) UN I TEO STATES ENV I AONMENTAL PROTECT I ON AGENCY REGION I
Environmental Services Div isi on 60 Westview Street lexi ngton 11A 02173 -3 185
MEP10RAN0UI1 DATE August 15 1990
r SUBJ Char 1es George Landf i 11 Site - F 1 i 7 ~o~d
FROM Oenn 1 s ses Va 1d8s - xiJY-rftSe Env1ronmental Stud1es ~ 1-
TO Oavid Dickerson RPM MA Superfund Sect1on
ESD personnel collected water samples from Flint Pond in Tyngsboro MA on June 16 1990 The result s for the vol at i l e organic and semi-volatile organic analyses is attac hed The CL P numbers corres pond to the following locations
Station CLP Number Location Number
TA IPOl AT528 Trip blank
SW01 AT529 Marsh bullbull b y F I int Pond near route 3
SW0 2 AT530 Marsh area by flint pond
SW03 AT531 F 1 int Pond
If you need additional i nformat ion on the s tat ion locations please contact myself or Dan Granz
If you have any questions please contact me at 860-4378
CH
AR
LE
S
GE
OR
GE
L
AN
D
RE
CL
AM
AT
ION
T
RU
ST
L
AN
DF
ILL
A
DM
INIS
TR
AT
I VE
R
EC
OR
D
r 1
(-~~
~
1-
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r~_J j
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lt ~-
shy
~
) poundSAT PROJECT LANDMARK ONE ONE VAN DE GRMFF DRIVE BURLINGTON MA 01amp03
- (617)22$-2050 bull FAX (6m229()046
July 24 1990 Revised August 10 1990
H-0-7 -24
Mr Dennis Gagne Regional Sampl e Control Custodian U S Environmental Protection Agency 90 Can a l Street Boston Massachusetts 02114
Re TID No 01-9007-10 Case No 14355 SOG No AT 528 Southwest Research Institut e Charles George Site Tyngsboro Ma Volatile 4 Aqueous AT528 throuqh AT531 Semivolatile 3AqueousfAT529 through AT531
Dear Mr Gagne
A validation was performed on the organic analytical data for 4 water samples collected by the Environaental Studies Secti on of USEPA at the Charles George site Four samplea were analyzed for volatiles and three samples were analyzed for semivolatiles The sabullplea were analyze-1 according to the 288 statement of Work (SOW) one trip blank and one set of matrix spikejaatrix spike duplicates were abullong the 4 samples There were no field blanks or field duplicates The data were evaluated based on the following parameters
bull data completeness bull holding times bull GCHS tuning bull calibration bull blanks bull surrogate recoveries bull bullatrix spikejmatrix s pike duplicates
field duplicate r esults internal standard performance
bull compound identification bull compo und quantitation
- All criteria were met for this parameter Table I summari zes the validation r ecommendations which were based o n the following information
)
Mr Denni s Gag-ne July 24 1990 Page Two Revi s e d August 10 1990
H-0 - 7 - 2 4
Calibratiopbull
IC CC ~~
llroa011ethane X
chloroethane X acetone 1 1-dicbloroethane XX vinyl acetate X
Abullbullociatad saaples VBLkOl VBLkOl AT528 AT528 AT529 AT529 AT530 ATSJO ATSJl AT531 AT531MS AT531MS AT531MSD AT532KSO
The non-detected 11 -dichloroethane will be estiaated (UJ) due to the calibration not aeetinq criteria No action ibull necessary for the reaaining coa pounds since they were not detected i n the volatile samples
Pe r cent RSD gt30 Percent D gt25 Est i ma te (J ) a ll posi t i ve res ults
xx Percent RSO Pe r c ent D gt50 Estimate ( J ) all pos i shytive res ults and estimate (UJ) all non-de t ects
RF RF lt0 05 Es t i ma t e (J) al l posi t ive resul t s and rejec t (R) all no n- dete c t s
Hr Dennis Gagne July 24 1990 Page Three Revsed August 10 1990
H-0-7-24
Semiyolatile cc ~
bia (2-chloroethyl) ether X 2-nitroaniline X 3-nitroaniline 2 4-dinitrophenol 4-nitroaniline X 4 6-dinitro-2-aethylphenol X
Aaaociated Saaples SBLXOl AT529 AT530 AT531 AT531MS AT531MSD
No action i a required since the coapounds listed above vere not detected in the aeaivolatile aaaplea
x Percent RSD gt3 0 Percent D gt25 Estiaate (J all pos itive results
Percent RSD Percent D gt50 Estimate (J) all posishytive res ults and estimate (UJ) all non-detects
RFRF lt0 05 Estimate (J all positive results and reject (R) all non-detects
bullbull
)
Mr Dennis Gagne July 24 1990 Page Four Revised Auqus t 10 1990
H-0-7-2 4
aurroqatt Rtcoyeriet
Semiyolatile
The semivolatile surrogates which did not meet criteria for percent recovery are sulldllarized below
Ill A
mJ_ IIIZ lBI IIIL zn AT5JlKS AT531MSD 26 J5
QC Liaita JS 10 21 to to to to 114 116 100
The laboratory noted in the cas e narrative that the aatrix apike and aatrix apikbull duplicate were extracted usinq 500 al rather than one liter due to an insufficient aaount of aaaple This is a d eviation froa the 288 sow which indicates that aatrix spike and aatrix spike duplicate saaplea should be extracted with the same volue as the original aaaple No action is necessary since the validity of the data for saaple AT531 is not a f fec ted
)
Mr Dennis Gagne July 24 1990 Page Five Revised August 1 0 1990
H-0-7 - 2 4
It appears that there was a problem during the extracshytion or concentration process tor ATSJlMSD In ATSllMSO two acid s urrogates recovered less than lOt Recoveries ot the two surrogates were within criteria in ATSJl and ATSllMS Since s urrogate recoveries in AT531 were all within criteria and only one surroqate was slightly low in aaaple AT531MS no action will be taken for the original aaaple ATSJl Matrix SpikeMatrix Spike Duplicate
StpiyolatiJa
la t IISUJtl and ATU1JISD QC
IJaitJI
IIUIIall ~ 1BAl RfQ 1BAl RfQ
HSIISD 1 4-dichlorobenzene 2523 36-97 HSIISD n-nitroao-di-n- 3129 41-116
propylamine IISIISD 1 2 4-trichlorobenzene 3431 39-98 HSIISD acenaphthene 3635 46-118 IISD phenol 4 158 12-89 42IISD 2-chlorophenol 2 177 27-123 40IISD 4-chloro-3-methylphenol 22 2 3-97
