Imagine the result
Maplewood Farms
SITE PREPARATION PLAN
24 Ball Hill Road
Berlin, Massachusetts
August 8, 2011
Site Preparation Plan 24 Ball Hill Road Berlin, Massachusetts
Richard G. Stromberg, CPG, LSP, LEP Principal Geologist
Prepared for:
Maplewood Farms
Prepared by:
ARCADIS U.S., Inc.
194 Forbes Road
Braintree
Massachusetts 02184
Tel 781 356 7300
Fax 781 356 2211
Our Ref.:
BN030465.0000
Date:
August 8, 2011
This document is intended only for the use
of the individual or entity for which it was
prepared and may contain information that
is privileged, confidential and exempt from
disclosure under applicable law. Any
dissemination, distribution or copying of
this document is strictly prohibited.
BN030465.0000_rpt_Soil Mgmt Plan Phase_Aug082011.doc:jc i
Table of Contents
1. General 1
1.1 Introduction 1
1.2 Site Environmental Background 5
1.3 Names and Addresses of Parties Involved 6
1.4 Overview of Screening and Testing Requirements for Soil Acceptance 7
2. Soil Testing Requirements 11
3. Laboratory Environmental Analyses 12
4. Soil Approval and Placement 14
4.1 Soil Approvals 14
4.2 Soil Placement and Tracking 14
5. Other Considerations 15
5.1 Site Access and Quantity Estimating 15
BN030465.0000_rpt_Soil Mgmt Plan Phase_Aug082011.doc:jc ii
Table of Contents
Figures
Figure 1 USGS Site Locus Map
Figure 2 SA Farms Soil Placement Layout and Current Grade Elevations and SA Farms Future Grade Elevations
Figure 3 Wetland Area and Buffer Zone Map
Figure 4 Zoning Map
Figure 5 MassDEP GIS Map
Tables
Table 1 Summary of Soil Data Results and Acceptance Criteria
Appendices
Appendix A Section of M.G.L. Chapter 40 Section 3A
Appendix B List of MCP Disposal Sites
Appendix C Background Sampling Analytical Data
Appendix D Soil Profile Package Information
Appendix E Private Well Completion Report and Testing
1
Site Preparation Plan
24 Ball Hill Road Berlin, Massachusetts
1. General
1.1 Introduction
The following is a “Site Preparation Plan”, Phase I Area prepared in support of the
planned use of a 4-acre portion of a parcel of land known as the Maplewood Farms
Site (“the Site”) for farming purposes located off of 24 Ball Hill Road in Berlin,
Massachusetts. The Phase I area is shown on Figure 1 and the area where soil will be
placed is shown on Figure 2. The portion of the property where soil will be placed in
Phase I is located on Lot A and B-1 just east of Ball Hill Road. The Owner is Tamara
and Archibald Johnston (individually) of 24 Ball Hill Road,the Operator is Lighthouse Environmental Management LLC. 184 Stone Street Clinton MA 01510 and the Operations Manager is Kevin Francis Gervais (617-699-5245).
The Phase I Site is currently a horse paddock and open vegetated land that has been
used for farming and agricultural purposes in the past and is proposed by the owner to
continue to be used for the same purposes (General Farming and Raising of
Livestock). A section of M.G.L. Chapter 40, Section 3A is provided in Appendix A that
apply to this property and these regulations. Although the clearing of land may be
greater than one acre, any amount of clearing for agricultural purposes is not
considered an industrial activity under the storm water regulations. Section 402(l)(1) of
the 1987 Water Quality Act exempts agricultural storm water discharges from NPDES
permitting requirements including storm water permitting. This exemption only applies,
however, if the clearing of land is solely for agricultural purposes.
The portion of this Phase I parcel that is planned for clearing, leveling, and construction
of a new horse paddock through import of soil is shown on Figure 2. This Phase I Area
is located outside of currently delineated wetland areas and buffer zones as shown on
Figure 3. This area will utilize the existing access road for placement of the soil from
an average elevation of 575’ to a planned elevation of Elev.610’ as shown on Figure 2.
A Stormwater Pollution and Protection Plan (SWPPP) filing for discharges from
construction activities (such as clearing, grading, excavating, and stockpiling) that
disturb one or more acres, are regulated under the National Pollutant Discharge
Elimination System (NPDES) stormwater program. Prior to discharging stormwater,
construction operators must obtain coverage under an NPDES permit, which is
administered by either the State (if it has been authorized to operate the NPDES
stormwater program) or EPA, depending on where the construction site is located.
According to the Operator, a SWPPP filing is not necessary due to agricultural
exemptions but dust and storm water will be controlled by the Operator.
BN030465.0000_rpt_Soil Mgmt Plan Phase_Aug082011.doc:jc
BN030465.0000_rpt_Soil Mgmt Plan Phase_Aug082011.doc:jc 2
Site Preparation Plan
24 Ball Hill Road Berlin, Massachusetts
Certain management practices will be exercised by the Owner, Operator, and
Operations Manager (Mr. Kevin Gervais) to prevent changes in runoff patterns toward the wetland areas and buffer zones located to the south.
The period of time expected to import the necessary soils is 6-12 months. It is expected that about 360,000 cy of soil will be required in the placement area to achieve the continued use of the property for agricultural purposes by the owner.
This management plan provides information for the specific placement of soil at this portion of the Site that meet certain physical and chemical criteria. This plan provides
the status of applicable land use regulations, areas to be cleared to some degree and leveled, and a discussion of applicable MCP regulations.
The information utilized for this plan was obtained from the owner, information on file at the Berlin Town Offices, and other publicly available information as well as testing and surveys conducted on the Site.
Coordination was made by the Operator with Berlin local officials for the “Right to Farm” bylaw recognized by Berlin and no filings were required. A Notice of Intent (NOI)
filing with the Berlin Conservation Commission (BCC) or Nashoba Board of Health was deemed not required at this time because work won’t be conducted in wetlands or buffer zones. The access road will be maintained outside the buffer zones.
The area of the Site is residentially-zoned land and open space as shown on Figure 4. Figure 5 is a MassDEP Geographic Information System (GIS) map for the Site.
Figure5 also provides the Area Resource Map from the MassDEP and indicates that the Site is not located within an MassDEP designated Zone II drinking water resource area, Interim Wellhead Protection Area (IWPA), sole source aquifers, or Area of Critical
Environmental Concern (ACEC). There are no mapped vernal pools or habitats for rare wildlife/species on or near the Phase I Site.
The Site is currently served by two private wells. The house well at 24 Ball Hill Road as shown on Figure 2 was drilled to 425 feet in bedrock yielding 25 gpm. Information regarding this house well was provided by Mr. Bill Brookings of the Nashoba Board of
Health via a telefax request on July13, 2011. The Well Completion Report and testing of the well is provided in Appendix E. The well was tested in September and October 2010 for primary/secondary drinking water parameters and coliform, manganese, and
iron exceeded criteria. The well was chlorinated and were re-tested in November 2010 and July 2011 and passed.
3
Site Preparation Plan
24 Ball Hill Road Berlin, Massachusetts
The well is currently used for human consumption this well replaced the previously
drilled two prior house wells, which have since been decommissioned and abandoned.
A second private well on 24 Ball Hill Road is near the barn and provised potable water,
which is used both for animal and human consumption. Mr. Brookings indicated there
were no municipal wells located within ½ mile of the Site.
The Site is bounded to the west by Ball Hill Road and to the north, east, and south by
property owned by the Owners. There will be no buildings constructed on the Phase I
Site as it is planned for a horse paddock and raising of livestock. The unpaved road will
be used for access by machinery. The road condition will be maintained by the Owner
such that visible dust will be kept to a minimum. Soil from the Site will not be tracked
onto Ball Hill Road. There will be no other water supply wells drilled on the Site.
There will also be no athletic fields or areas of high intensive children activity in the
area to be filled under this plan. There are also no planned communal vegetable
gardens or generation of produce for sale on the Site.
A review of MassDEP’s list of MCP Disposal Sites in Appendix B indicated that there
were no release sites located in the vicinity of the Site.
The geological conditions on the Site consist of an overburden veneer of thin to absent
glacial till over bedrock as mapped on the MassDEP GIS Surficial Geology map for
Berlin (Dec. 2009). The bedrock consists of gray, medium-grained schist and gneiss.
It has been determined that soil of sufficient chemical and physical quality is necessary
to be imported for the project to bring certain areas to the required grade for farming.
Lighthouse Environmental Management,LLC. has entered into agreement with owner to manage soil import activities. Arcadis was retained by Lighthouse to prepare the soil
re-use management plan on behalf of the Owner and to review candidate soils for
compliance with this plan. Arcadis, Lighthouse and the Owner were responsible to
ascertain that appropriate local and state regulations were reviewed for the intended
use of the Site and permits were acquired as necessary to implement the continued
future use. Lighthouse and the Owner are responsible through their contractual
arrangements for ensuring that only soils approved under this plan are brought to the
Site.
BN030465.0000_rpt_Soil Mgmt Plan Phase_Aug082011.doc:jc
4
Site Preparation Plan
24 Ball Hill Road Berlin, Massachusetts
The soil re-use activities and all other construction-related activities will be conducted
in accordance with this plan. It is the Owner’s and Lighthouse’s indication that the
filling will be conducted in the specified area as shown on Figure 2 which depict current
and planned grade. The owner and Lighthouse have indicated they have discussed
with the municipality, its boards and commissions the nature of the planned Site use
and necessary import of material to obtain elevations shown on Figures 2.
MassDEP’s Bureau of Waste Site Cleanup (BWSC) under the Massachusetts
Contingency Plan (MCP) does not provide approval for “<RCS-1” soil re-use at a site
like this one but requires that “anti-degradation” provisions at 310 CMR 40.0032 (3) be
followed for the soil to be chemically suitable. The physical suitability of the soil will be
determined by Lighthouse and the Owner. The Site is classified as “RCS-1” under the
MCP since the Site is located within 500 feet of a residence. The MCP groundwater
classification in the area is “GW-1, 2 and 3” for current or potential drinking water,
exposures to residential indoor air, and surface water bodies as defined in the MCP.
Re-use of soils on the Site from outside sources is necessary to create a level surface
for horse farming. The soil must also abide by certain physical acceptance
requirements and not significantly alter the drainage patterns in the area. It is
understood that certain fine grained silt/clay and some organic soils will be accepted as
long as hydrogen sulfide odors are not apparent and moisture is tolerated for mixing
with granular soils, but no dredge spoils or dredged organic silt or peat material will be
accepted unless specifically permitted for use in upland areas by the appropriate
agency and the LSP for this project.
The final goal of this plan is to formalize the soil management process and the soils
acceptance policy at the Site in order to meet re-use requirements and to give
generators a sufficient level of comfort that their material is being handled
appropriately.
BN030465.0000_rpt_Soil Mgmt Plan Phase_Aug082011.doc:jc
BN030465.0000_rpt_Soil Mgmt Plan Phase_Aug082011.doc:jc 5
Site Preparation Plan
24 Ball Hill Road Berlin, Massachusetts
The Owner and Lighthouse intend to conduct the soil management operations with
approved “clean” fill and natural soils from off-site locations that are considered to be
the following:
• Non-Massachusetts Contingency Plan (MCP) regulated soils (“<RCS-1”). Soils that
are recognized to contain fill materials (reworked natural soil or soil with some small
proportion of anthropogenic residual material) from non-MCP regulated sites, or
other soils brought from an MCP-regulated site that are < RCS-1 standards and not
considered part of a Disposal Site as defined in the MCP by the sending LSP. This
soil is also MCP restricted in that it must also meet MCP “anti-degradation provisions” at 40.0032. This requirement is addressed through the development of “Acceptance Criteria” in this plan.
• Naturally occurring, non-impacted soils that do not originate from within affected layers on an MCP site or a site with filling activities and are not otherwise regulated.
These soils generally will not require the amount of testing as soils noted above
and compliance with 40.0032 except as specifically requested by the Project LSP,
Lighthouse or the Owner based on certain site conditions or features (i.e. certain
clay that may contain certain metals and conductance). For natural soils to be
accepted without testing, a written Generator “Certification Statement” will be required outlining the basis for the statement subject to the approval of the Project LSP, Lighthouse, and the Owner.
Soils from on-going and proposed projects will be delivered to the appropriate section of the re-use area as specified by Lighthouse and the Owner and will be placed and tracked in accordance with procedures in this plan.
Approximately 360,000 cubic yards) of common soil fill is estimated for the project.
1.2 Site Environmental Background
The Site does not contain sensitive environmental receptors but groundwater is used
for drinking water and by residents and animals. The Owners live on parcels where soil will be imported. Surface water exists in a natural brook to the east of the Site.
BN030465.0000_rpt_Soil Mgmt Plan Phase_Aug082011.doc:jc 6
Site Preparation Plan
24 Ball Hill Road Berlin, Massachusetts
There were a series of analytical tests conducted on naturally occurring surface soils in
the Site in June 2011 by ARCADIS and Lighthouse. A total of three composite
samples designated as “PH I SS-1 through 6” located throughout the Phase I re-use
area to be developed were collected by Lighthouse and ARCADIS. Analysis included:
SVOCs, VOCs, TPH, and Priority Pollutant 13 Metals, pesticides/herbicides, PCBs,
and specific conductance. The analytical data sheets are included in Appendix C.
The results were used to summarize average and maximum Site “background”
concentrations as shown on Table 1. For comparative purposes, Table 1 also depicted
the current MCP RCS-1 values promulgated by MassDEP.
The significance of this background environmental testing is described later in this plan
for development of soil “Acceptance Criteria”.
1.3 Names and Addresses of Parties Involved
The owner of the property is:
- Tamara and Archibald Johnston, 24 Ball Hill Road, Berlin, MA
The Operator of the Site is:
- Lighthouse Environmental Management,LLC 184 Stone Street, Clinton MA 01510
The operations Manager of the Site for soil placement operations is:
- Mr. Kevin Francis Gervais (617-699-5245)
The “Site LSP” reviewing candidate soil packages is:
- Mr. Richard Stromberg, ARCADIS-US, Inc., 194 Forbes Road, Braintree, MA02184. Cell Phone: (617) 908-7094, Tel: (781) 356-7300 x203.
BN030465.0000_rpt_Soil Mgmt Plan Phase_Aug082011.doc:jc 7
Site Preparation Plan
24 Ball Hill Road Berlin, Massachusetts
1.4 Overview of Screening and Testing Requirements for Soil Acceptance
Soil to be placed at the Phase I part of the Site, other than some certified naturally-
occurring soils, will require field screening and analytical testing to conform with MCP
requirements and to demonstrate that the material is chemically suitable for the project.
The physical suitability will be reviewed and approved by Lighthouse and the Owner.
Soil Profile Package information for the approval candidate soils is provided in
Appendix D.
Screening Criteria
Lighthouse or a specified representative may conduct periodic screening of soils that
will be shipped to the Site to make sure soils are as represented. Candidate soil must
be evaluated by the generator for the following screening criteria and these results
must be addressed in the soil profiling package prepared by the generator. Candidate
soil being placed in the Site shall not exceed the following field screening/visual criteria:
• Field screening results of soil headspace from representative samples must not exhibit an average reading of Total Organic Vapors (TOV) in the jar headspace exceeding 2 parts per million (ppm) by volume due to volatile constituents. If screening has not been performed by the generator, it may be performed at the Site by Lighthouse or another designated party as appropriate to verify certain loads. If screening at the Site results in exceedances to the criteria above, the load(s) will be rejected.
• Visually, the soil must not exhibit any staining, odors, or other discolorations indicative of oil and hazardous material (OHM) releases as demonstrated by the representative of the soil to be imported.
• The urban fill soils must not contain any refuse, trash or solid waste. The soil may contain ancillary non-coated or non-painted bricks or non-coated/stained or non-impregnated concrete or cobbles less than 6 inches diameter if it is contained within certain fill soils in very small quantities. This material must be less than 5% of the fill material. If soils contain more than this amount, the above-listed excluded material must be physically separated and sent to a designated construction and demolition (C&D) or permitted Asphalt, Brick, Concrete (ABC) disposal facility by the generator. Loads received that contain more than the acceptable amount of solid waste will be rejected by Lighthouse and sent back to the site of origin at the generator’s cost.
BN030465.0000_rpt_Soil Mgmt Plan Phase_Aug082011.doc:jc 8
Site Preparation Plan
24 Ball Hill Road Berlin, Massachusetts
• Soil may contain naturally deposited silt and clay and a certain portion of naturally occurring organic content and moisture since drainage of the soil can occur on the Site while it is being worked as represented by Lighthouse. No dredge spoils will be allowed unless permitted by MassDEP.
• Upon arrival of the trucks at the Site, soils will be visually inspected and field screened from representative loads by Lighthouse or another designated party and discrete soil samples may be collected from a representative number of loads to prepare a composite sample from the candidate property for confirmatory analysis by the owner or Lighthouse at their discretion.
Rationale for Development of Analytical Acceptance Criteria
In developing the Acceptance Criteria for the Site, the following step-wise rationale was developed as described below for soils other than certified, non-impacted, naturally occurring soils. Naturally occurring soil may be subject to certain chemical testing based on site-specific conditions as evaluated by the generators engineer, qualified environmental professional (QEP) or LSP.
The rationale considered current MCP RCS-1 soil standards, the environmental conditions at and in the immediate vicinity of the Site, and characteristics of certain constituents that may be included in the candidate soil (adsorption coefficient, toxicity, and frequency of occurrence in the environment). Site-specific soil sampling was also performed from surface and near surface soils in and around the Phase I fill area of the Site to use this information as the primary tool for calculating Acceptance Criteria.
A summary of the background sampling results for the Site is provided on Table 1. This table includes the maximum concentration observed on the Site, the average concentration, three times (3X) the average concentration for use in calculating PAH/SVOC and metal Acceptance Criteria, MassDEP published “natural soil” concentrations, and current and current MCP RCS-1 standards.
These categories have been applied at similar sites in the Commonwealth of Massachusetts by ARCADIS for preparing acceptance criteria with MassDEP acknowledgement at one site.
BN030465.0000_rpt_Soil Mgmt Plan Phase_Aug082011.doc:jc 9
Site Preparation Plan
24 Ball Hill Road Berlin, Massachusetts
The average and maximum concentrations were utilized in developing Acceptance Criteria for Priority Pollutant -13 metals, PCBs, TPH, and SVOCs/SVOCs. With regard to “other metals”, the MassDEP published values for natural soils and RCS-1 standards (where available) should be consulted when site –specific data was generated. These “other metals” do not necessarily require testing for acceptance unless a given natural condition warranted testing for one of these metals by the generator, i.e. known natural accumulation of a certain element or elements in certain soils. Elevated concentrations of these metals at a candidate site not associated with natural conditions will not be accepted at this Site.
Once the Acceptance Criteria were selected, they were checked against current and proposed RCS-1 standards for compliance.
Summary of Acceptance Criteria
1. For VOCs all constituent concentrations must be below laboratory detectablelimits because no detectable levels were found in Site-specific sampling. A traceamount of a lone VOC may be accepted if it is clearly identified to be an outlier inthe data set and the soils are not part of a VOC release or if it is a laboratorycontaminant (acetone) or by product of the sampling preservative and soil. Thelaboratory detectable limits shall not be higher than MCP RCS-1 soil standardsfor a given VOC constituent. PCBs will not be accepted above a detection limit of0.1 ppm. A trace below 0.1 ppm in one sample may be accepted provided thegenerator certifies that there were no known releases of PCBs to the soils thatwould give rise to concentrations > 0.1 ppm and other samples are ND (minimumof two).
2. For TPH, levels of TPH were detected at 120-170 mg/kg. The levels wereattributed to some bits of asphalt in the loam and surface soil observed. Theaverage TPH concentration was 140 mg/kg and three times average was 420mg/kg which is below the current RCS-1 standard of 1,000 ppm. An AcceptanceCriteria of 300 ppm was developed to address both natural soils and soils thatcontained asphalt that may contain some TPH. Some averaging will be allowedfor certain cases. Since a certain proportion of fill already exists at the Site, avalue of 300 (asphalt or binder material source) was considered not tosignificantly exceed background and still be protective for future use since roadsand machinery traffic will be placed or occur on the development. TPH at thislimit must be from asphalt and not from a fuel oil release in the subject soils andwill not be accepted.
BN030465.0000_rpt_Soil Mgmt Plan Phase_Aug082011.doc:jc 10
Site Preparation Plan
24 Ball Hill Road Berlin, Massachusetts
3. The SVOC results indicated that a few target SVOCs were detectable, however,all of the detections were below the RCS-1 reportable concentrations. SomeSVOC compounds are considered by MassDEP to be ubiquitous in theenvironment (including some from forest fires) and are generally not consideredto be mobile in subsurface aqueous systems. Since certain SVOCs have beendocumented by MassDEP to be present in naturally occurring soils (especiallyforest mat with burnt wood remnants) as shown in Table 1, an AcceptanceCriteria of 3 times the one-half detection limit and the detected concentrationswere utilized. The concept of three times one-half DL or average concentrationwas acknowledged by MassDEP for SVOCs on a similar site. The AcceptanceCriteria ranged from 0.6 to 4.8 ppm.
4. With regard to the metals analyzed during the background sampling program,the results were fairly uniform with no significant deviations. In certain cases,levels of arsenic, chromium, and barium can be found in naturally depositedBoston Basin marine clays/silts like that excavated from the Central ArteryTunnel (CAT) project. Arithmetic mean arsenic concentrations from some ofthese soils as reported by MassDEP was 8 to 44 mg/kg for arsenic,(Memorandum from Paul Locke to Steve Lipman of MassDEP, July 2002). TheMADEP 90th percentile published background value for arsenic is 20 mg/kg.Arsenic is also known to be naturally occurring in Worcester County at levels of20-40 ppm (O’Neill,1995). The arsenic Acceptance Criteria was identified as< 20ppm based on an average concentration of 15 ppm with the RCS-1 of 20 ppm.Some slightly higher concentrations may be acceptad on a case by case basis.Other non-exempt fill soils containing arsenic must be below 20 ppm which is theRCS-1. This criteria is consistent with documented natural soil arsenicconcentrations in Worcester County.
With regard to lead, the average Site concentration was 26 ppm. Since most fill soils and some natural soils contain some levels of lead < 100 mg/kg, and the MassDEP Rural Soil concentration is 100 mg/kg, an Acceptance Criteria of 79 ppm was established which is consistent with the 3X concept and is not significantly above the Site maximum.
With regard to other metals Acceptance Criteria were chosen at 3X background which included detects and ½ detection limits where not detected.
BN030465.0000_rpt_Soil Mgmt Plan Phase_Aug082011.doc:jc 11
Site Preparation Plan
24 Ball Hill Road Berlin, Massachusetts
5. No pesticides/herbicides were detected at the Site. Since this is farmland, a traceof some pesticides/herbicides well below RCS-1 can be accepted on a case bycase basis as long as the predominance of samples are ND and concentrationscan be demonstrated to have resulted from properly applied materials.
6. The pH range should be 5-9 pH units and specific conductance should be lessthan 1,000 umhos/cm2 for granular soils as long as the metals are compliant. Inthe case of naturally deposited, non-impacted Boston Basin marine clay/silt, aconductance of 1,000-2,000 umhos/cm can be accepted in consideration ofmetal concentrations. This is well below MassDEP’s criteria of 4,000 umhos/cmfor unlined landfills. The acceptance of natural silty clay with higher conductancewill depend on the quantity and the available location for placement on the Site,i.e. not in close proximity to wetlands/streams.
The candidate soil must not originate from nor be contiguous with an MCP-regulated release area or “disposal site”, unless in certain circumstances, the soil can be taken from an MCP disposal site as long as the soil strata in question are not impacted above Acceptable Criteria as demonstrated by the Engineer/LSP. For example: a non-impacted fill zone or layer < RCS-1 that also meets Acceptance Criteria or a non-impacted natural soil layer below or above an impacted layer that also meets Acceptance Criteria. This must be documented and signed by the candidate site LSP/QEP or Engineer.
Laboratory results must meet these criteria. In certain instances, averaging within a given profile may be utilized. The averaging should be discussed with the Site LSP before the generator prepares the soil profile package.
2. Soil Testing Requirements
The majority of the soil that is scheduled to be placed in the Site is contemplated to originate from large construction projects where the soils have either been pre-
characterized during the engineering phase of the development or characterized from stockpiled soil. All soils to be placed in the Site will be pre-characterized by the generator, except in some cases non-impacted, naturally occurring soils where a
Generator’s Certification Statement is received and approved. Some testing of these soils may still be required.
12
Site Preparation Plan
24 Ball Hill Road Berlin, Massachusetts
Prior to placement of material in the Site, the Site LSP will review the pre-
characterization data packages of all potential candidate soils prior to acceptance of
the materials. This will be done to demonstrate that the soils from the generator’s
property are in compliance with Acceptance Criteria and other provisions of this plan.
The Site LSP, Owner or Lighthouse may also request to review any environmental
investigative reports regarding potential OHM release(s) and soil quality at the
originating property.
For acceptance of soils, the generator shall provide a soil profile package including
laboratory analytical data for the parameters listed in Section 3.0. The sampling
frequency shall be a minimum of one composite soil sample per every 500 cubic yards
of soil to be delivered, or at a frequency considered suitable and sufficient by the
Engineer/LSP/QEP for the soil in question (i.e. 1,000 cy for undisturbed, non-impacted
natural soil in proximity to regulated soil) as described in various MassDEP’s policies
for due diligence assessments. If sufficient analytical data is not available from the
generator, the owner, Lighthouse or the Site LSP, will require that the generator of the
soils collect additional samples. This will ensure that, at a minimum, the material is less
than the Acceptance Criteria set forth in this plan and the equivalent frequency of
testing requirements that is typically employed for MassDEP permitted Massachusetts
Landfills have been met. This will enable Lighthouse to provide the necessary
background information to verify that material deposited in the Site is acceptable.
In some cases, crushed bedrock may also be accepted and physical/chemical analysis
of the rock will be determined on a case-by-case basis for its intended use.
3. Laboratory Environmental Analyses
Samples requiring environmental analysis shall be submitted to a laboratory certified
by MassDEP for the chemical analyses required.
Environmental samples shall be collected, labeled, and preserved in accordance with
established protocols for the respective analysis, and submitted to the analytical
laboratory under chain-of-custody procedures.
BN030465.0000_rpt_Soil Mgmt Plan Phase_Aug082011.doc:jc
BN030465.0000_rpt_Soil Mgmt Plan Phase_Aug082011.doc:jc 13
Site Preparation Plan
24 Ball Hill Road Berlin, Massachusetts
Laboratory environmental analyses for the following parameters shall be in accordance
with the latest version of the specified test method:
Parameter EPA Test Method
Total Petroleum Hydrocarbons (GC-FID)(TPH)
ASTM D 3328
Volatile Organic Compounds (VOCs) 8260
Semi-Volatile Organic Compounds (SVOCs)
8270
Polychlorinated Biphenyls (PCBs), 8082
Priority Pollutant 13 or RCRA 8 Metals (and other Metals as Appropriate)
6010/7000
Pesticides/herbicides 8081B
Specific Conductance will be run. Reactive sulfide/cyanide, and pH will also be run if
there is reason to suspect that these hazardous waste characteristics need to be
evaluated. Sampling and QA/QC procedures acceptable to MassDEP will be adhered
to and QA/QC results will be considered by the generating facility in determining if the
soil profiling is acceptable.
