-LS
Client Matrix: % Moisture: 53.4
680-56861-3
Solid
Date Sampled: 04/14/2010 1255
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/27/2010 0930
20000
8260B Analysis Batch: 680-166861
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0508.d
3.5 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
3100000 U 3100000670000Acetone
12000000 U 120000002500000Acetonitrile
6100000 U 61000001500000Acrolein
6100000 U 61000002100000Acrylonitrile
55000 J 31000045000Benzene
310000 U 31000092000Bromoform
310000 U 31000092000Bromomethane
180000 J 15000001500002-Butanone (MEK)
310000 U 31000067000Carbon disulfide
310000 U 31000051000Carbon tetrachloride
310000 U 31000059000Chlorobenzene
310000 U 3100001300002-Chloro-1,3-butadiene
310000 U 310000100000Chlorodibromomethane
310000 U 310000170000Chloroethane
310000 U 31000067000Chloroform
310000 U 31000061000Chloromethane
310000 U 3100001300003-Chloro-1-propene
310000 U 31000051000cis-1,3-Dichloropropene
610000 U 6100002700001,2-Dibromo-3-Chloropropane
310000 U 310000100000Dibromomethane
310000 U 31000059000Dichlorobromomethane
310000 U 31000058000Dichlorodifluoromethane
310000 U 310000670001,1-Dichloroethane
310000 U 310000670001,2-Dichloroethane
310000 U 310000920001,1-Dichloroethene
310000 U 310000530001,2-Dichloropropane
310000 U 31000080000Ethylbenzene
310000 U 31000092000Ethylene Dibromide
310000 U 310000210000Ethyl methacrylate
1500000 U 15000002000002-Hexanone
310000 U 310000110000Iodomethane
12000000 U 120000003200000Isobutyl alcohol
6100000 U 61000001400000Methacrylonitrile
530000 31000060000Methylene Chloride
610000 U 610000280000Methyl methacrylate
1500000 U 15000002600004-Methyl-2-pentanone (MIBK)
1500000 U 1500000390000Pentachloroethane
6100000 U 61000001600000Propionitrile
310000 U 31000057000Styrene
310000 U 3100001500001,1,1,2-Tetrachloroethane
310000 U 310000980001,1,2,2-Tetrachloroethane
310000 U 310000120000Tetrachloroethene
6800000 31000051000Toluene
610000 U 610000180000trans-1,4-Dichloro-2-butene
310000 U 31000039000trans-1,2-Dichloroethene
310000 U 31000053000trans-1,3-Dichloropropene
TestAmerica Savannah Page 12 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-3-LS
Client Matrix: % Moisture: 53.4
680-56861-3
Solid
Date Sampled: 04/14/2010 1255
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/27/2010 0930
20000
8260B Analysis Batch: 680-166861
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0508.d
3.5 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
310000 U 310000360001,1,1-Trichloroethane
310000 U 310000800001,1,2-Trichloroethane
310000 U 31000080000Trichloroethene
310000 U 31000074000Trichlorofluoromethane
310000 U 3100001500001,2,3-Trichloropropane
610000 U 610000150000Vinyl acetate
310000 U 31000092000Vinyl chloride
610000 U 61000067000Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
0 65 - 124D4-Bromofluorobenzene
0 65 - 124DDibromofluoromethane
0 65 - 132DToluene-d8 (Surr)
TestAmerica Savannah Page 13 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-4-NS
Client Matrix: % Moisture: 12.4
680-56861-4
Solid
Date Sampled: 04/14/2010 1715
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/25/2010 2004
1000
8260B Analysis Batch: 680-166686
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0469.d
5.2 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
55000 U 5500012000Acetone
220000 U 22000045000Acetonitrile
110000 U 11000026000Acrolein
110000 U 11000037000Acrylonitrile
37000 5500800Benzene
5500 U 55001600Bromoform
5500 U 55001600Bromomethane
27000 U 2700026002-Butanone (MEK)
5500 U 55001200Carbon disulfide
5500 U 5500910Carbon tetrachloride
5500 U 55001100Chlorobenzene
5500 U 550023002-Chloro-1,3-butadiene
5500 U 55001900Chlorodibromomethane
5500 U 55003000Chloroethane
5500 U 55001200Chloroform
5500 U 55001100Chloromethane
5500 U 550024003-Chloro-1-propene
5500 U 5500910cis-1,3-Dichloropropene
11000 U 1100048001,2-Dibromo-3-Chloropropane
5500 U 55001900Dibromomethane
5500 U 55001100Dichlorobromomethane
5500 U 55001000Dichlorodifluoromethane
5500 U 550012001,1-Dichloroethane
5500 U 550012001,2-Dichloroethane
5500 U 550016001,1-Dichloroethene
5500 U 55009401,2-Dichloropropane
5500 U 55001400Ethylbenzene
5500 U 55001600Ethylene Dibromide
5500 U 55003700Ethyl methacrylate
27000 U 2700036002-Hexanone
5500 U 55002000Iodomethane
220000 U 22000057000Isobutyl alcohol
110000 U 11000025000Methacrylonitrile
5500 U 55001100Methylene Chloride
11000 U 110004900Methyl methacrylate
27000 U 2700046004-Methyl-2-pentanone (MIBK)
27000 U 270006900Pentachloroethane
110000 U 11000029000Propionitrile
5500 U 55001000Styrene
5500 U 550026001,1,1,2-Tetrachloroethane
5500 U 550018001,1,2,2-Tetrachloroethane
5500 U 55002100Tetrachloroethene
150000 5500920Toluene
11000 U 110003200trans-1,4-Dichloro-2-butene
5500 U 5500690trans-1,2-Dichloroethene
5500 U 5500960trans-1,3-Dichloropropene
TestAmerica Savannah Page 14 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-4-NS
Client Matrix: % Moisture: 12.4
680-56861-4
Solid
Date Sampled: 04/14/2010 1715
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/25/2010 2004
1000
8260B Analysis Batch: 680-166686
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0469.d
5.2 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
5500 U 55006501,1,1-Trichloroethane
5500 U 550014001,1,2-Trichloroethane
5500 U 55001400Trichloroethene
5500 U 55001300Trichlorofluoromethane
5500 U 550026001,2,3-Trichloropropane
11000 U 110002700Vinyl acetate
5500 U 55001600Vinyl chloride
11000 U 110001200Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
0 65 - 124D4-Bromofluorobenzene
0 65 - 124DDibromofluoromethane
0 65 - 132DToluene-d8 (Surr)
TestAmerica Savannah Page 15 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-4-LS
Client Matrix: % Moisture: 60.5
680-56861-5
Solid
Date Sampled: 04/14/2010 1735
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/27/2010 0953
50000
8260B Analysis Batch: 680-166861
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0509.d
3.2 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
9900000 U 99000002200000Acetone
40000000 U 400000008100000Acetonitrile
20000000 U 200000004700000Acrolein
20000000 U 200000006700000Acrylonitrile
990000 U 990000140000Benzene
990000 U 990000300000Bromoform
990000 U 990000300000Bromomethane
480000 J 49000004700002-Butanone (MEK)
990000 U 990000220000Carbon disulfide
990000 U 990000160000Carbon tetrachloride
990000 U 990000190000Chlorobenzene
990000 U 9900004200002-Chloro-1,3-butadiene
990000 U 990000340000Chlorodibromomethane
990000 U 990000530000Chloroethane
990000 U 990000220000Chloroform
990000 U 990000200000Chloromethane
990000 U 9900004300003-Chloro-1-propene
990000 U 990000160000cis-1,3-Dichloropropene
2000000 U 20000008700001,2-Dibromo-3-Chloropropane
990000 U 990000340000Dibromomethane
990000 U 990000190000Dichlorobromomethane
990000 U 990000190000Dichlorodifluoromethane
990000 U 9900002200001,1-Dichloroethane
990000 U 9900002200001,2-Dichloroethane
990000 U 9900003000001,1-Dichloroethene
990000 U 9900001700001,2-Dichloropropane
990000 U 990000260000Ethylbenzene
990000 U 990000300000Ethylene Dibromide
990000 U 990000670000Ethyl methacrylate
4900000 U 49000006500002-Hexanone
990000 U 990000360000Iodomethane
40000000 U 4000000010000000Isobutyl alcohol
20000000 U 200000004500000Methacrylonitrile
740000 J 990000190000Methylene Chloride
2000000 U 2000000890000Methyl methacrylate
4900000 U 49000008300004-Methyl-2-pentanone (MIBK)
4900000 U 49000001200000Pentachloroethane
20000000 U 200000005100000Propionitrile
990000 U 990000180000Styrene
990000 U 9900004700001,1,1,2-Tetrachloroethane
990000 U 9900003200001,1,2,2-Tetrachloroethane
990000 U 990000380000Tetrachloroethene
13000000 990000170000Toluene
2000000 U 2000000570000trans-1,4-Dichloro-2-butene
990000 U 990000120000trans-1,2-Dichloroethene
990000 U 990000170000trans-1,3-Dichloropropene
TestAmerica Savannah Page 16 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-4-LS
Client Matrix: % Moisture: 60.5
680-56861-5
Solid
Date Sampled: 04/14/2010 1735
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/27/2010 0953
50000
8260B Analysis Batch: 680-166861
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0509.d
3.2 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
990000 U 9900001200001,1,1-Trichloroethane
990000 U 9900002600001,1,2-Trichloroethane
990000 U 990000260000Trichloroethene
990000 U 990000240000Trichlorofluoromethane
990000 U 9900004700001,2,3-Trichloropropane
2000000 U 2000000490000Vinyl acetate
990000 U 990000300000Vinyl chloride
2000000 U 2000000220000Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
0 65 - 124D4-Bromofluorobenzene
0 65 - 124DDibromofluoromethane
0 65 - 132DToluene-d8 (Surr)
TestAmerica Savannah Page 17 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-3-US
Client Matrix: % Moisture: 75.7
680-56861-6
Solid
Date Sampled: 04/15/2010 0845
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/25/2010 2052
5000
8260B Analysis Batch: 680-166686
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0471.d
3.2 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
1600000 U 1600000350000Acetone
6400000 U 64000001300000Acetonitrile
3200000 U 3200000770000Acrolein
3200000 U 32000001100000Acrylonitrile
160000 U 16000023000Benzene
160000 U 16000048000Bromoform
160000 U 16000048000Bromomethane
800000 U 800000770002-Butanone (MEK)
160000 U 16000035000Carbon disulfide
160000 U 16000027000Carbon tetrachloride
160000 U 16000031000Chlorobenzene
160000 U 160000670002-Chloro-1,3-butadiene
160000 U 16000055000Chlorodibromomethane
160000 U 16000087000Chloroethane
160000 U 16000035000Chloroform
160000 U 16000032000Chloromethane
160000 U 160000710003-Chloro-1-propene
160000 U 16000027000cis-1,3-Dichloropropene
320000 U 3200001400001,2-Dibromo-3-Chloropropane
160000 U 16000055000Dibromomethane
160000 U 16000031000Dichlorobromomethane
160000 U 16000030000Dichlorodifluoromethane
160000 U 160000350001,1-Dichloroethane
160000 U 160000350001,2-Dichloroethane
160000 U 160000480001,1-Dichloroethene
160000 U 160000280001,2-Dichloropropane
160000 U 16000042000Ethylbenzene
160000 U 16000048000Ethylene Dibromide
160000 U 160000110000Ethyl methacrylate
800000 U 8000001100002-Hexanone
160000 U 16000058000Iodomethane
6400000 U 64000001700000Isobutyl alcohol
3200000 U 3200000740000Methacrylonitrile
160000 U 16000031000Methylene Chloride
320000 U 320000140000Methyl methacrylate
800000 U 8000001300004-Methyl-2-pentanone (MIBK)
800000 U 800000200000Pentachloroethane
3200000 U 3200000840000Propionitrile
160000 U 16000030000Styrene
160000 U 160000770001,1,1,2-Tetrachloroethane
160000 U 160000510001,1,2,2-Tetrachloroethane
160000 U 16000061000Tetrachloroethene
2000000 16000027000Toluene
320000 U 32000093000trans-1,4-Dichloro-2-butene
160000 U 16000020000trans-1,2-Dichloroethene
160000 U 16000028000trans-1,3-Dichloropropene
TestAmerica Savannah Page 18 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-3-US
Client Matrix: % Moisture: 75.7
680-56861-6
Solid
Date Sampled: 04/15/2010 0845
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/25/2010 2052
5000
8260B Analysis Batch: 680-166686
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0471.d
3.2 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
160000 U 160000190001,1,1-Trichloroethane
160000 U 160000420001,1,2-Trichloroethane
160000 U 16000042000Trichloroethene
160000 U 16000039000Trichlorofluoromethane
160000 U 160000770001,2,3-Trichloropropane
320000 U 32000080000Vinyl acetate
160000 U 16000048000Vinyl chloride
320000 U 32000035000Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
0 65 - 124D4-Bromofluorobenzene
0 65 - 124DDibromofluoromethane
0 65 - 132DToluene-d8 (Surr)
TestAmerica Savannah Page 19 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-5-NS
Client Matrix: % Moisture: 23.8
680-56861-7
Solid
Date Sampled: 04/15/2010 0950
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/25/2010 2115
04/25/2010 2115
40
8260B Analysis Batch: 680-166686
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0472.d
5.1 g
5 mL
5030A
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
2100 J 2600570Acetone
10000 U 100002100Acetonitrile
5100 U 51001200Acrolein
5100 U 51001800Acrylonitrile
260 U 26038Benzene
260 U 26077Bromoform
260 U 26077Bromomethane
1300 U 13001202-Butanone (MEK)
260 U 26057Carbon disulfide
260 U 26043Carbon tetrachloride
260 U 26049Chlorobenzene
260 U 2601102-Chloro-1,3-butadiene
260 U 26088Chlorodibromomethane
260 U 260140Chloroethane
260 U 26057Chloroform
260 U 26051Chloromethane
260 U 2601103-Chloro-1-propene
260 U 26043cis-1,3-Dichloropropene
510 U 5102301,2-Dibromo-3-Chloropropane
260 U 26088Dibromomethane
260 U 26050Dichlorobromomethane
260 U 26048Dichlorodifluoromethane
260 U 260571,1-Dichloroethane
260 U 260571,2-Dichloroethane
260 U 260771,1-Dichloroethene
260 U 260441,2-Dichloropropane
260 U 26067Ethylbenzene
260 U 26077Ethylene Dibromide
260 U 260180Ethyl methacrylate
1300 U 13001702-Hexanone
260 U 26093Iodomethane
10000 U 100002700Isobutyl alcohol
5100 U 51001200Methacrylonitrile
260 U 26050Methylene Chloride
510 U 510230Methyl methacrylate
1300 U 13002204-Methyl-2-pentanone (MIBK)
1300 U 1300320Pentachloroethane
5100 U 51001300Propionitrile
260 U 26048Styrene
260 U 2601201,1,1,2-Tetrachloroethane
260 U 260821,1,2,2-Tetrachloroethane
260 U 26098Tetrachloroethene
1100 26043Toluene
510 U 510150trans-1,4-Dichloro-2-butene
260 U 26032trans-1,2-Dichloroethene
260 U 26045trans-1,3-Dichloropropene
TestAmerica Savannah Page 20 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-5-NS
Client Matrix: % Moisture: 23.8
680-56861-7
Solid
Date Sampled: 04/15/2010 0950
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/25/2010 2115
04/25/2010 2115
40
8260B Analysis Batch: 680-166686
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0472.d
5.1 g
5 mL
5030A
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
260 U 260301,1,1-Trichloroethane
260 U 260671,1,2-Trichloroethane
260 U 26067Trichloroethene
260 U 26062Trichlorofluoromethane
260 U 2601201,2,3-Trichloropropane
510 U 510130Vinyl acetate
260 U 26077Vinyl chloride
510 U 51057Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
75 65 - 1244-Bromofluorobenzene
56 65 - 124XDibromofluoromethane
66 65 - 132Toluene-d8 (Surr)
TestAmerica Savannah Page 21 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-5-LS
Client Matrix: % Moisture: 68.0
680-56861-8
Solid
Date Sampled: 04/15/2010 1005
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/26/2010 1754
20000
8260B Analysis Batch: 680-166737
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0507.d
3.0 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
5200000 U 52000001100000Acetone
21000000 U 210000004300000Acetonitrile
10000000 U 100000002500000Acrolein
10000000 U 100000003500000Acrylonitrile
520000 U 52000076000Benzene
520000 U 520000160000Bromoform
520000 U 520000160000Bromomethane
2600000 U 26000002500002-Butanone (MEK)
520000 U 520000110000Carbon disulfide
520000 U 52000086000Carbon tetrachloride
520000 U 520000100000Chlorobenzene
520000 U 5200002200002-Chloro-1,3-butadiene
520000 U 520000180000Chlorodibromomethane
520000 U 520000280000Chloroethane
520000 U 520000110000Chloroform
520000 U 520000100000Chloromethane
520000 U 5200002300003-Chloro-1-propene
520000 U 52000086000cis-1,3-Dichloropropene
1000000 U 10000004600001,2-Dibromo-3-Chloropropane
520000 U 520000180000Dibromomethane
520000 U 520000100000Dichlorobromomethane
520000 U 52000098000Dichlorodifluoromethane
520000 U 5200001100001,1-Dichloroethane
520000 U 5200001100001,2-Dichloroethane
520000 U 5200001600001,1-Dichloroethene
520000 U 520000890001,2-Dichloropropane
520000 U 520000140000Ethylbenzene
520000 U 520000160000Ethylene Dibromide
520000 U 520000350000Ethyl methacrylate
2600000 U 26000003400002-Hexanone
520000 U 520000190000Iodomethane
21000000 U 210000005400000Isobutyl alcohol
10000000 U 100000002400000Methacrylonitrile
520000 U 520000100000Methylene Chloride
1000000 U 1000000470000Methyl methacrylate
2600000 U 26000004400004-Methyl-2-pentanone (MIBK)
2600000 U 2600000660000Pentachloroethane
10000000 U 100000002700000Propionitrile
520000 U 52000097000Styrene
520000 U 5200002500001,1,1,2-Tetrachloroethane
520000 U 5200001700001,1,2,2-Tetrachloroethane
520000 U 520000200000Tetrachloroethene
9800000 52000087000Toluene
1000000 U 1000000300000trans-1,4-Dichloro-2-butene
520000 U 52000066000trans-1,2-Dichloroethene
520000 U 52000090000trans-1,3-Dichloropropene
TestAmerica Savannah Page 22 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-5-LS
Client Matrix: % Moisture: 68.0
680-56861-8
Solid
Date Sampled: 04/15/2010 1005
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/26/2010 1754
20000
8260B Analysis Batch: 680-166737
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0507.d
3.0 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
520000 U 520000610001,1,1-Trichloroethane
520000 U 5200001400001,1,2-Trichloroethane
520000 U 520000140000Trichloroethene
520000 U 520000120000Trichlorofluoromethane
520000 U 5200002500001,2,3-Trichloropropane
1000000 U 1000000260000Vinyl acetate
520000 U 520000160000Vinyl chloride
1000000 U 1000000110000Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
0 65 - 124D4-Bromofluorobenzene
0 65 - 124DDibromofluoromethane
0 65 - 132DToluene-d8 (Surr)
TestAmerica Savannah Page 23 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-4-US
Client Matrix: % Moisture: 77.8
680-56861-9
Solid
Date Sampled: 04/15/2010 1100
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/23/2010 1641
1000
8260B Analysis Batch: 680-166615
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0396.d
3.6 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
310000 U 31000069000Acetone
1200000 U 1200000260000Acetonitrile
620000 U 620000150000Acrolein
620000 U 620000210000Acrylonitrile
31000 U 310004600Benzene
31000 U 310009400Bromoform
31000 U 310009400Bromomethane
160000 U 160000150002-Butanone (MEK)
31000 U 310006900Carbon disulfide
31000 U 310005200Carbon tetrachloride
31000 U 310006000Chlorobenzene
31000 U 31000130002-Chloro-1,3-butadiene
31000 U 3100011000Chlorodibromomethane
31000 U 3100017000Chloroethane
31000 U 310006900Chloroform
31000 U 310006200Chloromethane
31000 U 31000140003-Chloro-1-propene
31000 U 310005200cis-1,3-Dichloropropene
62000 U 62000270001,2-Dibromo-3-Chloropropane
31000 U 3100011000Dibromomethane
31000 U 310006100Dichlorobromomethane
31000 U 310005900Dichlorodifluoromethane
31000 U 3100069001,1-Dichloroethane
31000 U 3100069001,2-Dichloroethane
31000 U 3100094001,1-Dichloroethene
31000 U 3100054001,2-Dichloropropane
31000 U 310008100Ethylbenzene
31000 U 310009400Ethylene Dibromide
31000 U 3100021000Ethyl methacrylate
160000 U 160000210002-Hexanone
31000 U 3100011000Iodomethane
1200000 U 1200000320000Isobutyl alcohol
620000 U 620000140000Methacrylonitrile
31000 U 310006100Methylene Chloride
62000 U 6200028000Methyl methacrylate
160000 U 160000260004-Methyl-2-pentanone (MIBK)
160000 U 16000039000Pentachloroethane
620000 U 620000160000Propionitrile
31000 U 310005800Styrene
31000 U 31000150001,1,1,2-Tetrachloroethane
31000 U 31000100001,1,2,2-Tetrachloroethane
31000 U 3100012000Tetrachloroethene
1100000 310005200Toluene
62000 U 6200018000trans-1,4-Dichloro-2-butene
31000 U 310003900trans-1,2-Dichloroethene
31000 U 310005400trans-1,3-Dichloropropene
TestAmerica Savannah Page 24 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-4-US
Client Matrix: % Moisture: 77.8
680-56861-9
Solid
Date Sampled: 04/15/2010 1100
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/23/2010 1641
1000
8260B Analysis Batch: 680-166615
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0396.d
3.6 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
31000 U 3100037001,1,1-Trichloroethane
31000 U 3100081001,1,2-Trichloroethane
31000 U 310008100Trichloroethene
31000 U 310007500Trichlorofluoromethane
31000 U 31000150001,2,3-Trichloropropane
62000 U 6200016000Vinyl acetate
31000 U 310009400Vinyl chloride
62000 U 620006900Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
0 65 - 124D4-Bromofluorobenzene
0 65 - 124DDibromofluoromethane
0 65 - 132DToluene-d8 (Surr)
TestAmerica Savannah Page 25 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-6-NS
Client Matrix: % Moisture: 20.4
680-56861-10
Solid
Date Sampled: 04/15/2010 1105
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/25/2010 2202
400
8260B Analysis Batch: 680-166686
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0474.d
5.2 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
24000 U 240005300Acetone
97000 U 9700020000Acetonitrile
48000 U 4800012000Acrolein
48000 U 4800016000Acrylonitrile
2400 U 2400350Benzene
2400 U 2400720Bromoform
2400 U 2400720Bromomethane
12000 U 1200012002-Butanone (MEK)
2400 U 2400530Carbon disulfide
2400 U 2400400Carbon tetrachloride
2400 U 2400460Chlorobenzene
2400 U 240010002-Chloro-1,3-butadiene
2400 U 2400820Chlorodibromomethane
2400 U 24001300Chloroethane
2400 U 2400530Chloroform
2400 U 2400480Chloromethane
2400 U 240011003-Chloro-1-propene
2400 U 2400400cis-1,3-Dichloropropene
4800 U 480021001,2-Dibromo-3-Chloropropane
2400 U 2400820Dibromomethane
2400 U 2400470Dichlorobromomethane
2400 U 2400450Dichlorodifluoromethane
2400 U 24005301,1-Dichloroethane
2400 U 24005301,2-Dichloroethane
2400 U 24007201,1-Dichloroethene
2400 U 24004201,2-Dichloropropane
2400 U 2400630Ethylbenzene
2400 U 2400720Ethylene Dibromide
2400 U 24001600Ethyl methacrylate
12000 U 1200016002-Hexanone
2400 U 2400870Iodomethane
97000 U 9700025000Isobutyl alcohol
48000 U 4800011000Methacrylonitrile
2400 U 2400470Methylene Chloride
4800 U 48002200Methyl methacrylate
12000 U 1200020004-Methyl-2-pentanone (MIBK)
12000 U 120003000Pentachloroethane
48000 U 4800013000Propionitrile
2400 U 2400450Styrene
2400 U 240012001,1,1,2-Tetrachloroethane
2400 U 24007701,1,2,2-Tetrachloroethane
2400 U 2400920Tetrachloroethene
33000 2400410Toluene
4800 U 48001400trans-1,4-Dichloro-2-butene
2400 U 2400300trans-1,2-Dichloroethene
2400 U 2400420trans-1,3-Dichloropropene
TestAmerica Savannah Page 26 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-6-NS
Client Matrix: % Moisture: 20.4
680-56861-10
Solid
Date Sampled: 04/15/2010 1105
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/25/2010 2202
400
8260B Analysis Batch: 680-166686
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0474.d
5.2 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
2400 U 24002901,1,1-Trichloroethane
2400 U 24006301,1,2-Trichloroethane
2400 U 2400630Trichloroethene
2400 U 2400580Trichlorofluoromethane
2400 U 240012001,2,3-Trichloropropane
4800 U 48001200Vinyl acetate
2400 U 2400720Vinyl chloride
4800 U 4800530Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
0 65 - 124D4-Bromofluorobenzene
0 65 - 124DDibromofluoromethane
0 65 - 132DToluene-d8 (Surr)
TestAmerica Savannah Page 27 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-6-LS
Client Matrix: % Moisture: 59.4
680-56861-11
Solid
Date Sampled: 04/15/2010 1110
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/27/2010 1017
20000
8260B Analysis Batch: 680-166861
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0510.d
3.3 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
3700000 U 3700000820000Acetone
15000000 U 150000003100000Acetonitrile
7500000 U 75000001800000Acrolein
7500000 U 75000002500000Acrylonitrile
370000 U 37000054000Benzene
370000 U 370000110000Bromoform
370000 U 370000110000Bromomethane
1900000 U 19000001800002-Butanone (MEK)
370000 U 37000082000Carbon disulfide
370000 U 37000062000Carbon tetrachloride
370000 U 37000072000Chlorobenzene
370000 U 3700001600002-Chloro-1,3-butadiene
370000 U 370000130000Chlorodibromomethane
370000 U 370000200000Chloroethane
370000 U 37000082000Chloroform
370000 U 37000075000Chloromethane
370000 U 3700001600003-Chloro-1-propene
370000 U 37000062000cis-1,3-Dichloropropene
750000 U 7500003300001,2-Dibromo-3-Chloropropane
370000 U 370000130000Dibromomethane
370000 U 37000072000Dichlorobromomethane
370000 U 37000070000Dichlorodifluoromethane
370000 U 370000820001,1-Dichloroethane
370000 U 370000820001,2-Dichloroethane
370000 U 3700001100001,1-Dichloroethene
370000 U 370000640001,2-Dichloropropane
370000 U 37000097000Ethylbenzene
370000 U 370000110000Ethylene Dibromide
370000 U 370000250000Ethyl methacrylate
1900000 U 19000002500002-Hexanone
370000 U 370000130000Iodomethane
15000000 U 150000003900000Isobutyl alcohol
7500000 U 75000001700000Methacrylonitrile
420000 37000073000Methylene Chloride
750000 U 750000340000Methyl methacrylate
1900000 U 19000003100004-Methyl-2-pentanone (MIBK)
1900000 U 1900000470000Pentachloroethane
7500000 U 75000001900000Propionitrile
370000 U 37000069000Styrene
370000 U 3700001800001,1,1,2-Tetrachloroethane
370000 U 3700001200001,1,2,2-Tetrachloroethane
370000 U 370000140000Tetrachloroethene
14000000 37000063000Toluene
750000 U 750000220000trans-1,4-Dichloro-2-butene
370000 U 37000047000trans-1,2-Dichloroethene
370000 U 37000065000trans-1,3-Dichloropropene
TestAmerica Savannah Page 28 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-6-LS
Client Matrix: % Moisture: 59.4
680-56861-11
Solid
Date Sampled: 04/15/2010 1110
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/27/2010 1017
20000
8260B Analysis Batch: 680-166861
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0510.d
3.3 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
370000 U 370000440001,1,1-Trichloroethane
370000 U 370000970001,1,2-Trichloroethane
370000 U 37000097000Trichloroethene
370000 U 37000089000Trichlorofluoromethane
370000 U 3700001800001,2,3-Trichloropropane
750000 U 750000190000Vinyl acetate
370000 U 370000110000Vinyl chloride
750000 U 75000082000Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
0 65 - 124D4-Bromofluorobenzene
0 65 - 124DDibromofluoromethane
0 65 - 132DToluene-d8 (Surr)
TestAmerica Savannah Page 29 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-5-US
Client Matrix: % Moisture: 82.7
680-56861-12
Solid
Date Sampled: 04/15/2010 1145
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/26/2010 1312
2000
8260B Analysis Batch: 680-166737
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0495.d
3.2 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
910000 U 910000200000Acetone
3600000 U 3600000740000Acetonitrile
1800000 U 1800000430000Acrolein
1800000 U 1800000620000Acrylonitrile
91000 U 9100013000Benzene
91000 U 9100027000Bromoform
91000 U 9100027000Bromomethane
450000 U 450000430002-Butanone (MEK)
91000 U 9100020000Carbon disulfide
91000 U 9100015000Carbon tetrachloride
91000 U 9100017000Chlorobenzene
91000 U 91000380002-Chloro-1,3-butadiene
91000 U 9100031000Chlorodibromomethane
91000 U 9100049000Chloroethane
91000 U 9100020000Chloroform
91000 U 9100018000Chloromethane
91000 U 91000400003-Chloro-1-propene
91000 U 9100015000cis-1,3-Dichloropropene
180000 U 180000800001,2-Dibromo-3-Chloropropane
91000 U 9100031000Dibromomethane
91000 U 9100018000Dichlorobromomethane
91000 U 9100017000Dichlorodifluoromethane
91000 U 91000200001,1-Dichloroethane
91000 U 91000200001,2-Dichloroethane
91000 U 91000270001,1-Dichloroethene
91000 U 91000160001,2-Dichloropropane
91000 U 9100024000Ethylbenzene
91000 U 9100027000Ethylene Dibromide
91000 U 9100062000Ethyl methacrylate
450000 U 450000600002-Hexanone
91000 U 9100033000Iodomethane
3600000 U 3600000940000Isobutyl alcohol
1800000 U 1800000420000Methacrylonitrile
91000 U 9100018000Methylene Chloride
180000 U 18000081000Methyl methacrylate
450000 U 450000760004-Methyl-2-pentanone (MIBK)
450000 U 450000110000Pentachloroethane
1800000 U 1800000470000Propionitrile
91000 U 9100017000Styrene
91000 U 91000430001,1,1,2-Tetrachloroethane
91000 U 91000290001,1,2,2-Tetrachloroethane
91000 U 9100034000Tetrachloroethene
980000 9100015000Toluene
180000 U 18000053000trans-1,4-Dichloro-2-butene
91000 U 9100011000trans-1,2-Dichloroethene
91000 U 9100016000trans-1,3-Dichloropropene
TestAmerica Savannah Page 30 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-5-US
Client Matrix: % Moisture: 82.7
680-56861-12
Solid
Date Sampled: 04/15/2010 1145
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/26/2010 1312
2000
8260B Analysis Batch: 680-166737
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0495.d
3.2 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
91000 U 91000110001,1,1-Trichloroethane
91000 U 91000240001,1,2-Trichloroethane
91000 U 9100024000Trichloroethene
91000 U 9100022000Trichlorofluoromethane
91000 U 91000430001,2,3-Trichloropropane
180000 U 18000045000Vinyl acetate
91000 U 9100027000Vinyl chloride
180000 U 18000020000Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
0 65 - 124D4-Bromofluorobenzene
0 65 - 124DDibromofluoromethane
0 65 - 132DToluene-d8 (Surr)
TestAmerica Savannah Page 31 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-6-US
Client Matrix: % Moisture: 82.7
680-56861-13
Solid
Date Sampled: 04/15/2010 1415
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/25/2010 2313
2000
8260B Analysis Batch: 680-166686
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0477.d
3.5 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
830000 U 830000180000Acetone
3300000 U 3300000680000Acetonitrile
1700000 U 1700000400000Acrolein
1700000 U 1700000560000Acrylonitrile
83000 U 8300012000Benzene
83000 U 8300025000Bromoform
83000 U 8300025000Bromomethane
410000 U 410000400002-Butanone (MEK)
83000 U 8300018000Carbon disulfide
83000 U 8300014000Carbon tetrachloride
83000 U 8300016000Chlorobenzene
83000 U 83000350002-Chloro-1,3-butadiene
83000 U 8300028000Chlorodibromomethane
83000 U 8300045000Chloroethane
83000 U 8300018000Chloroform
83000 U 8300017000Chloromethane
83000 U 83000360003-Chloro-1-propene
83000 U 8300014000cis-1,3-Dichloropropene
170000 U 170000730001,2-Dibromo-3-Chloropropane
83000 U 8300028000Dibromomethane
83000 U 8300016000Dichlorobromomethane
83000 U 8300016000Dichlorodifluoromethane
83000 U 83000180001,1-Dichloroethane
83000 U 83000180001,2-Dichloroethane
83000 U 83000250001,1-Dichloroethene
83000 U 83000140001,2-Dichloropropane
83000 U 8300022000Ethylbenzene
83000 U 8300025000Ethylene Dibromide
83000 U 8300056000Ethyl methacrylate
410000 U 410000550002-Hexanone
83000 U 8300030000Iodomethane
3300000 U 3300000860000Isobutyl alcohol
1700000 U 1700000380000Methacrylonitrile
83000 U 8300016000Methylene Chloride
170000 U 17000074000Methyl methacrylate
410000 U 410000700004-Methyl-2-pentanone (MIBK)
410000 U 410000100000Pentachloroethane
1700000 U 1700000430000Propionitrile
83000 U 8300015000Styrene
83000 U 83000400001,1,1,2-Tetrachloroethane
83000 U 83000260001,1,2,2-Tetrachloroethane
83000 U 8300031000Tetrachloroethene
1800000 8300014000Toluene
170000 U 17000048000trans-1,4-Dichloro-2-butene
83000 U 8300010000trans-1,2-Dichloroethene
83000 U 8300014000trans-1,3-Dichloropropene
TestAmerica Savannah Page 32 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-6-US
Client Matrix: % Moisture: 82.7
680-56861-13
Solid
Date Sampled: 04/15/2010 1415
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/25/2010 2313
2000
8260B Analysis Batch: 680-166686
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0477.d
3.5 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
83000 U 8300098001,1,1-Trichloroethane
83000 U 83000220001,1,2-Trichloroethane
83000 U 8300022000Trichloroethene
83000 U 8300020000Trichlorofluoromethane
83000 U 83000400001,2,3-Trichloropropane
170000 U 17000041000Vinyl acetate
83000 U 8300025000Vinyl chloride
170000 U 17000018000Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
0 65 - 124D4-Bromofluorobenzene
0 65 - 124DDibromofluoromethane
0 65 - 132DToluene-d8 (Surr)
TestAmerica Savannah Page 33 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-7-NS
Client Matrix: % Moisture: 16.9
680-56861-14
Solid
Date Sampled: 04/15/2010 1505
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/26/2010 1359
2000
8260B Analysis Batch: 680-166737
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0497.d
6.2 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
97000 U 9700021000Acetone
390000 U 39000080000Acetonitrile
190000 U 19000047000Acrolein
190000 U 19000066000Acrylonitrile
110000 97001400Benzene
9700 U 97002900Bromoform
9700 U 97002900Bromomethane
49000 U 4900047002-Butanone (MEK)
9700 U 97002100Carbon disulfide
9700 U 97001600Carbon tetrachloride
9700 U 97001900Chlorobenzene
9700 U 970041002-Chloro-1,3-butadiene
9700 U 97003300Chlorodibromomethane
9700 U 97005200Chloroethane
9700 U 97002100Chloroform
9700 U 97001900Chloromethane
9700 U 970043003-Chloro-1-propene
9700 U 97001600cis-1,3-Dichloropropene
19000 U 1900085001,2-Dibromo-3-Chloropropane
9700 U 97003300Dibromomethane
9700 U 97001900Dichlorobromomethane
9700 U 97001800Dichlorodifluoromethane
9700 U 970021001,1-Dichloroethane
9700 U 970021001,2-Dichloroethane
9700 U 970029001,1-Dichloroethene
9700 U 970017001,2-Dichloropropane
9700 U 97002500Ethylbenzene
9700 U 97002900Ethylene Dibromide
9700 U 97006600Ethyl methacrylate
49000 U 4900064002-Hexanone
9700 U 97003500Iodomethane
390000 U 390000100000Isobutyl alcohol
190000 U 19000045000Methacrylonitrile
9700 U 97001900Methylene Chloride
19000 U 190008700Methyl methacrylate
49000 U 4900082004-Methyl-2-pentanone (MIBK)
49000 U 4900012000Pentachloroethane
190000 U 19000050000Propionitrile
9700 U 97001800Styrene
9700 U 970047001,1,1,2-Tetrachloroethane
9700 U 970031001,1,2,2-Tetrachloroethane
9700 U 97003700Tetrachloroethene
70000 97001600Toluene
19000 U 190005600trans-1,4-Dichloro-2-butene
9700 U 97001200trans-1,2-Dichloroethene
9700 U 97001700trans-1,3-Dichloropropene
TestAmerica Savannah Page 34 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-7-NS
Client Matrix: % Moisture: 16.9
680-56861-14
Solid
Date Sampled: 04/15/2010 1505
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/26/2010 1359
2000
8260B Analysis Batch: 680-166737
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0497.d
6.2 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
9700 U 970011001,1,1-Trichloroethane
9700 U 970025001,1,2-Trichloroethane
9700 U 97002500Trichloroethene
9700 U 97002300Trichlorofluoromethane
9700 U 970047001,2,3-Trichloropropane
19000 U 190004900Vinyl acetate
9700 U 97002900Vinyl chloride
19000 U 190002100Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
0 65 - 124D4-Bromofluorobenzene
0 65 - 124DDibromofluoromethane
0 65 - 132DToluene-d8 (Surr)
TestAmerica Savannah Page 35 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-7-LS
Client Matrix: % Moisture: 70.7
680-56861-15
Solid
Date Sampled: 04/15/2010 1520
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/26/2010 0000
20000
8260B Analysis Batch: 680-166686
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0479.d
3.4 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
5000000 U 50000001100000Acetone
20000000 U 200000004100000Acetonitrile
10000000 U 100000002400000Acrolein
10000000 U 100000003400000Acrylonitrile
500000 U 50000073000Benzene
500000 U 500000150000Bromoform
500000 U 500000150000Bromomethane
2500000 U 25000002400002-Butanone (MEK)
500000 U 500000110000Carbon disulfide
500000 U 50000083000Carbon tetrachloride
500000 U 50000096000Chlorobenzene
500000 U 5000002100002-Chloro-1,3-butadiene
500000 U 500000170000Chlorodibromomethane
500000 U 500000270000Chloroethane
500000 U 500000110000Chloroform
500000 U 500000100000Chloromethane
500000 U 5000002200003-Chloro-1-propene
500000 U 50000083000cis-1,3-Dichloropropene
1000000 U 10000004400001,2-Dibromo-3-Chloropropane
500000 U 500000170000Dibromomethane
500000 U 50000097000Dichlorobromomethane
500000 U 50000094000Dichlorodifluoromethane
500000 U 5000001100001,1-Dichloroethane
500000 U 5000001100001,2-Dichloroethane
500000 U 5000001500001,1-Dichloroethene
500000 U 500000860001,2-Dichloropropane
500000 U 500000130000Ethylbenzene
500000 U 500000150000Ethylene Dibromide
500000 U 500000340000Ethyl methacrylate
2500000 U 25000003300002-Hexanone
500000 U 500000180000Iodomethane
20000000 U 200000005200000Isobutyl alcohol
10000000 U 100000002300000Methacrylonitrile
500000 U 50000098000Methylene Chloride
1000000 U 1000000450000Methyl methacrylate
2500000 U 25000004200004-Methyl-2-pentanone (MIBK)
2500000 U 2500000630000Pentachloroethane
10000000 U 100000002600000Propionitrile
500000 U 50000093000Styrene
500000 U 5000002400001,1,1,2-Tetrachloroethane
500000 U 5000001600001,1,2,2-Tetrachloroethane
500000 U 500000190000Tetrachloroethene
5900000 50000084000Toluene
1000000 U 1000000290000trans-1,4-Dichloro-2-butene
500000 U 50000063000trans-1,2-Dichloroethene
500000 U 50000087000trans-1,3-Dichloropropene
TestAmerica Savannah Page 36 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-7-LS
Client Matrix: % Moisture: 70.7
680-56861-15
Solid
Date Sampled: 04/15/2010 1520
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/26/2010 0000
20000
8260B Analysis Batch: 680-166686
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0479.d
3.4 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
500000 U 500000590001,1,1-Trichloroethane
500000 U 5000001300001,1,2-Trichloroethane
500000 U 500000130000Trichloroethene
500000 U 500000120000Trichlorofluoromethane
500000 U 5000002400001,2,3-Trichloropropane
1000000 U 1000000250000Vinyl acetate
500000 U 500000150000Vinyl chloride
1000000 U 1000000110000Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
0 65 - 124D4-Bromofluorobenzene
0 65 - 124DDibromofluoromethane
0 65 - 132DToluene-d8 (Surr)
TestAmerica Savannah Page 37 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-7-US
Client Matrix: % Moisture: 73.7
680-56861-16
Solid
Date Sampled: 04/15/2010 1525
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/26/2010 0024
10000
8260B Analysis Batch: 680-166686
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0480.d
3.3 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
2900000 U 2900000630000Acetone
12000000 U 120000002400000Acetonitrile
5800000 U 58000001400000Acrolein
5800000 U 58000002000000Acrylonitrile
290000 U 29000042000Benzene
290000 U 29000086000Bromoform
290000 U 29000086000Bromomethane
1400000 U 14000001400002-Butanone (MEK)
290000 U 29000063000Carbon disulfide
290000 U 29000048000Carbon tetrachloride
290000 U 29000055000Chlorobenzene
290000 U 2900001200002-Chloro-1,3-butadiene
290000 U 29000098000Chlorodibromomethane
290000 U 290000160000Chloroethane
290000 U 29000063000Chloroform
290000 U 29000058000Chloromethane
290000 U 2900001300003-Chloro-1-propene
290000 U 29000048000cis-1,3-Dichloropropene
580000 U 5800002500001,2-Dibromo-3-Chloropropane
290000 U 29000098000Dibromomethane
290000 U 29000056000Dichlorobromomethane
290000 U 29000054000Dichlorodifluoromethane
290000 U 290000630001,1-Dichloroethane
290000 U 290000630001,2-Dichloroethane
290000 U 290000860001,1-Dichloroethene
290000 U 290000500001,2-Dichloropropane
290000 U 29000075000Ethylbenzene
290000 U 29000086000Ethylene Dibromide
290000 U 290000200000Ethyl methacrylate
1400000 U 14000001900002-Hexanone
290000 U 290000100000Iodomethane
12000000 U 120000003000000Isobutyl alcohol
5800000 U 58000001300000Methacrylonitrile
290000 U 29000056000Methylene Chloride
580000 U 580000260000Methyl methacrylate
1400000 U 14000002400004-Methyl-2-pentanone (MIBK)
1400000 U 1400000360000Pentachloroethane
5800000 U 58000001500000Propionitrile
290000 U 29000054000Styrene
290000 U 2900001400001,1,1,2-Tetrachloroethane
290000 U 290000920001,1,2,2-Tetrachloroethane
290000 U 290000110000Tetrachloroethene
2800000 29000048000Toluene
580000 U 580000170000trans-1,4-Dichloro-2-butene
290000 U 29000036000trans-1,2-Dichloroethene
290000 U 29000050000trans-1,3-Dichloropropene
TestAmerica Savannah Page 38 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-7-US
Client Matrix: % Moisture: 73.7
680-56861-16
Solid
Date Sampled: 04/15/2010 1525
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/26/2010 0024
10000
8260B Analysis Batch: 680-166686
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0480.d
3.3 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
290000 U 290000340001,1,1-Trichloroethane
290000 U 290000750001,1,2-Trichloroethane
290000 U 29000075000Trichloroethene
290000 U 29000069000Trichlorofluoromethane
290000 U 2900001400001,2,3-Trichloropropane
580000 U 580000140000Vinyl acetate
290000 U 29000086000Vinyl chloride
580000 U 58000063000Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
0 65 - 124D4-Bromofluorobenzene
0 65 - 124DDibromofluoromethane
0 65 - 132DToluene-d8 (Surr)
TestAmerica Savannah Page 39 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-8-NS
Client Matrix: % Moisture: 27.7
680-56861-17
Solid
Date Sampled: 04/15/2010 1600
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/27/2010 1040
200
8260B Analysis Batch: 680-166861
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0511.d
5.2 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
13000 U 130002900Acetone
53000 U 5300011000Acetonitrile
27000 U 270006400Acrolein
27000 U 270009000Acrylonitrile
390 J 1300190Benzene
1300 U 1300400Bromoform
1300 U 1300400Bromomethane
840 J 66006402-Butanone (MEK)
1300 U 1300290Carbon disulfide
1300 U 1300220Carbon tetrachloride
1300 U 1300260Chlorobenzene
1300 U 13005602-Chloro-1,3-butadiene
1300 U 1300450Chlorodibromomethane
1300 U 1300720Chloroethane
1300 U 1300290Chloroform
1300 U 1300270Chloromethane
1300 U 13005803-Chloro-1-propene
1300 U 1300220cis-1,3-Dichloropropene
2700 U 270012001,2-Dibromo-3-Chloropropane
1300 U 1300450Dibromomethane
1300 U 1300260Dichlorobromomethane
1300 U 1300250Dichlorodifluoromethane
1300 U 13002901,1-Dichloroethane
1300 U 13002901,2-Dichloroethane
1300 U 13004001,1-Dichloroethene
1300 U 13002301,2-Dichloropropane
1300 U 1300350Ethylbenzene
1300 U 1300400Ethylene Dibromide
1300 U 1300900Ethyl methacrylate
6600 U 66008802-Hexanone
1300 U 1300480Iodomethane
53000 U 5300014000Isobutyl alcohol
27000 U 270006100Methacrylonitrile
1600 1300260Methylene Chloride
2700 U 27001200Methyl methacrylate
6600 U 660011004-Methyl-2-pentanone (MIBK)
6600 U 66001700Pentachloroethane
27000 U 270006900Propionitrile
1300 U 1300250Styrene
1300 U 13006401,1,1,2-Tetrachloroethane
1300 U 13004301,1,2,2-Tetrachloroethane
1300 U 1300510Tetrachloroethene
17000 1300220Toluene
2700 U 2700770trans-1,4-Dichloro-2-butene
1300 U 1300170trans-1,2-Dichloroethene
1300 U 1300230trans-1,3-Dichloropropene
TestAmerica Savannah Page 40 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-8-NS
Client Matrix: % Moisture: 27.7
680-56861-17
Solid
Date Sampled: 04/15/2010 1600
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/27/2010 1040
200
8260B Analysis Batch: 680-166861
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0511.d
5.2 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
1300 U 13001601,1,1-Trichloroethane
1300 U 13003501,1,2-Trichloroethane
1300 U 1300350Trichloroethene
1300 U 1300320Trichlorofluoromethane