Mr Dennis Gagne July 24 1990 Page Six Revised August 10 1990
H-0-7-24
Due to matrix spike recoveries less than ten percent the undetected phenol and 2-chlorophenol in aample AT5J1 will be rejected (R) bull The remaining compounds which did not meet matrix spike criteria were not detected in the original aamp1e therefore no action is required
Very truly yours
ROY F WESTON INC
~~ Zoe Horton Ot9anic Data Reviewer
~~tA-o ltA_
Cheryl Blaine
~~~middotFmiddot-Tea Manager ESAT Reqion I
Zh Enclosure(amp)
)
CnnEB GEOROB Case 14355
TABLE I - Recommendations Summary
amp llli A
AT528 A A A AT529 A A A AT530 A A A AT531 A AA
A Accept all data
Accept the reaulta for the aaaple but eatiaate the non-detected 1 1-dichloroethane since calishybration criteria waa not aet Inatruaent rashyaponae to thia coapound ia not atable therefore quantitation aay be affected
Accept the reaulta for the aaaple but reject (R) the undetected phenol and 2-chlorophenol due to low aatrix spike duplicate recoveriea Thia aay indicate that in the original aaaple theae acid coapounda vera not recovered accurately during extraction poaaibly resulting in falae negatives
Charibullbull Georqe Table II - Tentatively Identified Compoundbull (TICbull) awamary
AT529
FURAN TETRAHYDRO
X - CoJapound was detected
)
Data s ummary Xey
A Acceptable data
J The associatec1 nWDerical value is an estimated quantity
R Rej act data due to qual ty control criteria The data are unusable (compound may or may not be present) Reaampl inq and reanalysis is necessary tor verification
u The compound was analyzed tor but was not detected The associated numerical value is the sample quantitation limit
UJ The coapound was analyzed tor but was not detected The saaple quantitfltion liait is an estiaated quantity
The capounc1 Vfla analyzed tor but waa not c1etected The saaple quantitation liait ia the same as the CRQL presentec1
CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL
ADMINISTRAT IVE RECORD
( ) 06ll9 lQDllflrf JnO 0616V9 oI6V9 0616119 06161 on-snvo
Ol bullbull bullbull m l-wJIICIIInliO
---------middotmiddotmiddot-------middotmiddotmiddotmiddot--middotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddot bull-IAJ1 101
-bullbulln -NIIIIAtt11
-bulln-oIO)JUOLmiddotll ll wbullbulln-o101J1bull1
-middotbullbull-z oa -wtd-z-14tt_
s 0middot-middotmiddot S tuldoldDIOJI0-[ 1--bull1
_1011bull1 -l l l __IO__ o
-0-JO Ioi~ IJI
-diDIdDJOIol-10-[ 1-l -
OOIdDJO)IP0-l l
- 1-JoOIPIIIbullbullu l 1I IIV AIIA
111)) Jo0 )1PtJIIIUCiqJI]
_Joell lol-1bull1-1 1 1 _nz
- IOIO)Iol-0-ll
( )UOJ )-Ioll-oIO JI-10 bullll
-ot-oJOllol-10middot 1 1
-ot-oJOl l-10 -1 1
M) 0UDqJI]
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01 PIJOIfl AIIJA
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l[SIY oun llSJY _ ~~~ d j JI
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CHARLES GEORGE LAND RECLAMATION TRUS T LANDFI LL
AOHINISTRATI VE RECORD
()
ann usn oun
_11_
6lSU
lllnll middot[ -~O~Dl~WObulll
_~~~~~
middot~middotlbullllllod lllj~-
lll~liimiddotZ -1bull11~1fMuoH1Jrpz
1-pHIIPI~I -Sl loHIJII~~Imiddotl
-~ludoiHI)IPft
-~~~PMgtJAIIImiddotZ -lodIIII~ [ middot OHI)ICbull
-~~~IIQOHIJIPftOI
OII J)jueGHIJIQbull
_bull lfdtl
-n-qoo~OJIPI~I middottll
1-lfdioHI)II~IOmiddotl
-~~~-liiIOiji-HIIIO middotZgtbullIq
P71 ~011101
p~~ ~bullmiddotz
~---~bullu-z
~---middot -NiqO~I1
-1HIJIPObull
-IbullAdold-U-Pmiddot-~~11bull1
1-lfIIAIII
~bull1110 ( iildoJdoOjOHIIOmiddotl)Ojq
1-lod AII1middotl
-NiqOHI JIPI Omiddotll
10110~ jA NOI
-NOqOHI JIP0middot1
-laqiiIHI JIP 0middot [ 1
_- o z
~Otf10 (1Aij1MHii10middotllbull lq
lliMIIIoiOIAOIY1
MIUfXI1 Jl IZS OIIOS
w bull bull ~bullbulll~bulloo bullbullll
_
CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL
AOHINISTRATI VE RECORD
~----~__ filii
til
tltMoshy
( I
06R9bull 06ll9 I QJ131111] UYO 0616l9 0616l9 0616ll9 IQ]41fn]1YO
11))-fJIIOUnliO
Ol -)Lecl( )lf l )orut
01 -OJifl(ljI ) NIIq)Q
Ol -Md(PmiddotpoundlI)OUIIpU)
Ol -Md( I )O
II -~~~-l f(~)OIWI
01 -IUUIlf (q)Ollel
111 ) lljd)J110middotUmiddot)0
Ul)l lfllld()JIj)llfUmiddotl)I U
01 -w10
01 -OJif1UI( I )ONII
P) lWqOJO)IP0bullpoundpound
l l l ) llfl lld lAlMCI )Il11
~middot lll)l~jlfdlAIIqmiddotUmiddot0
OS l-lfdoHJifOI4 01 -NiqOJO)IPIIIII 01 Jllj)I)Aulf4middot1Aui~Jbull bull
01 l)aulbull l lldiposoJlUmiddotI
OS 1--PIAbullIl_middot l middotOJ1)U)Qbull9t
OS au10JIUmiddott
Ol J lbulllWIfltllmiddotl~JO)IOmiddott
01 lll)llflfdAij11 )0
_)OIOJI)U)Qmiddottl
0) UljONiqjQ
os bull-fdonu os _lfdoJI UOmiddot middotz
_lry IU1Y OU1Y 6lS1Y n AIOUIOIYl 1101Ul0l Jl4WYS l fSn 0[51Y J8WII JldWS
tlSlY middoto11 CIS SSOI =nn u --o 1 1 1100 -s til OJOq1llluAj lllo U )Ji tQ uu
~ ~--~----4--===================- middot middotc~-====================--_j
- barcode 555910
- barcodetext SDMS Doc ID 555910
CH
AR
LE
S
GE
OR
GE
L
AN
D
RE
CL
AM
AT
ION
T
RU
ST
L
AN
DF
ILL
A
DM
INIS
TR
AT
I VE
R
EC
OR
D
r 1
(-~~
~
1-
I -
L 1
~
H i J
r~_J j
~
I ~ -
L-~bull s
-1
(
h y~ l
II
-~
1 JV ~ ~-middot-
lt ~-
shy
~
) poundSAT PROJECT LANDMARK ONE ONE VAN DE GRMFF DRIVE BURLINGTON MA 01amp03
- (617)22$-2050 bull FAX (6m229()046
July 24 1990 Revised August 10 1990
H-0-7 -24
Mr Dennis Gagne Regional Sampl e Control Custodian U S Environmental Protection Agency 90 Can a l Street Boston Massachusetts 02114
Re TID No 01-9007-10 Case No 14355 SOG No AT 528 Southwest Research Institut e Charles George Site Tyngsboro Ma Volatile 4 Aqueous AT528 throuqh AT531 Semivolatile 3AqueousfAT529 through AT531
Dear Mr Gagne