Laboratory analytical data sheets, chain-of-custody’s, and laboratory QA/QC reports
will be provided with the soil profiling packages along with pertinent maps/sketches and
field testing results for review by Lighthouse and the LSP.
14
Site Preparation Plan
24 Ball Hill Road Berlin, Massachusetts
4. Soil Approval and Placement
4.1 Soil Approvals
Once the generator’s Engineer, QEP or LSP representative has approved the
analytical results as described in this plan, a generator representative should forward
the results of the soil profile package or pre-characterization study in letter format with
attachments to Lighthouse who will provide initial feedback on the potential
acceptance of a given soil. Appendix D contains information on requirements for the
Soil Profile Package submittals. After initial approval is gained, the package will be
sent to the Site LSP for review. Characterization results from each candidate property
will be reviewed to confirm that the soil meets the requirements set forth in this plan.
The Site LSP will then prepare an acknowledgement and approval letter to the owner/
Lighthouse confirming the acceptance of the soil for confirmatory signature by
Lighthouse. The letter will specify the approved quantity, the quantity to be shipped,
dates, restrictions (if any), and other pertinent items. The letter will be forwarded by
Lighthouse to the generator.
4.2 Soil Placement and Tracking
Once the analytical data from the proposed generator’s property has been reviewed
and approved by the owner, Lighthouse, and the Site LSP, the soils will be designated
to a specific area which will be logged into the facility’s database, with the estimated
quantity. All soils being placed in the applicable area will require a MassDEP Material
Shipping Record (MSR) or Bill-of-Lading (BOL) to accompany each truckload. The
designated area will be placed on all MSRs or BOLs. The Site LSP will periodically
inspect the Site and records on file at the Site for conformance with this plan.
The trucks may be weighed at the Site or another location as specified by Lighthouse.
Scaling will be at Berlin Stone Co, 322 Sawyer Hill Road,Berlin MA. Once the truck
has been weighed on a certified scale it will be directed to place the material into a
specific area. The appropriate paperwork will be left on site at a designated location or
handed directly to on-site personnel. The Soil piles will be placed within the
designated area to be filled and will be spread out by the Site earth-works contractor
until the desired grade is met. Then the area will be noted and coded in the files.
BN030465.0000_rpt_Soil Mgmt Plan Phase_Aug082011.doc:jc
15
Site Preparation Plan
24 Ball Hill Road Berlin, Massachusetts
If the on-site personnel deem the material to be suspect after dumping the truck will be
rejected and sent back to the generator for additional testing, or returned at the
generator’s expense. If loads are received that contain large pieces of solid waste, the
pieces will be segregated and stockpiled for re-loading and transport back to the site of
origin at the generator’s expense.
5. Other Considerations
5.1 Site Access and Quantity Estimating
The Site is located about 40 miles west of Boston in Berlin.. From 495,Take 62W exit towards Berlin and after 0.5 mile you will see Sawyer Hill Road on your right, go down to 322 Sawyer Hill Road at Berlin Stone Co to do the scaling and then get back on 62W, follow 62W and then take left at the blinking yellow light on to Barnes Hill Road, take left on Linden Ave and then right on Ball Hill Road to reach Maplewood Farms 24 ball hill road. While leaving Maplewood exit right on Ball Hill Road to Linden Ave, take right on Linden Ave to 62E.Please note while coming in you have to go through Barnes Hill Road and not Linden Ave as there is a low weight bridge on Linden Ave."
Prior to shipment, trucks will be weighed at a certified scale. Access will be through the
access road into the Site and to the given phase area as directed by Lighthouse.
Roadways will be maintained for truck access. Hours of operation are 7:00 am to 3:30
pm from Monday to Friday and some Saturdays.
The owner maintains the appropriate equipment year-round to spread, dry, and
compact the soils.
BN030465.0000_rpt_Soil Mgmt Plan Phase_Aug082011.doc:jc
FIGURES
4
MassDEP - Bureau of Waste Site Cleanup MCP Numerical Ranking System Map: 500 feet & 0.5 Mile Radii Site Name:
24 Ball Hill Road Berlin, MA RTN: NAD83 MA Coordinates:
0mE, 0mN July 12, 2011
The information shown on this map is the best available at the date of printing. For more information please refer to www.mass.gov/mgis/massgis.htm
Page 1 of 1Map Output
7/12/2011http://maps.massgis.state.ma.us/servlet/com.esri.esrimap.Esrimap?ServiceName=matowns...
5
TABLES
DRAFT Table 1Summary of Soil Results and Acceptance CriteriaMaplewood Farms, 24 Ball Hill Road, Berlin, MA
OIL or HAZARDOUS MATERIAL
Berlin Site Max Concentration
Berlin Site Background Avg
3X Site Background AvgConcentration in
"Natural" Soil (MADEP, Spring 2002) RCS1 Berlin Acceptance Criteria PH 1 SS-1 PH 1 SS-2 PH 1 SS-3 MAX Avg 3X average
GC/MS SEMI VOC/PAHs BY 8270D mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg
1,2,4-Trichlorobenzene 0.4 0.4 1.1 NA 2 1.1 0.37 0.37 0.375 ND 0.4 1.12
1,2-Dichlorobenzene 0.4 0.4 1.1 NA 9 1.1 0.37 0.37 0.375 ND 0.4 1.12
1,3-Dichlorobenzene 0.4 0.4 1.1 NA 1 0.9 0.37 0.37 0.375 ND 0.4 1.12
1,4-Dichlorobenzene 0.4 0.4 1.1 NA 0.7 0.6 0.37 0.37 0.375 ND 0.4 1.12
2,2'-oxybis[1-chloropropane] 0.4 0.4 1.1 NA 0.7 0.6 0.37 0.37 0.375 ND 0.4 1.12
2,4,5-Trichlorophenol 0.4 0.4 1.1 NA 4 1.1 0.37 0.37 0.375 ND 0.4 1.12
2,4,6-Trichlorophenol 0.4 0.4 1.1 NA 0.7 0.6 0.37 0.37 0.375 ND 0.4 1.12
2,4-Dichlorophenol 0.4 0.4 1.1 NA 0.7 0.6 0.37 0.37 0.375 ND 0.4 1.12
2,4-Dimethylphenol 0.4 0.4 1.1 NA 0.7 0.6 0.37 0.37 0.375 ND 0.4 1.12
2,4-Dinitrophenol 0.4 0.4 1.1 NA 3 1.1 0.37 0.37 0.375 ND 0.4 1.12
2,4-Dinitrotoluene 0.4 0.4 1.1 NA 0.7 0.6 0.37 0.37 0.375 ND 0.4 1.12
2,6-Dinitrotoluene 0.4 0.4 1.1 NA 100 1.1 0.37 0.37 0.375 ND 0.4 1.12
2-Chloronaphthalene 0.4 0.4 1.1 NA 1000 1.1 0.37 0.37 0.375 ND 0.4 1.12
2-Chlorophenol 0.4 0.4 1.1 NA 0.7 0.6 0.37 0.37 0.375 ND 0.4 1.12
2-Methylnaphthalene 0.2 0.2 0.6 0.7 0.7 0.6 0.185 0.185 0.19 ND 0.2 0.56
2-Methylphenol 0.4 0.4 1.1 NA 500 1.1 0.37 0.37 0.375 ND 0.4 1.12
2-Nitrophenol 0.4 0.4 1.1 NA 100 1.1 0.37 0.37 0.375 ND 0.4 1.12
3 & 4 Methylphenol 0.4 0.4 1.1 NA 500 1.1 0.37 0.37 0.375 ND 0.4 1.12
3,3'-Dichlorobenzidine 0.8 0.8 2.3 NA 1 0.9 0.75 0.75 0.75 ND 0.8 2.25
4-Bromophenyl phenyl ether 0.4 0.4 1.1 NA 100 1.1 0.37 0.37 0.375 ND 0.4 1.12
4-Chloroaniline 0.8 0.8 2.3 NA 1 0.9 0.75 0.75 0.75 ND 0.8 2.25
4-Nitrophenol 1.9 1.9 5.6 NA 100 5 1.85 1.85 1.9 ND 1.9 5.60
Acenaphthene 0.2 0.2 0.6 0.5 4 0.6 0.185 0.185 0.19 ND 0.2 0.56
Acenaphthylene 0.2 0.2 0.6 0.5 1 0.6 0.185 0.185 0.19 ND 0.2 0.56
Acetophenone 0.4 0.4 1.1 NA 1000 1.1 0.37 0.37 0.375 ND 0.4 1.12
Aniline 1.9 1.9 5.6 NA 1000 5 1.85 1.85 1.9 ND 1.9 5.60
Anthracene 0.2 0.2 0.6 1.0 1000 0.6 0.185 0.185 0.19 ND 0.2 0.56
Azobenzene 0.4 0.4 1.1 NA NA 1.1 0.37 0.37 0.375 ND 0.4 1.12
Benzo[a]anthracene 0.8 0.6 1.7 7 7 1.7 0.38 0.8 0.5 0.8 0.6 1.68
Benzo[a]pyrene 0.9 0.7 2.0 2 2 1.9 0.47 0.93 0.64 0.93 0.7 2.04
Benzo[b]fluoranthene 1.5 1.0 3.1 7 7 3.1 0.68 1.5 0.94 1.5 1.0 3.12
Benzo[g,h,i]perylene 0.6 0.4 1.2 1,000 1000 1.2 0.185 0.64 0.41 0.64 0.4 1.24
Benzo[k]fluoranthene 0.5 0.4 1.2 1,000 70 1.2 0.195 0.52 0.44 0.52 0.4 1.16
Bis(2-chloroethoxy)methane 0.4 0.4 1.1 NA 500 1.1 0.37 0.37 0.375 ND 0.4 1.12
Bis(2-chloroethyl)ether 0.4 0.4 1.1 NA 0.7 0.6 0.37 0.37 0.375 ND 0.4 1.12
Bis(2-ethylhexyl) phthalate 3.1 1.3 3.8 200 200 3.8 3.1 0.37 0.375 3.1 1.3 3.85
Butyl benzyl phthalate 0.7 0.5 1.5 NA 100 1.5 0.74 0.37 0.375 0.74 0.5 1.49
Chrysene 1.1 0.8 2.3 70 70 2.3 0.53 1.1 0.68 1.1 0.8 2.31
Dibenz(a,h)anthracene 0.2 0.2 0.6 0.7 0.7 0.6 0.185 0.185 0.19 ND 0.2 0.56
Dibenzofuran 0.4 0.4 1.1 NA 100 1.1 0.37 0.37 0.375 ND 0.4 1.12
Diethyl phthalate 0.4 0.4 1.1 NA 10 1.1 0.37 0.37 0.375 ND 0.4 1.12
Dimethyl phthalate 0.4 0.4 1.1 NA 30 1.1 0.37 0.37 0.375 ND 0.4 1.12
Di-n-butyl phthalate 0.4 0.4 1.1 NA 50 1.1 0.37 0.37 0.375 ND 0.4 1.12
Di-n-octyl phthalate 0.4 0.4 1.1 NA 1000 1.1 0.37 0.37 0.375 ND 0.4 1.12
Fluoranthene 2.6 1.6 4.8 1,000 1000 4.8 0.86 2.6 1.3 2.6 1.6 4.76
Fluorene 0.2 0.2 0.6 1,000 1000 0.6 0.185 0.185 0.19 ND 0.2 0.56
Hexachlorobenzene 0.4 0.4 1.1 NA 0.7 0.6 0.37 0.37 0.375 ND 0.4 1.12
Hexachlorobutadiene 0.4 0.4 1.1 NA 6 1.1 0.37 0.37 0.375 ND 0.4 1.12
Hexachloroethane 0.4 0.4 1.1 NA 0.7 0.6 0.37 0.37 0.375 ND 0.4 1.12
Indeno[1,2,3-cd]pyrene 0.4 0.4 1.1 7 7 1.1 0.37 0.37 0.375 ND 0.4 1.12
Isophorone 0.4 0.4 1.1 NA 100 1.1 0.37 0.37 0.375 ND 0.4 1.12
Naphthalene 0.2 0.2 0.6 4 4 0.6 0.185 0.185 0.19 ND 0.2 0.56
Nitrobenzene 0.4 0.4 1.1 NA 500 1.1 0.37 0.37 0.375 ND 0.4 1.12
Pentachlorophenol 1.9 1.9 5.6 NA 3 2.9 1.85 1.85 1.9 ND 1.9 5.60
Phenanthrene 1.5 0.9 2.6 10 10 2.6 0.43 1.5 0.7 1.5 0.9 2.63
Phenol 0.4 0.4 1.1 NA 1 1.1 0.37 0.37 0.375 ND 0.4 1.12Pyrene 1.9 1.3 3.8 1,000 1000 3.8 0.76 1.9 1.1 1.9 1.3 3.76
DRAFT Table 1Summary of Soil Results and Acceptance CriteriaMaplewood Farms, 24 Ball Hill Road, Berlin, MA
OIL or HAZARDOUS MATERIAL
Berlin Site Max Concentration
Berlin Site Background Avg
3X Site Background AvgConcentration in
"Natural" Soil (MADEP, Spring 2002) RCS1 Berlin Acceptance Criteria PH 1 SS-1 PH 1 SS-2 PH 1 SS-3 MAX Avg 3X average
GC/MS SEMI VOC/PAHs BY 8270D mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg
GC/MS VOA BY 8260C mg/kg mg/kg mg/kg mg/kg mg/kg
1,1,1,2-Tetrachloroethane 0.0 0.0 0.0 ND 0.1 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
1,1,1-Trichloroethane 0.0 0.0 0.0 ND 30 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
1,1,2,2-Tetrachloroethane 0.0 0.0 0.0 ND 0.005 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
1,1,2-Trichloroethane 0.0 0.0 0.0 ND 0.1 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
1,1-Dichloroethane 0.0 0.0 0.0 ND 0.4 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
1,1-Dichloroethene 0.0 0.0 0.0 ND 3 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
1,1-Dichloropropene 0.0 0.0 0.0 ND NA ND 0.00215 0.0014 0.00155 ND 0.0 0.01
1,2,3-Trichlorobenzene 0.0 0.0 0.0 ND NA ND 0.00215 0.0014 0.00155 ND 0.0 0.01
1,2,3-Trichloropropane 0.0 0.0 0.0 ND 100 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
1,2,4-Trichlorobenzene 0.0 0.0 0.0 ND 2 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
1,2,4-Trimethylbenzene 0.0 0.0 0.0 ND 1000 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
1,2-Dibromo-3-Chloropropane 0.0 0.0 0.1 ND 10 ND 0.0215 0.014 0.0155 ND 0.0 0.05
1,2-Dichlorobenzene 0.0 0.0 0.0 ND 9 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
1,2-Dichloroethane 0.0 0.0 0.0 ND 0.1 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
1,2-Dichloropropane 0.0 0.0 0.0 ND 0.1 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
1,3,5-Trimethylbenzene 0.0 0.0 0.0 ND 10 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
1,3-Dichlorobenzene 0.0 0.0 0.0 ND 1 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
1,3-Dichloropropane 0.0 0.0 0.0 ND 500 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
1,4-Dichlorobenzene 0.0 0.0 0.0 ND 0.7 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
1,4-Dioxane 0.2 0.2 0.5 ND 0.2 ND 0.215 0.14 0.155 ND 0.2 0.51
2,2-Dichloropropane 0.0 0.0 0.0 ND NA ND 0.00215 0.0014 0.00155 ND 0.0 0.01
2-Butanone (MEK) 0.0 0.0 0.1 ND 4 ND 0.0215 0.014 0.0155 ND 0.0 0.05
2-Chlorotoluene 0.0 0.0 0.0 ND 100 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
2-Hexanone 0.0 0.0 0.1 ND 100 ND 0.0215 0.014 0.0155 ND 0.0 0.05
4-Chlorotoluene 0.0 0.0 0.0 ND NA ND 0.00215 0.0014 0.00155 ND 0.0 0.01
4-Isopropyltoluene 0.0 0.0 0.0 ND 100 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
4-Methyl-2-pentanone (MIBK) 0.0 0.0 0.1 ND 0.4 ND 0.0215 0.014 0.0155 ND 0.0 0.05
Acetone 0.2 0.2 0.5 ND 6 ND 0.215 0.14 0.155 ND 0.2 0.51
Benzene 0.0 0.0 0.0 ND 2 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
Bromobenzene 0.0 0.0 0.0 ND 100 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
Bromoform 0.0 0.0 0.0 ND 0.1 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
Bromomethane 0.0 0.0 0.0 ND 0.5 ND 0.00425 0.0028 0.00315 ND 0.0 0.01
Carbon disulfide 0.0 0.0 0.0 ND 100 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
Carbon tetrachloride 0.0 0.0 0.0 ND 5 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
Chlorobenzene 0.0 0.0 0.0 ND 1 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
Chlorobromomethane 0.0 0.0 0.0 ND NA ND 0.00215 0.0014 0.00155 ND 0.0 0.01
Chlorodibromomethane 0.0 0.0 0.0 ND 0.005 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
Chloroethane 0.0 0.0 0.0 ND 100 ND 0.00425 0.0028 0.00315 ND 0.0 0.01
Chloroform 0.0 0.0 0.0 ND 0.3 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
Chloromethane 0.0 0.0 0.0 ND 100 ND 0.00425 0.0028 0.00315 ND 0.0 0.01
cis-1,2-Dichloroethene 0.0 0.0 0.0 ND 0.3 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
cis-1,3-Dichloropropene 0.0 0.0 0.0 ND 0.01 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
Dibromomethane 0.0 0.0 0.0 ND 500 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
Dichlorobromomethane 0.0 0.0 0.0 ND 0.1 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
Dichlorodifluoromethane 0.0 0.0 0.0 ND 1000 ND 0.00425 0.0028 0.00315 ND 0.0 0.01
Ethyl ether 0.0 0.0 0.0 ND 100 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
Ethylbenzene 0.0 0.0 0.0 ND 40 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
Ethylene Dibromide 0.0 0.0 0.0 ND 0.1 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
Hexachlorobutadiene 0.0 0.0 0.0 ND 6 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
Isopropyl ether 0.0 0.0 0.0 ND 100 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
Isopropylbenzene 0.0 0.0 0.0 ND 1000 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
Methyl tert-butyl ether 0.0 0.0 0.0 ND 0.1 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
Methylene Chloride 0.0 0.0 0.0 ND 0.1 ND 0.0085 0.0055 0.0065 ND 0.0 0.02
m-Xylene & p-Xylene 0.0 0.0 0.0 ND 300 ND 0.00425 0.0028 0.00315 ND 0.0 0.01
Naphthalene 0.0 0.0 0.1 ND 4 ND 0.0215 0.014 0.0155 ND 0.0 0.05
n-Butylbenzene 0.0 0.0 0.0 ND NA ND 0.00215 0.0014 0.00155 ND 0.0 0.01
N-Propylbenzene 0.0 0.0 0.0 ND 100 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
o-Xylene 0.0 0.0 0.0 ND 300 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
DRAFT Table 1Summary of Soil Results and Acceptance CriteriaMaplewood Farms, 24 Ball Hill Road, Berlin, MA
OIL or HAZARDOUS MATERIAL
Berlin Site Max Concentration
Berlin Site Background Avg
3X Site Background AvgConcentration in
"Natural" Soil (MADEP, Spring 2002) RCS1 Berlin Acceptance Criteria PH 1 SS-1 PH 1 SS-2 PH 1 SS-3 MAX Avg 3X average
GC/MS SEMI VOC/PAHs BY 8270D mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg
sec-Butylbenzene 0.0 0.0 0.0 ND NA ND 0.00215 0.0014 0.00155 ND 0.0 0.01
Styrene 0.0 0.0 0.0 ND 3 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
Tert-amyl methyl ether 0.0 0.0 0.0 ND NA ND 0.00215 0.0014 0.00155 ND 0.0 0.01
Tert-butyl ethyl ether 0.0 0.0 0.0 ND NA ND 0.00215 0.0014 0.00155 ND 0.0 0.01
tert-Butylbenzene 0.0 0.0 0.0 ND 100 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
Tetrachloroethene 0.0 0.0 0.0 ND 1 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
Tetrahydrofuran 0.0 0.0 0.1 ND 500 ND 0.0215 0.014 0.0155 ND 0.0 0.05
Toluene 0.0 0.0 0.0 ND 30 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
trans-1,2-Dichloroethene 0.0 0.0 0.0 ND 1 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
trans-1,3-Dichloropropene 0.0 0.0 0.0 ND 0.01 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
Trichloroethene 0.0 0.0 0.0 ND 0.3 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
Trichlorofluoromethane 0.0 0.0 0.0 ND 1000 ND 0.00425 0.0028 0.00315 ND 0.0 0.01Vinyl chloride 0.0 0.0 0.0 ND 0.6 ND 0.00215 0.0014 0.00155 ND 0.0 0.01
GC SEMI VOA BY 8015B
Total Petroleum Hydrocarbons (C9-C36) 170.0 140.0 420.0 ND 1000 300 120 170 130 170 140.0 420.00
Pesticides BY 8081B mg/kg mg/kg mg/kg mg/kg mg/kg
4,4'-DDD 0.0 0.0 0.0 NA 4 ND (<0.15) 0.0055 0.0055 0.0055 ND 0.0 0.02
4,4'-DDE 0.0 0.0 0.0 NA 3 ND (<0.15) 0.0055 0.0055 0.0055 ND 0.0 0.02
4,4'-DDT 0.0 0.0 0.0 NA 3 ND (<0.15) 0.0055 0.0055 0.0055 ND 0.0 0.02
Aldrin 0.0 0.0 0.0 NA 0.04 ND (<0.15) 0.0055 0.0055 0.0055 ND 0.0 0.02
alpha-BHC 0.0 0.0 0.0 NA 50 ND (<0.15) 0.0055 0.0055 0.0055 ND 0.0 0.02
beta-BHC 0.0 0.0 0.0 NA 10 ND (<0.15) 0.0055 0.0055 0.0055 ND 0.0 0.02
Chlordane (technical) 0.3 0.3 0.8 NA 0.7 ND (<0.15) 0.275 0.28 0.28 ND 0.3 0.84
delta-BHC 0.0 0.0 0.0 NA 10 ND (<0.15) 0.0055 0.0055 0.0055 ND 0.0 0.02
Dieldrin 0.0 0.0 0.0 NA 0.05 ND (<0.15) 0.0055 0.0055 0.0055 ND 0.0 0.02
Endosulfan I 0.0 0.0 0.0 NA 0.5 ND (<0.15) 0.0055 0.0055 0.0055 ND 0.0 0.02
Endosulfan II 0.0 0.0 0.0 NA 0.5 ND (<0.15) 0.0055 0.0055 0.0055 ND 0.0 0.02
Endosulfan sulfate 0.0 0.0 0.0 NA NA ND (<0.15) 0.0055 0.0055 0.0055 ND 0.0 0.02
Endrin 0.0 0.0 0.0 NA 8 ND (<0.15) 0.0055 0.0055 0.0055 ND 0.0 0.02
Endrin ketone 0.0 0.0 0.0 NA NA ND (<0.15) 0.0055 0.0055 0.0055 ND 0.0 0.02
gamma-BHC (Lindane) 0.0 0.0 0.0 NA 0.003 ND (<0.15) 0.00165 0.0017 0.0017 ND 0.0 0.01
Heptachlor 0.0 0.0 0.0 NA 0.2 ND (<0.15) 0.0055 0.0055 0.0055 ND 0.0 0.02
Heptachlor epoxide 0.0 0.0 0.0 NA 0.09 ND (<0.15) 0.0055 0.0055 0.0055 ND 0.0 0.02
Hexachlorobenzene 0.0 0.0 0.0 NA 0.7 ND (<0.15) 0.0055 0.0055 0.0055 ND 0.0 0.02Methoxychlor 0.0 0.0 0.0 NA 200 ND (<0.15) 0.0055 0.0055 0.0055 ND 0.0 0.02
PCBs BY 8082A mg/kg mg/kg mg/kg mg/kg mg/kg
PCB-1016 0.1 0.1 0.2 NA 2 ND (<0.1) 0.055 0.055 0.055 ND 0.1 0.17
PCB-1221 0.1 0.1 0.2 NA 2 ND (<0.1) 0.055 0.055 0.055 ND 0.1 0.17
PCB-1232 0.1 0.1 0.2 NA 2 ND (<0.1) 0.055 0.055 0.055 ND 0.1 0.17
PCB-1242 0.1 0.1 0.2 NA 2 ND (<0.1) 0.055 0.055 0.055 ND 0.1 0.17
PCB-1248 0.1 0.1 0.2 NA 2 ND (<0.1) 0.055 0.055 0.055 ND 0.1 0.17
PCB-1254 0.1 0.1 0.2 NA 2 ND (<0.1) 0.055 0.055 0.055 ND 0.1 0.17
PCB-1260 0.1 0.1 0.2 NA 2 ND (<0.1) 0.055 0.055 0.055 ND 0.1 0.17
PCB-1262 0.1 0.1 0.2 NA 2 ND (<0.1) 0.055 0.055 0.055 ND 0.1 0.17PCB-1268 0.1 0.1 0.2 NA 2 ND (<0.1) 0.055 0.055 0.055 ND 0.1 0.17
Herbicides BY 8151A mg/kg mg/kg mg/kg mg/kg mg/kg
2,4,5-T 0.0 0.0 0.0 NA NA ND (<0.03) 0.0095 0.0095 0.0095 ND 0.0 0.03
2,4-D 0.0 0.0 0.0 NA NA ND (<0.03) 0.0095 0.0095 0.0095 ND 0.0 0.03
2,4-DB 0.0 0.0 0.0 NA NA ND (<0.03) 0.0095 0.0095 0.0095 ND 0.0 0.03
Dalapon 0.0 0.0 0.0 NA NA ND (<0.03) 0.0095 0.0095 0.0095 ND 0.0 0.03
Dicamba 0.0 0.0 0.0 NA NA ND (<0.03) 0.0095 0.0095 0.0095 ND 0.0 0.03
Dichlorprop 0.0 0.0 0.0 NA NA ND (<0.03) 0.0095 0.0095 0.0095 ND 0.0 0.03
Dinoseb 0.0 0.0 0.0 NA NA ND (<0.03) 0.0095 0.0095 0.0095 ND 0.0 0.03
MCPA 1.0 1.0 2.9 NA NA ND (<0.03) 0.95 0.95 0.95 ND 1.0 2.85
Mecoprop 1.0 1.0 2.9 NA NA ND (<0.03) 0.95 0.95 0.95 ND 1.0 2.85Silvex (2,4,5-TP) 0.0 0.0 0.0 NA 100 ND (<0.03) 0.0095 0.0095 0.0095 ND 0.0 0.03
DRAFT Table 1Summary of Soil Results and Acceptance CriteriaMaplewood Farms, 24 Ball Hill Road, Berlin, MA
OIL or HAZARDOUS MATERIAL
Berlin Site Max Concentration
Berlin Site Background Avg
3X Site Background AvgConcentration in
"Natural" Soil (MADEP, Spring 2002) RCS1 Berlin Acceptance Criteria PH 1 SS-1 PH 1 SS-2 PH 1 SS-3 MAX Avg 3X average
GC/MS SEMI VOC/PAHs BY 8270D mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg
METALS BY 6010B mg/kg mg/kg mg/kg mg/kg mg/kg
Antimony 0.3 0.3 0.9 1 20 0.9 0.325 0.32 0.295 ND 0.3 0.94
Arsenic 16.0 15.0 45.0 20 20 20 16 16 13 16 15.0 45.00
Beryllium 0.4 0.4 1.1 0.4 100 1.1 0.31 0.36 0.4 0.4 0.4 1.07
Cadmium 0.1 0.1 0.4 2 2 0.4 0.13 0.13 0.12 ND 0.1 0.38
Chromium 17.0 16.3 49.0 30 30 49 15 17 17 17 16.3 49.00
Copper 31.0 20.7 62.0 40 1000 62 20 31 11 31 20.7 62.00
Lead 31.0 26.3 79.0 300 300 79 31 27 21 31 26.3 79.00
Nickel 16.0 13.0 39.0 20 20 39 12 16 11 16 13.0 39.00
Selenium 0.3 0.3 0.9 0.5 400 0.9 0.325 0.32 0.295 ND 0.3 0.94
Silver 0.7 0.6 1.9 0.6 100 1.9 0.65 0.65 0.6 ND 0.6 1.90
Thallium 0.7 0.6 1.9 0.6 8 1.9 0.65 0.65 0.6 ND 0.6 1.90Zinc 37.0 35.3 106.0 100 2500 106 35 37 34 37 35.3 106.00
METALS BY 7471A mg/kg mg/kg mg/kg mg/kg mg/kg
Mercury 0.0 0.0 0.1 0.3 20 0.1 0.0385 0.0385 0.039 ND 0.0 0.12
GENERAL CHEMISTRY BY MOISTURE % % % % % 0
Percent Moisture 12.0 11.0 33.0 NA NA No Free Water 10 11 12 12 11.0 33.00Percent Solids 90.0 89.0 267.0 NA NA 90 89 88 90 89.0 267.00
GENERAL CHEMISTRY BY SM 2510B umhos/cm umhos/cm umhos/cm umhos/cm umhos/cm
Specific Conductance 500.0 370.0 1110.0 NA NA <1,000 290 500 320 500 370.0 1110.00
General Notes:
NA= Not Applicable, NS= Not Sampled
One-half the laboratory detection limit (DL) is shown in yellow and was utilized to estimate the average concentration shown.