1300 U 13006401,2,3-Trichloropropane
2700 U 2700660Vinyl acetate
1300 U 1300400Vinyl chloride
2700 U 2700290Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
96 65 - 1244-Bromofluorobenzene
77 65 - 124Dibromofluoromethane
75 65 - 132Toluene-d8 (Surr)
TestAmerica Savannah Page 41 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-8-LS
Client Matrix: % Moisture: 75.4
680-56861-18
Solid
Date Sampled: 04/15/2010 1615
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/27/2010 1104
20000
8260B Analysis Batch: 680-166861
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0512.d
3.1 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
6600000 U 66000001400000Acetone
26000000 U 260000005400000Acetonitrile
13000000 U 130000003100000Acrolein
13000000 U 130000004500000Acrylonitrile
660000 U 66000096000Benzene
660000 U 660000200000Bromoform
660000 U 660000200000Bromomethane
3300000 U 33000003100002-Butanone (MEK)
660000 U 660000140000Carbon disulfide
660000 U 660000110000Carbon tetrachloride
660000 U 660000130000Chlorobenzene
660000 U 6600002800002-Chloro-1,3-butadiene
660000 U 660000220000Chlorodibromomethane
660000 U 660000350000Chloroethane
660000 U 660000140000Chloroform
660000 U 660000130000Chloromethane
660000 U 6600002900003-Chloro-1-propene
660000 U 660000110000cis-1,3-Dichloropropene
1300000 U 13000005800001,2-Dibromo-3-Chloropropane
660000 U 660000220000Dibromomethane
660000 U 660000130000Dichlorobromomethane
660000 U 660000120000Dichlorodifluoromethane
660000 U 6600001400001,1-Dichloroethane
660000 U 6600001400001,2-Dichloroethane
660000 U 6600002000001,1-Dichloroethene
660000 U 6600001100001,2-Dichloropropane
660000 U 660000170000Ethylbenzene
660000 U 660000200000Ethylene Dibromide
660000 U 660000450000Ethyl methacrylate
3300000 U 33000004300002-Hexanone
660000 U 660000240000Iodomethane
26000000 U 260000006800000Isobutyl alcohol
13000000 U 130000003000000Methacrylonitrile
610000 J 660000130000Methylene Chloride
1300000 U 1300000590000Methyl methacrylate
3300000 U 33000005500004-Methyl-2-pentanone (MIBK)
3300000 U 3300000830000Pentachloroethane
13000000 U 130000003400000Propionitrile
660000 U 660000120000Styrene
660000 U 6600003100001,1,1,2-Tetrachloroethane
660000 U 6600002100001,1,2,2-Tetrachloroethane
660000 U 660000250000Tetrachloroethene
14000000 660000110000Toluene
1300000 U 1300000380000trans-1,4-Dichloro-2-butene
660000 U 66000083000trans-1,2-Dichloroethene
660000 U 660000110000trans-1,3-Dichloropropene
TestAmerica Savannah Page 42 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-8-LS
Client Matrix: % Moisture: 75.4
680-56861-18
Solid
Date Sampled: 04/15/2010 1615
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/27/2010 1104
20000
8260B Analysis Batch: 680-166861
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0512.d
3.1 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
660000 U 660000770001,1,1-Trichloroethane
660000 U 6600001700001,1,2-Trichloroethane
660000 U 660000170000Trichloroethene
660000 U 660000160000Trichlorofluoromethane
660000 U 6600003100001,2,3-Trichloropropane
1300000 U 1300000330000Vinyl acetate
660000 U 660000200000Vinyl chloride
1300000 U 1300000140000Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
0 65 - 124D4-Bromofluorobenzene
0 65 - 124DDibromofluoromethane
0 65 - 132DToluene-d8 (Surr)
TestAmerica Savannah Page 43 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-8-US
Client Matrix: % Moisture: 86.3
680-56861-19
Solid
Date Sampled: 04/15/2010 1620
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/26/2010 1509
1000
8260B Analysis Batch: 680-166737
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0500.d
3.2 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
570000 U 570000130000Acetone
2300000 U 2300000470000Acetonitrile
1100000 U 1100000270000Acrolein
1100000 U 1100000390000Acrylonitrile
57000 U 570008300Benzene
57000 U 5700017000Bromoform
57000 U 5700017000Bromomethane
290000 U 290000270002-Butanone (MEK)
57000 U 5700013000Carbon disulfide
57000 U 570009500Carbon tetrachloride
57000 U 5700011000Chlorobenzene
57000 U 57000240002-Chloro-1,3-butadiene
57000 U 5700019000Chlorodibromomethane
57000 U 5700031000Chloroethane
57000 U 5700013000Chloroform
57000 U 5700011000Chloromethane
57000 U 57000250003-Chloro-1-propene
57000 U 570009500cis-1,3-Dichloropropene
110000 U 110000500001,2-Dibromo-3-Chloropropane
57000 U 5700019000Dibromomethane
57000 U 5700011000Dichlorobromomethane
57000 U 5700011000Dichlorodifluoromethane
57000 U 57000130001,1-Dichloroethane
57000 U 57000130001,2-Dichloroethane
57000 U 57000170001,1-Dichloroethene
57000 U 5700098001,2-Dichloropropane
57000 U 5700015000Ethylbenzene
57000 U 5700017000Ethylene Dibromide
57000 U 5700039000Ethyl methacrylate
290000 U 290000380002-Hexanone
57000 U 5700021000Iodomethane
2300000 U 2300000590000Isobutyl alcohol
1100000 U 1100000260000Methacrylonitrile
57000 U 5700011000Methylene Chloride
110000 U 11000051000Methyl methacrylate
290000 U 290000480004-Methyl-2-pentanone (MIBK)
290000 U 29000072000Pentachloroethane
1100000 U 1100000300000Propionitrile
57000 U 5700011000Styrene
57000 U 57000270001,1,1,2-Tetrachloroethane
57000 U 57000180001,1,2,2-Tetrachloroethane
57000 U 5700022000Tetrachloroethene
810000 570009600Toluene
110000 U 11000033000trans-1,4-Dichloro-2-butene
57000 U 570007200trans-1,2-Dichloroethene
57000 U 570009900trans-1,3-Dichloropropene
TestAmerica Savannah Page 44 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-8-US
Client Matrix: % Moisture: 86.3
680-56861-19
Solid
Date Sampled: 04/15/2010 1620
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/26/2010 1509
1000
8260B Analysis Batch: 680-166737
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0500.d
3.2 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
57000 U 5700067001,1,1-Trichloroethane
57000 U 57000150001,1,2-Trichloroethane
57000 U 5700015000Trichloroethene
57000 U 5700014000Trichlorofluoromethane
57000 U 57000270001,2,3-Trichloropropane
110000 U 11000029000Vinyl acetate
57000 U 5700017000Vinyl chloride
110000 U 11000013000Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
0 65 - 124D4-Bromofluorobenzene
0 65 - 124DDibromofluoromethane
0 65 - 132DToluene-d8 (Surr)
TestAmerica Savannah Page 45 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-1-US
Client Matrix: % Moisture: 62.6
680-56861-20
Solid
Date Sampled: 04/15/2010 1700
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/26/2010 1533
2000
8260B Analysis Batch: 680-166737
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0501.d
3.4 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
390000 U 39000087000Acetone
1600000 U 1600000320000Acetonitrile
790000 U 790000190000Acrolein
790000 U 790000270000Acrylonitrile
55000 390005700Benzene
39000 U 3900012000Bromoform
39000 U 3900012000Bromomethane
200000 U 200000190002-Butanone (MEK)
39000 U 390008700Carbon disulfide
39000 U 390006500Carbon tetrachloride
39000 U 390007600Chlorobenzene
39000 U 39000170002-Chloro-1,3-butadiene
39000 U 3900013000Chlorodibromomethane
39000 U 3900021000Chloroethane
39000 U 390008700Chloroform
39000 U 390007900Chloromethane
39000 U 39000170003-Chloro-1-propene
39000 U 390006500cis-1,3-Dichloropropene
79000 U 79000350001,2-Dibromo-3-Chloropropane
39000 U 3900013000Dibromomethane
39000 U 390007600Dichlorobromomethane
39000 U 390007400Dichlorodifluoromethane
39000 U 3900087001,1-Dichloroethane
39000 U 3900087001,2-Dichloroethane
39000 U 39000120001,1-Dichloroethene
39000 U 3900068001,2-Dichloropropane
39000 U 3900010000Ethylbenzene
39000 U 3900012000Ethylene Dibromide
39000 U 3900027000Ethyl methacrylate
200000 U 200000260002-Hexanone
39000 U 3900014000Iodomethane
1600000 U 1600000410000Isobutyl alcohol
790000 U 790000180000Methacrylonitrile
39000 U 390007700Methylene Chloride
79000 U 7900035000Methyl methacrylate
200000 U 200000330004-Methyl-2-pentanone (MIBK)
200000 U 20000050000Pentachloroethane
790000 U 790000200000Propionitrile
39000 U 390007300Styrene
39000 U 39000190001,1,1,2-Tetrachloroethane
39000 U 39000130001,1,2,2-Tetrachloroethane
39000 U 3900015000Tetrachloroethene
820000 390006600Toluene
79000 U 7900023000trans-1,4-Dichloro-2-butene
39000 U 390005000trans-1,2-Dichloroethene
39000 U 390006800trans-1,3-Dichloropropene
TestAmerica Savannah Page 46 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-1-US
Client Matrix: % Moisture: 62.6
680-56861-20
Solid
Date Sampled: 04/15/2010 1700
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/26/2010 1533
2000
8260B Analysis Batch: 680-166737
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0501.d
3.4 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
39000 U 3900046001,1,1-Trichloroethane
39000 U 39000100001,1,2-Trichloroethane
39000 U 3900010000Trichloroethene
39000 U 390009400Trichlorofluoromethane
39000 U 39000190001,2,3-Trichloropropane
79000 U 7900020000Vinyl acetate
39000 U 3900012000Vinyl chloride
79000 U 790008700Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
0 65 - 124D4-Bromofluorobenzene
0 65 - 124DDibromofluoromethane
0 65 - 132DToluene-d8 (Surr)
TestAmerica Savannah Page 47 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-2-NS
Client Matrix: % Moisture: 14.5
680-56861-21
Solid
Date Sampled: 04/16/2010 0840
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/26/2010 1556
2000
8260B Analysis Batch: 680-166737
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0502.d
6.3 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
93000 U 9300020000Acetone
370000 U 37000076000Acetonitrile
190000 U 19000045000Acrolein
190000 U 19000063000Acrylonitrile
17000 93001400Benzene
9300 U 93002800Bromoform
9300 U 93002800Bromomethane
46000 U 4600045002-Butanone (MEK)
9300 U 93002000Carbon disulfide
14000 93001500Carbon tetrachloride
9300 U 93001800Chlorobenzene
9300 U 930039002-Chloro-1,3-butadiene
9300 U 93003200Chlorodibromomethane
9300 U 93005000Chloroethane
2100 J 93002000Chloroform
9300 U 93001900Chloromethane
9300 U 930041003-Chloro-1-propene
9300 U 93001500cis-1,3-Dichloropropene
19000 U 1900082001,2-Dibromo-3-Chloropropane
9300 U 93003200Dibromomethane
9300 U 93001800Dichlorobromomethane
9300 U 93001700Dichlorodifluoromethane
9300 U 930020001,1-Dichloroethane
9300 U 930020001,2-Dichloroethane
9300 U 930028001,1-Dichloroethene
9300 U 930016001,2-Dichloropropane
9300 U 93002400Ethylbenzene
9300 U 93002800Ethylene Dibromide
9300 U 93006300Ethyl methacrylate
46000 U 4600061002-Hexanone
9300 U 93003300Iodomethane
370000 U 37000097000Isobutyl alcohol
190000 U 19000043000Methacrylonitrile
9300 U 93001800Methylene Chloride
19000 U 190008400Methyl methacrylate
46000 U 4600078004-Methyl-2-pentanone (MIBK)
46000 U 4600012000Pentachloroethane
190000 U 19000048000Propionitrile
9300 U 93001700Styrene
9300 U 930045001,1,1,2-Tetrachloroethane
9300 U 930030001,1,2,2-Tetrachloroethane
9300 U 93003500Tetrachloroethene
290000 93001600Toluene
19000 U 190005400trans-1,4-Dichloro-2-butene
9300 U 93001200trans-1,2-Dichloroethene
9300 U 93001600trans-1,3-Dichloropropene
TestAmerica Savannah Page 48 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-2-NS
Client Matrix: % Moisture: 14.5
680-56861-21
Solid
Date Sampled: 04/16/2010 0840
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/26/2010 1556
2000
8260B Analysis Batch: 680-166737
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0502.d
6.3 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
9300 U 930011001,1,1-Trichloroethane
9300 U 930024001,1,2-Trichloroethane
9300 U 93002400Trichloroethene
9300 U 93002200Trichlorofluoromethane
9300 U 930045001,2,3-Trichloropropane
19000 U 190004600Vinyl acetate
9300 U 93002800Vinyl chloride
19000 U 190002000Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
0 65 - 124D4-Bromofluorobenzene
0 65 - 124DDibromofluoromethane
0 65 - 132DToluene-d8 (Surr)
TestAmerica Savannah Page 49 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-2-LS
Client Matrix: % Moisture: 66.8
680-56861-22
Solid
Date Sampled: 04/16/2010 0850
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/26/2010 1620
50000
8260B Analysis Batch: 680-166737
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0503.d
3.3 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
11000000 U 110000002500000Acetone
46000000 U 460000009300000Acetonitrile
23000000 U 230000005500000Acrolein
23000000 U 230000007800000Acrylonitrile
1100000 U 1100000170000Benzene
1100000 U 1100000340000Bromoform
1100000 U 1100000340000Bromomethane
5700000 U 57000005500002-Butanone (MEK)
1100000 U 1100000250000Carbon disulfide
1100000 U 1100000190000Carbon tetrachloride
1100000 U 1100000220000Chlorobenzene
1100000 U 11000004800002-Chloro-1,3-butadiene
1100000 U 1100000390000Chlorodibromomethane
1100000 U 1100000620000Chloroethane
1100000 U 1100000250000Chloroform
1100000 U 1100000230000Chloromethane
1100000 U 11000005000003-Chloro-1-propene
1100000 U 1100000190000cis-1,3-Dichloropropene
2300000 U 230000010000001,2-Dibromo-3-Chloropropane
1100000 U 1100000390000Dibromomethane
1100000 U 1100000220000Dichlorobromomethane
1100000 U 1100000210000Dichlorodifluoromethane
1100000 U 11000002500001,1-Dichloroethane
1100000 U 11000002500001,2-Dichloroethane
1100000 U 11000003400001,1-Dichloroethene
1100000 U 11000002000001,2-Dichloropropane
1100000 U 1100000300000Ethylbenzene
1100000 U 1100000340000Ethylene Dibromide
1100000 U 1100000780000Ethyl methacrylate
5700000 U 57000007500002-Hexanone
1100000 U 1100000410000Iodomethane
46000000 U 4600000012000000Isobutyl alcohol
23000000 U 230000005200000Methacrylonitrile
1100000 U 1100000220000Methylene Chloride
2300000 U 23000001000000Methyl methacrylate
5700000 U 57000009600004-Methyl-2-pentanone (MIBK)
5700000 U 57000001400000Pentachloroethane
23000000 U 230000005900000Propionitrile
1100000 U 1100000210000Styrene
1100000 U 11000005500001,1,1,2-Tetrachloroethane
1100000 U 11000003600001,1,2,2-Tetrachloroethane
1100000 U 1100000430000Tetrachloroethene
9400000 1100000190000Toluene
2300000 U 2300000660000trans-1,4-Dichloro-2-butene
1100000 U 1100000140000trans-1,2-Dichloroethene
1100000 U 1100000200000trans-1,3-Dichloropropene
TestAmerica Savannah Page 50 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-2-LS
Client Matrix: % Moisture: 66.8
680-56861-22
Solid
Date Sampled: 04/16/2010 0850
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/26/2010 1620
50000
8260B Analysis Batch: 680-166737
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0503.d
3.3 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
1100000 U 11000001300001,1,1-Trichloroethane
1100000 U 11000003000001,1,2-Trichloroethane
1100000 U 1100000300000Trichloroethene
1100000 U 1100000270000Trichlorofluoromethane
1100000 U 11000005500001,2,3-Trichloropropane
2300000 U 2300000570000Vinyl acetate
1100000 U 1100000340000Vinyl chloride
2300000 U 2300000250000Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
0 65 - 124D4-Bromofluorobenzene
0 65 - 124DDibromofluoromethane
0 65 - 132DToluene-d8 (Surr)
TestAmerica Savannah Page 51 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-2-US
Client Matrix: % Moisture: 78.7
680-56861-23
Solid
Date Sampled: 04/16/2010 0930
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/26/2010 1643
1000
8260B Analysis Batch: 680-166737
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0504.d
3.2 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
370000 U 37000081000Acetone
1500000 U 1500000300000Acetonitrile
730000 U 730000180000Acrolein
730000 U 730000250000Acrylonitrile
12000 J 370005400Benzene
37000 U 3700011000Bromoform
37000 U 3700011000Bromomethane
180000 U 180000180002-Butanone (MEK)
37000 U 370008100Carbon disulfide
37000 U 370006100Carbon tetrachloride
37000 U 370007000Chlorobenzene
37000 U 37000150002-Chloro-1,3-butadiene
37000 U 3700012000Chlorodibromomethane
37000 U 3700020000Chloroethane
37000 U 370008100Chloroform
37000 U 370007300Chloromethane
37000 U 37000160003-Chloro-1-propene
37000 U 370006100cis-1,3-Dichloropropene
73000 U 73000320001,2-Dibromo-3-Chloropropane
37000 U 3700012000Dibromomethane
37000 U 370007100Dichlorobromomethane
37000 U 370006900Dichlorodifluoromethane
37000 U 3700081001,1-Dichloroethane
37000 U 3700081001,2-Dichloroethane
37000 U 37000110001,1-Dichloroethene
37000 U 3700063001,2-Dichloropropane
37000 U 370009500Ethylbenzene
37000 U 3700011000Ethylene Dibromide
37000 U 3700025000Ethyl methacrylate
180000 U 180000240002-Hexanone
37000 U 3700013000Iodomethane
1500000 U 1500000380000Isobutyl alcohol
730000 U 730000170000Methacrylonitrile
37000 U 370007200Methylene Chloride
73000 U 7300033000Methyl methacrylate
180000 U 180000310004-Methyl-2-pentanone (MIBK)
180000 U 18000046000Pentachloroethane
730000 U 730000190000Propionitrile
37000 U 370006800Styrene
37000 U 37000180001,1,1,2-Tetrachloroethane
37000 U 37000120001,1,2,2-Tetrachloroethane
37000 U 3700014000Tetrachloroethene
640000 370006200Toluene
73000 U 7300021000trans-1,4-Dichloro-2-butene
37000 U 370004600trans-1,2-Dichloroethene
37000 U 370006400trans-1,3-Dichloropropene
TestAmerica Savannah Page 52 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-2-US
Client Matrix: % Moisture: 78.7
680-56861-23
Solid
Date Sampled: 04/16/2010 0930
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/19/2010 1610
04/26/2010 1643
1000
8260B Analysis Batch: 680-166737
Prep Batch: 680-166108
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
m0504.d
3.2 g
5 g
5035
MSM
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
37000 U 3700043001,1,1-Trichloroethane
37000 U 3700095001,1,2-Trichloroethane
37000 U 370009500Trichloroethene
37000 U 370008800Trichlorofluoromethane
37000 U 37000180001,2,3-Trichloropropane
73000 U 7300018000Vinyl acetate
37000 U 3700011000Vinyl chloride
73000 U 730008100Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
0 65 - 124D4-Bromofluorobenzene
0 65 - 124DDibromofluoromethane
0 65 - 132DToluene-d8 (Surr)
TestAmerica Savannah Page 53 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
FB-1
Client Matrix:
680-56861-24FB
Water
Date Sampled: 04/15/2010 1735
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 1451
04/20/2010 1451
1.0
8260B Analysis Batch: 680-166185
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
p0101.d
5 mL
5 mL
5030B
MSP
Analyte Result (ug/L) Qualifier MDL RL
8.4 J 255.0Acetone
40 U 4010Acetonitrile
20 U 207.4Acrolein
20 U 207.2Acrylonitrile
1.0 U 1.00.25Benzene
1.0 U 1.00.50Bromoform
1.0 U 1.00.80Bromomethane
1.5 J 101.02-Butanone (MEK)
2.0 U * 2.00.60Carbon disulfide
1.0 U 1.00.50Carbon tetrachloride
1.0 U 1.00.25Chlorobenzene
1.0 U 1.00.302-Chloro-1,3-butadiene
1.0 U 1.00.10Chlorodibromomethane
1.0 U 1.01.0Chloroethane
1.0 U 1.00.14Chloroform
1.0 U 1.00.33Chloromethane
1.0 U 1.00.203-Chloro-1-propene
1.0 U 1.00.11cis-1,3-Dichloropropene
1.0 U 1.00.441,2-Dibromo-3-Chloropropane
1.0 U 1.00.20Dibromomethane
1.0 U 1.00.25Dichlorobromomethane
1.0 U 1.00.25Dichlorodifluoromethane
1.0 U 1.00.251,1-Dichloroethane
1.0 U 1.00.101,2-Dichloroethane
1.0 U 1.00.111,1-Dichloroethene
1.0 U 1.00.131,2-Dichloropropane
0.18 J 1.00.11Ethylbenzene
1.0 U 1.00.25Ethylene Dibromide
1.0 U 1.00.25Ethyl methacrylate
10 U 101.02-Hexanone
5.0 U 5.01.0Iodomethane
40 U 4011Isobutyl alcohol
20 U 203.3Methacrylonitrile
5.0 U 5.01.0Methylene Chloride
1.0 U 1.00.48Methyl methacrylate
10 U 101.04-Methyl-2-pentanone (MIBK)
5.0 U 5.01.2Pentachloroethane
20 U 204.6Propionitrile
1.0 U 1.00.11Styrene
1.0 U 1.00.331,1,1,2-Tetrachloroethane
1.0 U 1.00.181,1,2,2-Tetrachloroethane
1.0 U 1.00.15Tetrachloroethene
2.7 1.00.33Toluene
2.0 U 2.00.50trans-1,4-Dichloro-2-butene
1.0 U 1.00.20trans-1,2-Dichloroethene
1.0 U 1.00.21trans-1,3-Dichloropropene
TestAmerica Savannah Page 54 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
FB-1
Client Matrix:
680-56861-24FB
Water
Date Sampled: 04/15/2010 1735
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 1451
04/20/2010 1451
1.0
8260B Analysis Batch: 680-166185
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
p0101.d
5 mL
5 mL
5030B
MSP
Analyte Result (ug/L) Qualifier MDL RL
1.0 U 1.00.501,1,1-Trichloroethane
1.0 U 1.00.131,1,2-Trichloroethane
1.0 U 1.00.13Trichloroethene
1.0 U 1.00.25Trichlorofluoromethane
1.0 U 1.00.411,2,3-Trichloropropane
2.0 U 2.00.28Vinyl acetate
1.0 U 1.00.18Vinyl chloride
0.39 J 2.00.20Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
100 75 - 1204-Bromofluorobenzene
91 75 - 121Dibromofluoromethane
103 75 - 120Toluene-d8 (Surr)
TestAmerica Savannah Page 55 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
FB-2
Client Matrix:
680-56861-25FB
Water
Date Sampled: 04/16/2010 0945
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 1521
04/20/2010 1521
1.0
8260B Analysis Batch: 680-166185
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
p0103.d
5 mL
5 mL
5030B
MSP
Analyte Result (ug/L) Qualifier MDL RL
7.7 J 255.0Acetone
40 U 4010Acetonitrile
20 U 207.4Acrolein
20 U 207.2Acrylonitrile
1.0 U 1.00.25Benzene
1.0 U 1.00.50Bromoform
1.0 U 1.00.80Bromomethane
1.7 J 101.02-Butanone (MEK)
2.0 U * 2.00.60Carbon disulfide
1.0 U 1.00.50Carbon tetrachloride
1.0 U 1.00.25Chlorobenzene
1.0 U 1.00.302-Chloro-1,3-butadiene
1.0 U 1.00.10Chlorodibromomethane
1.0 U 1.01.0Chloroethane
1.0 U 1.00.14Chloroform
1.0 U 1.00.33Chloromethane
1.0 U 1.00.203-Chloro-1-propene
1.0 U 1.00.11cis-1,3-Dichloropropene
1.0 U 1.00.441,2-Dibromo-3-Chloropropane
1.0 U 1.00.20Dibromomethane
1.0 U 1.00.25Dichlorobromomethane
1.0 U 1.00.25Dichlorodifluoromethane
1.0 U 1.00.251,1-Dichloroethane
1.0 U 1.00.101,2-Dichloroethane
1.0 U 1.00.111,1-Dichloroethene
1.0 U 1.00.131,2-Dichloropropane
0.14 J 1.00.11Ethylbenzene
1.0 U 1.00.25Ethylene Dibromide
1.0 U 1.00.25Ethyl methacrylate
10 U 101.02-Hexanone
5.0 U 5.01.0Iodomethane
40 U 4011Isobutyl alcohol
20 U 203.3Methacrylonitrile
5.0 U 5.01.0Methylene Chloride
1.0 U 1.00.48Methyl methacrylate
10 U 101.04-Methyl-2-pentanone (MIBK)
5.0 U 5.01.2Pentachloroethane
20 U 204.6Propionitrile
1.0 U 1.00.11Styrene
1.0 U 1.00.331,1,1,2-Tetrachloroethane
1.0 U 1.00.181,1,2,2-Tetrachloroethane
1.0 U 1.00.15Tetrachloroethene
2.5 1.00.33Toluene
2.0 U 2.00.50trans-1,4-Dichloro-2-butene
1.0 U 1.00.20trans-1,2-Dichloroethene
1.0 U 1.00.21trans-1,3-Dichloropropene
TestAmerica Savannah Page 56 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
FB-2
Client Matrix:
680-56861-25FB
Water
Date Sampled: 04/16/2010 0945
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 1521
04/20/2010 1521
1.0
8260B Analysis Batch: 680-166185
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
p0103.d
5 mL
5 mL
5030B
MSP
Analyte Result (ug/L) Qualifier MDL RL
1.0 U 1.00.501,1,1-Trichloroethane
1.0 U 1.00.131,1,2-Trichloroethane
1.0 U 1.00.13Trichloroethene
1.0 U 1.00.25Trichlorofluoromethane
1.0 U 1.00.411,2,3-Trichloropropane
2.0 U 2.00.28Vinyl acetate
1.0 U 1.00.18Vinyl chloride
0.40 J 2.00.20Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
99 75 - 1204-Bromofluorobenzene
93 75 - 121Dibromofluoromethane
100 75 - 120Toluene-d8 (Surr)
TestAmerica Savannah Page 57 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
TB-1
Client Matrix:
680-56861-26TB
Water
Date Sampled: 04/14/2010 0000
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 1551
04/20/2010 1551
1.0
8260B Analysis Batch: 680-166185
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
p0105.d
5 mL
5 mL
5030B
MSP
Analyte Result (ug/L) Qualifier MDL RL
5.0 J 255.0Acetone
40 U 4010Acetonitrile
20 U 207.4Acrolein
20 U 207.2Acrylonitrile
1.0 U 1.00.25Benzene
1.0 U 1.00.50Bromoform
1.0 U 1.00.80Bromomethane
10 U 101.02-Butanone (MEK)
2.0 U * 2.00.60Carbon disulfide
1.0 U 1.00.50Carbon tetrachloride
1.0 U 1.00.25Chlorobenzene
1.0 U 1.00.302-Chloro-1,3-butadiene
1.0 U 1.00.10Chlorodibromomethane
1.0 U 1.01.0Chloroethane
1.0 U 1.00.14Chloroform
1.0 U 1.00.33Chloromethane
1.0 U 1.00.203-Chloro-1-propene
1.0 U 1.00.11cis-1,3-Dichloropropene
1.0 U 1.00.441,2-Dibromo-3-Chloropropane
1.0 U 1.00.20Dibromomethane
1.0 U 1.00.25Dichlorobromomethane
1.0 U 1.00.25Dichlorodifluoromethane
1.0 U 1.00.251,1-Dichloroethane
1.0 U 1.00.101,2-Dichloroethane
1.0 U 1.00.111,1-Dichloroethene
1.0 U 1.00.131,2-Dichloropropane
1.0 U 1.00.11Ethylbenzene
1.0 U 1.00.25Ethylene Dibromide
1.0 U 1.00.25Ethyl methacrylate
10 U 101.02-Hexanone
5.0 U 5.01.0Iodomethane
40 U 4011Isobutyl alcohol
20 U 203.3Methacrylonitrile
5.0 U 5.01.0Methylene Chloride
1.0 U 1.00.48Methyl methacrylate
10 U 101.04-Methyl-2-pentanone (MIBK)
5.0 U 5.01.2Pentachloroethane
20 U 204.6Propionitrile
1.0 U 1.00.11Styrene
1.0 U 1.00.331,1,1,2-Tetrachloroethane
1.0 U 1.00.181,1,2,2-Tetrachloroethane
1.0 U 1.00.15Tetrachloroethene
1.0 U 1.00.33Toluene
2.0 U 2.00.50trans-1,4-Dichloro-2-butene
1.0 U 1.00.20trans-1,2-Dichloroethene
1.0 U 1.00.21trans-1,3-Dichloropropene
TestAmerica Savannah Page 58 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
TB-1
Client Matrix:
680-56861-26TB
Water
Date Sampled: 04/14/2010 0000
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 1551
04/20/2010 1551
1.0
8260B Analysis Batch: 680-166185
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
p0105.d
5 mL
5 mL
5030B
MSP
Analyte Result (ug/L) Qualifier MDL RL
1.0 U 1.00.501,1,1-Trichloroethane
1.0 U 1.00.131,1,2-Trichloroethane
1.0 U 1.00.13Trichloroethene
1.0 U 1.00.25Trichlorofluoromethane
1.0 U 1.00.411,2,3-Trichloropropane
2.0 U 2.00.28Vinyl acetate
1.0 U 1.00.18Vinyl chloride
2.0 U 2.00.20Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
99 75 - 1204-Bromofluorobenzene
90 75 - 121Dibromofluoromethane
102 75 - 120Toluene-d8 (Surr)
TestAmerica Savannah Page 59 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
TB-2
Client Matrix:
680-56861-27TB
Water
Date Sampled: 04/15/2010 0000
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 1621
04/20/2010 1621
1.0
8260B Analysis Batch: 680-166185
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
p0107.d
5 mL
5 mL
5030B
MSP
Analyte Result (ug/L) Qualifier MDL RL
25 U 255.0Acetone
40 U 4010Acetonitrile
20 U 207.4Acrolein
20 U 207.2Acrylonitrile
1.0 U 1.00.25Benzene
1.0 U 1.00.50Bromoform
1.0 U 1.00.80Bromomethane
10 U 101.02-Butanone (MEK)
2.0 U * 2.00.60Carbon disulfide
1.0 U 1.00.50Carbon tetrachloride
1.0 U 1.00.25Chlorobenzene
1.0 U 1.00.302-Chloro-1,3-butadiene
1.0 U 1.00.10Chlorodibromomethane
1.0 U 1.01.0Chloroethane
1.0 U 1.00.14Chloroform
1.0 U 1.00.33Chloromethane
1.0 U 1.00.203-Chloro-1-propene
1.0 U 1.00.11cis-1,3-Dichloropropene
1.0 U 1.00.441,2-Dibromo-3-Chloropropane
1.0 U 1.00.20Dibromomethane
1.0 U 1.00.25Dichlorobromomethane
1.0 U 1.00.25Dichlorodifluoromethane
1.0 U 1.00.251,1-Dichloroethane
1.0 U 1.00.101,2-Dichloroethane
1.0 U 1.00.111,1-Dichloroethene
1.0 U 1.00.131,2-Dichloropropane
1.0 U 1.00.11Ethylbenzene
1.0 U 1.00.25Ethylene Dibromide
1.0 U 1.00.25Ethyl methacrylate
10 U 101.02-Hexanone
5.0 U 5.01.0Iodomethane
40 U 4011Isobutyl alcohol
20 U 203.3Methacrylonitrile
5.0 U 5.01.0Methylene Chloride
1.0 U 1.00.48Methyl methacrylate
10 U 101.04-Methyl-2-pentanone (MIBK)
5.0 U 5.01.2Pentachloroethane
20 U 204.6Propionitrile
1.0 U 1.00.11Styrene
1.0 U 1.00.331,1,1,2-Tetrachloroethane
1.0 U 1.00.181,1,2,2-Tetrachloroethane
1.0 U 1.00.15Tetrachloroethene
1.0 U 1.00.33Toluene
2.0 U 2.00.50trans-1,4-Dichloro-2-butene
1.0 U 1.00.20trans-1,2-Dichloroethene
1.0 U 1.00.21trans-1,3-Dichloropropene
TestAmerica Savannah Page 60 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
TB-2
Client Matrix:
680-56861-27TB
Water
Date Sampled: 04/15/2010 0000
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 1621
04/20/2010 1621
1.0
8260B Analysis Batch: 680-166185
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
p0107.d
5 mL
5 mL
5030B
MSP
Analyte Result (ug/L) Qualifier MDL RL
1.0 U 1.00.501,1,1-Trichloroethane
1.0 U 1.00.131,1,2-Trichloroethane
1.0 U 1.00.13Trichloroethene
1.0 U 1.00.25Trichlorofluoromethane
1.0 U 1.00.411,2,3-Trichloropropane
2.0 U 2.00.28Vinyl acetate
1.0 U 1.00.18Vinyl chloride
2.0 U 2.00.20Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
98 75 - 1204-Bromofluorobenzene
93 75 - 121Dibromofluoromethane
102 75 - 120Toluene-d8 (Surr)
TestAmerica Savannah Page 61 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
RB-1
Client Matrix:
680-56861-28RB
Water
Date Sampled: 04/16/2010 1000
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 1652
04/20/2010 1652
1.0
8260B Analysis Batch: 680-166185
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
p0109.d
5 mL
5 mL
5030B
MSP
Analyte Result (ug/L) Qualifier MDL RL
9.5 J 255.0Acetone
40 U 4010Acetonitrile
20 U 207.4Acrolein
20 U 207.2Acrylonitrile
1.0 U 1.00.25Benzene
1.0 U 1.00.50Bromoform
1.0 U 1.00.80Bromomethane
1.2 J 101.02-Butanone (MEK)
2.0 U * 2.00.60Carbon disulfide
1.0 U 1.00.50Carbon tetrachloride
1.0 U 1.00.25Chlorobenzene
1.0 U 1.00.302-Chloro-1,3-butadiene
1.0 U 1.00.10Chlorodibromomethane
1.0 U 1.01.0Chloroethane
1.0 U 1.00.14Chloroform
1.0 U 1.00.33Chloromethane
1.0 U 1.00.203-Chloro-1-propene
1.0 U 1.00.11cis-1,3-Dichloropropene
1.0 U 1.00.441,2-Dibromo-3-Chloropropane
1.0 U 1.00.20Dibromomethane
1.0 U 1.00.25Dichlorobromomethane
1.0 U 1.00.25Dichlorodifluoromethane
1.0 U 1.00.251,1-Dichloroethane
1.0 U 1.00.101,2-Dichloroethane
1.0 U 1.00.111,1-Dichloroethene
1.0 U 1.00.131,2-Dichloropropane
1.0 U 1.00.11Ethylbenzene
1.0 U 1.00.25Ethylene Dibromide
1.0 U 1.00.25Ethyl methacrylate
10 U 101.02-Hexanone
5.0 U 5.01.0Iodomethane
40 U 4011Isobutyl alcohol
20 U 203.3Methacrylonitrile
5.0 U 5.01.0Methylene Chloride
1.0 U 1.00.48Methyl methacrylate
10 U 101.04-Methyl-2-pentanone (MIBK)
5.0 U 5.01.2Pentachloroethane
20 U 204.6Propionitrile
1.0 U 1.00.11Styrene
1.0 U 1.00.331,1,1,2-Tetrachloroethane
1.0 U 1.00.181,1,2,2-Tetrachloroethane
1.0 U 1.00.15Tetrachloroethene
1.3 1.00.33Toluene
2.0 U 2.00.50trans-1,4-Dichloro-2-butene
1.0 U 1.00.20trans-1,2-Dichloroethene
1.0 U 1.00.21trans-1,3-Dichloropropene
TestAmerica Savannah Page 62 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
RB-1
Client Matrix:
680-56861-28RB
Water
Date Sampled: 04/16/2010 1000
Date Received: 04/17/2010 1045
8260B Volatile Organic Compounds (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 1652
04/20/2010 1652
1.0
8260B Analysis Batch: 680-166185
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
p0109.d
5 mL
5 mL
5030B
MSP
Analyte Result (ug/L) Qualifier MDL RL
1.0 U 1.00.501,1,1-Trichloroethane
1.0 U 1.00.131,1,2-Trichloroethane
1.0 U 1.00.13Trichloroethene
1.0 U 1.00.25Trichlorofluoromethane
1.0 U 1.00.411,2,3-Trichloropropane
2.0 U 2.00.28Vinyl acetate
1.0 U 1.00.18Vinyl chloride
2.0 U 2.00.20Xylenes, Total
Surrogate %Rec Acceptance LimitsQualifier
94 75 - 1204-Bromofluorobenzene
92 75 - 121Dibromofluoromethane
103 75 - 120Toluene-d8 (Surr)
TestAmerica Savannah Page 63 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-1-LS
Client Matrix: % Moisture: 53.4
680-56861-1
Solid
Date Sampled: 04/14/2010 0950
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/03/2010 1733
10
8270C Analysis Batch: 680-167447
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1006.d
30.04 g
10 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
71000 U 710008800Acenaphthene
71000 U 710007700Acenaphthylene
71000 U 710006000Acetophenone
71000 U 7100060002-Acetylaminofluorene
14000000 U 14000000580000alpha,alpha-Dimethyl phenethylamine
71000 U 7100079004-Aminobiphenyl
140000 U 1400007300Aniline
71000 U 710005400Anthracene
71000 U 7100012000Aramite, Total
71000 U 710005800Benzo[a]anthracene
71000 U 7100011000Benzo[a]pyrene
71000 U 710008100Benzo[b]fluoranthene
32000 J 710004700Benzo[g,h,i]perylene
71000 U 7100014000Benzo[k]fluoranthene
71000 U 710007100Benzyl alcohol
1100000 7100060001,1'-Biphenyl
71000 U 710008400Bis(2-chloroethoxy)methane
71000 U 710009600Bis(2-chloroethyl)ether
71000 U 710006400bis(chloroisopropyl) ether
71000 U 710007100Bis(2-ethylhexyl) phthalate
71000 U 7100077004-Bromophenyl phenyl ether
71000 U 710005600Butyl benzyl phthalate
140000 U 140000110004-Chloroaniline
71000 U 7100075004-Chloro-3-methylphenol
71000 U 7100084002-Chloronaphthalene
71000 U 7100086002-Chlorophenol
71000 U 7100079004-Chlorophenyl phenyl ether
71000 U 710004500Chrysene
71000 U 7100036000Diallate
34000 J 710005100Dibenz(a,h)anthracene
71000 U 710007100Dibenzofuran
71000 U 7100079001,2-Dichlorobenzene
71000 U 7100073001,3-Dichlorobenzene
71000 U 7100075001,4-Dichlorobenzene
140000 U 14000060003,3'-Dichlorobenzidine
71000 U 7100075002,4-Dichlorophenol
71000 U 7100058002,6-Dichlorophenol
71000 U 710007500Diethyl phthalate
27000 J 710005400Dimethoate
71000 U 7100036007,12-Dimethylbenz(a)anthracene
360000 U 3600001800003,3'-Dimethylbenzidine
71000 U 7100094002,4-Dimethylphenol
71000 U 710007300Dimethyl phthalate
71000 U 710006400Di-n-butyl phthalate
71000 U 7100051001,3-Dinitrobenzene
360000 U 360000360004,6-Dinitro-2-methylphenol
TestAmerica Savannah Page 64 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-1-LS
Client Matrix: % Moisture: 53.4
680-56861-1
Solid
Date Sampled: 04/14/2010 0950
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/03/2010 1733
10
8270C Analysis Batch: 680-167447
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1006.d
30.04 g
10 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
360000 U 3600001800002,4-Dinitrophenol
71000 U 71000100002,4-Dinitrotoluene
71000 U 7100090002,6-Dinitrotoluene
71000 U 710006200Di-n-octyl phthalate
71000 U 7100034000Dinoseb
71000 U 71000260001,4-Dioxane
71000 U 710003600Disulfoton
71000 U 710006600Ethyl methanesulfonate
71000 U 710004700Ethyl Parathion
71000 U * 710006200Famphur
71000 U 710006900Fluoranthene
71000 U 710007700Fluorene
71000 U 710008400Hexachlorobenzene
71000 U 710007700Hexachlorobutadiene
71000 U 710008800Hexachlorocyclopentadiene
71000 U 710006000Hexachloroethane
36000000 U 360000002800000Hexachlorophene
71000 U * 710006200Hexachloropropene
32000 J 710006000Indeno[1,2,3-cd]pyrene
71000 U 710007100Isophorone
71000 U 710005100Isosafrole
14000000 U 14000000180000Methapyrilene
71000 U 7100088003-Methylcholanthrene
71000 U * 710003600Methyl methanesulfonate
21000 J 7100081002-Methylnaphthalene
71000 U 710005600Methyl parathion
71000 U 7100058002-Methylphenol
12000 J 7100092003 & 4 Methylphenol
8000 J 710006400Naphthalene
71000 U * 7100036001,4-Naphthoquinone
71000 U * 71000140001-Naphthylamine
71000 U 7100073002-Naphthylamine
360000 U 36000096002-Nitroaniline
360000 U 36000099003-Nitroaniline
360000 U 360000100004-Nitroaniline
71000 U 710005600Nitrobenzene
71000 U 7100088002-Nitrophenol
360000 U 360000710004-Nitrophenol
710000 U 7100001800004-Nitroquinoline-1-oxide
71000 U 710005600N-Nitro-o-toluidine
71000 U 710006000N-Nitrosodiethylamine
71000 U 7100026000N-Nitrosodimethylamine
71000 U 710005100N-Nitrosodi-n-butylamine
71000 U 710006900N-Nitrosodi-n-propylamine
71000 U 710007100N-Nitrosodiphenylamine
71000 U 710005400N-Nitrosomethylethylamine
TestAmerica Savannah Page 65 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-1-LS
Client Matrix: % Moisture: 53.4
680-56861-1
Solid
Date Sampled: 04/14/2010 0950
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/03/2010 1733
10
8270C Analysis Batch: 680-167447
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1006.d
30.04 g
10 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
71000 U 710005800N-Nitrosomorpholine
71000 U 710004500N-Nitrosopiperidine
71000 U 710003900N-Nitrosopyrrolidine
20000 J * 710008600o,o',o''-Triethylphosphorothioate
71000 U 710004100p-Dimethylamino azobenzene
71000 U 710005400Pentachlorobenzene
71000 U 710004500Pentachloronitrobenzene
360000 U 36000071000Pentachlorophenol
71000 U 710007100Phenacetin
6800 J 710005800Phenanthrene
71000 U 710007300Phenol
71000 U * 710004700Phorate
71000 U 7100036002-Picoline
360000 U * 360000180000p-Phenylene diamine
71000 U 710005100Pronamide
71000 U 710005800Pyrene
71000 U 710006200Pyridine
71000 U 710005100Safrole, Total
71000 U 710004300Sulfotepp
71000 U 7100066001,2,4,5-Tetrachlorobenzene
71000 U 7100047002,3,4,6-Tetrachlorophenol
71000 U 710004900Thionazin
71000 U 7100075002-Toluidine
71000 U 7100066001,2,4-Trichlorobenzene
71000 U 7100075002,4,5-Trichlorophenol
71000 U 7100062002,4,6-Trichlorophenol
71000 U 71000360001,3,5-Trinitrobenzene
Surrogate %Rec Acceptance LimitsQualifier
0 34 - 130D2,4,6-Tribromophenol
0 34 - 130D2-Fluorobiphenyl
0 30 - 130D2-Fluorophenol
0 39 - 130DTerphenyl-d14
0 30 - 130DPhenol-d5
0 27 - 130DNitrobenzene-d5
TestAmerica Savannah Page 66 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-1-LS
Client Matrix: % Moisture: 53.4
680-56861-1
Solid
Date Sampled: 04/14/2010 0950
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/10/2010 1028
100
8270C Analysis Batch: 680-167967
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1155.d
30.04 g
10 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
2500000 71000073000Diphenyl ether
Surrogate %Rec Acceptance LimitsQualifier
0 34 - 130D2,4,6-Tribromophenol
0 34 - 130D2-Fluorobiphenyl
0 30 - 130D2-Fluorophenol
0 39 - 130DTerphenyl-d14
0 30 - 130DPhenol-d5
0 27 - 130DNitrobenzene-d5
TestAmerica Savannah Page 67 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-3-NS
Client Matrix: % Moisture: 21.3
680-56861-2
Solid
Date Sampled: 04/14/2010 1245
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/03/2010 1758
10
8270C Analysis Batch: 680-167447
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1007.d
30.05 g
1.0 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
770 J 4200520Acenaphthene
4200 U 4200460Acenaphthylene
4200 U 4200360Acetophenone
4200 U 42003602-Acetylaminofluorene
850000 U 85000034000alpha,alpha-Dimethyl phenethylamine
4200 U 42004704-Aminobiphenyl
8400 U 8400430Aniline
4200 U 4200320Anthracene
4200 U 4200720Aramite, Total
4200 U 4200340Benzo[a]anthracene
4200 U 4200660Benzo[a]pyrene
4200 U 4200480Benzo[b]fluoranthene
910 J 4200280Benzo[g,h,i]perylene
4200 U 4200820Benzo[k]fluoranthene
4200 U 4200420Benzyl alcohol
51000 42003601,1'-Biphenyl
4200 U 4200490Bis(2-chloroethoxy)methane
4200 U 4200570Bis(2-chloroethyl)ether
4200 U 4200380bis(chloroisopropyl) ether
4200 U 4200420Bis(2-ethylhexyl) phthalate
4200 U 42004604-Bromophenyl phenyl ether
4200 U 4200330Butyl benzyl phthalate
8400 U 84006604-Chloroaniline
4200 U 42004404-Chloro-3-methylphenol
4200 U 42004902-Chloronaphthalene
4200 U 42005102-Chlorophenol
4200 U 42004704-Chlorophenyl phenyl ether
4200 U 4200270Chrysene
4200 U 42002200Diallate
800 J 4200300Dibenz(a,h)anthracene
510 J 4200420Dibenzofuran
4200 U 42004701,2-Dichlorobenzene
4200 U 42004301,3-Dichlorobenzene
4200 U 42004401,4-Dichlorobenzene
8400 U 84003603,3'-Dichlorobenzidine
4200 U 42004402,4-Dichlorophenol
4200 U 42003402,6-Dichlorophenol
470 J 4200440Diethyl phthalate
4200 U 4200320Dimethoate
4200 U 42002207,12-Dimethylbenz(a)anthracene
22000 U 22000110003,3'-Dimethylbenzidine
4200 U 42005602,4-Dimethylphenol
4200 U 4200430Dimethyl phthalate
4200 U 4200380Di-n-butyl phthalate
4200 U 42003001,3-Dinitrobenzene
22000 U 2200022004,6-Dinitro-2-methylphenol
TestAmerica Savannah Page 68 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-3-NS
Client Matrix: % Moisture: 21.3
680-56861-2
Solid
Date Sampled: 04/14/2010 1245
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/03/2010 1758
10
8270C Analysis Batch: 680-167447
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1007.d
30.05 g
1.0 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
22000 U 22000110002,4-Dinitrophenol
4200 U 42006202,4-Dinitrotoluene
4200 U 42005302,6-Dinitrotoluene
4200 U 4200370Di-n-octyl phthalate
4200 U 42002000Dinoseb
4200 U 420015001,4-Dioxane
4200 U 4200220Disulfoton
4200 U 4200390Ethyl methanesulfonate
4200 U 4200280Ethyl Parathion
4200 U * 4200370Famphur
4200 U 4200410Fluoranthene
500 J 4200460Fluorene
4200 U 4200490Hexachlorobenzene
4200 U 4200460Hexachlorobutadiene
4200 U 4200520Hexachlorocyclopentadiene
4200 U 4200360Hexachloroethane
2200000 U 2200000160000Hexachlorophene
4200 U * 4200370Hexachloropropene
720 J 4200360Indeno[1,2,3-cd]pyrene
4200 U 4200420Isophorone
4200 U 4200300Isosafrole
850000 U 85000011000Methapyrilene
4200 U 42005203-Methylcholanthrene
4200 U * 4200220Methyl methanesulfonate
680 J 42004802-Methylnaphthalene
4200 U 4200330Methyl parathion
4200 U 42003402-Methylphenol
1600 J 42005503 & 4 Methylphenol
2000 J 4200380Naphthalene
4200 U * 42002201,4-Naphthoquinone
4200 U * 42008401-Naphthylamine
4200 U 42004302-Naphthylamine
22000 U 220005702-Nitroaniline
22000 U 220005803-Nitroaniline
22000 U 220006204-Nitroaniline
4200 U 4200330Nitrobenzene
4200 U 42005202-Nitrophenol
22000 U 2200042004-Nitrophenol
42000 U 42000110004-Nitroquinoline-1-oxide
4200 U 4200330N-Nitro-o-toluidine
4200 U 4200360N-Nitrosodiethylamine
4200 U 42001500N-Nitrosodimethylamine
4200 U 4200300N-Nitrosodi-n-butylamine
4200 U 4200410N-Nitrosodi-n-propylamine
4200 U 4200420N-Nitrosodiphenylamine
4200 U 4200320N-Nitrosomethylethylamine
TestAmerica Savannah Page 69 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-3-NS
Client Matrix: % Moisture: 21.3
680-56861-2
Solid
Date Sampled: 04/14/2010 1245
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/03/2010 1758
10
8270C Analysis Batch: 680-167447
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1007.d
30.05 g
1.0 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
4200 U 4200340N-Nitrosomorpholine
4200 U 4200270N-Nitrosopiperidine
4200 U 4200230N-Nitrosopyrrolidine
1200 J * 4200510o,o',o''-Triethylphosphorothioate
4200 U 4200240p-Dimethylamino azobenzene
4200 U 4200320Pentachlorobenzene
4200 U 4200270Pentachloronitrobenzene
22000 U 220004200Pentachlorophenol
4200 U 4200420Phenacetin
1100 J 4200340Phenanthrene
4200 U 4200430Phenol
4200 U * 4200280Phorate
4200 U 42002202-Picoline
22000 U * 2200011000p-Phenylene diamine
4200 U 4200300Pronamide
4200 U 4200340Pyrene
4200 U 4200370Pyridine
4200 U 4200300Safrole, Total
4200 U 4200250Sulfotepp
4200 U 42003901,2,4,5-Tetrachlorobenzene
4200 U 42002802,3,4,6-Tetrachlorophenol
4200 U 4200290Thionazin
4200 U 42004402-Toluidine
4200 U 42003901,2,4-Trichlorobenzene
4200 U 42004402,4,5-Trichlorophenol
4200 U 42003702,4,6-Trichlorophenol
4200 U 420022001,3,5-Trinitrobenzene
Surrogate %Rec Acceptance LimitsQualifier
0 34 - 130D2,4,6-Tribromophenol
0 34 - 130D2-Fluorobiphenyl
0 30 - 130D2-Fluorophenol
0 39 - 130DTerphenyl-d14
0 30 - 130DPhenol-d5
0 27 - 130DNitrobenzene-d5
TestAmerica Savannah Page 70 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-3-NS
Client Matrix: % Moisture: 21.3
680-56861-2
Solid
Date Sampled: 04/14/2010 1245
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/10/2010 1052
100
8270C Analysis Batch: 680-167967
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1156.d
30.05 g
1.0 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
140000 420004300Diphenyl ether
Surrogate %Rec Acceptance LimitsQualifier
0 34 - 130D2,4,6-Tribromophenol
0 34 - 130D2-Fluorobiphenyl
0 30 - 130D2-Fluorophenol
0 39 - 130DTerphenyl-d14
0 30 - 130DPhenol-d5
0 27 - 130DNitrobenzene-d5
TestAmerica Savannah Page 71 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-3-LS