A validation was performed on the organic analytical data for 4 water samples collected by the Environaental Studies Secti on of USEPA at the Charles George site Four samplea were analyzed for volatiles and three samples were analyzed for semivolatiles The sabullplea were analyze-1 according to the 288 statement of Work (SOW) one trip blank and one set of matrix spikejaatrix spike duplicates were abullong the 4 samples There were no field blanks or field duplicates The data were evaluated based on the following parameters
bull data completeness bull holding times bull GCHS tuning bull calibration bull blanks bull surrogate recoveries bull bullatrix spikejmatrix s pike duplicates
field duplicate r esults internal standard performance
bull compound identification bull compo und quantitation
- All criteria were met for this parameter Table I summari zes the validation r ecommendations which were based o n the following information
)
Mr Denni s Gag-ne July 24 1990 Page Two Revi s e d August 10 1990
H-0 - 7 - 2 4
Calibratiopbull
IC CC ~~
llroa011ethane X
chloroethane X acetone 1 1-dicbloroethane XX vinyl acetate X
Abullbullociatad saaples VBLkOl VBLkOl AT528 AT528 AT529 AT529 AT530 ATSJO ATSJl AT531 AT531MS AT531MS AT531MSD AT532KSO
The non-detected 11 -dichloroethane will be estiaated (UJ) due to the calibration not aeetinq criteria No action ibull necessary for the reaaining coa pounds since they were not detected i n the volatile samples
Pe r cent RSD gt30 Percent D gt25 Est i ma te (J ) a ll posi t i ve res ults
xx Percent RSO Pe r c ent D gt50 Estimate ( J ) all pos i shytive res ults and estimate (UJ) all non-de t ects
RF RF lt0 05 Es t i ma t e (J) al l posi t ive resul t s and rejec t (R) all no n- dete c t s
Hr Dennis Gagne July 24 1990 Page Three Revsed August 10 1990
H-0-7-24
Semiyolatile cc ~
bia (2-chloroethyl) ether X 2-nitroaniline X 3-nitroaniline 2 4-dinitrophenol 4-nitroaniline X 4 6-dinitro-2-aethylphenol X
Aaaociated Saaples SBLXOl AT529 AT530 AT531 AT531MS AT531MSD
No action i a required since the coapounds listed above vere not detected in the aeaivolatile aaaplea
x Percent RSD gt3 0 Percent D gt25 Estiaate (J all pos itive results
Percent RSD Percent D gt50 Estimate (J) all posishytive res ults and estimate (UJ) all non-detects
RFRF lt0 05 Estimate (J all positive results and reject (R) all non-detects
bullbull
)
Mr Dennis Gagne July 24 1990 Page Four Revised Auqus t 10 1990
H-0-7-2 4
aurroqatt Rtcoyeriet
Semiyolatile
The semivolatile surrogates which did not meet criteria for percent recovery are sulldllarized below
Ill A
mJ_ IIIZ lBI IIIL zn AT5JlKS AT531MSD 26 J5
QC Liaita JS 10 21 to to to to 114 116 100
The laboratory noted in the cas e narrative that the aatrix apike and aatrix apikbull duplicate were extracted usinq 500 al rather than one liter due to an insufficient aaount of aaaple This is a d eviation froa the 288 sow which indicates that aatrix spike and aatrix spike duplicate saaplea should be extracted with the same volue as the original aaaple No action is necessary since the validity of the data for saaple AT531 is not a f fec ted
)
Mr Dennis Gagne July 24 1990 Page Five Revised August 1 0 1990
H-0-7 - 2 4
It appears that there was a problem during the extracshytion or concentration process tor ATSJlMSD In ATSllMSO two acid s urrogates recovered less than lOt Recoveries ot the two surrogates were within criteria in ATSJl and ATSllMS Since s urrogate recoveries in AT531 were all within criteria and only one surroqate was slightly low in aaaple AT531MS no action will be taken for the original aaaple ATSJl Matrix SpikeMatrix Spike Duplicate
StpiyolatiJa
la t IISUJtl and ATU1JISD QC
IJaitJI
IIUIIall ~ 1BAl RfQ 1BAl RfQ
HSIISD 1 4-dichlorobenzene 2523 36-97 HSIISD n-nitroao-di-n- 3129 41-116
propylamine IISIISD 1 2 4-trichlorobenzene 3431 39-98 HSIISD acenaphthene 3635 46-118 IISD phenol 4 158 12-89 42IISD 2-chlorophenol 2 177 27-123 40IISD 4-chloro-3-methylphenol 22 2 3-97
Mr Dennis Gagne July 24 1990 Page Six Revised August 10 1990
H-0-7-24
Due to matrix spike recoveries less than ten percent the undetected phenol and 2-chlorophenol in aample AT5J1 will be rejected (R) bull The remaining compounds which did not meet matrix spike criteria were not detected in the original aamp1e therefore no action is required
Very truly yours
ROY F WESTON INC
~~ Zoe Horton Ot9anic Data Reviewer
~~tA-o ltA_
Cheryl Blaine
~~~middotFmiddot-Tea Manager ESAT Reqion I
Zh Enclosure(amp)
)
CnnEB GEOROB Case 14355
TABLE I - Recommendations Summary
amp llli A
AT528 A A A AT529 A A A AT530 A A A AT531 A AA
A Accept all data
Accept the reaulta for the aaaple but eatiaate the non-detected 1 1-dichloroethane since calishybration criteria waa not aet Inatruaent rashyaponae to thia coapound ia not atable therefore quantitation aay be affected
Accept the reaulta for the aaaple but reject (R) the undetected phenol and 2-chlorophenol due to low aatrix spike duplicate recoveriea Thia aay indicate that in the original aaaple theae acid coapounda vera not recovered accurately during extraction poaaibly resulting in falae negatives
Charibullbull Georqe Table II - Tentatively Identified Compoundbull (TICbull) awamary
AT529
FURAN TETRAHYDRO
X - CoJapound was detected
)
Data s ummary Xey
A Acceptable data
J The associatec1 nWDerical value is an estimated quantity
R Rej act data due to qual ty control criteria The data are unusable (compound may or may not be present) Reaampl inq and reanalysis is necessary tor verification
u The compound was analyzed tor but was not detected The associated numerical value is the sample quantitation limit
UJ The coapound was analyzed tor but was not detected The saaple quantitfltion liait is an estiaated quantity
The capounc1 Vfla analyzed tor but waa not c1etected The saaple quantitation liait ia the same as the CRQL presentec1
CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL
ADMINISTRAT IVE RECORD
( ) 06ll9 lQDllflrf JnO 0616V9 oI6V9 0616119 06161 on-snvo
Ol bullbull bullbull m l-wJIICIIInliO
---------middotmiddotmiddot-------middotmiddotmiddotmiddot--middotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddot bull-IAJ1 101
-bullbulln -NIIIIAtt11
-bulln-oIO)JUOLmiddotll ll wbullbulln-o101J1bull1
-middotbullbull-z oa -wtd-z-14tt_
s 0middot-middotmiddot S tuldoldDIOJI0-[ 1--bull1
_1011bull1 -l l l __IO__ o
-0-JO Ioi~ IJI
-diDIdDJOIol-10-[ 1-l -
OOIdDJO)IP0-l l
- 1-JoOIPIIIbullbullu l 1I IIV AIIA
111)) Jo0 )1PtJIIIUCiqJI]
_Joell lol-1bull1-1 1 1 _nz
- IOIO)Iol-0-ll
( )UOJ )-Ioll-oIO JI-10 bullll
-ot-oJOllol-10middot 1 1
-ot-oJOl l-10 -1 1
M) 0UDqJI]
JO )Ioll-l Aiol
01 PIJOIfl AIIJA
01 -~~~-middotmiddot 01 __Jo01]
l[SIY oun llSJY _ ~~~ d j JI
I[SIr oun
WI _11110A OIOQIeampAI~H)JIIQ
~
CHARLES GEORGE LAND RECLAMATION TRUS T LANDFI LL
AOHINISTRATI VE RECORD
()
ann usn oun
_11_
6lSU
lllnll middot[ -~O~Dl~WObulll
_~~~~~
middot~middotlbullllllod lllj~-
lll~liimiddotZ -1bull11~1fMuoH1Jrpz
1-pHIIPI~I -Sl loHIJII~~Imiddotl
-~ludoiHI)IPft
-~~~PMgtJAIIImiddotZ -lodIIII~ [ middot OHI)ICbull
-~~~IIQOHIJIPftOI
OII J)jueGHIJIQbull
_bull lfdtl
-n-qoo~OJIPI~I middottll
1-lfdioHI)II~IOmiddotl
-~~~-liiIOiji-HIIIO middotZgtbullIq
P71 ~011101
p~~ ~bullmiddotz
~---~bullu-z
~---middot -NiqO~I1
-1HIJIPObull
-IbullAdold-U-Pmiddot-~~11bull1
1-lfIIAIII
~bull1110 ( iildoJdoOjOHIIOmiddotl)Ojq
1-lod AII1middotl
-NiqOHI JIPI Omiddotll
10110~ jA NOI
-NOqOHI JIP0middot1
-laqiiIHI JIP 0middot [ 1
_- o z
~Otf10 (1Aij1MHii10middotllbull lq
lliMIIIoiOIAOIY1
MIUfXI1 Jl IZS OIIOS
w bull bull ~bullbulll~bulloo bullbullll
_
CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL
AOHINISTRATI VE RECORD
~----~__ filii
til
tltMoshy
( I
06R9bull 06ll9 I QJ131111] UYO 0616l9 0616l9 0616ll9 IQ]41fn]1YO
11))-fJIIOUnliO
Ol -)Lecl( )lf l )orut
01 -OJifl(ljI ) NIIq)Q
Ol -Md(PmiddotpoundlI)OUIIpU)
Ol -Md( I )O
II -~~~-l f(~)OIWI
01 -IUUIlf (q)Ollel
111 ) lljd)J110middotUmiddot)0
Ul)l lfllld()JIj)llfUmiddotl)I U
01 -w10
01 -OJif1UI( I )ONII
P) lWqOJO)IP0bullpoundpound
l l l ) llfl lld lAlMCI )Il11
~middot lll)l~jlfdlAIIqmiddotUmiddot0
OS l-lfdoHJifOI4 01 -NiqOJO)IPIIIII 01 Jllj)I)Aulf4middot1Aui~Jbull bull
01 l)aulbull l lldiposoJlUmiddotI
OS 1--PIAbullIl_middot l middotOJ1)U)Qbull9t
OS au10JIUmiddott
Ol J lbulllWIfltllmiddotl~JO)IOmiddott
01 lll)llflfdAij11 )0
_)OIOJI)U)Qmiddottl
0) UljONiqjQ
os bull-fdonu os _lfdoJI UOmiddot middotz
_lry IU1Y OU1Y 6lS1Y n AIOUIOIYl 1101Ul0l Jl4WYS l fSn 0[51Y J8WII JldWS
tlSlY middoto11 CIS SSOI =nn u --o 1 1 1100 -s til OJOq1llluAj lllo U )Ji tQ uu
~ ~--~----4--===================- middot middotc~-====================--_j
- barcode 555910
- barcodetext SDMS Doc ID 555910
) poundSAT PROJECT LANDMARK ONE ONE VAN DE GRMFF DRIVE BURLINGTON MA 01amp03
- (617)22$-2050 bull FAX (6m229()046
July 24 1990 Revised August 10 1990
H-0-7 -24
Mr Dennis Gagne Regional Sampl e Control Custodian U S Environmental Protection Agency 90 Can a l Street Boston Massachusetts 02114
Re TID No 01-9007-10 Case No 14355 SOG No AT 528 Southwest Research Institut e Charles George Site Tyngsboro Ma Volatile 4 Aqueous AT528 throuqh AT531 Semivolatile 3AqueousfAT529 through AT531
Dear Mr Gagne
A validation was performed on the organic analytical data for 4 water samples collected by the Environaental Studies Secti on of USEPA at the Charles George site Four samplea were analyzed for volatiles and three samples were analyzed for semivolatiles The sabullplea were analyze-1 according to the 288 statement of Work (SOW) one trip blank and one set of matrix spikejaatrix spike duplicates were abullong the 4 samples There were no field blanks or field duplicates The data were evaluated based on the following parameters
bull data completeness bull holding times bull GCHS tuning bull calibration bull blanks bull surrogate recoveries bull bullatrix spikejmatrix s pike duplicates
field duplicate r esults internal standard performance
bull compound identification bull compo und quantitation
- All criteria were met for this parameter Table I summari zes the validation r ecommendations which were based o n the following information
)
Mr Denni s Gag-ne July 24 1990 Page Two Revi s e d August 10 1990
H-0 - 7 - 2 4
Calibratiopbull
IC CC ~~
llroa011ethane X
chloroethane X acetone 1 1-dicbloroethane XX vinyl acetate X
Abullbullociatad saaples VBLkOl VBLkOl AT528 AT528 AT529 AT529 AT530 ATSJO ATSJl AT531 AT531MS AT531MS AT531MSD AT532KSO
The non-detected 11 -dichloroethane will be estiaated (UJ) due to the calibration not aeetinq criteria No action ibull necessary for the reaaining coa pounds since they were not detected i n the volatile samples
Pe r cent RSD gt30 Percent D gt25 Est i ma te (J ) a ll posi t i ve res ults
xx Percent RSO Pe r c ent D gt50 Estimate ( J ) all pos i shytive res ults and estimate (UJ) all non-de t ects
RF RF lt0 05 Es t i ma t e (J) al l posi t ive resul t s and rejec t (R) all no n- dete c t s
Hr Dennis Gagne July 24 1990 Page Three Revsed August 10 1990
H-0-7-24
Semiyolatile cc ~
bia (2-chloroethyl) ether X 2-nitroaniline X 3-nitroaniline 2 4-dinitrophenol 4-nitroaniline X 4 6-dinitro-2-aethylphenol X
Aaaociated Saaples SBLXOl AT529 AT530 AT531 AT531MS AT531MSD
No action i a required since the coapounds listed above vere not detected in the aeaivolatile aaaplea
x Percent RSD gt3 0 Percent D gt25 Estiaate (J all pos itive results
Percent RSD Percent D gt50 Estimate (J) all posishytive res ults and estimate (UJ) all non-detects