PAHs:3 times site ave. including 1/2 Detection Limits for non-detect samples were used to calc. Acceptance Criteria.
Arsenic: Levels are somewhat elevated in Worcester County as Doc. By DEP (30 ppm or so). Value of 20 was selected but may range to 30 in natural non-impacted soils.
Otherwise soils > 20 ppm Arsenic without exempt status cannot be accepted.
Chromium: 30 is Hex Chromium Std. Chromium can be accepted to 49 ppm with demonstration hex chromium is <30 ppm.
PCBs: No PCBs < 0.10 can be accepted.
Pest/Herbs: Trace levels of pesticides/herbicides can be accepted on case-bycase basis..
Lead and TPH: These are typical constituents in fill soils. Lead value of 79 ppm used as 3X. 300 ppm TPH acceptable from asphalt and not from a fuel oil release.
Conductance: <1,000 umhos/cm can be accepted provided conc's of other metals are low enough.
Trace levels of VOCs may be accepted on case-by-case basis.
Nickel:Nickel 3X ave. was 39 and levels can be accepted up to 39 ppm from natural non-impacted, non-MCP reportable soils.
Otherwise soils > 20 ppm Nickel without exempt status cannot be accepted.
Appendix A
Section of M.G.L. Chapter 40 Section
3A
Appendix B
List of MCP Disposal Sites
Appendix C
Background Sampling Analytical Data
ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica WestfieldWestfield Executive Park53 Southampton RoadWestfield, MA 01085Tel: (413)572-4000
TestAmerica Job ID: 360-34572-1Client Project/Site: 28 Ball Hill RoadRevision: 1
For:ARCADIS U.S., Inc194 Forbes RoadBraintree, Massachusetts 02184
Attn: Mr. Rick Stromberg
Authorized for release by:07/01/2011 02:58:20 PMJoe ChimiReport Production [email protected]
Designee for
Becky MasonProject Manager [email protected]
Results relate only to the items tested and the sample(s) as received by the laboratory.The test results in this report meet all 2003 NELAC requirements for accredited parameters,exceptions are noted in this report. Pursuant to NELAC, this report may not be reproducedexcept in full, and with written approval from the laboratory. For questions please contactthe Project Manager at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signatureis intended to be the legally binding equivalent of a traditionally handwritten signature.
Page 1 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Table of Contents
Client: ARCADIS U.S., IncProject/Site: 28 Ball Hill Road
TestAmerica Job ID: 360-34572-1
Page 2 of 65TestAmerica Westfield
07/01/2011
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 32
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 33
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 37
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 39
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 59
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 61
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 63
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 65
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Case NarrativeClient: ARCADIS U.S., Inc TestAmerica Job ID: 360-34572-1
Project/Site: 28 Ball Hill Road
Job ID: 360-34572-1
Laboratory: TestAmerica Westfield
Narrative
Revision 1: Report was revised on 07/01/2011 to report method 8270D at a lower dilution. This final report replaces the final report
generated on 06/30/2011.
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,
the reporting limits are adjusted relative to the dilution required.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the
individual sections below.
RECEIPT
The samples were received on 06/17/2011; the samples arrived in good condition, properly preserved and on ice. The temperature of the
coolers at receipt was 0.8 C.
Note: All samples which require thermal preservation are considered acceptable if the arrival temperature is within 2 C of the required
temperature or method specified range. For samples with a specified temperature of 4 C, samples with a temperature ranging from just
above freezing temperature of water to 6 C shall be acceptable. Samples that are hand delivered immediately following collection may not
meet these criteria, however they will be deemed acceptable according to NELAC and State standards, if there is evidence that the chilling
process has begun, such as arrival on ice, etc.
TestAmerica’s Reporting Limits (RLs) for this report may not always meet WSC-CAM-III method reporting limits due to various reasons
such as methodology, dilutions or moisture content (soils). TestAmerica’s MA pivot table EDD documents which compound(s) exceed
certain regulatory standards. If not included with your deliverables, please contact your Project Manager about the availability of this EDD
for your report.
VOLATILE ORGANIC COMPOUNDS (GC-MS)
Samples PH 1 SS-1 (360-34572-1), PH 1 SS-2 (360-34572-2) and PH 1 SS-3 (360-34572-3) were analyzed for volatile organic
compounds (GC-MS) in accordance with SW846 8260C. The samples were prepared on 06/26/2011 and analyzed on 06/27/2011.
1,4-Dioxane exceeded the rpd limit for LCSD 360-75985/2-A. Refer to the QC report for details.
1,1,2,2-Tetrachloroethane, 2-Hexanone, 4-Methyl-2-pentanone (MIBK) and Tetrahydrofuran failed the continuing calibration verification
(CCV) criteria low; Dichlorodifluoromethane failed the criteria high.
No other difficulties were encountered during the VOC analyses.
All other quality control parameters were within the acceptance limits.
SEMIVOLATILE ORGANIC COMPOUNDS (GC-MS)
Samples PH 1 SS-1 (360-34572-1), PH 1 SS-2 (360-34572-2) and PH 1 SS-3 (360-34572-3) were analyzed for semivolatile organic
compounds (GC-MS) in accordance with SW846 8270D. The samples were prepared on 06/21/2011 and analyzed on 06/24/2011 and
06/25/2011.
Aniline failed the recovery criteria low for LCS 360-75634/2-A and LCSD 360-75634/3-A. Refer to the QC report for details.
The calibration curve used quadratic regression for 1,2,4-Trichlorobenzene, 2,4-Dimethylphenol, 2-Nitrophenol, Hexachlorobutadiene,
Isophorone and Naphthalene.
Samples PH 1 SS-1 (360-34572-1)[2X], PH 1 SS-2 (360-34572-2)[2X] and PH 1 SS-3 (360-34572-3)[2X] required dilution prior to analysis
due to black color. The reporting limits have been adjusted accordingly.
TestAmerica Westfield
Page 3 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Case NarrativeClient: ARCADIS U.S., Inc TestAmerica Job ID: 360-34572-1
Project/Site: 28 Ball Hill Road
Job ID: 360-34572-1 (Continued)
Laboratory: TestAmerica Westfield (Continued)
No other difficulties were encountered during the SVOC analyses.
All other quality control parameters were within the acceptance limits.
CHLORINATED PESTICIDES
Samples PH 1 SS-1 (360-34572-1), PH 1 SS-2 (360-34572-2) and PH 1 SS-3 (360-34572-3) were analyzed for chlorinated pesticides in
accordance with EPA SW-846 Method 8081A. The samples were prepared and analyzed on 06/21/2011.
4,4'-DDD and Endrin failed the recovery criteria high for LCS 360-75557/9-A. 4,4'-DDD, 4,4'-DDE, Endrin and Heptachlor failed the
recovery criteria high for LCSD 360-75557/10-A. These analytes were not detected in the associated samples. Results would be biased
high. Refer to the QC report for details.
For the opening continuing calibration verification (CCV), 4,4’-DDT failed the criteria low (primary column only). 4,4’-DDD failed the criteria
high (primary column only) and 4,4’-DDE, Dieldrin, Endosulfan I, Endosulfan II, Endosulfan sulfate, Endrin and Heptachlor failed the
criteria high (secondary column only). For the closing CCV, 4,4’-DDT and Methoxychlor failed the criteria low (primary and secondary
columns). The associated samples PH 1 SS-1 (360-34572-1), PH 1 SS-2 (360-34572-2) and PH 1 SS-3 (360-34572-3) were re-analyzed
with similar results. The original results are reported. 4,4’-DDD and 4,4’-DDE failed the criteria high (primary column only) and Endrin
failed the criteria high (secondary column only).
No other difficulties were encountered during the pesticides analyses.
All other quality control parameters were within the acceptance limits.
POLYCHLORINATED BIPHENYLS (PCBS)
Samples PH 1 SS-1 (360-34572-1), PH 1 SS-2 (360-34572-2) and PH 1 SS-3 (360-34572-3) were analyzed for polychlorinated biphenyls
(PCBs) in accordance with SW846 8082A. The samples were prepared and analyzed on 06/21/2011.
No difficulties were encountered during the PCBs analyses.
All quality control parameters were within the acceptance limits.
CHLORINATED HERBICIDES
Samples PH 1 SS-1 (360-34572-1), PH 1 SS-2 (360-34572-2) and PH 1 SS-3 (360-34572-3) were analyzed for chlorinated herbicides in
accordance with EPA SW-846 Method 8151A. The samples were prepared on 06/24/2011 and analyzed on 06/26/2011.
This analysis was performed at TestAmerica Edison, 777 New Durham Road, Edison, NJ 08817.
The following required QA/QC procedures, which may affect Presumptive Certainty, were not met: This method was performed using
laboratory in-house control limits rather than MCP program control limits.
2,4-Dichlorophenylacetic acid failed the surrogate recovery criteria high for PH 1 SS-1 (360-34572-1). No target analytes were detected in
this sample. Results would be biased high. Refer to the QC report for details.
Dinoseb failed the recovery criteria low for LCSD 460-77865/3-A. Dalapon and Dinoseb exceeded the rpd limit. Percent recoveries for the
LCS were within control limits. Refer to the QC report for details.
No other difficulties were encountered during the herbicides analyses.
All other quality control parameters were within the acceptance limits.
TOTAL METALS (ICP)
Samples PH 1 SS-1 (360-34572-1), PH 1 SS-2 (360-34572-2) and PH 1 SS-3 (360-34572-3) were analyzed for total metals (ICP) in
accordance with EPA SW-846 Method 6010B. The samples were prepared and analyzed on 06/20/2011.
At the request of the client, a modified MCP analyte list (EPA PP13 vs. WSC CAM III-A) was reported for this job.
TestAmerica Westfield
Page 4 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Case NarrativeClient: ARCADIS U.S., Inc TestAmerica Job ID: 360-34572-1
Project/Site: 28 Ball Hill Road
Job ID: 360-34572-1 (Continued)
Laboratory: TestAmerica Westfield (Continued)
No difficulties were encountered during the metals analyses.
All quality control parameters were within the acceptance limits.
TOTAL MERCURY
Samples PH 1 SS-1 (360-34572-1), PH 1 SS-2 (360-34572-2) and PH 1 SS-3 (360-34572-3) were analyzed for total mercury in
accordance with EPA SW-846 Method 7471A. The samples were prepared and analyzed on 06/20/2011.
No difficulties were encountered during the mercury analyses.
All quality control parameters were within the acceptance limits.
DIESEL RANGE ORGANICS
Samples PH 1 SS-1 (360-34572-1), PH 1 SS-2 (360-34572-2) and PH 1 SS-3 (360-34572-3) were analyzed for diesel range organics in
accordance with EPA SW-846 Method 8015B - DRO. The samples were prepared on 06/21/2011 and analyzed on 06/23/2011.
Samples PH 1 SS-1 (360-34572-1)[10X], PH 1 SS-2 (360-34572-2)[10X] and PH 1 SS-3 (360-34572-3)[10X] required dilution prior to
analysis due dark, black color. The reporting limits have been adjusted accordingly.
No difficulties were encountered during the DRO analyses.
All quality control parameters were within the acceptance limits.
PERCENT SOLIDS
Samples PH 1 SS-1 (360-34572-1), PH 1 SS-2 (360-34572-2) and PH 1 SS-3 (360-34572-3) were analyzed for percent solids in
accordance with EPA Moisture. The samples were analyzed on 06/20/2011.
No difficulties were encountered during the % solids analyses.
All quality control parameters were within the acceptance limits.
SPECIFIC CONDUCTIVITY
Samples PH 1 SS-1 (360-34572-1), PH 1 SS-2 (360-34572-2) and PH 1 SS-3 (360-34572-3) were analyzed for specific conductivity in
accordance with SM20 2510B. The samples were leached on 06/23/2011 and analyzed on 06/23/2011.
No difficulties were encountered during the conductivity analyses.
All quality control parameters were within the acceptance limits.
TestAmerica Westfield
Page 5 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Project #:
RTN:
Matrices: Groundwater/Surface Water Soil/Sediment Drinking Water Air
7470/7471 Hg Mass DEP VPH 8081 Pesticides 7196 Hex CrCAM III B CAM IV A CAM V B CAM VI B7010 Metals Mass DEP EPH 8151 Herbicides 8330 ExplosivesCAM III C CAM IV B CAM V C CAM VIII A
6020 Metals 8082 PCB9014 Total Cyanide/PAC 332.0 Perchlorate
CAM III D CAM V A CAM VI A CAM VIII B
A Yes No
B Yes No
C Yes No
D Yes No
Yes No
Yes No
F Yes No
G Yes No1
H Yes No
I Yes No
Signature: Position:
Printed Name: Date:
This form has been electronically signed and approved
TestAmerica Westfield
CAM IX A
This form provides certifications for the following data set: list Laboratory Sample ID Number(s):
Project Location:
Were all QC performance standards specified in the CAM protocol(s) achieved?
1 All negative responses must be addressed in an attached laboratory narrative.
Responses to Questions G, H and I below are required for "Presumptive Certainty" status
Laboratory Name: 360-34572-1
Laboratory Director
CAM III A
CAM II B
6010 Metals
Does the laboratory report comply with all the reporting requirements specified in CAM VII A, "Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data"?
b. APH and TO-15 Methods only: Was the complete analyte list reported for each method?E
Were all required corrective actions and analytical response actions specified in the selected CAM protocol(s) implemented for all identified performance standard non-conformances?
a. VPH, EPH and APH Methods only: Was each method conducted without significant modification(s)? (Refer to the individual method(s) for a list of significant modifications).
Were all applicable CAM protocol QC and performance standard non-conformances identified and evaluated in a laboratory narrative (including all "No" responses to Questions A through E)?
Steven C. Hartmann 6/28/11 15:08
MassDEP Analytical Protocol Certification Form
I, the undersigned, attest under the pains and penalties of perjury that, based upon my personal inquiry of those responsible for obtaining the information, the material contained in this analytical report is, to the best of my knowledge and belief,
Data User Note: Data that achieve "Presumptive Certainty" status may not necessarily meet the data usability and representativeness requirements described in 310 CMR 40. 1056 (2)(k) and WCS-07-350
CAM IX B
Other:
Berlin MA
is accurate and complete.
Were the reporting limits at or below all CAM reporting limits specified in the selected CAM protocol(s)?
Were results reported for the complete analyte list specified in the selected CAM protocol(s) ?
Were the analytical method(s) and all associated QC requirements specified in the selected CAM protocol(s) followed?
TO-15 VOC
CAM Protocols (check all that apply below):
360-34572-(1-3)
Were all samples received in a condition consistent with those described on the Chain-of-Custody, properly preserved (including temperature) in the field or laboratory, and prepared/analyzed within method holding time.
8270 SVOC
8260 VOCCAM II A
Mass DEP APH
Affirmative Responses to Questions A through F are required for "Presumptive Certainty" status
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
X
Page 6 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Project #:
RTN:
Matrices: Groundwater/Surface Water Soil/Sediment Drinking Water Air
7470/7471 Hg Mass DEP VPH 8081 Pesticides 7196 Hex Cr
CAM III B CAM IV A CAM V B CAM VI B7010 Metals Mass DEP EPH 8151 Herbicides 8330 Explosives
CAM III C CAM IV B CAM V C CAM VIII A
6020 Metals 8082 PCB9014 Total Cyanide/PAC 332.0 Perchlorate
CAM III D CAM V A CAM VI A CAM VIII B
A Yes No
B Yes No
C Yes No
D Yes No
Yes No
Yes No
F Yes No
G Yes No1
H Yes No
I Yes No
Signature: Position:
Printed Name: Date:
MassDEP Analytical Protocol Certification Form
I, the undersigned, attest under the pains and penalties of perjury that, based upon my personal inquiry of those responsible for obtaining the information, the material contained in this analytical report is, to the best of my knowledge and belief,
Data User Note: Data that achieve "Presumptive Certainty" status may not necessarily meet the data usability and representativeness requirements described in 310 CMR 40. 1056 (2)(k) and WCS-07-350
CAM IX B
Other:
a. VPH, EPH and APH Methods only: Was each method conducted without significant modification(s)? (Refer to the individual method(s) for a list of significant modifications). E
TestAmerica Edison
CAM II B
6010 Metals
Does the laboratory report comply with all the reporting requirements specified in CAM VII A, "Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data"?
Were all required corrective actions and analytical response actions specified in the selected CAM protocol(s) implemented for all identified performance standard non-conformances?
Affirmative Responses to Questions A through F are required for "Presumptive Certainty" status
Were all samples received in a condition consistent with those described on the Chain-of-Custody, properly preserved (including temperature) in the field or laboratory, and prepared/analyzed within method holding time.
Were the analytical method(s) and all associated QC requirements specified in the selected CAM protocol(s) followed?
Catalina Dalangin
GC SemiVolatiles Manager II
is accurate and complete.
CAM III A
b. APH and TO-15 Methods only: Was the complete analyte list reported for each method?
Were all applicable CAM protocol QC and performance standard non-conformances identified and evaluated in a laboratory narrative (including all "No" responses to Questions A through E)?
CAM IX ATO-15 VOC
CAM Protocols (check all that apply below):
6/29/11 0:00
Were all QC performance standards specified in the CAM protocol(s) achieved?
1 All negative responses must be addressed in an attached laboratory narrative.
Responses to Questions G, H and I below are required for "Presumptive Certainty" status
Were the reporting limits at or below all CAM reporting limits specified in the selected CAM protocol(s)?
Were results reported for the complete analyte list specified in the selected CAM protocol(s) ?