Client Matrix: % Moisture: 53.4
680-56861-3
Solid
Date Sampled: 04/14/2010 1255
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/03/2010 1822
10
8270C Analysis Batch: 680-167447
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1008.d
30.06 g
10 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
10000 J 710008800Acenaphthene
71000 U 710007700Acenaphthylene
71000 U 710006000Acetophenone
71000 U 7100060002-Acetylaminofluorene
14000000 U 14000000580000alpha,alpha-Dimethyl phenethylamine
71000 U 7100079004-Aminobiphenyl
140000 U 1400007300Aniline
71000 U 710005400Anthracene
71000 U 7100012000Aramite, Total
71000 U 710005800Benzo[a]anthracene
71000 U 7100011000Benzo[a]pyrene
71000 U 710008100Benzo[b]fluoranthene
71000 U 710004700Benzo[g,h,i]perylene
71000 U 7100014000Benzo[k]fluoranthene
71000 U 710007100Benzyl alcohol
1000000 7100060001,1'-Biphenyl
71000 U 710008400Bis(2-chloroethoxy)methane
71000 U 710009600Bis(2-chloroethyl)ether
71000 U 710006400bis(chloroisopropyl) ether
71000 U 710007100Bis(2-ethylhexyl) phthalate
71000 U 7100077004-Bromophenyl phenyl ether
71000 U 710005600Butyl benzyl phthalate
140000 U 140000110004-Chloroaniline
71000 U 7100075004-Chloro-3-methylphenol
71000 U 7100084002-Chloronaphthalene
71000 U 7100086002-Chlorophenol
71000 U 7100079004-Chlorophenyl phenyl ether
71000 U 710004500Chrysene
71000 U 7100036000Diallate
71000 U 710005100Dibenz(a,h)anthracene
7900 J 710007100Dibenzofuran
71000 U 7100079001,2-Dichlorobenzene
71000 U 7100073001,3-Dichlorobenzene
71000 U 7100075001,4-Dichlorobenzene
140000 U 14000060003,3'-Dichlorobenzidine
71000 U 7100075002,4-Dichlorophenol
71000 U 7100058002,6-Dichlorophenol
71000 U 710007500Diethyl phthalate
71000 U 710005400Dimethoate
71000 U 7100036007,12-Dimethylbenz(a)anthracene
360000 U 3600001800003,3'-Dimethylbenzidine
71000 U 7100094002,4-Dimethylphenol
71000 U 710007300Dimethyl phthalate
71000 U 710006400Di-n-butyl phthalate
71000 U 7100051001,3-Dinitrobenzene
360000 U 360000360004,6-Dinitro-2-methylphenol
TestAmerica Savannah Page 72 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-3-LS
Client Matrix: % Moisture: 53.4
680-56861-3
Solid
Date Sampled: 04/14/2010 1255
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/03/2010 1822
10
8270C Analysis Batch: 680-167447
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1008.d
30.06 g
10 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
360000 U 3600001800002,4-Dinitrophenol
71000 U 71000100002,4-Dinitrotoluene
71000 U 7100090002,6-Dinitrotoluene
71000 U 710006200Di-n-octyl phthalate
71000 U 7100034000Dinoseb
71000 U 71000260001,4-Dioxane
71000 U 710003600Disulfoton
71000 U 710006600Ethyl methanesulfonate
71000 U 710004700Ethyl Parathion
71000 U * 710006200Famphur
71000 U 710006900Fluoranthene
71000 U 710007700Fluorene
71000 U 710008400Hexachlorobenzene
71000 U 710007700Hexachlorobutadiene
71000 U 710008800Hexachlorocyclopentadiene
71000 U 710006000Hexachloroethane
36000000 U 360000002800000Hexachlorophene
71000 U * 710006200Hexachloropropene
71000 U 710006000Indeno[1,2,3-cd]pyrene
71000 U 710007100Isophorone
71000 U 710005100Isosafrole
14000000 U 14000000180000Methapyrilene
71000 U 7100088003-Methylcholanthrene
71000 U * 710003600Methyl methanesulfonate
9800 J 7100081002-Methylnaphthalene
71000 U 710005600Methyl parathion
71000 U 7100058002-Methylphenol
71000 U 7100092003 & 4 Methylphenol
35000 J 710006400Naphthalene
71000 U * 7100036001,4-Naphthoquinone
71000 U * 71000140001-Naphthylamine
71000 U 7100073002-Naphthylamine
360000 U 36000096002-Nitroaniline
360000 U 36000099003-Nitroaniline
360000 U 360000100004-Nitroaniline
71000 U 710005600Nitrobenzene
71000 U 7100088002-Nitrophenol
360000 U 360000710004-Nitrophenol
710000 U 7100001800004-Nitroquinoline-1-oxide
71000 U 710005600N-Nitro-o-toluidine
71000 U 710006000N-Nitrosodiethylamine
71000 U 7100026000N-Nitrosodimethylamine
71000 U 710005100N-Nitrosodi-n-butylamine
71000 U 710006900N-Nitrosodi-n-propylamine
71000 U 710007100N-Nitrosodiphenylamine
71000 U 710005400N-Nitrosomethylethylamine
TestAmerica Savannah Page 73 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-3-LS
Client Matrix: % Moisture: 53.4
680-56861-3
Solid
Date Sampled: 04/14/2010 1255
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/03/2010 1822
10
8270C Analysis Batch: 680-167447
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1008.d
30.06 g
10 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
71000 U 710005800N-Nitrosomorpholine
71000 U 710004500N-Nitrosopiperidine
71000 U 710003900N-Nitrosopyrrolidine
71000 U * 710008600o,o',o''-Triethylphosphorothioate
71000 U 710004100p-Dimethylamino azobenzene
71000 U 710005400Pentachlorobenzene
71000 U 710004500Pentachloronitrobenzene
360000 U 36000071000Pentachlorophenol
71000 U 710007100Phenacetin
11000 J 710005800Phenanthrene
71000 U 710007300Phenol
71000 U * 710004700Phorate
71000 U 7100036002-Picoline
360000 U * 360000180000p-Phenylene diamine
71000 U 710005100Pronamide
71000 U 710005800Pyrene
71000 U 710006200Pyridine
71000 U 710005100Safrole, Total
71000 U 710004300Sulfotepp
71000 U 7100066001,2,4,5-Tetrachlorobenzene
71000 U 7100047002,3,4,6-Tetrachlorophenol
71000 U 710004900Thionazin
71000 U 7100075002-Toluidine
71000 U 7100066001,2,4-Trichlorobenzene
71000 U 7100075002,4,5-Trichlorophenol
71000 U 7100062002,4,6-Trichlorophenol
71000 U 71000360001,3,5-Trinitrobenzene
Surrogate %Rec Acceptance LimitsQualifier
0 34 - 130D2,4,6-Tribromophenol
0 34 - 130D2-Fluorobiphenyl
0 30 - 130D2-Fluorophenol
0 39 - 130DTerphenyl-d14
0 30 - 130DPhenol-d5
0 27 - 130DNitrobenzene-d5
TestAmerica Savannah Page 74 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-3-LS
Client Matrix: % Moisture: 53.4
680-56861-3
Solid
Date Sampled: 04/14/2010 1255
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/10/2010 1116
100
8270C Analysis Batch: 680-167967
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1157.d
30.06 g
10 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
2400000 71000073000Diphenyl ether
Surrogate %Rec Acceptance LimitsQualifier
0 34 - 130D2,4,6-Tribromophenol
0 34 - 130D2-Fluorobiphenyl
0 30 - 130D2-Fluorophenol
0 39 - 130DTerphenyl-d14
0 30 - 130DPhenol-d5
0 27 - 130DNitrobenzene-d5
TestAmerica Savannah Page 75 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-4-NS
Client Matrix: % Moisture: 12.4
680-56861-4
Solid
Date Sampled: 04/14/2010 1715
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/04/2010 1506
100
8270C Analysis Batch: 680-167473
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1016a.d
30.10 g
1.0 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
38000 U 380004700Acenaphthene
38000 U 380004100Acenaphthylene
38000 U 380003200Acetophenone
38000 U 3800032002-Acetylaminofluorene
7600000 U 7600000310000alpha,alpha-Dimethyl phenethylamine
38000 U 3800042004-Aminobiphenyl
75000 U 750003900Aniline
38000 U 380002800Anthracene
38000 U 380006500Aramite, Total
38000 U 380003100Benzo[a]anthracene
38000 U 380005900Benzo[a]pyrene
38000 U 380004300Benzo[b]fluoranthene
38000 U 380002500Benzo[g,h,i]perylene
38000 U 380007400Benzo[k]fluoranthene
38000 U 380003800Benzyl alcohol
360000 3800032001,1'-Biphenyl
38000 U 380004400Bis(2-chloroethoxy)methane
38000 U 380005100Bis(2-chloroethyl)ether
38000 U 380003400bis(chloroisopropyl) ether
38000 U 380003800Bis(2-ethylhexyl) phthalate
38000 U 3800041004-Bromophenyl phenyl ether
38000 U 380003000Butyl benzyl phthalate
75000 U 7500059004-Chloroaniline
38000 U 3800040004-Chloro-3-methylphenol
38000 U 3800044002-Chloronaphthalene
38000 U 3800046002-Chlorophenol
38000 U 3800042004-Chlorophenyl phenyl ether
38000 U 380002400Chrysene
38000 U 3800019000Diallate
38000 U 380002700Dibenz(a,h)anthracene
38000 U 380003800Dibenzofuran
38000 U 3800042001,2-Dichlorobenzene
38000 U 3800039001,3-Dichlorobenzene
38000 U 3800040001,4-Dichlorobenzene
75000 U 7500032003,3'-Dichlorobenzidine
38000 U 3800040002,4-Dichlorophenol
38000 U 3800031002,6-Dichlorophenol
38000 U 380004000Diethyl phthalate
38000 U 380002800Dimethoate
38000 U 3800019007,12-Dimethylbenz(a)anthracene
190000 U 190000950003,3'-Dimethylbenzidine
38000 U 3800050002,4-Dimethylphenol
38000 U 380003900Dimethyl phthalate
38000 U 380003400Di-n-butyl phthalate
38000 U 3800027001,3-Dinitrobenzene
190000 U 190000190004,6-Dinitro-2-methylphenol
TestAmerica Savannah Page 76 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-4-NS
Client Matrix: % Moisture: 12.4
680-56861-4
Solid
Date Sampled: 04/14/2010 1715
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/04/2010 1506
100
8270C Analysis Batch: 680-167473
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1016a.d
30.10 g
1.0 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
190000 U 190000940002,4-Dinitrophenol
38000 U 3800056002,4-Dinitrotoluene
38000 U 3800048002,6-Dinitrotoluene
38000 U 380003300Di-n-octyl phthalate
38000 U 3800018000Dinoseb
38000 U 38000140001,4-Dioxane
38000 U 380001900Disulfoton
38000 U 380003500Ethyl methanesulfonate
38000 U 380002500Ethyl Parathion
38000 U 380003300Famphur
38000 U 380003600Fluoranthene
38000 U 380004100Fluorene
38000 U 380004400Hexachlorobenzene
38000 U 380004100Hexachlorobutadiene
38000 U 380004700Hexachlorocyclopentadiene
38000 U 380003200Hexachloroethane
19000000 U 190000001500000Hexachlorophene
38000 U 380003300Hexachloropropene
38000 U 380003200Indeno[1,2,3-cd]pyrene
38000 U 380003800Isophorone
38000 U 380002700Isosafrole
7600000 U 760000094000Methapyrilene
38000 U 3800047003-Methylcholanthrene
38000 U 380001900Methyl methanesulfonate
38000 U 3800043002-Methylnaphthalene
38000 U 380003000Methyl parathion
38000 U 3800031002-Methylphenol
38000 U 3800049003 & 4 Methylphenol
38000 U 380003400Naphthalene
38000 U 3800019001,4-Naphthoquinone
38000 U 3800075001-Naphthylamine
38000 U 3800039002-Naphthylamine
190000 U 19000051002-Nitroaniline
190000 U 19000052003-Nitroaniline
190000 U 19000056004-Nitroaniline
38000 U 380003000Nitrobenzene
38000 U 3800047002-Nitrophenol
190000 U 190000380004-Nitrophenol
380000 U 380000940004-Nitroquinoline-1-oxide
38000 U 380003000N-Nitro-o-toluidine
38000 U 380003200N-Nitrosodiethylamine
38000 U 3800014000N-Nitrosodimethylamine
38000 U 380002700N-Nitrosodi-n-butylamine
38000 U 380003600N-Nitrosodi-n-propylamine
38000 U 380003800N-Nitrosodiphenylamine
38000 U 380002800N-Nitrosomethylethylamine
TestAmerica Savannah Page 77 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-4-NS
Client Matrix: % Moisture: 12.4
680-56861-4
Solid
Date Sampled: 04/14/2010 1715
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/04/2010 1506
100
8270C Analysis Batch: 680-167473
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1016a.d
30.10 g
1.0 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
38000 U 380003100N-Nitrosomorpholine
38000 U 380002400N-Nitrosopiperidine
38000 U 380002000N-Nitrosopyrrolidine
38000 U 380004600o,o',o''-Triethylphosphorothioate
38000 U 380002200p-Dimethylamino azobenzene
38000 U 380002800Pentachlorobenzene
38000 U 380002400Pentachloronitrobenzene
190000 U 19000038000Pentachlorophenol
38000 U 380003800Phenacetin
38000 U 380003100Phenanthrene
38000 U 380003900Phenol
38000 U 380002500Phorate
38000 U 3800019002-Picoline
190000 U 19000095000p-Phenylene diamine
38000 U 380002700Pronamide
38000 U 380003100Pyrene
38000 U 380003300Pyridine
38000 U 380002700Safrole, Total
38000 U 380002300Sulfotepp
38000 U 3800035001,2,4,5-Tetrachlorobenzene
38000 U 3800025002,3,4,6-Tetrachlorophenol
38000 U 380002600Thionazin
38000 U 3800040002-Toluidine
38000 U 3800035001,2,4-Trichlorobenzene
38000 U 3800040002,4,5-Trichlorophenol
38000 U 3800033002,4,6-Trichlorophenol
38000 U 38000190001,3,5-Trinitrobenzene
Surrogate %Rec Acceptance LimitsQualifier
0 34 - 130D2,4,6-Tribromophenol
0 34 - 130D2-Fluorobiphenyl
0 30 - 130D2-Fluorophenol
0 39 - 130DTerphenyl-d14
0 30 - 130DPhenol-d5
0 27 - 130DNitrobenzene-d5
TestAmerica Savannah Page 78 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-4-NS
Client Matrix: % Moisture: 12.4
680-56861-4
Solid
Date Sampled: 04/14/2010 1715
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/10/2010 1140
200
8270C Analysis Batch: 680-167967
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1158.d
30.10 g
1.0 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
1200000 750007700Diphenyl ether
Surrogate %Rec Acceptance LimitsQualifier
0 34 - 130D2,4,6-Tribromophenol
0 34 - 130D2-Fluorobiphenyl
0 30 - 130D2-Fluorophenol
0 39 - 130DTerphenyl-d14
0 30 - 130DPhenol-d5
0 27 - 130DNitrobenzene-d5
TestAmerica Savannah Page 79 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-4-LS
Client Matrix: % Moisture: 60.5
680-56861-5
Solid
Date Sampled: 04/14/2010 1735
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/03/2010 1910
10
8270C Analysis Batch: 680-167447
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1010.d
30.05 g
20 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
170000 U 17000021000Acenaphthene
170000 U 17000018000Acenaphthylene
170000 U 17000014000Acetophenone
170000 U 170000140002-Acetylaminofluorene
34000000 U 340000001400000alpha,alpha-Dimethyl phenethylamine
170000 U 170000190004-Aminobiphenyl
330000 U 33000017000Aniline
170000 U 17000013000Anthracene
170000 U 17000029000Aramite, Total
170000 U 17000014000Benzo[a]anthracene
170000 U 17000026000Benzo[a]pyrene
170000 U 17000019000Benzo[b]fluoranthene
170000 U 17000011000Benzo[g,h,i]perylene
170000 U 17000033000Benzo[k]fluoranthene
170000 U 17000017000Benzyl alcohol
1600000 170000140001,1'-Biphenyl
170000 U 17000020000Bis(2-chloroethoxy)methane
170000 U 17000023000Bis(2-chloroethyl)ether
170000 U 17000015000bis(chloroisopropyl) ether
170000 U 17000017000Bis(2-ethylhexyl) phthalate
170000 U 170000180004-Bromophenyl phenyl ether
170000 U 17000013000Butyl benzyl phthalate
330000 U 330000260004-Chloroaniline
170000 U 170000180004-Chloro-3-methylphenol
170000 U 170000200002-Chloronaphthalene
170000 U 170000200002-Chlorophenol
170000 U 170000190004-Chlorophenyl phenyl ether
170000 U 17000011000Chrysene
170000 U 17000086000Diallate
170000 U 17000012000Dibenz(a,h)anthracene
170000 U 17000017000Dibenzofuran
170000 U 170000190001,2-Dichlorobenzene
170000 U 170000170001,3-Dichlorobenzene
170000 U 170000180001,4-Dichlorobenzene
330000 U 330000140003,3'-Dichlorobenzidine
170000 U 170000180002,4-Dichlorophenol
170000 U 170000140002,6-Dichlorophenol
170000 U 17000018000Diethyl phthalate
170000 U 17000013000Dimethoate
170000 U 17000086007,12-Dimethylbenz(a)anthracene
860000 U 8600004200003,3'-Dimethylbenzidine
170000 U 170000220002,4-Dimethylphenol
170000 U 17000017000Dimethyl phthalate
170000 U 17000015000Di-n-butyl phthalate
170000 U 170000120001,3-Dinitrobenzene
860000 U 860000860004,6-Dinitro-2-methylphenol
TestAmerica Savannah Page 80 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-4-LS
Client Matrix: % Moisture: 60.5
680-56861-5
Solid
Date Sampled: 04/14/2010 1735
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/03/2010 1910
10
8270C Analysis Batch: 680-167447
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1010.d
30.05 g
20 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
860000 U 8600004200002,4-Dinitrophenol
170000 U 170000250002,4-Dinitrotoluene
170000 U 170000210002,6-Dinitrotoluene
170000 U 17000015000Di-n-octyl phthalate
170000 U 17000081000Dinoseb
170000 U 170000610001,4-Dioxane
170000 U 1700008600Disulfoton
170000 U 17000016000Ethyl methanesulfonate
170000 U 17000011000Ethyl Parathion
170000 U * 17000015000Famphur
170000 U 17000016000Fluoranthene
170000 U 17000018000Fluorene
170000 U 17000020000Hexachlorobenzene
170000 U 17000018000Hexachlorobutadiene
170000 U 17000021000Hexachlorocyclopentadiene
170000 U 17000014000Hexachloroethane
86000000 U 860000006600000Hexachlorophene
170000 U * 17000015000Hexachloropropene
170000 U 17000014000Indeno[1,2,3-cd]pyrene
170000 U 17000017000Isophorone
170000 U 17000012000Isosafrole
34000000 U 34000000420000Methapyrilene
170000 U 170000210003-Methylcholanthrene
170000 U * 1700008600Methyl methanesulfonate
170000 U 170000190002-Methylnaphthalene
170000 U 17000013000Methyl parathion
170000 U 170000140002-Methylphenol
170000 U 170000220003 & 4 Methylphenol
170000 U 17000015000Naphthalene
170000 U * 17000086001,4-Naphthoquinone
170000 U * 170000330001-Naphthylamine
170000 U 170000170002-Naphthylamine
860000 U 860000230002-Nitroaniline
860000 U 860000230003-Nitroaniline
860000 U 860000250004-Nitroaniline
170000 U 17000013000Nitrobenzene
170000 U 170000210002-Nitrophenol
860000 U 8600001700004-Nitrophenol
1700000 U 17000004200004-Nitroquinoline-1-oxide
170000 U 17000013000N-Nitro-o-toluidine
170000 U 17000014000N-Nitrosodiethylamine
170000 U 17000061000N-Nitrosodimethylamine
170000 U 17000012000N-Nitrosodi-n-butylamine
170000 U 17000016000N-Nitrosodi-n-propylamine
170000 U 17000017000N-Nitrosodiphenylamine
170000 U 17000013000N-Nitrosomethylethylamine
TestAmerica Savannah Page 81 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-4-LS
Client Matrix: % Moisture: 60.5
680-56861-5
Solid
Date Sampled: 04/14/2010 1735
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/03/2010 1910
10
8270C Analysis Batch: 680-167447
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1010.d
30.05 g
20 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
170000 U 17000014000N-Nitrosomorpholine
170000 U 17000011000N-Nitrosopiperidine
170000 U 1700009100N-Nitrosopyrrolidine
170000 U * 17000020000o,o',o''-Triethylphosphorothioate
170000 U 1700009600p-Dimethylamino azobenzene
170000 U 17000013000Pentachlorobenzene
170000 U 17000011000Pentachloronitrobenzene
860000 U 860000170000Pentachlorophenol
170000 U 17000017000Phenacetin
170000 U 17000014000Phenanthrene
170000 U 17000017000Phenol
170000 U * 17000011000Phorate
170000 U 17000086002-Picoline
860000 U * 860000420000p-Phenylene diamine
170000 U 17000012000Pronamide
170000 U 17000014000Pyrene
170000 U 17000015000Pyridine
170000 U 17000012000Safrole, Total
170000 U 17000010000Sulfotepp
170000 U 170000160001,2,4,5-Tetrachlorobenzene
170000 U 170000110002,3,4,6-Tetrachlorophenol
170000 U 17000012000Thionazin
170000 U 170000180002-Toluidine
170000 U 170000160001,2,4-Trichlorobenzene
170000 U 170000180002,4,5-Trichlorophenol
170000 U 170000150002,4,6-Trichlorophenol
170000 U 170000860001,3,5-Trinitrobenzene
Surrogate %Rec Acceptance LimitsQualifier
0 34 - 130D2,4,6-Tribromophenol
0 34 - 130D2-Fluorobiphenyl
0 30 - 130D2-Fluorophenol
0 39 - 130DTerphenyl-d14
0 30 - 130DPhenol-d5
0 27 - 130DNitrobenzene-d5
TestAmerica Savannah Page 82 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-4-LS
Client Matrix: % Moisture: 60.5
680-56861-5
Solid
Date Sampled: 04/14/2010 1735
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/10/2010 1203
50
8270C Analysis Batch: 680-167967
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1159.d
30.05 g
20 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
5200000 83000086000Diphenyl ether
Surrogate %Rec Acceptance LimitsQualifier
0 34 - 130D2,4,6-Tribromophenol
0 34 - 130D2-Fluorobiphenyl
0 30 - 130D2-Fluorophenol
0 39 - 130DTerphenyl-d14
0 30 - 130DPhenol-d5
0 27 - 130DNitrobenzene-d5
TestAmerica Savannah Page 83 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-3-US
Client Matrix: % Moisture: 75.7
680-56861-6
Solid
Date Sampled: 04/15/2010 0845
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/03/2010 1934
10
8270C Analysis Batch: 680-167447
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1011.d
30.02 g
15 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
200000 U 20000025000Acenaphthene
200000 U 20000022000Acenaphthylene
200000 U 20000017000Acetophenone
200000 U 200000170002-Acetylaminofluorene
41000000 U 410000001700000alpha,alpha-Dimethyl phenethylamine
200000 U 200000230004-Aminobiphenyl
410000 U 41000021000Aniline
200000 U 20000015000Anthracene
200000 U 20000035000Aramite, Total
200000 U 20000017000Benzo[a]anthracene
200000 U 20000032000Benzo[a]pyrene
200000 U 20000023000Benzo[b]fluoranthene
200000 U 20000014000Benzo[g,h,i]perylene
200000 U 20000040000Benzo[k]fluoranthene
200000 U 20000020000Benzyl alcohol
340000 200000170001,1'-Biphenyl
200000 U 20000024000Bis(2-chloroethoxy)methane
200000 U 20000028000Bis(2-chloroethyl)ether
200000 U 20000018000bis(chloroisopropyl) ether
200000 U 20000020000Bis(2-ethylhexyl) phthalate
200000 U 200000220004-Bromophenyl phenyl ether
200000 U 20000016000Butyl benzyl phthalate
410000 U 410000320004-Chloroaniline
200000 U 200000220004-Chloro-3-methylphenol
200000 U 200000240002-Chloronaphthalene
200000 U 200000250002-Chlorophenol
200000 U 200000230004-Chlorophenyl phenyl ether
200000 U 20000013000Chrysene
200000 U 200000100000Diallate
200000 U 20000015000Dibenz(a,h)anthracene
200000 U 20000020000Dibenzofuran
200000 U 200000230001,2-Dichlorobenzene
200000 U 200000210001,3-Dichlorobenzene
200000 U 200000220001,4-Dichlorobenzene
410000 U 410000170003,3'-Dichlorobenzidine
200000 U 200000220002,4-Dichlorophenol
200000 U 200000170002,6-Dichlorophenol
200000 U 20000022000Diethyl phthalate
200000 U 20000015000Dimethoate
200000 U 200000100007,12-Dimethylbenz(a)anthracene
1000000 U 10000005100003,3'-Dimethylbenzidine
200000 U 200000270002,4-Dimethylphenol
200000 U 20000021000Dimethyl phthalate
200000 U 20000018000Di-n-butyl phthalate
200000 U 200000150001,3-Dinitrobenzene
1000000 U 10000001000004,6-Dinitro-2-methylphenol
TestAmerica Savannah Page 84 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-3-US
Client Matrix: % Moisture: 75.7
680-56861-6
Solid
Date Sampled: 04/15/2010 0845
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/03/2010 1934
10
8270C Analysis Batch: 680-167447
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1011.d
30.02 g
15 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
1000000 U 10000005100002,4-Dinitrophenol
200000 U 200000300002,4-Dinitrotoluene
200000 U 200000260002,6-Dinitrotoluene
200000 U 20000018000Di-n-octyl phthalate
200000 U 20000099000Dinoseb
200000 U 200000740001,4-Dioxane
200000 U 20000010000Disulfoton
200000 U 20000019000Ethyl methanesulfonate
200000 U 20000014000Ethyl Parathion
200000 U * 20000018000Famphur
200000 U 20000020000Fluoranthene
200000 U 20000022000Fluorene
200000 U 20000024000Hexachlorobenzene
200000 U 20000022000Hexachlorobutadiene
200000 U 20000025000Hexachlorocyclopentadiene
200000 U 20000017000Hexachloroethane
100000000 U 1000000008000000Hexachlorophene
200000 U * 20000018000Hexachloropropene
200000 U 20000017000Indeno[1,2,3-cd]pyrene
200000 U 20000020000Isophorone
200000 U 20000015000Isosafrole
41000000 U 41000000510000Methapyrilene
200000 U 200000250003-Methylcholanthrene
200000 U * 20000010000Methyl methanesulfonate
200000 U 200000230002-Methylnaphthalene
200000 U 20000016000Methyl parathion
200000 U 200000170002-Methylphenol
200000 U 200000270003 & 4 Methylphenol
200000 U 20000018000Naphthalene
200000 U * 200000100001,4-Naphthoquinone
200000 U * 200000410001-Naphthylamine
200000 U 200000210002-Naphthylamine
1000000 U 1000000280002-Nitroaniline
1000000 U 1000000280003-Nitroaniline
1000000 U 1000000300004-Nitroaniline
200000 U 20000016000Nitrobenzene
200000 U 200000250002-Nitrophenol
1000000 U 10000002000004-Nitrophenol
2000000 U 20000005100004-Nitroquinoline-1-oxide
200000 U 20000016000N-Nitro-o-toluidine
200000 U 20000017000N-Nitrosodiethylamine
200000 U 20000074000N-Nitrosodimethylamine
200000 U 20000015000N-Nitrosodi-n-butylamine
200000 U 20000020000N-Nitrosodi-n-propylamine
200000 U 20000020000N-Nitrosodiphenylamine
200000 U 20000015000N-Nitrosomethylethylamine
TestAmerica Savannah Page 85 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-3-US
Client Matrix: % Moisture: 75.7
680-56861-6
Solid
Date Sampled: 04/15/2010 0845
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/03/2010 1934
10
8270C Analysis Batch: 680-167447
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1011.d
30.02 g
15 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
200000 U 20000017000N-Nitrosomorpholine
200000 U 20000013000N-Nitrosopiperidine
200000 U 20000011000N-Nitrosopyrrolidine
200000 U * 20000025000o,o',o''-Triethylphosphorothioate
200000 U 20000012000p-Dimethylamino azobenzene
200000 U 20000015000Pentachlorobenzene
200000 U 20000013000Pentachloronitrobenzene
1000000 U 1000000200000Pentachlorophenol
200000 U 20000020000Phenacetin
200000 U 20000017000Phenanthrene
200000 U 20000021000Phenol
200000 U * 20000014000Phorate
200000 U 200000100002-Picoline
1000000 U * 1000000510000p-Phenylene diamine
200000 U 20000015000Pronamide
22000 J 20000017000Pyrene
200000 U 20000018000Pyridine
200000 U 20000015000Safrole, Total
200000 U 20000012000Sulfotepp
200000 U 200000190001,2,4,5-Tetrachlorobenzene
200000 U 200000140002,3,4,6-Tetrachlorophenol
200000 U 20000014000Thionazin
200000 U 200000220002-Toluidine
200000 U 200000190001,2,4-Trichlorobenzene
200000 U 200000220002,4,5-Trichlorophenol
200000 U 200000180002,4,6-Trichlorophenol
200000 U 2000001000001,3,5-Trinitrobenzene
1100000 20000021000Diphenyl ether
Surrogate %Rec Acceptance LimitsQualifier
0 34 - 130D2,4,6-Tribromophenol
0 34 - 130D2-Fluorobiphenyl
0 30 - 130D2-Fluorophenol
0 39 - 130DTerphenyl-d14
0 30 - 130DPhenol-d5
0 27 - 130DNitrobenzene-d5
TestAmerica Savannah Page 86 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-5-NS
Client Matrix: % Moisture: 23.8
680-56861-7
Solid
Date Sampled: 04/15/2010 0950
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/03/2010 1958
10
8270C Analysis Batch: 680-167447
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1012.d
30.12 g
1.0 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
4300 U 4300540Acenaphthene
4300 U 4300470Acenaphthylene
4300 U 4300370Acetophenone
4300 U 43003702-Acetylaminofluorene
880000 U 88000035000alpha,alpha-Dimethyl phenethylamine
4300 U 43004804-Aminobiphenyl
8600 U 8600440Aniline
4300 U 4300330Anthracene
4300 U 4300750Aramite, Total
4300 U 4300350Benzo[a]anthracene
4300 U 4300680Benzo[a]pyrene
4300 U 4300500Benzo[b]fluoranthene
4300 U 4300290Benzo[g,h,i]perylene
4300 U 4300850Benzo[k]fluoranthene
4300 U 4300430Benzyl alcohol
4300 U 43003701,1'-Biphenyl
4300 U 4300510Bis(2-chloroethoxy)methane
4300 U 4300590Bis(2-chloroethyl)ether
4300 U 4300390bis(chloroisopropyl) ether
4300 U 4300430Bis(2-ethylhexyl) phthalate
4300 U 43004704-Bromophenyl phenyl ether
4300 U 4300340Butyl benzyl phthalate
8600 U 86006804-Chloroaniline
4300 U 43004604-Chloro-3-methylphenol
4300 U 43005102-Chloronaphthalene
4300 U 43005202-Chlorophenol
4300 U 43004804-Chlorophenyl phenyl ether
4300 U 4300270Chrysene
4300 U 43002200Diallate
4300 U 4300310Dibenz(a,h)anthracene
4300 U 4300430Dibenzofuran
4300 U 43004801,2-Dichlorobenzene
4300 U 43004401,3-Dichlorobenzene
4300 U 43004601,4-Dichlorobenzene
8600 U 86003703,3'-Dichlorobenzidine
4300 U 43004602,4-Dichlorophenol
4300 U 43003502,6-Dichlorophenol
4300 U 4300460Diethyl phthalate
4300 U 4300330Dimethoate
4300 U 43002207,12-Dimethylbenz(a)anthracene
22000 U 22000110003,3'-Dimethylbenzidine
4300 U 43005802,4-Dimethylphenol
4300 U 4300440Dimethyl phthalate
4300 U 4300390Di-n-butyl phthalate
4300 U 43003101,3-Dinitrobenzene
22000 U 2200022004,6-Dinitro-2-methylphenol
TestAmerica Savannah Page 87 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-5-NS
Client Matrix: % Moisture: 23.8
680-56861-7
Solid
Date Sampled: 04/15/2010 0950
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/03/2010 1958
10
8270C Analysis Batch: 680-167447
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1012.d
30.12 g
1.0 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
22000 U 22000110002,4-Dinitrophenol
4300 U 43006402,4-Dinitrotoluene
4300 U 43005502,6-Dinitrotoluene
4300 U 4300380Di-n-octyl phthalate
4300 U 43002100Dinoseb
4300 U 430016001,4-Dioxane
4300 U 4300220Disulfoton
4300 U 4300410Ethyl methanesulfonate
4300 U 4300290Ethyl Parathion
4300 U * 4300380Famphur
4300 U 4300420Fluoranthene
4300 U 4300470Fluorene
4300 U 4300510Hexachlorobenzene
4300 U 4300470Hexachlorobutadiene
4300 U 4300540Hexachlorocyclopentadiene
4300 U 4300370Hexachloroethane
2200000 U 2200000170000Hexachlorophene
4300 U * 4300380Hexachloropropene
4300 U 4300370Indeno[1,2,3-cd]pyrene
4300 U 4300430Isophorone
4300 U 4300310Isosafrole
880000 U 88000011000Methapyrilene
4300 U 43005403-Methylcholanthrene
4300 U * 4300220Methyl methanesulfonate
4300 U 43005002-Methylnaphthalene
4300 U 4300340Methyl parathion
4300 U 43003502-Methylphenol
630 J 43005603 & 4 Methylphenol
4300 U 4300390Naphthalene
4300 U * 43002201,4-Naphthoquinone
4300 U * 43008601-Naphthylamine
4300 U 43004402-Naphthylamine
3500 J 220005902-Nitroaniline
22000 U 220006003-Nitroaniline
22000 U 220006404-Nitroaniline
4300 U 4300340Nitrobenzene
4300 U 43005402-Nitrophenol
22000 U 2200043004-Nitrophenol
43000 U 43000110004-Nitroquinoline-1-oxide
4300 U 4300340N-Nitro-o-toluidine
4300 U 4300370N-Nitrosodiethylamine
4300 U 43001600N-Nitrosodimethylamine
4300 U 4300310N-Nitrosodi-n-butylamine
4300 U 4300420N-Nitrosodi-n-propylamine
4300 U 4300430N-Nitrosodiphenylamine
4300 U 4300330N-Nitrosomethylethylamine
TestAmerica Savannah Page 88 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-5-NS
Client Matrix: % Moisture: 23.8
680-56861-7
Solid
Date Sampled: 04/15/2010 0950
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/03/2010 1958
10
8270C Analysis Batch: 680-167447
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1012.d
30.12 g
1.0 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
4300 U 4300350N-Nitrosomorpholine
4300 U 4300270N-Nitrosopiperidine
4300 U 4300240N-Nitrosopyrrolidine
4300 U * 4300520o,o',o''-Triethylphosphorothioate
4300 U 4300250p-Dimethylamino azobenzene
4300 U 4300330Pentachlorobenzene
4300 U 4300270Pentachloronitrobenzene
22000 U 220004300Pentachlorophenol
4300 U 4300430Phenacetin
4300 U 4300350Phenanthrene
4300 U 4300440Phenol
4300 U * 4300290Phorate
4300 U 43002202-Picoline
22000 U * 2200011000p-Phenylene diamine
4300 U 4300310Pronamide
4300 U 4300350Pyrene
4300 U 4300380Pyridine
4300 U 4300310Safrole, Total
4300 U 4300260Sulfotepp
4300 U 43004101,2,4,5-Tetrachlorobenzene
4300 U 43002902,3,4,6-Tetrachlorophenol
4300 U 4300300Thionazin
4300 U 43004602-Toluidine
4300 U 43004101,2,4-Trichlorobenzene
4300 U 43004602,4,5-Trichlorophenol
4300 U 43003802,4,6-Trichlorophenol
4300 U 430022001,3,5-Trinitrobenzene
12000 4300440Diphenyl ether
Surrogate %Rec Acceptance LimitsQualifier
0 34 - 130D2,4,6-Tribromophenol
0 34 - 130D2-Fluorobiphenyl
0 30 - 130D2-Fluorophenol
0 39 - 130DTerphenyl-d14
0 30 - 130DPhenol-d5
0 27 - 130DNitrobenzene-d5
TestAmerica Savannah Page 89 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-5-LS
Client Matrix: % Moisture: 68.0
680-56861-8
Solid
Date Sampled: 04/15/2010 1005
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/03/2010 2022
10
8270C Analysis Batch: 680-167447
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1013.d
30.02 g
10 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
100000 U 10000013000Acenaphthene
100000 U 10000011000Acenaphthylene
100000 U 1000008700Acetophenone
100000 U 10000087002-Acetylaminofluorene
21000000 U 21000000840000alpha,alpha-Dimethyl phenethylamine
100000 U 100000120004-Aminobiphenyl
210000 U 21000011000Aniline
100000 U 1000007800Anthracene
100000 U 10000018000Aramite, Total
100000 U 1000008400Benzo[a]anthracene
100000 U 10000016000Benzo[a]pyrene
100000 U 10000012000Benzo[b]fluoranthene
100000 U 1000006900Benzo[g,h,i]perylene
100000 U 10000020000Benzo[k]fluoranthene
100000 U 10000010000Benzyl alcohol
940000 10000087001,1'-Biphenyl
100000 U 10000012000Bis(2-chloroethoxy)methane
100000 U 10000014000Bis(2-chloroethyl)ether
100000 U 1000009400bis(chloroisopropyl) ether
100000 U 10000010000Bis(2-ethylhexyl) phthalate
100000 U 100000110004-Bromophenyl phenyl ether
100000 U 1000008100Butyl benzyl phthalate
210000 U 210000160004-Chloroaniline
100000 U 100000110004-Chloro-3-methylphenol
100000 U 100000120002-Chloronaphthalene
100000 U 100000120002-Chlorophenol
100000 U 100000120004-Chlorophenyl phenyl ether
100000 U 1000006500Chrysene
100000 U 10000053000Diallate
100000 U 1000007500Dibenz(a,h)anthracene
100000 U 10000010000Dibenzofuran
100000 U 100000120001,2-Dichlorobenzene
100000 U 100000110001,3-Dichlorobenzene
100000 U 100000110001,4-Dichlorobenzene
210000 U 21000087003,3'-Dichlorobenzidine
100000 U 100000110002,4-Dichlorophenol
100000 U 10000084002,6-Dichlorophenol
100000 U 10000011000Diethyl phthalate
100000 U 1000007800Dimethoate
100000 U 10000053007,12-Dimethylbenz(a)anthracene
530000 U 5300002600003,3'-Dimethylbenzidine
100000 U 100000140002,4-Dimethylphenol
100000 U 10000011000Dimethyl phthalate
100000 U 1000009400Di-n-butyl phthalate
100000 U 10000075001,3-Dinitrobenzene
530000 U 530000530004,6-Dinitro-2-methylphenol
TestAmerica Savannah Page 90 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-5-LS
Client Matrix: % Moisture: 68.0
680-56861-8
Solid
Date Sampled: 04/15/2010 1005
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/03/2010 2022
10
8270C Analysis Batch: 680-167447
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1013.d
30.02 g
10 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
530000 U 5300002600002,4-Dinitrophenol
100000 U 100000150002,4-Dinitrotoluene
100000 U 100000130002,6-Dinitrotoluene
100000 U 1000009000Di-n-octyl phthalate
100000 U 10000050000Dinoseb
100000 U 100000370001,4-Dioxane
100000 U 1000005300Disulfoton
100000 U 1000009700Ethyl methanesulfonate
100000 U 1000006900Ethyl Parathion
100000 U * 1000009000Famphur
100000 U 10000010000Fluoranthene
100000 U 10000011000Fluorene
100000 U 10000012000Hexachlorobenzene
100000 U 10000011000Hexachlorobutadiene
100000 U 10000013000Hexachlorocyclopentadiene
100000 U 1000008700Hexachloroethane
53000000 U 530000004100000Hexachlorophene
100000 U * 1000009000Hexachloropropene
100000 U 1000008700Indeno[1,2,3-cd]pyrene
100000 U 10000010000Isophorone
100000 U 1000007500Isosafrole
21000000 U 21000000260000Methapyrilene
100000 U 100000130003-Methylcholanthrene
100000 U * 1000005300Methyl methanesulfonate
100000 U 100000120002-Methylnaphthalene
100000 U 1000008100Methyl parathion
100000 U 10000084002-Methylphenol
100000 U 100000130003 & 4 Methylphenol
100000 U 1000009400Naphthalene
100000 U * 10000053001,4-Naphthoquinone
100000 U * 100000210001-Naphthylamine
100000 U 100000110002-Naphthylamine
530000 U 530000140002-Nitroaniline
530000 U 530000140003-Nitroaniline
530000 U 530000150004-Nitroaniline
100000 U 1000008100Nitrobenzene
100000 U 100000130002-Nitrophenol
530000 U 5300001000004-Nitrophenol
1000000 U 10000002600004-Nitroquinoline-1-oxide
100000 U 1000008100N-Nitro-o-toluidine
100000 U 1000008700N-Nitrosodiethylamine
100000 U 10000037000N-Nitrosodimethylamine
100000 U 1000007500N-Nitrosodi-n-butylamine
100000 U 10000010000N-Nitrosodi-n-propylamine
100000 U 10000010000N-Nitrosodiphenylamine
100000 U 1000007800N-Nitrosomethylethylamine
TestAmerica Savannah Page 91 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-5-LS
Client Matrix: % Moisture: 68.0
680-56861-8
Solid
Date Sampled: 04/15/2010 1005
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/03/2010 2022
10
8270C Analysis Batch: 680-167447
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1013.d
30.02 g
10 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
100000 U 1000008400N-Nitrosomorpholine
100000 U 1000006500N-Nitrosopiperidine
100000 U 1000005600N-Nitrosopyrrolidine
100000 U * 10000012000o,o',o''-Triethylphosphorothioate
100000 U 1000005900p-Dimethylamino azobenzene
100000 U 1000007800Pentachlorobenzene
100000 U 1000006500Pentachloronitrobenzene
530000 U 530000100000Pentachlorophenol
100000 U 10000010000Phenacetin
100000 U 1000008400Phenanthrene
100000 U 10000011000Phenol
100000 U * 1000006900Phorate
100000 U 10000053002-Picoline
530000 U * 530000260000p-Phenylene diamine
100000 U 1000007500Pronamide
100000 U 1000008400Pyrene
100000 U 1000009000Pyridine
100000 U 1000007500Safrole, Total
100000 U 1000006200Sulfotepp
100000 U 10000097001,2,4,5-Tetrachlorobenzene
100000 U 10000069002,3,4,6-Tetrachlorophenol
100000 U 1000007200Thionazin
100000 U 100000110002-Toluidine
100000 U 10000097001,2,4-Trichlorobenzene
100000 U 100000110002,4,5-Trichlorophenol
100000 U 10000090002,4,6-Trichlorophenol
100000 U 100000530001,3,5-Trinitrobenzene
Surrogate %Rec Acceptance LimitsQualifier
0 34 - 130D2,4,6-Tribromophenol
0 34 - 130D2-Fluorobiphenyl
0 30 - 130D2-Fluorophenol
0 39 - 130DTerphenyl-d14
0 30 - 130DPhenol-d5
0 27 - 130DNitrobenzene-d5
TestAmerica Savannah Page 92 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-5-LS
Client Matrix: % Moisture: 68.0
680-56861-8
Solid
Date Sampled: 04/15/2010 1005
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/10/2010 1227
50
8270C Analysis Batch: 680-167967
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1160.d
30.02 g
10 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
2800000 51000053000Diphenyl ether
Surrogate %Rec Acceptance LimitsQualifier
0 34 - 130D2,4,6-Tribromophenol
0 34 - 130D2-Fluorobiphenyl
0 30 - 130D2-Fluorophenol
0 39 - 130DTerphenyl-d14
0 30 - 130DPhenol-d5
0 27 - 130DNitrobenzene-d5
TestAmerica Savannah Page 93 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-4-US
Client Matrix: % Moisture: 77.8
680-56861-9
Solid
Date Sampled: 04/15/2010 1100
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/03/2010 2046
10
8270C Analysis Batch: 680-167447
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1014.d
30.11 g
5.0 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
74000 U 740009200Acenaphthene
74000 U 740008100Acenaphthylene
74000 U 740006300Acetophenone
74000 U 7400063002-Acetylaminofluorene
15000000 U 15000000600000alpha,alpha-Dimethyl phenethylamine
74000 U 7400083004-Aminobiphenyl
150000 U 1500007600Aniline
74000 U 740005600Anthracene
74000 U 7400013000Aramite, Total
74000 U 740006000Benzo[a]anthracene
74000 U 7400012000Benzo[a]pyrene
74000 U 740008500Benzo[b]fluoranthene
74000 U 740004900Benzo[g,h,i]perylene
74000 U 7400015000Benzo[k]fluoranthene
74000 U 740007400Benzyl alcohol
180000 7400063001,1'-Biphenyl
74000 U 740008700Bis(2-chloroethoxy)methane
74000 U 7400010000Bis(2-chloroethyl)ether
74000 U 740006700bis(chloroisopropyl) ether
74000 U 740007400Bis(2-ethylhexyl) phthalate
74000 U 7400081004-Bromophenyl phenyl ether
74000 U 740005800Butyl benzyl phthalate
150000 U 150000120004-Chloroaniline
74000 U 7400078004-Chloro-3-methylphenol
74000 U 7400087002-Chloronaphthalene
74000 U 7400090002-Chlorophenol
74000 U 7400083004-Chlorophenyl phenyl ether
74000 U 740004700Chrysene
74000 U 7400038000Diallate
74000 U 740005400Dibenz(a,h)anthracene
74000 U 740007400Dibenzofuran
74000 U 7400083001,2-Dichlorobenzene
74000 U 7400076001,3-Dichlorobenzene
74000 U 7400078001,4-Dichlorobenzene
150000 U 15000063003,3'-Dichlorobenzidine
74000 U 7400078002,4-Dichlorophenol
74000 U 7400060002,6-Dichlorophenol
74000 U 740007800Diethyl phthalate
74000 U 740005600Dimethoate
74000 U 7400038007,12-Dimethylbenz(a)anthracene
380000 U 3800001900003,3'-Dimethylbenzidine
74000 U 7400099002,4-Dimethylphenol
74000 U 740007600Dimethyl phthalate
74000 U 740006700Di-n-butyl phthalate
74000 U 7400054001,3-Dinitrobenzene
380000 U 380000380004,6-Dinitro-2-methylphenol
TestAmerica Savannah Page 94 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-4-US
Client Matrix: % Moisture: 77.8
680-56861-9
Solid
Date Sampled: 04/15/2010 1100
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/03/2010 2046
10
8270C Analysis Batch: 680-167447
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1014.d
30.11 g
5.0 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
380000 U 3800001900002,4-Dinitrophenol
74000 U 74000110002,4-Dinitrotoluene
74000 U 7400094002,6-Dinitrotoluene
74000 U 740006500Di-n-octyl phthalate
74000 U 7400036000Dinoseb
74000 U 74000270001,4-Dioxane
74000 U 740003800Disulfoton
74000 U 740006900Ethyl methanesulfonate
74000 U 740004900Ethyl Parathion
74000 U * 740006500Famphur
74000 U 740007200Fluoranthene
74000 U 740008100Fluorene
74000 U 740008700Hexachlorobenzene
74000 U 740008100Hexachlorobutadiene
74000 U 740009200Hexachlorocyclopentadiene
74000 U 740006300Hexachloroethane
38000000 U 380000002900000Hexachlorophene
74000 U * 740006500Hexachloropropene
74000 U 740006300Indeno[1,2,3-cd]pyrene
74000 U 740007400Isophorone
74000 U 740005400Isosafrole
15000000 U 15000000190000Methapyrilene
74000 U 7400092003-Methylcholanthrene
74000 U * 740003800Methyl methanesulfonate
74000 U 7400085002-Methylnaphthalene
74000 U 740005800Methyl parathion
74000 U 7400060002-Methylphenol
74000 U 7400096003 & 4 Methylphenol
74000 U 740006700Naphthalene
74000 U * 7400038001,4-Naphthoquinone
74000 U * 74000150001-Naphthylamine
74000 U 7400076002-Naphthylamine
380000 U 380000100002-Nitroaniline
380000 U 380000100003-Nitroaniline
380000 U 380000110004-Nitroaniline
74000 U 740005800Nitrobenzene
74000 U 7400092002-Nitrophenol
380000 U 380000740004-Nitrophenol
740000 U 7400001900004-Nitroquinoline-1-oxide
74000 U 740005800N-Nitro-o-toluidine
74000 U 740006300N-Nitrosodiethylamine
74000 U 7400027000N-Nitrosodimethylamine
74000 U 740005400N-Nitrosodi-n-butylamine
74000 U 740007200N-Nitrosodi-n-propylamine
74000 U 740007400N-Nitrosodiphenylamine
74000 U 740005600N-Nitrosomethylethylamine
TestAmerica Savannah Page 95 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-4-US
Client Matrix: % Moisture: 77.8
680-56861-9
Solid
Date Sampled: 04/15/2010 1100
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/03/2010 2046
10
8270C Analysis Batch: 680-167447
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1014.d
30.11 g
5.0 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
74000 U 740006000N-Nitrosomorpholine
74000 U 740004700N-Nitrosopiperidine
74000 U 740004000N-Nitrosopyrrolidine
74000 U * 740009000o,o',o''-Triethylphosphorothioate
74000 U 740004300p-Dimethylamino azobenzene
74000 U 740005600Pentachlorobenzene
74000 U 740004700Pentachloronitrobenzene
380000 U 38000074000Pentachlorophenol
74000 U 740007400Phenacetin
74000 U 740006000Phenanthrene
74000 U 740007600Phenol
74000 U * 740004900Phorate
74000 U 7400038002-Picoline
380000 U * 380000190000p-Phenylene diamine
74000 U 740005400Pronamide
74000 U 740006000Pyrene
74000 U 740006500Pyridine
74000 U 740005400Safrole, Total
74000 U 740004500Sulfotepp
74000 U 7400069001,2,4,5-Tetrachlorobenzene
74000 U 7400049002,3,4,6-Tetrachlorophenol
74000 U 740005200Thionazin
74000 U 7400078002-Toluidine
74000 U 7400069001,2,4-Trichlorobenzene
74000 U 7400078002,4,5-Trichlorophenol
74000 U 7400065002,4,6-Trichlorophenol
74000 U 74000380001,3,5-Trinitrobenzene
570000 740007600Diphenyl ether
Surrogate %Rec Acceptance LimitsQualifier
0 34 - 130D2,4,6-Tribromophenol
0 34 - 130D2-Fluorobiphenyl
0 30 - 130D2-Fluorophenol
0 39 - 130DTerphenyl-d14
0 30 - 130DPhenol-d5
0 27 - 130DNitrobenzene-d5
TestAmerica Savannah Page 96 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-6-NS