RFRF lt0 05 Estimate (J all positive results and reject (R) all non-detects
bullbull
)
Mr Dennis Gagne July 24 1990 Page Four Revised Auqus t 10 1990
H-0-7-2 4
aurroqatt Rtcoyeriet
Semiyolatile
The semivolatile surrogates which did not meet criteria for percent recovery are sulldllarized below
Ill A
mJ_ IIIZ lBI IIIL zn AT5JlKS AT531MSD 26 J5
QC Liaita JS 10 21 to to to to 114 116 100
The laboratory noted in the cas e narrative that the aatrix apike and aatrix apikbull duplicate were extracted usinq 500 al rather than one liter due to an insufficient aaount of aaaple This is a d eviation froa the 288 sow which indicates that aatrix spike and aatrix spike duplicate saaplea should be extracted with the same volue as the original aaaple No action is necessary since the validity of the data for saaple AT531 is not a f fec ted
)
Mr Dennis Gagne July 24 1990 Page Five Revised August 1 0 1990
H-0-7 - 2 4
It appears that there was a problem during the extracshytion or concentration process tor ATSJlMSD In ATSllMSO two acid s urrogates recovered less than lOt Recoveries ot the two surrogates were within criteria in ATSJl and ATSllMS Since s urrogate recoveries in AT531 were all within criteria and only one surroqate was slightly low in aaaple AT531MS no action will be taken for the original aaaple ATSJl Matrix SpikeMatrix Spike Duplicate
StpiyolatiJa
la t IISUJtl and ATU1JISD QC
IJaitJI
IIUIIall ~ 1BAl RfQ 1BAl RfQ
HSIISD 1 4-dichlorobenzene 2523 36-97 HSIISD n-nitroao-di-n- 3129 41-116
propylamine IISIISD 1 2 4-trichlorobenzene 3431 39-98 HSIISD acenaphthene 3635 46-118 IISD phenol 4 158 12-89 42IISD 2-chlorophenol 2 177 27-123 40IISD 4-chloro-3-methylphenol 22 2 3-97
Mr Dennis Gagne July 24 1990 Page Six Revised August 10 1990
H-0-7-24
Due to matrix spike recoveries less than ten percent the undetected phenol and 2-chlorophenol in aample AT5J1 will be rejected (R) bull The remaining compounds which did not meet matrix spike criteria were not detected in the original aamp1e therefore no action is required
Very truly yours
ROY F WESTON INC
~~ Zoe Horton Ot9anic Data Reviewer
~~tA-o ltA_
Cheryl Blaine
~~~middotFmiddot-Tea Manager ESAT Reqion I
Zh Enclosure(amp)
)
CnnEB GEOROB Case 14355
TABLE I - Recommendations Summary
amp llli A
AT528 A A A AT529 A A A AT530 A A A AT531 A AA
A Accept all data
Accept the reaulta for the aaaple but eatiaate the non-detected 1 1-dichloroethane since calishybration criteria waa not aet Inatruaent rashyaponae to thia coapound ia not atable therefore quantitation aay be affected
Accept the reaulta for the aaaple but reject (R) the undetected phenol and 2-chlorophenol due to low aatrix spike duplicate recoveriea Thia aay indicate that in the original aaaple theae acid coapounda vera not recovered accurately during extraction poaaibly resulting in falae negatives
Charibullbull Georqe Table II - Tentatively Identified Compoundbull (TICbull) awamary
AT529
FURAN TETRAHYDRO
X - CoJapound was detected
)
Data s ummary Xey
A Acceptable data
J The associatec1 nWDerical value is an estimated quantity
R Rej act data due to qual ty control criteria The data are unusable (compound may or may not be present) Reaampl inq and reanalysis is necessary tor verification
u The compound was analyzed tor but was not detected The associated numerical value is the sample quantitation limit
UJ The coapound was analyzed tor but was not detected The saaple quantitfltion liait is an estiaated quantity
The capounc1 Vfla analyzed tor but waa not c1etected The saaple quantitation liait ia the same as the CRQL presentec1
CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL
ADMINISTRAT IVE RECORD
( ) 06ll9 lQDllflrf JnO 0616V9 oI6V9 0616119 06161 on-snvo
Ol bullbull bullbull m l-wJIICIIInliO
---------middotmiddotmiddot-------middotmiddotmiddotmiddot--middotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddot bull-IAJ1 101
-bullbulln -NIIIIAtt11
-bulln-oIO)JUOLmiddotll ll wbullbulln-o101J1bull1
-middotbullbull-z oa -wtd-z-14tt_
s 0middot-middotmiddot S tuldoldDIOJI0-[ 1--bull1
_1011bull1 -l l l __IO__ o
-0-JO Ioi~ IJI
-diDIdDJOIol-10-[ 1-l -
OOIdDJO)IP0-l l
- 1-JoOIPIIIbullbullu l 1I IIV AIIA
111)) Jo0 )1PtJIIIUCiqJI]
_Joell lol-1bull1-1 1 1 _nz
- IOIO)Iol-0-ll
( )UOJ )-Ioll-oIO JI-10 bullll
-ot-oJOllol-10middot 1 1
-ot-oJOl l-10 -1 1
M) 0UDqJI]
JO )Ioll-l Aiol
01 PIJOIfl AIIJA
01 -~~~-middotmiddot 01 __Jo01]
l[SIY oun llSJY _ ~~~ d j JI
I[SIr oun
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~
CHARLES GEORGE LAND RECLAMATION TRUS T LANDFI LL
AOHINISTRATI VE RECORD
()
ann usn oun
_11_
6lSU
lllnll middot[ -~O~Dl~WObulll
_~~~~~
middot~middotlbullllllod lllj~-
lll~liimiddotZ -1bull11~1fMuoH1Jrpz
1-pHIIPI~I -Sl loHIJII~~Imiddotl
-~ludoiHI)IPft
-~~~PMgtJAIIImiddotZ -lodIIII~ [ middot OHI)ICbull
-~~~IIQOHIJIPftOI
OII J)jueGHIJIQbull
_bull lfdtl
-n-qoo~OJIPI~I middottll
1-lfdioHI)II~IOmiddotl
-~~~-liiIOiji-HIIIO middotZgtbullIq
P71 ~011101
p~~ ~bullmiddotz
~---~bullu-z
~---middot -NiqO~I1
-1HIJIPObull
-IbullAdold-U-Pmiddot-~~11bull1
1-lfIIAIII
~bull1110 ( iildoJdoOjOHIIOmiddotl)Ojq
1-lod AII1middotl
-NiqOHI JIPI Omiddotll
10110~ jA NOI
-NOqOHI JIP0middot1
-laqiiIHI JIP 0middot [ 1
_- o z
~Otf10 (1Aij1MHii10middotllbull lq
lliMIIIoiOIAOIY1
MIUfXI1 Jl IZS OIIOS
w bull bull ~bullbulll~bulloo bullbullll
_
CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL
AOHINISTRATI VE RECORD
~----~__ filii
til
tltMoshy
( I
06R9bull 06ll9 I QJ131111] UYO 0616l9 0616l9 0616ll9 IQ]41fn]1YO
11))-fJIIOUnliO
Ol -)Lecl( )lf l )orut
01 -OJifl(ljI ) NIIq)Q
Ol -Md(PmiddotpoundlI)OUIIpU)
Ol -Md( I )O
II -~~~-l f(~)OIWI
01 -IUUIlf (q)Ollel
111 ) lljd)J110middotUmiddot)0