360-34572-1, 360-34572-2 and 360-34572-3
Laboratory Name:
8270 SVOC
8260 VOC
CAM II A
This form provides certifications for the following data set: list Laboratory Sample ID Number(s):
Project Location:
360-34572-1
28 Ball Hill Road
Mass DEP APH
X
X
X
X
X
X
X
X
X
X
Page 7 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Detection SummaryTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Client Sample ID: PH 1 SS-1 Lab Sample ID: 360-34572-1
Analyte Result Qualifier Unit Method Prep TypeD
☼
Dil Fac
Benzo[a]anthracene 380
RL
370 ug/Kg 8270D Total/NA2
MDL
☼Benzo[a]pyrene 8270D Total/NA470 370 ug/Kg 2
☼Benzo[b]fluoranthene 8270D Total/NA680 370 ug/Kg 2
☼Bis(2-ethylhexyl) phthalate 8270D Total/NA3100 740 ug/Kg 2
☼Chrysene 8270D Total/NA530 370 ug/Kg 2
☼Fluoranthene 8270D Total/NA860 370 ug/Kg 2
☼Phenanthrene 8270D Total/NA430 370 ug/Kg 2
☼Pyrene 8270D Total/NA760 370 ug/Kg 2
☼Arsenic 6010B Total/NA16 1.3 mg/Kg 1
☼Beryllium 6010B Total/NA0.31 0.26 mg/Kg 1
☼Chromium 6010B Total/NA15 0.65 mg/Kg 1
☼Copper 6010B Total/NA20 2.6 mg/Kg 1
☼Nickel 6010B Total/NA12 2.6 mg/Kg 1
☼Lead 6010B Total/NA31 0.65 mg/Kg 1
☼Zinc 6010B Total/NA35 3.3 mg/Kg 1
Analyte Result Qualifier Unit Method Prep TypeD
☼
Dil Fac
Total Petroleum Hydrocarbons
(C9-C36)
120
RL
36 mg/Kg 8015B Total/NA10
RL
Specific Conductance SM 2510B Soluble290 3.9 umhos/cm 1
Client Sample ID: PH 1 SS-2 Lab Sample ID: 360-34572-2
Analyte Result Qualifier Unit Method Prep TypeD
☼
Dil Fac
Benzo[a]anthracene 800
RL
370 ug/Kg 8270D Total/NA2
MDL
☼Benzo[a]pyrene 8270D Total/NA930 370 ug/Kg 2
☼Benzo[b]fluoranthene 8270D Total/NA1500 370 ug/Kg 2
☼Benzo[g,h,i]perylene 8270D Total/NA640 370 ug/Kg 2
☼Benzo[k]fluoranthene 8270D Total/NA520 390 ug/Kg 2
☼Chrysene 8270D Total/NA1100 370 ug/Kg 2
☼Fluoranthene 8270D Total/NA2600 370 ug/Kg 2
☼Phenanthrene 8270D Total/NA1500 370 ug/Kg 2
☼Pyrene 8270D Total/NA1900 370 ug/Kg 2
☼Arsenic 6010B Total/NA16 1.3 mg/Kg 1
☼Beryllium 6010B Total/NA0.36 0.26 mg/Kg 1
☼Chromium 6010B Total/NA17 0.64 mg/Kg 1
☼Copper 6010B Total/NA31 2.6 mg/Kg 1
☼Nickel 6010B Total/NA16 2.6 mg/Kg 1
☼Lead 6010B Total/NA27 0.64 mg/Kg 1
☼Zinc 6010B Total/NA37 3.2 mg/Kg 1
☼Mercury 7471A Total/NA0.077 0.071 mg/Kg 1
Analyte Result Qualifier Unit Method Prep TypeD
☼
Dil Fac
Total Petroleum Hydrocarbons
(C9-C36)
170
RL
36 mg/Kg 8015B Total/NA10
RL
Specific Conductance SM 2510B Soluble500 4.0 umhos/cm 1
Client Sample ID: PH 1 SS-3 Lab Sample ID: 360-34572-3
Analyte Result Qualifier Unit Method Prep TypeD
☼
Dil Fac
Benzo[a]anthracene 500
RL
380 ug/Kg 8270D Total/NA2
MDL
☼Benzo[a]pyrene 8270D Total/NA640 380 ug/Kg 2
☼Benzo[b]fluoranthene 8270D Total/NA940 380 ug/Kg 2
☼Benzo[g,h,i]perylene 8270D Total/NA410 380 ug/Kg 2
☼Benzo[k]fluoranthene 8270D Total/NA440 400 ug/Kg 2
☼Chrysene 8270D Total/NA680 380 ug/Kg 2
TestAmerica Westfield
Page 8 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Detection SummaryTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Client Sample ID: PH 1 SS-3 (Continued) Lab Sample ID: 360-34572-3
Analyte Result Qualifier Unit Method Prep TypeD
☼
Dil Fac
Fluoranthene 1300
RL
380 ug/Kg 8270D Total/NA2
MDL
☼Phenanthrene 8270D Total/NA700 380 ug/Kg 2
☼Pyrene 8270D Total/NA1100 380 ug/Kg 2
☼Arsenic 6010B Total/NA13 1.2 mg/Kg 1
☼Beryllium 6010B Total/NA0.40 0.24 mg/Kg 1
☼Chromium 6010B Total/NA17 0.59 mg/Kg 1
☼Copper 6010B Total/NA11 2.4 mg/Kg 1
☼Nickel 6010B Total/NA11 2.4 mg/Kg 1
☼Lead 6010B Total/NA21 0.59 mg/Kg 1
☼Zinc 6010B Total/NA34 3.0 mg/Kg 1
Analyte Result Qualifier Unit Method Prep TypeD
☼
Dil Fac
Total Petroleum Hydrocarbons
(C9-C36)
130
RL
37 mg/Kg 8015B Total/NA10
RL
Specific Conductance SM 2510B Soluble320 3.9 umhos/cm 1
TestAmerica Westfield
Page 9 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Method SummaryTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Method Method Description LaboratoryProtocol
MA DEP8260C Volatile Organic Compounds (GC/MS) TAL WFD
MA DEP8270D Semivolatile Organic Compounds (GC/MS) TAL WFD
SW8468015B 8100M (Modified) Total Extractable Petroleum Hydrocarbons TAL WFD
MA DEP8081B Organochlorine Pesticides (GC/ECD) TAL WFD
MA DEP8082A Polychlorinated Biphenyls (GC/ECD) TAL WFD
SW8468151A Herbicides (GC) TAL EDI
SW8466010B Metals (ICP) TAL WFD
SW8467471A Mercury (CVAA) TAL WFD
EPAMoisture Percent Moisture TAL WFD
SMSM 2510B Conductivity, Specific Conductance TAL WFD
Protocol References:
EPA = US Environmental Protection Agency
MA DEP = Massachusetts Department Of Environmental Protection
SM = "Standard Methods For The Examination Of Water And Wastewater",
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL EDI = TestAmerica Edison, 777 New Durham Road, Edison, NJ 08817, TEL (732)549-3900
TAL WFD = TestAmerica Westfield, Westfield Executive Park, 53 Southampton Road, Westfield, MA 01085, TEL (413)572-4000
TestAmerica Westfield
Page 10 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Sample SummaryTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
360-34572-1 PH 1 SS-1 Solid 06/16/11 14:00 06/17/11 16:55
360-34572-2 PH 1 SS-2 Solid 06/16/11 14:00 06/17/11 16:55
360-34572-3 PH 1 SS-3 Solid 06/16/11 14:00 06/17/11 16:55
TestAmerica Westfield
Page 11 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Client Sample ResultsTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Method: 8260C - Volatile Organic Compounds (GC/MS)
Lab Sample ID: 360-34572-1Client Sample ID: PH 1 SS-1
Matrix: SolidDate Collected: 06/16/11 14:00
Percent Solids: 89.9Date Received: 06/17/11 16:55
Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
1,1,1,2-Tetrachloroethane ND 4.3 ug/Kg ☼ 06/26/11 10:49 06/27/11 07:50 1
Analyte
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼1,1,1-Trichloroethane ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼1,1,2,2-Tetrachloroethane ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼1,1,2-Trichloroethane ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼1,1-Dichloroethane ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼1,1-Dichloroethene ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼1,1-Dichloropropene ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼1,2,3-Trichlorobenzene ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼1,2,3-Trichloropropane ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼1,2,4-Trichlorobenzene ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼1,2,4-Trimethylbenzene ND
43 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼1,2-Dibromo-3-Chloropropane ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼1,2-Dichlorobenzene ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼1,2-Dichloroethane ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼1,2-Dichloropropane ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼1,3,5-Trimethylbenzene ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼1,3-Dichlorobenzene ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼1,3-Dichloropropane ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼1,4-Dichlorobenzene ND
430 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼1,4-Dioxane ND *
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼2,2-Dichloropropane ND
43 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼2-Butanone (MEK) ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼2-Chlorotoluene ND
43 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼2-Hexanone ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼4-Chlorotoluene ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼4-Isopropyltoluene ND
43 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼4-Methyl-2-pentanone (MIBK) ND
430 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Acetone ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Benzene ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Bromobenzene ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Bromoform ND
8.5 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Bromomethane ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Carbon disulfide ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Carbon tetrachloride ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Chlorobenzene ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Chlorobromomethane ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Chlorodibromomethane ND
8.5 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Chloroethane ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Chloroform ND
8.5 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Chloromethane ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼cis-1,2-Dichloroethene ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼cis-1,3-Dichloropropene ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Dibromomethane ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Dichlorobromomethane ND
8.5 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Dichlorodifluoromethane ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Ethyl ether ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Ethylbenzene ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Ethylene Dibromide ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Hexachlorobutadiene ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Isopropyl ether ND
TestAmerica Westfield
Page 12 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Client Sample ResultsTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Method: 8260C - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 360-34572-1Client Sample ID: PH 1 SS-1
Matrix: SolidDate Collected: 06/16/11 14:00
Percent Solids: 89.9Date Received: 06/17/11 16:55
Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Isopropylbenzene ND 4.3 ug/Kg ☼ 06/26/11 10:49 06/27/11 07:50 1
Analyte
8.5 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼m-Xylene & p-Xylene ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Methyl tert-butyl ether ND
17 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Methylene Chloride ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼n-Butylbenzene ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼N-Propylbenzene ND
43 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Naphthalene ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼o-Xylene ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼sec-Butylbenzene ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Styrene ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Tert-amyl methyl ether ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Tert-butyl ethyl ether ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼tert-Butylbenzene ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Tetrachloroethene ND
43 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Tetrahydrofuran ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Toluene ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼trans-1,2-Dichloroethene ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼trans-1,3-Dichloropropene ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Trichloroethene ND
8.5 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Trichlorofluoromethane ND
4.3 ug/Kg 06/26/11 10:49 06/27/11 07:50 1☼Vinyl chloride ND
Qualifier Prepared Analyzed Dil Fac % Recovery Limits
4-Bromofluorobenzene 108 70 - 130 06/26/11 10:49 06/27/11 07:50 1
Surrogate
Dibromofluoromethane 108 06/26/11 10:49 06/27/11 07:50 170 - 130
Toluene-d8 (Surr) 103 06/26/11 10:49 06/27/11 07:50 170 - 130
Lab Sample ID: 360-34572-2Client Sample ID: PH 1 SS-2
Matrix: SolidDate Collected: 06/16/11 14:00
Percent Solids: 88.6Date Received: 06/17/11 16:55
Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
1,1,1,2-Tetrachloroethane ND 2.8 ug/Kg ☼ 06/26/11 10:49 06/27/11 08:14 1
Analyte
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼1,1,1-Trichloroethane ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼1,1,2,2-Tetrachloroethane ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼1,1,2-Trichloroethane ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼1,1-Dichloroethane ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼1,1-Dichloroethene ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼1,1-Dichloropropene ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼1,2,3-Trichlorobenzene ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼1,2,3-Trichloropropane ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼1,2,4-Trichlorobenzene ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼1,2,4-Trimethylbenzene ND
28 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼1,2-Dibromo-3-Chloropropane ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼1,2-Dichlorobenzene ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼1,2-Dichloroethane ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼1,2-Dichloropropane ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼1,3,5-Trimethylbenzene ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼1,3-Dichlorobenzene ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼1,3-Dichloropropane ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼1,4-Dichlorobenzene ND
280 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼1,4-Dioxane ND *
TestAmerica Westfield
Page 13 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Client Sample ResultsTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Method: 8260C - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 360-34572-2Client Sample ID: PH 1 SS-2
Matrix: SolidDate Collected: 06/16/11 14:00
Percent Solids: 88.6Date Received: 06/17/11 16:55
Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
2,2-Dichloropropane ND 2.8 ug/Kg ☼ 06/26/11 10:49 06/27/11 08:14 1
Analyte
28 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼2-Butanone (MEK) ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼2-Chlorotoluene ND
28 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼2-Hexanone ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼4-Chlorotoluene ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼4-Isopropyltoluene ND
28 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼4-Methyl-2-pentanone (MIBK) ND
280 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼Acetone ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼Benzene ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼Bromobenzene ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼Bromoform ND
5.6 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼Bromomethane ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼Carbon disulfide ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼Carbon tetrachloride ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼Chlorobenzene ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼Chlorobromomethane ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼Chlorodibromomethane ND
5.6 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼Chloroethane ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼Chloroform ND
5.6 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼Chloromethane ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼cis-1,2-Dichloroethene ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼cis-1,3-Dichloropropene ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼Dibromomethane ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼Dichlorobromomethane ND
5.6 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼Dichlorodifluoromethane ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼Ethyl ether ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼Ethylbenzene ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼Ethylene Dibromide ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼Hexachlorobutadiene ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼Isopropyl ether ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼Isopropylbenzene ND
5.6 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼m-Xylene & p-Xylene ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼Methyl tert-butyl ether ND
11 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼Methylene Chloride ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼n-Butylbenzene ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼N-Propylbenzene ND
28 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼Naphthalene ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼o-Xylene ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼sec-Butylbenzene ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼Styrene ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼Tert-amyl methyl ether ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼Tert-butyl ethyl ether ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼tert-Butylbenzene ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼Tetrachloroethene ND
28 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼Tetrahydrofuran ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼Toluene ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼trans-1,2-Dichloroethene ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼trans-1,3-Dichloropropene ND
2.8 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼Trichloroethene ND
5.6 ug/Kg 06/26/11 10:49 06/27/11 08:14 1☼Trichlorofluoromethane ND
TestAmerica Westfield
Page 14 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Client Sample ResultsTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Method: 8260C - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 360-34572-2Client Sample ID: PH 1 SS-2
Matrix: SolidDate Collected: 06/16/11 14:00
Percent Solids: 88.6Date Received: 06/17/11 16:55
Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Vinyl chloride ND 2.8 ug/Kg ☼ 06/26/11 10:49 06/27/11 08:14 1
Analyte
Qualifier Prepared Analyzed Dil Fac % Recovery Limits
4-Bromofluorobenzene 105 70 - 130 06/26/11 10:49 06/27/11 08:14 1
Surrogate
Dibromofluoromethane 107 06/26/11 10:49 06/27/11 08:14 170 - 130
Toluene-d8 (Surr) 102 06/26/11 10:49 06/27/11 08:14 170 - 130
Lab Sample ID: 360-34572-3Client Sample ID: PH 1 SS-3
Matrix: SolidDate Collected: 06/16/11 14:00
Percent Solids: 88.1Date Received: 06/17/11 16:55
Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
1,1,1,2-Tetrachloroethane ND 3.1 ug/Kg ☼ 06/26/11 10:49 06/27/11 08:39 1
Analyte
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼1,1,1-Trichloroethane ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼1,1,2,2-Tetrachloroethane ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼1,1,2-Trichloroethane ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼1,1-Dichloroethane ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼1,1-Dichloroethene ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼1,1-Dichloropropene ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼1,2,3-Trichlorobenzene ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼1,2,3-Trichloropropane ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼1,2,4-Trichlorobenzene ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼1,2,4-Trimethylbenzene ND
31 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼1,2-Dibromo-3-Chloropropane ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼1,2-Dichlorobenzene ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼1,2-Dichloroethane ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼1,2-Dichloropropane ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼1,3,5-Trimethylbenzene ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼1,3-Dichlorobenzene ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼1,3-Dichloropropane ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼1,4-Dichlorobenzene ND
310 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼1,4-Dioxane ND *
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼2,2-Dichloropropane ND
31 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼2-Butanone (MEK) ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼2-Chlorotoluene ND
31 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼2-Hexanone ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼4-Chlorotoluene ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼4-Isopropyltoluene ND
31 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼4-Methyl-2-pentanone (MIBK) ND
310 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼Acetone ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼Benzene ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼Bromobenzene ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼Bromoform ND
6.3 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼Bromomethane ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼Carbon disulfide ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼Carbon tetrachloride ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼Chlorobenzene ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼Chlorobromomethane ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼Chlorodibromomethane ND
6.3 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼Chloroethane ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼Chloroform ND
6.3 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼Chloromethane ND
TestAmerica Westfield
Page 15 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Client Sample ResultsTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Method: 8260C - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 360-34572-3Client Sample ID: PH 1 SS-3
Matrix: SolidDate Collected: 06/16/11 14:00
Percent Solids: 88.1Date Received: 06/17/11 16:55
Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
cis-1,2-Dichloroethene ND 3.1 ug/Kg ☼ 06/26/11 10:49 06/27/11 08:39 1
Analyte
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼cis-1,3-Dichloropropene ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼Dibromomethane ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼Dichlorobromomethane ND
6.3 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼Dichlorodifluoromethane ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼Ethyl ether ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼Ethylbenzene ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼Ethylene Dibromide ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼Hexachlorobutadiene ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼Isopropyl ether ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼Isopropylbenzene ND
6.3 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼m-Xylene & p-Xylene ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼Methyl tert-butyl ether ND
13 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼Methylene Chloride ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼n-Butylbenzene ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼N-Propylbenzene ND
31 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼Naphthalene ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼o-Xylene ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼sec-Butylbenzene ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼Styrene ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼Tert-amyl methyl ether ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼Tert-butyl ethyl ether ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼tert-Butylbenzene ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼Tetrachloroethene ND
31 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼Tetrahydrofuran ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼Toluene ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼trans-1,2-Dichloroethene ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼trans-1,3-Dichloropropene ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼Trichloroethene ND
6.3 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼Trichlorofluoromethane ND
3.1 ug/Kg 06/26/11 10:49 06/27/11 08:39 1☼Vinyl chloride ND
Qualifier Prepared Analyzed Dil Fac % Recovery Limits
4-Bromofluorobenzene 108 70 - 130 06/26/11 10:49 06/27/11 08:39 1
Surrogate
Dibromofluoromethane 107 06/26/11 10:49 06/27/11 08:39 170 - 130
Toluene-d8 (Surr) 105 06/26/11 10:49 06/27/11 08:39 170 - 130
TestAmerica Westfield
Page 16 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Client Sample ResultsTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Lab Sample ID: 360-34572-1Client Sample ID: PH 1 SS-1
Matrix: SolidDate Collected: 06/16/11 14:00
Percent Solids: 89.9Date Received: 06/17/11 16:55
Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
1,2,4-Trichlorobenzene ND 740 ug/Kg ☼ 06/21/11 11:45 06/30/11 16:56 2
Analyte
740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼1,2-Dichlorobenzene ND
740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼1,3-Dichlorobenzene ND
740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼1,4-Dichlorobenzene ND
740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼2,2'-oxybis[1-chloropropane] ND
740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼2,4,5-Trichlorophenol ND
740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼2,4,6-Trichlorophenol ND
740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼2,4-Dichlorophenol ND
740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼2,4-Dimethylphenol ND
740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼2,4-Dinitrophenol ND
740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼2,4-Dinitrotoluene ND
740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼2,6-Dinitrotoluene ND
740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼2-Chloronaphthalene ND
740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼2-Chlorophenol ND
370 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼2-Methylnaphthalene ND
740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼2-Methylphenol ND
740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼2-Nitrophenol ND
740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼3 & 4 Methylphenol ND
1500 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼3,3'-Dichlorobenzidine ND
740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼4-Bromophenyl phenyl ether ND
1500 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼4-Chloroaniline ND
3700 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼4-Nitrophenol ND
370 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Acenaphthene ND
370 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Acenaphthylene ND
740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Acetophenone ND
3700 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Aniline ND *
370 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Anthracene ND
740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Azobenzene ND
370 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Benzo[a]anthracene 380
370 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Benzo[a]pyrene 470
370 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Benzo[b]fluoranthene 680
370 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Benzo[g,h,i]perylene ND
390 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Benzo[k]fluoranthene ND
740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Bis(2-chloroethoxy)methane ND
740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Bis(2-chloroethyl)ether ND
740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Bis(2-ethylhexyl) phthalate 3100
740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Butyl benzyl phthalate ND
370 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Chrysene 530
740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Di-n-butyl phthalate ND
740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Di-n-octyl phthalate ND
370 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Dibenz(a,h)anthracene ND
740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Dibenzofuran ND
740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Diethyl phthalate ND
740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Dimethyl phthalate ND
370 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Fluoranthene 860
370 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Fluorene ND
740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Hexachlorobenzene ND
740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Hexachlorobutadiene ND
740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Hexachloroethane ND
740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Indeno[1,2,3-cd]pyrene ND
TestAmerica Westfield
Page 17 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Client Sample ResultsTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 360-34572-1Client Sample ID: PH 1 SS-1
Matrix: SolidDate Collected: 06/16/11 14:00
Percent Solids: 89.9Date Received: 06/17/11 16:55
Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Isophorone ND 740 ug/Kg ☼ 06/21/11 11:45 06/30/11 16:56 2
Analyte
370 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Naphthalene ND
740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Nitrobenzene ND
3700 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Pentachlorophenol ND
370 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Phenanthrene 430
740 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Phenol ND
370 ug/Kg 06/21/11 11:45 06/30/11 16:56 2☼Pyrene 760
Qualifier Prepared Analyzed Dil Fac % Recovery Limits
2,4,6-Tribromophenol 38 30 - 130 06/21/11 11:45 06/30/11 16:56 2
Surrogate
2-Fluorophenol 41 06/21/11 11:45 06/30/11 16:56 230 - 130
Nitrobenzene-d5 41 06/21/11 11:45 06/30/11 16:56 230 - 130
Phenol-d5 37 06/21/11 11:45 06/30/11 16:56 230 - 130
Terphenyl-d14 40 06/21/11 11:45 06/30/11 16:56 230 - 130
2-Fluorobiphenyl 41 06/21/11 11:45 06/30/11 16:56 230 - 130
Lab Sample ID: 360-34572-2Client Sample ID: PH 1 SS-2
Matrix: SolidDate Collected: 06/16/11 14:00
Percent Solids: 88.6Date Received: 06/17/11 16:55
Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
1,2,4-Trichlorobenzene ND 740 ug/Kg ☼ 06/21/11 11:45 06/30/11 17:30 2
Analyte
740 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼1,2-Dichlorobenzene ND
740 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼1,3-Dichlorobenzene ND
740 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼1,4-Dichlorobenzene ND
740 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼2,2'-oxybis[1-chloropropane] ND
740 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼2,4,5-Trichlorophenol ND
740 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼2,4,6-Trichlorophenol ND
740 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼2,4-Dichlorophenol ND
740 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼2,4-Dimethylphenol ND