Client Matrix: % Moisture: 20.4
680-56861-10
Solid
Date Sampled: 04/15/2010 1105
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/04/2010 1442
50
8270C Analysis Batch: 680-167473
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1015a.d
30.03 g
1.0 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
21000 U 210002600Acenaphthene
21000 U 210002300Acenaphthylene
21000 U 210001800Acetophenone
21000 U 2100018002-Acetylaminofluorene
4200000 U 4200000170000alpha,alpha-Dimethyl phenethylamine
21000 U 2100023004-Aminobiphenyl
41000 U 410002100Aniline
21000 U 210001600Anthracene
21000 U 210003600Aramite, Total
21000 U 210001700Benzo[a]anthracene
21000 U 210003300Benzo[a]pyrene
21000 U 210002400Benzo[b]fluoranthene
21000 U 210001400Benzo[g,h,i]perylene
21000 U 210004100Benzo[k]fluoranthene
21000 U 210002100Benzyl alcohol
290000 2100018001,1'-Biphenyl
21000 U 210002400Bis(2-chloroethoxy)methane
21000 U 210002800Bis(2-chloroethyl)ether
21000 U 210001900bis(chloroisopropyl) ether
21000 U 210002100Bis(2-ethylhexyl) phthalate
21000 U 2100023004-Bromophenyl phenyl ether
21000 U 210001600Butyl benzyl phthalate
41000 U 4100033004-Chloroaniline
21000 U 2100022004-Chloro-3-methylphenol
21000 U 2100024002-Chloronaphthalene
21000 U 2100025002-Chlorophenol
21000 U 2100023004-Chlorophenyl phenyl ether
21000 U 210001300Chrysene
21000 U 2100011000Diallate
21000 U 210001500Dibenz(a,h)anthracene
21000 U 210002100Dibenzofuran
21000 U 2100023001,2-Dichlorobenzene
21000 U 2100021001,3-Dichlorobenzene
21000 U 2100022001,4-Dichlorobenzene
41000 U 4100018003,3'-Dichlorobenzidine
21000 U 2100022002,4-Dichlorophenol
21000 U 2100017002,6-Dichlorophenol
21000 U 210002200Diethyl phthalate
21000 U 210001600Dimethoate
21000 U 2100011007,12-Dimethylbenz(a)anthracene
110000 U 110000520003,3'-Dimethylbenzidine
21000 U 2100028002,4-Dimethylphenol
21000 U 210002100Dimethyl phthalate
21000 U 210001900Di-n-butyl phthalate
21000 U 2100015001,3-Dinitrobenzene
110000 U 110000110004,6-Dinitro-2-methylphenol
TestAmerica Savannah Page 97 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-6-NS
Client Matrix: % Moisture: 20.4
680-56861-10
Solid
Date Sampled: 04/15/2010 1105
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/04/2010 1442
50
8270C Analysis Batch: 680-167473
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1015a.d
30.03 g
1.0 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
110000 U 110000520002,4-Dinitrophenol
21000 U 2100031002,4-Dinitrotoluene
21000 U 2100026002,6-Dinitrotoluene
21000 U 210001800Di-n-octyl phthalate
21000 U 2100010000Dinoseb
21000 U 2100075001,4-Dioxane
21000 U 210001100Disulfoton
21000 U 210001900Ethyl methanesulfonate
21000 U 210001400Ethyl Parathion
21000 U 210001800Famphur
21000 U 210002000Fluoranthene
21000 U 210002300Fluorene
21000 U 210002400Hexachlorobenzene
21000 U 210002300Hexachlorobutadiene
21000 U 210002600Hexachlorocyclopentadiene
21000 U 210001800Hexachloroethane
11000000 U 11000000820000Hexachlorophene
21000 U 210001800Hexachloropropene
21000 U 210001800Indeno[1,2,3-cd]pyrene
21000 U 210002100Isophorone
21000 U 210001500Isosafrole
4200000 U 420000052000Methapyrilene
21000 U 2100026003-Methylcholanthrene
21000 U 210001100Methyl methanesulfonate
21000 U 2100024002-Methylnaphthalene
21000 U 210001600Methyl parathion
21000 U 2100017002-Methylphenol
21000 U 2100027003 & 4 Methylphenol
21000 U 210001900Naphthalene
21000 U 2100011001,4-Naphthoquinone
21000 U 2100041001-Naphthylamine
21000 U 2100021002-Naphthylamine
110000 U 11000028002-Nitroaniline
110000 U 11000029003-Nitroaniline
110000 U 11000031004-Nitroaniline
21000 U 210001600Nitrobenzene
21000 U 2100026002-Nitrophenol
110000 U 110000210004-Nitrophenol
210000 U 210000520004-Nitroquinoline-1-oxide
21000 U 210001600N-Nitro-o-toluidine
21000 U 210001800N-Nitrosodiethylamine
21000 U 210007500N-Nitrosodimethylamine
21000 U 210001500N-Nitrosodi-n-butylamine
21000 U 210002000N-Nitrosodi-n-propylamine
21000 U 210002100N-Nitrosodiphenylamine
21000 U 210001600N-Nitrosomethylethylamine
TestAmerica Savannah Page 98 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-6-NS
Client Matrix: % Moisture: 20.4
680-56861-10
Solid
Date Sampled: 04/15/2010 1105
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/04/2010 1442
50
8270C Analysis Batch: 680-167473
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1015a.d
30.03 g
1.0 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
21000 U 210001700N-Nitrosomorpholine
21000 U 210001300N-Nitrosopiperidine
21000 U 210001100N-Nitrosopyrrolidine
21000 U 210002500o,o',o''-Triethylphosphorothioate
21000 U 210001200p-Dimethylamino azobenzene
21000 U 210001600Pentachlorobenzene
21000 U 210001300Pentachloronitrobenzene
110000 U 11000021000Pentachlorophenol
21000 U 210002100Phenacetin
21000 U 210001700Phenanthrene
21000 U 210002100Phenol
21000 U 210001400Phorate
21000 U 2100011002-Picoline
110000 U 11000052000p-Phenylene diamine
21000 U 210001500Pronamide
21000 U 210001700Pyrene
21000 U 210001800Pyridine
21000 U 210001500Safrole, Total
21000 U 210001300Sulfotepp
21000 U 2100019001,2,4,5-Tetrachlorobenzene
21000 U 2100014002,3,4,6-Tetrachlorophenol
21000 U 210001400Thionazin
21000 U 2100022002-Toluidine
21000 U 2100019001,2,4-Trichlorobenzene
21000 U 2100022002,4,5-Trichlorophenol
21000 U 2100018002,4,6-Trichlorophenol
21000 U 21000110001,3,5-Trinitrobenzene
Surrogate %Rec Acceptance LimitsQualifier
0 34 - 130D2,4,6-Tribromophenol
0 34 - 130D2-Fluorobiphenyl
0 30 - 130D2-Fluorophenol
0 39 - 130DTerphenyl-d14
0 30 - 130DPhenol-d5
0 27 - 130DNitrobenzene-d5
TestAmerica Savannah Page 99 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-6-NS
Client Matrix: % Moisture: 20.4
680-56861-10
Solid
Date Sampled: 04/15/2010 1105
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/10/2010 1250
200
8270C Analysis Batch: 680-167967
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1161.d
30.03 g
1.0 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
830000 830008500Diphenyl ether
Surrogate %Rec Acceptance LimitsQualifier
0 34 - 130D2,4,6-Tribromophenol
0 34 - 130D2-Fluorobiphenyl
0 30 - 130D2-Fluorophenol
0 39 - 130DTerphenyl-d14
0 30 - 130DPhenol-d5
0 27 - 130DNitrobenzene-d5
TestAmerica Savannah Page 100 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-6-LS
Client Matrix: % Moisture: 59.4
680-56861-11
Solid
Date Sampled: 04/15/2010 1110
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/04/2010 1021
10
8270C Analysis Batch: 680-167473
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1016.d
30.05 g
20 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
160000 U 16000020000Acenaphthene
160000 U 16000018000Acenaphthylene
160000 U 16000014000Acetophenone
160000 U 160000140002-Acetylaminofluorene
33000000 U 330000001300000alpha,alpha-Dimethyl phenethylamine
160000 U 160000180004-Aminobiphenyl
320000 U 32000017000Aniline
160000 U 16000012000Anthracene
160000 U 16000028000Aramite, Total
160000 U 16000013000Benzo[a]anthracene
160000 U 16000026000Benzo[a]pyrene
160000 U 16000019000Benzo[b]fluoranthene
160000 U 16000011000Benzo[g,h,i]perylene
160000 U 16000032000Benzo[k]fluoranthene
160000 U 16000016000Benzyl alcohol
800000 160000140001,1'-Biphenyl
160000 U 16000019000Bis(2-chloroethoxy)methane
160000 U 16000022000Bis(2-chloroethyl)ether
160000 U 16000015000bis(chloroisopropyl) ether
160000 U 16000016000Bis(2-ethylhexyl) phthalate
160000 U 160000180004-Bromophenyl phenyl ether
160000 U 16000013000Butyl benzyl phthalate
320000 U 320000260004-Chloroaniline
160000 U 160000170004-Chloro-3-methylphenol
160000 U 160000190002-Chloronaphthalene
160000 U 160000200002-Chlorophenol
160000 U 160000180004-Chlorophenyl phenyl ether
160000 U 16000010000Chrysene
160000 U 16000084000Diallate
160000 U 16000012000Dibenz(a,h)anthracene
160000 U 16000016000Dibenzofuran
160000 U 160000180001,2-Dichlorobenzene
160000 U 160000170001,3-Dichlorobenzene
160000 U 160000170001,4-Dichlorobenzene
320000 U 320000140003,3'-Dichlorobenzidine
160000 U 160000170002,4-Dichlorophenol
160000 U 160000130002,6-Dichlorophenol
160000 U 16000017000Diethyl phthalate
160000 U 16000012000Dimethoate
160000 U 16000084007,12-Dimethylbenz(a)anthracene
840000 U 8400004100003,3'-Dimethylbenzidine
160000 U 160000220002,4-Dimethylphenol
160000 U 16000017000Dimethyl phthalate
160000 U 16000015000Di-n-butyl phthalate
160000 U 160000120001,3-Dinitrobenzene
840000 U 840000840004,6-Dinitro-2-methylphenol
TestAmerica Savannah Page 101 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-6-LS
Client Matrix: % Moisture: 59.4
680-56861-11
Solid
Date Sampled: 04/15/2010 1110
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/04/2010 1021
10
8270C Analysis Batch: 680-167473
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1016.d
30.05 g
20 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
840000 U 8400004100002,4-Dinitrophenol
160000 U 160000240002,4-Dinitrotoluene
160000 U 160000210002,6-Dinitrotoluene
160000 U 16000014000Di-n-octyl phthalate
160000 U 16000079000Dinoseb
160000 U 160000590001,4-Dioxane
160000 U 1600008400Disulfoton
160000 U 16000015000Ethyl methanesulfonate
160000 U 16000011000Ethyl Parathion
160000 U 16000014000Famphur
160000 U 16000016000Fluoranthene
160000 U 16000018000Fluorene
160000 U 16000019000Hexachlorobenzene
160000 U 16000018000Hexachlorobutadiene
160000 U 16000020000Hexachlorocyclopentadiene
160000 U 16000014000Hexachloroethane
84000000 U 840000006400000Hexachlorophene
160000 U 16000014000Hexachloropropene
160000 U 16000014000Indeno[1,2,3-cd]pyrene
160000 U 16000016000Isophorone
160000 U 16000012000Isosafrole
33000000 U 33000000410000Methapyrilene
160000 U 160000200003-Methylcholanthrene
160000 U 1600008400Methyl methanesulfonate
160000 U 160000190002-Methylnaphthalene
160000 U 16000013000Methyl parathion
160000 U 160000130002-Methylphenol
160000 U 160000210003 & 4 Methylphenol
160000 U 16000015000Naphthalene
160000 U 16000084001,4-Naphthoquinone
160000 U 160000320001-Naphthylamine
160000 U 160000170002-Naphthylamine
840000 U 840000220002-Nitroaniline
840000 U 840000230003-Nitroaniline
840000 U 840000240004-Nitroaniline
160000 U 16000013000Nitrobenzene
160000 U 160000200002-Nitrophenol
840000 U 8400001600004-Nitrophenol
1600000 U 16000004100004-Nitroquinoline-1-oxide
160000 U 16000013000N-Nitro-o-toluidine
160000 U 16000014000N-Nitrosodiethylamine
160000 U 16000059000N-Nitrosodimethylamine
160000 U 16000012000N-Nitrosodi-n-butylamine
160000 U 16000016000N-Nitrosodi-n-propylamine
160000 U 16000016000N-Nitrosodiphenylamine
160000 U 16000012000N-Nitrosomethylethylamine
TestAmerica Savannah Page 102 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-6-LS
Client Matrix: % Moisture: 59.4
680-56861-11
Solid
Date Sampled: 04/15/2010 1110
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/04/2010 1021
10
8270C Analysis Batch: 680-167473
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1016.d
30.05 g
20 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
160000 U 16000013000N-Nitrosomorpholine
160000 U 16000010000N-Nitrosopiperidine
160000 U 1600008800N-Nitrosopyrrolidine
160000 U 16000020000o,o',o''-Triethylphosphorothioate
160000 U 1600009300p-Dimethylamino azobenzene
160000 U 16000012000Pentachlorobenzene
160000 U 16000010000Pentachloronitrobenzene
840000 U 840000160000Pentachlorophenol
160000 U 16000016000Phenacetin
160000 U 16000013000Phenanthrene
160000 U 16000017000Phenol
160000 U 16000011000Phorate
160000 U 16000084002-Picoline
840000 U 840000410000p-Phenylene diamine
160000 U 16000012000Pronamide
160000 U 16000013000Pyrene
160000 U 16000014000Pyridine
160000 U 16000012000Safrole, Total
160000 U 1600009800Sulfotepp
160000 U 160000150001,2,4,5-Tetrachlorobenzene
160000 U 160000110002,3,4,6-Tetrachlorophenol
160000 U 16000011000Thionazin
160000 U 160000170002-Toluidine
160000 U 160000150001,2,4-Trichlorobenzene
160000 U 160000170002,4,5-Trichlorophenol
160000 U 160000140002,4,6-Trichlorophenol
160000 U 160000840001,3,5-Trinitrobenzene
2500000 16000017000Diphenyl ether
Surrogate %Rec Acceptance LimitsQualifier
0 34 - 130D2,4,6-Tribromophenol
0 34 - 130D2-Fluorobiphenyl
0 30 - 130D2-Fluorophenol
0 39 - 130DTerphenyl-d14
0 30 - 130DPhenol-d5
0 27 - 130DNitrobenzene-d5
TestAmerica Savannah Page 103 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-5-US
Client Matrix: % Moisture: 82.7
680-56861-12
Solid
Date Sampled: 04/15/2010 1145
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/04/2010 1045
10
8270C Analysis Batch: 680-167473
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1017.d
30.18 g
10 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
190000 U 19000024000Acenaphthene
190000 U 19000021000Acenaphthylene
190000 U 19000016000Acetophenone
190000 U 190000160002-Acetylaminofluorene
39000000 U 390000001600000alpha,alpha-Dimethyl phenethylamine
190000 U 190000210004-Aminobiphenyl
380000 U 38000020000Aniline
190000 U 19000014000Anthracene
190000 U 19000033000Aramite, Total
190000 U 19000016000Benzo[a]anthracene
190000 U 19000030000Benzo[a]pyrene
190000 U 19000022000Benzo[b]fluoranthene
190000 U 19000013000Benzo[g,h,i]perylene
190000 U 19000037000Benzo[k]fluoranthene
190000 U 19000019000Benzyl alcohol
160000 J 190000160001,1'-Biphenyl
190000 U 19000022000Bis(2-chloroethoxy)methane
190000 U 19000026000Bis(2-chloroethyl)ether
190000 U 19000017000bis(chloroisopropyl) ether
190000 U 19000019000Bis(2-ethylhexyl) phthalate
190000 U 190000210004-Bromophenyl phenyl ether
190000 U 19000015000Butyl benzyl phthalate
380000 U 380000300004-Chloroaniline
190000 U 190000200004-Chloro-3-methylphenol
190000 U 190000220002-Chloronaphthalene
190000 U 190000230002-Chlorophenol
190000 U 190000210004-Chlorophenyl phenyl ether
190000 U 19000012000Chrysene
190000 U 19000098000Diallate
190000 U 19000014000Dibenz(a,h)anthracene
190000 U 19000019000Dibenzofuran
190000 U 190000210001,2-Dichlorobenzene
190000 U 190000200001,3-Dichlorobenzene
190000 U 190000200001,4-Dichlorobenzene
380000 U 380000160003,3'-Dichlorobenzidine
190000 U 190000200002,4-Dichlorophenol
190000 U 190000160002,6-Dichlorophenol
190000 U 19000020000Diethyl phthalate
190000 U 19000014000Dimethoate
190000 U 19000098007,12-Dimethylbenz(a)anthracene
980000 U 9800004800003,3'-Dimethylbenzidine
190000 U 190000250002,4-Dimethylphenol
190000 U 19000020000Dimethyl phthalate
190000 U 19000017000Di-n-butyl phthalate
190000 U 190000140001,3-Dinitrobenzene
980000 U 980000980004,6-Dinitro-2-methylphenol
TestAmerica Savannah Page 104 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-5-US
Client Matrix: % Moisture: 82.7
680-56861-12
Solid
Date Sampled: 04/15/2010 1145
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/04/2010 1045
10
8270C Analysis Batch: 680-167473
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1017.d
30.18 g
10 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
980000 U 9800004800002,4-Dinitrophenol
190000 U 190000280002,4-Dinitrotoluene
190000 U 190000240002,6-Dinitrotoluene
190000 U 19000017000Di-n-octyl phthalate
190000 U 19000092000Dinoseb
190000 U 190000690001,4-Dioxane
190000 U 1900009800Disulfoton
190000 U 19000018000Ethyl methanesulfonate
190000 U 19000013000Ethyl Parathion
190000 U 19000017000Famphur
190000 U 19000018000Fluoranthene
190000 U 19000021000Fluorene
190000 U 19000022000Hexachlorobenzene
190000 U 19000021000Hexachlorobutadiene
190000 U 19000024000Hexachlorocyclopentadiene
190000 U 19000016000Hexachloroethane
98000000 U 980000007500000Hexachlorophene
190000 U 19000017000Hexachloropropene
190000 U 19000016000Indeno[1,2,3-cd]pyrene
190000 U 19000019000Isophorone
190000 U 19000014000Isosafrole
39000000 U 39000000480000Methapyrilene
190000 U 190000240003-Methylcholanthrene
190000 U 1900009800Methyl methanesulfonate
190000 U 190000220002-Methylnaphthalene
190000 U 19000015000Methyl parathion
190000 U 190000160002-Methylphenol
190000 U 190000250003 & 4 Methylphenol
190000 U 19000017000Naphthalene
190000 U 19000098001,4-Naphthoquinone
190000 U 190000380001-Naphthylamine
190000 U 190000200002-Naphthylamine
980000 U 980000260002-Nitroaniline
980000 U 980000260003-Nitroaniline
980000 U 980000280004-Nitroaniline
190000 U 19000015000Nitrobenzene
190000 U 190000240002-Nitrophenol
980000 U 9800001900004-Nitrophenol
1900000 U 19000004800004-Nitroquinoline-1-oxide
190000 U 19000015000N-Nitro-o-toluidine
190000 U 19000016000N-Nitrosodiethylamine
190000 U 19000069000N-Nitrosodimethylamine
190000 U 19000014000N-Nitrosodi-n-butylamine
190000 U 19000018000N-Nitrosodi-n-propylamine
190000 U 19000019000N-Nitrosodiphenylamine
190000 U 19000014000N-Nitrosomethylethylamine
TestAmerica Savannah Page 105 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-5-US
Client Matrix: % Moisture: 82.7
680-56861-12
Solid
Date Sampled: 04/15/2010 1145
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/04/2010 1045
10
8270C Analysis Batch: 680-167473
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1017.d
30.18 g
10 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
190000 U 19000016000N-Nitrosomorpholine
190000 U 19000012000N-Nitrosopiperidine
190000 U 19000010000N-Nitrosopyrrolidine
190000 U 19000023000o,o',o''-Triethylphosphorothioate
190000 U 19000011000p-Dimethylamino azobenzene
190000 U 19000014000Pentachlorobenzene
190000 U 19000012000Pentachloronitrobenzene
980000 U 980000190000Pentachlorophenol
190000 U 19000019000Phenacetin
190000 U 19000016000Phenanthrene
190000 U 19000020000Phenol
190000 U 19000013000Phorate
190000 U 19000098002-Picoline
980000 U 980000480000p-Phenylene diamine
190000 U 19000014000Pronamide
190000 U 19000016000Pyrene
190000 U 19000017000Pyridine
190000 U 19000014000Safrole, Total
190000 U 19000012000Sulfotepp
190000 U 190000180001,2,4,5-Tetrachlorobenzene
190000 U 190000130002,3,4,6-Tetrachlorophenol
190000 U 19000013000Thionazin
190000 U 190000200002-Toluidine
190000 U 190000180001,2,4-Trichlorobenzene
190000 U 190000200002,4,5-Trichlorophenol
190000 U 190000170002,4,6-Trichlorophenol
190000 U 190000980001,3,5-Trinitrobenzene
530000 19000020000Diphenyl ether
Surrogate %Rec Acceptance LimitsQualifier
0 34 - 130D2,4,6-Tribromophenol
0 34 - 130D2-Fluorobiphenyl
0 30 - 130D2-Fluorophenol
0 39 - 130DTerphenyl-d14
0 30 - 130DPhenol-d5
0 27 - 130DNitrobenzene-d5
TestAmerica Savannah Page 106 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-6-US
Client Matrix: % Moisture: 82.7
680-56861-13
Solid
Date Sampled: 04/15/2010 1415
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/04/2010 1108
10
8270C Analysis Batch: 680-167473
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1018.d
30.07 g
10 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
190000 U 19000024000Acenaphthene
190000 U 19000021000Acenaphthylene
190000 U 19000016000Acetophenone
190000 U 190000160002-Acetylaminofluorene
39000000 U 390000001600000alpha,alpha-Dimethyl phenethylamine
190000 U 190000210004-Aminobiphenyl
380000 U 38000020000Aniline
190000 U 19000014000Anthracene
190000 U 19000033000Aramite, Total
190000 U 19000016000Benzo[a]anthracene
190000 U 19000030000Benzo[a]pyrene
190000 U 19000022000Benzo[b]fluoranthene
190000 U 19000013000Benzo[g,h,i]perylene
190000 U 19000038000Benzo[k]fluoranthene
190000 U 19000019000Benzyl alcohol
140000 J 190000160001,1'-Biphenyl
190000 U 19000023000Bis(2-chloroethoxy)methane
190000 U 19000026000Bis(2-chloroethyl)ether
190000 U 19000017000bis(chloroisopropyl) ether
190000 U 19000019000Bis(2-ethylhexyl) phthalate
190000 U 190000210004-Bromophenyl phenyl ether
190000 U 19000015000Butyl benzyl phthalate
380000 U 380000300004-Chloroaniline
190000 U 190000200004-Chloro-3-methylphenol
190000 U 190000230002-Chloronaphthalene
190000 U 190000230002-Chlorophenol
190000 U 190000210004-Chlorophenyl phenyl ether
190000 U 19000012000Chrysene
190000 U 19000098000Diallate
190000 U 19000014000Dibenz(a,h)anthracene
190000 U 19000019000Dibenzofuran
190000 U 190000210001,2-Dichlorobenzene
190000 U 190000200001,3-Dichlorobenzene
190000 U 190000200001,4-Dichlorobenzene
380000 U 380000160003,3'-Dichlorobenzidine
190000 U 190000200002,4-Dichlorophenol
190000 U 190000160002,6-Dichlorophenol
190000 U 19000020000Diethyl phthalate
190000 U 19000014000Dimethoate
190000 U 19000098007,12-Dimethylbenz(a)anthracene
980000 U 9800004800003,3'-Dimethylbenzidine
190000 U 190000250002,4-Dimethylphenol
190000 U 19000020000Dimethyl phthalate
190000 U 19000017000Di-n-butyl phthalate
190000 U 190000140001,3-Dinitrobenzene
980000 U 980000980004,6-Dinitro-2-methylphenol
TestAmerica Savannah Page 107 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-6-US
Client Matrix: % Moisture: 82.7
680-56861-13
Solid
Date Sampled: 04/15/2010 1415
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/04/2010 1108
10
8270C Analysis Batch: 680-167473
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1018.d
30.07 g
10 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
980000 U 9800004800002,4-Dinitrophenol
190000 U 190000280002,4-Dinitrotoluene
190000 U 190000240002,6-Dinitrotoluene
190000 U 19000017000Di-n-octyl phthalate
190000 U 19000092000Dinoseb
190000 U 190000690001,4-Dioxane
190000 U 1900009800Disulfoton
190000 U 19000018000Ethyl methanesulfonate
190000 U 19000013000Ethyl Parathion
190000 U 19000017000Famphur
190000 U 19000018000Fluoranthene
190000 U 19000021000Fluorene
190000 U 19000023000Hexachlorobenzene
190000 U 19000021000Hexachlorobutadiene
190000 U 19000024000Hexachlorocyclopentadiene
190000 U 19000016000Hexachloroethane
98000000 U 980000007500000Hexachlorophene
190000 U 19000017000Hexachloropropene
190000 U 19000016000Indeno[1,2,3-cd]pyrene
190000 U 19000019000Isophorone
190000 U 19000014000Isosafrole
39000000 U 39000000480000Methapyrilene
190000 U 190000240003-Methylcholanthrene
190000 U 1900009800Methyl methanesulfonate
190000 U 190000220002-Methylnaphthalene
190000 U 19000015000Methyl parathion
190000 U 190000160002-Methylphenol
190000 U 190000250003 & 4 Methylphenol
190000 U 19000017000Naphthalene
190000 U 19000098001,4-Naphthoquinone
190000 U 190000380001-Naphthylamine
190000 U 190000200002-Naphthylamine
980000 U 980000260002-Nitroaniline
980000 U 980000270003-Nitroaniline
980000 U 980000280004-Nitroaniline
190000 U 19000015000Nitrobenzene
190000 U 190000240002-Nitrophenol
980000 U 9800001900004-Nitrophenol
1900000 U 19000004800004-Nitroquinoline-1-oxide
190000 U 19000015000N-Nitro-o-toluidine
190000 U 19000016000N-Nitrosodiethylamine
190000 U 19000069000N-Nitrosodimethylamine
190000 U 19000014000N-Nitrosodi-n-butylamine
190000 U 19000018000N-Nitrosodi-n-propylamine
190000 U 19000019000N-Nitrosodiphenylamine
190000 U 19000014000N-Nitrosomethylethylamine
TestAmerica Savannah Page 108 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-6-US
Client Matrix: % Moisture: 82.7
680-56861-13
Solid
Date Sampled: 04/15/2010 1415
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/04/2010 1108
10
8270C Analysis Batch: 680-167473
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1018.d
30.07 g
10 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
190000 U 19000016000N-Nitrosomorpholine
190000 U 19000012000N-Nitrosopiperidine
190000 U 19000010000N-Nitrosopyrrolidine
190000 U 19000023000o,o',o''-Triethylphosphorothioate
190000 U 19000011000p-Dimethylamino azobenzene
190000 U 19000014000Pentachlorobenzene
190000 U 19000012000Pentachloronitrobenzene
980000 U 980000190000Pentachlorophenol
190000 U 19000019000Phenacetin
190000 U 19000016000Phenanthrene
190000 U 19000020000Phenol
190000 U 19000013000Phorate
190000 U 19000098002-Picoline
980000 U 980000480000p-Phenylene diamine
190000 U 19000014000Pronamide
190000 U 19000016000Pyrene
190000 U 19000017000Pyridine
190000 U 19000014000Safrole, Total
190000 U 19000012000Sulfotepp
190000 U 190000180001,2,4,5-Tetrachlorobenzene
190000 U 190000130002,3,4,6-Tetrachlorophenol
190000 U 19000013000Thionazin
190000 U 190000200002-Toluidine
190000 U 190000180001,2,4-Trichlorobenzene
190000 U 190000200002,4,5-Trichlorophenol
190000 U 190000170002,4,6-Trichlorophenol
190000 U 190000980001,3,5-Trinitrobenzene
400000 19000020000Diphenyl ether
Surrogate %Rec Acceptance LimitsQualifier
0 34 - 130D2,4,6-Tribromophenol
0 34 - 130D2-Fluorobiphenyl
0 30 - 130D2-Fluorophenol
0 39 - 130DTerphenyl-d14
0 30 - 130DPhenol-d5
0 27 - 130DNitrobenzene-d5
TestAmerica Savannah Page 109 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-7-NS
Client Matrix: % Moisture: 16.9
680-56861-14
Solid
Date Sampled: 04/15/2010 1505
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/04/2010 1132
10
8270C Analysis Batch: 680-167473
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1019.d
30.02 g
1.0 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
4000 U 4000490Acenaphthene
4000 U 4000430Acenaphthylene
4000 U 4000340Acetophenone
4000 U 40003402-Acetylaminofluorene
810000 U 81000032000alpha,alpha-Dimethyl phenethylamine
4000 U 40004504-Aminobiphenyl
7900 U 7900410Aniline
4000 U 4000300Anthracene
4000 U 4000690Aramite, Total
4000 U 4000320Benzo[a]anthracene
4000 U 4000630Benzo[a]pyrene
4000 U 4000460Benzo[b]fluoranthene
4000 U 4000260Benzo[g,h,i]perylene
4000 U 4000780Benzo[k]fluoranthene
4000 U 4000400Benzyl alcohol
18000 40003401,1'-Biphenyl
4000 U 4000470Bis(2-chloroethoxy)methane
4000 U 4000540Bis(2-chloroethyl)ether
4000 U 4000360bis(chloroisopropyl) ether
4000 U 4000400Bis(2-ethylhexyl) phthalate
4000 U 40004304-Bromophenyl phenyl ether
4000 U 4000310Butyl benzyl phthalate
7900 U 79006304-Chloroaniline
4000 U 40004204-Chloro-3-methylphenol
4000 U 40004702-Chloronaphthalene
4000 U 40004802-Chlorophenol
4000 U 40004504-Chlorophenyl phenyl ether
4000 U 4000250Chrysene
4000 U 40002000Diallate
4000 U 4000290Dibenz(a,h)anthracene
4000 U 4000400Dibenzofuran
4000 U 40004501,2-Dichlorobenzene
4000 U 40004101,3-Dichlorobenzene
4000 U 40004201,4-Dichlorobenzene
7900 U 79003403,3'-Dichlorobenzidine
4000 U 40004202,4-Dichlorophenol
4000 U 40003202,6-Dichlorophenol
4000 U 4000420Diethyl phthalate
4000 U 4000300Dimethoate
4000 U 40002007,12-Dimethylbenz(a)anthracene
20000 U 20000100003,3'-Dimethylbenzidine
4000 U 40005302,4-Dimethylphenol
4000 U 4000410Dimethyl phthalate
4000 U 4000360Di-n-butyl phthalate
4000 U 40002901,3-Dinitrobenzene
20000 U 2000020004,6-Dinitro-2-methylphenol
TestAmerica Savannah Page 110 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-7-NS
Client Matrix: % Moisture: 16.9
680-56861-14
Solid
Date Sampled: 04/15/2010 1505
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/04/2010 1132
10
8270C Analysis Batch: 680-167473
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1019.d
30.02 g
1.0 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
20000 U 20000100002,4-Dinitrophenol
4000 U 40005902,4-Dinitrotoluene
4000 U 40005102,6-Dinitrotoluene
4000 U 4000350Di-n-octyl phthalate
4000 U 40001900Dinoseb
4000 U 400014001,4-Dioxane
410 J 4000200Disulfoton
4000 U 4000370Ethyl methanesulfonate
4000 U 4000260Ethyl Parathion
4000 U 4000350Famphur
4000 U 4000380Fluoranthene
4000 U 4000430Fluorene
4000 U 4000470Hexachlorobenzene
4000 U 4000430Hexachlorobutadiene
4000 U 4000490Hexachlorocyclopentadiene
4000 U 4000340Hexachloroethane
2000000 U 2000000160000Hexachlorophene
4000 U 4000350Hexachloropropene
4000 U 4000340Indeno[1,2,3-cd]pyrene
4000 U 4000400Isophorone
4000 U 4000290Isosafrole
810000 U 81000010000Methapyrilene
4000 U 40004903-Methylcholanthrene
4000 U 4000200Methyl methanesulfonate
4000 U 40004602-Methylnaphthalene
4000 U 4000310Methyl parathion
4000 U 40003202-Methylphenol
530 J 40005203 & 4 Methylphenol
4000 U 4000360Naphthalene
4000 U 40002001,4-Naphthoquinone
4000 U 40007901-Naphthylamine
4000 U 40004102-Naphthylamine
20000 U 200005402-Nitroaniline
20000 U 200005503-Nitroaniline
20000 U 200005904-Nitroaniline
4000 U 4000310Nitrobenzene
4000 U 40004902-Nitrophenol
20000 U 2000040004-Nitrophenol
40000 U 40000100004-Nitroquinoline-1-oxide
4000 U 4000310N-Nitro-o-toluidine
4000 U 4000340N-Nitrosodiethylamine
4000 U 40001400N-Nitrosodimethylamine
4000 U 4000290N-Nitrosodi-n-butylamine
4000 U 4000380N-Nitrosodi-n-propylamine
4000 U 4000400N-Nitrosodiphenylamine
4000 U 4000300N-Nitrosomethylethylamine
TestAmerica Savannah Page 111 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-7-NS
Client Matrix: % Moisture: 16.9
680-56861-14
Solid
Date Sampled: 04/15/2010 1505
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/04/2010 1132
10
8270C Analysis Batch: 680-167473
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1019.d
30.02 g
1.0 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
4000 U 4000320N-Nitrosomorpholine
4000 U 4000250N-Nitrosopiperidine
4000 U 4000220N-Nitrosopyrrolidine
4000 U 4000480o,o',o''-Triethylphosphorothioate
4000 U 4000230p-Dimethylamino azobenzene
4000 U 4000300Pentachlorobenzene
4000 U 4000250Pentachloronitrobenzene
20000 U 200004000Pentachlorophenol
4000 U 4000400Phenacetin
4000 U 4000320Phenanthrene
4000 U 4000410Phenol
4000 U 4000260Phorate
4000 U 40002002-Picoline
20000 U 2000010000p-Phenylene diamine
4000 U 4000290Pronamide
490 J 4000320Pyrene
4000 U 4000350Pyridine
4000 U 4000290Safrole, Total
4000 U 4000240Sulfotepp
4000 U 40003701,2,4,5-Tetrachlorobenzene
4000 U 40002602,3,4,6-Tetrachlorophenol
4000 U 4000280Thionazin
4000 U 40004202-Toluidine
4000 U 40003701,2,4-Trichlorobenzene
4000 U 40004202,4,5-Trichlorophenol
4000 U 40003502,4,6-Trichlorophenol
4000 U 400020001,3,5-Trinitrobenzene
59000 4000410Diphenyl ether
Surrogate %Rec Acceptance LimitsQualifier
0 34 - 130D2,4,6-Tribromophenol
0 34 - 130D2-Fluorobiphenyl
0 30 - 130D2-Fluorophenol
0 39 - 130DTerphenyl-d14
0 30 - 130DPhenol-d5
0 27 - 130DNitrobenzene-d5
TestAmerica Savannah Page 112 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-7-LS
Client Matrix: % Moisture: 70.7
680-56861-15
Solid
Date Sampled: 04/15/2010 1520
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/04/2010 1156
10
8270C Analysis Batch: 680-167473
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1020.d
30.15 g
10 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
110000 U 11000014000Acenaphthene
110000 U 11000012000Acenaphthylene
110000 U 1100009500Acetophenone
110000 U 11000095002-Acetylaminofluorene
23000000 U 23000000920000alpha,alpha-Dimethyl phenethylamine
110000 U 110000130004-Aminobiphenyl
220000 U 22000012000Aniline
110000 U 1100008500Anthracene
110000 U 11000019000Aramite, Total
110000 U 1100009200Benzo[a]anthracene
110000 U 11000018000Benzo[a]pyrene
110000 U 11000013000Benzo[b]fluoranthene
110000 U 1100007500Benzo[g,h,i]perylene
110000 U 11000022000Benzo[k]fluoranthene
110000 U 11000011000Benzyl alcohol
620000 11000095001,1'-Biphenyl
110000 U 11000013000Bis(2-chloroethoxy)methane
110000 U 11000015000Bis(2-chloroethyl)ether
110000 U 11000010000bis(chloroisopropyl) ether
110000 U 11000011000Bis(2-ethylhexyl) phthalate
110000 U 110000120004-Bromophenyl phenyl ether
110000 U 1100008800Butyl benzyl phthalate
220000 U 220000180004-Chloroaniline
110000 U 110000120004-Chloro-3-methylphenol
110000 U 110000130002-Chloronaphthalene
110000 U 110000140002-Chlorophenol
110000 U 110000130004-Chlorophenyl phenyl ether
110000 U 1100007100Chrysene
110000 U 11000058000Diallate
110000 U 1100008100Dibenz(a,h)anthracene
110000 U 11000011000Dibenzofuran
110000 U 110000130001,2-Dichlorobenzene
110000 U 110000120001,3-Dichlorobenzene
110000 U 110000120001,4-Dichlorobenzene
220000 U 22000095003,3'-Dichlorobenzidine
110000 U 110000120002,4-Dichlorophenol
110000 U 11000092002,6-Dichlorophenol
110000 U 11000012000Diethyl phthalate
110000 U 1100008500Dimethoate
110000 U 11000058007,12-Dimethylbenz(a)anthracene
580000 U 5800002800003,3'-Dimethylbenzidine
110000 U 110000150002,4-Dimethylphenol
110000 U 11000012000Dimethyl phthalate
110000 U 11000010000Di-n-butyl phthalate
110000 U 11000081001,3-Dinitrobenzene
580000 U 580000580004,6-Dinitro-2-methylphenol
TestAmerica Savannah Page 113 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-7-LS
Client Matrix: % Moisture: 70.7
680-56861-15
Solid
Date Sampled: 04/15/2010 1520
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/04/2010 1156
10
8270C Analysis Batch: 680-167473
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1020.d
30.15 g
10 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
580000 U 5800002800002,4-Dinitrophenol
110000 U 110000170002,4-Dinitrotoluene
110000 U 110000140002,6-Dinitrotoluene
110000 U 1100009800Di-n-octyl phthalate
110000 U 11000054000Dinoseb
110000 U 110000410001,4-Dioxane
110000 U 1100005800Disulfoton
110000 U 11000011000Ethyl methanesulfonate
110000 U 1100007500Ethyl Parathion
110000 U 1100009800Famphur
110000 U 11000011000Fluoranthene
110000 U 11000012000Fluorene
110000 U 11000013000Hexachlorobenzene
110000 U 11000012000Hexachlorobutadiene
110000 U 11000014000Hexachlorocyclopentadiene
110000 U 1100009500Hexachloroethane
58000000 U 580000004400000Hexachlorophene
110000 U 1100009800Hexachloropropene
110000 U 1100009500Indeno[1,2,3-cd]pyrene
110000 U 11000011000Isophorone
110000 U 1100008100Isosafrole
23000000 U 23000000280000Methapyrilene
110000 U 110000140003-Methylcholanthrene
110000 U 1100005800Methyl methanesulfonate
110000 U 110000130002-Methylnaphthalene
110000 U 1100008800Methyl parathion
110000 U 11000092002-Methylphenol
25000 J 110000150003 & 4 Methylphenol
110000 U 11000010000Naphthalene
110000 U 11000058001,4-Naphthoquinone
110000 U 110000220001-Naphthylamine
110000 U 110000120002-Naphthylamine
580000 U 580000150002-Nitroaniline
580000 U 580000160003-Nitroaniline
580000 U 580000170004-Nitroaniline
110000 U 1100008800Nitrobenzene
110000 U 110000140002-Nitrophenol
580000 U 5800001100004-Nitrophenol
1100000 U 11000002800004-Nitroquinoline-1-oxide
110000 U 1100008800N-Nitro-o-toluidine
110000 U 1100009500N-Nitrosodiethylamine
110000 U 11000041000N-Nitrosodimethylamine
110000 U 1100008100N-Nitrosodi-n-butylamine
110000 U 11000011000N-Nitrosodi-n-propylamine
110000 U 11000011000N-Nitrosodiphenylamine
110000 U 1100008500N-Nitrosomethylethylamine
TestAmerica Savannah Page 114 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-7-LS
Client Matrix: % Moisture: 70.7
680-56861-15
Solid
Date Sampled: 04/15/2010 1520
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/04/2010 1156
10
8270C Analysis Batch: 680-167473
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1020.d
30.15 g
10 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
110000 U 1100009200N-Nitrosomorpholine
110000 U 1100007100N-Nitrosopiperidine
110000 U 1100006100N-Nitrosopyrrolidine
110000 U 11000014000o,o',o''-Triethylphosphorothioate
110000 U 1100006500p-Dimethylamino azobenzene
110000 U 1100008500Pentachlorobenzene
110000 U 1100007100Pentachloronitrobenzene
580000 U 580000110000Pentachlorophenol
110000 U 11000011000Phenacetin
110000 U 1100009200Phenanthrene
110000 U 11000012000Phenol
110000 U 1100007500Phorate
110000 U 11000058002-Picoline
580000 U 580000280000p-Phenylene diamine
110000 U 1100008100Pronamide
110000 U 1100009200Pyrene
110000 U 1100009800Pyridine
110000 U 1100008100Safrole, Total
110000 U 1100006800Sulfotepp
110000 U 110000110001,2,4,5-Tetrachlorobenzene
110000 U 11000075002,3,4,6-Tetrachlorophenol
110000 U 1100007800Thionazin
110000 U 110000120002-Toluidine
110000 U 110000110001,2,4-Trichlorobenzene
110000 U 110000120002,4,5-Trichlorophenol
110000 U 11000098002,4,6-Trichlorophenol
110000 U 110000580001,3,5-Trinitrobenzene
2100000 11000012000Diphenyl ether
Surrogate %Rec Acceptance LimitsQualifier
0 34 - 130D2,4,6-Tribromophenol
0 34 - 130D2-Fluorobiphenyl
0 30 - 130D2-Fluorophenol
0 39 - 130DTerphenyl-d14
0 30 - 130DPhenol-d5
0 27 - 130DNitrobenzene-d5
TestAmerica Savannah Page 115 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-7-US
Client Matrix: % Moisture: 73.7
680-56861-16
Solid
Date Sampled: 04/15/2010 1525
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/04/2010 1219
10
8270C Analysis Batch: 680-167473
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1021.d
30.02 g
15 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
190000 U 19000023000Acenaphthene
190000 U 19000021000Acenaphthylene
190000 U 19000016000Acetophenone
190000 U 190000160002-Acetylaminofluorene
38000000 U 380000001500000alpha,alpha-Dimethyl phenethylamine
190000 U 190000210004-Aminobiphenyl
380000 U 38000019000Aniline
190000 U 19000014000Anthracene
190000 U 19000033000Aramite, Total
190000 U 19000015000Benzo[a]anthracene
190000 U 19000030000Benzo[a]pyrene
190000 U 19000022000Benzo[b]fluoranthene
190000 U 19000013000Benzo[g,h,i]perylene
190000 U 19000037000Benzo[k]fluoranthene
190000 U 19000019000Benzyl alcohol
230000 190000160001,1'-Biphenyl
190000 U 19000022000Bis(2-chloroethoxy)methane
190000 U 19000026000Bis(2-chloroethyl)ether
190000 U 19000017000bis(chloroisopropyl) ether
190000 U 19000019000Bis(2-ethylhexyl) phthalate
190000 U 190000210004-Bromophenyl phenyl ether
190000 U 19000015000Butyl benzyl phthalate
380000 U 380000300004-Chloroaniline
190000 U 190000200004-Chloro-3-methylphenol
190000 U 190000220002-Chloronaphthalene
190000 U 190000230002-Chlorophenol
190000 U 190000210004-Chlorophenyl phenyl ether
190000 U 19000012000Chrysene
190000 U 19000097000Diallate
190000 U 19000014000Dibenz(a,h)anthracene
190000 U 19000019000Dibenzofuran
190000 U 190000210001,2-Dichlorobenzene
190000 U 190000190001,3-Dichlorobenzene
190000 U 190000200001,4-Dichlorobenzene
380000 U 380000160003,3'-Dichlorobenzidine
190000 U 190000200002,4-Dichlorophenol
190000 U 190000150002,6-Dichlorophenol
190000 U 19000020000Diethyl phthalate
190000 U 19000014000Dimethoate
190000 U 19000097007,12-Dimethylbenz(a)anthracene
970000 U 9700004800003,3'-Dimethylbenzidine
190000 U 190000250002,4-Dimethylphenol
190000 U 19000019000Dimethyl phthalate
190000 U 19000017000Di-n-butyl phthalate
190000 U 190000140001,3-Dinitrobenzene
970000 U 970000970004,6-Dinitro-2-methylphenol
TestAmerica Savannah Page 116 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-7-US
Client Matrix: % Moisture: 73.7
680-56861-16
Solid
Date Sampled: 04/15/2010 1525
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/04/2010 1219
10
8270C Analysis Batch: 680-167473
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1021.d
30.02 g
15 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
970000 U 9700004700002,4-Dinitrophenol
190000 U 190000280002,4-Dinitrotoluene
190000 U 190000240002,6-Dinitrotoluene
190000 U 19000017000Di-n-octyl phthalate
190000 U 19000091000Dinoseb
190000 U 190000680001,4-Dioxane
190000 U 1900009700Disulfoton
190000 U 19000018000Ethyl methanesulfonate
190000 U 19000013000Ethyl Parathion
190000 U 19000017000Famphur
190000 U 19000018000Fluoranthene
190000 U 19000021000Fluorene
190000 U 19000022000Hexachlorobenzene
190000 U 19000021000Hexachlorobutadiene
190000 U 19000023000Hexachlorocyclopentadiene
190000 U 19000016000Hexachloroethane
97000000 U 970000007400000Hexachlorophene
190000 U 19000017000Hexachloropropene
190000 U 19000016000Indeno[1,2,3-cd]pyrene
190000 U 19000019000Isophorone
190000 U 19000014000Isosafrole
38000000 U 38000000470000Methapyrilene
190000 U 190000230003-Methylcholanthrene
190000 U 1900009700Methyl methanesulfonate
190000 U 190000220002-Methylnaphthalene
190000 U 19000015000Methyl parathion
190000 U 190000150002-Methylphenol
190000 U 190000250003 & 4 Methylphenol
190000 U 19000017000Naphthalene
190000 U 19000097001,4-Naphthoquinone
190000 U 190000380001-Naphthylamine
190000 U 190000190002-Naphthylamine
970000 U 970000260002-Nitroaniline
970000 U 970000260003-Nitroaniline
970000 U 970000280004-Nitroaniline
190000 U 19000015000Nitrobenzene
190000 U 190000230002-Nitrophenol
970000 U 9700001900004-Nitrophenol
1900000 U 19000004700004-Nitroquinoline-1-oxide
190000 U 19000015000N-Nitro-o-toluidine
190000 U 19000016000N-Nitrosodiethylamine
190000 U 19000068000N-Nitrosodimethylamine
190000 U 19000014000N-Nitrosodi-n-butylamine
190000 U 19000018000N-Nitrosodi-n-propylamine
190000 U 19000019000N-Nitrosodiphenylamine
190000 U 19000014000N-Nitrosomethylethylamine
TestAmerica Savannah Page 117 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-7-US
Client Matrix: % Moisture: 73.7
680-56861-16
Solid
Date Sampled: 04/15/2010 1525
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/04/2010 1219
10
8270C Analysis Batch: 680-167473
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1021.d
30.02 g
15 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
190000 U 19000015000N-Nitrosomorpholine
190000 U 19000012000N-Nitrosopiperidine
190000 U 19000010000N-Nitrosopyrrolidine
190000 U 19000023000o,o',o''-Triethylphosphorothioate
190000 U 19000011000p-Dimethylamino azobenzene
190000 U 19000014000Pentachlorobenzene
190000 U 19000012000Pentachloronitrobenzene
970000 U 970000190000Pentachlorophenol
190000 U 19000019000Phenacetin
190000 U 19000015000Phenanthrene
190000 U 19000019000Phenol
190000 U 19000013000Phorate
190000 U 19000097002-Picoline
970000 U 970000480000p-Phenylene diamine
190000 U 19000014000Pronamide
190000 U 19000015000Pyrene
190000 U 19000017000Pyridine
190000 U 19000014000Safrole, Total
190000 U 19000011000Sulfotepp
190000 U 190000180001,2,4,5-Tetrachlorobenzene
190000 U 190000130002,3,4,6-Tetrachlorophenol
190000 U 19000013000Thionazin
190000 U 190000200002-Toluidine
190000 U 190000180001,2,4-Trichlorobenzene
190000 U 190000200002,4,5-Trichlorophenol
190000 U 190000170002,4,6-Trichlorophenol
190000 U 190000970001,3,5-Trinitrobenzene
680000 19000019000Diphenyl ether
Surrogate %Rec Acceptance LimitsQualifier
0 34 - 130D2,4,6-Tribromophenol
0 34 - 130D2-Fluorobiphenyl
0 30 - 130D2-Fluorophenol
0 39 - 130DTerphenyl-d14
0 30 - 130DPhenol-d5
0 27 - 130DNitrobenzene-d5
TestAmerica Savannah Page 118 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-8-NS
Client Matrix: % Moisture: 27.7
680-56861-17
Solid
Date Sampled: 04/15/2010 1600
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/04/2010 1243
10
8270C Analysis Batch: 680-167473
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1022.d
30.03 g
1.0 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
4600 U 4600570Acenaphthene
4600 U 4600500Acenaphthylene
4600 U 4600390Acetophenone
4600 U 46003902-Acetylaminofluorene
930000 U 93000037000alpha,alpha-Dimethyl phenethylamine
4600 U 46005104-Aminobiphenyl
9100 U 9100470Aniline
4600 U 4600350Anthracene
4600 U 4600790Aramite, Total
4600 U 4600370Benzo[a]anthracene
4600 U 4600720Benzo[a]pyrene
4600 U 4600520Benzo[b]fluoranthene
4600 U 4600300Benzo[g,h,i]perylene
4600 U 4600900Benzo[k]fluoranthene
4600 U 4600460Benzyl alcohol
4600 U 46003901,1'-Biphenyl
4600 U 4600540Bis(2-chloroethoxy)methane
4600 U 4600620Bis(2-chloroethyl)ether
4600 U 4600410bis(chloroisopropyl) ether
4600 U 4600460Bis(2-ethylhexyl) phthalate
4600 U 46005004-Bromophenyl phenyl ether
4600 U 4600360Butyl benzyl phthalate
9100 U 91007204-Chloroaniline
4600 U 46004804-Chloro-3-methylphenol
4600 U 46005402-Chloronaphthalene
4600 U 46005502-Chlorophenol
4600 U 46005104-Chlorophenyl phenyl ether
4600 U 4600290Chrysene
4600 U 46002300Diallate
4600 U 4600330Dibenz(a,h)anthracene