Ul)l lfllld()JIj)llfUmiddotl)I U
01 -w10
01 -OJif1UI( I )ONII
P) lWqOJO)IP0bullpoundpound
l l l ) llfl lld lAlMCI )Il11
~middot lll)l~jlfdlAIIqmiddotUmiddot0
OS l-lfdoHJifOI4 01 -NiqOJO)IPIIIII 01 Jllj)I)Aulf4middot1Aui~Jbull bull
01 l)aulbull l lldiposoJlUmiddotI
OS 1--PIAbullIl_middot l middotOJ1)U)Qbull9t
OS au10JIUmiddott
Ol J lbulllWIfltllmiddotl~JO)IOmiddott
01 lll)llflfdAij11 )0
_)OIOJI)U)Qmiddottl
0) UljONiqjQ
os bull-fdonu os _lfdoJI UOmiddot middotz
_lry IU1Y OU1Y 6lS1Y n AIOUIOIYl 1101Ul0l Jl4WYS l fSn 0[51Y J8WII JldWS
tlSlY middoto11 CIS SSOI =nn u --o 1 1 1100 -s til OJOq1llluAj lllo U )Ji tQ uu
~ ~--~----4--===================- middot middotc~-====================--_j
- barcode 555910
- barcodetext SDMS Doc ID 555910
)
Mr Denni s Gag-ne July 24 1990 Page Two Revi s e d August 10 1990
H-0 - 7 - 2 4
Calibratiopbull
IC CC ~~
llroa011ethane X
chloroethane X acetone 1 1-dicbloroethane XX vinyl acetate X
Abullbullociatad saaples VBLkOl VBLkOl AT528 AT528 AT529 AT529 AT530 ATSJO ATSJl AT531 AT531MS AT531MS AT531MSD AT532KSO
The non-detected 11 -dichloroethane will be estiaated (UJ) due to the calibration not aeetinq criteria No action ibull necessary for the reaaining coa pounds since they were not detected i n the volatile samples
Pe r cent RSD gt30 Percent D gt25 Est i ma te (J ) a ll posi t i ve res ults
xx Percent RSO Pe r c ent D gt50 Estimate ( J ) all pos i shytive res ults and estimate (UJ) all non-de t ects
RF RF lt0 05 Es t i ma t e (J) al l posi t ive resul t s and rejec t (R) all no n- dete c t s
Hr Dennis Gagne July 24 1990 Page Three Revsed August 10 1990
H-0-7-24
Semiyolatile cc ~
bia (2-chloroethyl) ether X 2-nitroaniline X 3-nitroaniline 2 4-dinitrophenol 4-nitroaniline X 4 6-dinitro-2-aethylphenol X
Aaaociated Saaples SBLXOl AT529 AT530 AT531 AT531MS AT531MSD
No action i a required since the coapounds listed above vere not detected in the aeaivolatile aaaplea
x Percent RSD gt3 0 Percent D gt25 Estiaate (J all pos itive results
Percent RSD Percent D gt50 Estimate (J) all posishytive res ults and estimate (UJ) all non-detects
RFRF lt0 05 Estimate (J all positive results and reject (R) all non-detects
bullbull
)
Mr Dennis Gagne July 24 1990 Page Four Revised Auqus t 10 1990
H-0-7-2 4
aurroqatt Rtcoyeriet
Semiyolatile
The semivolatile surrogates which did not meet criteria for percent recovery are sulldllarized below
Ill A
mJ_ IIIZ lBI IIIL zn AT5JlKS AT531MSD 26 J5
QC Liaita JS 10 21 to to to to 114 116 100
The laboratory noted in the cas e narrative that the aatrix apike and aatrix apikbull duplicate were extracted usinq 500 al rather than one liter due to an insufficient aaount of aaaple This is a d eviation froa the 288 sow which indicates that aatrix spike and aatrix spike duplicate saaplea should be extracted with the same volue as the original aaaple No action is necessary since the validity of the data for saaple AT531 is not a f fec ted
)
Mr Dennis Gagne July 24 1990 Page Five Revised August 1 0 1990
H-0-7 - 2 4
It appears that there was a problem during the extracshytion or concentration process tor ATSJlMSD In ATSllMSO two acid s urrogates recovered less than lOt Recoveries ot the two surrogates were within criteria in ATSJl and ATSllMS Since s urrogate recoveries in AT531 were all within criteria and only one surroqate was slightly low in aaaple AT531MS no action will be taken for the original aaaple ATSJl Matrix SpikeMatrix Spike Duplicate
StpiyolatiJa
la t IISUJtl and ATU1JISD QC
IJaitJI
IIUIIall ~ 1BAl RfQ 1BAl RfQ
HSIISD 1 4-dichlorobenzene 2523 36-97 HSIISD n-nitroao-di-n- 3129 41-116
propylamine IISIISD 1 2 4-trichlorobenzene 3431 39-98 HSIISD acenaphthene 3635 46-118 IISD phenol 4 158 12-89 42IISD 2-chlorophenol 2 177 27-123 40IISD 4-chloro-3-methylphenol 22 2 3-97
Mr Dennis Gagne July 24 1990 Page Six Revised August 10 1990
H-0-7-24
Due to matrix spike recoveries less than ten percent the undetected phenol and 2-chlorophenol in aample AT5J1 will be rejected (R) bull The remaining compounds which did not meet matrix spike criteria were not detected in the original aamp1e therefore no action is required
Very truly yours
ROY F WESTON INC
~~ Zoe Horton Ot9anic Data Reviewer
~~tA-o ltA_
Cheryl Blaine
~~~middotFmiddot-Tea Manager ESAT Reqion I
Zh Enclosure(amp)
)
CnnEB GEOROB Case 14355
TABLE I - Recommendations Summary
amp llli A
AT528 A A A AT529 A A A AT530 A A A AT531 A AA
A Accept all data
Accept the reaulta for the aaaple but eatiaate the non-detected 1 1-dichloroethane since calishybration criteria waa not aet Inatruaent rashyaponae to thia coapound ia not atable therefore quantitation aay be affected
Accept the reaulta for the aaaple but reject (R) the undetected phenol and 2-chlorophenol due to low aatrix spike duplicate recoveriea Thia aay indicate that in the original aaaple theae acid coapounda vera not recovered accurately during extraction poaaibly resulting in falae negatives
Charibullbull Georqe Table II - Tentatively Identified Compoundbull (TICbull) awamary
AT529
FURAN TETRAHYDRO
X - CoJapound was detected
)
Data s ummary Xey
A Acceptable data
J The associatec1 nWDerical value is an estimated quantity
R Rej act data due to qual ty control criteria The data are unusable (compound may or may not be present) Reaampl inq and reanalysis is necessary tor verification
u The compound was analyzed tor but was not detected The associated numerical value is the sample quantitation limit
UJ The coapound was analyzed tor but was not detected The saaple quantitfltion liait is an estiaated quantity
The capounc1 Vfla analyzed tor but waa not c1etected The saaple quantitation liait ia the same as the CRQL presentec1
CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL
ADMINISTRAT IVE RECORD
( ) 06ll9 lQDllflrf JnO 0616V9 oI6V9 0616119 06161 on-snvo
Ol bullbull bullbull m l-wJIICIIInliO
---------middotmiddotmiddot-------middotmiddotmiddotmiddot--middotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddot bull-IAJ1 101
-bullbulln -NIIIIAtt11
-bulln-oIO)JUOLmiddotll ll wbullbulln-o101J1bull1
-middotbullbull-z oa -wtd-z-14tt_
s 0middot-middotmiddot S tuldoldDIOJI0-[ 1--bull1
_1011bull1 -l l l __IO__ o
-0-JO Ioi~ IJI
-diDIdDJOIol-10-[ 1-l -
OOIdDJO)IP0-l l
- 1-JoOIPIIIbullbullu l 1I IIV AIIA
111)) Jo0 )1PtJIIIUCiqJI]
_Joell lol-1bull1-1 1 1 _nz
- IOIO)Iol-0-ll
( )UOJ )-Ioll-oIO JI-10 bullll
-ot-oJOllol-10middot 1 1
-ot-oJOl l-10 -1 1
M) 0UDqJI]
JO )Ioll-l Aiol
01 PIJOIfl AIIJA
01 -~~~-middotmiddot 01 __Jo01]
l[SIY oun llSJY _ ~~~ d j JI
I[SIr oun
WI _11110A OIOQIeampAI~H)JIIQ
~
CHARLES GEORGE LAND RECLAMATION TRUS T LANDFI LL
AOHINISTRATI VE RECORD
()
ann usn oun
_11_
6lSU
lllnll middot[ -~O~Dl~WObulll
_~~~~~
middot~middotlbullllllod lllj~-
lll~liimiddotZ -1bull11~1fMuoH1Jrpz
1-pHIIPI~I -Sl loHIJII~~Imiddotl
-~ludoiHI)IPft
-~~~PMgtJAIIImiddotZ -lodIIII~ [ middot OHI)ICbull
-~~~IIQOHIJIPftOI
OII J)jueGHIJIQbull
_bull lfdtl
-n-qoo~OJIPI~I middottll
1-lfdioHI)II~IOmiddotl
-~~~-liiIOiji-HIIIO middotZgtbullIq
P71 ~011101
p~~ ~bullmiddotz
~---~bullu-z
~---middot -NiqO~I1
-1HIJIPObull
-IbullAdold-U-Pmiddot-~~11bull1
1-lfIIAIII
~bull1110 ( iildoJdoOjOHIIOmiddotl)Ojq
1-lod AII1middotl
-NiqOHI JIPI Omiddotll
10110~ jA NOI
-NOqOHI JIP0middot1
-laqiiIHI JIP 0middot [ 1
_- o z
~Otf10 (1Aij1MHii10middotllbull lq
lliMIIIoiOIAOIY1
MIUfXI1 Jl IZS OIIOS
w bull bull ~bullbulll~bulloo bullbullll
_
CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL
AOHINISTRATI VE RECORD
~----~__ filii
til
tltMoshy
( I
06R9bull 06ll9 I QJ131111] UYO 0616l9 0616l9 0616ll9 IQ]41fn]1YO
11))-fJIIOUnliO
Ol -)Lecl( )lf l )orut
01 -OJifl(ljI ) NIIq)Q
Ol -Md(PmiddotpoundlI)OUIIpU)
Ol -Md( I )O
II -~~~-l f(~)OIWI
01 -IUUIlf (q)Ollel
111 ) lljd)J110middotUmiddot)0
Ul)l lfllld()JIj)llfUmiddotl)I U
01 -w10
01 -OJif1UI( I )ONII
P) lWqOJO)IP0bullpoundpound
l l l ) llfl lld lAlMCI )Il11
~middot lll)l~jlfdlAIIqmiddotUmiddot0
OS l-lfdoHJifOI4 01 -NiqOJO)IPIIIII 01 Jllj)I)Aulf4middot1Aui~Jbull bull
01 l)aulbull l lldiposoJlUmiddotI
OS 1--PIAbullIl_middot l middotOJ1)U)Qbull9t
OS au10JIUmiddott
Ol J lbulllWIfltllmiddotl~JO)IOmiddott
01 lll)llflfdAij11 )0
_)OIOJI)U)Qmiddottl
0) UljONiqjQ
os bull-fdonu os _lfdoJI UOmiddot middotz
_lry IU1Y OU1Y 6lS1Y n AIOUIOIYl 1101Ul0l Jl4WYS l fSn 0[51Y J8WII JldWS
tlSlY middoto11 CIS SSOI =nn u --o 1 1 1100 -s til OJOq1llluAj lllo U )Ji tQ uu
~ ~--~----4--===================- middot middotc~-====================--_j
- barcode 555910
- barcodetext SDMS Doc ID 555910
Hr Dennis Gagne July 24 1990 Page Three Revsed August 10 1990
H-0-7-24
Semiyolatile cc ~
bia (2-chloroethyl) ether X 2-nitroaniline X 3-nitroaniline 2 4-dinitrophenol 4-nitroaniline X 4 6-dinitro-2-aethylphenol X
Aaaociated Saaples SBLXOl AT529 AT530 AT531 AT531MS AT531MSD
No action i a required since the coapounds listed above vere not detected in the aeaivolatile aaaplea
x Percent RSD gt3 0 Percent D gt25 Estiaate (J all pos itive results
Percent RSD Percent D gt50 Estimate (J) all posishytive res ults and estimate (UJ) all non-detects
RFRF lt0 05 Estimate (J all positive results and reject (R) all non-detects
bullbull
)
Mr Dennis Gagne July 24 1990 Page Four Revised Auqus t 10 1990
H-0-7-2 4
aurroqatt Rtcoyeriet
Semiyolatile
The semivolatile surrogates which did not meet criteria for percent recovery are sulldllarized below
Ill A
mJ_ IIIZ lBI IIIL zn AT5JlKS AT531MSD 26 J5
QC Liaita JS 10 21 to to to to 114 116 100
The laboratory noted in the cas e narrative that the aatrix apike and aatrix apikbull duplicate were extracted usinq 500 al rather than one liter due to an insufficient aaount of aaaple This is a d eviation froa the 288 sow which indicates that aatrix spike and aatrix spike duplicate saaplea should be extracted with the same volue as the original aaaple No action is necessary since the validity of the data for saaple AT531 is not a f fec ted
)
Mr Dennis Gagne July 24 1990 Page Five Revised August 1 0 1990
H-0-7 - 2 4
It appears that there was a problem during the extracshytion or concentration process tor ATSJlMSD In ATSllMSO two acid s urrogates recovered less than lOt Recoveries ot the two surrogates were within criteria in ATSJl and ATSllMS Since s urrogate recoveries in AT531 were all within criteria and only one surroqate was slightly low in aaaple AT531MS no action will be taken for the original aaaple ATSJl Matrix SpikeMatrix Spike Duplicate
StpiyolatiJa
la t IISUJtl and ATU1JISD QC
IJaitJI
IIUIIall ~ 1BAl RfQ 1BAl RfQ
HSIISD 1 4-dichlorobenzene 2523 36-97 HSIISD n-nitroao-di-n- 3129 41-116
propylamine IISIISD 1 2 4-trichlorobenzene 3431 39-98 HSIISD acenaphthene 3635 46-118 IISD phenol 4 158 12-89 42IISD 2-chlorophenol 2 177 27-123 40IISD 4-chloro-3-methylphenol 22 2 3-97
Mr Dennis Gagne July 24 1990 Page Six Revised August 10 1990
H-0-7-24
Due to matrix spike recoveries less than ten percent the undetected phenol and 2-chlorophenol in aample AT5J1 will be rejected (R) bull The remaining compounds which did not meet matrix spike criteria were not detected in the original aamp1e therefore no action is required
Very truly yours
ROY F WESTON INC
~~ Zoe Horton Ot9anic Data Reviewer
~~tA-o ltA_
Cheryl Blaine
~~~middotFmiddot-Tea Manager ESAT Reqion I
Zh Enclosure(amp)
)
CnnEB GEOROB Case 14355
TABLE I - Recommendations Summary
amp llli A