740 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼2,4-Dinitrophenol ND
740 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼2,4-Dinitrotoluene ND
740 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼2,6-Dinitrotoluene ND
740 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼2-Chloronaphthalene ND
740 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼2-Chlorophenol ND
370 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼2-Methylnaphthalene ND
740 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼2-Methylphenol ND
740 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼2-Nitrophenol ND
740 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼3 & 4 Methylphenol ND
1500 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼3,3'-Dichlorobenzidine ND
740 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼4-Bromophenyl phenyl ether ND
1500 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼4-Chloroaniline ND
3700 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼4-Nitrophenol ND
370 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Acenaphthene ND
370 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Acenaphthylene ND
740 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Acetophenone ND
3700 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Aniline ND *
370 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Anthracene ND
740 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Azobenzene ND
370 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Benzo[a]anthracene 800
370 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Benzo[a]pyrene 930
370 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Benzo[b]fluoranthene 1500
TestAmerica Westfield
Page 18 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Client Sample ResultsTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 360-34572-2Client Sample ID: PH 1 SS-2
Matrix: SolidDate Collected: 06/16/11 14:00
Percent Solids: 88.6Date Received: 06/17/11 16:55
Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Benzo[g,h,i]perylene 640 370 ug/Kg ☼ 06/21/11 11:45 06/30/11 17:30 2
Analyte
390 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Benzo[k]fluoranthene 520
740 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Bis(2-chloroethoxy)methane ND
740 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Bis(2-chloroethyl)ether ND
740 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Bis(2-ethylhexyl) phthalate ND
740 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Butyl benzyl phthalate ND
370 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Chrysene 1100
740 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Di-n-butyl phthalate ND
740 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Di-n-octyl phthalate ND
370 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Dibenz(a,h)anthracene ND
740 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Dibenzofuran ND
740 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Diethyl phthalate ND
740 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Dimethyl phthalate ND
370 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Fluoranthene 2600
370 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Fluorene ND
740 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Hexachlorobenzene ND
740 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Hexachlorobutadiene ND
740 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Hexachloroethane ND
740 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Indeno[1,2,3-cd]pyrene ND
740 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Isophorone ND
370 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Naphthalene ND
740 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Nitrobenzene ND
3700 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Pentachlorophenol ND
370 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Phenanthrene 1500
740 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Phenol ND
370 ug/Kg 06/21/11 11:45 06/30/11 17:30 2☼Pyrene 1900
Qualifier Prepared Analyzed Dil Fac % Recovery Limits
2,4,6-Tribromophenol 45 30 - 130 06/21/11 11:45 06/30/11 17:30 2
Surrogate
2-Fluorophenol 48 06/21/11 11:45 06/30/11 17:30 230 - 130
Nitrobenzene-d5 45 06/21/11 11:45 06/30/11 17:30 230 - 130
Phenol-d5 44 06/21/11 11:45 06/30/11 17:30 230 - 130
Terphenyl-d14 49 06/21/11 11:45 06/30/11 17:30 230 - 130
2-Fluorobiphenyl 46 06/21/11 11:45 06/30/11 17:30 230 - 130
Lab Sample ID: 360-34572-3Client Sample ID: PH 1 SS-3
Matrix: SolidDate Collected: 06/16/11 14:00
Percent Solids: 88.1Date Received: 06/17/11 16:55
Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
1,2,4-Trichlorobenzene ND 750 ug/Kg ☼ 06/21/11 11:45 06/30/11 18:05 2
Analyte
750 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼1,2-Dichlorobenzene ND
750 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼1,3-Dichlorobenzene ND
750 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼1,4-Dichlorobenzene ND
750 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼2,2'-oxybis[1-chloropropane] ND
750 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼2,4,5-Trichlorophenol ND
750 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼2,4,6-Trichlorophenol ND
750 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼2,4-Dichlorophenol ND
750 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼2,4-Dimethylphenol ND
750 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼2,4-Dinitrophenol ND
750 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼2,4-Dinitrotoluene ND
750 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼2,6-Dinitrotoluene ND
TestAmerica Westfield
Page 19 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Client Sample ResultsTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 360-34572-3Client Sample ID: PH 1 SS-3
Matrix: SolidDate Collected: 06/16/11 14:00
Percent Solids: 88.1Date Received: 06/17/11 16:55
Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
2-Chloronaphthalene ND 750 ug/Kg ☼ 06/21/11 11:45 06/30/11 18:05 2
Analyte
750 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼2-Chlorophenol ND
380 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼2-Methylnaphthalene ND
750 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼2-Methylphenol ND
750 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼2-Nitrophenol ND
750 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼3 & 4 Methylphenol ND
1500 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼3,3'-Dichlorobenzidine ND
750 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼4-Bromophenyl phenyl ether ND
1500 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼4-Chloroaniline ND
3800 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼4-Nitrophenol ND
380 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Acenaphthene ND
380 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Acenaphthylene ND
750 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Acetophenone ND
3800 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Aniline ND *
380 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Anthracene ND
750 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Azobenzene ND
380 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Benzo[a]anthracene 500
380 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Benzo[a]pyrene 640
380 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Benzo[b]fluoranthene 940
380 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Benzo[g,h,i]perylene 410
400 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Benzo[k]fluoranthene 440
750 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Bis(2-chloroethoxy)methane ND
750 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Bis(2-chloroethyl)ether ND
750 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Bis(2-ethylhexyl) phthalate ND
750 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Butyl benzyl phthalate ND
380 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Chrysene 680
750 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Di-n-butyl phthalate ND
750 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Di-n-octyl phthalate ND
380 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Dibenz(a,h)anthracene ND
750 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Dibenzofuran ND
750 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Diethyl phthalate ND
750 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Dimethyl phthalate ND
380 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Fluoranthene 1300
380 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Fluorene ND
750 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Hexachlorobenzene ND
750 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Hexachlorobutadiene ND
750 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Hexachloroethane ND
750 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Indeno[1,2,3-cd]pyrene ND
750 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Isophorone ND
380 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Naphthalene ND
750 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Nitrobenzene ND
3800 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Pentachlorophenol ND
380 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Phenanthrene 700
750 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Phenol ND
380 ug/Kg 06/21/11 11:45 06/30/11 18:05 2☼Pyrene 1100
Qualifier Prepared Analyzed Dil Fac % Recovery Limits
2,4,6-Tribromophenol 41 30 - 130 06/21/11 11:45 06/30/11 18:05 2
Surrogate
2-Fluorophenol 44 06/21/11 11:45 06/30/11 18:05 230 - 130
Nitrobenzene-d5 41 06/21/11 11:45 06/30/11 18:05 230 - 130
Phenol-d5 42 06/21/11 11:45 06/30/11 18:05 230 - 130
TestAmerica Westfield
Page 20 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Client Sample ResultsTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 360-34572-3Client Sample ID: PH 1 SS-3
Matrix: SolidDate Collected: 06/16/11 14:00
Percent Solids: 88.1Date Received: 06/17/11 16:55
Qualifier Prepared Analyzed Dil Fac % Recovery Limits
Terphenyl-d14 46 30 - 130 06/21/11 11:45 06/30/11 18:05 2
Surrogate
2-Fluorobiphenyl 43 06/21/11 11:45 06/30/11 18:05 230 - 130
TestAmerica Westfield
Page 21 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Client Sample ResultsTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Method: 8015B - 8100M (Modified) Total Extractable Petroleum Hydrocarbons
Lab Sample ID: 360-34572-1Client Sample ID: PH 1 SS-1
Matrix: SolidDate Collected: 06/16/11 14:00
Percent Solids: 89.9Date Received: 06/17/11 16:55
Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac
Total Petroleum Hydrocarbons
(C9-C36)
120 36 mg/Kg ☼ 06/21/11 10:12 06/23/11 13:12 10
Analyte
Qualifier Prepared Analyzed Dil Fac % Recovery Limits
o-Terphenyl 73 40 - 140 06/21/11 10:12 06/23/11 13:12 10
Surrogate
Lab Sample ID: 360-34572-2Client Sample ID: PH 1 SS-2
Matrix: SolidDate Collected: 06/16/11 14:00
Percent Solids: 88.6Date Received: 06/17/11 16:55
Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac
Total Petroleum Hydrocarbons
(C9-C36)
170 36 mg/Kg ☼ 06/21/11 10:12 06/23/11 13:43 10
Analyte
Qualifier Prepared Analyzed Dil Fac % Recovery Limits
o-Terphenyl 63 40 - 140 06/21/11 10:12 06/23/11 13:43 10
Surrogate
Lab Sample ID: 360-34572-3Client Sample ID: PH 1 SS-3
Matrix: SolidDate Collected: 06/16/11 14:00
Percent Solids: 88.1Date Received: 06/17/11 16:55
Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac
Total Petroleum Hydrocarbons
(C9-C36)
130 37 mg/Kg ☼ 06/21/11 10:12 06/23/11 14:15 10
Analyte
Qualifier Prepared Analyzed Dil Fac % Recovery Limits
o-Terphenyl 99 40 - 140 06/21/11 10:12 06/23/11 14:15 10
Surrogate
TestAmerica Westfield
Page 22 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Client Sample ResultsTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Method: 8081B - Organochlorine Pesticides (GC/ECD)
Lab Sample ID: 360-34572-1Client Sample ID: PH 1 SS-1
Matrix: SolidDate Collected: 06/16/11 14:00
Percent Solids: 89.9Date Received: 06/17/11 16:55
Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
4,4'-DDD ND * 11 ug/Kg ☼ 06/21/11 09:51 06/21/11 17:19 1
Analyte
11 ug/Kg 06/21/11 09:51 06/21/11 17:19 1☼4,4'-DDE ND *
11 ug/Kg 06/21/11 09:51 06/21/11 17:19 1☼4,4'-DDT ND
11 ug/Kg 06/21/11 09:51 06/21/11 17:19 1☼Aldrin ND
11 ug/Kg 06/21/11 09:51 06/21/11 17:19 1☼alpha-BHC ND
11 ug/Kg 06/21/11 09:51 06/21/11 17:19 1☼beta-BHC ND
3.3 ug/Kg 06/21/11 09:51 06/21/11 17:19 1☼gamma-BHC (Lindane) ND
11 ug/Kg 06/21/11 09:51 06/21/11 17:19 1☼delta-BHC ND
550 ug/Kg 06/21/11 09:51 06/21/11 17:19 1☼Chlordane (technical) ND
11 ug/Kg 06/21/11 09:51 06/21/11 17:19 1☼Dieldrin ND
11 ug/Kg 06/21/11 09:51 06/21/11 17:19 1☼Endosulfan I ND
11 ug/Kg 06/21/11 09:51 06/21/11 17:19 1☼Endosulfan II ND
11 ug/Kg 06/21/11 09:51 06/21/11 17:19 1☼Endosulfan sulfate ND
11 ug/Kg 06/21/11 09:51 06/21/11 17:19 1☼Endrin ND
11 ug/Kg 06/21/11 09:51 06/21/11 17:19 1☼Endrin ketone ND
11 ug/Kg 06/21/11 09:51 06/21/11 17:19 1☼Heptachlor ND
11 ug/Kg 06/21/11 09:51 06/21/11 17:19 1☼Heptachlor epoxide ND
11 ug/Kg 06/21/11 09:51 06/21/11 17:19 1☼Hexachlorobenzene ND
11 ug/Kg 06/21/11 09:51 06/21/11 17:19 1☼Methoxychlor ND
Qualifier Prepared Analyzed Dil Fac % Recovery Limits
Tetrachloro-m-xylene 86 30 - 150 06/21/11 09:51 06/21/11 17:19 1
Surrogate
Tetrachloro-m-xylene 78 06/21/11 09:51 06/21/11 17:19 130 - 150
DCB Decachlorobiphenyl 97 06/21/11 09:51 06/21/11 17:19 130 - 150
DCB Decachlorobiphenyl 110 06/21/11 09:51 06/21/11 17:19 130 - 150
Lab Sample ID: 360-34572-2Client Sample ID: PH 1 SS-2
Matrix: SolidDate Collected: 06/16/11 14:00
Percent Solids: 88.6Date Received: 06/17/11 16:55
Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
4,4'-DDD ND * 11 ug/Kg ☼ 06/21/11 09:51 06/21/11 17:40 1
Analyte
11 ug/Kg 06/21/11 09:51 06/21/11 17:40 1☼4,4'-DDE ND *
11 ug/Kg 06/21/11 09:51 06/21/11 17:40 1☼4,4'-DDT ND
11 ug/Kg 06/21/11 09:51 06/21/11 17:40 1☼Aldrin ND
11 ug/Kg 06/21/11 09:51 06/21/11 17:40 1☼alpha-BHC ND
11 ug/Kg 06/21/11 09:51 06/21/11 17:40 1☼beta-BHC ND
3.4 ug/Kg 06/21/11 09:51 06/21/11 17:40 1☼gamma-BHC (Lindane) ND
11 ug/Kg 06/21/11 09:51 06/21/11 17:40 1☼delta-BHC ND
560 ug/Kg 06/21/11 09:51 06/21/11 17:40 1☼Chlordane (technical) ND
11 ug/Kg 06/21/11 09:51 06/21/11 17:40 1☼Dieldrin ND
11 ug/Kg 06/21/11 09:51 06/21/11 17:40 1☼Endosulfan I ND
11 ug/Kg 06/21/11 09:51 06/21/11 17:40 1☼Endosulfan II ND
11 ug/Kg 06/21/11 09:51 06/21/11 17:40 1☼Endosulfan sulfate ND
11 ug/Kg 06/21/11 09:51 06/21/11 17:40 1☼Endrin ND
11 ug/Kg 06/21/11 09:51 06/21/11 17:40 1☼Endrin ketone ND
11 ug/Kg 06/21/11 09:51 06/21/11 17:40 1☼Heptachlor ND
11 ug/Kg 06/21/11 09:51 06/21/11 17:40 1☼Heptachlor epoxide ND
11 ug/Kg 06/21/11 09:51 06/21/11 17:40 1☼Hexachlorobenzene ND
11 ug/Kg 06/21/11 09:51 06/21/11 17:40 1☼Methoxychlor ND
TestAmerica Westfield
Page 23 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Client Sample ResultsTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Method: 8081B - Organochlorine Pesticides (GC/ECD) (Continued)
Qualifier Prepared Analyzed Dil Fac % Recovery Limits
Tetrachloro-m-xylene 90 30 - 150 06/21/11 09:51 06/21/11 17:40 1
Surrogate
Tetrachloro-m-xylene 80 06/21/11 09:51 06/21/11 17:40 130 - 150
DCB Decachlorobiphenyl 115 06/21/11 09:51 06/21/11 17:40 130 - 150
DCB Decachlorobiphenyl 118 06/21/11 09:51 06/21/11 17:40 130 - 150
Lab Sample ID: 360-34572-3Client Sample ID: PH 1 SS-3
Matrix: SolidDate Collected: 06/16/11 14:00
Percent Solids: 88.1Date Received: 06/17/11 16:55
Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
4,4'-DDD ND * 11 ug/Kg ☼ 06/21/11 09:51 06/21/11 18:02 1
Analyte
11 ug/Kg 06/21/11 09:51 06/21/11 18:02 1☼4,4'-DDE ND *
11 ug/Kg 06/21/11 09:51 06/21/11 18:02 1☼4,4'-DDT ND
11 ug/Kg 06/21/11 09:51 06/21/11 18:02 1☼Aldrin ND
11 ug/Kg 06/21/11 09:51 06/21/11 18:02 1☼alpha-BHC ND
11 ug/Kg 06/21/11 09:51 06/21/11 18:02 1☼beta-BHC ND
3.4 ug/Kg 06/21/11 09:51 06/21/11 18:02 1☼gamma-BHC (Lindane) ND
11 ug/Kg 06/21/11 09:51 06/21/11 18:02 1☼delta-BHC ND
560 ug/Kg 06/21/11 09:51 06/21/11 18:02 1☼Chlordane (technical) ND
11 ug/Kg 06/21/11 09:51 06/21/11 18:02 1☼Dieldrin ND
11 ug/Kg 06/21/11 09:51 06/21/11 18:02 1☼Endosulfan I ND
11 ug/Kg 06/21/11 09:51 06/21/11 18:02 1☼Endosulfan II ND
11 ug/Kg 06/21/11 09:51 06/21/11 18:02 1☼Endosulfan sulfate ND
11 ug/Kg 06/21/11 09:51 06/21/11 18:02 1☼Endrin ND
11 ug/Kg 06/21/11 09:51 06/21/11 18:02 1☼Endrin ketone ND
11 ug/Kg 06/21/11 09:51 06/21/11 18:02 1☼Heptachlor ND
11 ug/Kg 06/21/11 09:51 06/21/11 18:02 1☼Heptachlor epoxide ND
11 ug/Kg 06/21/11 09:51 06/21/11 18:02 1☼Hexachlorobenzene ND
11 ug/Kg 06/21/11 09:51 06/21/11 18:02 1☼Methoxychlor ND
Qualifier Prepared Analyzed Dil Fac % Recovery Limits
Tetrachloro-m-xylene 86 30 - 150 06/21/11 09:51 06/21/11 18:02 1
Surrogate
Tetrachloro-m-xylene 77 06/21/11 09:51 06/21/11 18:02 130 - 150
DCB Decachlorobiphenyl 110 06/21/11 09:51 06/21/11 18:02 130 - 150
DCB Decachlorobiphenyl 110 06/21/11 09:51 06/21/11 18:02 130 - 150
TestAmerica Westfield
Page 24 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Client Sample ResultsTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Method: 8082A - Polychlorinated Biphenyls (GC/ECD)
Lab Sample ID: 360-34572-1Client Sample ID: PH 1 SS-1
Matrix: SolidDate Collected: 06/16/11 14:00
Percent Solids: 89.9Date Received: 06/17/11 16:55
Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
PCB-1016 ND 110 ug/Kg ☼ 06/21/11 09:51 06/21/11 17:12 1
Analyte
110 ug/Kg 06/21/11 09:51 06/21/11 17:12 1☼PCB-1221 ND
110 ug/Kg 06/21/11 09:51 06/21/11 17:12 1☼PCB-1232 ND
110 ug/Kg 06/21/11 09:51 06/21/11 17:12 1☼PCB-1242 ND
110 ug/Kg 06/21/11 09:51 06/21/11 17:12 1☼PCB-1248 ND
110 ug/Kg 06/21/11 09:51 06/21/11 17:12 1☼PCB-1254 ND
110 ug/Kg 06/21/11 09:51 06/21/11 17:12 1☼PCB-1260 ND
110 ug/Kg 06/21/11 09:51 06/21/11 17:12 1☼PCB-1262 ND
110 ug/Kg 06/21/11 09:51 06/21/11 17:12 1☼PCB-1268 ND
Qualifier Prepared Analyzed Dil Fac % Recovery Limits
Tetrachloro-m-xylene 82 30 - 150 06/21/11 09:51 06/21/11 17:12 1
Surrogate
Tetrachloro-m-xylene 91 06/21/11 09:51 06/21/11 17:12 130 - 150
DCB Decachlorobiphenyl 83 06/21/11 09:51 06/21/11 17:12 130 - 150
DCB Decachlorobiphenyl 89 06/21/11 09:51 06/21/11 17:12 130 - 150
Lab Sample ID: 360-34572-2Client Sample ID: PH 1 SS-2
Matrix: SolidDate Collected: 06/16/11 14:00
Percent Solids: 88.6Date Received: 06/17/11 16:55
Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
PCB-1016 ND 110 ug/Kg ☼ 06/21/11 09:51 06/21/11 17:34 1
Analyte
110 ug/Kg 06/21/11 09:51 06/21/11 17:34 1☼PCB-1221 ND
110 ug/Kg 06/21/11 09:51 06/21/11 17:34 1☼PCB-1232 ND
110 ug/Kg 06/21/11 09:51 06/21/11 17:34 1☼PCB-1242 ND
110 ug/Kg 06/21/11 09:51 06/21/11 17:34 1☼PCB-1248 ND
110 ug/Kg 06/21/11 09:51 06/21/11 17:34 1☼PCB-1254 ND
110 ug/Kg 06/21/11 09:51 06/21/11 17:34 1☼PCB-1260 ND
110 ug/Kg 06/21/11 09:51 06/21/11 17:34 1☼PCB-1262 ND
110 ug/Kg 06/21/11 09:51 06/21/11 17:34 1☼PCB-1268 ND
Qualifier Prepared Analyzed Dil Fac % Recovery Limits
Tetrachloro-m-xylene 86 30 - 150 06/21/11 09:51 06/21/11 17:34 1
Surrogate
Tetrachloro-m-xylene 95 06/21/11 09:51 06/21/11 17:34 130 - 150
DCB Decachlorobiphenyl 82 06/21/11 09:51 06/21/11 17:34 130 - 150
DCB Decachlorobiphenyl 84 06/21/11 09:51 06/21/11 17:34 130 - 150
Lab Sample ID: 360-34572-3Client Sample ID: PH 1 SS-3
Matrix: SolidDate Collected: 06/16/11 14:00
Percent Solids: 88.1Date Received: 06/17/11 16:55
Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
PCB-1016 ND 110 ug/Kg ☼ 06/21/11 09:51 06/21/11 17:56 1
Analyte
110 ug/Kg 06/21/11 09:51 06/21/11 17:56 1☼PCB-1221 ND
110 ug/Kg 06/21/11 09:51 06/21/11 17:56 1☼PCB-1232 ND
110 ug/Kg 06/21/11 09:51 06/21/11 17:56 1☼PCB-1242 ND
110 ug/Kg 06/21/11 09:51 06/21/11 17:56 1☼PCB-1248 ND
110 ug/Kg 06/21/11 09:51 06/21/11 17:56 1☼PCB-1254 ND
110 ug/Kg 06/21/11 09:51 06/21/11 17:56 1☼PCB-1260 ND
110 ug/Kg 06/21/11 09:51 06/21/11 17:56 1☼PCB-1262 ND
110 ug/Kg 06/21/11 09:51 06/21/11 17:56 1☼PCB-1268 ND
Qualifier Prepared Analyzed Dil Fac % Recovery Limits
Tetrachloro-m-xylene 78 30 - 150 06/21/11 09:51 06/21/11 17:56 1
Surrogate
TestAmerica Westfield
Page 25 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Client Sample ResultsTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Method: 8082A - Polychlorinated Biphenyls (GC/ECD) (Continued)
Lab Sample ID: 360-34572-3Client Sample ID: PH 1 SS-3
Matrix: SolidDate Collected: 06/16/11 14:00
Percent Solids: 88.1Date Received: 06/17/11 16:55
Qualifier Prepared Analyzed Dil Fac % Recovery Limits
Tetrachloro-m-xylene 93 30 - 150 06/21/11 09:51 06/21/11 17:56 1
Surrogate
DCB Decachlorobiphenyl 81 06/21/11 09:51 06/21/11 17:56 130 - 150
DCB Decachlorobiphenyl 84 06/21/11 09:51 06/21/11 17:56 130 - 150
TestAmerica Westfield
Page 26 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Client Sample ResultsTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Method: 8151A - Herbicides (GC)
Lab Sample ID: 360-34572-1Client Sample ID: PH 1 SS-1
Matrix: SolidDate Collected: 06/16/11 14:00
Percent Solids: 89.9Date Received: 06/17/11 16:55
Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Dalapon ND * 19 ug/Kg ☼ 06/24/11 10:56 06/26/11 20:50 1
Analyte
19 ug/Kg 06/24/11 10:56 06/26/11 20:50 1☼Dicamba ND
19 ug/Kg 06/24/11 10:56 06/26/11 20:50 1☼Dichlorprop ND
19 ug/Kg 06/24/11 10:56 06/26/11 20:50 1☼2,4-D ND
19 ug/Kg 06/24/11 10:56 06/26/11 20:50 1☼2,4-DB ND
19 ug/Kg 06/24/11 10:56 06/26/11 20:50 1☼Silvex (2,4,5-TP) ND
19 ug/Kg 06/24/11 10:56 06/26/11 20:50 1☼2,4,5-T ND
19 ug/Kg 06/24/11 10:56 06/26/11 20:50 1☼Dinoseb ND *
1900 ug/Kg 06/24/11 10:56 06/26/11 20:50 1☼MCPA ND
1900 ug/Kg 06/24/11 10:56 06/26/11 20:50 1☼Mecoprop ND
Qualifier Prepared Analyzed Dil Fac % Recovery Limits
2,4-Dichlorophenylacetic acid 137 101 - 150 06/24/11 10:56 06/26/11 20:50 1
Surrogate
2,4-Dichlorophenylacetic acid 173 X 06/24/11 10:56 06/26/11 20:50 1101 - 150
Lab Sample ID: 360-34572-2Client Sample ID: PH 1 SS-2
Matrix: SolidDate Collected: 06/16/11 14:00
Percent Solids: 88.6Date Received: 06/17/11 16:55
Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Dalapon ND * 19 ug/Kg ☼ 06/24/11 10:56 06/26/11 21:21 1
Analyte
19 ug/Kg 06/24/11 10:56 06/26/11 21:21 1☼Dicamba ND
19 ug/Kg 06/24/11 10:56 06/26/11 21:21 1☼Dichlorprop ND
19 ug/Kg 06/24/11 10:56 06/26/11 21:21 1☼2,4-D ND
19 ug/Kg 06/24/11 10:56 06/26/11 21:21 1☼2,4-DB ND
19 ug/Kg 06/24/11 10:56 06/26/11 21:21 1☼Silvex (2,4,5-TP) ND
19 ug/Kg 06/24/11 10:56 06/26/11 21:21 1☼2,4,5-T ND
19 ug/Kg 06/24/11 10:56 06/26/11 21:21 1☼Dinoseb ND *
1900 ug/Kg 06/24/11 10:56 06/26/11 21:21 1☼MCPA ND
1900 ug/Kg 06/24/11 10:56 06/26/11 21:21 1☼Mecoprop ND
Qualifier Prepared Analyzed Dil Fac % Recovery Limits
2,4-Dichlorophenylacetic acid 136 101 - 150 06/24/11 10:56 06/26/11 21:21 1
Surrogate
2,4-Dichlorophenylacetic acid 149 06/24/11 10:56 06/26/11 21:21 1101 - 150
Lab Sample ID: 360-34572-3Client Sample ID: PH 1 SS-3
Matrix: SolidDate Collected: 06/16/11 14:00
Percent Solids: 88.1Date Received: 06/17/11 16:55
Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Dalapon ND * 19 ug/Kg ☼ 06/24/11 10:56 06/26/11 21:51 1
Analyte
19 ug/Kg 06/24/11 10:56 06/26/11 21:51 1☼Dicamba ND
19 ug/Kg 06/24/11 10:56 06/26/11 21:51 1☼Dichlorprop ND
19 ug/Kg 06/24/11 10:56 06/26/11 21:51 1☼2,4-D ND
19 ug/Kg 06/24/11 10:56 06/26/11 21:51 1☼2,4-DB ND
19 ug/Kg 06/24/11 10:56 06/26/11 21:51 1☼Silvex (2,4,5-TP) ND
19 ug/Kg 06/24/11 10:56 06/26/11 21:51 1☼2,4,5-T ND
19 ug/Kg 06/24/11 10:56 06/26/11 21:51 1☼Dinoseb ND *
1900 ug/Kg 06/24/11 10:56 06/26/11 21:51 1☼MCPA ND
1900 ug/Kg 06/24/11 10:56 06/26/11 21:51 1☼Mecoprop ND
Qualifier Prepared Analyzed Dil Fac % Recovery Limits
2,4-Dichlorophenylacetic acid 142 101 - 150 06/24/11 10:56 06/26/11 21:51 1
Surrogate
2,4-Dichlorophenylacetic acid 146 06/24/11 10:56 06/26/11 21:51 1101 - 150
TestAmerica Westfield
Page 27 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Client Sample ResultsTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Method: 6010B - Metals (ICP)
Lab Sample ID: 360-34572-1Client Sample ID: PH 1 SS-1
Matrix: SolidDate Collected: 06/16/11 14:00
Percent Solids: 89.9Date Received: 06/17/11 16:55
Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Silver ND 1.3 mg/Kg ☼ 06/20/11 07:33 06/20/11 16:09 1
Analyte
1.3 mg/Kg 06/20/11 07:33 06/20/11 16:09 1☼Arsenic 16
0.26 mg/Kg 06/20/11 07:33 06/20/11 16:09 1☼Beryllium 0.31
0.26 mg/Kg 06/20/11 07:33 06/20/11 16:09 1☼Cadmium ND
0.65 mg/Kg 06/20/11 07:33 06/20/11 16:09 1☼Chromium 15
2.6 mg/Kg 06/20/11 07:33 06/20/11 16:09 1☼Copper 20
2.6 mg/Kg 06/20/11 07:33 06/20/11 16:09 1☼Nickel 12
0.65 mg/Kg 06/20/11 07:33 06/20/11 16:09 1☼Lead 31
0.65 mg/Kg 06/20/11 07:33 06/20/11 16:09 1☼Selenium ND
1.3 mg/Kg 06/20/11 07:33 06/20/11 16:09 1☼Thallium ND
3.3 mg/Kg 06/20/11 07:33 06/20/11 16:09 1☼Zinc 35
0.65 mg/Kg 06/20/11 07:33 06/20/11 16:09 1☼Antimony ND
Lab Sample ID: 360-34572-2Client Sample ID: PH 1 SS-2
Matrix: SolidDate Collected: 06/16/11 14:00
Percent Solids: 88.6Date Received: 06/17/11 16:55
Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Silver ND 1.3 mg/Kg ☼ 06/20/11 07:33 06/20/11 16:12 1
Analyte
1.3 mg/Kg 06/20/11 07:33 06/20/11 16:12 1☼Arsenic 16
0.26 mg/Kg 06/20/11 07:33 06/20/11 16:12 1☼Beryllium 0.36
0.26 mg/Kg 06/20/11 07:33 06/20/11 16:12 1☼Cadmium ND
0.64 mg/Kg 06/20/11 07:33 06/20/11 16:12 1☼Chromium 17
2.6 mg/Kg 06/20/11 07:33 06/20/11 16:12 1☼Copper 31
2.6 mg/Kg 06/20/11 07:33 06/20/11 16:12 1☼Nickel 16
0.64 mg/Kg 06/20/11 07:33 06/20/11 16:12 1☼Lead 27
0.64 mg/Kg 06/20/11 07:33 06/20/11 16:12 1☼Selenium ND
1.3 mg/Kg 06/20/11 07:33 06/20/11 16:12 1☼Thallium ND
3.2 mg/Kg 06/20/11 07:33 06/20/11 16:12 1☼Zinc 37
0.64 mg/Kg 06/20/11 07:33 06/20/11 16:12 1☼Antimony ND
Lab Sample ID: 360-34572-3Client Sample ID: PH 1 SS-3
Matrix: SolidDate Collected: 06/16/11 14:00
Percent Solids: 88.1Date Received: 06/17/11 16:55
Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Silver ND 1.2 mg/Kg ☼ 06/20/11 07:33 06/20/11 16:15 1
Analyte
1.2 mg/Kg 06/20/11 07:33 06/20/11 16:15 1☼Arsenic 13
0.24 mg/Kg 06/20/11 07:33 06/20/11 16:15 1☼Beryllium 0.40
0.24 mg/Kg 06/20/11 07:33 06/20/11 16:15 1☼Cadmium ND
0.59 mg/Kg 06/20/11 07:33 06/20/11 16:15 1☼Chromium 17
2.4 mg/Kg 06/20/11 07:33 06/20/11 16:15 1☼Copper 11
2.4 mg/Kg 06/20/11 07:33 06/20/11 16:15 1☼Nickel 11
0.59 mg/Kg 06/20/11 07:33 06/20/11 16:15 1☼Lead 21
0.59 mg/Kg 06/20/11 07:33 06/20/11 16:15 1☼Selenium ND
1.2 mg/Kg 06/20/11 07:33 06/20/11 16:15 1☼Thallium ND
3.0 mg/Kg 06/20/11 07:33 06/20/11 16:15 1☼Zinc 34
0.59 mg/Kg 06/20/11 07:33 06/20/11 16:15 1☼Antimony ND
TestAmerica Westfield
Page 28 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Client Sample ResultsTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Method: 7471A - Mercury (CVAA)
Lab Sample ID: 360-34572-1Client Sample ID: PH 1 SS-1
Matrix: SolidDate Collected: 06/16/11 14:00
Percent Solids: 89.9Date Received: 06/17/11 16:55
Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Mercury ND 0.077 mg/Kg ☼ 06/20/11 10:07 06/20/11 15:08 1
Analyte
Lab Sample ID: 360-34572-2Client Sample ID: PH 1 SS-2
Matrix: SolidDate Collected: 06/16/11 14:00
Percent Solids: 88.6Date Received: 06/17/11 16:55
Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Mercury 0.077 0.071 mg/Kg ☼ 06/20/11 10:07 06/20/11 15:10 1
Analyte
Lab Sample ID: 360-34572-3Client Sample ID: PH 1 SS-3
Matrix: SolidDate Collected: 06/16/11 14:00
Percent Solids: 88.1Date Received: 06/17/11 16:55
Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Mercury ND 0.078 mg/Kg ☼ 06/20/11 10:07 06/20/11 15:12 1
Analyte
TestAmerica Westfield
Page 29 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Client Sample ResultsTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
General Chemistry
Lab Sample ID: 360-34572-1Client Sample ID: PH 1 SS-1
Matrix: SolidDate Collected: 06/16/11 14:00
Date Received: 06/17/11 16:55
Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac
Percent Moisture 10 1.0 % 06/20/11 11:46 1
Analyte
1.0 % 06/20/11 11:46 1Percent Solids 90
Lab Sample ID: 360-34572-2Client Sample ID: PH 1 SS-2
Matrix: SolidDate Collected: 06/16/11 14:00
Date Received: 06/17/11 16:55
Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac
Percent Moisture 11 1.0 % 06/20/11 11:46 1
Analyte
1.0 % 06/20/11 11:46 1Percent Solids 89
Lab Sample ID: 360-34572-3Client Sample ID: PH 1 SS-3
Matrix: SolidDate Collected: 06/16/11 14:00
Date Received: 06/17/11 16:55
Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac
Percent Moisture 12 1.0 % 06/20/11 11:46 1
Analyte
1.0 % 06/20/11 11:46 1Percent Solids 88
TestAmerica Westfield
Page 30 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Client Sample ResultsTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
General Chemistry - Soluble
Lab Sample ID: 360-34572-1Client Sample ID: PH 1 SS-1
Matrix: SolidDate Collected: 06/16/11 14:00
Date Received: 06/17/11 16:55
Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac
Specific Conductance 290 3.9 umhos/cm 06/23/11 14:00 1
Analyte
Lab Sample ID: 360-34572-2Client Sample ID: PH 1 SS-2
Matrix: SolidDate Collected: 06/16/11 14:00
Date Received: 06/17/11 16:55
Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac
Specific Conductance 500 4.0 umhos/cm 06/23/11 14:00 1
Analyte
Lab Sample ID: 360-34572-3Client Sample ID: PH 1 SS-3
Matrix: SolidDate Collected: 06/16/11 14:00
Date Received: 06/17/11 16:55
Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac
Specific Conductance 320 3.9 umhos/cm 06/23/11 14:00 1
Analyte
TestAmerica Westfield
Page 31 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Definitions/GlossaryTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Qualifiers
GC/MS VOA
Qualifier Description
* RPD of the LCS and LCSD exceeds the control limits
Qualifier
GC/MS Semi VOA
Qualifier Description
* LCS or LCSD exceeds the control limits
Qualifier
GC Semi VOA
Qualifier Description
* LCS or LCSD exceeds the control limits
Qualifier
* RPD of the LCS and LCSD exceeds the control limits
E Result exceeded calibration range.
X Surrogate is outside control limits
Glossary
These commonly used abbreviations may or may not be present in this report.
☼ Listed under the "D" column to designate that the result is reported on a dry weight basis.
Abbreviation
EPA United States Environmental Protection Agency
ND Not Detected above the reporting level.
MDL Method Detection Limit
RL Reporting Limit
RE, RE1 (etc.) Indicates a Re-extraction or Reanalysis of the sample.
%R Percent Recovery
RPD Relative Percent Difference, a measure of the relative difference between two points.