4600 U 4600460Dibenzofuran
4600 U 46005101,2-Dichlorobenzene
4600 U 46004701,3-Dichlorobenzene
4600 U 46004801,4-Dichlorobenzene
9100 U 91003903,3'-Dichlorobenzidine
4600 U 46004802,4-Dichlorophenol
4600 U 46003702,6-Dichlorophenol
4600 U 4600480Diethyl phthalate
4600 U 4600350Dimethoate
4600 U 46002307,12-Dimethylbenz(a)anthracene
23000 U 23000120003,3'-Dimethylbenzidine
4600 U 46006102,4-Dimethylphenol
4600 U 4600470Dimethyl phthalate
4600 U 4600410Di-n-butyl phthalate
4600 U 46003301,3-Dinitrobenzene
23000 U 2300023004,6-Dinitro-2-methylphenol
TestAmerica Savannah Page 119 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-8-NS
Client Matrix: % Moisture: 27.7
680-56861-17
Solid
Date Sampled: 04/15/2010 1600
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/04/2010 1243
10
8270C Analysis Batch: 680-167473
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1022.d
30.03 g
1.0 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
23000 U 23000110002,4-Dinitrophenol
4600 U 46006802,4-Dinitrotoluene
4600 U 46005802,6-Dinitrotoluene
4600 U 4600400Di-n-octyl phthalate
4600 U 46002200Dinoseb
4600 U 460017001,4-Dioxane
4600 U 4600230Disulfoton
4600 U 4600430Ethyl methanesulfonate
4600 U 4600300Ethyl Parathion
4600 U 4600400Famphur
4600 U 4600440Fluoranthene
4600 U 4600500Fluorene
4600 U 4600540Hexachlorobenzene
4600 U 4600500Hexachlorobutadiene
4600 U 4600570Hexachlorocyclopentadiene
4600 U 4600390Hexachloroethane
2300000 U 2300000180000Hexachlorophene
4600 U 4600400Hexachloropropene
4600 U 4600390Indeno[1,2,3-cd]pyrene
4600 U 4600460Isophorone
4600 U 4600330Isosafrole
930000 U 93000011000Methapyrilene
4600 U 46005703-Methylcholanthrene
4600 U 4600230Methyl methanesulfonate
4600 U 46005202-Methylnaphthalene
4600 U 4600360Methyl parathion
4600 U 46003702-Methylphenol
4600 U 46005903 & 4 Methylphenol
4600 U 4600410Naphthalene
4600 U 46002301,4-Naphthoquinone
4600 U 46009101-Naphthylamine
4600 U 46004702-Naphthylamine
23000 U 230006202-Nitroaniline
23000 U 230006403-Nitroaniline
23000 U 230006804-Nitroaniline
4600 U 4600360Nitrobenzene
4600 U 46005702-Nitrophenol
23000 U 2300046004-Nitrophenol
46000 U 46000110004-Nitroquinoline-1-oxide
4600 U 4600360N-Nitro-o-toluidine
4600 U 4600390N-Nitrosodiethylamine
4600 U 46001700N-Nitrosodimethylamine
4600 U 4600330N-Nitrosodi-n-butylamine
4600 U 4600440N-Nitrosodi-n-propylamine
4600 U 4600460N-Nitrosodiphenylamine
4600 U 4600350N-Nitrosomethylethylamine
TestAmerica Savannah Page 120 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-8-NS
Client Matrix: % Moisture: 27.7
680-56861-17
Solid
Date Sampled: 04/15/2010 1600
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/04/2010 1243
10
8270C Analysis Batch: 680-167473
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1022.d
30.03 g
1.0 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
4600 U 4600370N-Nitrosomorpholine
4600 U 4600290N-Nitrosopiperidine
4600 U 4600250N-Nitrosopyrrolidine
4600 U 4600550o,o',o''-Triethylphosphorothioate
4600 U 4600260p-Dimethylamino azobenzene
4600 U 4600350Pentachlorobenzene
4600 U 4600290Pentachloronitrobenzene
23000 U 230004600Pentachlorophenol
4600 U 4600460Phenacetin
4600 U 4600370Phenanthrene
4600 U 4600470Phenol
4600 U 4600300Phorate
4600 U 46002302-Picoline
23000 U 2300012000p-Phenylene diamine
4600 U 4600330Pronamide
4600 U 4600370Pyrene
4600 U 4600400Pyridine
4600 U 4600330Safrole, Total
4600 U 4600280Sulfotepp
4600 U 46004301,2,4,5-Tetrachlorobenzene
4600 U 46003002,3,4,6-Tetrachlorophenol
4600 U 4600320Thionazin
4600 U 46004802-Toluidine
4600 U 46004301,2,4-Trichlorobenzene
4600 U 46004802,4,5-Trichlorophenol
4600 U 46004002,4,6-Trichlorophenol
4600 U 460023001,3,5-Trinitrobenzene
700 J 4600470Diphenyl ether
Surrogate %Rec Acceptance LimitsQualifier
0 34 - 130D2,4,6-Tribromophenol
0 34 - 130D2-Fluorobiphenyl
0 30 - 130D2-Fluorophenol
0 39 - 130DTerphenyl-d14
0 30 - 130DPhenol-d5
0 27 - 130DNitrobenzene-d5
TestAmerica Savannah Page 121 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-8-LS
Client Matrix: % Moisture: 75.4
680-56861-18
Solid
Date Sampled: 04/15/2010 1615
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/04/2010 1307
10
8270C Analysis Batch: 680-167473
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1023.d
30.00 g
10 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
130000 U 13000017000Acenaphthene
130000 U 13000015000Acenaphthylene
130000 U 13000011000Acetophenone
130000 U 130000110002-Acetylaminofluorene
27000000 U 270000001100000alpha,alpha-Dimethyl phenethylamine
130000 U 130000150004-Aminobiphenyl
270000 U 27000014000Aniline
130000 U 13000010000Anthracene
130000 U 13000023000Aramite, Total
130000 U 13000011000Benzo[a]anthracene
130000 U 13000021000Benzo[a]pyrene
130000 U 13000015000Benzo[b]fluoranthene
130000 U 1300008900Benzo[g,h,i]perylene
130000 U 13000026000Benzo[k]fluoranthene
130000 U 13000013000Benzyl alcohol
760000 130000110001,1'-Biphenyl
130000 U 13000016000Bis(2-chloroethoxy)methane
130000 U 13000018000Bis(2-chloroethyl)ether
130000 U 13000012000bis(chloroisopropyl) ether
130000 U 13000013000Bis(2-ethylhexyl) phthalate
130000 U 130000150004-Bromophenyl phenyl ether
130000 U 13000011000Butyl benzyl phthalate
270000 U 270000210004-Chloroaniline
130000 U 130000140004-Chloro-3-methylphenol
130000 U 130000160002-Chloronaphthalene
130000 U 130000160002-Chlorophenol
130000 U 130000150004-Chlorophenyl phenyl ether
130000 U 1300008500Chrysene
130000 U 13000069000Diallate
130000 U 1300009800Dibenz(a,h)anthracene
130000 U 13000013000Dibenzofuran
130000 U 130000150001,2-Dichlorobenzene
130000 U 130000140001,3-Dichlorobenzene
130000 U 130000140001,4-Dichlorobenzene
270000 U 270000110003,3'-Dichlorobenzidine
130000 U 130000140002,4-Dichlorophenol
130000 U 130000110002,6-Dichlorophenol
130000 U 13000014000Diethyl phthalate
130000 U 13000010000Dimethoate
130000 U 13000069007,12-Dimethylbenz(a)anthracene
690000 U 6900003400003,3'-Dimethylbenzidine
130000 U 130000180002,4-Dimethylphenol
130000 U 13000014000Dimethyl phthalate
130000 U 13000012000Di-n-butyl phthalate
130000 U 13000098001,3-Dinitrobenzene
690000 U 690000690004,6-Dinitro-2-methylphenol
TestAmerica Savannah Page 122 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-8-LS
Client Matrix: % Moisture: 75.4
680-56861-18
Solid
Date Sampled: 04/15/2010 1615
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/04/2010 1307
10
8270C Analysis Batch: 680-167473
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1023.d
30.00 g
10 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
690000 U 6900003400002,4-Dinitrophenol
130000 U 130000200002,4-Dinitrotoluene
130000 U 130000170002,6-Dinitrotoluene
130000 U 13000012000Di-n-octyl phthalate
130000 U 13000065000Dinoseb
130000 U 130000490001,4-Dioxane
130000 U 1300006900Disulfoton
130000 U 13000013000Ethyl methanesulfonate
130000 U 1300008900Ethyl Parathion
130000 U 13000012000Famphur
130000 U 13000013000Fluoranthene
130000 U 13000015000Fluorene
130000 U 13000016000Hexachlorobenzene
130000 U 13000015000Hexachlorobutadiene
130000 U 13000017000Hexachlorocyclopentadiene
130000 U 13000011000Hexachloroethane
69000000 U 690000005300000Hexachlorophene
130000 U 13000012000Hexachloropropene
130000 U 13000011000Indeno[1,2,3-cd]pyrene
130000 U 13000013000Isophorone
130000 U 1300009800Isosafrole
27000000 U 27000000340000Methapyrilene
130000 U 130000170003-Methylcholanthrene
130000 U 1300006900Methyl methanesulfonate
130000 U 130000150002-Methylnaphthalene
130000 U 13000011000Methyl parathion
130000 U 130000110002-Methylphenol
130000 U 130000170003 & 4 Methylphenol
130000 U 13000012000Naphthalene
130000 U 13000069001,4-Naphthoquinone
130000 U 130000270001-Naphthylamine
130000 U 130000140002-Naphthylamine
690000 U 690000180002-Nitroaniline
690000 U 690000190003-Nitroaniline
690000 U 690000200004-Nitroaniline
130000 U 13000011000Nitrobenzene
130000 U 130000170002-Nitrophenol
690000 U 6900001300004-Nitrophenol
1300000 U 13000003400004-Nitroquinoline-1-oxide
130000 U 13000011000N-Nitro-o-toluidine
130000 U 13000011000N-Nitrosodiethylamine
130000 U 13000049000N-Nitrosodimethylamine
130000 U 1300009800N-Nitrosodi-n-butylamine
130000 U 13000013000N-Nitrosodi-n-propylamine
130000 U 13000013000N-Nitrosodiphenylamine
130000 U 13000010000N-Nitrosomethylethylamine
TestAmerica Savannah Page 123 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-8-LS
Client Matrix: % Moisture: 75.4
680-56861-18
Solid
Date Sampled: 04/15/2010 1615
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/04/2010 1307
10
8270C Analysis Batch: 680-167473
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1023.d
30.00 g
10 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
130000 U 13000011000N-Nitrosomorpholine
130000 U 1300008500N-Nitrosopiperidine
130000 U 1300007300N-Nitrosopyrrolidine
130000 U 13000016000o,o',o''-Triethylphosphorothioate
130000 U 1300007700p-Dimethylamino azobenzene
130000 U 13000010000Pentachlorobenzene
130000 U 1300008500Pentachloronitrobenzene
690000 U 690000130000Pentachlorophenol
130000 U 13000013000Phenacetin
130000 U 13000011000Phenanthrene
130000 U 13000014000Phenol
130000 U 1300008900Phorate
130000 U 13000069002-Picoline
690000 U 690000340000p-Phenylene diamine
130000 U 1300009800Pronamide
15000 J 13000011000Pyrene
130000 U 13000012000Pyridine
130000 U 1300009800Safrole, Total
130000 U 1300008100Sulfotepp
130000 U 130000130001,2,4,5-Tetrachlorobenzene
130000 U 13000089002,3,4,6-Tetrachlorophenol
130000 U 1300009400Thionazin
130000 U 130000140002-Toluidine
130000 U 130000130001,2,4-Trichlorobenzene
130000 U 130000140002,4,5-Trichlorophenol
130000 U 130000120002,4,6-Trichlorophenol
130000 U 130000690001,3,5-Trinitrobenzene
2500000 13000014000Diphenyl ether
Surrogate %Rec Acceptance LimitsQualifier
0 34 - 130D2,4,6-Tribromophenol
0 34 - 130D2-Fluorobiphenyl
0 30 - 130D2-Fluorophenol
0 39 - 130DTerphenyl-d14
0 30 - 130DPhenol-d5
0 27 - 130DNitrobenzene-d5
TestAmerica Savannah Page 124 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-8-US
Client Matrix: % Moisture: 86.3
680-56861-19
Solid
Date Sampled: 04/15/2010 1620
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/04/2010 1331
10
8270C Analysis Batch: 680-167473
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1024.d
30.04 g
10 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
240000 U 24000030000Acenaphthene
240000 U 24000026000Acenaphthylene
240000 U 24000020000Acetophenone
240000 U 240000200002-Acetylaminofluorene
49000000 U 490000002000000alpha,alpha-Dimethyl phenethylamine
240000 U 240000270004-Aminobiphenyl
480000 U 48000025000Aniline
240000 U 24000018000Anthracene
240000 U 24000042000Aramite, Total
240000 U 24000020000Benzo[a]anthracene
240000 U 24000038000Benzo[a]pyrene
240000 U 24000028000Benzo[b]fluoranthene
240000 U 24000016000Benzo[g,h,i]perylene
240000 U 24000047000Benzo[k]fluoranthene
240000 U 24000024000Benzyl alcohol
33000 J 240000200001,1'-Biphenyl
240000 U 24000028000Bis(2-chloroethoxy)methane
240000 U 24000033000Bis(2-chloroethyl)ether
240000 U 24000022000bis(chloroisopropyl) ether
240000 U 24000024000Bis(2-ethylhexyl) phthalate
240000 U 240000260004-Bromophenyl phenyl ether
240000 U 24000019000Butyl benzyl phthalate
480000 U 480000380004-Chloroaniline
240000 U 240000260004-Chloro-3-methylphenol
240000 U 240000280002-Chloronaphthalene
240000 U 240000290002-Chlorophenol
240000 U 240000270004-Chlorophenyl phenyl ether
240000 U 24000015000Chrysene
240000 U 240000120000Diallate
240000 U 24000018000Dibenz(a,h)anthracene
240000 U 24000024000Dibenzofuran
240000 U 240000270001,2-Dichlorobenzene
240000 U 240000250001,3-Dichlorobenzene
240000 U 240000260001,4-Dichlorobenzene
480000 U 480000200003,3'-Dichlorobenzidine
240000 U 240000260002,4-Dichlorophenol
240000 U 240000200002,6-Dichlorophenol
240000 U 24000026000Diethyl phthalate
240000 U 24000018000Dimethoate
240000 U 240000120007,12-Dimethylbenz(a)anthracene
1200000 U 12000006100003,3'-Dimethylbenzidine
240000 U 240000320002,4-Dimethylphenol
240000 U 24000025000Dimethyl phthalate
240000 U 24000022000Di-n-butyl phthalate
240000 U 240000180001,3-Dinitrobenzene
1200000 U 12000001200004,6-Dinitro-2-methylphenol
TestAmerica Savannah Page 125 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-8-US
Client Matrix: % Moisture: 86.3
680-56861-19
Solid
Date Sampled: 04/15/2010 1620
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/04/2010 1331
10
8270C Analysis Batch: 680-167473
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1024.d
30.04 g
10 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
1200000 U 12000006100002,4-Dinitrophenol
240000 U 240000360002,4-Dinitrotoluene
240000 U 240000310002,6-Dinitrotoluene
240000 U 24000021000Di-n-octyl phthalate
240000 U 240000120000Dinoseb
240000 U 240000880001,4-Dioxane
240000 U 24000012000Disulfoton
240000 U 24000023000Ethyl methanesulfonate
240000 U 24000016000Ethyl Parathion
240000 U 24000021000Famphur
240000 U 24000023000Fluoranthene
240000 U 24000026000Fluorene
240000 U 24000028000Hexachlorobenzene
240000 U 24000026000Hexachlorobutadiene
240000 U 24000030000Hexachlorocyclopentadiene
240000 U 24000020000Hexachloroethane
120000000 U 1200000009500000Hexachlorophene
240000 U 24000021000Hexachloropropene
240000 U 24000020000Indeno[1,2,3-cd]pyrene
240000 U 24000024000Isophorone
240000 U 24000018000Isosafrole
49000000 U 49000000610000Methapyrilene
240000 U 240000300003-Methylcholanthrene
240000 U 24000012000Methyl methanesulfonate
240000 U 240000280002-Methylnaphthalene
240000 U 24000019000Methyl parathion
240000 U 240000200002-Methylphenol
240000 U 240000310003 & 4 Methylphenol
240000 U 24000022000Naphthalene
240000 U 240000120001,4-Naphthoquinone
240000 U 240000480001-Naphthylamine
240000 U 240000250002-Naphthylamine
1200000 U 1200000330002-Nitroaniline
1200000 U 1200000340003-Nitroaniline
1200000 U 1200000360004-Nitroaniline
240000 U 24000019000Nitrobenzene
240000 U 240000300002-Nitrophenol
1200000 U 12000002400004-Nitrophenol
2400000 U 24000006100004-Nitroquinoline-1-oxide
240000 U 24000019000N-Nitro-o-toluidine
240000 U 24000020000N-Nitrosodiethylamine
240000 U 24000088000N-Nitrosodimethylamine
240000 U 24000018000N-Nitrosodi-n-butylamine
240000 U 24000023000N-Nitrosodi-n-propylamine
240000 U 24000024000N-Nitrosodiphenylamine
240000 U 24000018000N-Nitrosomethylethylamine
TestAmerica Savannah Page 126 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-8-US
Client Matrix: % Moisture: 86.3
680-56861-19
Solid
Date Sampled: 04/15/2010 1620
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/04/2010 1331
10
8270C Analysis Batch: 680-167473
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1024.d
30.04 g
10 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
240000 U 24000020000N-Nitrosomorpholine
240000 U 24000015000N-Nitrosopiperidine
240000 U 24000013000N-Nitrosopyrrolidine
240000 U 24000029000o,o',o''-Triethylphosphorothioate
240000 U 24000014000p-Dimethylamino azobenzene
240000 U 24000018000Pentachlorobenzene
240000 U 24000015000Pentachloronitrobenzene
1200000 U 1200000240000Pentachlorophenol
240000 U 24000024000Phenacetin
240000 U 24000020000Phenanthrene
240000 U 24000025000Phenol
240000 U 24000016000Phorate
240000 U 240000120002-Picoline
1200000 U 1200000610000p-Phenylene diamine
240000 U 24000018000Pronamide
240000 U 24000020000Pyrene
240000 U 24000021000Pyridine
240000 U 24000018000Safrole, Total
240000 U 24000015000Sulfotepp
240000 U 240000230001,2,4,5-Tetrachlorobenzene
240000 U 240000160002,3,4,6-Tetrachlorophenol
240000 U 24000017000Thionazin
240000 U 240000260002-Toluidine
240000 U 240000230001,2,4-Trichlorobenzene
240000 U 240000260002,4,5-Trichlorophenol
240000 U 240000210002,4,6-Trichlorophenol
240000 U 2400001200001,3,5-Trinitrobenzene
110000 J 24000025000Diphenyl ether
Surrogate %Rec Acceptance LimitsQualifier
0 34 - 130D2,4,6-Tribromophenol
0 34 - 130D2-Fluorobiphenyl
0 30 - 130D2-Fluorophenol
0 39 - 130DTerphenyl-d14
0 30 - 130DPhenol-d5
0 27 - 130DNitrobenzene-d5
TestAmerica Savannah Page 127 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-1-US
Client Matrix: % Moisture: 62.6
680-56861-20
Solid
Date Sampled: 04/15/2010 1700
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/04/2010 1354
10
8270C Analysis Batch: 680-167473
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1025.d
30.02 g
10 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
88000 U 8800011000Acenaphthene
88000 U 880009600Acenaphthylene
88000 U 880007500Acetophenone
88000 U 8800075002-Acetylaminofluorene
18000000 U 18000000720000alpha,alpha-Dimethyl phenethylamine
88000 U 8800099004-Aminobiphenyl
180000 U 1800009100Aniline
88000 U 880006700Anthracene
88000 U 8800015000Aramite, Total
88000 U 880007200Benzo[a]anthracene
88000 U 8800014000Benzo[a]pyrene
88000 U 8800010000Benzo[b]fluoranthene
88000 U 880005900Benzo[g,h,i]perylene
88000 U 8800017000Benzo[k]fluoranthene
88000 U 880008800Benzyl alcohol
230000 8800075001,1'-Biphenyl
88000 U 8800010000Bis(2-chloroethoxy)methane
88000 U 8800012000Bis(2-chloroethyl)ether
88000 U 880008000bis(chloroisopropyl) ether
88000 U 880008800Bis(2-ethylhexyl) phthalate
88000 U 8800096004-Bromophenyl phenyl ether
88000 U 880006900Butyl benzyl phthalate
180000 U 180000140004-Chloroaniline
88000 U 8800094004-Chloro-3-methylphenol
88000 U 88000100002-Chloronaphthalene
88000 U 88000110002-Chlorophenol
88000 U 8800099004-Chlorophenyl phenyl ether
88000 U 880005600Chrysene
88000 U 8800045000Diallate
88000 U 880006400Dibenz(a,h)anthracene
88000 U 880008800Dibenzofuran
88000 U 8800099001,2-Dichlorobenzene
88000 U 8800091001,3-Dichlorobenzene
88000 U 8800094001,4-Dichlorobenzene
180000 U 18000075003,3'-Dichlorobenzidine
88000 U 8800094002,4-Dichlorophenol
88000 U 8800072002,6-Dichlorophenol
88000 U 880009400Diethyl phthalate
88000 U 880006700Dimethoate
88000 U 8800045007,12-Dimethylbenz(a)anthracene
450000 U 4500002200003,3'-Dimethylbenzidine
88000 U 88000120002,4-Dimethylphenol
88000 U 880009100Dimethyl phthalate
88000 U 880008000Di-n-butyl phthalate
88000 U 8800064001,3-Dinitrobenzene
450000 U 450000450004,6-Dinitro-2-methylphenol
TestAmerica Savannah Page 128 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-1-US
Client Matrix: % Moisture: 62.6
680-56861-20
Solid
Date Sampled: 04/15/2010 1700
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/04/2010 1354
10
8270C Analysis Batch: 680-167473
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1025.d
30.02 g
10 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
450000 U 4500002200002,4-Dinitrophenol
88000 U 88000130002,4-Dinitrotoluene
88000 U 88000110002,6-Dinitrotoluene
88000 U 880007800Di-n-octyl phthalate
88000 U 8800043000Dinoseb
88000 U 88000320001,4-Dioxane
88000 U 880004500Disulfoton
88000 U 880008300Ethyl methanesulfonate
88000 U 880005900Ethyl Parathion
88000 U 880007800Famphur
88000 U 880008600Fluoranthene
88000 U 880009600Fluorene
88000 U 8800010000Hexachlorobenzene
88000 U 880009600Hexachlorobutadiene
88000 U 8800011000Hexachlorocyclopentadiene
88000 U 880007500Hexachloroethane
45000000 U 450000003500000Hexachlorophene
88000 U 880007800Hexachloropropene
88000 U 880007500Indeno[1,2,3-cd]pyrene
88000 U 880008800Isophorone
88000 U 880006400Isosafrole
18000000 U 18000000220000Methapyrilene
88000 U 88000110003-Methylcholanthrene
88000 U 880004500Methyl methanesulfonate
15000 J 88000100002-Methylnaphthalene
88000 U 880006900Methyl parathion
88000 U 8800072002-Methylphenol
88000 U 88000110003 & 4 Methylphenol
88000 U 880008000Naphthalene
88000 U 8800045001,4-Naphthoquinone
88000 U 88000180001-Naphthylamine
88000 U 8800091002-Naphthylamine
450000 U 450000120002-Nitroaniline
450000 U 450000120003-Nitroaniline
450000 U 450000130004-Nitroaniline
88000 U 880006900Nitrobenzene
88000 U 88000110002-Nitrophenol
450000 U 450000880004-Nitrophenol
880000 U 8800002200004-Nitroquinoline-1-oxide
88000 U 880006900N-Nitro-o-toluidine
88000 U 880007500N-Nitrosodiethylamine
88000 U 8800032000N-Nitrosodimethylamine
88000 U 880006400N-Nitrosodi-n-butylamine
88000 U 880008600N-Nitrosodi-n-propylamine
88000 U 880008800N-Nitrosodiphenylamine
88000 U 880006700N-Nitrosomethylethylamine
TestAmerica Savannah Page 129 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-1-US
Client Matrix: % Moisture: 62.6
680-56861-20
Solid
Date Sampled: 04/15/2010 1700
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 2315
05/04/2010 1354
10
8270C Analysis Batch: 680-167473
Prep Batch: 680-166147
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1025.d
30.02 g
10 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
88000 U 880007200N-Nitrosomorpholine
88000 U 880005600N-Nitrosopiperidine
88000 U 880004800N-Nitrosopyrrolidine
88000 U 8800011000o,o',o''-Triethylphosphorothioate
88000 U 880005100p-Dimethylamino azobenzene
88000 U 880006700Pentachlorobenzene
88000 U 880005600Pentachloronitrobenzene
450000 U 45000088000Pentachlorophenol
88000 U 880008800Phenacetin
88000 U 880007200Phenanthrene
88000 U 880009100Phenol
88000 U 880005900Phorate
88000 U 8800045002-Picoline
450000 U 450000220000p-Phenylene diamine
88000 U 880006400Pronamide
88000 U 880007200Pyrene
88000 U 880007800Pyridine
88000 U 880006400Safrole, Total
88000 U 880005300Sulfotepp
88000 U 8800083001,2,4,5-Tetrachlorobenzene
88000 U 8800059002,3,4,6-Tetrachlorophenol
88000 U 880006100Thionazin
88000 U 8800094002-Toluidine
88000 U 8800083001,2,4-Trichlorobenzene
88000 U 8800094002,4,5-Trichlorophenol
88000 U 8800078002,4,6-Trichlorophenol
88000 U 88000450001,3,5-Trinitrobenzene
780000 880009100Diphenyl ether
Surrogate %Rec Acceptance LimitsQualifier
0 34 - 130D2,4,6-Tribromophenol
0 34 - 130D2-Fluorobiphenyl
0 30 - 130D2-Fluorophenol
0 39 - 130DTerphenyl-d14
0 30 - 130DPhenol-d5
0 27 - 130DNitrobenzene-d5
TestAmerica Savannah Page 130 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-2-NS
Client Matrix: % Moisture: 14.5
680-56861-21
Solid
Date Sampled: 04/16/2010 0840
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 1628
05/04/2010 1529
50
8270C Analysis Batch: 680-167473
Prep Batch: 680-166138
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1026.d
30.08 g
1 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
19000 U 190002400Acenaphthene
19000 U 190002100Acenaphthylene
19000 U 190001600Acetophenone
19000 U 1900016002-Acetylaminofluorene
3900000 U 3900000160000alpha,alpha-Dimethyl phenethylamine
19000 U 1900022004-Aminobiphenyl
38000 U 380002000Aniline
19000 U 190001500Anthracene
19000 U 190003300Aramite, Total
19000 U 190001600Benzo[a]anthracene
19000 U 190003000Benzo[a]pyrene
19000 U 190002200Benzo[b]fluoranthene
19000 U 190001300Benzo[g,h,i]perylene
19000 U 190003800Benzo[k]fluoranthene
5900 J 190001900Benzyl alcohol
33000 1900016001,1'-Biphenyl
19000 U 190002300Bis(2-chloroethoxy)methane
19000 U 190002600Bis(2-chloroethyl)ether
19000 U 190001700bis(chloroisopropyl) ether
19000 U 190001900Bis(2-ethylhexyl) phthalate
19000 U 1900021004-Bromophenyl phenyl ether
19000 U 190001500Butyl benzyl phthalate
38000 U 3800030004-Chloroaniline
19000 U 1900020004-Chloro-3-methylphenol
19000 U 1900023002-Chloronaphthalene
19000 U 1900023002-Chlorophenol
19000 U 1900022004-Chlorophenyl phenyl ether
19000 U 190001200Chrysene
19000 U 190009900Diallate
19000 U 190001400Dibenz(a,h)anthracene
19000 U 190001900Dibenzofuran
19000 U 1900022001,2-Dichlorobenzene
19000 U 1900020001,3-Dichlorobenzene
19000 U 1900020001,4-Dichlorobenzene
38000 U 3800016003,3'-Dichlorobenzidine
19000 U 1900020002,4-Dichlorophenol
19000 U 1900016002,6-Dichlorophenol
19000 U 190002000Diethyl phthalate
19000 U 190001500Dimethoate
19000 U 190009907,12-Dimethylbenz(a)anthracene
99000 U 99000490003,3'-Dimethylbenzidine
19000 U 1900026002,4-Dimethylphenol
19000 U 190002000Dimethyl phthalate
19000 U 190001700Di-n-butyl phthalate
19000 U 1900014001,3-Dinitrobenzene
99000 U 9900099004,6-Dinitro-2-methylphenol
TestAmerica Savannah Page 131 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-2-NS
Client Matrix: % Moisture: 14.5
680-56861-21
Solid
Date Sampled: 04/16/2010 0840
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 1628
05/04/2010 1529
50
8270C Analysis Batch: 680-167473
Prep Batch: 680-166138
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1026.d
30.08 g
1 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
99000 U 99000480002,4-Dinitrophenol
19000 U 1900029002,4-Dinitrotoluene
19000 U 1900024002,6-Dinitrotoluene
19000 U 190001700Di-n-octyl phthalate
19000 U 190009300Dinoseb
19000 U 1900070001,4-Dioxane
19000 U 19000990Disulfoton
19000 U 190001800Ethyl methanesulfonate
19000 U 190001300Ethyl Parathion
19000 U 190001700Famphur
19000 U 190001900Fluoranthene
19000 U 190002100Fluorene
19000 U 190002300Hexachlorobenzene
19000 U 190002100Hexachlorobutadiene
19000 U 190002400Hexachlorocyclopentadiene
19000 U 190001600Hexachloroethane
9900000 U 9900000760000Hexachlorophene
19000 U 190001700Hexachloropropene
19000 U 190001600Indeno[1,2,3-cd]pyrene
19000 U 190001900Isophorone
19000 U 190001400Isosafrole
3900000 U 390000048000Methapyrilene
19000 U 1900024003-Methylcholanthrene
19000 U 19000990Methyl methanesulfonate
19000 U 1900022002-Methylnaphthalene
19000 U 190001500Methyl parathion
19000 U 1900016002-Methylphenol
19000 U 1900025003 & 4 Methylphenol
19000 U 190001700Naphthalene
19000 U 190009901,4-Naphthoquinone
19000 U 1900038001-Naphthylamine
19000 U 1900020002-Naphthylamine
99000 U 9900026002-Nitroaniline
99000 U 9900027003-Nitroaniline
99000 U 9900029004-Nitroaniline
19000 U 190001500Nitrobenzene
19000 U 1900024002-Nitrophenol
99000 U 99000190004-Nitrophenol
190000 U 190000480004-Nitroquinoline-1-oxide
19000 U 190001500N-Nitro-o-toluidine
19000 U 190001600N-Nitrosodiethylamine
19000 U 190007000N-Nitrosodimethylamine
19000 U 190001400N-Nitrosodi-n-butylamine
19000 U 190001900N-Nitrosodi-n-propylamine
19000 U 190001900N-Nitrosodiphenylamine
19000 U 190001500N-Nitrosomethylethylamine
TestAmerica Savannah Page 132 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-2-NS
Client Matrix: % Moisture: 14.5
680-56861-21
Solid
Date Sampled: 04/16/2010 0840
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 1628
05/04/2010 1529
50
8270C Analysis Batch: 680-167473
Prep Batch: 680-166138
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1026.d
30.08 g
1 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
19000 U 190001600N-Nitrosomorpholine
19000 U 190001200N-Nitrosopiperidine
19000 U 190001000N-Nitrosopyrrolidine
8600 J 190002300o,o',o''-Triethylphosphorothioate
19000 U 190001100p-Dimethylamino azobenzene
19000 U 190001500Pentachlorobenzene
19000 U 190001200Pentachloronitrobenzene
99000 U 9900019000Pentachlorophenol
19000 U 190001900Phenacetin
19000 U 190001600Phenanthrene
19000 U 190002000Phenol
19000 U 190001300Phorate
19000 U 190009902-Picoline
99000 U 9900049000p-Phenylene diamine
19000 U 190001400Pronamide
19000 U 190001600Pyrene
19000 U 190001700Pyridine
19000 U 190001400Safrole, Total
19000 U 190001200Sulfotepp
19000 U 1900018001,2,4,5-Tetrachlorobenzene
19000 U 1900013002,3,4,6-Tetrachlorophenol
19000 U 190001300Thionazin
19000 U 1900020002-Toluidine
19000 U 1900018001,2,4-Trichlorobenzene
19000 U 1900020002,4,5-Trichlorophenol
19000 U 1900017002,4,6-Trichlorophenol
19000 U 1900099001,3,5-Trinitrobenzene
120000 190002000Diphenyl ether
Surrogate %Rec Acceptance LimitsQualifier
0 34 - 130D2,4,6-Tribromophenol
0 34 - 130D2-Fluorobiphenyl
0 30 - 130D2-Fluorophenol
0 39 - 130DTerphenyl-d14
0 30 - 130DPhenol-d5
0 27 - 130DNitrobenzene-d5
TestAmerica Savannah Page 133 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-2-LS
Client Matrix: % Moisture: 66.8
680-56861-22
Solid
Date Sampled: 04/16/2010 0850
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 1628
05/04/2010 1553
10
8270C Analysis Batch: 680-167473
Prep Batch: 680-166138
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1027.d
30.11 g
20 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
200000 U 20000025000Acenaphthene
200000 U 20000022000Acenaphthylene
200000 U 20000017000Acetophenone
200000 U 200000170002-Acetylaminofluorene
40000000 U 400000001600000alpha,alpha-Dimethyl phenethylamine
200000 U 200000220004-Aminobiphenyl
400000 U 40000020000Aniline
200000 U 20000015000Anthracene
200000 U 20000034000Aramite, Total
200000 U 20000016000Benzo[a]anthracene
200000 U 20000031000Benzo[a]pyrene
200000 U 20000023000Benzo[b]fluoranthene
200000 U 20000013000Benzo[g,h,i]perylene
200000 U 20000039000Benzo[k]fluoranthene
200000 U 20000020000Benzyl alcohol
470000 200000170001,1'-Biphenyl
200000 U 20000023000Bis(2-chloroethoxy)methane
200000 U 20000027000Bis(2-chloroethyl)ether
200000 U 20000018000bis(chloroisopropyl) ether
200000 U 20000020000Bis(2-ethylhexyl) phthalate
200000 U 200000220004-Bromophenyl phenyl ether
200000 U 20000016000Butyl benzyl phthalate
400000 U 400000310004-Chloroaniline
200000 U 200000210004-Chloro-3-methylphenol
200000 U 200000230002-Chloronaphthalene
200000 U 200000240002-Chlorophenol
200000 U 200000220004-Chlorophenyl phenyl ether
200000 U 20000013000Chrysene
200000 U 200000100000Diallate
200000 U 20000014000Dibenz(a,h)anthracene
200000 U 20000020000Dibenzofuran
200000 U 200000220001,2-Dichlorobenzene
200000 U 200000200001,3-Dichlorobenzene
200000 U 200000210001,4-Dichlorobenzene
400000 U 400000170003,3'-Dichlorobenzidine
200000 U 200000210002,4-Dichlorophenol
200000 U 200000160002,6-Dichlorophenol
200000 U 20000021000Diethyl phthalate
200000 U 20000015000Dimethoate
200000 U 200000100007,12-Dimethylbenz(a)anthracene
1000000 U 10000005000003,3'-Dimethylbenzidine
200000 U 200000260002,4-Dimethylphenol
200000 U 20000020000Dimethyl phthalate
200000 U 20000018000Di-n-butyl phthalate
200000 U 200000140001,3-Dinitrobenzene
1000000 U 10000001000004,6-Dinitro-2-methylphenol
TestAmerica Savannah Page 134 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-2-LS
Client Matrix: % Moisture: 66.8
680-56861-22
Solid
Date Sampled: 04/16/2010 0850
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 1628
05/04/2010 1553
10
8270C Analysis Batch: 680-167473
Prep Batch: 680-166138
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1027.d
30.11 g
20 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
1000000 U 10000005000002,4-Dinitrophenol
200000 U 200000290002,4-Dinitrotoluene
200000 U 200000250002,6-Dinitrotoluene
200000 U 20000017000Di-n-octyl phthalate
200000 U 20000096000Dinoseb
200000 U 200000720001,4-Dioxane
200000 U 20000010000Disulfoton
200000 U 20000019000Ethyl methanesulfonate
200000 U 20000013000Ethyl Parathion
200000 U 20000017000Famphur
200000 U 20000019000Fluoranthene
200000 U 20000022000Fluorene
200000 U 20000023000Hexachlorobenzene
200000 U 20000022000Hexachlorobutadiene
200000 U 20000025000Hexachlorocyclopentadiene
200000 U 20000017000Hexachloroethane
100000000 U 1000000007800000Hexachlorophene
200000 U 20000017000Hexachloropropene
200000 U 20000017000Indeno[1,2,3-cd]pyrene
200000 U 20000020000Isophorone
200000 U 20000014000Isosafrole
40000000 U 40000000500000Methapyrilene
200000 U 200000250003-Methylcholanthrene
200000 U 20000010000Methyl methanesulfonate
200000 U 200000230002-Methylnaphthalene
200000 U 20000016000Methyl parathion
200000 U 200000160002-Methylphenol
200000 U 200000260003 & 4 Methylphenol
200000 U 20000018000Naphthalene
200000 U 200000100001,4-Naphthoquinone
200000 U 200000400001-Naphthylamine
200000 U 200000200002-Naphthylamine
1000000 U 1000000270002-Nitroaniline
1000000 U 1000000280003-Nitroaniline
1000000 U 1000000290004-Nitroaniline
200000 U 20000016000Nitrobenzene
200000 U 200000250002-Nitrophenol
1000000 U 10000002000004-Nitrophenol
2000000 U 20000005000004-Nitroquinoline-1-oxide
200000 U 20000016000N-Nitro-o-toluidine
200000 U 20000017000N-Nitrosodiethylamine
200000 U 20000072000N-Nitrosodimethylamine
200000 U 20000014000N-Nitrosodi-n-butylamine
200000 U 20000019000N-Nitrosodi-n-propylamine
200000 U 20000020000N-Nitrosodiphenylamine
200000 U 20000015000N-Nitrosomethylethylamine
TestAmerica Savannah Page 135 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-2-LS
Client Matrix: % Moisture: 66.8
680-56861-22
Solid
Date Sampled: 04/16/2010 0850
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 1628
05/04/2010 1553
10
8270C Analysis Batch: 680-167473
Prep Batch: 680-166138
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g1027.d
30.11 g
20 mL
1 uL
3546
MSG
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
200000 U 20000016000N-Nitrosomorpholine
200000 U 20000013000N-Nitrosopiperidine
200000 U 20000011000N-Nitrosopyrrolidine
200000 U 20000024000o,o',o''-Triethylphosphorothioate
200000 U 20000011000p-Dimethylamino azobenzene
200000 U 20000015000Pentachlorobenzene
200000 U 20000013000Pentachloronitrobenzene
1000000 U 1000000200000Pentachlorophenol
200000 U 20000020000Phenacetin
200000 U 20000016000Phenanthrene
200000 U 20000020000Phenol
200000 U 20000013000Phorate
200000 U 200000100002-Picoline
1000000 U 1000000500000p-Phenylene diamine
200000 U 20000014000Pronamide
200000 U 20000016000Pyrene
200000 U 20000017000Pyridine
200000 U 20000014000Safrole, Total
200000 U 20000012000Sulfotepp
200000 U 200000190001,2,4,5-Tetrachlorobenzene
200000 U 200000130002,3,4,6-Tetrachlorophenol
200000 U 20000014000Thionazin
200000 U 200000210002-Toluidine
200000 U 200000190001,2,4-Trichlorobenzene
200000 U 200000210002,4,5-Trichlorophenol
200000 U 200000170002,4,6-Trichlorophenol
200000 U 2000001000001,3,5-Trinitrobenzene
1400000 20000020000Diphenyl ether
Surrogate %Rec Acceptance LimitsQualifier
0 34 - 130D2,4,6-Tribromophenol
0 34 - 130D2-Fluorobiphenyl
0 30 - 130D2-Fluorophenol
0 39 - 130DTerphenyl-d14
0 30 - 130DPhenol-d5
0 27 - 130DNitrobenzene-d5
TestAmerica Savannah Page 136 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-2-US
Client Matrix: % Moisture: 78.7
680-56861-23
Solid
Date Sampled: 04/16/2010 0930
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 1628
04/23/2010 1826
1.0
8270C Analysis Batch: 680-166548
Prep Batch: 680-166138
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
n7044.d
30.10 g
20 mL
1 uL
3546
MSN
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
31000 U 310003800Acenaphthene
31000 U 310003400Acenaphthylene
31000 U 310002600Acetophenone
31000 U 3100026002-Acetylaminofluorene
6300000 U 6300000250000alpha,alpha-Dimethyl phenethylamine
31000 U 3100035004-Aminobiphenyl
62000 U 620003200Aniline
31000 U 310002300Anthracene
31000 U 310005300Aramite, Total
31000 U 310002500Benzo[a]anthracene
31000 U 310004900Benzo[a]pyrene
31000 U 310003600Benzo[b]fluoranthene
31000 U 310002100Benzo[g,h,i]perylene
31000 U 310006100Benzo[k]fluoranthene
31000 U 310003100Benzyl alcohol
55000 3100026001,1'-Biphenyl
31000 U 310003700Bis(2-chloroethoxy)methane
31000 U 310004200Bis(2-chloroethyl)ether
31000 U 310002800bis(chloroisopropyl) ether
31000 U 310003100Bis(2-ethylhexyl) phthalate
31000 U 3100034004-Bromophenyl phenyl ether
31000 U 310002400Butyl benzyl phthalate
62000 U 6200049004-Chloroaniline
31000 U 3100033004-Chloro-3-methylphenol
31000 U 3100037002-Chloronaphthalene
31000 U 3100037002-Chlorophenol
31000 U 3100035004-Chlorophenyl phenyl ether
31000 U 310002000Chrysene
31000 U 3100016000Diallate
31000 U 310002200Dibenz(a,h)anthracene
31000 U 310003100Dibenzofuran
31000 U 3100035001,2-Dichlorobenzene
31000 U 3100032001,3-Dichlorobenzene
31000 U 3100033001,4-Dichlorobenzene
62000 U 6200026003,3'-Dichlorobenzidine
31000 U 3100033002,4-Dichlorophenol
31000 U 3100025002,6-Dichlorophenol
31000 U 310003300Diethyl phthalate
31000 U 310002300Dimethoate
31000 U 3100016007,12-Dimethylbenz(a)anthracene
160000 U 160000780003,3'-Dimethylbenzidine
31000 U 3100041002,4-Dimethylphenol
31000 U 310003200Dimethyl phthalate
31000 U 310002800Di-n-butyl phthalate
31000 U 3100022001,3-Dinitrobenzene
160000 U 160000160004,6-Dinitro-2-methylphenol
TestAmerica Savannah Page 137 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-2-US
Client Matrix: % Moisture: 78.7
680-56861-23
Solid
Date Sampled: 04/16/2010 0930
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 1628
04/23/2010 1826
1.0
8270C Analysis Batch: 680-166548
Prep Batch: 680-166138
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
n7044.d
30.10 g
20 mL
1 uL
3546
MSN
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
160000 U 160000780002,4-Dinitrophenol
31000 U 3100046002,4-Dinitrotoluene
31000 U 3100039002,6-Dinitrotoluene
31000 U 310002700Di-n-octyl phthalate
31000 U 3100015000Dinoseb
31000 U 31000110001,4-Dioxane
31000 U 310001600Disulfoton
31000 U 310002900Ethyl methanesulfonate
31000 U 310002100Ethyl Parathion
31000 U * 310002700Famphur
31000 U 310003000Fluoranthene
31000 U 310003400Fluorene
31000 U 310003700Hexachlorobenzene
31000 U 310003400Hexachlorobutadiene
31000 U 310003800Hexachlorocyclopentadiene
31000 U 310002600Hexachloroethane
16000000 U * 160000001200000Hexachlorophene
31000 U * 310002700Hexachloropropene
31000 U 310002600Indeno[1,2,3-cd]pyrene
31000 U 310003100Isophorone
31000 U 310002200Isosafrole
6300000 U 630000078000Methapyrilene
31000 U 3100038003-Methylcholanthrene
31000 U * 310001600Methyl methanesulfonate
31000 U 3100036002-Methylnaphthalene
31000 U 310002400Methyl parathion
31000 U 3100025002-Methylphenol
31000 U 3100040003 & 4 Methylphenol
31000 U 310002800Naphthalene
31000 U * 3100016001,4-Naphthoquinone
31000 U * 3100062001-Naphthylamine
31000 U 3100032002-Naphthylamine
160000 U 16000042002-Nitroaniline
160000 U 16000043003-Nitroaniline
160000 U 16000046004-Nitroaniline
31000 U 310002400Nitrobenzene
31000 U 3100038002-Nitrophenol
160000 U 160000310004-Nitrophenol
310000 U 310000780004-Nitroquinoline-1-oxide
31000 U 310002400N-Nitro-o-toluidine
31000 U 310002600N-Nitrosodiethylamine
31000 U 3100011000N-Nitrosodimethylamine
31000 U 310002200N-Nitrosodi-n-butylamine
31000 U 310003000N-Nitrosodi-n-propylamine
31000 U 310003100N-Nitrosodiphenylamine
31000 U 310002300N-Nitrosomethylethylamine
TestAmerica Savannah Page 138 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-2-US
Client Matrix: % Moisture: 78.7
680-56861-23
Solid
Date Sampled: 04/16/2010 0930
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/20/2010 1628
04/23/2010 1826
1.0
8270C Analysis Batch: 680-166548
Prep Batch: 680-166138
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
n7044.d
30.10 g
20 mL
1 uL
3546
MSN
Analyte DryWt Corrected: Y Result (ug/Kg) Qualifier MDL RL
31000 U 310002500N-Nitrosomorpholine
31000 U 310002000N-Nitrosopiperidine
31000 U 310001700N-Nitrosopyrrolidine
31000 U 310003700o,o',o''-Triethylphosphorothioate
31000 U 310001800p-Dimethylamino azobenzene
31000 U 310002300Pentachlorobenzene
31000 U 310002000Pentachloronitrobenzene
160000 U 16000031000Pentachlorophenol
31000 U 310003100Phenacetin
31000 U 310002500Phenanthrene
31000 U 310003200Phenol
31000 U 310002100Phorate
31000 U 3100016002-Picoline
160000 U 16000078000p-Phenylene diamine
31000 U 310002200Pronamide
5000 J 310002500Pyrene
31000 U 310002700Pyridine
31000 U 310002200Safrole, Total
31000 U 310001900Sulfotepp
31000 U 3100029001,2,4,5-Tetrachlorobenzene
31000 U 3100021002,3,4,6-Tetrachlorophenol
31000 U 310002200Thionazin
31000 U 3100033002-Toluidine
31000 U 3100029001,2,4-Trichlorobenzene
31000 U 3100033002,4,5-Trichlorophenol
31000 U 3100027002,4,6-Trichlorophenol
31000 U 31000160001,3,5-Trinitrobenzene
160000 310003200Diphenyl ether
Surrogate %Rec Acceptance LimitsQualifier
0 34 - 130D2,4,6-Tribromophenol
0 34 - 130D2-Fluorobiphenyl
0 30 - 130D2-Fluorophenol
0 39 - 130DTerphenyl-d14
0 30 - 130DPhenol-d5
0 27 - 130DNitrobenzene-d5
TestAmerica Savannah Page 139 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
RB-1
Client Matrix:
680-56861-28RB
Water
Date Sampled: 04/16/2010 1000
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/21/2010 1423
04/25/2010 0023
1.0
8270C Analysis Batch: 680-166696
Prep Batch: 680-166243
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g0754.d
1060 mL
1 mL
1 uL
3520C
MSG
Analyte Result (ug/L) Qualifier MDL RL
9.4 U 9.40.72Acenaphthene
9.4 U 9.40.80Acenaphthylene
9.4 U 9.40.54Acetophenone
9.4 U 9.41.52-Acetylaminofluorene
1900 U * 190033alpha,alpha-Dimethyl phenethylamine
9.4 U 9.41.14-Aminobiphenyl
19 U 192.0Aniline
9.4 U 9.40.65Anthracene
9.4 U 9.40.86Aramite, Total
9.4 U 9.40.52Benzo[a]anthracene
9.4 U 9.40.67Benzo[a]pyrene
9.4 U 9.42.5Benzo[b]fluoranthene
9.4 U 9.40.82Benzo[g,h,i]perylene
9.4 U 9.41.1Benzo[k]fluoranthene
9.4 U 9.41.0Benzyl alcohol
9.4 U 9.40.551,1'-Biphenyl
9.4 U * 9.40.89Bis(2-chloroethoxy)methane
9.4 U 9.41.0Bis(2-chloroethyl)ether
9.4 U 9.40.74bis(chloroisopropyl) ether
9.4 U 9.41.5Bis(2-ethylhexyl) phthalate
9.4 U 9.40.734-Bromophenyl phenyl ether
9.4 U 9.41.1Butyl benzyl phthalate
19 U 192.14-Chloroaniline
9.4 U 9.40.944-Chloro-3-methylphenol
9.4 U 9.40.752-Chloronaphthalene
9.4 U 9.40.822-Chlorophenol
9.4 U 9.40.794-Chlorophenyl phenyl ether
9.4 U 9.40.48Chrysene
9.4 U 9.40.74Diallate
9.4 U 9.40.94Dibenz(a,h)anthracene
9.4 U 9.40.75Dibenzofuran
9.4 U 9.40.501,2-Dichlorobenzene
9.4 U 9.40.561,3-Dichlorobenzene
9.4 U 9.40.511,4-Dichlorobenzene
57 U 57283,3'-Dichlorobenzidine
9.4 U 9.41.02,4-Dichlorophenol
9.4 U 9.40.692,6-Dichlorophenol
9.4 U 9.40.83Diethyl phthalate
9.4 U 9.40.71Dimethoate
9.4 U 9.41.17,12-Dimethylbenz(a)anthracene
19 U 199.43,3'-Dimethylbenzidine
9.4 U 9.43.82,4-Dimethylphenol
9.4 U 9.40.93Dimethyl phthalate
9.4 U 9.40.78Di-n-butyl phthalate
9.4 U 9.40.571,3-Dinitrobenzene
47 U 479.44,6-Dinitro-2-methylphenol
TestAmerica Savannah Page 140 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
RB-1
Client Matrix:
680-56861-28RB
Water
Date Sampled: 04/16/2010 1000
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/21/2010 1423
04/25/2010 0023
1.0
8270C Analysis Batch: 680-166696
Prep Batch: 680-166243
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g0754.d
1060 mL
1 mL
1 uL
3520C
MSG
Analyte Result (ug/L) Qualifier MDL RL
47 U 479.42,4-Dinitrophenol
9.4 U 9.41.12,4-Dinitrotoluene
9.4 U 9.41.02,6-Dinitrotoluene
9.4 U 9.41.3Di-n-octyl phthalate
9.4 U 9.44.7Dinoseb
9.4 U 9.43.21,4-Dioxane
9.4 U 9.40.75Disulfoton
9.4 U 9.40.91Ethyl methanesulfonate
9.4 U 9.41.2Ethyl Parathion
9.4 U * 9.41.0Famphur
9.4 U 9.40.70Fluoranthene
9.4 U 9.40.91Fluorene
9.4 U 9.40.75Hexachlorobenzene
9.4 U 9.40.58Hexachlorobutadiene
9.4 U 9.42.4Hexachlorocyclopentadiene
9.4 U 9.40.72Hexachloroethane
4700 U 470025Hexachlorophene
9.4 U * 9.41.3Hexachloropropene
9.4 U 9.40.94Indeno[1,2,3-cd]pyrene
9.4 U 9.40.85Isophorone
9.4 U 9.40.47Isosafrole
1900 U * 19002.5Methapyrilene
9.4 U 9.41.33-Methylcholanthrene
9.4 U * 9.40.57Methyl methanesulfonate
9.4 U 9.40.742-Methylnaphthalene
9.4 U 9.40.83Methyl parathion
9.4 U 9.40.842-Methylphenol
9.4 U 9.41.23 & 4 Methylphenol
9.4 U 9.40.66Naphthalene
9.4 U * 9.40.581,4-Naphthoquinone
9.4 U * 9.41.01-Naphthylamine
9.4 U 9.41.42-Naphthylamine
47 U 471.22-Nitroaniline
47 U 474.73-Nitroaniline
47 U 474.74-Nitroaniline
9.4 U 9.40.69Nitrobenzene
9.4 U 9.40.722-Nitrophenol
47 U 471.84-Nitrophenol
19 U 199.44-Nitroquinoline-1-oxide