TestAmerica Westfield
Page 32 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
QC Association SummaryTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
GC/MS VOA
Prep Batch: 75985
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Total/NA Solid 5035LCS 360-75985/1-A Lab Control Sample
Total/NA Solid 5035LCSD 360-75985/2-A Lab Control Sample Dup
Total/NA Solid 5035MB 360-75985/3-A Method Blank
Total/NA Solid 5035360-34572-1 PH 1 SS-1
Total/NA Solid 5035360-34572-2 PH 1 SS-2
Total/NA Solid 5035360-34572-3 PH 1 SS-3
Analysis Batch: 75986
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Total/NA Solid 8260C 75985LCS 360-75985/1-A Lab Control Sample
Total/NA Solid 8260C 75985LCSD 360-75985/2-A Lab Control Sample Dup
Total/NA Solid 8260C 75985MB 360-75985/3-A Method Blank
Total/NA Solid 8260C 75985360-34572-1 PH 1 SS-1
Total/NA Solid 8260C 75985360-34572-2 PH 1 SS-2
Total/NA Solid 8260C 75985360-34572-3 PH 1 SS-3
GC/MS Semi VOA
Prep Batch: 75634
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Total/NA Solid 3546MB 360-75634/1-A Method Blank
Total/NA Solid 3546LCS 360-75634/2-A Lab Control Sample
Total/NA Solid 3546LCSD 360-75634/3-A Lab Control Sample Dup
Total/NA Solid 3546360-34572-1 PH 1 SS-1
Total/NA Solid 3546360-34572-2 PH 1 SS-2
Total/NA Solid 3546360-34572-3 PH 1 SS-3
Analysis Batch: 75961
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Total/NA Solid 8270D 75634MB 360-75634/1-A Method Blank
Total/NA Solid 8270D 75634LCS 360-75634/2-A Lab Control Sample
Total/NA Solid 8270D 75634LCSD 360-75634/3-A Lab Control Sample Dup
Analysis Batch: 76250
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Total/NA Solid 8270D 75634360-34572-1 PH 1 SS-1
Total/NA Solid 8270D 75634360-34572-2 PH 1 SS-2
Total/NA Solid 8270D 75634360-34572-3 PH 1 SS-3
GC Semi VOA
Analysis Batch: 75520
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Total/NA Solid 8082A 75557MB 360-75557/1-A Method Blank
Total/NA Solid 8082A 75557LCS 360-75557/2-A Lab Control Sample
Total/NA Solid 8082A 75557LCSD 360-75557/3-A Lab Control Sample Dup
Prep Batch: 75555
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Total/NA Solid 3546MB 360-75555/1-A Method Blank
Total/NA Solid 3546LCS 360-75555/2-A Lab Control Sample
Total/NA Solid 3546LCSD 360-75555/3-A Lab Control Sample Dup
TestAmerica Westfield
Page 33 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
QC Association SummaryTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
GC Semi VOA (Continued)
Prep Batch: 75555 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Total/NA Solid 3546360-34572-1 PH 1 SS-1
Total/NA Solid 3546360-34572-2 PH 1 SS-2
Total/NA Solid 3546360-34572-3 PH 1 SS-3
Prep Batch: 75557
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Total/NA Solid 3546MB 360-75557/1-A Method Blank
Total/NA Solid 3546MB 360-75557/1-A Method Blank
Total/NA Solid 3546LCS 360-75557/2-A Lab Control Sample
Total/NA Solid 3546LCSD 360-75557/3-A Lab Control Sample Dup
Total/NA Solid 3546360-34572-1 PH 1 SS-1
Total/NA Solid 3546360-34572-1 PH 1 SS-1
Total/NA Solid 3546360-34572-2 PH 1 SS-2
Total/NA Solid 3546360-34572-2 PH 1 SS-2
Total/NA Solid 3546360-34572-3 PH 1 SS-3
Total/NA Solid 3546360-34572-3 PH 1 SS-3
Total/NA Solid 3546LCS 360-75557/9-A Lab Control Sample
Total/NA Solid 3546LCSD 360-75557/10-A Lab Control Sample Dup
Analysis Batch: 75607
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Total/NA Solid 8015B 75555MB 360-75555/1-A Method Blank
Total/NA Solid 8015B 75555LCS 360-75555/2-A Lab Control Sample
Total/NA Solid 8015B 75555LCSD 360-75555/3-A Lab Control Sample Dup
Analysis Batch: 75643
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Total/NA Solid 8082A 75557360-34572-1 PH 1 SS-1
Total/NA Solid 8082A 75557360-34572-2 PH 1 SS-2
Total/NA Solid 8082A 75557360-34572-3 PH 1 SS-3
Analysis Batch: 75661
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Total/NA Solid 8081B 75557MB 360-75557/1-A Method Blank
Total/NA Solid 8081B 75557LCS 360-75557/9-A Lab Control Sample
Total/NA Solid 8081B 75557LCSD 360-75557/10-A Lab Control Sample Dup
Total/NA Solid 8081B 75557360-34572-1 PH 1 SS-1
Total/NA Solid 8081B 75557360-34572-2 PH 1 SS-2
Total/NA Solid 8081B 75557360-34572-3 PH 1 SS-3
Analysis Batch: 75828
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Total/NA Solid 8015B 75555360-34572-1 PH 1 SS-1
Total/NA Solid 8015B 75555360-34572-2 PH 1 SS-2
Total/NA Solid 8015B 75555360-34572-3 PH 1 SS-3
Prep Batch: 77865
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Total/NA Solid 8151AMB 460-77865/1-A Method Blank
Total/NA Solid 8151ALCS 460-77865/2-A Lab Control Sample
Total/NA Solid 8151ALCSD 460-77865/3-A Lab Control Sample Dup
Total/NA Solid 8151A360-34572-1 PH 1 SS-1
TestAmerica Westfield
Page 34 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
QC Association SummaryTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
GC Semi VOA (Continued)
Prep Batch: 77865 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Total/NA Solid 8151A360-34572-2 PH 1 SS-2
Total/NA Solid 8151A360-34572-3 PH 1 SS-3
Analysis Batch: 78058
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Total/NA Solid 8151A 77865360-34572-1 PH 1 SS-1
Total/NA Solid 8151A 77865360-34572-2 PH 1 SS-2
Total/NA Solid 8151A 77865360-34572-3 PH 1 SS-3
Total/NA Solid 8151A 77865LCS 460-77865/2-A Lab Control Sample
Total/NA Solid 8151A 77865LCSD 460-77865/3-A Lab Control Sample Dup
Total/NA Solid 8151A 77865MB 460-77865/1-A Method Blank
Metals
Prep Batch: 75498
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Total/NA Solid 3050BMB 360-75498/1-A Method Blank
Total/NA Solid 3050BLCSSRM 360-75498/2-A Lab Control Sample
Total/NA Solid 3050BLCDSRM 360-75498/3-A LCDSRMLab Control Sample Dup
Total/NA Solid 3050B360-34572-1 PH 1 SS-1
Total/NA Solid 3050B360-34572-2 PH 1 SS-2
Total/NA Solid 3050B360-34572-3 PH 1 SS-3
Prep Batch: 75533
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Total/NA Solid 7471AMB 360-75533/1-A Method Blank
Total/NA Solid 7471ALCSSRM 360-75533/2-A Lab Control Sample
Total/NA Solid 7471ALCDSRM 360-75533/3-A LCDSRMLab Control Sample Dup
Total/NA Solid 7471A360-34572-1 PH 1 SS-1
Total/NA Solid 7471A360-34572-2 PH 1 SS-2
Total/NA Solid 7471A360-34572-3 PH 1 SS-3
Analysis Batch: 75577
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Total/NA Solid 7471A 75533MB 360-75533/1-A Method Blank
Total/NA Solid 7471A 75533LCSSRM 360-75533/2-A Lab Control Sample
Total/NA Solid 7471A 75533LCDSRM 360-75533/3-A LCDSRMLab Control Sample Dup
Total/NA Solid 7471A 75533360-34572-1 PH 1 SS-1
Total/NA Solid 7471A 75533360-34572-2 PH 1 SS-2
Total/NA Solid 7471A 75533360-34572-3 PH 1 SS-3
Analysis Batch: 75614
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Total/NA Solid 6010B 75498MB 360-75498/1-A Method Blank
Total/NA Solid 6010B 75498LCSSRM 360-75498/2-A Lab Control Sample
Total/NA Solid 6010B 75498LCDSRM 360-75498/3-A LCDSRMLab Control Sample Dup
Total/NA Solid 6010B 75498360-34572-1 PH 1 SS-1
Total/NA Solid 6010B 75498360-34572-2 PH 1 SS-2
Total/NA Solid 6010B 75498360-34572-3 PH 1 SS-3
TestAmerica Westfield
Page 35 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
QC Association SummaryTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
General Chemistry
Analysis Batch: 75547
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Total/NA Solid Moisture360-34572-1 PH 1 SS-1
Total/NA Solid Moisture360-34572-2 PH 1 SS-2
Total/NA Solid Moisture360-34572-3 PH 1 SS-3
Leach Batch: 75814
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soluble Solid DI LeachMB 360-75814/1-A Method Blank
Soluble Solid DI LeachLCS 360-75814/2-A Lab Control Sample
Soluble Solid DI Leach360-34572-1 PH 1 SS-1
Soluble Solid DI Leach360-34572-2 PH 1 SS-2
Soluble Solid DI Leach360-34572-3 PH 1 SS-3
Analysis Batch: 75858
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soluble Solid SM 2510BMB 360-75814/1-A Method Blank
Soluble Solid SM 2510BLCS 360-75814/2-A Lab Control Sample
Soluble Solid SM 2510B360-34572-1 PH 1 SS-1
Soluble Solid SM 2510B360-34572-2 PH 1 SS-2
Soluble Solid SM 2510B360-34572-3 PH 1 SS-3
TestAmerica Westfield
Page 36 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Surrogate SummaryTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Method: 8260C - Volatile Organic Compounds (GC/MS)Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (70-130) (70-130) (70-130)
BFB DBFM TOL
108 108 103360-34572-1
Percent Surrogate Recovery (Acceptance Limits)
PH 1 SS-1
105 107 102360-34572-2 PH 1 SS-2
108 107 105360-34572-3 PH 1 SS-3
114 105 109LCS 360-75985/1-A Lab Control Sample
112 105 107LCSD 360-75985/2-A Lab Control Sample Dup
118 109 106MB 360-75985/3-A Method Blank
Surrogate Legend
BFB = 4-Bromofluorobenzene
DBFM = Dibromofluoromethane
TOL = Toluene-d8 (Surr)
Method: 8270D - Semivolatile Organic Compounds (GC/MS)Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (30-130) (30-130) (30-130) (30-130) (30-130) (30-130)
TBP 2FP NBZ PHL TPH FBP
38 41 41 37 40 41360-34572-1
Percent Surrogate Recovery (Acceptance Limits)
PH 1 SS-1
45 48 45 4944 46360-34572-2 PH 1 SS-2
41 44 41 4642 43360-34572-3 PH 1 SS-3
63 61 59 6562 62LCS 360-75634/2-A Lab Control Sample
63 62 61 6562 63LCSD 360-75634/3-A Lab Control Sample Dup
61 65 63 6564 61MB 360-75634/1-A Method Blank
Surrogate Legend
TBP = 2,4,6-Tribromophenol
2FP = 2-Fluorophenol
NBZ = Nitrobenzene-d5
PHL = Phenol-d5
TPH = Terphenyl-d14
FBP = 2-Fluorobiphenyl
Method: 8015B - 8100M (Modified) Total Extractable Petroleum HydrocarbonsPrep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (40-140)
OTPH1
73360-34572-1
Percent Surrogate Recovery (Acceptance Limits)
PH 1 SS-1
63360-34572-2 PH 1 SS-2
99360-34572-3 PH 1 SS-3
80LCS 360-75555/2-A Lab Control Sample
86LCSD 360-75555/3-A Lab Control Sample Dup
83MB 360-75555/1-A Method Blank
Surrogate Legend
OTPH = o-Terphenyl
TestAmerica Westfield
Page 37 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Surrogate SummaryTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Method: 8081B - Organochlorine Pesticides (GC/ECD)Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (30-150) (30-150) (30-150) (30-150)
TCX1 TCX2 DCB1 DCB2
86 78 97 110360-34572-1
Percent Surrogate Recovery (Acceptance Limits)
PH 1 SS-1
90 80 115 118360-34572-2 PH 1 SS-2
86 77 110 110360-34572-3 PH 1 SS-3
87 88 86 102LCS 360-75557/9-A Lab Control Sample
95 94 89 110LCSD 360-75557/10-A Lab Control Sample Dup
87 90 83 97MB 360-75557/1-A Method Blank
Surrogate Legend
TCX = Tetrachloro-m-xylene
DCB = DCB Decachlorobiphenyl
Method: 8082A - Polychlorinated Biphenyls (GC/ECD)Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (30-150) (30-150) (30-150) (30-150)
TCX1 TCX2 DCB1 DCB2
82 91 83 89360-34572-1
Percent Surrogate Recovery (Acceptance Limits)
PH 1 SS-1
86 95 82 84360-34572-2 PH 1 SS-2
78 93 81 84360-34572-3 PH 1 SS-3
93 82 101 94LCS 360-75557/2-A Lab Control Sample
98 86 101 98LCSD 360-75557/3-A Lab Control Sample Dup
91 85 99 93MB 360-75557/1-A Method Blank
Surrogate Legend
TCX = Tetrachloro-m-xylene
DCB = DCB Decachlorobiphenyl
Method: 8151A - Herbicides (GC)Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (101-150) (101-150)
DCPA1 DCPA2
137 173 X360-34572-1
Percent Surrogate Recovery (Acceptance Limits)
PH 1 SS-1
136 149360-34572-2 PH 1 SS-2
142 146360-34572-3 PH 1 SS-3
118 135LCS 460-77865/2-A Lab Control Sample
109 118LCSD 460-77865/3-A Lab Control Sample Dup
142 121MB 460-77865/1-A Method Blank
Surrogate Legend
DCPA = 2,4-Dichlorophenylacetic acid
TestAmerica Westfield
Page 38 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
QC Sample ResultsTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Method: 8260C - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 360-75985/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 75986 Prep Batch: 75985
Result Qualifier Unit D Prepared Analyzed Dil FacRL MDL
1,1,1,2-Tetrachloroethane ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1
MB MB
Analyte
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 11,1,1-Trichloroethane
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 11,1,2,2-Tetrachloroethane
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 11,1,2-Trichloroethane
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 11,1-Dichloroethane
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 11,1-Dichloroethene
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 11,1-Dichloropropene
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 11,2,3-Trichlorobenzene
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 11,2,3-Trichloropropane
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 11,2,4-Trichlorobenzene
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 11,2,4-Trimethylbenzene
ND 25 ug/Kg 06/26/11 10:49 06/27/11 04:14 11,2-Dibromo-3-Chloropropane
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 11,2-Dichlorobenzene
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 11,2-Dichloroethane
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 11,2-Dichloropropane
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 11,3,5-Trimethylbenzene
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 11,3-Dichlorobenzene
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 11,3-Dichloropropane
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 11,4-Dichlorobenzene
ND 250 ug/Kg 06/26/11 10:49 06/27/11 04:14 11,4-Dioxane
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 12,2-Dichloropropane
ND 25 ug/Kg 06/26/11 10:49 06/27/11 04:14 12-Butanone (MEK)
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 12-Chlorotoluene
ND 25 ug/Kg 06/26/11 10:49 06/27/11 04:14 12-Hexanone
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 14-Chlorotoluene
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 14-Isopropyltoluene
ND 25 ug/Kg 06/26/11 10:49 06/27/11 04:14 14-Methyl-2-pentanone (MIBK)
ND 250 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Acetone
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Benzene
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Bromobenzene
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Bromoform
ND 5.0 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Bromomethane
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Carbon disulfide
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Carbon tetrachloride
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Chlorobenzene
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Chlorobromomethane
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Chlorodibromomethane
ND 5.0 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Chloroethane
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Chloroform
ND 5.0 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Chloromethane
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1cis-1,2-Dichloroethene
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1cis-1,3-Dichloropropene
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Dibromomethane
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Dichlorobromomethane
ND 5.0 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Dichlorodifluoromethane
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Ethyl ether
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Ethylbenzene
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Ethylene Dibromide
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Hexachlorobutadiene
TestAmerica Westfield
Page 39 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
QC Sample ResultsTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Method: 8260C - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 360-75985/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 75986 Prep Batch: 75985
Result Qualifier Unit D Prepared Analyzed Dil FacRL MDL
Isopropyl ether ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1
MB MB
Analyte
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Isopropylbenzene
ND 5.0 ug/Kg 06/26/11 10:49 06/27/11 04:14 1m-Xylene & p-Xylene
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Methyl tert-butyl ether
ND 10 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Methylene Chloride
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1n-Butylbenzene
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1N-Propylbenzene
ND 25 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Naphthalene
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1o-Xylene
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1sec-Butylbenzene
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Styrene
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Tert-amyl methyl ether
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Tert-butyl ethyl ether
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1tert-Butylbenzene
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Tetrachloroethene
ND 25 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Tetrahydrofuran
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Toluene
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1trans-1,2-Dichloroethene
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1trans-1,3-Dichloropropene
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Trichloroethene
ND 5.0 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Trichlorofluoromethane
ND 2.5 ug/Kg 06/26/11 10:49 06/27/11 04:14 1Vinyl chloride
% Recovery Qualifier Prepared Analyzed Dil FacLimits
4-Bromofluorobenzene 118 70 - 130 06/27/11 04:14 1
MB MB
Surrogate
06/26/11 10:49
109 06/26/11 10:49 06/27/11 04:14 1Dibromofluoromethane 70 - 130
106 06/26/11 10:49 06/27/11 04:14 1Toluene-d8 (Surr) 70 - 130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 360-75985/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 75986 Prep Batch: 75985
Spike
Added Result Qualifier Unit % Rec
% Rec.
Limits
1,1,1,2-Tetrachloroethane 100 101 ug/Kg 101 70 - 130
DAnalyte
LCS LCS
1,1,1-Trichloroethane 100 104 ug/Kg 104 70 - 130
1,1,2,2-Tetrachloroethane 100 74.0 ug/Kg 74 70 - 130
1,1,2-Trichloroethane 100 96.0 ug/Kg 96 70 - 130
1,1-Dichloroethane 100 104 ug/Kg 104 70 - 130
1,1-Dichloroethene 100 97.0 ug/Kg 97 70 - 130
1,1-Dichloropropene 100 93.5 ug/Kg 94 70 - 130
1,2,3-Trichlorobenzene 100 106 ug/Kg 106 70 - 130
1,2,3-Trichloropropane 100 101 ug/Kg 101 70 - 130
1,2,4-Trichlorobenzene 100 102 ug/Kg 102 70 - 130
1,2,4-Trimethylbenzene 100 102 ug/Kg 102 70 - 130
1,2-Dibromo-3-Chloropropane 100 109 ug/Kg 109 70 - 130
1,2-Dichlorobenzene 100 94.5 ug/Kg 95 70 - 130
1,2-Dichloroethane 100 97.0 ug/Kg 97 70 - 130
1,2-Dichloropropane 100 87.5 ug/Kg 88 70 - 130
1,3,5-Trimethylbenzene 100 96.0 ug/Kg 96 70 - 130
TestAmerica Westfield
Page 40 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
QC Sample ResultsTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Method: 8260C - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 360-75985/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 75986 Prep Batch: 75985
Spike
Added Result Qualifier Unit % Rec
% Rec.
Limits
1,3-Dichlorobenzene 100 98.0 ug/Kg 98 70 - 130
DAnalyte
LCS LCS
1,3-Dichloropropane 100 99.0 ug/Kg 99 70 - 130
1,4-Dichlorobenzene 100 89.0 ug/Kg 89 70 - 130
1,4-Dioxane 1000 931 ug/Kg 93 70 - 130
2,2-Dichloropropane 100 89.0 ug/Kg 89 70 - 130
2-Butanone (MEK) 1000 805 ug/Kg 81 70 - 130
2-Chlorotoluene 100 94.0 ug/Kg 94 70 - 130
2-Hexanone 1000 766 ug/Kg 77 70 - 130
4-Chlorotoluene 100 97.0 ug/Kg 97 70 - 130
4-Isopropyltoluene 100 103 ug/Kg 103 70 - 130
4-Methyl-2-pentanone (MIBK) 1000 738 ug/Kg 74 70 - 130
Acetone 1000 899 ug/Kg 90 70 - 130
Benzene 100 94.0 ug/Kg 94 70 - 130
Bromobenzene 100 85.5 ug/Kg 86 70 - 130
Bromoform 100 94.0 ug/Kg 94 70 - 130
Bromomethane 100 84.5 ug/Kg 85 70 - 130
Carbon disulfide 100 119 ug/Kg 119 70 - 130
Carbon tetrachloride 100 94.5 ug/Kg 95 70 - 130
Chlorobenzene 100 89.5 ug/Kg 90 70 - 130
Chlorobromomethane 100 102 ug/Kg 102 70 - 130
Chlorodibromomethane 100 104 ug/Kg 104 70 - 130
Chloroethane 100 87.0 ug/Kg 87 70 - 130
Chloroform 100 99.5 ug/Kg 100 70 - 130
Chloromethane 100 102 ug/Kg 102 70 - 130
cis-1,2-Dichloroethene 100 100 ug/Kg 100 70 - 130
cis-1,3-Dichloropropene 100 93.0 ug/Kg 93 70 - 130
Dibromomethane 100 102 ug/Kg 102 70 - 130
Dichlorobromomethane 100 96.5 ug/Kg 97 70 - 130
Dichlorodifluoromethane 100 92.0 ug/Kg 92 70 - 130
Ethyl ether 100 104 ug/Kg 104 70 - 130
Ethylbenzene 100 87.0 ug/Kg 87 70 - 130
Ethylene Dibromide 100 108 ug/Kg 108 70 - 130
Hexachlorobutadiene 100 99.5 ug/Kg 100 70 - 130
Isopropyl ether 100 95.0 ug/Kg 95 70 - 130
Isopropylbenzene 100 98.0 ug/Kg 98 70 - 130
m-Xylene & p-Xylene 200 174 ug/Kg 87 70 - 130
Methyl tert-butyl ether 100 101 ug/Kg 101 70 - 130
Methylene Chloride 100 92.0 ug/Kg 92 70 - 130
n-Butylbenzene 100 87.5 ug/Kg 88 70 - 130
N-Propylbenzene 100 88.5 ug/Kg 89 70 - 130
Naphthalene 100 99.0 ug/Kg 99 70 - 130
o-Xylene 100 96.5 ug/Kg 97 70 - 130
sec-Butylbenzene 100 97.5 ug/Kg 98 70 - 130
Styrene 100 102 ug/Kg 102 70 - 130
Tert-amyl methyl ether 100 98.0 ug/Kg 98 70 - 130
Tert-butyl ethyl ether 100 101 ug/Kg 101 70 - 130
tert-Butylbenzene 100 102 ug/Kg 102 70 - 130
Tetrachloroethene 100 96.5 ug/Kg 97 70 - 130
Tetrahydrofuran 1000 879 ug/Kg 88 70 - 130
Toluene 100 99.0 ug/Kg 99 70 - 130
TestAmerica Westfield
Page 41 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
QC Sample ResultsTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Method: 8260C - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 360-75985/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 75986 Prep Batch: 75985
Spike
Added Result Qualifier Unit % Rec
% Rec.
Limits
trans-1,2-Dichloroethene 100 98.5 ug/Kg 99 70 - 130
DAnalyte
LCS LCS
trans-1,3-Dichloropropene 100 87.0 ug/Kg 87 70 - 130
Trichloroethene 100 98.5 ug/Kg 99 70 - 130
Trichlorofluoromethane 100 80.5 ug/Kg 81 70 - 130
Vinyl chloride 100 94.5 ug/Kg 95 70 - 130
Qualifier % Recovery Limits
4-Bromofluorobenzene 70 - 130
Surrogate
114
LCS LCS
105Dibromofluoromethane 70 - 130
109Toluene-d8 (Surr) 70 - 130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 360-75985/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 75986 Prep Batch: 75985
Spike
Added Result Qualifier Unit % Rec
% Rec.
Limits RPD Limit
1,1,1,2-Tetrachloroethane 100 103 ug/Kg 103 70 - 130 2 20
DAnalyte
RPDLCSD LCSD
1,1,1-Trichloroethane 100 102 ug/Kg 102 70 - 130 2 20
1,1,2,2-Tetrachloroethane 100 74.5 ug/Kg 75 70 - 130 1 20
1,1,2-Trichloroethane 100 95.5 ug/Kg 96 70 - 130 1 20
1,1-Dichloroethane 100 105 ug/Kg 105 70 - 130 1 20
1,1-Dichloroethene 100 98.0 ug/Kg 98 70 - 130 1 20
1,1-Dichloropropene 100 94.0 ug/Kg 94 70 - 130 1 20
1,2,3-Trichlorobenzene 100 110 ug/Kg 110 70 - 130 4 20
1,2,3-Trichloropropane 100 102 ug/Kg 102 70 - 130 1 20
1,2,4-Trichlorobenzene 100 108 ug/Kg 108 70 - 130 6 20
1,2,4-Trimethylbenzene 100 104 ug/Kg 104 70 - 130 2 20
1,2-Dibromo-3-Chloropropane 100 110 ug/Kg 110 70 - 130 1 20
1,2-Dichlorobenzene 100 96.0 ug/Kg 96 70 - 130 2 20
1,2-Dichloroethane 100 96.5 ug/Kg 97 70 - 130 1 20
1,2-Dichloropropane 100 87.0 ug/Kg 87 70 - 130 1 20
1,3,5-Trimethylbenzene 100 98.0 ug/Kg 98 70 - 130 2 20
1,3-Dichlorobenzene 100 101 ug/Kg 101 70 - 130 3 20
1,3-Dichloropropane 100 98.0 ug/Kg 98 70 - 130 1 20
1,4-Dichlorobenzene 100 90.5 ug/Kg 91 70 - 130 2 20
1,4-Dioxane 1000 1170 * ug/Kg 117 70 - 130 22 20
2,2-Dichloropropane 100 79.0 ug/Kg 79 70 - 130 12 20
2-Butanone (MEK) 1000 842 ug/Kg 84 70 - 130 4 20
2-Chlorotoluene 100 95.0 ug/Kg 95 70 - 130 1 20
2-Hexanone 1000 787 ug/Kg 79 70 - 130 3 20
4-Chlorotoluene 100 100 ug/Kg 100 70 - 130 3 20
4-Isopropyltoluene 100 104 ug/Kg 104 70 - 130 1 20
4-Methyl-2-pentanone (MIBK) 1000 754 ug/Kg 75 70 - 130 2 20
Acetone 1000 945 ug/Kg 94 70 - 130 5 20
Benzene 100 95.0 ug/Kg 95 70 - 130 1 20
Bromobenzene 100 85.5 ug/Kg 86 70 - 130 0 20
Bromoform 100 95.5 ug/Kg 96 70 - 130 2 20
Bromomethane 100 86.5 ug/Kg 87 70 - 130 2 20
Carbon disulfide 100 121 ug/Kg 121 70 - 130 2 20
TestAmerica Westfield
Page 42 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
QC Sample ResultsTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Method: 8260C - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 360-75985/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 75986 Prep Batch: 75985
Spike
Added Result Qualifier Unit % Rec
% Rec.