9.4 U 9.41.4N-Nitro-o-toluidine
9.4 U 9.40.88N-Nitrosodiethylamine
9.4 U 9.42.6N-Nitrosodimethylamine
9.4 U * 9.40.91N-Nitrosodi-n-butylamine
9.4 U 9.40.68N-Nitrosodi-n-propylamine
9.4 U 9.40.87N-Nitrosodiphenylamine
9.4 U 9.43.1N-Nitrosomethylethylamine
TestAmerica Savannah Page 141 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
RB-1
Client Matrix:
680-56861-28RB
Water
Date Sampled: 04/16/2010 1000
Date Received: 04/17/2010 1045
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Method:
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
04/21/2010 1423
04/25/2010 0023
1.0
8270C Analysis Batch: 680-166696
Prep Batch: 680-166243
Injection Volume:
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID:
g0754.d
1060 mL
1 mL
1 uL
3520C
MSG
Analyte Result (ug/L) Qualifier MDL RL
9.4 U 9.40.79N-Nitrosomorpholine
9.4 U 9.40.83N-Nitrosopiperidine
9.4 U 9.40.94N-Nitrosopyrrolidine
9.4 U * 9.40.94o,o',o''-Triethylphosphorothioate
9.4 U 9.40.75p-Dimethylamino azobenzene
9.4 U 9.40.49Pentachlorobenzene
9.4 U 9.40.74Pentachloronitrobenzene
47 U 471.9Pentachlorophenol
9.4 U 9.41.3Phenacetin
9.4 U 9.40.73Phenanthrene
9.4 U 9.40.78Phenol
9.4 U 9.40.82Phorate
9.4 U 9.41.32-Picoline
1900 U 19009.4p-Phenylene diamine
9.4 U 9.40.84Pronamide
9.4 U 9.40.59Pyrene
47 U 472.2Pyridine
9.4 U 9.40.75Safrole, Total
9.4 U 9.40.50Sulfotepp
9.4 U 9.40.721,2,4,5-Tetrachlorobenzene
9.4 U 9.40.682,3,4,6-Tetrachlorophenol
9.4 U 9.40.86Thionazin
9.4 U 9.41.32-Toluidine
9.4 U 9.40.531,2,4-Trichlorobenzene
9.4 U 9.41.12,4,5-Trichlorophenol
9.4 U 9.40.802,4,6-Trichlorophenol
9.4 U 9.41.91,3,5-Trinitrobenzene
Surrogate %Rec Acceptance LimitsQualifier
96 40 - 1392,4,6-Tribromophenol
78 50 - 1132-Fluorobiphenyl
73 36 - 1102-Fluorophenol
101 10 - 121Terphenyl-d14
77 38 - 116Phenol-d5
83 45 - 112Nitrobenzene-d5
TestAmerica Savannah Page 142 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-1-LS
Client Matrix: % Moisture: 53.4
680-56861-1
Solid
Date Sampled: 04/14/2010 0950
Date Received: 04/17/2010 1045
6010B Metals (ICP)
Method: 6010B Analysis Batch: 680-166538 Instrument ID:
Preparation: Prep Batch: 680-166337 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 1.10 g
Date Analyzed: 04/23/2010 0555 Final Weight/Volume: 100 mL
Date Prepared: 04/21/2010 1618
3050B
ICPD
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
1.5 J 3.91.2Arsenic
37 1.90.58Barium
0.24 J 0.970.19Cadmium
13 1.90.97Chromium
120 1.91.0Lead
4.9 U 4.91.9Selenium
0.30 J 1.90.19Silver
7471A Mercury (CVAA)
Method: 7471A Analysis Batch: 680-167080 Instrument ID:
Preparation: Prep Batch: 680-166757 Lab File ID: N/A
Dilution: 10 Initial Weight/Volume: 0.60 g
Date Analyzed: 04/28/2010 1852 Final Weight/Volume: 50 mL
Date Prepared: 04/26/2010 1523
7471A
LEEMAN1
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
3.8 0.360.15Mercury
TestAmerica Savannah Page 143 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-3-NS
Client Matrix: % Moisture: 21.3
680-56861-2
Solid
Date Sampled: 04/14/2010 1245
Date Received: 04/17/2010 1045
6010B Metals (ICP)
Method: 6010B Analysis Batch: 680-166538 Instrument ID:
Preparation: Prep Batch: 680-166337 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 1.20 g
Date Analyzed: 04/23/2010 0600 Final Weight/Volume: 100 mL
Date Prepared: 04/21/2010 1618
3050B
ICPD
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
2.1 U 2.10.62Arsenic
4.0 1.10.32Barium
0.53 U 0.530.11Cadmium
1.6 1.10.53Chromium
2.9 1.10.56Lead
2.6 U 2.61.1Selenium
1.1 U 1.10.10Silver
7471A Mercury (CVAA)
Method: 7471A Analysis Batch: 680-167080 Instrument ID:
Preparation: Prep Batch: 680-166757 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 0.53 g
Date Analyzed: 04/28/2010 1856 Final Weight/Volume: 50 mL
Date Prepared: 04/26/2010 1523
7471A
LEEMAN1
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
0.012 J 0.0240.0098Mercury
TestAmerica Savannah Page 144 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-3-LS
Client Matrix: % Moisture: 53.4
680-56861-3
Solid
Date Sampled: 04/14/2010 1255
Date Received: 04/17/2010 1045
6010B Metals (ICP)
Method: 6010B Analysis Batch: 680-166869 Instrument ID:
Preparation: Prep Batch: 680-166528 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 1.18 g
Date Analyzed: 04/26/2010 2134 Final Weight/Volume: 100 mL
Date Prepared: 04/23/2010 1017
3050B
ICPD
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
2.5 J 3.61.1Arsenic
22 1.80.55Barium
0.27 J 0.910.18Cadmium
16 1.80.91Chromium
41 1.80.96Lead
4.5 U 4.51.8Selenium
0.62 J B 1.80.17Silver
7471A Mercury (CVAA)
Method: 7471A Analysis Batch: 680-166898 Instrument ID:
Preparation: Prep Batch: 680-166534 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 0.58 g
Date Analyzed: 04/27/2010 1635 Final Weight/Volume: 50 mL
Date Prepared: 04/23/2010 1046
7471A
LEEMAN1
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
0.66 0.0370.015Mercury
TestAmerica Savannah Page 145 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-4-NS
Client Matrix: % Moisture: 12.4
680-56861-4
Solid
Date Sampled: 04/14/2010 1715
Date Received: 04/17/2010 1045
6010B Metals (ICP)
Method: 6010B Analysis Batch: 680-166869 Instrument ID:
Preparation: Prep Batch: 680-166528 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 1.12 g
Date Analyzed: 04/26/2010 2139 Final Weight/Volume: 100 mL
Date Prepared: 04/23/2010 1017
3050B
ICPD
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
2.0 U 2.00.60Arsenic
3.5 1.00.31Barium
0.51 U 0.510.10Cadmium
1.5 1.00.51Chromium
0.95 J 1.00.54Lead
2.5 U 2.51.0Selenium
0.10 J B 1.00.098Silver
7471A Mercury (CVAA)
Method: 7471A Analysis Batch: 680-166898 Instrument ID:
Preparation: Prep Batch: 680-166534 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 0.58 g
Date Analyzed: 04/27/2010 1638 Final Weight/Volume: 50 mL
Date Prepared: 04/23/2010 1046
7471A
LEEMAN1
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
0.020 U 0.0200.0081Mercury
TestAmerica Savannah Page 146 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-4-LS
Client Matrix: % Moisture: 60.5
680-56861-5
Solid
Date Sampled: 04/14/2010 1735
Date Received: 04/17/2010 1045
6010B Metals (ICP)
Method: 6010B Analysis Batch: 680-166869 Instrument ID:
Preparation: Prep Batch: 680-166528 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 1.08 g
Date Analyzed: 04/26/2010 2144 Final Weight/Volume: 100 mL
Date Prepared: 04/23/2010 1017
3050B
ICPD
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
2.1 J 4.71.4Arsenic
16 2.30.70Barium
0.40 J 1.20.23Cadmium
13 2.31.2Chromium
59 2.31.2Lead
5.9 U 5.92.3Selenium
0.41 J B 2.30.22Silver
7471A Mercury (CVAA)
Method: 7471A Analysis Batch: 680-166898 Instrument ID:
Preparation: Prep Batch: 680-166534 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 0.54 g
Date Analyzed: 04/27/2010 1641 Final Weight/Volume: 50 mL
Date Prepared: 04/23/2010 1046
7471A
LEEMAN1
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
0.26 0.0470.019Mercury
TestAmerica Savannah Page 147 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-3-US
Client Matrix: % Moisture: 75.7
680-56861-6
Solid
Date Sampled: 04/15/2010 0845
Date Received: 04/17/2010 1045
6010B Metals (ICP)
Method: 6010B Analysis Batch: 680-166869 Instrument ID:
Preparation: Prep Batch: 680-166528 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 1.07 g
Date Analyzed: 04/26/2010 2149 Final Weight/Volume: 100 mL
Date Prepared: 04/23/2010 1017
3050B
ICPD
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
2.8 J 7.72.3Arsenic
13 3.81.2Barium
0.38 J 1.90.38Cadmium
11 3.81.9Chromium
40 3.82.0Lead
9.6 U 9.63.8Selenium
3.8 U 3.80.37Silver
7471A Mercury (CVAA)
Method: 7471A Analysis Batch: 680-166898 Instrument ID:
Preparation: Prep Batch: 680-166534 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 0.52 g
Date Analyzed: 04/27/2010 1644 Final Weight/Volume: 50 mL
Date Prepared: 04/23/2010 1046
7471A
LEEMAN1
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
0.24 0.0790.032Mercury
TestAmerica Savannah Page 148 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-5-NS
Client Matrix: % Moisture: 23.8
680-56861-7
Solid
Date Sampled: 04/15/2010 0950
Date Received: 04/17/2010 1045
6010B Metals (ICP)
Method: 6010B Analysis Batch: 680-166869 Instrument ID:
Preparation: Prep Batch: 680-166528 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 1.11 g
Date Analyzed: 04/26/2010 2155 Final Weight/Volume: 100 mL
Date Prepared: 04/23/2010 1017
3050B
ICPD
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
2.0 J 2.40.70Arsenic
120 1.20.35Barium
0.18 J 0.590.12Cadmium
18 1.20.59Chromium
12 1.20.63Lead
3.0 U 3.01.2Selenium
0.15 J B 1.20.11Silver
7471A Mercury (CVAA)
Method: 7471A Analysis Batch: 680-166898 Instrument ID:
Preparation: Prep Batch: 680-166534 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 0.54 g
Date Analyzed: 04/27/2010 1647 Final Weight/Volume: 50 mL
Date Prepared: 04/23/2010 1046
7471A
LEEMAN1
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
0.024 U 0.0240.010Mercury
TestAmerica Savannah Page 149 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-5-LS
Client Matrix: % Moisture: 68.0
680-56861-8
Solid
Date Sampled: 04/15/2010 1005
Date Received: 04/17/2010 1045
6010B Metals (ICP)
Method: 6010B Analysis Batch: 680-166869 Instrument ID:
Preparation: Prep Batch: 680-166528 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 1.18 g
Date Analyzed: 04/26/2010 2200 Final Weight/Volume: 100 mL
Date Prepared: 04/23/2010 1017
3050B
ICPD
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
2.5 J 5.31.6Arsenic
23 2.60.79Barium
0.55 J 1.30.26Cadmium
24 2.61.3Chromium
75 2.61.4Lead
6.6 U 6.62.6Selenium
0.42 J B 2.60.25Silver
7471A Mercury (CVAA)
Method: 7471A Analysis Batch: 680-166898 Instrument ID:
Preparation: Prep Batch: 680-166534 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 0.59 g
Date Analyzed: 04/27/2010 1650 Final Weight/Volume: 50 mL
Date Prepared: 04/23/2010 1046
7471A
LEEMAN1
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
0.40 0.0530.022Mercury
TestAmerica Savannah Page 150 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-4-US
Client Matrix: % Moisture: 77.8
680-56861-9
Solid
Date Sampled: 04/15/2010 1100
Date Received: 04/17/2010 1045
6010B Metals (ICP)
Method: 6010B Analysis Batch: 680-166869 Instrument ID:
Preparation: Prep Batch: 680-166528 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 1.09 g
Date Analyzed: 04/26/2010 2205 Final Weight/Volume: 100 mL
Date Prepared: 04/23/2010 1017
3050B
ICPD
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
3.3 J 8.32.4Arsenic
27 4.11.2Barium
0.77 J 2.10.41Cadmium
23 4.12.1Chromium
49 4.12.2Lead
10 U 104.1Selenium
0.42 J B 4.10.40Silver
7471A Mercury (CVAA)
Method: 7471A Analysis Batch: 680-166898 Instrument ID:
Preparation: Prep Batch: 680-166534 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 0.59 g
Date Analyzed: 04/27/2010 1653 Final Weight/Volume: 50 mL
Date Prepared: 04/23/2010 1046
7471A
LEEMAN1
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
1.1 0.0760.031Mercury
TestAmerica Savannah Page 151 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-6-NS
Client Matrix: % Moisture: 20.4
680-56861-10
Solid
Date Sampled: 04/15/2010 1105
Date Received: 04/17/2010 1045
6010B Metals (ICP)
Method: 6010B Analysis Batch: 680-166869 Instrument ID:
Preparation: Prep Batch: 680-166528 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 1.06 g
Date Analyzed: 04/26/2010 2210 Final Weight/Volume: 100 mL
Date Prepared: 04/23/2010 1017
3050B
ICPD
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
2.0 J 2.40.70Arsenic
150 1.20.36Barium
0.59 U 0.590.12Cadmium
13 1.20.59Chromium
7.6 1.20.63Lead
3.0 U 3.01.2Selenium
1.2 U 1.20.11Silver
7471A Mercury (CVAA)
Method: 7471A Analysis Batch: 680-166898 Instrument ID:
Preparation: Prep Batch: 680-166534 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 0.59 g
Date Analyzed: 04/27/2010 1655 Final Weight/Volume: 50 mL
Date Prepared: 04/23/2010 1046
7471A
LEEMAN1
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
0.021 U 0.0210.0087Mercury
TestAmerica Savannah Page 152 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-6-LS
Client Matrix: % Moisture: 59.4
680-56861-11
Solid
Date Sampled: 04/15/2010 1110
Date Received: 04/17/2010 1045
6010B Metals (ICP)
Method: 6010B Analysis Batch: 680-166869 Instrument ID:
Preparation: Prep Batch: 680-166528 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 1.15 g
Date Analyzed: 04/26/2010 2226 Final Weight/Volume: 100 mL
Date Prepared: 04/23/2010 1017
3050B
ICPD
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
1.3 J 4.31.3Arsenic
16 2.10.64Barium
0.31 J 1.10.21Cadmium
17 2.11.1Chromium
51 2.11.1Lead
5.3 U 5.32.1Selenium
0.53 J B 2.10.21Silver
7471A Mercury (CVAA)
Method: 7471A Analysis Batch: 680-166898 Instrument ID:
Preparation: Prep Batch: 680-166534 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 0.51 g
Date Analyzed: 04/27/2010 1659 Final Weight/Volume: 50 mL
Date Prepared: 04/23/2010 1046
7471A
LEEMAN1
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
0.43 0.0480.020Mercury
TestAmerica Savannah Page 153 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-5-US
Client Matrix: % Moisture: 82.7
680-56861-12
Solid
Date Sampled: 04/15/2010 1145
Date Received: 04/17/2010 1045
6010B Metals (ICP)
Method: 6010B Analysis Batch: 680-166869 Instrument ID:
Preparation: Prep Batch: 680-166528 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 1.11 g
Date Analyzed: 04/26/2010 2231 Final Weight/Volume: 100 mL
Date Prepared: 04/23/2010 1017
3050B
ICPD
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
3.6 J 103.1Arsenic
18 5.21.6Barium
0.52 J 2.60.52Cadmium
27 5.22.6Chromium
28 5.22.8Lead
13 U 135.2Selenium
5.2 U 5.20.50Silver
7471A Mercury (CVAA)
Method: 7471A Analysis Batch: 680-166898 Instrument ID:
Preparation: Prep Batch: 680-166534 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 0.55 g
Date Analyzed: 04/27/2010 1701 Final Weight/Volume: 50 mL
Date Prepared: 04/23/2010 1046
7471A
LEEMAN1
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
0.25 0.110.043Mercury
TestAmerica Savannah Page 154 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-6-US
Client Matrix: % Moisture: 82.7
680-56861-13
Solid
Date Sampled: 04/15/2010 1415
Date Received: 04/17/2010 1045
6010B Metals (ICP)
Method: 6010B Analysis Batch: 680-166869 Instrument ID:
Preparation: Prep Batch: 680-166528 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 1.07 g
Date Analyzed: 04/26/2010 2236 Final Weight/Volume: 100 mL
Date Prepared: 04/23/2010 1017
3050B
ICPD
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
3.4 J 113.2Arsenic
18 5.41.6Barium
0.61 J 2.70.54Cadmium
15 5.42.7Chromium
43 5.42.9Lead
14 U 145.4Selenium
0.52 J B 5.40.52Silver
7471A Mercury (CVAA)
Method: 7471A Analysis Batch: 680-166898 Instrument ID:
Preparation: Prep Batch: 680-166534 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 0.60 g
Date Analyzed: 04/27/2010 1710 Final Weight/Volume: 50 mL
Date Prepared: 04/23/2010 1046
7471A
LEEMAN1
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
0.33 0.0970.040Mercury
TestAmerica Savannah Page 155 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-7-NS
Client Matrix: % Moisture: 16.9
680-56861-14
Solid
Date Sampled: 04/15/2010 1505
Date Received: 04/17/2010 1045
6010B Metals (ICP)
Method: 6010B Analysis Batch: 680-166869 Instrument ID:
Preparation: Prep Batch: 680-166528 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 1.16 g
Date Analyzed: 04/26/2010 2241 Final Weight/Volume: 100 mL
Date Prepared: 04/23/2010 1017
3050B
ICPD
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
2.1 U 2.10.61Arsenic
18 1.00.31Barium
0.52 U 0.520.10Cadmium
7.3 1.00.52Chromium
2.6 1.00.55Lead
2.6 U 2.61.0Selenium
1.0 U 1.00.10Silver
7471A Mercury (CVAA)
Method: 7471A Analysis Batch: 680-166898 Instrument ID:
Preparation: Prep Batch: 680-166534 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 0.53 g
Date Analyzed: 04/27/2010 1444 Final Weight/Volume: 50 mL
Date Prepared: 04/23/2010 1046
7471A
LEEMAN1
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
0.023 U 0.0230.0093Mercury
TestAmerica Savannah Page 156 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-7-LS
Client Matrix: % Moisture: 70.7
680-56861-15
Solid
Date Sampled: 04/15/2010 1520
Date Received: 04/17/2010 1045
6010B Metals (ICP)
Method: 6010B Analysis Batch: 680-167105 Instrument ID:
Preparation: Prep Batch: 680-166825 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 1.13 g
Date Analyzed: 04/28/2010 2232 Final Weight/Volume: 100 mL
Date Prepared: 04/27/2010 0909
3050B
ICPD
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
3.1 J 6.01.8Arsenic
18 3.00.91Barium
0.47 J 1.50.30Cadmium
31 3.01.5Chromium
27 3.01.6Lead
7.5 U 7.53.0Selenium
0.30 J 3.00.29Silver
7471A Mercury (CVAA)
Method: 7471A Analysis Batch: 680-167080 Instrument ID:
Preparation: Prep Batch: 680-166757 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 0.56 g
Date Analyzed: 04/28/2010 1859 Final Weight/Volume: 50 mL
Date Prepared: 04/26/2010 1523
7471A
LEEMAN1
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
0.52 0.0610.025Mercury
TestAmerica Savannah Page 157 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-7-US
Client Matrix: % Moisture: 73.7
680-56861-16
Solid
Date Sampled: 04/15/2010 1525
Date Received: 04/17/2010 1045
6010B Metals (ICP)
Method: 6010B Analysis Batch: 680-167105 Instrument ID:
Preparation: Prep Batch: 680-166825 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 1.07 g
Date Analyzed: 04/28/2010 2237 Final Weight/Volume: 100 mL
Date Prepared: 04/27/2010 0909
3050B
ICPD
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
2.6 J 7.12.1Arsenic
12 3.61.1Barium
0.48 J 1.80.36Cadmium
24 3.61.8Chromium
32 3.61.9Lead
8.9 U 8.93.6Selenium
3.6 U 3.60.34Silver
7471A Mercury (CVAA)
Method: 7471A Analysis Batch: 680-167080 Instrument ID:
Preparation: Prep Batch: 680-166757 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 0.55 g
Date Analyzed: 04/28/2010 1901 Final Weight/Volume: 50 mL
Date Prepared: 04/26/2010 1523
7471A
LEEMAN1
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
0.59 0.0690.028Mercury
TestAmerica Savannah Page 158 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-8-NS
Client Matrix: % Moisture: 27.7
680-56861-17
Solid
Date Sampled: 04/15/2010 1600
Date Received: 04/17/2010 1045
6010B Metals (ICP)
Method: 6010B Analysis Batch: 680-167105 Instrument ID:
Preparation: Prep Batch: 680-166825 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 1.13 g
Date Analyzed: 04/28/2010 2242 Final Weight/Volume: 100 mL
Date Prepared: 04/27/2010 0909
3050B
ICPD
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
1.1 J 2.40.72Arsenic
120 1.20.37Barium
0.61 U 0.610.12Cadmium
15 1.20.61Chromium
13 1.20.65Lead
3.1 U 3.11.2Selenium
1.2 U 1.20.12Silver
7471A Mercury (CVAA)
Method: 7471A Analysis Batch: 680-167080 Instrument ID:
Preparation: Prep Batch: 680-166757 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 0.62 g
Date Analyzed: 04/28/2010 1910 Final Weight/Volume: 50 mL
Date Prepared: 04/26/2010 1523
7471A
LEEMAN1
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
0.022 U 0.0220.0091Mercury
TestAmerica Savannah Page 159 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-8-LS
Client Matrix: % Moisture: 75.4
680-56861-18
Solid
Date Sampled: 04/15/2010 1615
Date Received: 04/17/2010 1045
6010B Metals (ICP)
Method: 6010B Analysis Batch: 680-167105 Instrument ID:
Preparation: Prep Batch: 680-166825 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 1.04 g
Date Analyzed: 04/28/2010 2247 Final Weight/Volume: 100 mL
Date Prepared: 04/27/2010 0909
3050B
ICPD
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
3.3 J 7.82.3Arsenic
37 3.91.2Barium
0.67 J 2.00.39Cadmium
54 3.92.0Chromium
100 3.92.1Lead
9.8 U 9.83.9Selenium
0.51 J 3.90.38Silver
7471A Mercury (CVAA)
Method: 7471A Analysis Batch: 680-167080 Instrument ID:
Preparation: Prep Batch: 680-166757 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 0.64 g
Date Analyzed: 04/28/2010 1913 Final Weight/Volume: 50 mL
Date Prepared: 04/26/2010 1523
7471A
LEEMAN1
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
0.86 0.0640.026Mercury
TestAmerica Savannah Page 160 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-8-US
Client Matrix: % Moisture: 86.3
680-56861-19
Solid
Date Sampled: 04/15/2010 1620
Date Received: 04/17/2010 1045
6010B Metals (ICP)
Method: 6010B Analysis Batch: 680-167105 Instrument ID:
Preparation: Prep Batch: 680-166825 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 1.01 g
Date Analyzed: 04/28/2010 2252 Final Weight/Volume: 100 mL
Date Prepared: 04/27/2010 0909
3050B
ICPD
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
14 U 144.3Arsenic
15 7.22.2Barium
3.6 U 3.60.72Cadmium
23 7.23.6Chromium
38 7.23.8Lead
18 U 187.2Selenium
7.2 U 7.20.69Silver
7471A Mercury (CVAA)
Method: 7471A Analysis Batch: 680-167080 Instrument ID:
Preparation: Prep Batch: 680-166757 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 0.55 g
Date Analyzed: 04/28/2010 1916 Final Weight/Volume: 50 mL
Date Prepared: 04/26/2010 1523
7471A
LEEMAN1
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
0.48 0.130.054Mercury
TestAmerica Savannah Page 161 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-1-US
Client Matrix: % Moisture: 62.6
680-56861-20
Solid
Date Sampled: 04/15/2010 1700
Date Received: 04/17/2010 1045
6010B Metals (ICP)
Method: 6010B Analysis Batch: 680-167105 Instrument ID:
Preparation: Prep Batch: 680-166825 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 1.15 g
Date Analyzed: 04/28/2010 2258 Final Weight/Volume: 100 mL
Date Prepared: 04/27/2010 0909
3050B
ICPD
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
3.0 J 4.71.4Arsenic
28 2.30.70Barium
0.33 J 1.20.23Cadmium
22 2.31.2Chromium
24 2.31.2Lead
5.8 U 5.82.3Selenium
0.24 J 2.30.22Silver
7471A Mercury (CVAA)
Method: 7471A Analysis Batch: 680-167080 Instrument ID:
Preparation: Prep Batch: 680-166757 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 0.56 g
Date Analyzed: 04/28/2010 1919 Final Weight/Volume: 50 mL
Date Prepared: 04/26/2010 1523
7471A
LEEMAN1
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
0.72 0.0480.020Mercury
TestAmerica Savannah Page 162 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-2-NS
Client Matrix: % Moisture: 14.5
680-56861-21
Solid
Date Sampled: 04/16/2010 0840
Date Received: 04/17/2010 1045
6010B Metals (ICP)
Method: 6010B Analysis Batch: 680-167105 Instrument ID:
Preparation: Prep Batch: 680-166825 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 1.10 g
Date Analyzed: 04/28/2010 2303 Final Weight/Volume: 100 mL
Date Prepared: 04/27/2010 0909
3050B
ICPD
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
2.1 U 2.10.63Arsenic
4.2 1.10.32Barium
0.53 U 0.530.11Cadmium
1.1 U 1.10.53Chromium
1.7 1.10.56Lead
2.7 U 2.71.1Selenium
1.1 U 1.10.10Silver
7471A Mercury (CVAA)
Method: 7471A Analysis Batch: 680-167080 Instrument ID:
Preparation: Prep Batch: 680-166757 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 0.56 g
Date Analyzed: 04/28/2010 1922 Final Weight/Volume: 50 mL
Date Prepared: 04/26/2010 1523
7471A
LEEMAN1
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
0.012 J 0.0210.0086Mercury
TestAmerica Savannah Page 163 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-2-LS
Client Matrix: % Moisture: 66.8
680-56861-22
Solid
Date Sampled: 04/16/2010 0850
Date Received: 04/17/2010 1045
6010B Metals (ICP)
Method: 6010B Analysis Batch: 680-167105 Instrument ID:
Preparation: Prep Batch: 680-166825 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 1.13 g
Date Analyzed: 04/28/2010 2308 Final Weight/Volume: 100 mL
Date Prepared: 04/27/2010 0909
3050B
ICPD
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
3.4 J 5.31.6Arsenic
39 2.70.80Barium
0.46 J 1.30.27Cadmium
23 2.71.3Chromium
41 2.71.4Lead
6.7 U 6.72.7Selenium
0.88 J 2.70.26Silver
7471A Mercury (CVAA)
Method: 7471A Analysis Batch: 680-167080 Instrument ID:
Preparation: Prep Batch: 680-166757 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 0.51 g
Date Analyzed: 04/28/2010 1925 Final Weight/Volume: 50 mL
Date Prepared: 04/26/2010 1523
7471A
LEEMAN1
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
1.1 0.0590.024Mercury
TestAmerica Savannah Page 164 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
IBS-2-US
Client Matrix: % Moisture: 78.7
680-56861-23
Solid
Date Sampled: 04/16/2010 0930
Date Received: 04/17/2010 1045
6010B Metals (ICP)
Method: 6010B Analysis Batch: 680-167105 Instrument ID:
Preparation: Prep Batch: 680-166825 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 1.12 g
Date Analyzed: 04/28/2010 2324 Final Weight/Volume: 100 mL
Date Prepared: 04/27/2010 0909
3050B
ICPD
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
2.5 J 8.42.5Arsenic
23 4.21.3Barium
0.51 J 2.10.42Cadmium
19 4.22.1Chromium
36 4.22.2Lead
10 U 104.2Selenium
4.2 U 4.20.40Silver
7471A Mercury (CVAA)
Method: 7471A Analysis Batch: 680-167080 Instrument ID:
Preparation: Prep Batch: 680-166757 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 0.56 g
Date Analyzed: 04/28/2010 1928 Final Weight/Volume: 50 mL
Date Prepared: 04/26/2010 1523
7471A
LEEMAN1
Analyte DryWt Corrected: Y Result (mg/Kg) Qualifier MDL RL
1.1 0.0840.034Mercury
TestAmerica Savannah Page 165 of 238
Analytical Data
Client: Ashland Inc. Job Number: 680-56861-1
Client Sample ID:
Lab Sample ID:
RB-1
Client Matrix:
680-56861-28RB
Water
Date Sampled: 04/16/2010 1000
Date Received: 04/17/2010 1045
6010B Metals (ICP)
Method: 6010B Analysis Batch: 680-166320 Instrument ID:
Preparation: Prep Batch: 680-166297 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 50 mL
Date Analyzed: 04/21/2010 2034 Final Weight/Volume: 50 mL
Date Prepared: 04/21/2010 1215
3010A
ICPD
Analyte Result (ug/L) Qualifier MDL RL
20 U 204.6Arsenic
2.8 J 102.3Barium
5.0 U 5.02.0Cadmium
10 U 101.2Chromium
10 U 104.0Lead
20 U 206.4Selenium
10 U 100.89Silver
7470A Mercury (CVAA)
Method: 7470A Analysis Batch: 680-166435 Instrument ID:
Preparation: Prep Batch: 680-166268 Lab File ID: N/A
Dilution: 1.0 Initial Weight/Volume: 50 mL
Date Analyzed: 04/22/2010 1230 Final Weight/Volume: 50 mL
Date Prepared: 04/21/2010 1021
7470A
LEEMAN1
Analyte Result (ug/L) Qualifier MDL RL
0.20 U 0.200.091Mercury
TestAmerica Savannah Page 166 of 238
DATA REPORTING QUALIFIERS
Client: Ashland Inc. Job Number: 680-56861-1
Lab Section Qualifier Description
GC/MS VOA
Indicates the analyte was analyzed for but not detected.U
LCS or LCSD exceeds the control limits*
Result is less than the RL but greater than or equal to the MDL
and the concentration is an approximate value.
J
Surrogate is outside control limitsX
Surrogate or matrix spike recoveries were not obtained
because the extract was diluted for analysis; also compounds
analyzed at a dilution may be flagged with a D.
D
GC/MS Semi VOA
Indicates the analyte was analyzed for but not detected.U
LCS or LCSD exceeds the control limits*
MS or MSD exceeds the control limitsF
MS, MSD: The analyte present in the original sample is 4 times
greater than the matrix spike concentration; therefore, control
limits are not applicable.
4
Result exceeded calibration range.E
Result is less than the RL but greater than or equal to the MDL
and the concentration is an approximate value.
J
RPD of the LCS and LCSD exceeds the control limits*
Surrogate or matrix spike recoveries were not obtained
because the extract was diluted for analysis; also compounds
analyzed at a dilution may be flagged with a D.
D
Metals
Compound was found in the blank and sample.B
Indicates the analyte was analyzed for but not detected.U
Result is less than the RL but greater than or equal to the MDL
and the concentration is an approximate value.
J
TestAmerica Savannah
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QUALITY CONTROL RESULTS
TestAmerica Savannah
Page 168 of 238
Quality Control Results
Client: Ashland Inc. Job Number: 680-56861-1
QC Association Summary
Lab Sample ID Client Sample ID Client Matrix Method Prep Batch
Report
Basis
GC/MS VOA
Prep Batch: 680-166108
SolidIBS-1-LS 5035680-56861-1 T
SolidIBS-3-NS 5035680-56861-2 T
SolidIBS-3-LS 5035680-56861-3 T
SolidIBS-4-NS 5035680-56861-4 T
SolidIBS-4-LS 5035680-56861-5 T
SolidIBS-3-US 5035680-56861-6 T
SolidIBS-5-LS 5035680-56861-8 T
SolidIBS-4-US 5035680-56861-9 T
SolidIBS-6-NS 5035680-56861-10 T
SolidIBS-6-LS 5035680-56861-11 T
SolidIBS-5-US 5035680-56861-12 T
SolidIBS-6-US 5035680-56861-13 T
SolidIBS-7-NS 5035680-56861-14 T
SolidIBS-7-LS 5035680-56861-15 T
SolidIBS-7-US 5035680-56861-16 T
SolidIBS-8-NS 5035680-56861-17 T
SolidIBS-8-LS 5035680-56861-18 T
SolidIBS-8-US 5035680-56861-19 T
SolidIBS-1-US 5035680-56861-20 T
SolidIBS-2-NS 5035680-56861-21 T
SolidIBS-2-LS 5035680-56861-22 T
SolidIBS-2-US 5035680-56861-23 T
Analysis Batch:680-166185
Lab Control Sample Water 8260BLCS 680-166185/6 T
Lab Control Sample Duplicate Water 8260BLCSD 680-166185/7 T
Method Blank Water 8260BMB 680-166185/9 T
WaterFB-1 8260B680-56861-24FB T
WaterFB-2 8260B680-56861-25FB T
WaterTB-1 8260B680-56861-26TB T
WaterTB-2 8260B680-56861-27TB T
WaterRB-1 8260B680-56861-28RB T
Analysis Batch:680-166615
Lab Control Sample Solid 8260BLCS 680-166615/6 T
Lab Control Sample Duplicate Solid 8260BLCSD 680-166615/7 T
Method Blank Solid 8260BMB 680-166615/8 T
Solid 680-166108IBS-4-US 8260B680-56861-9 T
TestAmerica Savannah
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Quality Control Results
Client: Ashland Inc. Job Number: 680-56861-1
QC Association Summary
Lab Sample ID Client Sample ID Client Matrix Method Prep Batch
Report
Basis
GC/MS VOA
Analysis Batch:680-166686
Lab Control Sample Solid 8260BLCS 680-166686/6 T
Lab Control Sample Duplicate Solid 8260BLCSD 680-166686/7 T
Method Blank Solid 8260BMB 680-166686/8 T
Solid 680-166108IBS-1-LS 8260B680-56861-1 T
Solid 680-166108IBS-3-NS 8260B680-56861-2 T
Solid 680-166108IBS-4-NS 8260B680-56861-4 T
Solid 680-166108IBS-3-US 8260B680-56861-6 T
SolidIBS-5-NS 8260B680-56861-7 T
Solid 680-166108IBS-6-NS 8260B680-56861-10 T
Solid 680-166108IBS-6-US 8260B680-56861-13 T
Solid 680-166108IBS-7-LS 8260B680-56861-15 T
Solid 680-166108IBS-7-US 8260B680-56861-16 T
Analysis Batch:680-166737
Lab Control Sample Solid 8260BLCS 680-166737/6 T
Lab Control Sample Duplicate Solid 8260BLCSD 680-166737/7 T
Method Blank Solid 8260BMB 680-166737/8 T
Solid 680-166108IBS-5-LS 8260B680-56861-8 T
Solid 680-166108IBS-5-US 8260B680-56861-12 T
Solid 680-166108IBS-7-NS 8260B680-56861-14 T
Solid 680-166108IBS-8-US 8260B680-56861-19 T
Solid 680-166108IBS-1-US 8260B680-56861-20 T
Solid 680-166108IBS-2-NS 8260B680-56861-21 T
Solid 680-166108IBS-2-LS 8260B680-56861-22 T
Solid 680-166108IBS-2-US 8260B680-56861-23 T
Analysis Batch:680-166861
Lab Control Sample Solid 8260BLCS 680-166861/7 T
Lab Control Sample Duplicate Solid 8260BLCSD 680-166861/8 T
Method Blank Solid 8260BMB 680-166861/9 T
Solid 680-166108IBS-3-LS 8260B680-56861-3 T
Solid 680-166108IBS-4-LS 8260B680-56861-5 T
Solid 680-166108IBS-6-LS 8260B680-56861-11 T
Solid 680-166108IBS-8-NS 8260B680-56861-17 T
Solid 680-166108IBS-8-LS 8260B680-56861-18 T
Report Basis
T = Total
TestAmerica Savannah
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Quality Control Results
Client: Ashland Inc. Job Number: 680-56861-1
QC Association Summary
Lab Sample ID Client Sample ID Client Matrix Method Prep Batch
Report
Basis
GC/MS Semi VOA
Prep Batch: 680-166138
Lab Control Sample Solid 3546LCS 680-166138/12-A T
SolidIBS-2-NS 3546680-56861-21 T
Matrix Spike Solid 3546680-56861-21MS T
Matrix Spike Duplicate Solid 3546680-56861-21MSD T
SolidIBS-2-LS 3546680-56861-22 T
SolidIBS-2-US 3546680-56861-23 T
Prep Batch: 680-166147
Lab Control Sample Solid 3546LCS 680-166147/22-A T
Method Blank Solid 3546MB 680-166147/21-A T
SolidIBS-1-LS 3546680-56861-1 T
SolidIBS-3-NS 3546680-56861-2 T
SolidIBS-3-LS 3546680-56861-3 T
SolidIBS-4-NS 3546680-56861-4 T
SolidIBS-4-LS 3546680-56861-5 T
SolidIBS-3-US 3546680-56861-6 T
SolidIBS-5-NS 3546680-56861-7 T
SolidIBS-5-LS 3546680-56861-8 T
SolidIBS-4-US 3546680-56861-9 T
SolidIBS-6-NS 3546680-56861-10 T
SolidIBS-6-LS 3546680-56861-11 T
SolidIBS-5-US 3546680-56861-12 T
SolidIBS-6-US 3546680-56861-13 T
SolidIBS-7-NS 3546680-56861-14 T
SolidIBS-7-LS 3546680-56861-15 T
SolidIBS-7-US 3546680-56861-16 T
SolidIBS-8-NS 3546680-56861-17 T
SolidIBS-8-LS 3546680-56861-18 T
SolidIBS-8-US 3546680-56861-19 T
SolidIBS-1-US 3546680-56861-20 T
Prep Batch: 680-166243
Lab Control Sample Water 3520CLCS 680-166243/8-A T
Lab Control Sample Duplicate Water 3520CLCSD 680-166243/9-A T
Method Blank Water 3520CMB 680-166243/7-A T
WaterRB-1 3520C680-56861-28RB T
Analysis Batch:680-166547
Lab Control Sample Solid 680-1661388270CLCS 680-166138/12-A T
Analysis Batch:680-166548
Solid 680-166138IBS-2-US 8270C680-56861-23 T
Analysis Batch:680-166687
Lab Control Sample Water 680-1662438270CLCS 680-166243/8-A T
TestAmerica Savannah
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Quality Control Results
Client: Ashland Inc. Job Number: 680-56861-1
QC Association Summary
Lab Sample ID Client Sample ID Client Matrix Method Prep Batch
Report
Basis
GC/MS Semi VOA
Analysis Batch:680-166695
Lab Control Sample Duplicate Water 680-1662438270CLCSD 680-166243/9-A T
Method Blank Water 680-1662438270CMB 680-166243/7-A T
Analysis Batch:680-166696
Water 680-166243RB-1 8270C680-56861-28RB T
Analysis Batch:680-167447
Lab Control Sample Solid 680-1661478270CLCS 680-166147/22-A T
Method Blank Solid 680-1661478270CMB 680-166147/21-A T
Solid 680-166147IBS-1-LS 8270C680-56861-1 T
Solid 680-166147IBS-3-NS 8270C680-56861-2 T
Solid 680-166147IBS-3-LS 8270C680-56861-3 T
Solid 680-166147IBS-4-LS 8270C680-56861-5 T
Solid 680-166147IBS-3-US 8270C680-56861-6 T
Solid 680-166147IBS-5-NS 8270C680-56861-7 T
Solid 680-166147IBS-5-LS 8270C680-56861-8 T
Solid 680-166147IBS-4-US 8270C680-56861-9 T
Analysis Batch:680-167473
Solid 680-166147IBS-4-NS 8270C680-56861-4 T
Solid 680-166147IBS-6-NS 8270C680-56861-10 T
Solid 680-166147IBS-6-LS 8270C680-56861-11 T
Solid 680-166147IBS-5-US 8270C680-56861-12 T
Solid 680-166147IBS-6-US 8270C680-56861-13 T
Solid 680-166147IBS-7-NS 8270C680-56861-14 T
Solid 680-166147IBS-7-LS 8270C680-56861-15 T
Solid 680-166147IBS-7-US 8270C680-56861-16 T
Solid 680-166147IBS-8-NS 8270C680-56861-17 T
Solid 680-166147IBS-8-LS 8270C680-56861-18 T
Solid 680-166147IBS-8-US 8270C680-56861-19 T
Solid 680-166147IBS-1-US 8270C680-56861-20 T
Solid 680-166138IBS-2-NS 8270C680-56861-21 T
Matrix Spike Solid 680-1661388270C680-56861-21MS T
Matrix Spike Duplicate Solid 680-1661388270C680-56861-21MSD T
Solid 680-166138IBS-2-LS 8270C680-56861-22 T
Analysis Batch:680-167967
Solid 680-166147IBS-1-LS 8270C680-56861-1 T
Solid 680-166147IBS-3-NS 8270C680-56861-2 T
Solid 680-166147IBS-3-LS 8270C680-56861-3 T
Solid 680-166147IBS-4-NS 8270C680-56861-4 T
Solid 680-166147IBS-4-LS 8270C680-56861-5 T
Solid 680-166147IBS-5-LS 8270C680-56861-8 T
Solid 680-166147IBS-6-NS 8270C680-56861-10 T
TestAmerica Savannah
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Quality Control Results
Client: Ashland Inc. Job Number: 680-56861-1
QC Association Summary
Lab Sample ID Client Sample ID Client Matrix Method Prep Batch
Report
Basis
Report Basis
T = Total
TestAmerica Savannah
Page 173 of 238
Quality Control Results
Client: Ashland Inc. Job Number: 680-56861-1
QC Association Summary
Lab Sample ID Client Sample ID Client Matrix Method Prep Batch
Report
Basis
Metals
Prep Batch: 680-166268
Lab Control Sample Water 7470ALCS 680-166266/7-B T
Method Blank Water 7470AMB 680-166266/6-B T
WaterRB-1 7470A680-56861-28RB T
Matrix Spike Water 7470A680-56861-28MS T
Matrix Spike Duplicate Water 7470A680-56861-28MSD T
Prep Batch: 680-166297
Lab Control Sample Water 3010ALCS 680-166297/19-A T
Method Blank Water 3010AMB 680-166297/18-A T
WaterRB-1 3010A680-56861-28RB T
Analysis Batch:680-166320
Lab Control Sample Water 680-1662976010BLCS 680-166297/19-A T
Method Blank Water 680-1662976010BMB 680-166297/18-A T
Water 680-166297RB-1 6010B680-56861-28RB T
Prep Batch: 680-166337
Lab Control Sample Solid 3050BLCS 680-166337/24-A T
Method Blank Solid 3050BMB 680-166337/23-A T
SolidIBS-1-LS 3050B680-56861-1 T
SolidIBS-3-NS 3050B680-56861-2 T
Analysis Batch:680-166435
Lab Control Sample Water 680-1662687470ALCS 680-166266/7-B T
Method Blank Water 680-1662687470AMB 680-166266/6-B T
Water 680-166268RB-1 7470A680-56861-28RB T
Matrix Spike Water 680-1662687470A680-56861-28MS T
Matrix Spike Duplicate Water 680-1662687470A680-56861-28MSD T
TestAmerica Savannah
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Quality Control Results
Client: Ashland Inc. Job Number: 680-56861-1
QC Association Summary
Lab Sample ID Client Sample ID Client Matrix Method Prep Batch
Report
Basis
Metals
Prep Batch: 680-166528
Lab Control Sample Solid 3050BLCS 680-166528/24-A T
Method Blank Solid 3050BMB 680-166528/23-A T
SolidIBS-3-LS 3050B680-56861-3 T
SolidIBS-4-NS 3050B680-56861-4 T
SolidIBS-4-LS 3050B680-56861-5 T
SolidIBS-3-US 3050B680-56861-6 T
SolidIBS-5-NS 3050B680-56861-7 T
SolidIBS-5-LS 3050B680-56861-8 T
SolidIBS-4-US 3050B680-56861-9 T
SolidIBS-6-NS 3050B680-56861-10 T
SolidIBS-6-LS 3050B680-56861-11 T
SolidIBS-5-US 3050B680-56861-12 T
SolidIBS-6-US 3050B680-56861-13 T
SolidIBS-7-NS 3050B680-56861-14 T
Matrix Spike Solid 3050B680-56861-14MS T
Matrix Spike Duplicate Solid 3050B680-56861-14MSD T
Prep Batch: 680-166534
Lab Control Sample Solid 7471ALCS 680-166534/24-A T
Method Blank Solid 7471AMB 680-166534/23-A T
SolidIBS-3-LS 7471A680-56861-3 T
SolidIBS-4-NS 7471A680-56861-4 T
SolidIBS-4-LS 7471A680-56861-5 T
SolidIBS-3-US 7471A680-56861-6 T
SolidIBS-5-NS 7471A680-56861-7 T
SolidIBS-5-LS 7471A680-56861-8 T
SolidIBS-4-US 7471A680-56861-9 T
SolidIBS-6-NS 7471A680-56861-10 T
SolidIBS-6-LS 7471A680-56861-11 T
SolidIBS-5-US 7471A680-56861-12 T
SolidIBS-6-US 7471A680-56861-13 T
SolidIBS-7-NS 7471A680-56861-14 T
Matrix Spike Solid 7471A680-56861-14MS T
Matrix Spike Duplicate Solid 7471A680-56861-14MSD T
Analysis Batch:680-166538
Lab Control Sample Solid 680-1663376010BLCS 680-166337/24-A T
Method Blank Solid 680-1663376010BMB 680-166337/23-A T
Solid 680-166337IBS-1-LS 6010B680-56861-1 T
Solid 680-166337IBS-3-NS 6010B680-56861-2 T
TestAmerica Savannah
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Quality Control Results
Client: Ashland Inc. Job Number: 680-56861-1
QC Association Summary
Lab Sample ID Client Sample ID Client Matrix Method Prep Batch
Report
Basis
Metals
Prep Batch: 680-166757
Lab Control Sample Solid 7471ALCS 680-166757/20-A T
Method Blank Solid 7471AMB 680-166757/19-A T
SolidIBS-1-LS 7471A680-56861-1 T
SolidIBS-3-NS 7471A680-56861-2 T
SolidIBS-7-LS 7471A680-56861-15 T
SolidIBS-7-US 7471A680-56861-16 T
SolidIBS-8-NS 7471A680-56861-17 T
SolidIBS-8-LS 7471A680-56861-18 T
SolidIBS-8-US 7471A680-56861-19 T
SolidIBS-1-US 7471A680-56861-20 T
SolidIBS-2-NS 7471A680-56861-21 T
SolidIBS-2-LS 7471A680-56861-22 T
SolidIBS-2-US 7471A680-56861-23 T
Matrix Spike Solid 7471A680-56861-23MS T
Matrix Spike Duplicate Solid 7471A680-56861-23MSD T
Prep Batch: 680-166825
Lab Control Sample Solid 3050BLCS 680-166825/23-A T
Method Blank Solid 3050BMB 680-166825/22-A T
SolidIBS-7-LS 3050B680-56861-15 T
SolidIBS-7-US 3050B680-56861-16 T
SolidIBS-8-NS 3050B680-56861-17 T
SolidIBS-8-LS 3050B680-56861-18 T
SolidIBS-8-US 3050B680-56861-19 T
SolidIBS-1-US 3050B680-56861-20 T
SolidIBS-2-NS 3050B680-56861-21 T
SolidIBS-2-LS 3050B680-56861-22 T
SolidIBS-2-US 3050B680-56861-23 T
TestAmerica Savannah
Page 176 of 238
Quality Control Results
Client: Ashland Inc. Job Number: 680-56861-1
QC Association Summary
Lab Sample ID Client Sample ID Client Matrix Method Prep Batch
Report
Basis
Metals
Analysis Batch:680-166869
Lab Control Sample Solid 680-1665286010BLCS 680-166528/24-A T
Method Blank Solid 680-1665286010BMB 680-166528/23-A T
Solid 680-166528IBS-3-LS 6010B680-56861-3 T
Solid 680-166528IBS-4-NS 6010B680-56861-4 T
Solid 680-166528IBS-4-LS 6010B680-56861-5 T
Solid 680-166528IBS-3-US 6010B680-56861-6 T
Solid 680-166528IBS-5-NS 6010B680-56861-7 T
Solid 680-166528IBS-5-LS 6010B680-56861-8 T
Solid 680-166528IBS-4-US 6010B680-56861-9 T
Solid 680-166528IBS-6-NS 6010B680-56861-10 T
Solid 680-166528IBS-6-LS 6010B680-56861-11 T
Solid 680-166528IBS-5-US 6010B680-56861-12 T
Solid 680-166528IBS-6-US 6010B680-56861-13 T
Solid 680-166528IBS-7-NS 6010B680-56861-14 T
Matrix Spike Solid 680-1665286010B680-56861-14MS T
Matrix Spike Duplicate Solid 680-1665286010B680-56861-14MSD T
Analysis Batch:680-166898
Lab Control Sample Solid 680-1665347471ALCS 680-166534/24-A T
Method Blank Solid 680-1665347471AMB 680-166534/23-A T
Solid 680-166534IBS-3-LS 7471A680-56861-3 T
Solid 680-166534IBS-4-NS 7471A680-56861-4 T
Solid 680-166534IBS-4-LS 7471A680-56861-5 T
Solid 680-166534IBS-3-US 7471A680-56861-6 T
Solid 680-166534IBS-5-NS 7471A680-56861-7 T
Solid 680-166534IBS-5-LS 7471A680-56861-8 T
Solid 680-166534IBS-4-US 7471A680-56861-9 T
Solid 680-166534IBS-6-NS 7471A680-56861-10 T
Solid 680-166534IBS-6-LS 7471A680-56861-11 T
Solid 680-166534IBS-5-US 7471A680-56861-12 T
Solid 680-166534IBS-6-US 7471A680-56861-13 T
Solid 680-166534IBS-7-NS 7471A680-56861-14 T
Matrix Spike Solid 680-1665347471A680-56861-14MS T
Matrix Spike Duplicate Solid 680-1665347471A680-56861-14MSD T
TestAmerica Savannah
Page 177 of 238
Quality Control Results
Client: Ashland Inc. Job Number: 680-56861-1
QC Association Summary
Lab Sample ID Client Sample ID Client Matrix Method Prep Batch
Report
Basis
Metals
Analysis Batch:680-167080
Lab Control Sample Solid 680-1667577471ALCS 680-166757/20-A T
Method Blank Solid 680-1667577471AMB 680-166757/19-A T
Solid 680-166757IBS-1-LS 7471A680-56861-1 T
Solid 680-166757IBS-3-NS 7471A680-56861-2 T
Solid 680-166757IBS-7-LS 7471A680-56861-15 T
Solid 680-166757IBS-7-US 7471A680-56861-16 T
Solid 680-166757IBS-8-NS 7471A680-56861-17 T
Solid 680-166757IBS-8-LS 7471A680-56861-18 T
Solid 680-166757IBS-8-US 7471A680-56861-19 T
Solid 680-166757IBS-1-US 7471A680-56861-20 T
Solid 680-166757IBS-2-NS 7471A680-56861-21 T
Solid 680-166757IBS-2-LS 7471A680-56861-22 T
Solid 680-166757IBS-2-US 7471A680-56861-23 T
Matrix Spike Solid 680-1667577471A680-56861-23MS T
Matrix Spike Duplicate Solid 680-1667577471A680-56861-23MSD T
Analysis Batch:680-167105
Lab Control Sample Solid 680-1668256010BLCS 680-166825/23-A T
Method Blank Solid 680-1668256010BMB 680-166825/22-A T
Solid 680-166825IBS-7-LS 6010B680-56861-15 T
Solid 680-166825IBS-7-US 6010B680-56861-16 T
Solid 680-166825IBS-8-NS 6010B680-56861-17 T
Solid 680-166825IBS-8-LS 6010B680-56861-18 T
Solid 680-166825IBS-8-US 6010B680-56861-19 T
Solid 680-166825IBS-1-US 6010B680-56861-20 T
Solid 680-166825IBS-2-NS 6010B680-56861-21 T
Solid 680-166825IBS-2-LS 6010B680-56861-22 T
Solid 680-166825IBS-2-US 6010B680-56861-23 T
Report Basis
T = Total
TestAmerica Savannah
Page 178 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
Surrogate Recovery Report
8260B Volatile Organic Compounds (GC/MS)
Client Matrix: Solid
Lab Sample ID Client Sample ID
BFB DBFM TOL
%Rec %Rec %Rec
680-56861-1 IBS-1-LS 0D 0D 0D
680-56861-2 IBS-3-NS 0D 0D 0D
680-56861-3 IBS-3-LS 0D 0D 0D
680-56861-4 IBS-4-NS 0D 0D 0D
680-56861-5 IBS-4-LS 0D 0D 0D
680-56861-6 IBS-3-US 0D 0D 0D
680-56861-7 IBS-5-NS 75 56X 66
680-56861-8 IBS-5-LS 0D 0D 0D
680-56861-9 IBS-4-US 0D 0D 0D
680-56861-10 IBS-6-NS 0D 0D 0D
680-56861-11 IBS-6-LS 0D 0D 0D
680-56861-12 IBS-5-US 0D 0D 0D
680-56861-13 IBS-6-US 0D 0D 0D
680-56861-14 IBS-7-NS 0D 0D 0D
680-56861-15 IBS-7-LS 0D 0D 0D
680-56861-16 IBS-7-US 0D 0D 0D
680-56861-17 IBS-8-NS 96 77 75
680-56861-18 IBS-8-LS 0D 0D 0D
680-56861-19 IBS-8-US 0D 0D 0D
680-56861-20 IBS-1-US 0D 0D 0D
680-56861-21 IBS-2-NS 0D 0D 0D
680-56861-22 IBS-2-LS 0D 0D 0D
680-56861-23 IBS-2-US 0D 0D 0D
MB 680-166615/8 104 92 100
MB 680-166686/8 113 93 108
MB 680-166737/8 122 97 122
MB 680-166861/9 121 103 112
LCS 680-166615/6 101 96 98
LCS 680-166686/6 91 79 88
Surrogate Acceptance Limits
BFB = 4-Bromofluorobenzene 65-124
DBFM = Dibromofluoromethane 65-124
TOL = Toluene-d8 (Surr) 65-132
TestAmerica Savannah
Page 179 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
Surrogate Recovery Report
8260B Volatile Organic Compounds (GC/MS)
Client Matrix: Solid
Lab Sample ID Client Sample ID
BFB DBFM TOL
%Rec %Rec %Rec
LCS 680-166737/6 103 78 95
LCS 680-166861/7 113 104 103
LCSD 680-166615/7 94 85 94
LCSD 680-166686/7 94 80 92
LCSD 680-166737/7 103 80 94
LCSD 680-166861/8 106 92 93
Surrogate Acceptance Limits
BFB = 4-Bromofluorobenzene 65-124
DBFM = Dibromofluoromethane 65-124
TOL = Toluene-d8 (Surr) 65-132
TestAmerica Savannah
Page 180 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
Surrogate Recovery Report
8260B Volatile Organic Compounds (GC/MS)
Client Matrix: Water
Lab Sample ID Client Sample ID
BFB DBFM TOL
%Rec %Rec %Rec
680-56861-24 FB-1 100 91 103
680-56861-25 FB-2 99 93 100
680-56861-26 TB-1 99 90 102
680-56861-27 TB-2 98 93 102
680-56861-28 RB-1 94 92 103
MB 680-166185/9 100 100 105
LCS 680-166185/6 99 99 111
LCSD 680-166185/7 99 102 107
Surrogate Acceptance Limits
BFB = 4-Bromofluorobenzene 75-120
DBFM = Dibromofluoromethane 75-121
TOL = Toluene-d8 (Surr) 75-120
TestAmerica Savannah
Page 181 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
Surrogate Recovery Report
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Client Matrix: Solid
Lab Sample ID Client Sample ID
TBP FBP 2FP TPH PHL NBZ
%Rec %Rec %Rec %Rec %Rec %Rec
680-56861-1 IBS-1-LS 0D 0D 0D 0D 0D 0D
680-56861-1 IBS-1-LS 0D 0D 0D 0D 0D 0D
680-56861-2 IBS-3-NS 0D 0D 0D 0D 0D 0D
680-56861-2 IBS-3-NS 0D 0D 0D 0D 0D 0D
680-56861-3 IBS-3-LS 0D 0D 0D 0D 0D 0D
680-56861-3 IBS-3-LS 0D 0D 0D 0D 0D 0D
680-56861-4 IBS-4-NS 0D 0D 0D 0D 0D 0D
680-56861-4 IBS-4-NS 0D 0D 0D 0D 0D 0D
680-56861-5 IBS-4-LS 0D 0D 0D 0D 0D 0D
680-56861-5 IBS-4-LS 0D 0D 0D 0D 0D 0D
680-56861-6 IBS-3-US 0D 0D 0D 0D 0D 0D
680-56861-7 IBS-5-NS 0D 0D 0D 0D 0D 0D
680-56861-8 IBS-5-LS 0D 0D 0D 0D 0D 0D
680-56861-8 IBS-5-LS 0D 0D 0D 0D 0D 0D
680-56861-9 IBS-4-US 0D 0D 0D 0D 0D 0D
680-56861-10 IBS-6-NS 0D 0D 0D 0D 0D 0D
680-56861-10 IBS-6-NS 0D 0D 0D 0D 0D 0D
680-56861-11 IBS-6-LS 0D 0D 0D 0D 0D 0D
680-56861-12 IBS-5-US 0D 0D 0D 0D 0D 0D
680-56861-13 IBS-6-US 0D 0D 0D 0D 0D 0D
680-56861-14 IBS-7-NS 0D 0D 0D 0D 0D 0D
680-56861-15 IBS-7-LS 0D 0D 0D 0D 0D 0D
680-56861-16 IBS-7-US 0D 0D 0D 0D 0D 0D
680-56861-17 IBS-8-NS 0D 0D 0D 0D 0D 0D
680-56861-18 IBS-8-LS 0D 0D 0D 0D 0D 0D
680-56861-19 IBS-8-US 0D 0D 0D 0D 0D 0D
680-56861-20 IBS-1-US 0D 0D 0D 0D 0D 0D
680-56861-21 IBS-2-NS 0D 0D 0D 0D 0D 0D
680-56861-22 IBS-2-LS 0D 0D 0D 0D 0D 0D
Surrogate Acceptance Limits
TBP = 2,4,6-Tribromophenol 34-130
FBP = 2-Fluorobiphenyl 34-130
2FP = 2-Fluorophenol 30-130
TPH = Terphenyl-d14 39-130
PHL = Phenol-d5 30-130
NBZ = Nitrobenzene-d5 27-130
TestAmerica Savannah
Page 182 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
Surrogate Recovery Report
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Client Matrix: Solid
Lab Sample ID Client Sample ID
TBP FBP 2FP TPH PHL NBZ
%Rec %Rec %Rec %Rec %Rec %Rec
680-56861-23 IBS-2-US 0D 0D 0D 0D 0D 0D
MB 680-166147/21-A 94 81 76 99 81 78
LCS 680-166138/12-A 80 60 57 69 62 60
LCS 680-166147/22-A 101 82 70 95 79 74
680-56861-21 MS IBS-2-NS MS 0D 0D 0D 0D 0D 0D
680-56861-21 MSD IBS-2-NS MSD 0D 0D 0D 0D 0D 0D
Surrogate Acceptance Limits
TBP = 2,4,6-Tribromophenol 34-130
FBP = 2-Fluorobiphenyl 34-130
2FP = 2-Fluorophenol 30-130
TPH = Terphenyl-d14 39-130
PHL = Phenol-d5 30-130
NBZ = Nitrobenzene-d5 27-130
TestAmerica Savannah
Page 183 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
Surrogate Recovery Report
8270C Semivolatile Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)
Client Matrix: Water
Lab Sample ID Client Sample ID
TBP FBP 2FP TPH PHL NBZ
%Rec %Rec %Rec %Rec %Rec %Rec
680-56861-28 RB-1 96 78 73 101 77 83
MB 680-166243/7-A 102 88 75 103 82 90
LCS 680-166243/8-A 110 95 80 103 87 92
LCSD
680-166243/9-A
103 87 79 100 85 91
Surrogate Acceptance Limits
TBP = 2,4,6-Tribromophenol 40-139
FBP = 2-Fluorobiphenyl 50-113
2FP = 2-Fluorophenol 36-110
TPH = Terphenyl-d14 10-121
PHL = Phenol-d5 38-116
NBZ = Nitrobenzene-d5 45-112
TestAmerica Savannah
Page 184 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
WaterClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
04/20/2010 1251
Method Blank - Batch: 680-166185
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 680-166185
Prep Batch: N/A
04/20/2010 1251
pq093.d
5 mL
5 mL
Units: ug/L
Method: 8260B
Preparation: 5030B
MSPMB 680-166185/9
Analyte Result Qual MDL RL
25 U 255.0Acetone
40 U 4010Acetonitrile
20 U 207.4Acrolein
20 U 207.2Acrylonitrile
1.0 U 1.00.25Benzene
1.0 U 1.00.50Bromoform
1.0 U 1.00.80Bromomethane
10 U 101.02-Butanone (MEK)
2.0 U 2.00.60Carbon disulfide
1.0 U 1.00.50Carbon tetrachloride
1.0 U 1.00.25Chlorobenzene
1.0 U 1.00.302-Chloro-1,3-butadiene
1.0 U 1.00.10Chlorodibromomethane
1.0 U 1.01.0Chloroethane
1.0 U 1.00.14Chloroform
1.0 U 1.00.33Chloromethane
1.0 U 1.00.203-Chloro-1-propene
1.0 U 1.00.11cis-1,3-Dichloropropene
1.0 U 1.00.441,2-Dibromo-3-Chloropropane
1.0 U 1.00.20Dibromomethane
1.0 U 1.00.25Dichlorobromomethane
1.0 U 1.00.25Dichlorodifluoromethane
1.0 U 1.00.251,1-Dichloroethane
1.0 U 1.00.101,2-Dichloroethane
1.0 U 1.00.111,1-Dichloroethene
1.0 U 1.00.131,2-Dichloropropane
1.0 U 1.00.11Ethylbenzene
1.0 U 1.00.25Ethylene Dibromide
1.0 U 1.00.25Ethyl methacrylate
10 U 101.02-Hexanone
5.0 U 5.01.0Iodomethane
40 U 4011Isobutyl alcohol
20 U 203.3Methacrylonitrile
5.0 U 5.01.0Methylene Chloride
1.0 U 1.00.48Methyl methacrylate
10 U 101.04-Methyl-2-pentanone (MIBK)
5.0 U 5.01.2Pentachloroethane
20 U 204.6Propionitrile
1.0 U 1.00.11Styrene
1.0 U 1.00.331,1,1,2-Tetrachloroethane
1.0 U 1.00.181,1,2,2-Tetrachloroethane
1.0 U 1.00.15Tetrachloroethene
1.0 U 1.00.33Toluene
TestAmerica Savannah Page 185 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
WaterClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
04/20/2010 1251
Method Blank - Batch: 680-166185
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 680-166185
Prep Batch: N/A
04/20/2010 1251
pq093.d
5 mL
5 mL
Units: ug/L
Method: 8260B
Preparation: 5030B
MSPMB 680-166185/9
Analyte Result Qual MDL RL
2.0 U 2.00.50trans-1,4-Dichloro-2-butene
1.0 U 1.00.20trans-1,2-Dichloroethene
1.0 U 1.00.21trans-1,3-Dichloropropene
1.0 U 1.00.501,1,1-Trichloroethane
1.0 U 1.00.131,1,2-Trichloroethane
1.0 U 1.00.13Trichloroethene
1.0 U 1.00.25Trichlorofluoromethane
1.0 U 1.00.411,2,3-Trichloropropane
2.0 U 2.00.28Vinyl acetate
1.0 U 1.00.18Vinyl chloride
2.0 U 2.00.20Xylenes, Total
Surrogate % Rec Acceptance Limits
4-Bromofluorobenzene 100 75 - 120
Dibromofluoromethane 100 75 - 121
Toluene-d8 (Surr) 105 75 - 120
TestAmerica Savannah Page 186 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
04/20/2010 1041
04/20/2010 1111
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report - Batch: 680-166185
1.0
1.0
Water
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Water
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
ug/L
04/20/2010 1041
Prep Batch: N/A
Analysis Batch: 680-166185
pq085.d
5 mL
5 mL
pq087.d
5 mL
5 mL
ug/L
04/20/2010 1111
Analysis Batch: 680-166185
Prep Batch: N/A
Method: 8260B
Preparation: 5030B
MSP
MSP
LCS 680-166185/6
LCSD 680-166185/7
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
132128 17 - 175 3 50Acetone
106112 77 - 119 5 30Benzene
9392 62 - 133 1 30Bromoform
107138 12 - 184 26 50Bromomethane
110109 33 - 157 0 302-Butanone (MEK)
142137 55 - 131 4 30 * *Carbon disulfide
120128 71 - 135 6 30Carbon tetrachloride
102103 85 - 116 1 30Chlorobenzene
102104 75 - 133 2 30Chlorodibromomethane
12397 40 - 165 24 50Chloroethane
111108 82 - 120 3 30Chloroform
141133 48 - 142 6 50Chloromethane
116123 76 - 126 6 30cis-1,3-Dichloropropene
95100 49 - 140 5 301,2-Dibromo-3-Chloropropane
108116 78 - 119 7 30Dibromomethane
112119 78 - 127 6 30Dichlorobromomethane
151145 34 - 154 4 30Dichlorodifluoromethane
111107 74 - 127 4 301,1-Dichloroethane
114121 66 - 132 6 301,2-Dichloroethane
9995 62 - 141 4 301,1-Dichloroethene
114117 73 - 124 3 301,2-Dichloropropane
103107 86 - 116 3 30Ethylbenzene
101103 80 - 121 2 30Ethylene Dibromide
103109 34 - 161 5 302-Hexanone
112115 70 - 125 3 30Methylene Chloride
110120 40 - 151 9 304-Methyl-2-pentanone (MIBK)
99104 82 - 122 5 30Styrene
103107 81 - 128 3 301,1,1,2-Tetrachloroethane
9999 69 - 129 0 301,1,2,2-Tetrachloroethane
101104 76 - 126 3 30Tetrachloroethene
106110 81 - 117 4 30Toluene
10198 72 - 131 3 30trans-1,2-Dichloroethene
115127 73 - 128 10 30trans-1,3-Dichloropropene
TestAmerica Savannah Page 187 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
04/20/2010 1041
04/20/2010 1111
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report - Batch: 680-166185
1.0
1.0
Water
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Water
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
ug/L
04/20/2010 1041
Prep Batch: N/A
Analysis Batch: 680-166185
pq085.d
5 mL
5 mL
pq087.d
5 mL
5 mL
ug/L
04/20/2010 1111
Analysis Batch: 680-166185
Prep Batch: N/A
Method: 8260B
Preparation: 5030B
MSP
MSP
LCS 680-166185/6
LCSD 680-166185/7
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
118127 76 - 127 8 301,1,1-Trichloroethane
108111 75 - 121 3 301,1,2-Trichloroethane
100108 84 - 115 8 30Trichloroethene
133132 58 - 149 1 50Trichlorofluoromethane
9393 70 - 130 0 301,2,3-Trichloropropane
131129 10 - 217 1 30Vinyl acetate
113111 59 - 144 2 50Vinyl chloride
102107 84 - 118 4 30Xylenes, Total
Surrogate LCS % Rec LCSD % Rec Acceptance Limits
4-Bromofluorobenzene 99 99 75 - 120
Dibromofluoromethane 99 102 75 - 121
Toluene-d8 (Surr) 111 107 75 - 120
TestAmerica Savannah Page 188 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
SolidClient Matrix:
40Dilution:
Date Analyzed:
Lab Sample ID:
04/23/2010 1128
Method Blank - Batch: 680-166615
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 680-166615
Prep Batch: N/A mq219.d
5 g
5 mL
N/A
Units: ug/Kg
Method: 8260B
Preparation: N/A
MSMMB 680-166615/8
Analyte Result Qual MDL RL
2000 U 2000440Acetone
8000 U 80001600Acetonitrile
4000 U 4000960Acrolein
4000 U 40001400Acrylonitrile
200 U 20029Benzene
200 U 20060Bromoform
200 U 20060Bromomethane
1000 U 1000962-Butanone (MEK)
200 U 20044Carbon disulfide
200 U 20033Carbon tetrachloride
200 U 20038Chlorobenzene
200 U 200842-Chloro-1,3-butadiene
200 U 20068Chlorodibromomethane
200 U 200110Chloroethane
200 U 20044Chloroform
200 U 20040Chloromethane
200 U 200883-Chloro-1-propene
200 U 20033cis-1,3-Dichloropropene
400 U 4001801,2-Dibromo-3-Chloropropane
200 U 20068Dibromomethane
200 U 20039Dichlorobromomethane
200 U 20038Dichlorodifluoromethane
200 U 200441,1-Dichloroethane
200 U 200441,2-Dichloroethane
200 U 200601,1-Dichloroethene
200 U 200341,2-Dichloropropane
200 U 20052Ethylbenzene
200 U 20060Ethylene Dibromide
200 U 200140Ethyl methacrylate
1000 U 10001302-Hexanone
200 U 20072Iodomethane
8000 U 80002100Isobutyl alcohol
4000 U 4000920Methacrylonitrile
200 U 20039Methylene Chloride
400 U 400180Methyl methacrylate
1000 U 10001704-Methyl-2-pentanone (MIBK)
1000 U 1000250Pentachloroethane
4000 U 40001000Propionitrile
200 U 20037Styrene
200 U 200961,1,1,2-Tetrachloroethane
200 U 200641,1,2,2-Tetrachloroethane
200 U 20076Tetrachloroethene
200 U 20034Toluene
TestAmerica Savannah Page 189 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
SolidClient Matrix:
40Dilution:
Date Analyzed:
Lab Sample ID:
04/23/2010 1128
Method Blank - Batch: 680-166615
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 680-166615
Prep Batch: N/A mq219.d
5 g
5 mL
N/A
Units: ug/Kg
Method: 8260B
Preparation: N/A
MSMMB 680-166615/8
Analyte Result Qual MDL RL
400 U 400120trans-1,4-Dichloro-2-butene
200 U 20025trans-1,2-Dichloroethene
200 U 20035trans-1,3-Dichloropropene
200 U 200241,1,1-Trichloroethane
200 U 200521,1,2-Trichloroethane
200 U 20052Trichloroethene
200 U 20048Trichlorofluoromethane
200 U 200961,2,3-Trichloropropane
400 U 400100Vinyl acetate
200 U 20060Vinyl chloride
400 U 40044Xylenes, Total
Surrogate % Rec Acceptance Limits
4-Bromofluorobenzene 104 65 - 124
Dibromofluoromethane 92 65 - 124
Toluene-d8 (Surr) 100 65 - 132
TestAmerica Savannah Page 190 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
04/23/2010 0954
04/23/2010 1018
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report - Batch: 680-166615
40
40
Solid
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Solid
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
ug/Kg
Prep Batch: N/A
Analysis Batch: 680-166615
N/A
mq216.d
5 g
5 mL
mq217.d
5 g
5 mL
ug/Kg
Analysis Batch: 680-166615
Prep Batch: N/A
Method: 8260B
Preparation: N/A
N/A
MSM
MSM
LCS 680-166615/6
LCSD 680-166615/7
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
8492 16 - 202 9 50Acetone
9499 63 - 130 5 50Benzene
98102 66 - 127 4 50Bromoform
8594 54 - 146 10 50Bromomethane
8997 19 - 192 9 502-Butanone (MEK)
8698 46 - 134 13 50Carbon disulfide
9094 60 - 136 4 50Carbon tetrachloride
9396 77 - 120 4 50Chlorobenzene
96100 70 - 126 5 50Chlorodibromomethane
6184 26 - 166 32 50Chloroethane
8897 68 - 127 10 50Chloroform
101111 46 - 137 9 50Chloromethane
9398 66 - 137 4 50cis-1,3-Dichloropropene
99102 62 - 140 4 501,2-Dibromo-3-Chloropropane
9197 61 - 138 6 50Dibromomethane
9498 64 - 137 4 50Dichlorobromomethane
92103 17 - 163 11 50Dichlorodifluoromethane
8897 65 - 130 10 501,1-Dichloroethane
9498 62 - 140 5 501,2-Dichloroethane
7183 59 - 137 15 501,1-Dichloroethene
9496 66 - 135 2 501,2-Dichloropropane
96101 77 - 121 6 50Ethylbenzene
9295 61 - 138 3 50Ethylene Dibromide
9298 47 - 151 6 502-Hexanone
87100 65 - 126 14 50Methylene Chloride
115123 50 - 148 6 504-Methyl-2-pentanone (MIBK)
97104 75 - 123 7 50Styrene
9297 72 - 124 5 501,1,1,2-Tetrachloroethane
9094 65 - 130 5 501,1,2,2-Tetrachloroethane
107112 76 - 120 5 50Tetrachloroethene
9398 67 - 132 6 50Toluene
8594 66 - 127 10 50trans-1,2-Dichloroethene
95100 64 - 138 5 50trans-1,3-Dichloropropene
TestAmerica Savannah Page 191 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
04/23/2010 0954
04/23/2010 1018
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report - Batch: 680-166615
40
40
Solid
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Solid
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
ug/Kg
Prep Batch: N/A
Analysis Batch: 680-166615
N/A
mq216.d
5 g
5 mL
mq217.d
5 g
5 mL
ug/Kg
Analysis Batch: 680-166615
Prep Batch: N/A
Method: 8260B
Preparation: N/A
N/A
MSM
MSM
LCS 680-166615/6
LCSD 680-166615/7
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
95100 56 - 140 6 501,1,1-Trichloroethane
97101 62 - 138 5 501,1,2-Trichloroethane
9193 68 - 133 2 50Trichloroethene
8999 33 - 152 10 50Trichlorofluoromethane
9695 65 - 132 1 501,2,3-Trichloropropane
8397 10 - 254 15 50Vinyl acetate
92102 56 - 139 10 50Vinyl chloride
9498 76 - 122 4 50Xylenes, Total
Surrogate LCS % Rec LCSD % Rec Acceptance Limits
4-Bromofluorobenzene 101 94 65 - 124
Dibromofluoromethane 96 85 65 - 124
Toluene-d8 (Surr) 98 94 65 - 132
TestAmerica Savannah Page 192 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
SolidClient Matrix:
40Dilution:
Date Analyzed:
Lab Sample ID:
04/25/2010 1531
Method Blank - Batch: 680-166686
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 680-166686
Prep Batch: N/A mq237.d
5 g
5 mL
N/A
Units: ug/Kg
Method: 8260B
Preparation: N/A
MSMMB 680-166686/8
Analyte Result Qual MDL RL
2000 U 2000440Acetone
8000 U 80001600Acetonitrile
4000 U 4000960Acrolein
4000 U 40001400Acrylonitrile
200 U 20029Benzene
200 U 20060Bromoform
200 U 20060Bromomethane
1000 U 1000962-Butanone (MEK)
200 U 20044Carbon disulfide
200 U 20033Carbon tetrachloride
200 U 20038Chlorobenzene
200 U 200842-Chloro-1,3-butadiene
200 U 20068Chlorodibromomethane
200 U 200110Chloroethane
200 U 20044Chloroform
200 U 20040Chloromethane
200 U 200883-Chloro-1-propene
200 U 20033cis-1,3-Dichloropropene
400 U 4001801,2-Dibromo-3-Chloropropane
200 U 20068Dibromomethane
200 U 20039Dichlorobromomethane
200 U 20038Dichlorodifluoromethane
200 U 200441,1-Dichloroethane
200 U 200441,2-Dichloroethane
200 U 200601,1-Dichloroethene
200 U 200341,2-Dichloropropane
200 U 20052Ethylbenzene
200 U 20060Ethylene Dibromide
200 U 200140Ethyl methacrylate
1000 U 10001302-Hexanone
200 U 20072Iodomethane
8000 U 80002100Isobutyl alcohol
4000 U 4000920Methacrylonitrile
200 U 20039Methylene Chloride
400 U 400180Methyl methacrylate
1000 U 10001704-Methyl-2-pentanone (MIBK)
1000 U 1000250Pentachloroethane
4000 U 40001000Propionitrile
200 U 20037Styrene
200 U 200961,1,1,2-Tetrachloroethane
200 U 200641,1,2,2-Tetrachloroethane
200 U 20076Tetrachloroethene
200 U 20034Toluene
TestAmerica Savannah Page 193 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
SolidClient Matrix:
40Dilution:
Date Analyzed:
Lab Sample ID:
04/25/2010 1531
Method Blank - Batch: 680-166686
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 680-166686
Prep Batch: N/A mq237.d
5 g
5 mL
N/A
Units: ug/Kg
Method: 8260B
Preparation: N/A
MSMMB 680-166686/8
Analyte Result Qual MDL RL
400 U 400120trans-1,4-Dichloro-2-butene
200 U 20025trans-1,2-Dichloroethene
200 U 20035trans-1,3-Dichloropropene
200 U 200241,1,1-Trichloroethane
200 U 200521,1,2-Trichloroethane
200 U 20052Trichloroethene
200 U 20048Trichlorofluoromethane
200 U 200961,2,3-Trichloropropane
400 U 400100Vinyl acetate
200 U 20060Vinyl chloride
400 U 40044Xylenes, Total
Surrogate % Rec Acceptance Limits
4-Bromofluorobenzene 113 65 - 124
Dibromofluoromethane 93 65 - 124
Toluene-d8 (Surr) 108 65 - 132
TestAmerica Savannah Page 194 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
04/25/2010 1420
04/25/2010 1444
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report - Batch: 680-166686
40
40
Solid
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Solid
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
ug/Kg
Prep Batch: N/A
Analysis Batch: 680-166686
N/A
mq235.d
5 g
5 mL
mq236.d
5 g
5 mL
ug/Kg
Analysis Batch: 680-166686
Prep Batch: N/A
Method: 8260B
Preparation: N/A
N/A
MSM
MSM
LCS 680-166686/6
LCSD 680-166686/7
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
7776 16 - 202 0 50Acetone
8784 63 - 130 3 50Benzene
9598 66 - 127 3 50Bromoform
8279 54 - 146 4 50Bromomethane
8087 19 - 192 8 502-Butanone (MEK)
7574 46 - 134 1 50Carbon disulfide
9489 60 - 136 5 50Carbon tetrachloride
8888 77 - 120 0 50Chlorobenzene
9394 70 - 126 1 50Chlorodibromomethane
6152 26 - 166 17 50Chloroethane
7979 68 - 127 0 50Chloroform
8251 46 - 137 47 50Chloromethane
8989 66 - 137 0 50cis-1,3-Dichloropropene
99101 62 - 140 2 501,2-Dibromo-3-Chloropropane
8889 61 - 138 0 50Dibromomethane
9289 64 - 137 3 50Dichlorobromomethane
8078 17 - 163 3 50Dichlorodifluoromethane
7777 65 - 130 1 501,1-Dichloroethane
9695 62 - 140 1 501,2-Dichloroethane
8688 59 - 137 3 501,1-Dichloroethene
8785 66 - 135 2 501,2-Dichloropropane
9491 77 - 121 2 50Ethylbenzene
9189 61 - 138 2 50Ethylene Dibromide
9196 47 - 151 6 502-Hexanone
7675 65 - 126 1 50Methylene Chloride
115117 50 - 148 1 504-Methyl-2-pentanone (MIBK)
9493 75 - 123 1 50Styrene
9092 72 - 124 1 501,1,1,2-Tetrachloroethane
8689 65 - 130 3 501,1,2,2-Tetrachloroethane
106105 76 - 120 1 50Tetrachloroethene
9188 67 - 132 4 50Toluene
7675 66 - 127 0 50trans-1,2-Dichloroethene
9692 64 - 138 4 50trans-1,3-Dichloropropene
TestAmerica Savannah Page 195 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
04/25/2010 1420
04/25/2010 1444
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report - Batch: 680-166686
40
40
Solid
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Solid
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
ug/Kg
Prep Batch: N/A
Analysis Batch: 680-166686
N/A
mq235.d
5 g
5 mL
mq236.d
5 g
5 mL
ug/Kg
Analysis Batch: 680-166686
Prep Batch: N/A
Method: 8260B
Preparation: N/A
N/A
MSM
MSM
LCS 680-166686/6
LCSD 680-166686/7
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
9792 56 - 140 5 501,1,1-Trichloroethane
9392 62 - 138 1 501,1,2-Trichloroethane
8785 68 - 133 2 50Trichloroethene
8480 33 - 152 5 50Trichlorofluoromethane
8991 65 - 132 2 501,2,3-Trichloropropane
7880 10 - 254 3 50Vinyl acetate
7379 56 - 139 7 50Vinyl chloride
9187 76 - 122 4 50Xylenes, Total
Surrogate LCS % Rec LCSD % Rec Acceptance Limits
4-Bromofluorobenzene 91 94 65 - 124
Dibromofluoromethane 79 80 65 - 124
Toluene-d8 (Surr) 88 92 65 - 132
TestAmerica Savannah Page 196 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
SolidClient Matrix:
40Dilution:
Date Analyzed:
Lab Sample ID:
04/26/2010 0946
Method Blank - Batch: 680-166737
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 680-166737
Prep Batch: N/A mq243.d
5 g
5 mL
N/A
Units: ug/Kg
Method: 8260B
Preparation: N/A
MSMMB 680-166737/8
Analyte Result Qual MDL RL
2000 U 2000440Acetone
8000 U 80001600Acetonitrile
4000 U 4000960Acrolein
4000 U 40001400Acrylonitrile
200 U 20029Benzene
200 U 20060Bromoform
200 U 20060Bromomethane
1000 U 1000962-Butanone (MEK)
200 U 20044Carbon disulfide
200 U 20033Carbon tetrachloride
200 U 20038Chlorobenzene
200 U 200842-Chloro-1,3-butadiene
200 U 20068Chlorodibromomethane
200 U 200110Chloroethane
200 U 20044Chloroform
200 U 20040Chloromethane
200 U 200883-Chloro-1-propene
200 U 20033cis-1,3-Dichloropropene
400 U 4001801,2-Dibromo-3-Chloropropane
200 U 20068Dibromomethane
200 U 20039Dichlorobromomethane
200 U 20038Dichlorodifluoromethane
200 U 200441,1-Dichloroethane
200 U 200441,2-Dichloroethane
200 U 200601,1-Dichloroethene
200 U 200341,2-Dichloropropane
200 U 20052Ethylbenzene
200 U 20060Ethylene Dibromide
200 U 200140Ethyl methacrylate
1000 U 10001302-Hexanone
200 U 20072Iodomethane
8000 U 80002100Isobutyl alcohol
4000 U 4000920Methacrylonitrile
200 U 20039Methylene Chloride
400 U 400180Methyl methacrylate
1000 U 10001704-Methyl-2-pentanone (MIBK)
1000 U 1000250Pentachloroethane
4000 U 40001000Propionitrile
200 U 20037Styrene
200 U 200961,1,1,2-Tetrachloroethane
200 U 200641,1,2,2-Tetrachloroethane
200 U 20076Tetrachloroethene
200 U 20034Toluene
TestAmerica Savannah Page 197 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
SolidClient Matrix:
40Dilution:
Date Analyzed:
Lab Sample ID:
04/26/2010 0946
Method Blank - Batch: 680-166737
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 680-166737
Prep Batch: N/A mq243.d
5 g
5 mL
N/A
Units: ug/Kg
Method: 8260B
Preparation: N/A
MSMMB 680-166737/8
Analyte Result Qual MDL RL
400 U 400120trans-1,4-Dichloro-2-butene
200 U 20025trans-1,2-Dichloroethene
200 U 20035trans-1,3-Dichloropropene
200 U 200241,1,1-Trichloroethane
200 U 200521,1,2-Trichloroethane
200 U 20052Trichloroethene
200 U 20048Trichlorofluoromethane
200 U 200961,2,3-Trichloropropane
400 U 400100Vinyl acetate
200 U 20060Vinyl chloride
400 U 40044Xylenes, Total
Surrogate % Rec Acceptance Limits
4-Bromofluorobenzene 122 65 - 124
Dibromofluoromethane 97 65 - 124
Toluene-d8 (Surr) 122 65 - 132
TestAmerica Savannah Page 198 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
04/26/2010 0835
04/26/2010 0859
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report - Batch: 680-166737
40
40
Solid
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Solid
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
ug/Kg
Prep Batch: N/A
Analysis Batch: 680-166737
N/A
mq241.d
5 g
5 mL
mq242.d
5 g
5 mL
ug/Kg
Analysis Batch: 680-166737
Prep Batch: N/A
Method: 8260B
Preparation: N/A
N/A
MSM
MSM
LCS 680-166737/6
LCSD 680-166737/7
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
8598 16 - 202 14 50Acetone
8991 63 - 130 2 50Benzene
111119 66 - 127 7 50Bromoform
7766 54 - 146 15 50Bromomethane
9296 19 - 192 5 502-Butanone (MEK)
9093 46 - 134 3 50Carbon disulfide
100106 60 - 136 5 50Carbon tetrachloride
9696 77 - 120 1 50Chlorobenzene
102104 70 - 126 2 50Chlorodibromomethane
5856 26 - 166 2 50Chloroethane
8486 68 - 127 3 50Chloroform
7879 46 - 137 1 50Chloromethane
9295 66 - 137 3 50cis-1,3-Dichloropropene
123123 62 - 140 0 501,2-Dibromo-3-Chloropropane
9699 61 - 138 3 50Dibromomethane
94101 64 - 137 7 50Dichlorobromomethane
7677 17 - 163 2 50Dichlorodifluoromethane
8082 65 - 130 2 501,1-Dichloroethane
99102 62 - 140 3 501,2-Dichloroethane
7877 59 - 137 1 501,1-Dichloroethene
9294 66 - 135 2 501,2-Dichloropropane
101101 77 - 121 0 50Ethylbenzene
96100 61 - 138 4 50Ethylene Dibromide
107112 47 - 151 5 502-Hexanone
7882 65 - 126 4 50Methylene Chloride
128138 50 - 148 7 504-Methyl-2-pentanone (MIBK)
104103 75 - 123 1 50Styrene
9997 72 - 124 1 501,1,1,2-Tetrachloroethane
9094 65 - 130 5 501,1,2,2-Tetrachloroethane
118119 76 - 120 0 50Tetrachloroethene
9495 67 - 132 1 50Toluene
7372 66 - 127 2 50trans-1,2-Dichloroethene
100106 64 - 138 7 50trans-1,3-Dichloropropene
TestAmerica Savannah Page 199 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
04/26/2010 0835
04/26/2010 0859
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report - Batch: 680-166737
40
40
Solid
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Solid
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
ug/Kg
Prep Batch: N/A
Analysis Batch: 680-166737
N/A
mq241.d
5 g
5 mL
mq242.d
5 g
5 mL
ug/Kg
Analysis Batch: 680-166737
Prep Batch: N/A
Method: 8260B
Preparation: N/A
N/A
MSM
MSM
LCS 680-166737/6
LCSD 680-166737/7
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
109111 56 - 140 2 501,1,1-Trichloroethane
100104 62 - 138 3 501,1,2-Trichloroethane
9395 68 - 133 2 50Trichloroethene
8384 33 - 152 2 50Trichlorofluoromethane
103105 65 - 132 2 501,2,3-Trichloropropane
7681 10 - 254 7 50Vinyl acetate
7069 56 - 139 1 50Vinyl chloride
9998 76 - 122 1 50Xylenes, Total
Surrogate LCS % Rec LCSD % Rec Acceptance Limits
4-Bromofluorobenzene 103 103 65 - 124
Dibromofluoromethane 78 80 65 - 124
Toluene-d8 (Surr) 95 94 65 - 132
TestAmerica Savannah Page 200 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
SolidClient Matrix:
40Dilution:
Date Analyzed:
Lab Sample ID:
04/27/2010 0903
Method Blank - Batch: 680-166861
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 680-166861
Prep Batch: N/A mq261.d
5 g
5 mL
N/A
Units: ug/Kg
Method: 8260B
Preparation: N/A
MSMMB 680-166861/9
Analyte Result Qual MDL RL
2000 U 2000440Acetone
8000 U 80001600Acetonitrile
4000 U 4000960Acrolein
4000 U 40001400Acrylonitrile
200 U 20029Benzene
200 U 20060Bromoform
200 U 20060Bromomethane
1000 U 1000962-Butanone (MEK)
200 U 20044Carbon disulfide
200 U 20033Carbon tetrachloride
200 U 20038Chlorobenzene
200 U 200842-Chloro-1,3-butadiene
200 U 20068Chlorodibromomethane
200 U 200110Chloroethane
200 U 20044Chloroform
200 U 20040Chloromethane
200 U 200883-Chloro-1-propene
200 U 20033cis-1,3-Dichloropropene
400 U 4001801,2-Dibromo-3-Chloropropane
200 U 20068Dibromomethane
200 U 20039Dichlorobromomethane
200 U 20038Dichlorodifluoromethane
200 U 200441,1-Dichloroethane
200 U 200441,2-Dichloroethane
200 U 200601,1-Dichloroethene
200 U 200341,2-Dichloropropane
200 U 20052Ethylbenzene
200 U 20060Ethylene Dibromide
200 U 200140Ethyl methacrylate
1000 U 10001302-Hexanone
200 U 20072Iodomethane
8000 U 80002100Isobutyl alcohol
4000 U 4000920Methacrylonitrile
200 U 20039Methylene Chloride
400 U 400180Methyl methacrylate
1000 U 10001704-Methyl-2-pentanone (MIBK)
1000 U 1000250Pentachloroethane
4000 U 40001000Propionitrile
200 U 20037Styrene
200 U 200961,1,1,2-Tetrachloroethane
200 U 200641,1,2,2-Tetrachloroethane
200 U 20076Tetrachloroethene
200 U 20034Toluene
TestAmerica Savannah Page 201 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
SolidClient Matrix:
40Dilution:
Date Analyzed:
Lab Sample ID:
04/27/2010 0903
Method Blank - Batch: 680-166861
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 680-166861
Prep Batch: N/A mq261.d
5 g
5 mL
N/A
Units: ug/Kg
Method: 8260B
Preparation: N/A
MSMMB 680-166861/9
Analyte Result Qual MDL RL
400 U 400120trans-1,4-Dichloro-2-butene
200 U 20025trans-1,2-Dichloroethene
200 U 20035trans-1,3-Dichloropropene
200 U 200241,1,1-Trichloroethane
200 U 200521,1,2-Trichloroethane
200 U 20052Trichloroethene
200 U 20048Trichlorofluoromethane
200 U 200961,2,3-Trichloropropane
400 U 400100Vinyl acetate
200 U 20060Vinyl chloride
400 U 40044Xylenes, Total
Surrogate % Rec Acceptance Limits
4-Bromofluorobenzene 121 65 - 124
Dibromofluoromethane 103 65 - 124
Toluene-d8 (Surr) 112 65 - 132
TestAmerica Savannah Page 202 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
04/27/2010 0753
04/27/2010 0816
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report - Batch: 680-166861
40
40
Solid
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Solid
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
ug/Kg
Prep Batch: N/A
Analysis Batch: 680-166861
N/A
mq259.d
5 g
5 mL
mq260.d
5 g
5 mL
ug/Kg
Analysis Batch: 680-166861
Prep Batch: N/A
Method: 8260B
Preparation: N/A
N/A
MSM
MSM
LCS 680-166861/7
LCSD 680-166861/8
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
92105 16 - 202 14 50Acetone
96106 63 - 130 10 50Benzene
94103 66 - 127 9 50Bromoform
8193 54 - 146 14 50Bromomethane
95105 19 - 192 10 502-Butanone (MEK)
97111 46 - 134 14 50Carbon disulfide
91102 60 - 136 12 50Carbon tetrachloride
95100 77 - 120 5 50Chlorobenzene
93101 70 - 126 8 50Chlorodibromomethane
6465 26 - 166 2 50Chloroethane
95106 68 - 127 11 50Chloroform
102125 46 - 137 20 50Chloromethane
8999 66 - 137 11 50cis-1,3-Dichloropropene
9094 62 - 140 5 501,2-Dibromo-3-Chloropropane
8799 61 - 138 13 50Dibromomethane
92101 64 - 137 9 50Dichlorobromomethane
99115 17 - 163 15 50Dichlorodifluoromethane
94107 65 - 130 12 501,1-Dichloroethane
8898 62 - 140 10 501,2-Dichloroethane
94112 59 - 137 18 501,1-Dichloroethene
8998 66 - 135 10 501,2-Dichloropropane
95104 77 - 121 9 50Ethylbenzene
90101 61 - 138 12 50Ethylene Dibromide
8491 47 - 151 8 502-Hexanone
96110 65 - 126 13 50Methylene Chloride
109122 50 - 148 11 504-Methyl-2-pentanone (MIBK)
9198 75 - 123 8 50Styrene
92100 72 - 124 9 501,1,1,2-Tetrachloroethane
92102 65 - 130 10 501,1,2,2-Tetrachloroethane
9199 76 - 120 9 50Tetrachloroethene
96105 67 - 132 9 50Toluene
96105 66 - 127 10 50trans-1,2-Dichloroethene
90100 64 - 138 11 50trans-1,3-Dichloropropene
TestAmerica Savannah Page 203 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
04/27/2010 0753
04/27/2010 0816
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report - Batch: 680-166861
40
40
Solid
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Solid
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
ug/Kg
Prep Batch: N/A
Analysis Batch: 680-166861
N/A
mq259.d
5 g
5 mL
mq260.d
5 g
5 mL
ug/Kg
Analysis Batch: 680-166861
Prep Batch: N/A
Method: 8260B
Preparation: N/A
N/A
MSM
MSM
LCS 680-166861/7
LCSD 680-166861/8
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
93100 56 - 140 8 501,1,1-Trichloroethane
8797 62 - 138 10 501,1,2-Trichloroethane
89100 68 - 133 12 50Trichloroethene
96112 33 - 152 16 50Trichlorofluoromethane
8893 65 - 132 5 501,2,3-Trichloropropane
93107 10 - 254 15 50Vinyl acetate
103126 56 - 139 20 50Vinyl chloride
93102 76 - 122 8 50Xylenes, Total
Surrogate LCS % Rec LCSD % Rec Acceptance Limits
4-Bromofluorobenzene 113 106 65 - 124
Dibromofluoromethane 104 92 65 - 124
Toluene-d8 (Surr) 103 93 65 - 132
TestAmerica Savannah Page 204 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
Solid
1.0
04/22/2010 2329Date Analyzed:
Lab Control Sample - Batch: 680-166138
Client Matrix:
Lab Sample ID:
Dilution:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
n7005.d
04/20/2010 1628
Analysis Batch: 680-166547
Prep Batch: 680-166138
30.07 g
1 mL
1 uL
Units: ug/Kg
Method: 8270C
Preparation: 3546
MSNLCS 680-166138/12-A
Analyte QualLimit% Rec.ResultSpike Amount
3330 2060 62 37 - 130Acenaphthene
3330 2130 64 37 - 130Acenaphthylene
3330 1560 47 22 - 130Acetophenone
3330 2720 82 10 - 1302-Acetylaminofluorene
16600 14700 88 J E10 - 130alpha,alpha-Dimethyl phenethylamine
3330 362 11 10 - 1304-Aminobiphenyl
3330 1570 47 13 - 130Aniline
3330 2340 70 39 - 130Anthracene
3330 2970 89 10 - 130Aramite, Total
3330 2400 72 40 - 130Benzo[a]anthracene
3330 2500 75 43 - 130Benzo[a]pyrene
3330 2450 74 35 - 130Benzo[b]fluoranthene
3330 2230 67 37 - 130Benzo[g,h,i]perylene
3330 2300 69 34 - 130Benzo[k]fluoranthene
3330 2040 61 25 - 130Benzyl alcohol
3330 2070 62 31 - 1301,1'-Biphenyl
3330 2750 83 30 - 130Bis(2-chloroethoxy)methane
3330 1980 60 16 - 130Bis(2-chloroethyl)ether
3330 2100 63 15 - 130bis(chloroisopropyl) ether
3330 2620 79 38 - 130Bis(2-ethylhexyl) phthalate
3330 2370 71 35 - 1304-Bromophenyl phenyl ether
3330 2800 84 41 - 130Butyl benzyl phthalate
3330 2000 60 23 - 1304-Chloroaniline
3330 2400 72 36 - 1304-Chloro-3-methylphenol
3330 2050 62 35 - 1302-Chloronaphthalene
3330 1990 60 32 - 1302-Chlorophenol
3330 2330 70 40 - 1304-Chlorophenyl phenyl ether
3330 2330 70 43 - 130Chrysene
3330 2410 72 10 - 130Diallate
3330 2350 71 36 - 130Dibenz(a,h)anthracene
3330 2120 64 38 - 130Dibenzofuran
3330 1710 51 27 - 1301,2-Dichlorobenzene
3330 1640 49 25 - 1301,3-Dichlorobenzene
3330 1630 49 26 - 1301,4-Dichlorobenzene
3330 2840 85 28 - 1303,3'-Dichlorobenzidine
3330 2150 65 35 - 1302,4-Dichlorophenol
3330 2170 65 10 - 1302,6-Dichlorophenol
3330 2420 73 42 - 130Diethyl phthalate
3330 2260 68 10 - 130Dimethoate
3330 2570 77 10 - 1307,12-Dimethylbenz(a)anthracene
3330 1700 15 U10 - 1303,3'-Dimethylbenzidine
6650 4250 64 31 - 1302,4-Dimethylphenol
3330 2360 71 43 - 130Dimethyl phthalate
TestAmerica Savannah Page 205 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
Solid
1.0
04/22/2010 2329Date Analyzed:
Lab Control Sample - Batch: 680-166138
Client Matrix:
Lab Sample ID:
Dilution:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
n7005.d
04/20/2010 1628
Analysis Batch: 680-166547
Prep Batch: 680-166138
30.07 g
1 mL
1 uL
Units: ug/Kg
Method: 8270C
Preparation: 3546
MSNLCS 680-166138/12-A
Analyte QualLimit% Rec.ResultSpike Amount
3330 2630 79 39 - 130Di-n-butyl phthalate
3330 2660 80 10 - 1301,3-Dinitrobenzene
3330 2870 86 22 - 1304,6-Dinitro-2-methylphenol
3330 3190 96 10 - 1372,4-Dinitrophenol
3330 2610 79 36 - 1302,4-Dinitrotoluene
3330 2510 75 38 - 1302,6-Dinitrotoluene
3330 2550 77 37 - 130Di-n-octyl phthalate
3330 2760 83 10 - 130Dinoseb
3330 627 19 10 - 1301,4-Dioxane
3330 2710 82 10 - 130Disulfoton
3330 1800 54 10 - 130Ethyl methanesulfonate
3330 2990 90 10 - 130Ethyl Parathion
3330 205 6 J *10 - 130Famphur
3330 2370 71 40 - 130Fluoranthene
3330 2220 67 38 - 130Fluorene
3330 2170 65 40 - 130Hexachlorobenzene
3330 1940 58 29 - 130Hexachlorobutadiene
3330 1740 52 10 - 130Hexachlorocyclopentadiene
3330 1700 51 23 - 130Hexachloroethane
16600 170000 5 U *10 - 130Hexachlorophene
3330 330 0 U *10 - 130Hexachloropropene
3330 2430 73 34 - 130Indeno[1,2,3-cd]pyrene
3330 1940 58 30 - 130Isophorone
3330 2350 71 10 - 130Isosafrole
3330 3240 97 J10 - 130Methapyrilene
3330 1650 50 10 - 1303-Methylcholanthrene
3330 180 5 J *10 - 130Methyl methanesulfonate
3330 2050 62 35 - 1302-Methylnaphthalene
3330 2850 86 10 - 130Methyl parathion
3330 2150 65 32 - 1302-Methylphenol
3330 2170 65 31 - 1303 & 4 Methylphenol
3330 1880 57 32 - 130Naphthalene
3330 18.0 1 J *10 - 1301,4-Naphthoquinone
3330 81.2 2 J *10 - 1301-Naphthylamine
3330 758 23 10 - 1302-Naphthylamine
3330 2380 71 29 - 1302-Nitroaniline
3330 2260 68 30 - 1303-Nitroaniline
3330 2520 76 32 - 1304-Nitroaniline
3330 1890 57 24 - 130Nitrobenzene
3330 2130 64 31 - 1302-Nitrophenol
3330 2750 83 18 - 1304-Nitrophenol
3330 2510 75 J10 - 1304-Nitroquinoline-1-oxide
3330 2190 66 10 - 130N-Nitro-o-toluidine
TestAmerica Savannah Page 206 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
Solid
1.0
04/22/2010 2329Date Analyzed:
Lab Control Sample - Batch: 680-166138
Client Matrix:
Lab Sample ID:
Dilution:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
n7005.d
04/20/2010 1628
Analysis Batch: 680-166547
Prep Batch: 680-166138
30.07 g
1 mL
1 uL
Units: ug/Kg
Method: 8270C
Preparation: 3546
MSNLCS 680-166138/12-A
Analyte QualLimit% Rec.ResultSpike Amount
3330 1910 58 10 - 130N-Nitrosodiethylamine
3330 1810 54 11 - 130N-Nitrosodimethylamine
3330 2370 71 10 - 130N-Nitrosodi-n-butylamine
3330 2380 72 26 - 130N-Nitrosodi-n-propylamine
3330 2460 74 43 - 130N-Nitrosodiphenylamine
3330 1940 58 10 - 130N-Nitrosomethylethylamine
3330 2320 70 10 - 130N-Nitrosomorpholine
3330 2070 62 10 - 130N-Nitrosopiperidine
3330 2130 64 10 - 130N-Nitrosopyrrolidine
3330 3760 113 10 - 130o,o',o''-Triethylphosphorothioate
3330 2610 78 10 - 130p-Dimethylamino azobenzene
3330 2210 67 10 - 130Pentachlorobenzene
3330 2500 75 10 - 130Pentachloronitrobenzene
3330 2770 83 26 - 130Pentachlorophenol
3330 2600 78 10 - 130Phenacetin
3330 2270 68 38 - 130Phenanthrene
3330 1950 59 31 - 130Phenol
3330 2320 70 10 - 130Phorate
3330 1340 40 10 - 1302-Picoline
16600 2390 14 10 - 130p-Phenylene diamine
3330 2520 76 10 - 130Pronamide
3330 2300 69 40 - 130Pyrene
3330 991 30 10 - 130Pyridine
3330 2230 67 10 - 130Safrole, Total
3330 2280 68 10 - 130Sulfotepp
3330 2020 61 10 - 1301,2,4,5-Tetrachlorobenzene
3330 2520 76 10 - 1302,3,4,6-Tetrachlorophenol
3330 2620 79 10 - 130Thionazin
3330 1070 32 10 - 1302-Toluidine
3330 1830 55 30 - 1301,2,4-Trichlorobenzene
3330 2260 68 38 - 1302,4,5-Trichlorophenol
3330 2150 65 36 - 1302,4,6-Trichlorophenol
3330 2880 87 10 - 1301,3,5-Trinitrobenzene
Surrogate % Rec Acceptance Limits
2,4,6-Tribromophenol 80 34 - 130
2-Fluorobiphenyl 60 34 - 130
2-Fluorophenol 57 30 - 130
Terphenyl-d14 69 39 - 130
Phenol-d5 62 30 - 130
Nitrobenzene-d5 60 27 - 130
TestAmerica Savannah Page 207 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
05/04/2010 1617
05/04/2010 1641
Solid
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 680-166138
50
50
MS Lab Sample ID:
MSD Lab Sample ID:
Client Matrix:
Date Prepared:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Client Matrix: Solid
Analysis Batch: 680-167473
Analysis Batch: 680-167473
04/20/2010 1628
04/20/2010 1628
Prep Batch: 680-166138
Prep Batch: 680-166138
g1028.d
30.03 g
1 mL
1 uL
g1029.d
30.09 g
1 mL
1 uL
Method: 8270C
Preparation: 3546
MSG
MSG
680-56861-21
680-56861-21
Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS
% Rec.
0 0 37 - 130 NC 50 U F U FAcenaphthene
56 0 37 - 130 NC 50 J U FAcenaphthylene
44 0 22 - 130 NC 50 J U FAcetophenone
0 43 10 - 130 NC 50 U F J2-Acetylaminofluorene
NC NC 10 - 130 NC 50 U Ualpha,alpha-Dimethyl phenethylamine
0 0 10 - 130 NC 50 U F U F4-Aminobiphenyl
0 0 13 - 130 NC 50 U F U FAniline
69 52 39 - 130 27 50 J JAnthracene
0 0 10 - 130 NC 50 U F U FAramite, Total
68 60 40 - 130 13 50 J JBenzo[a]anthracene
0 0 43 - 130 NC 50 U F U FBenzo[a]pyrene
59 0 35 - 130 NC 50 J U FBenzo[b]fluoranthene
62 57 37 - 130 8 50 J JBenzo[g,h,i]perylene
0 0 34 - 130 NC 50 U F U FBenzo[k]fluoranthene
-59 -61 25 - 130 2 50 J F J FBenzyl alcohol
-224 -248 31 - 130 4 50 4 41,1'-Biphenyl
79 0 30 - 130 NC 50 J U FBis(2-chloroethoxy)methane
0 0 16 - 130 NC 50 U F U FBis(2-chloroethyl)ether
66 52 15 - 130 23 50 J Jbis(chloroisopropyl) ether
87 65 38 - 130 30 50 J JBis(2-ethylhexyl) phthalate
71 55 35 - 130 26 50 J J4-Bromophenyl phenyl ether
91 78 41 - 130 16 50 J JButyl benzyl phthalate
0 0 23 - 130 NC 50 U F U F4-Chloroaniline
0 0 36 - 130 NC 50 U F U F4-Chloro-3-methylphenol
61 0 35 - 130 NC 50 J U F2-Chloronaphthalene
0 0 32 - 130 NC 50 U F U F2-Chlorophenol
0 59 40 - 130 NC 50 U F J4-Chlorophenyl phenyl ether
69 63 43 - 130 10 50 J JChrysene
NC NC 10 - 130 NC 50 U UDiallate
63 55 36 - 130 14 50 J JDibenz(a,h)anthracene
TestAmerica Savannah Page 208 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
05/04/2010 1617
05/04/2010 1641
Solid
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 680-166138
50
50
MS Lab Sample ID:
MSD Lab Sample ID:
Client Matrix:
Date Prepared:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Client Matrix: Solid
Analysis Batch: 680-167473
Analysis Batch: 680-167473
04/20/2010 1628
04/20/2010 1628
Prep Batch: 680-166138
Prep Batch: 680-166138
g1028.d
30.03 g
1 mL
1 uL
g1029.d
30.09 g
1 mL
1 uL
Method: 8270C
Preparation: 3546
MSG
MSG
680-56861-21
680-56861-21
Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS
% Rec.
63 60 38 - 130 5 50 J JDibenzofuran
59 0 27 - 130 NC 50 J U F1,2-Dichlorobenzene
0 0 25 - 130 NC 50 U F U F1,3-Dichlorobenzene
57 0 26 - 130 NC 50 J U F1,4-Dichlorobenzene
0 0 28 - 130 NC 50 U F U F3,3'-Dichlorobenzidine
0 0 35 - 130 NC 50 U F U F2,4-Dichlorophenol
0 0 10 - 130 NC 50 U F U F2,6-Dichlorophenol
84 69 42 - 130 20 50 J JDiethyl phthalate
50 45 10 - 130 11 50 J JDimethoate
0 31 10 - 130 NC 50 U F J7,12-Dimethylbenz(a)anthracene
NC NC 10 - 130 NC 50 U U3,3'-Dimethylbenzidine
0 0 31 - 130 NC 50 U F U F2,4-Dimethylphenol
0 52 43 - 130 NC 50 U F JDimethyl phthalate
102 92 39 - 130 11 50 J JDi-n-butyl phthalate
0 0 10 - 130 NC 50 U F U F1,3-Dinitrobenzene
NC NC 22 - 130 NC 50 U U4,6-Dinitro-2-methylphenol
NC NC 10 - 137 NC 50 U U2,4-Dinitrophenol
0 0 36 - 130 NC 50 U F U F2,4-Dinitrotoluene
0 0 38 - 130 NC 50 U F U F2,6-Dinitrotoluene
83 66 37 - 130 24 50 J JDi-n-octyl phthalate
NC NC 10 - 130 NC 50 U UDinoseb
NC NC 10 - 130 NC 50 U U1,4-Dioxane
63 0 10 - 130 NC 50 J U FDisulfoton
0 0 10 - 130 NC 50 U F U FEthyl methanesulfonate
2530 0 10 - 130 NC 50 F U FEthyl Parathion
49 0 10 - 130 NC 50 J U FFamphur
68 56 40 - 130 20 50 J JFluoranthene
57 0 38 - 130 NC 50 J U FFluorene
66 0 40 - 130 NC 50 J U FHexachlorobenzene
67 0 29 - 130 NC 50 J U FHexachlorobutadiene
TestAmerica Savannah Page 209 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
05/04/2010 1617
05/04/2010 1641
Solid
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 680-166138
50
50
MS Lab Sample ID:
MSD Lab Sample ID:
Client Matrix:
Date Prepared:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Client Matrix: Solid
Analysis Batch: 680-167473
Analysis Batch: 680-167473
04/20/2010 1628
04/20/2010 1628
Prep Batch: 680-166138
Prep Batch: 680-166138
g1028.d
30.03 g
1 mL
1 uL
g1029.d
30.09 g
1 mL
1 uL
Method: 8270C
Preparation: 3546
MSG
MSG
680-56861-21
680-56861-21
Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS
% Rec.