Limits RPD Limit
Carbon tetrachloride 100 95.0 ug/Kg 95 70 - 130 1 20
DAnalyte
RPDLCSD LCSD
Chlorobenzene 100 92.0 ug/Kg 92 70 - 130 3 20
Chlorobromomethane 100 102 ug/Kg 102 70 - 130 0 20
Chlorodibromomethane 100 103 ug/Kg 103 70 - 130 1 20
Chloroethane 100 87.5 ug/Kg 88 70 - 130 1 20
Chloroform 100 101 ug/Kg 101 70 - 130 1 20
Chloromethane 100 104 ug/Kg 104 70 - 130 2 20
cis-1,2-Dichloroethene 100 101 ug/Kg 101 70 - 130 1 20
cis-1,3-Dichloropropene 100 93.5 ug/Kg 94 70 - 130 1 20
Dibromomethane 100 101 ug/Kg 101 70 - 130 1 20
Dichlorobromomethane 100 96.0 ug/Kg 96 70 - 130 1 20
Dichlorodifluoromethane 100 91.0 ug/Kg 91 70 - 130 1 20
Ethyl ether 100 106 ug/Kg 106 70 - 130 2 20
Ethylbenzene 100 89.0 ug/Kg 89 70 - 130 2 20
Ethylene Dibromide 100 108 ug/Kg 108 70 - 130 0 20
Hexachlorobutadiene 100 103 ug/Kg 103 70 - 130 3 20
Isopropyl ether 100 95.5 ug/Kg 96 70 - 130 1 20
Isopropylbenzene 100 100 ug/Kg 100 70 - 130 2 20
m-Xylene & p-Xylene 200 179 ug/Kg 89 70 - 130 3 20
Methyl tert-butyl ether 100 100 ug/Kg 100 70 - 130 1 20
Methylene Chloride 100 92.5 ug/Kg 93 70 - 130 1 20
n-Butylbenzene 100 89.5 ug/Kg 90 70 - 130 2 20
N-Propylbenzene 100 90.5 ug/Kg 91 70 - 130 2 20
Naphthalene 100 102 ug/Kg 102 70 - 130 2 20
o-Xylene 100 101 ug/Kg 101 70 - 130 4 20
sec-Butylbenzene 100 97.0 ug/Kg 97 70 - 130 1 20
Styrene 100 104 ug/Kg 104 70 - 130 2 20
Tert-amyl methyl ether 100 97.5 ug/Kg 98 70 - 130 1 20
Tert-butyl ethyl ether 100 100 ug/Kg 100 70 - 130 0 20
tert-Butylbenzene 100 101 ug/Kg 101 70 - 130 0 20
Tetrachloroethene 100 97.5 ug/Kg 98 70 - 130 1 20
Tetrahydrofuran 1000 889 ug/Kg 89 70 - 130 1 20
Toluene 100 100 ug/Kg 100 70 - 130 1 20
trans-1,2-Dichloroethene 100 100 ug/Kg 100 70 - 130 2 20
trans-1,3-Dichloropropene 100 87.0 ug/Kg 87 70 - 130 0 20
Trichloroethene 100 99.5 ug/Kg 100 70 - 130 1 20
Trichlorofluoromethane 100 80.0 ug/Kg 80 70 - 130 1 20
Vinyl chloride 100 95.5 ug/Kg 96 70 - 130 1 20
Qualifier % Recovery Limits
4-Bromofluorobenzene 70 - 130
Surrogate
112
LCSD LCSD
105Dibromofluoromethane 70 - 130
107Toluene-d8 (Surr) 70 - 130
TestAmerica Westfield
Page 43 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
QC Sample ResultsTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 360-75634/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 75961 Prep Batch: 75634
Result Qualifier Unit D Prepared Analyzed Dil FacRL MDL
1,2,4-Trichlorobenzene ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 1
MB MB
Analyte
ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 11,2-Dichlorobenzene
ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 11,3-Dichlorobenzene
ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 11,4-Dichlorobenzene
ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 12,2'-oxybis[1-chloropropane]
ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 12,4,5-Trichlorophenol
ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 12,4,6-Trichlorophenol
ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 12,4-Dichlorophenol
ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 12,4-Dimethylphenol
ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 12,4-Dinitrophenol
ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 12,4-Dinitrotoluene
ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 12,6-Dinitrotoluene
ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 12-Chloronaphthalene
ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 12-Chlorophenol
ND 170 ug/Kg 06/21/11 11:45 06/24/11 21:43 12-Methylnaphthalene
ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 12-Methylphenol
ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 12-Nitrophenol
ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 13 & 4 Methylphenol
ND 670 ug/Kg 06/21/11 11:45 06/24/11 21:43 13,3'-Dichlorobenzidine
ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 14-Bromophenyl phenyl ether
ND 670 ug/Kg 06/21/11 11:45 06/24/11 21:43 14-Chloroaniline
ND 1700 ug/Kg 06/21/11 11:45 06/24/11 21:43 14-Nitrophenol
ND 170 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Acenaphthene
ND 170 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Acenaphthylene
ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Acetophenone
ND 1700 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Aniline
ND 170 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Anthracene
ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Azobenzene
ND 170 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Benzo[a]anthracene
ND 170 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Benzo[a]pyrene
ND 170 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Benzo[b]fluoranthene
ND 170 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Benzo[g,h,i]perylene
ND 180 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Benzo[k]fluoranthene
ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Bis(2-chloroethoxy)methane
ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Bis(2-chloroethyl)ether
ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Bis(2-ethylhexyl) phthalate
ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Butyl benzyl phthalate
ND 170 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Chrysene
ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Di-n-butyl phthalate
ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Di-n-octyl phthalate
ND 170 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Dibenz(a,h)anthracene
ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Dibenzofuran
ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Diethyl phthalate
ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Dimethyl phthalate
ND 170 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Fluoranthene
ND 170 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Fluorene
ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Hexachlorobenzene
ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Hexachlorobutadiene
ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Hexachloroethane
TestAmerica Westfield
Page 44 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
QC Sample ResultsTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 360-75634/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 75961 Prep Batch: 75634
Result Qualifier Unit D Prepared Analyzed Dil FacRL MDL
Indeno[1,2,3-cd]pyrene ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 1
MB MB
Analyte
ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Isophorone
ND 170 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Naphthalene
ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Nitrobenzene
ND 1700 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Pentachlorophenol
ND 170 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Phenanthrene
ND 330 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Phenol
ND 170 ug/Kg 06/21/11 11:45 06/24/11 21:43 1Pyrene
% Recovery Qualifier Prepared Analyzed Dil FacLimits
2,4,6-Tribromophenol 61 30 - 130 06/24/11 21:43 1
MB MB
Surrogate
06/21/11 11:45
65 06/21/11 11:45 06/24/11 21:43 12-Fluorophenol 30 - 130
63 06/21/11 11:45 06/24/11 21:43 1Nitrobenzene-d5 30 - 130
64 06/21/11 11:45 06/24/11 21:43 1Phenol-d5 30 - 130
65 06/21/11 11:45 06/24/11 21:43 1Terphenyl-d14 30 - 130
61 06/21/11 11:45 06/24/11 21:43 12-Fluorobiphenyl 30 - 130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 360-75634/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 75961 Prep Batch: 75634
Spike
Added Result Qualifier Unit % Rec
% Rec.
Limits
1,2,4-Trichlorobenzene 1330 747 ug/Kg 56 40 - 140
DAnalyte
LCS LCS
1,2-Dichlorobenzene 1330 810 ug/Kg 61 40 - 140
1,3-Dichlorobenzene 1330 787 ug/Kg 59 40 - 140
1,4-Dichlorobenzene 1330 783 ug/Kg 59 40 - 140
2,2'-oxybis[1-chloropropane] 1330 897 ug/Kg 67 40 - 140
2,4,5-Trichlorophenol 1330 953 ug/Kg 72 30 - 130
2,4,6-Trichlorophenol 1330 930 ug/Kg 70 30 - 130
2,4-Dichlorophenol 1330 940 ug/Kg 71 30 - 130
2,4-Dimethylphenol 1330 923 ug/Kg 69 30 - 130
2,4-Dinitrophenol 1330 610 ug/Kg 46 30 - 130
2,4-Dinitrotoluene 1330 1060 ug/Kg 79 40 - 140
2,6-Dinitrotoluene 1330 973 ug/Kg 73 40 - 140
2-Chloronaphthalene 1330 900 ug/Kg 68 40 - 140
2-Chlorophenol 1330 890 ug/Kg 67 30 - 130
2-Methylnaphthalene 1330 907 ug/Kg 68 40 - 140
2-Methylphenol 1330 927 ug/Kg 70 30 - 130
2-Nitrophenol 1330 827 ug/Kg 62 30 - 130
3 & 4 Methylphenol 1330 970 ug/Kg 73 30 - 130
3,3'-Dichlorobenzidine 1330 1040 ug/Kg 78 40 - 140
4-Bromophenyl phenyl ether 1330 947 ug/Kg 71 40 - 140
4-Chloroaniline 1330 767 ug/Kg 58 40 - 140
4-Nitrophenol 1330 ND ug/Kg 72 30 - 130
Acenaphthene 1330 1110 ug/Kg 83 40 - 140
Acenaphthylene 1330 947 ug/Kg 71 40 - 140
Acetophenone 1330 867 ug/Kg 65 40 - 140
Aniline 1330 ND * ug/Kg 34 40 - 140
Anthracene 1330 1090 ug/Kg 82 40 - 140
TestAmerica Westfield
Page 45 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
QC Sample ResultsTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 360-75634/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 75961 Prep Batch: 75634
Spike
Added Result Qualifier Unit % Rec
% Rec.
Limits
Azobenzene 1330 830 ug/Kg 62 40 - 140
DAnalyte
LCS LCS
Benzo[a]anthracene 1330 1180 ug/Kg 88 40 - 140
Benzo[a]pyrene 1330 1210 ug/Kg 91 40 - 140
Benzo[b]fluoranthene 1330 1100 ug/Kg 82 40 - 140
Benzo[g,h,i]perylene 1330 1180 ug/Kg 89 40 - 140
Benzo[k]fluoranthene 1330 1230 ug/Kg 92 40 - 140
Bis(2-chloroethoxy)methane 1330 887 ug/Kg 67 40 - 140
Bis(2-chloroethyl)ether 1330 827 ug/Kg 62 40 - 140
Bis(2-ethylhexyl) phthalate 1330 1040 ug/Kg 78 40 - 140
Butyl benzyl phthalate 1330 1010 ug/Kg 76 40 - 140
Chrysene 1330 1200 ug/Kg 90 40 - 140
Di-n-butyl phthalate 1330 1060 ug/Kg 79 40 - 140
Di-n-octyl phthalate 1330 1060 ug/Kg 79 40 - 140
Dibenz(a,h)anthracene 1330 1220 ug/Kg 92 40 - 140
Dibenzofuran 1330 950 ug/Kg 71 40 - 140
Diethyl phthalate 1330 990 ug/Kg 74 40 - 140
Dimethyl phthalate 1330 977 ug/Kg 73 40 - 140
Fluoranthene 1330 1030 ug/Kg 77 40 - 140
Fluorene 1330 1130 ug/Kg 85 40 - 140
Hexachlorobenzene 1330 930 ug/Kg 70 40 - 140
Hexachlorobutadiene 1330 760 ug/Kg 57 40 - 140
Hexachloroethane 1330 803 ug/Kg 60 40 - 140
Indeno[1,2,3-cd]pyrene 1330 1210 ug/Kg 91 40 - 140
Isophorone 1330 723 ug/Kg 54 40 - 140
Naphthalene 1330 860 ug/Kg 65 40 - 140
Nitrobenzene 1330 833 ug/Kg 63 40 - 140
Pentachlorophenol 1330 ND ug/Kg 68 30 - 130
Phenanthrene 1330 1100 ug/Kg 83 40 - 140
Phenol 1330 947 ug/Kg 71 30 - 130
Pyrene 1330 1150 ug/Kg 87 40 - 140
Qualifier % Recovery Limits
2,4,6-Tribromophenol 30 - 130
Surrogate
63
LCS LCS
612-Fluorophenol 30 - 130
59Nitrobenzene-d5 30 - 130
62Phenol-d5 30 - 130
65Terphenyl-d14 30 - 130
622-Fluorobiphenyl 30 - 130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 360-75634/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 75961 Prep Batch: 75634
Spike
Added Result Qualifier Unit % Rec
% Rec.
Limits RPD Limit
1,2,4-Trichlorobenzene 1330 800 ug/Kg 60 40 - 140 7 30
DAnalyte
RPDLCSD LCSD
1,2-Dichlorobenzene 1330 837 ug/Kg 63 40 - 140 3 30
1,3-Dichlorobenzene 1330 813 ug/Kg 61 40 - 140 3 30
1,4-Dichlorobenzene 1330 830 ug/Kg 62 40 - 140 6 30
2,2'-oxybis[1-chloropropane] 1330 927 ug/Kg 70 40 - 140 3 30
TestAmerica Westfield
Page 46 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
QC Sample ResultsTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 360-75634/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 75961 Prep Batch: 75634
Spike
Added Result Qualifier Unit % Rec
% Rec.
Limits RPD Limit
2,4,5-Trichlorophenol 1330 973 ug/Kg 73 30 - 130 2 30
DAnalyte
RPDLCSD LCSD
2,4,6-Trichlorophenol 1330 953 ug/Kg 72 30 - 130 2 30
2,4-Dichlorophenol 1330 983 ug/Kg 74 30 - 130 5 30
2,4-Dimethylphenol 1330 943 ug/Kg 71 30 - 130 2 30
2,4-Dinitrophenol 1330 617 ug/Kg 46 30 - 130 1 30
2,4-Dinitrotoluene 1330 1070 ug/Kg 80 40 - 140 1 30
2,6-Dinitrotoluene 1330 957 ug/Kg 72 40 - 140 2 30
2-Chloronaphthalene 1330 920 ug/Kg 69 40 - 140 2 30
2-Chlorophenol 1330 923 ug/Kg 69 30 - 130 4 30
2-Methylnaphthalene 1330 970 ug/Kg 73 40 - 140 7 30
2-Methylphenol 1330 973 ug/Kg 73 30 - 130 5 30
2-Nitrophenol 1330 870 ug/Kg 65 30 - 130 5 30
3 & 4 Methylphenol 1330 980 ug/Kg 74 30 - 130 1 30
3,3'-Dichlorobenzidine 1330 1100 ug/Kg 83 40 - 140 6 30
4-Bromophenyl phenyl ether 1330 990 ug/Kg 74 40 - 140 4 30
4-Chloroaniline 1330 787 ug/Kg 59 40 - 140 3 30
4-Nitrophenol 1330 ND ug/Kg 69 30 - 130 4 30
Acenaphthene 1330 1160 ug/Kg 87 40 - 140 5 30
Acenaphthylene 1330 973 ug/Kg 73 40 - 140 3 30
Acetophenone 1330 910 ug/Kg 68 40 - 140 5 30
Aniline 1330 ND * ug/Kg 34 40 - 140 1 30
Anthracene 1330 1160 ug/Kg 87 40 - 140 6 30
Azobenzene 1330 883 ug/Kg 66 40 - 140 6 30
Benzo[a]anthracene 1330 1210 ug/Kg 91 40 - 140 3 30
Benzo[a]pyrene 1330 1220 ug/Kg 92 40 - 140 1 30
Benzo[b]fluoranthene 1330 1110 ug/Kg 84 40 - 140 2 30
Benzo[g,h,i]perylene 1330 1190 ug/Kg 89 40 - 140 1 30
Benzo[k]fluoranthene 1330 1250 ug/Kg 94 40 - 140 2 30
Bis(2-chloroethoxy)methane 1330 930 ug/Kg 70 40 - 140 5 30
Bis(2-chloroethyl)ether 1330 877 ug/Kg 66 40 - 140 6 30
Bis(2-ethylhexyl) phthalate 1330 1050 ug/Kg 79 40 - 140 1 30
Butyl benzyl phthalate 1330 1020 ug/Kg 77 40 - 140 1 30
Chrysene 1330 1210 ug/Kg 91 40 - 140 1 30
Di-n-butyl phthalate 1330 1070 ug/Kg 80 40 - 140 1 30
Di-n-octyl phthalate 1330 1080 ug/Kg 81 40 - 140 2 30
Dibenz(a,h)anthracene 1330 1230 ug/Kg 92 40 - 140 1 30
Dibenzofuran 1330 967 ug/Kg 73 40 - 140 2 30
Diethyl phthalate 1330 1030 ug/Kg 77 40 - 140 4 30
Dimethyl phthalate 1330 977 ug/Kg 73 40 - 140 0 30
Fluoranthene 1330 1060 ug/Kg 80 40 - 140 3 30
Fluorene 1330 1160 ug/Kg 87 40 - 140 2 30
Hexachlorobenzene 1330 977 ug/Kg 73 40 - 140 5 30
Hexachlorobutadiene 1330 790 ug/Kg 59 40 - 140 4 30
Hexachloroethane 1330 820 ug/Kg 62 40 - 140 2 30
Indeno[1,2,3-cd]pyrene 1330 1200 ug/Kg 90 40 - 140 0 30
Isophorone 1330 767 ug/Kg 58 40 - 140 6 30
Naphthalene 1330 933 ug/Kg 70 40 - 140 8 30
Nitrobenzene 1330 897 ug/Kg 67 40 - 140 7 30
Pentachlorophenol 1330 ND ug/Kg 69 30 - 130 2 30
Phenanthrene 1330 1130 ug/Kg 85 40 - 140 3 30
TestAmerica Westfield
Page 47 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
QC Sample ResultsTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 360-75634/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 75961 Prep Batch: 75634
Spike
Added Result Qualifier Unit % Rec
% Rec.
Limits RPD Limit
Phenol 1330 973 ug/Kg 73 30 - 130 3 30
DAnalyte
RPDLCSD LCSD
Pyrene 1330 1160 ug/Kg 87 40 - 140 1 30
Qualifier % Recovery Limits
2,4,6-Tribromophenol 30 - 130
Surrogate
63
LCSD LCSD
622-Fluorophenol 30 - 130
61Nitrobenzene-d5 30 - 130
62Phenol-d5 30 - 130
65Terphenyl-d14 30 - 130
632-Fluorobiphenyl 30 - 130
Method: 8015B - 8100M (Modified) Total Extractable Petroleum Hydrocarbons
Client Sample ID: Method BlankLab Sample ID: MB 360-75555/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 75607 Prep Batch: 75555
Result Qualifier Unit D Prepared Analyzed Dil FacRL RL
Total Petroleum Hydrocarbons
(C9-C36)
ND 3.3 mg/Kg 06/20/11 12:36 06/21/11 09:47 1
MB MB
Analyte
% Recovery Qualifier Prepared Analyzed Dil FacLimits
o-Terphenyl 83 40 - 140 06/21/11 09:47 1
MB MB
Surrogate
06/20/11 12:36
Client Sample ID: Lab Control SampleLab Sample ID: LCS 360-75555/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 75607 Prep Batch: 75555
Spike
Added Result Qualifier Unit % Rec
% Rec.
Limits
Total Petroleum Hydrocarbons
(C9-C36)
167 117 mg/Kg 70 60 - 140
DAnalyte
LCS LCS
Qualifier % Recovery Limits
o-Terphenyl 40 - 140
Surrogate
80
LCS LCS
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 360-75555/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 75607 Prep Batch: 75555
Spike
Added Result Qualifier Unit % Rec
% Rec.
Limits RPD Limit
Total Petroleum Hydrocarbons
(C9-C36)
167 125 mg/Kg 75 60 - 140 7 50
DAnalyte
RPDLCSD LCSD
Qualifier % Recovery Limits
o-Terphenyl 40 - 140
Surrogate
86
LCSD LCSD
TestAmerica Westfield
Page 48 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
QC Sample ResultsTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Method: 8081B - Organochlorine Pesticides (GC/ECD)
Client Sample ID: Method BlankLab Sample ID: MB 360-75557/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 75661 Prep Batch: 75557
Result Qualifier Unit D Prepared Analyzed Dil FacRL MDL
4,4'-DDD ND 10 ug/Kg 06/20/11 12:38 06/21/11 16:14 1
MB MB
Analyte
ND 10 ug/Kg 06/20/11 12:38 06/21/11 16:14 14,4'-DDE
ND 10 ug/Kg 06/20/11 12:38 06/21/11 16:14 14,4'-DDT
ND 10 ug/Kg 06/20/11 12:38 06/21/11 16:14 1Aldrin
ND 10 ug/Kg 06/20/11 12:38 06/21/11 16:14 1alpha-BHC
ND 10 ug/Kg 06/20/11 12:38 06/21/11 16:14 1beta-BHC
ND 3.0 ug/Kg 06/20/11 12:38 06/21/11 16:14 1gamma-BHC (Lindane)
ND 10 ug/Kg 06/20/11 12:38 06/21/11 16:14 1delta-BHC
ND 500 ug/Kg 06/20/11 12:38 06/21/11 16:14 1Chlordane (technical)
ND 10 ug/Kg 06/20/11 12:38 06/21/11 16:14 1Dieldrin
ND 10 ug/Kg 06/20/11 12:38 06/21/11 16:14 1Endosulfan I
ND 10 ug/Kg 06/20/11 12:38 06/21/11 16:14 1Endosulfan II
ND 10 ug/Kg 06/20/11 12:38 06/21/11 16:14 1Endosulfan sulfate
ND 10 ug/Kg 06/20/11 12:38 06/21/11 16:14 1Endrin
ND 10 ug/Kg 06/20/11 12:38 06/21/11 16:14 1Endrin ketone
ND 10 ug/Kg 06/20/11 12:38 06/21/11 16:14 1Heptachlor
ND 10 ug/Kg 06/20/11 12:38 06/21/11 16:14 1Heptachlor epoxide
ND 10 ug/Kg 06/20/11 12:38 06/21/11 16:14 1Hexachlorobenzene
ND 10 ug/Kg 06/20/11 12:38 06/21/11 16:14 1Methoxychlor
% Recovery Qualifier Prepared Analyzed Dil FacLimits
Tetrachloro-m-xylene 87 30 - 150 06/21/11 16:14 1
MB MB
Surrogate
06/20/11 12:38
90 06/20/11 12:38 06/21/11 16:14 1Tetrachloro-m-xylene 30 - 150
83 06/20/11 12:38 06/21/11 16:14 1DCB Decachlorobiphenyl 30 - 150
97 06/20/11 12:38 06/21/11 16:14 1DCB Decachlorobiphenyl 30 - 150
Client Sample ID: Lab Control SampleLab Sample ID: LCS 360-75557/9-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 75661 Prep Batch: 75557
Spike
Added Result Qualifier Unit % Rec
% Rec.
Limits
4,4'-DDD 60.0 87.0 * ug/Kg 145 40 - 140
DAnalyte
LCS LCS
4,4'-DDE 60.0 83.1 ug/Kg 139 40 - 140
4,4'-DDT 60.0 78.5 ug/Kg 131 40 - 140
Aldrin 60.0 74.6 ug/Kg 124 40 - 140
alpha-BHC 60.0 66.9 ug/Kg 112 40 - 140
beta-BHC 60.0 73.2 ug/Kg 122 40 - 140
gamma-BHC (Lindane) 60.0 67.2 ug/Kg 112 40 - 140
delta-BHC 60.0 58.9 ug/Kg 98 40 - 140
Dieldrin 60.0 76.3 ug/Kg 127 40 - 140
Endosulfan I 60.0 75.9 ug/Kg 127 40 - 140
Endosulfan II 60.0 76.9 ug/Kg 128 40 - 140
Endosulfan sulfate 60.0 76.0 ug/Kg 127 40 - 140
Endrin 60.0 93.1 * ug/Kg 155 40 - 140
Endrin ketone 60.0 74.7 ug/Kg 125 40 - 140
Heptachlor 60.0 78.7 ug/Kg 131 40 - 140
Heptachlor epoxide 60.0 69.5 ug/Kg 116 40 - 140
Hexachlorobenzene 60.0 61.0 ug/Kg 102 40 - 140
Methoxychlor 60.0 76.5 ug/Kg 128 40 - 140
TestAmerica Westfield
Page 49 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
QC Sample ResultsTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Method: 8081B - Organochlorine Pesticides (GC/ECD) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 360-75557/9-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 75661 Prep Batch: 75557
Qualifier % Recovery Limits
Tetrachloro-m-xylene 30 - 150
Surrogate
87
LCS LCS
88Tetrachloro-m-xylene 30 - 150
86DCB Decachlorobiphenyl 30 - 150
102DCB Decachlorobiphenyl 30 - 150
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 360-75557/10-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 75661 Prep Batch: 75557
Spike
Added Result Qualifier Unit % Rec
% Rec.
Limits RPD Limit
4,4'-DDD 60.0 96.2 * ug/Kg 160 40 - 140 10 30
DAnalyte
RPDLCSD LCSD
4,4'-DDE 60.0 90.4 * ug/Kg 151 40 - 140 8 30
4,4'-DDT 60.0 82.3 ug/Kg 137 40 - 140 5 30
Aldrin 60.0 80.9 ug/Kg 135 40 - 140 8 30
alpha-BHC 60.0 74.4 ug/Kg 124 40 - 140 11 30
beta-BHC 60.0 79.1 ug/Kg 132 40 - 140 8 30
gamma-BHC (Lindane) 60.0 71.3 ug/Kg 119 40 - 140 6 30
delta-BHC 60.0 62.4 ug/Kg 104 40 - 140 6 30
Dieldrin 60.0 82.7 ug/Kg 138 40 - 140 8 30
Endosulfan I 60.0 81.6 ug/Kg 136 40 - 140 7 30
Endosulfan II 60.0 81.8 ug/Kg 136 40 - 140 6 30
Endosulfan sulfate 60.0 81.6 ug/Kg 136 40 - 140 7 30
Endrin 60.0 105 E * ug/Kg 175 40 - 140 12 30
Endrin ketone 60.0 80.6 ug/Kg 134 40 - 140 8 30
Heptachlor 60.0 85.7 * ug/Kg 143 40 - 140 9 30
Heptachlor epoxide 60.0 74.9 ug/Kg 125 40 - 140 7 30
Hexachlorobenzene 60.0 65.9 ug/Kg 110 40 - 140 8 30
Methoxychlor 60.0 80.8 ug/Kg 135 40 - 140 5 30
Qualifier % Recovery Limits
Tetrachloro-m-xylene 30 - 150
Surrogate
95
LCSD LCSD
94Tetrachloro-m-xylene 30 - 150
89DCB Decachlorobiphenyl 30 - 150
110DCB Decachlorobiphenyl 30 - 150
Method: 8082A - Polychlorinated Biphenyls (GC/ECD)
Client Sample ID: Method BlankLab Sample ID: MB 360-75557/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 75520 Prep Batch: 75557
Result Qualifier Unit D Prepared Analyzed Dil FacRL MDL
PCB-1016 ND 100 ug/Kg 06/20/11 12:38 06/20/11 17:00 1
MB MB
Analyte
ND 100 ug/Kg 06/20/11 12:38 06/20/11 17:00 1PCB-1221
ND 100 ug/Kg 06/20/11 12:38 06/20/11 17:00 1PCB-1232
ND 100 ug/Kg 06/20/11 12:38 06/20/11 17:00 1PCB-1242
ND 100 ug/Kg 06/20/11 12:38 06/20/11 17:00 1PCB-1248
ND 100 ug/Kg 06/20/11 12:38 06/20/11 17:00 1PCB-1254
ND 100 ug/Kg 06/20/11 12:38 06/20/11 17:00 1PCB-1260
TestAmerica Westfield
Page 50 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
QC Sample ResultsTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Method: 8082A - Polychlorinated Biphenyls (GC/ECD) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 360-75557/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 75520 Prep Batch: 75557
Result Qualifier Unit D Prepared Analyzed Dil FacRL MDL
PCB-1262 ND 100 ug/Kg 06/20/11 12:38 06/20/11 17:00 1
MB MB
Analyte
ND 100 ug/Kg 06/20/11 12:38 06/20/11 17:00 1PCB-1268
% Recovery Qualifier Prepared Analyzed Dil FacLimits
Tetrachloro-m-xylene 91 30 - 150 06/20/11 17:00 1
MB MB
Surrogate
06/20/11 12:38
85 06/20/11 12:38 06/20/11 17:00 1Tetrachloro-m-xylene 30 - 150
99 06/20/11 12:38 06/20/11 17:00 1DCB Decachlorobiphenyl 30 - 150
93 06/20/11 12:38 06/20/11 17:00 1DCB Decachlorobiphenyl 30 - 150
Client Sample ID: Lab Control SampleLab Sample ID: LCS 360-75557/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 75520 Prep Batch: 75557
Spike
Added Result Qualifier Unit % Rec
% Rec.
Limits
PCB-1016 500 507 ug/Kg 101 40 - 140
DAnalyte
LCS LCS
PCB-1260 500 547 ug/Kg 109 40 - 140
Qualifier % Recovery Limits
Tetrachloro-m-xylene 30 - 150
Surrogate
93
LCS LCS
82Tetrachloro-m-xylene 30 - 150
101DCB Decachlorobiphenyl 30 - 150
94DCB Decachlorobiphenyl 30 - 150
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 360-75557/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 75520 Prep Batch: 75557
Spike
Added Result Qualifier Unit % Rec
% Rec.