0 0 10 - 130 NC 50 U F U FHexachlorocyclopentadiene
75 53 23 - 130 36 50 J JHexachloroethane
NC NC 10 - 130 NC 50 U UHexachlorophene
0 0 10 - 130 NC 50 U F U FHexachloropropene
59 56 34 - 130 6 50 J JIndeno[1,2,3-cd]pyrene
58 0 30 - 130 NC 50 J U FIsophorone
62 0 10 - 130 NC 50 J U FIsosafrole
NC NC 10 - 130 NC 50 U UMethapyrilene
0 0 10 - 130 NC 50 U F U F3-Methylcholanthrene
0 0 10 - 130 NC 50 U F U FMethyl methanesulfonate
61 0 35 - 130 NC 50 J U F2-Methylnaphthalene
0 0 10 - 130 NC 50 U F U FMethyl parathion
0 0 32 - 130 NC 50 U F U F2-Methylphenol
0 0 31 - 130 NC 50 U F U F3 & 4 Methylphenol
63 51 32 - 130 21 50 J JNaphthalene
0 0 10 - 130 NC 50 U F U F1,4-Naphthoquinone
NC 0 10 - 130 NC 50 U U F1-Naphthylamine
0 0 10 - 130 NC 50 U F U F2-Naphthylamine
0 449 29 - 130 NC 50 U F J F2-Nitroaniline
0 0 30 - 130 NC 50 U F U F3-Nitroaniline
0 0 32 - 130 NC 50 U F U F4-Nitroaniline
0 0 24 - 130 NC 50 U F U FNitrobenzene
0 0 31 - 130 NC 50 U F U F2-Nitrophenol
NC NC 18 - 130 NC 50 U U4-Nitrophenol
NC NC 10 - 130 NC 50 U U4-Nitroquinoline-1-oxide
0 0 10 - 130 NC 50 U F U FN-Nitro-o-toluidine
0 0 10 - 130 NC 50 U F U FN-Nitrosodiethylamine
NC NC 11 - 130 NC 50 U UN-Nitrosodimethylamine
0 45 10 - 130 NC 50 U F JN-Nitrosodi-n-butylamine
57 0 26 - 130 NC 50 J U FN-Nitrosodi-n-propylamine
TestAmerica Savannah Page 210 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
05/04/2010 1617
05/04/2010 1641
Solid
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 680-166138
50
50
MS Lab Sample ID:
MSD Lab Sample ID:
Client Matrix:
Date Prepared:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Client Matrix: Solid
Analysis Batch: 680-167473
Analysis Batch: 680-167473
04/20/2010 1628
04/20/2010 1628
Prep Batch: 680-166138
Prep Batch: 680-166138
g1028.d
30.03 g
1 mL
1 uL
g1029.d
30.09 g
1 mL
1 uL
Method: 8270C
Preparation: 3546
MSG
MSG
680-56861-21
680-56861-21
Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS
% Rec.
54 51 43 - 130 7 50 J JN-Nitrosodiphenylamine
0 0 10 - 130 NC 50 U F U FN-Nitrosomethylethylamine
0 0 10 - 130 NC 50 U F U FN-Nitrosomorpholine
57 45 10 - 130 24 50 J JN-Nitrosopiperidine
0 0 10 - 130 NC 50 U F U FN-Nitrosopyrrolidine
12 -58 10 - 130 36 50 J J Fo,o',o''-Triethylphosphorothioate
41 42 10 - 130 2 50 J Jp-Dimethylamino azobenzene
67 54 10 - 130 21 50 J JPentachlorobenzene
0 0 10 - 130 NC 50 U F U FPentachloronitrobenzene
NC NC 26 - 130 NC 50 U UPentachlorophenol
0 0 10 - 130 NC 50 U F U FPhenacetin
63 55 38 - 130 13 50 J JPhenanthrene
0 0 31 - 130 NC 50 U F U FPhenol
55 0 10 - 130 NC 50 J U FPhorate
0 0 10 - 130 NC 50 U F U F2-Picoline
NC NC 10 - 130 NC 50 U Up-Phenylene diamine
57 49 10 - 130 16 50 J JPronamide
61 55 40 - 130 11 50 J JPyrene
0 0 10 - 130 NC 50 U F U FPyridine
59 45 10 - 130 27 50 J JSafrole, Total
96 84 10 - 130 13 50 J JSulfotepp
0 0 10 - 130 NC 50 U F U F1,2,4,5-Tetrachlorobenzene
50 41 10 - 130 21 50 J J2,3,4,6-Tetrachlorophenol
57 0 10 - 130 NC 50 J U FThionazin
0 0 10 - 130 NC 50 U F U F2-Toluidine
58 48 30 - 130 20 50 J J1,2,4-Trichlorobenzene
0 0 38 - 130 NC 50 U F U F2,4,5-Trichlorophenol
0 0 36 - 130 NC 50 U F U F2,4,6-Trichlorophenol
NC NC 10 - 130 NC 50 U U1,3,5-Trinitrobenzene
-1020 -1120 10 - 130 6 50 4 4Diphenyl ether
TestAmerica Savannah Page 211 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
Surrogate MS % Rec MSD % Rec Acceptance Limits
2,4,6-Tribromophenol 0 0 34 - 130D D
2-Fluorobiphenyl 0 0 34 - 130D D
2-Fluorophenol 0 0 30 - 130D D
Terphenyl-d14 0 0 39 - 130D D
Phenol-d5 0 0 30 - 130D D
Nitrobenzene-d5 0 0 27 - 130D D
TestAmerica Savannah Page 212 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
SolidClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
05/03/2010 1645
Method Blank - Batch: 680-166147
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Analysis Batch: 680-167447
Prep Batch: 680-166147
04/20/2010 2315
g1004.d
30.11 g
1.0 mL
1 uL
Units: ug/Kg
Method: 8270C
Preparation: 3546
MSGMB 680-166147/21-A
Analyte Result Qual MDL RL
330 U 33041Acenaphthene
330 U 33036Acenaphthylene
330 U 33028Acetophenone
330 U 330282-Acetylaminofluorene
67000 U 670002700alpha,alpha-Dimethyl phenethylamine
330 U 330374-Aminobiphenyl
660 U 66034Aniline
330 U 33025Anthracene
330 U 33057Aramite, Total
330 U 33027Benzo[a]anthracene
330 U 33052Benzo[a]pyrene
330 U 33038Benzo[b]fluoranthene
330 U 33022Benzo[g,h,i]perylene
330 U 33065Benzo[k]fluoranthene
330 U 33033Benzyl alcohol
330 U 330281,1'-Biphenyl
330 U 33039Bis(2-chloroethoxy)methane
330 U 33045Bis(2-chloroethyl)ether
330 U 33030bis(chloroisopropyl) ether
330 U 33033Bis(2-ethylhexyl) phthalate
330 U 330364-Bromophenyl phenyl ether
330 U 33026Butyl benzyl phthalate
660 U 660524-Chloroaniline
330 U 330354-Chloro-3-methylphenol
330 U 330392-Chloronaphthalene
330 U 330402-Chlorophenol
330 U 330374-Chlorophenyl phenyl ether
330 U 33021Chrysene
330 U 330170Diallate
330 U 33024Dibenz(a,h)anthracene
330 U 33033Dibenzofuran
330 U 330371,2-Dichlorobenzene
330 U 330341,3-Dichlorobenzene
330 U 330351,4-Dichlorobenzene
660 U 660283,3'-Dichlorobenzidine
330 U 330352,4-Dichlorophenol
330 U 330272,6-Dichlorophenol
330 U 33035Diethyl phthalate
330 U 33025Dimethoate
330 U 330177,12-Dimethylbenz(a)anthracene
1700 U 17008303,3'-Dimethylbenzidine
330 U 330442,4-Dimethylphenol
330 U 33034Dimethyl phthalate
TestAmerica Savannah Page 213 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
SolidClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
05/03/2010 1645
Method Blank - Batch: 680-166147
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Analysis Batch: 680-167447
Prep Batch: 680-166147
04/20/2010 2315
g1004.d
30.11 g
1.0 mL
1 uL
Units: ug/Kg
Method: 8270C
Preparation: 3546
MSGMB 680-166147/21-A
Analyte Result Qual MDL RL
330 U 33030Di-n-butyl phthalate
330 U 330241,3-Dinitrobenzene
1700 U 17001704,6-Dinitro-2-methylphenol
1700 U 17008302,4-Dinitrophenol
330 U 330492,4-Dinitrotoluene
330 U 330422,6-Dinitrotoluene
330 U 33029Di-n-octyl phthalate
330 U 330160Dinoseb
330 U 3301201,4-Dioxane
330 U 33017Disulfoton
330 U 33031Ethyl methanesulfonate
330 U 33022Ethyl Parathion
330 U 33029Famphur
330 U 33032Fluoranthene
330 U 33036Fluorene
330 U 33039Hexachlorobenzene
330 U 33036Hexachlorobutadiene
330 U 33041Hexachlorocyclopentadiene
330 U 33028Hexachloroethane
170000 U 17000013000Hexachlorophene
330 U 33029Hexachloropropene
330 U 33028Indeno[1,2,3-cd]pyrene
330 U 33033Isophorone
330 U 33024Isosafrole
67000 U 67000830Methapyrilene
330 U 330413-Methylcholanthrene
330 U 33017Methyl methanesulfonate
330 U 330382-Methylnaphthalene
330 U 33026Methyl parathion
330 U 330272-Methylphenol
330 U 330433 & 4 Methylphenol
330 U 33030Naphthalene
330 U 330171,4-Naphthoquinone
330 U 330661-Naphthylamine
330 U 330342-Naphthylamine
1700 U 1700452-Nitroaniline
1700 U 1700463-Nitroaniline
1700 U 1700494-Nitroaniline
330 U 33026Nitrobenzene
330 U 330412-Nitrophenol
1700 U 17003304-Nitrophenol
3300 U 33008304-Nitroquinoline-1-oxide
330 U 33026N-Nitro-o-toluidine
TestAmerica Savannah Page 214 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
SolidClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
05/03/2010 1645
Method Blank - Batch: 680-166147
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Analysis Batch: 680-167447
Prep Batch: 680-166147
04/20/2010 2315
g1004.d
30.11 g
1.0 mL
1 uL
Units: ug/Kg
Method: 8270C
Preparation: 3546
MSGMB 680-166147/21-A
Analyte Result Qual MDL RL
330 U 33028N-Nitrosodiethylamine
330 U 330120N-Nitrosodimethylamine
330 U 33024N-Nitrosodi-n-butylamine
330 U 33032N-Nitrosodi-n-propylamine
330 U 33033N-Nitrosodiphenylamine
330 U 33025N-Nitrosomethylethylamine
330 U 33027N-Nitrosomorpholine
330 U 33021N-Nitrosopiperidine
330 U 33018N-Nitrosopyrrolidine
330 U 33040o,o',o''-Triethylphosphorothioate
330 U 33019p-Dimethylamino azobenzene
330 U 33025Pentachlorobenzene
330 U 33021Pentachloronitrobenzene
1700 U 1700330Pentachlorophenol
330 U 33033Phenacetin
330 U 33027Phenanthrene
330 U 33034Phenol
330 U 33022Phorate
330 U 330172-Picoline
1700 U 1700830p-Phenylene diamine
330 U 33024Pronamide
330 U 33027Pyrene
330 U 33029Pyridine
330 U 33024Safrole, Total
330 U 33020Sulfotepp
330 U 330311,2,4,5-Tetrachlorobenzene
330 U 330222,3,4,6-Tetrachlorophenol
330 U 33023Thionazin
330 U 330352-Toluidine
330 U 330311,2,4-Trichlorobenzene
330 U 330352,4,5-Trichlorophenol
330 U 330292,4,6-Trichlorophenol
330 U 3301701,3,5-Trinitrobenzene
330 U 33034Diphenyl ether
Surrogate % Rec Acceptance Limits
2,4,6-Tribromophenol 94 34 - 130
2-Fluorobiphenyl 81 34 - 130
2-Fluorophenol 76 30 - 130
Terphenyl-d14 99 39 - 130
Phenol-d5 81 30 - 130
Nitrobenzene-d5 78 27 - 130
TestAmerica Savannah Page 215 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
Solid
1.0
05/03/2010 1709Date Analyzed:
Lab Control Sample - Batch: 680-166147
Client Matrix:
Lab Sample ID:
Dilution:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
g1005.d
04/20/2010 2315
Analysis Batch: 680-167447
Prep Batch: 680-166147
30.08 g
1.0 mL
1 uL
Units: ug/Kg
Method: 8270C
Preparation: 3546
MSGLCS 680-166147/22-A
Analyte QualLimit% Rec.ResultSpike Amount
3320 2710 82 37 - 130Acenaphthene
3320 2890 87 37 - 130Acenaphthylene
3320 2010 61 22 - 130Acetophenone
3320 3260 98 10 - 1302-Acetylaminofluorene
16600 16700 100 J E10 - 130alpha,alpha-Dimethyl phenethylamine
3320 423 13 10 - 1304-Aminobiphenyl
3320 1090 33 13 - 130Aniline
3320 3260 98 39 - 130Anthracene
3320 2900 87 10 - 130Aramite, Total
3320 3670 111 10 - 130Aramite, Total
3320 3780 114 10 - 130Aramite, Total
3320 3100 93 40 - 130Benzo[a]anthracene
3320 3200 96 43 - 130Benzo[a]pyrene
3320 3270 98 35 - 130Benzo[b]fluoranthene
3320 2830 85 37 - 130Benzo[g,h,i]perylene
3320 3460 104 34 - 130Benzo[k]fluoranthene
3320 2650 80 25 - 130Benzyl alcohol
3320 2850 86 31 - 1301,1'-Biphenyl
3320 3400 102 30 - 130Bis(2-chloroethoxy)methane
3320 2440 73 16 - 130Bis(2-chloroethyl)ether
3320 2660 80 15 - 130bis(chloroisopropyl) ether
3320 3620 109 38 - 130Bis(2-ethylhexyl) phthalate
3320 3240 97 35 - 1304-Bromophenyl phenyl ether
3320 3600 108 41 - 130Butyl benzyl phthalate
3320 1220 37 23 - 1304-Chloroaniline
3320 2860 86 36 - 1304-Chloro-3-methylphenol
3320 2830 85 35 - 1302-Chloronaphthalene
3320 2600 78 32 - 1302-Chlorophenol
3320 3060 92 40 - 1304-Chlorophenyl phenyl ether
3320 3360 101 43 - 130Chrysene
3320 3040 91 10 - 130Diallate
3320 2840 85 36 - 130Dibenz(a,h)anthracene
3320 2810 85 38 - 130Dibenzofuran
3320 2410 72 27 - 1301,2-Dichlorobenzene
3320 2240 67 25 - 1301,3-Dichlorobenzene
3320 2350 71 26 - 1301,4-Dichlorobenzene
3320 3190 96 28 - 1303,3'-Dichlorobenzidine
3320 2550 77 35 - 1302,4-Dichlorophenol
3320 2720 82 10 - 1302,6-Dichlorophenol
3320 3220 97 42 - 130Diethyl phthalate
3320 2140 64 10 - 130Dimethoate
3320 3380 102 10 - 1307,12-Dimethylbenz(a)anthracene
3320 1700 13 U10 - 1303,3'-Dimethylbenzidine
TestAmerica Savannah Page 216 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
Solid
1.0
05/03/2010 1709Date Analyzed:
Lab Control Sample - Batch: 680-166147
Client Matrix:
Lab Sample ID:
Dilution:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
g1005.d
04/20/2010 2315
Analysis Batch: 680-167447
Prep Batch: 680-166147
30.08 g
1.0 mL
1 uL
Units: ug/Kg
Method: 8270C
Preparation: 3546
MSGLCS 680-166147/22-A
Analyte QualLimit% Rec.ResultSpike Amount
6650 5190 78 31 - 1302,4-Dimethylphenol
3320 3050 92 43 - 130Dimethyl phthalate
3320 3460 104 39 - 130Di-n-butyl phthalate
3320 3250 98 10 - 1301,3-Dinitrobenzene
3320 3650 110 22 - 1304,6-Dinitro-2-methylphenol
3320 3360 101 10 - 1372,4-Dinitrophenol
3320 3160 95 36 - 1302,4-Dinitrotoluene
3320 3140 95 38 - 1302,6-Dinitrotoluene
3320 3770 113 37 - 130Di-n-octyl phthalate
3320 3700 111 10 - 130Dinoseb
3320 1020 31 10 - 1301,4-Dioxane
3320 3440 103 10 - 130Disulfoton
3320 2130 64 10 - 130Ethyl methanesulfonate
3320 3620 109 10 - 130Ethyl Parathion
3320 135 4 J *10 - 130Famphur
3320 3120 94 40 - 130Fluoranthene
3320 3030 91 38 - 130Fluorene
3320 2950 89 40 - 130Hexachlorobenzene
3320 2730 82 29 - 130Hexachlorobutadiene
3320 1070 32 10 - 130Hexachlorocyclopentadiene
3320 2420 73 23 - 130Hexachloroethane
16600 170000 36 U10 - 130Hexachlorophene
3320 330 0 U *10 - 130Hexachloropropene
3320 2850 86 34 - 130Indeno[1,2,3-cd]pyrene
3320 2380 72 30 - 130Isophorone
3320 2820 85 10 - 130Isosafrole
3320 3060 92 J10 - 130Methapyrilene
3320 2000 60 10 - 1303-Methylcholanthrene
3320 207 6 J *10 - 130Methyl methanesulfonate
3320 2650 80 35 - 1302-Methylnaphthalene
3320 3040 92 10 - 130Methyl parathion
3320 2750 83 32 - 1302-Methylphenol
3320 3520 106 31 - 1303 & 4 Methylphenol
3320 3310 100 32 - 130Naphthalene
3320 330 0 U *10 - 1301,4-Naphthoquinone
3320 330 1 U *10 - 1301-Naphthylamine
3320 764 23 10 - 1302-Naphthylamine
3320 2590 78 29 - 1302-Nitroaniline
3320 1930 58 30 - 1303-Nitroaniline
3320 2630 79 32 - 1304-Nitroaniline
3320 2240 68 24 - 130Nitrobenzene
3320 2610 79 31 - 1302-Nitrophenol
3320 3080 93 18 - 1304-Nitrophenol
TestAmerica Savannah Page 217 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
Solid
1.0
05/03/2010 1709Date Analyzed:
Lab Control Sample - Batch: 680-166147
Client Matrix:
Lab Sample ID:
Dilution:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
g1005.d
04/20/2010 2315
Analysis Batch: 680-167447
Prep Batch: 680-166147
30.08 g
1.0 mL
1 uL
Units: ug/Kg
Method: 8270C
Preparation: 3546
MSGLCS 680-166147/22-A
Analyte QualLimit% Rec.ResultSpike Amount
3320 1900 57 J10 - 1304-Nitroquinoline-1-oxide
3320 1820 55 10 - 130N-Nitro-o-toluidine
3320 2520 76 10 - 130N-Nitrosodiethylamine
3320 2290 69 11 - 130N-Nitrosodimethylamine
3320 3890 117 10 - 130N-Nitrosodi-n-butylamine
3320 3120 94 26 - 130N-Nitrosodi-n-propylamine
3320 3400 102 43 - 130N-Nitrosodiphenylamine
3320 2300 69 10 - 130N-Nitrosomethylethylamine
3320 3160 95 10 - 130N-Nitrosomorpholine
3320 2620 79 10 - 130N-Nitrosopiperidine
3320 3060 92 10 - 130N-Nitrosopyrrolidine
3320 4760 143 *10 - 130o,o',o''-Triethylphosphorothioate
3320 3000 90 10 - 130p-Dimethylamino azobenzene
3320 2800 84 10 - 130Pentachlorobenzene
3320 3340 101 10 - 130Pentachloronitrobenzene
3320 3720 112 26 - 130Pentachlorophenol
3320 3150 95 10 - 130Phenacetin
3320 3030 91 38 - 130Phenanthrene
3320 2390 72 31 - 130Phenol
3320 4490 135 *10 - 130Phorate
3320 587 18 10 - 1302-Picoline
16600 1700 4 U *10 - 130p-Phenylene diamine
3320 3220 97 10 - 130Pronamide
3320 3040 91 40 - 130Pyrene
3320 1460 44 10 - 130Pyridine
3320 2870 86 10 - 130Safrole, Total
3320 3090 93 10 - 130Sulfotepp
3320 2720 82 10 - 1301,2,4,5-Tetrachlorobenzene
3320 2990 90 10 - 1302,3,4,6-Tetrachlorophenol
3320 3220 97 10 - 130Thionazin
3320 606 18 10 - 1302-Toluidine
3320 2450 74 30 - 1301,2,4-Trichlorobenzene
3320 2960 89 38 - 1302,4,5-Trichlorophenol
3320 2670 80 36 - 1302,4,6-Trichlorophenol
3320 1960 59 10 - 1301,3,5-Trinitrobenzene
3320 2760 83 10 - 130Diphenyl ether
Surrogate % Rec Acceptance Limits
2,4,6-Tribromophenol 101 34 - 130
2-Fluorobiphenyl 82 34 - 130
2-Fluorophenol 70 30 - 130
Terphenyl-d14 95 39 - 130
Phenol-d5 79 30 - 130
TestAmerica Savannah Page 218 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
Surrogate % Rec Acceptance Limits
Nitrobenzene-d5 74 27 - 130
TestAmerica Savannah Page 219 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
WaterClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
04/24/2010 1924
Method Blank - Batch: 680-166243
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Analysis Batch: 680-166695
Prep Batch: 680-166243
04/21/2010 1423
g0748.d
1000 mL
1 mL
1 uL
Units: ug/L
Method: 8270C
Preparation: 3520C
MSGMB 680-166243/7-A
Analyte Result Qual MDL RL
10 U 100.76Acenaphthene
10 U 100.85Acenaphthylene
10 U 100.57Acetophenone
10 U 101.62-Acetylaminofluorene
2000 U 200035alpha,alpha-Dimethyl phenethylamine
10 U 101.24-Aminobiphenyl
20 U 202.1Aniline
10 U 100.69Anthracene
10 U 100.91Aramite, Total
10 U 100.55Benzo[a]anthracene
10 U 100.71Benzo[a]pyrene
10 U 102.6Benzo[b]fluoranthene
10 U 100.87Benzo[g,h,i]perylene
10 U 101.2Benzo[k]fluoranthene
10 U 101.1Benzyl alcohol
10 U 100.581,1'-Biphenyl
10 U 100.94Bis(2-chloroethoxy)methane
10 U 101.1Bis(2-chloroethyl)ether
10 U 100.78bis(chloroisopropyl) ether
10 U 101.6Bis(2-ethylhexyl) phthalate
10 U 100.774-Bromophenyl phenyl ether
10 U 101.2Butyl benzyl phthalate
20 U 202.24-Chloroaniline
10 U 101.04-Chloro-3-methylphenol
10 U 100.802-Chloronaphthalene
10 U 100.872-Chlorophenol
10 U 100.844-Chlorophenyl phenyl ether
10 U 100.51Chrysene
10 U 100.78Diallate
10 U 101.0Dibenz(a,h)anthracene
10 U 100.79Dibenzofuran
10 U 100.531,2-Dichlorobenzene
10 U 100.591,3-Dichlorobenzene
10 U 100.541,4-Dichlorobenzene
60 U 60303,3'-Dichlorobenzidine
10 U 101.12,4-Dichlorophenol
10 U 100.732,6-Dichlorophenol
10 U 100.88Diethyl phthalate
10 U 100.75Dimethoate
10 U 101.27,12-Dimethylbenz(a)anthracene
20 U 20103,3'-Dimethylbenzidine
10 U 104.02,4-Dimethylphenol
10 U 100.99Dimethyl phthalate
TestAmerica Savannah Page 220 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
WaterClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
04/24/2010 1924
Method Blank - Batch: 680-166243
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Analysis Batch: 680-166695
Prep Batch: 680-166243
04/21/2010 1423
g0748.d
1000 mL
1 mL
1 uL
Units: ug/L
Method: 8270C
Preparation: 3520C
MSGMB 680-166243/7-A
Analyte Result Qual MDL RL
10 U 100.83Di-n-butyl phthalate
10 U 100.601,3-Dinitrobenzene
50 U 50104,6-Dinitro-2-methylphenol
50 U 50102,4-Dinitrophenol
10 U 101.22,4-Dinitrotoluene
10 U 101.12,6-Dinitrotoluene
10 U 101.4Di-n-octyl phthalate
10 U 105.0Dinoseb
10 U 103.41,4-Dioxane
10 U 100.79Disulfoton
10 U 100.96Ethyl methanesulfonate
10 U 101.3Ethyl Parathion
10 U 101.1Famphur
10 U 100.74Fluoranthene
10 U 100.96Fluorene
10 U 100.79Hexachlorobenzene
10 U 100.62Hexachlorobutadiene
10 U 102.5Hexachlorocyclopentadiene
10 U 100.76Hexachloroethane
5000 U 500027Hexachlorophene
10 U 101.4Hexachloropropene
10 U 101.0Indeno[1,2,3-cd]pyrene
10 U 100.90Isophorone
10 U 100.50Isosafrole
2000 U 20002.7Methapyrilene
10 U 101.43-Methylcholanthrene
10 U 100.60Methyl methanesulfonate
10 U 100.782-Methylnaphthalene
10 U 100.88Methyl parathion
10 U 100.892-Methylphenol
10 U 101.33 & 4 Methylphenol
10 U 100.70Naphthalene
10 U 100.621,4-Naphthoquinone
10 U 101.11-Naphthylamine
10 U 101.52-Naphthylamine
50 U 501.32-Nitroaniline
50 U 505.03-Nitroaniline
50 U 505.04-Nitroaniline
10 U 100.73Nitrobenzene
10 U 100.762-Nitrophenol
50 U 501.94-Nitrophenol
20 U 20104-Nitroquinoline-1-oxide
10 U 101.5N-Nitro-o-toluidine
TestAmerica Savannah Page 221 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
WaterClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
04/24/2010 1924
Method Blank - Batch: 680-166243
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Analysis Batch: 680-166695
Prep Batch: 680-166243
04/21/2010 1423
g0748.d
1000 mL
1 mL
1 uL
Units: ug/L
Method: 8270C
Preparation: 3520C
MSGMB 680-166243/7-A
Analyte Result Qual MDL RL
10 U 100.93N-Nitrosodiethylamine
10 U 102.8N-Nitrosodimethylamine
10 U 100.96N-Nitrosodi-n-butylamine
10 U 100.72N-Nitrosodi-n-propylamine
10 U 100.92N-Nitrosodiphenylamine
10 U 103.3N-Nitrosomethylethylamine
10 U 100.84N-Nitrosomorpholine
10 U 100.88N-Nitrosopiperidine
10 U 101.0N-Nitrosopyrrolidine
10 U 101.0o,o',o''-Triethylphosphorothioate
10 U 100.79p-Dimethylamino azobenzene
10 U 100.52Pentachlorobenzene
10 U 100.78Pentachloronitrobenzene
50 U 502.0Pentachlorophenol
10 U 101.4Phenacetin
10 U 100.77Phenanthrene
10 U 100.83Phenol
10 U 100.87Phorate
10 U 101.42-Picoline
2000 U 200010p-Phenylene diamine
10 U 100.89Pronamide
10 U 100.63Pyrene
50 U 502.3Pyridine
10 U 100.80Safrole, Total
10 U 100.53Sulfotepp
10 U 100.761,2,4,5-Tetrachlorobenzene
10 U 100.722,3,4,6-Tetrachlorophenol
10 U 100.91Thionazin
10 U 101.42-Toluidine
10 U 100.561,2,4-Trichlorobenzene
10 U 101.22,4,5-Trichlorophenol
10 U 100.852,4,6-Trichlorophenol
10 U 102.01,3,5-Trinitrobenzene
Surrogate % Rec Acceptance Limits
2,4,6-Tribromophenol 102 40 - 139
2-Fluorobiphenyl 88 50 - 113
2-Fluorophenol 75 36 - 110
Terphenyl-d14 103 10 - 121
Phenol-d5 82 38 - 116
Nitrobenzene-d5 90 45 - 112
TestAmerica Savannah Page 222 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
04/25/2010 2044
04/24/2010 2059
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report - Batch: 680-166243
1.0
1.0
Water
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Client Matrix: Water
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
ug/L
04/21/2010 1423
Prep Batch: 680-166243
Analysis Batch: 680-166687
g0794.d
1000 mL
1 mL
1 uL
g0752.d
1000 mL
1 mL
1 uL
ug/L
04/21/2010 1423
Analysis Batch: 680-166695
Prep Batch: 680-166243
Method: 8270C
Preparation: 3520C
MSG
MSG
LCS 680-166243/8-A
LCSD 680-166243/9-A
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
8998 45 - 117 9 40Acenaphthene
91100 51 - 112 9 40Acenaphthylene
7883 25 - 110 6 40Acetophenone
105103 69 - 123 2 402-Acetylaminofluorene
221197 10 - 158 11 40 J E * J E *alpha,alpha-Dimethyl phenethylamine
2432 10 - 130 28 404-Aminobiphenyl
7876 10 - 114 2 40Aniline
93100 52 - 116 7 40Anthracene
114102 10 - 150 3 40Aramite, Total
99102 10 - 150 3 40Aramite, Total
99102 10 - 150 3 40Aramite, Total
114117 10 - 150 3 40Aramite, Total
99117 10 - 150 3 40Aramite, Total
99117 10 - 150 3 40Aramite, Total
11496 10 - 150 3 40Aramite, Total
9996 10 - 150 3 40Aramite, Total
9996 10 - 150 3 40Aramite, Total
100101 49 - 124 1 40Benzo[a]anthracene
100102 48 - 120 2 40Benzo[a]pyrene
106101 46 - 126 5 40Benzo[b]fluoranthene
9999 51 - 117 0 40Benzo[g,h,i]perylene
101106 47 - 126 5 40Benzo[k]fluoranthene
9192 34 - 113 1 40Benzyl alcohol
94101 47 - 112 8 401,1'-Biphenyl
124130 50 - 112 5 40 * *Bis(2-chloroethoxy)methane
9496 43 - 110 2 40Bis(2-chloroethyl)ether
9697 42 - 110 1 40bis(chloroisopropyl) ether
122118 47 - 134 3 40Bis(2-ethylhexyl) phthalate
96103 42 - 110 8 404-Bromophenyl phenyl ether
121123 52 - 135 2 40Butyl benzyl phthalate
9091 10 - 110 1 404-Chloroaniline
9298 46 - 118 6 404-Chloro-3-methylphenol
94101 47 - 110 7 402-Chloronaphthalene
TestAmerica Savannah Page 223 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
04/25/2010 2044
04/24/2010 2059
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report - Batch: 680-166243
1.0
1.0
Water
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Client Matrix: Water
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
ug/L
04/21/2010 1423
Prep Batch: 680-166243
Analysis Batch: 680-166687
g0794.d
1000 mL
1 mL
1 uL
g0752.d
1000 mL
1 mL
1 uL
ug/L
04/21/2010 1423
Analysis Batch: 680-166695
Prep Batch: 680-166243
Method: 8270C
Preparation: 3520C
MSG
MSG
LCS 680-166243/8-A
LCSD 680-166243/9-A
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
8486 47 - 110 2 402-Chlorophenol
97105 46 - 114 8 404-Chlorophenyl phenyl ether
98101 51 - 123 4 40Chrysene
98108 36 - 145 10 40Diallate
100100 46 - 124 0 40Dibenz(a,h)anthracene
9099 50 - 112 10 40Dibenzofuran
7475 39 - 110 1 401,2-Dichlorobenzene
7273 36 - 110 1 401,3-Dichlorobenzene
7271 38 - 110 1 401,4-Dichlorobenzene
107103 10 - 113 3 403,3'-Dichlorobenzidine
8689 46 - 115 4 402,4-Dichlorophenol
8689 46 - 130 3 402,6-Dichlorophenol
103112 51 - 119 8 40Diethyl phthalate
88100 28 - 142 12 40Dimethoate
9392 39 - 130 2 407,12-Dimethylbenz(a)anthracene
2218 10 - 130 17 40 J3,3'-Dimethylbenzidine
8993 36 - 110 5 402,4-Dimethylphenol
99108 50 - 116 9 40Dimethyl phthalate
108113 49 - 123 5 40Di-n-butyl phthalate
10594 53 - 136 11 401,3-Dinitrobenzene
119100 29 - 167 17 404,6-Dinitro-2-methylphenol
135112 10 - 189 18 402,4-Dinitrophenol
108104 49 - 128 4 402,4-Dinitrotoluene
100103 45 - 131 3 402,6-Dinitrotoluene
122122 44 - 134 0 40Di-n-octyl phthalate
10988 50 - 144 21 40Dinoseb
5968 11 - 110 14 401,4-Dioxane
111116 40 - 130 4 40Disulfoton
7577 32 - 130 3 40Ethyl methanesulfonate
106102 60 - 140 4 40Ethyl Parathion
718 10 - 130 90 40 J *Famphur
9498 50 - 120 4 40Fluoranthene
95101 50 - 115 6 40Fluorene
TestAmerica Savannah Page 224 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
04/25/2010 2044
04/24/2010 2059
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report - Batch: 680-166243
1.0
1.0
Water
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Client Matrix: Water
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
ug/L
04/21/2010 1423
Prep Batch: 680-166243
Analysis Batch: 680-166687
g0794.d
1000 mL
1 mL
1 uL
g0752.d
1000 mL
1 mL
1 uL
ug/L
04/21/2010 1423
Analysis Batch: 680-166695
Prep Batch: 680-166243
Method: 8270C
Preparation: 3520C
MSG
MSG
LCS 680-166243/8-A
LCSD 680-166243/9-A
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
9299 48 - 119 7 40Hexachlorobenzene
8083 40 - 110 3 40Hexachlorobutadiene
4439 10 - 110 10 40Hexachlorocyclopentadiene
7575 33 - 110 0 40Hexachloroethane
6948 10 - 130 36 40 J JHexachlorophene
00 10 - 130 NC 40 U * U *Hexachloropropene
9899 40 - 126 1 40Indeno[1,2,3-cd]pyrene
8794 50 - 111 8 40Isophorone
8996 37 - 130 8 40Isosafrole
101142 10 - 130 34 40 J * JMethapyrilene
6464 62 - 130 1 403-Methylcholanthrene
77 10 - 130 1 40 J * J *Methyl methanesulfonate
8589 46 - 110 4 402-Methylnaphthalene
106104 51 - 146 3 40Methyl parathion
9291 46 - 110 1 402-Methylphenol
9394 43 - 110 2 403 & 4 Methylphenol
8386 41 - 110 3 40Naphthalene
911 10 - 130 22 40 J *1,4-Naphthoquinone
22 10 - 130 5 40 J * J *1-Naphthylamine
3032 10 - 130 6 402-Naphthylamine
100103 45 - 122 3 402-Nitroaniline
9297 30 - 116 6 403-Nitroaniline
98103 36 - 125 5 404-Nitroaniline
8889 46 - 110 1 40Nitrobenzene
9288 42 - 120 4 402-Nitrophenol
102111 30 - 122 8 404-Nitrophenol
7861 10 - 151 24 404-Nitroquinoline-1-oxide
8788 45 - 130 1 40N-Nitro-o-toluidine
9391 48 - 130 2 40N-Nitrosodiethylamine
100105 33 - 110 5 40N-Nitrosodimethylamine
138140 41 - 130 1 40 * *N-Nitrosodi-n-butylamine
110110 45 - 112 1 40N-Nitrosodi-n-propylamine
105111 47 - 119 6 40N-Nitrosodiphenylamine
TestAmerica Savannah Page 225 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
04/25/2010 2044
04/24/2010 2059
Lab Control Sample/
Lab Control Sample Duplicate Recovery Report - Batch: 680-166243
1.0
1.0
Water
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
Client Matrix: Water
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Injection Volume:
ug/L
04/21/2010 1423
Prep Batch: 680-166243
Analysis Batch: 680-166687
g0794.d
1000 mL
1 mL
1 uL
g0752.d
1000 mL
1 mL
1 uL
ug/L
04/21/2010 1423
Analysis Batch: 680-166695
Prep Batch: 680-166243
Method: 8270C
Preparation: 3520C
MSG
MSG
LCS 680-166243/8-A
LCSD 680-166243/9-A
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
9090 47 - 130 0 40N-Nitrosomethylethylamine
108107 35 - 130 1 40N-Nitrosomorpholine
9197 53 - 130 6 40N-Nitrosopiperidine
106102 50 - 130 4 40N-Nitrosopyrrolidine
177183 23 - 162 3 40 * *o,o',o''-Triethylphosphorothioate
10892 29 - 169 16 40p-Dimethylamino azobenzene
8794 52 - 130 8 40Pentachlorobenzene
9799 52 - 130 3 40Pentachloronitrobenzene
111111 37 - 132 1 40Pentachlorophenol
103104 62 - 130 2 40Phenacetin
97101 52 - 117 4 40Phenanthrene
8285 39 - 110 3 40Phenol
105111 29 - 181 5 40Phorate
7782 10 - 130 6 402-Picoline
3434 10 - 130 0 40 J Jp-Phenylene diamine
97103 64 - 134 5 40Pronamide
100102 52 - 125 2 40Pyrene
6975 10 - 110 9 40Pyridine
8993 39 - 130 4 40Safrole, Total
97105 44 - 130 8 40Sulfotepp
8188 41 - 130 9 401,2,4,5-Tetrachlorobenzene
8993 38 - 130 4 402,3,4,6-Tetrachlorophenol
102112 48 - 135 10 40Thionazin
5355 27 - 130 3 402-Toluidine
8081 41 - 110 0 401,2,4-Trichlorobenzene
8994 47 - 122 5 402,4,5-Trichlorophenol
9096 46 - 120 6 402,4,6-Trichlorophenol
9665 10 - 200 39 401,3,5-Trinitrobenzene
Surrogate LCS % Rec LCSD % Rec Acceptance Limits
2,4,6-Tribromophenol 110 103 40 - 139
2-Fluorobiphenyl 95 87 50 - 113
2-Fluorophenol 80 79 36 - 110
TestAmerica Savannah Page 226 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
Surrogate LCS % Rec LCSD % Rec Acceptance Limits
Terphenyl-d14 103 100 10 - 121
Phenol-d5 87 85 38 - 116
Nitrobenzene-d5 92 91 45 - 112
TestAmerica Savannah Page 227 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
WaterClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
04/21/2010 1906
Method Blank - Batch: 680-166297
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 680-166320
Prep Batch: 680-166297
04/21/2010 1215
50 mL
50 mL
Units: ug/L
Method: 6010B
Preparation: 3010A
N/A
ICPDMB 680-166297/18-A
Analyte Result Qual MDL RL
20 U 204.6Arsenic
10 U 102.3Barium
5.0 U 5.02.0Cadmium
10 U 101.2Chromium
10 U 104.0Lead
20 U 206.4Selenium
10 U 100.89Silver
Water
1.0
04/21/2010 1911Date Analyzed:
Lab Control Sample - Batch: 680-166297
Client Matrix:
Lab Sample ID:
Dilution:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
04/21/2010 1215
Analysis Batch: 680-166320
Prep Batch: 680-166297
50 mL
50 mL
Units: ug/L
Method: 6010B
Preparation: 3010A
N/A
ICPDLCS 680-166297/19-A
Analyte QualLimit% Rec.ResultSpike Amount
2000 1970 98 75 - 125Arsenic
2000 2090 104 75 - 125Barium
50.0 51.7 103 75 - 125Cadmium
200 204 102 75 - 125Chromium
500 506 101 75 - 125Lead
2000 2050 102 75 - 125Selenium
50.0 50.1 100 75 - 125Silver
TestAmerica Savannah Page 228 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
SolidClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
04/22/2010 1427
Method Blank - Batch: 680-166337
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 680-166538
Prep Batch: 680-166337
04/21/2010 1618
1.00 g
100 mL
Units: mg/Kg
Method: 6010B
Preparation: 3050B
N/A
ICPDMB 680-166337/23-A
Analyte Result Qual MDL RL
2.0 U 2.00.59Arsenic
1.0 U 1.00.30Barium
0.50 U 0.500.10Cadmium
1.0 U 1.00.50Chromium
1.0 U 1.00.53Lead
2.5 U 2.51.0Selenium
1.0 U 1.00.096Silver
Solid
1.0
04/22/2010 1431Date Analyzed:
Lab Control Sample - Batch: 680-166337
Client Matrix:
Lab Sample ID:
Dilution:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
04/21/2010 1618
Analysis Batch: 680-166538
Prep Batch: 680-166337
1.00 g
100 mL
Units: mg/Kg
Method: 6010B
Preparation: 3050B
N/A
ICPDLCS 680-166337/24-A
Analyte QualLimit% Rec.ResultSpike Amount
200 192 96 75 - 125Arsenic
200 206 103 75 - 125Barium
5.00 5.08 102 75 - 125Cadmium
20.0 20.4 102 75 - 125Chromium
50.0 50.2 100 75 - 125Lead
200 197 99 75 - 125Selenium
5.00 4.93 99 75 - 125Silver
TestAmerica Savannah Page 229 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
SolidClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
04/26/2010 2021
Method Blank - Batch: 680-166528
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 680-166869
Prep Batch: 680-166528
04/23/2010 1017
1.00 g
100 mL
Units: mg/Kg
Method: 6010B
Preparation: 3050B
N/A
ICPDMB 680-166528/23-A
Analyte Result Qual MDL RL
2.0 U 2.00.59Arsenic
1.0 U 1.00.30Barium
0.50 U 0.500.10Cadmium
1.0 U 1.00.50Chromium
1.0 U 1.00.53Lead
2.5 U 2.51.0Selenium
0.133 J 1.00.096Silver
Solid
1.0
04/26/2010 2026Date Analyzed:
Lab Control Sample - Batch: 680-166528
Client Matrix:
Lab Sample ID:
Dilution:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
04/23/2010 1017
Analysis Batch: 680-166869
Prep Batch: 680-166528
1.00 g
100 mL
Units: mg/Kg
Method: 6010B
Preparation: 3050B
N/A
ICPDLCS 680-166528/24-A
Analyte QualLimit% Rec.ResultSpike Amount
200 184 92 75 - 125Arsenic
200 195 98 75 - 125Barium
5.00 4.75 95 75 - 125Cadmium
20.0 19.4 97 75 - 125Chromium
50.0 47.8 96 75 - 125Lead
200 185 92 75 - 125Selenium
5.00 4.84 97 75 - 125Silver
TestAmerica Savannah Page 230 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
04/26/2010 2247
04/26/2010 2252
Solid
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 680-166528
1.0
1.0
MS Lab Sample ID:
MSD Lab Sample ID:
Client Matrix:
Date Prepared:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Solid
Analysis Batch: 680-166869
Analysis Batch: 680-166869
04/23/2010 1017
04/23/2010 1017
Prep Batch: 680-166528
Prep Batch: 680-166528
1.16 g
100 mL
1.16 g
100 mL
Method: 6010B
Preparation: 3050B
N/A
N/A
ICPD
ICPD
680-56861-14
680-56861-14
Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS
% Rec.
95 94 75 - 125 1 20Arsenic
102 102 75 - 125 1 20Barium
97 96 75 - 125 0 20Cadmium
103 102 75 - 125 1 20Chromium
98 98 75 - 125 0 20Lead
93 92 75 - 125 0 20Selenium
100 98 75 - 125 1 20Silver
TestAmerica Savannah Page 231 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
SolidClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
04/28/2010 2226
Method Blank - Batch: 680-166825
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 680-167105
Prep Batch: 680-166825
04/27/2010 0909
1.00 g
100 mL
Units: mg/Kg
Method: 6010B
Preparation: 3050B
N/A
ICPDMB 680-166825/22-A
Analyte Result Qual MDL RL
2.0 U 2.00.59Arsenic
1.0 U 1.00.30Barium
0.50 U 0.500.10Cadmium
1.0 U 1.00.50Chromium
1.0 U 1.00.53Lead
2.5 U 2.51.0Selenium
1.0 U 1.00.096Silver
Solid
1.0
04/28/2010 2221Date Analyzed:
Lab Control Sample - Batch: 680-166825
Client Matrix:
Lab Sample ID:
Dilution:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
04/27/2010 0909
Analysis Batch: 680-167105
Prep Batch: 680-166825
1.00 g
100 mL
Units: mg/Kg
Method: 6010B
Preparation: 3050B
N/A
ICPDLCS 680-166825/23-A
Analyte QualLimit% Rec.ResultSpike Amount
200 197 99 75 - 125Arsenic
200 211 106 75 - 125Barium
5.00 5.07 101 75 - 125Cadmium
20.0 20.7 103 75 - 125Chromium
50.0 49.8 100 75 - 125Lead
200 200 100 75 - 125Selenium
5.00 5.03 101 75 - 125Silver
TestAmerica Savannah Page 232 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
WaterClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
04/22/2010 1115
Method Blank - Batch: 680-166268
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 680-166435
Prep Batch: 680-166268
04/21/2010 1021
50 mL
50 mL
Units: ug/L
Method: 7470A
Preparation: 7470A
N/A
LEEMAN1MB 680-166266/6-B
Analyte Result Qual MDL RL
0.20 U 0.200.091Mercury
Water
1.0
04/22/2010 1119Date Analyzed:
Lab Control Sample - Batch: 680-166268
Client Matrix:
Lab Sample ID:
Dilution:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
04/21/2010 1021
Analysis Batch: 680-166435
Prep Batch: 680-166268
50 mL
50 mL
Units: ug/L
Method: 7470A
Preparation: 7470A
N/A
LEEMAN1LCS 680-166266/7-B
Analyte QualLimit% Rec.ResultSpike Amount
2.50 2.33 93 80 - 120Mercury
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
04/22/2010 1233
04/22/2010 1236
Water
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 680-166268
1.0
1.0
MS Lab Sample ID:
MSD Lab Sample ID:
Client Matrix:
Date Prepared:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Water
Analysis Batch: 680-166435
Analysis Batch: 680-166435
04/21/2010 1021
04/21/2010 1021
Prep Batch: 680-166268
Prep Batch: 680-166268
50 mL
50 mL
50 mL
50 mL
Method: 7470A
Preparation: 7470A
N/A
N/A
LEEMAN1
LEEMAN1
680-56861-28
680-56861-28
Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS
% Rec.
89 89 80 - 120 0 20Mercury
TestAmerica Savannah Page 233 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
SolidClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
04/27/2010 1322
Method Blank - Batch: 680-166534
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 680-166898
Prep Batch: 680-166534
04/23/2010 1046
0.50 g
50 mL
Units: mg/Kg
Method: 7471A
Preparation: 7471A
N/A
LEEMAN1MB 680-166534/23-A
Analyte Result Qual MDL RL
0.020 U 0.0200.0082Mercury
Solid
1.0
04/27/2010 1325Date Analyzed:
Lab Control Sample - Batch: 680-166534
Client Matrix:
Lab Sample ID:
Dilution:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
04/23/2010 1046
Analysis Batch: 680-166898
Prep Batch: 680-166534
0.50 g
50 mL
Units: mg/Kg
Method: 7471A
Preparation: 7471A
N/A
LEEMAN1LCS 680-166534/24-A
Analyte QualLimit% Rec.ResultSpike Amount
0.250 0.236 94 80 - 120Mercury
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
04/27/2010 1447
04/27/2010 1450
Solid
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 680-166534
1.0
1.0
MS Lab Sample ID:
MSD Lab Sample ID:
Client Matrix:
Date Prepared:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Solid
Analysis Batch: 680-166898
Analysis Batch: 680-166898
04/23/2010 1046
04/23/2010 1046
Prep Batch: 680-166534
Prep Batch: 680-166534
0.53 g
50 mL
0.54 g
50 mL
Method: 7471A
Preparation: 7471A
N/A
N/A
LEEMAN1
LEEMAN1
680-56861-14
680-56861-14
Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS
% Rec.
88 83 80 - 120 8 20Mercury
TestAmerica Savannah Page 234 of 238
Quality Control Results
Job Number: 680-56861-1Client: Ashland Inc.
SolidClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
04/28/2010 1844
Method Blank - Batch: 680-166757
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 680-167080
Prep Batch: 680-166757
04/26/2010 1535
0.51 g
50 mL
Units: mg/Kg
Method: 7471A
Preparation: 7471A
N/A
LEEMAN1MB 680-166757/19-A
Analyte Result Qual MDL RL
0.020 U 0.0200.0080Mercury
Solid
1.0
04/28/2010 1847Date Analyzed:
Lab Control Sample - Batch: 680-166757
Client Matrix:
Lab Sample ID:
Dilution:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
04/26/2010 1535
Analysis Batch: 680-167080
Prep Batch: 680-166757
0.51 g
50 mL
Units: mg/Kg
Method: 7471A
Preparation: 7471A
N/A
LEEMAN1LCS 680-166757/20-A
Analyte QualLimit% Rec.ResultSpike Amount
0.245 0.254 103 80 - 120Mercury
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
04/28/2010 1931
04/28/2010 1933
Solid
Matrix Spike/
Matrix Spike Duplicate Recovery Report - Batch: 680-166757
1.0
1.0
MS Lab Sample ID:
MSD Lab Sample ID:
Client Matrix:
Date Prepared:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Solid
Analysis Batch: 680-167080
Analysis Batch: 680-167080
04/26/2010 1523
04/26/2010 1523
Prep Batch: 680-166757
Prep Batch: 680-166757
0.56 g
50 mL
0.56 g
50 mL
Method: 7471A
Preparation: 7471A
N/A
N/A
LEEMAN1
LEEMAN1
680-56861-23
680-56861-23
Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS
% Rec.
101 94 80 - 120 2 20Mercury
TestAmerica Savannah Page 235 of 238
Page 236 of 238
Page 237 of 238
Login Sample Receipt Check List
Client: Ashland Inc. Job Number: 680-56861-1
Login Number: 56861
Question T / F/ NA Comment
Creator: Daughtry, Beth
List Source: TestAmerica Savannah
List Number: 1
Radioactivity either was not measured or, if measured, is at or below
background
N/A
The cooler's custody seal, if present, is intact. True
The cooler or samples do not appear to have been compromised or
tampered with.
True
Samples were received on ice. True 6 coolers rec'd 4/17/10; 7th cooler rec'd on 4/19
Cooler Temperature is acceptable. True
Cooler Temperature is recorded. True 4/17 Rcpt - 0.8, 1.4, 0.9, 0.6, 1.9, 2.0 C; 4/19
recpt @ 0.2 C
COC is present. True
COC is filled out in ink and legible. True
COC is filled out with all pertinent information. True
There are no discrepancies between the sample IDs on the containers and
the COC.
True
Samples are received within Holding Time. True
Sample containers have legible labels. False Client labeled outside baggie on soil containers
had to place on containers
Containers are not broken or leaking. True
Sample collection date/times are provided. True
Appropriate sample containers are used. True
Sample bottles are completely filled. True
There is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
True
VOA sample vials do not have headspace or bubble is <6mm (1/4") in
diameter.
True
If necessary, staff have been informed of any short hold time or quick TAT
needs
True
Multiphasic samples are not present. N/A
Samples do not require splitting or compositing. N/A
Is the Field Sampler's name present on COC? True
Sample Preservation Verified True
TestAmerica Savannah
Page 238 of 238