Limits RPD Limit
PCB-1016 500 550 ug/Kg 110 40 - 140 8 30
DAnalyte
RPDLCSD LCSD
PCB-1260 500 560 ug/Kg 112 40 - 140 2 30
Qualifier % Recovery Limits
Tetrachloro-m-xylene 30 - 150
Surrogate
98
LCSD LCSD
86Tetrachloro-m-xylene 30 - 150
101DCB Decachlorobiphenyl 30 - 150
98DCB Decachlorobiphenyl 30 - 150
Method: 8151A - Herbicides (GC)
Client Sample ID: Method BlankLab Sample ID: MB 460-77865/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 78058 Prep Batch: 77865
Result Qualifier Unit D Prepared Analyzed Dil FacRL MDL
Dalapon ND 17 ug/Kg 06/24/11 10:56 06/26/11 23:23 1
MB MB
Analyte
ND 17 ug/Kg 06/24/11 10:56 06/26/11 23:23 1Dicamba
ND 17 ug/Kg 06/24/11 10:56 06/26/11 23:23 1Dichlorprop
ND 17 ug/Kg 06/24/11 10:56 06/26/11 23:23 12,4-D
ND 17 ug/Kg 06/24/11 10:56 06/26/11 23:23 12,4-DB
TestAmerica Westfield
Page 51 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
QC Sample ResultsTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Method: 8151A - Herbicides (GC) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 460-77865/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 78058 Prep Batch: 77865
Result Qualifier Unit D Prepared Analyzed Dil FacRL MDL
Silvex (2,4,5-TP) ND 17 ug/Kg 06/24/11 10:56 06/26/11 23:23 1
MB MB
Analyte
ND 17 ug/Kg 06/24/11 10:56 06/26/11 23:23 12,4,5-T
ND 17 ug/Kg 06/24/11 10:56 06/26/11 23:23 1Dinoseb
ND 1700 ug/Kg 06/24/11 10:56 06/26/11 23:23 1MCPA
ND 1700 ug/Kg 06/24/11 10:56 06/26/11 23:23 1Mecoprop
% Recovery Qualifier Prepared Analyzed Dil FacLimits
2,4-Dichlorophenylacetic acid 142 101 - 150 06/26/11 23:23 1
MB MB
Surrogate
06/24/11 10:56
121 06/24/11 10:56 06/26/11 23:23 12,4-Dichlorophenylacetic acid 101 - 150
Client Sample ID: Lab Control SampleLab Sample ID: LCS 460-77865/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 78058 Prep Batch: 77865
Spike
Added Result Qualifier Unit % Rec
% Rec.
Limits
Dalapon 167 220 ug/Kg 132 63 - 150
DAnalyte
LCS LCS
Dalapon 167 205 ug/Kg 123 63 - 150
Dicamba 167 196 ug/Kg 118 51 - 145
Dicamba 167 203 ug/Kg 122 51 - 145
Dichlorprop 167 133 ug/Kg 80 37 - 150
Dichlorprop 167 176 ug/Kg 106 37 - 150
2,4-D 167 171 ug/Kg 103 52 - 150
2,4-D 167 213 ug/Kg 128 52 - 150
2,4-DB 167 246 ug/Kg 148 10 - 150
2,4-DB 167 177 ug/Kg 106 10 - 150
Silvex (2,4,5-TP) 167 199 ug/Kg 120 73 - 148
Silvex (2,4,5-TP) 167 204 ug/Kg 122 73 - 148
2,4,5-T 167 178 ug/Kg 107 69 - 150
2,4,5-T 167 175 ug/Kg 105 69 - 150
Dinoseb 167 139 ug/Kg 83 42 - 140
Dinoseb 167 150 ug/Kg 90 42 - 140
MCPA 16700 16200 ug/Kg 97 70 - 130
MCPA 16700 18600 ug/Kg 112 70 - 130
Mecoprop 16700 19800 ug/Kg 119 70 - 130
Mecoprop 16700 21400 ug/Kg 128 70 - 130
Qualifier % Recovery Limits
2,4-Dichlorophenylacetic acid 101 - 150
Surrogate
118
LCS LCS
1352,4-Dichlorophenylacetic acid 101 - 150
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 460-77865/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 78058 Prep Batch: 77865
Spike
Added Result Qualifier Unit % Rec
% Rec.
Limits RPD Limit
Dalapon 167 153 * ug/Kg 92 63 - 150 36 30
DAnalyte
RPDLCSD LCSD
Dalapon 167 150 * ug/Kg 90 63 - 150 31 30
Dicamba 167 169 ug/Kg 101 51 - 145 18 30
Dicamba 167 167 ug/Kg 100 51 - 145 16 30
TestAmerica Westfield
Page 52 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
QC Sample ResultsTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Method: 8151A - Herbicides (GC) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 460-77865/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 78058 Prep Batch: 77865
Spike
Added Result Qualifier Unit % Rec
% Rec.
Limits RPD Limit
Dichlorprop 167 114 ug/Kg 68 37 - 150 15 30
DAnalyte
RPDLCSD LCSD
Dichlorprop 167 152 ug/Kg 91 37 - 150 14 30
2,4-D 167 249 ug/Kg 150 52 - 150 16 30
2,4-D 167 199 ug/Kg 119 52 - 150 15 30
2,4-DB 167 243 ug/Kg 146 10 - 150 1 30
2,4-DB 167 205 ug/Kg 123 10 - 150 15 30
Silvex (2,4,5-TP) 167 172 ug/Kg 103 73 - 148 15 30
Silvex (2,4,5-TP) 167 174 ug/Kg 104 73 - 148 16 30
2,4,5-T 167 162 ug/Kg 97 69 - 150 9 30
2,4,5-T 167 157 ug/Kg 94 69 - 150 11 30
Dinoseb 167 55.5 * ug/Kg 33 42 - 140 86 30
Dinoseb 167 61.0 * ug/Kg 37 42 - 140 84 30
MCPA 16700 14500 ug/Kg 87 70 - 130 11 30
MCPA 16700 18100 ug/Kg 109 70 - 130 3 30
Mecoprop 16700 18300 ug/Kg 110 70 - 130 16 30
Mecoprop 16700 17900 ug/Kg 107 70 - 130 10 30
Qualifier % Recovery Limits
2,4-Dichlorophenylacetic acid 101 - 150
Surrogate
109
LCSD LCSD
1182,4-Dichlorophenylacetic acid 101 - 150
Method: 6010B - Metals (ICP)
Client Sample ID: Method BlankLab Sample ID: MB 360-75498/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 75614 Prep Batch: 75498
Result Qualifier Unit D Prepared Analyzed Dil FacRL MDL
Silver ND 1.0 mg/Kg 06/20/11 07:33 06/20/11 15:04 1
MB MB
Analyte
ND 1.0 mg/Kg 06/20/11 07:33 06/20/11 15:04 1Arsenic
ND 0.20 mg/Kg 06/20/11 07:33 06/20/11 15:04 1Beryllium
ND 0.20 mg/Kg 06/20/11 07:33 06/20/11 15:04 1Cadmium
ND 0.50 mg/Kg 06/20/11 07:33 06/20/11 15:04 1Chromium
ND 2.0 mg/Kg 06/20/11 07:33 06/20/11 15:04 1Copper
ND 2.0 mg/Kg 06/20/11 07:33 06/20/11 15:04 1Nickel
ND 0.50 mg/Kg 06/20/11 07:33 06/20/11 15:04 1Lead
ND 0.50 mg/Kg 06/20/11 07:33 06/20/11 15:04 1Selenium
ND 1.0 mg/Kg 06/20/11 07:33 06/20/11 15:04 1Thallium
ND 2.5 mg/Kg 06/20/11 07:33 06/20/11 15:04 1Zinc
ND 0.50 mg/Kg 06/20/11 07:33 06/20/11 15:04 1Antimony
Client Sample ID: Lab Control Sample DupLab Sample ID: LCDSRM 360-75498/3-A
LCDSRM
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 75614 Prep Batch: 75498
Spike
Added Result Qualifier Unit % Rec
% Rec.
Limits RPD Limit
Silver 67.5 54.8 mg/Kg 81 56.9 - 113 3 30
DAnalyte
RPDLCDSRM LCDSRM
Arsenic 90.0 77.4 mg/Kg 86 61 - 117 2 30
TestAmerica Westfield
Page 53 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
QC Sample ResultsTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Method: 6010B - Metals (ICP) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCDSRM 360-75498/3-A
LCDSRM
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 75614 Prep Batch: 75498
Spike
Added Result Qualifier Unit % Rec
% Rec.
Limits RPD Limit
Beryllium 83.0 67.8 mg/Kg 82 65.8 - 112 4 30
DAnalyte
RPDLCDSRM LCDSRM
Cadmium 106 85.3 mg/Kg 80 65.6 - 113 2 30
Chromium 272 240 mg/Kg 88 68.0 - 124 5 30
Copper 157 138 mg/Kg 88 70.7 - 117 5 30
Nickel 179 150 mg/Kg 84 67.6 - 117 3 30
Lead 267 203 mg/Kg 76 64.8 - 110 4 30
Selenium 154 115 mg/Kg 75 53.1 - 110 1 30
Thallium 286 223 mg/Kg 78 61.9 - 116 1 30
Zinc 655 517 mg/Kg 79 67.5 - 116 3 30
Antimony 152 30.2 mg/Kg 20 10.0 - 110 7 30
Client Sample ID: Lab Control SampleLab Sample ID: LCSSRM 360-75498/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 75614 Prep Batch: 75498
Spike
Added Result Qualifier Unit % Rec
% Rec.
Limits
Silver 67.5 56.6 mg/Kg 84 56.9 - 113
DAnalyte
LCSSRM LCSSRM
Arsenic 90.0 78.6 mg/Kg 87 61 - 117
Beryllium 83.0 70.5 mg/Kg 85 65.8 - 112
Cadmium 106 86.9 mg/Kg 82 65.6 - 113
Chromium 272 251 mg/Kg 92 68.0 - 124
Copper 157 146 mg/Kg 93 70.7 - 117
Nickel 179 155 mg/Kg 86 67.6 - 117
Lead 267 210 mg/Kg 79 64.8 - 110
Selenium 154 116 mg/Kg 76 53.1 - 110
Thallium 286 226 mg/Kg 79 61.9 - 116
Zinc 655 532 mg/Kg 81 67.5 - 116
Antimony 152 32.4 mg/Kg 21 10.0 - 110
Method: 7471A - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 360-75533/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 75577 Prep Batch: 75533
Result Qualifier Unit D Prepared Analyzed Dil FacRL MDL
Mercury ND 0.10 mg/Kg 06/20/11 10:07 06/20/11 14:42 1
MB MB
Analyte
Client Sample ID: Lab Control Sample DupLab Sample ID: LCDSRM 360-75533/3-A
LCDSRM
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 75577 Prep Batch: 75533
Spike
Added Result Qualifier Unit % Rec
% Rec.
Limits RPD Limit
Mercury 9.36 8.41 mg/Kg 90 46.5 - 135 2 30
DAnalyte
RPDLCDSRM LCDSRM
TestAmerica Westfield
Page 54 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
QC Sample ResultsTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Method: 7471A - Mercury (CVAA) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCSSRM 360-75533/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 75577 Prep Batch: 75533
Spike
Added Result Qualifier Unit % Rec
% Rec.
Limits
Mercury 10.3 8.60 mg/Kg 83 46.5 - 135
DAnalyte
LCSSRM LCSSRM
Method: SM 2510B - Conductivity, Specific Conductance
Client Sample ID: Method BlankLab Sample ID: MB 360-75814/1-A
Matrix: Solid Prep Type: Soluble
Analysis Batch: 75858
Result Qualifier Unit D Prepared Analyzed Dil FacRL RL
Specific Conductance ND 4.0 umhos/cm 06/23/11 14:00 1
MB MB
Analyte
Client Sample ID: Lab Control SampleLab Sample ID: LCS 360-75814/2-A
Matrix: Solid Prep Type: Soluble
Analysis Batch: 75858
Spike
Added Result Qualifier Unit % Rec
% Rec.
Limits
Specific Conductance 5640 5600 umhos/cm 99 85 - 115
DAnalyte
LCS LCS
TestAmerica Westfield
Page 55 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Pesticide PEM Data
Page 56 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Page 57 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Page 58 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Lab ChronicleClient: ARCADIS U.S., Inc TestAmerica Job ID: 360-34572-1
Project/Site: 28 Ball Hill Road
Client Sample ID: PH 1 SS-1 Lab Sample ID: 360-34572-1Matrix: SolidDate Collected: 06/16/11 14:00
Percent Solids: 89.9Date Received: 06/17/11 16:55
Batch
Type
Batch
Method Run
Dilution
Factor
Batch
Number
Prepared
Or Analyzed Analyst LabPrep Type
Total/NA Prep 5035 06/26/11 10:49 SS75985 TAL WFD
Total/NA Analysis 8260C 1 75986 06/27/11 07:50 SS TAL WFD
Total/NA Prep 3546 75634 06/21/11 11:45 OG TAL WFD
Total/NA Analysis 8270D 2 76250 06/30/11 16:56 CMR TAL WFD
Total/NA Prep 3546 75557 06/21/11 09:51 OG TAL WFD
Total/NA Analysis 8082A 1 75643 06/21/11 17:12 BRB TAL WFD
Total/NA Analysis 8081B 1 75661 06/21/11 17:19 BRB TAL WFD
Total/NA Prep 3546 75555 06/21/11 10:12 OG TAL WFD
Total/NA Analysis 8015B 10 75828 06/23/11 13:12 BRB TAL WFD
Total/NA Prep 8151A 77865 06/24/11 10:56 ME TAL EDI
Total/NA Analysis 8151A 1 78058 06/26/11 20:50 SK TAL EDI
Total/NA Prep 7471A 75533 06/20/11 10:07 EMN TAL WFD
Total/NA Analysis 7471A 1 75577 06/20/11 15:08 EMN TAL WFD
Total/NA Prep 3050B 75498 06/20/11 07:33 EMN TAL WFD
Total/NA Analysis 6010B 1 75614 06/20/11 16:09 TJS TAL WFD
Total/NA Analysis Moisture 1 75547 06/20/11 11:46 EMN TAL WFD
Soluble Leach DI Leach 75814 06/23/11 09:50 AMS TAL WFD
Soluble Analysis SM 2510B 1 75858 06/23/11 14:00 AMS TAL WFD
Client Sample ID: PH 1 SS-2 Lab Sample ID: 360-34572-2Matrix: SolidDate Collected: 06/16/11 14:00
Percent Solids: 88.6Date Received: 06/17/11 16:55
Batch
Type
Batch
Method Run
Dilution
Factor
Batch
Number
Prepared
Or Analyzed Analyst LabPrep Type
Total/NA Prep 5035 06/26/11 10:49 SS75985 TAL WFD
Total/NA Analysis 8260C 1 75986 06/27/11 08:14 SS TAL WFD
Total/NA Prep 3546 75634 06/21/11 11:45 OG TAL WFD
Total/NA Analysis 8270D 2 76250 06/30/11 17:30 CMR TAL WFD
Total/NA Prep 3546 75557 06/21/11 09:51 OG TAL WFD
Total/NA Analysis 8082A 1 75643 06/21/11 17:34 BRB TAL WFD
Total/NA Analysis 8081B 1 75661 06/21/11 17:40 BRB TAL WFD
Total/NA Prep 3546 75555 06/21/11 10:12 OG TAL WFD
Total/NA Analysis 8015B 10 75828 06/23/11 13:43 BRB TAL WFD
Total/NA Prep 8151A 77865 06/24/11 10:56 ME TAL EDI
Total/NA Analysis 8151A 1 78058 06/26/11 21:21 SK TAL EDI
Total/NA Prep 7471A 75533 06/20/11 10:07 EMN TAL WFD
Total/NA Analysis 7471A 1 75577 06/20/11 15:10 EMN TAL WFD
Total/NA Prep 3050B 75498 06/20/11 07:33 EMN TAL WFD
Total/NA Analysis 6010B 1 75614 06/20/11 16:12 TJS TAL WFD
Total/NA Analysis Moisture 1 75547 06/20/11 11:46 EMN TAL WFD
Soluble Leach DI Leach 75814 06/23/11 09:50 AMS TAL WFD
Soluble Analysis SM 2510B 1 75858 06/23/11 14:00 AMS TAL WFD
TestAmerica Westfield
Page 59 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Lab ChronicleClient: ARCADIS U.S., Inc TestAmerica Job ID: 360-34572-1
Project/Site: 28 Ball Hill Road
Client Sample ID: PH 1 SS-3 Lab Sample ID: 360-34572-3Matrix: SolidDate Collected: 06/16/11 14:00
Percent Solids: 88.1Date Received: 06/17/11 16:55
Batch
Type
Batch
Method Run
Dilution
Factor
Batch
Number
Prepared
Or Analyzed Analyst LabPrep Type
Total/NA Prep 5035 06/26/11 10:49 SS75985 TAL WFD
Total/NA Analysis 8260C 1 75986 06/27/11 08:39 SS TAL WFD
Total/NA Prep 3546 75634 06/21/11 11:45 OG TAL WFD
Total/NA Analysis 8270D 2 76250 06/30/11 18:05 CMR TAL WFD
Total/NA Prep 3546 75557 06/21/11 09:51 OG TAL WFD
Total/NA Analysis 8082A 1 75643 06/21/11 17:56 BRB TAL WFD
Total/NA Analysis 8081B 1 75661 06/21/11 18:02 BRB TAL WFD
Total/NA Prep 3546 75555 06/21/11 10:12 OG TAL WFD
Total/NA Analysis 8015B 10 75828 06/23/11 14:15 BRB TAL WFD
Total/NA Prep 8151A 77865 06/24/11 10:56 ME TAL EDI
Total/NA Analysis 8151A 1 78058 06/26/11 21:51 SK TAL EDI
Total/NA Prep 7471A 75533 06/20/11 10:07 EMN TAL WFD
Total/NA Analysis 7471A 1 75577 06/20/11 15:12 EMN TAL WFD
Total/NA Prep 3050B 75498 06/20/11 07:33 EMN TAL WFD
Total/NA Analysis 6010B 1 75614 06/20/11 16:15 TJS TAL WFD
Total/NA Analysis Moisture 1 75547 06/20/11 11:46 EMN TAL WFD
Soluble Leach DI Leach 75814 06/23/11 09:50 AMS TAL WFD
Soluble Analysis SM 2510B 1 75858 06/23/11 14:00 AMS TAL WFD
Laboratory References:
TAL EDI = TestAmerica Edison, 777 New Durham Road, Edison, NJ 08817, TEL (732)549-3900
TAL WFD = TestAmerica Westfield, Westfield Executive Park, 53 Southampton Road, Westfield, MA 01085, TEL (413)572-4000
TestAmerica Westfield
Page 60 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Certification SummaryTestAmerica Job ID: 360-34572-1Client: ARCADIS U.S., Inc
Project/Site: 28 Ball Hill Road
Laboratory Program Certification IDAuthority EPA Region
TestAmerica Westfield PH-0494State ProgramConnecticut 1
TestAmerica Westfield MA00014State ProgramMaine 1
TestAmerica Westfield M-MA014State ProgramMassachusetts 1
TestAmerica Westfield 2539NELACNew Hampshire 1
TestAmerica Westfield 10843NELACNew York 2
TestAmerica Westfield 647North Carolina DENRNorth Carolina 4
TestAmerica Westfield LAO00057State ProgramRhode Island 1
TestAmerica Westfield VT-10843State ProgramVermont 1
TestAmerica Edison PH-0200State ProgramConnecticut 1
TestAmerica Edison N/ADelaware DNRECDelaware 3
TestAmerica Edison 12028NELACNew Jersey 2
TestAmerica Edison 11452NELACNew York 2
TestAmerica Edison 68-00522NELACPennsylvania 3
TestAmerica Edison LAO00132State ProgramRhode Island 1
TestAmerica Edison NJCA-003-08USDAUSDA
Accreditation may not be offered or required for all methods and analytes reported in this package. Please contact your project manager for the laboratory’s current list
of certified methods and analytes.
TestAmerica Westfield
Page 61 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
State Accreditation Matrix
New Hampshire
(NELAC) prim. Mass ConnFlorida
(NELAC)North
Carolina
821-R-02-012 Toxicity, Acute (48-Hour)(list upon request) NP NP
SM 4500 Cl F Chlorine, Residual NP
SM 9215E Heterotrophic Plate Count (SimPlate) P
SM 9222D Coliforms, Fecal (Membrane Filter) P/NP
SM 9223 Coliforms, Total, and E.Coli (Colilert-P/A) P
SM 9224 Coliforms, Total, and E.Coli (Enumeration) P
1103.1 E.coli
Enterolert Enterococcus
200.8 Rev 5.4 Metals (ICP/MS) (list upon request) NP/P NP/P NP/P
200.7 Rev 4.4 Metals (ICP)(list upon request) NP/P NP/P NP/P
6010B Metals (ICP)(list upon request) NP/SW NP/SW
245.1 Mercury (CVAA) NP/P NP NP/P
7470A Mercury (CVAA) NP NP
7471A Mercury (CVAA) SW SW
SM 2340B Total Hardness (as CaCO3) by calculation NP/P NP NP/P
3005A Preparation, Total Recoverable or Dissolved Metals NP/P NP/P
3010A Preparation, Total Metals NP/P NP/P
3020A Preparation, Total Metals NP/P/SW NP/P/SW
3050B Preparation, Metals SW SW
504.1 EDB, DBCP and 1,2,3-TCP (GC) P P P
608 Organochlorine Pest/PCBs (list upon request) NP NP NP
625 Semivolatile Org Comp (GC/MS)(list upon request) NP NP
3546 Microwave Extraction SW
3510C Liquid-Liquid Extraction (Separatory Funnel) NP NP
3540C Soxhlet Extraction SW
3550B Ultrasonic Extraction SW SW
600/4-81-045 Polychlorinated Biphenyls (PCBs) (GC) NP NP
8081A Organochlorine Pesticides (GC)(list upon request) NP/SW NP/SW
8082 PCBs by Gas Chromatography(list upon request) NP/SW NP/SW
8270C Semivolatile Comp.(GC/MS)(list upon request) NP/SW NP/SW
CT ETPH Conn - Ext. Total petroleum Hydrocarbons (GC) NP/SW
MA-EPH Mass - Extractable Petroleum Hydrocarbons (GC) NP/SW NP/SW
524.2 Volatile Org Comp (GC/MS)(list upon request) P P P
524.2 Trihalomethane compounds P P P
624 Volatile Org Comp (GC/MS)(list upon request) NP NP NP
5035 Closed System Purge and Trap SW SW
5030B Purge and Trap NP NP
8260B Volatile Org Comp. (GC/MS)(list upon request) NP/SW NP/SW
MAVPH Mass - Volatile Petroleum Hydrocarbons (GC) NP/SW NP/SW
180.1 Turbidity, Nephelometric P P P
300 Anions, Ion Chromatography NP/P NP/P NP/P
410.4 COD NP NP NP
1010 Ignitability, Pensky-Martens Closed-Cup Method SW SW
10-107-06-2 Nitrogen, Total Kjeldahl NP NP NP
7196A Chromium, Hexavalent NP/SW NP/SW
9012A Cyanide, Total and/or Amenable NP/SW NP/SW
9030B Sulfide, Distillation (Acid Soluble and Insoluble) NP NP
9040B pH NP NP
9045C pH SW SW
L107041C Nitrogen, Nitrate NP P NP/P
L107-06-1B Nitrogen Ammonia NP NP NP/P
L204001A CN Cyanide, Total P NP/P NP/P
L210-001A Phenolics, Total Recoverable NP NP NP
SM 2320B Alkalinity NP/P NP/P NP/P
SM 2510B Conductivity, Specific Conductance NP/P NP/P NP/P
SM 2540C Solids, Total Dissolved (TDS) NP/P NP/P NP/P
SM 2540D Solids, Total Suspended (TSS) NP NP NP
SM 3500 CR D Chromium, Hexavalent NP NP
SM 4500 H+ B pH NP/P NP/P NP/P
SM 4500 NO2 B Nitrogen, Nitrite NP P NP/P
SM 4500 P E Phosphorus, Orthophosphate NP/P NP NP/P
SM 4500 P E Phosphorus, Total NP NP NP
SM 4500 S2 D Sulfide, Total NP NP
SM 5210B BOD, 5-Day NP NP NP
SM 5310B Organic Carbon, Total (TOC) NP/P NP NP/P
Not all organic compounds are accreditied under NELACFor methods with multiple compounds all compounds may not meet NELAC criteria, listing should be obtained from the laboratory
The lab carries additional accreditations with several states. This is the laboratories typcial listing but is subject to change based on the laboratories current certification standing.
State where Primary Accreditation is Carried
Method Name Description
ambient/ source
NP=Non Potable P= Potable SW=Solid Waste WI-QA-040r5 last updated 3/2/2011
Page 62 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Login Sample Receipt Checklist
Client: ARCADIS U.S., Inc Job Number: 360-34572-1
Login Number: 34572
Question Answer Comment
Creator: Beaumier, Janine E
List Source: TestAmerica Westfield
List Number: 1
N/ARadioactivity either was not measured or, if measured, is at or below
background
N/AThe cooler's custody seal, if present, is intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the sample IDs on the containers and
the COC.
TrueSamples are received within Holding Time.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueVOA sample vials do not have headspace or bubble is <6mm (1/4") in
diameter.
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica Westfield
Page 63 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Login Sample Receipt Checklist
Client: ARCADIS U.S., Inc Job Number: 360-34572-1
Login Number: 34572
Question Answer Comment
Creator: Retana, Camille
List Source: TestAmerica Edison
List Creation: 06/21/11 03:38 PMList Number: 1
N/ARadioactivity either was not measured or, if measured, is at or below
background
TrueThe cooler's custody seal, if present, is intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
FalseCooler Temperature is acceptable.
TrueCooler Temperature is recorded. 8.4°C IR # 50
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the sample IDs on the containers and
the COC.
TrueSamples are received within Holding Time.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueVOA sample vials do not have headspace or bubble is <6mm (1/4") in
diameter.
N/AMultiphasic samples are not present.
N/ASamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica Westfield
Page 64 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Page 65 of 65 07/01/2011
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Appendix D
Soil Profile Package Information
Appendix D - Soil Profile Package Requirements Maplewood Farms Site Preparation Plan
Berlin, Massachusetts
A Soil Profile Package shall be prepared by the candidate site owner/generator and Engineering Consultant/LSP, signed and dated for review by the owner/Lighthouse and the Site LSP.
The following information is required in the Soil Profile Package to obtain approval for the reuse of soil at the above referenced location: 1. Name of property owner (generator), and Engineering Consultant/LSP.
2. Project Name and Location, MCP Release Tracking Number (if applicable), and MCP historyrelative to candidate soils.
3. The quantity of soil planned for reuse, and the amount of soil samples collected (minimum 1sample/500 cy of soil).
4. A site sketch or map of the soils depicting sampling locations and field screening results.
5. The analytical data sheets and a summary of the analytical results in comparison toAcceptance Criteria in the Riverview Industrial Park Soil Re-use Management Plan,demonstrating that results meet the criteria and a discussion on the basis for averaging, ifutilized.
6. Discussion of shipment schedule, transporter (if known), and other pertinent coordinationitems.
A summary of the Acceptance Criteria is attached as Table 1. This information should be provided with the Soil Profile Package for completion.
Two copies of the Soil Profiling Package must be sent to Lighthouse which will be reviewed, and; if acceptable, forwarded to the Site LSP. The Site LSP will review the package and will issue a letter of acknowledgement and acceptance to Lighthouse or the generator for countersignature. The package will then be forwarded to the generator.
If the candidate soil is non-impacted natural soil, a generator/LSP certification letter will be required for review by Lighthouse and the Site LSP.
Appendix E
Private Well Completion Report and
Testing