AT528 A A A AT529 A A A AT530 A A A AT531 A AA
A Accept all data
Accept the reaulta for the aaaple but eatiaate the non-detected 1 1-dichloroethane since calishybration criteria waa not aet Inatruaent rashyaponae to thia coapound ia not atable therefore quantitation aay be affected
Accept the reaulta for the aaaple but reject (R) the undetected phenol and 2-chlorophenol due to low aatrix spike duplicate recoveriea Thia aay indicate that in the original aaaple theae acid coapounda vera not recovered accurately during extraction poaaibly resulting in falae negatives
Charibullbull Georqe Table II - Tentatively Identified Compoundbull (TICbull) awamary
AT529
FURAN TETRAHYDRO
X - CoJapound was detected
)
Data s ummary Xey
A Acceptable data
J The associatec1 nWDerical value is an estimated quantity
R Rej act data due to qual ty control criteria The data are unusable (compound may or may not be present) Reaampl inq and reanalysis is necessary tor verification
u The compound was analyzed tor but was not detected The associated numerical value is the sample quantitation limit
UJ The coapound was analyzed tor but was not detected The saaple quantitfltion liait is an estiaated quantity
The capounc1 Vfla analyzed tor but waa not c1etected The saaple quantitation liait ia the same as the CRQL presentec1
CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL
ADMINISTRAT IVE RECORD
( ) 06ll9 lQDllflrf JnO 0616V9 oI6V9 0616119 06161 on-snvo
Ol bullbull bullbull m l-wJIICIIInliO
---------middotmiddotmiddot-------middotmiddotmiddotmiddot--middotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddot bull-IAJ1 101
-bullbulln -NIIIIAtt11
-bulln-oIO)JUOLmiddotll ll wbullbulln-o101J1bull1
-middotbullbull-z oa -wtd-z-14tt_
s 0middot-middotmiddot S tuldoldDIOJI0-[ 1--bull1
_1011bull1 -l l l __IO__ o
-0-JO Ioi~ IJI
-diDIdDJOIol-10-[ 1-l -
OOIdDJO)IP0-l l
- 1-JoOIPIIIbullbullu l 1I IIV AIIA
111)) Jo0 )1PtJIIIUCiqJI]
_Joell lol-1bull1-1 1 1 _nz
- IOIO)Iol-0-ll
( )UOJ )-Ioll-oIO JI-10 bullll
-ot-oJOllol-10middot 1 1
-ot-oJOl l-10 -1 1
M) 0UDqJI]
JO )Ioll-l Aiol
01 PIJOIfl AIIJA
01 -~~~-middotmiddot 01 __Jo01]
l[SIY oun llSJY _ ~~~ d j JI
I[SIr oun
WI _11110A OIOQIeampAI~H)JIIQ
~
CHARLES GEORGE LAND RECLAMATION TRUS T LANDFI LL
AOHINISTRATI VE RECORD
()
ann usn oun
_11_
6lSU
lllnll middot[ -~O~Dl~WObulll
_~~~~~
middot~middotlbullllllod lllj~-
lll~liimiddotZ -1bull11~1fMuoH1Jrpz
1-pHIIPI~I -Sl loHIJII~~Imiddotl
-~ludoiHI)IPft
-~~~PMgtJAIIImiddotZ -lodIIII~ [ middot OHI)ICbull
-~~~IIQOHIJIPftOI
OII J)jueGHIJIQbull
_bull lfdtl
-n-qoo~OJIPI~I middottll
1-lfdioHI)II~IOmiddotl
-~~~-liiIOiji-HIIIO middotZgtbullIq
P71 ~011101
p~~ ~bullmiddotz
~---~bullu-z
~---middot -NiqO~I1
-1HIJIPObull
-IbullAdold-U-Pmiddot-~~11bull1
1-lfIIAIII
~bull1110 ( iildoJdoOjOHIIOmiddotl)Ojq
1-lod AII1middotl
-NiqOHI JIPI Omiddotll
10110~ jA NOI
-NOqOHI JIP0middot1
-laqiiIHI JIP 0middot [ 1
_- o z
~Otf10 (1Aij1MHii10middotllbull lq
lliMIIIoiOIAOIY1
MIUfXI1 Jl IZS OIIOS
w bull bull ~bullbulll~bulloo bullbullll
_
CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL
AOHINISTRATI VE RECORD
~----~__ filii
til
tltMoshy
( I
06R9bull 06ll9 I QJ131111] UYO 0616l9 0616l9 0616ll9 IQ]41fn]1YO
11))-fJIIOUnliO
Ol -)Lecl( )lf l )orut
01 -OJifl(ljI ) NIIq)Q
Ol -Md(PmiddotpoundlI)OUIIpU)
Ol -Md( I )O
II -~~~-l f(~)OIWI
01 -IUUIlf (q)Ollel
111 ) lljd)J110middotUmiddot)0
Ul)l lfllld()JIj)llfUmiddotl)I U
01 -w10
01 -OJif1UI( I )ONII
P) lWqOJO)IP0bullpoundpound
l l l ) llfl lld lAlMCI )Il11
~middot lll)l~jlfdlAIIqmiddotUmiddot0
OS l-lfdoHJifOI4 01 -NiqOJO)IPIIIII 01 Jllj)I)Aulf4middot1Aui~Jbull bull
01 l)aulbull l lldiposoJlUmiddotI
OS 1--PIAbullIl_middot l middotOJ1)U)Qbull9t
OS au10JIUmiddott
Ol J lbulllWIfltllmiddotl~JO)IOmiddott
01 lll)llflfdAij11 )0
_)OIOJI)U)Qmiddottl
0) UljONiqjQ
os bull-fdonu os _lfdoJI UOmiddot middotz
_lry IU1Y OU1Y 6lS1Y n AIOUIOIYl 1101Ul0l Jl4WYS l fSn 0[51Y J8WII JldWS
tlSlY middoto11 CIS SSOI =nn u --o 1 1 1100 -s til OJOq1llluAj lllo U )Ji tQ uu
~ ~--~----4--===================- middot middotc~-====================--_j
- barcode 555910
- barcodetext SDMS Doc ID 555910
bullbull
)
Mr Dennis Gagne July 24 1990 Page Four Revised Auqus t 10 1990
H-0-7-2 4
aurroqatt Rtcoyeriet
Semiyolatile
The semivolatile surrogates which did not meet criteria for percent recovery are sulldllarized below
Ill A
mJ_ IIIZ lBI IIIL zn AT5JlKS AT531MSD 26 J5
QC Liaita JS 10 21 to to to to 114 116 100
The laboratory noted in the cas e narrative that the aatrix apike and aatrix apikbull duplicate were extracted usinq 500 al rather than one liter due to an insufficient aaount of aaaple This is a d eviation froa the 288 sow which indicates that aatrix spike and aatrix spike duplicate saaplea should be extracted with the same volue as the original aaaple No action is necessary since the validity of the data for saaple AT531 is not a f fec ted
)
Mr Dennis Gagne July 24 1990 Page Five Revised August 1 0 1990
H-0-7 - 2 4
It appears that there was a problem during the extracshytion or concentration process tor ATSJlMSD In ATSllMSO two acid s urrogates recovered less than lOt Recoveries ot the two surrogates were within criteria in ATSJl and ATSllMS Since s urrogate recoveries in AT531 were all within criteria and only one surroqate was slightly low in aaaple AT531MS no action will be taken for the original aaaple ATSJl Matrix SpikeMatrix Spike Duplicate
StpiyolatiJa
la t IISUJtl and ATU1JISD QC
IJaitJI
IIUIIall ~ 1BAl RfQ 1BAl RfQ
HSIISD 1 4-dichlorobenzene 2523 36-97 HSIISD n-nitroao-di-n- 3129 41-116
propylamine IISIISD 1 2 4-trichlorobenzene 3431 39-98 HSIISD acenaphthene 3635 46-118 IISD phenol 4 158 12-89 42IISD 2-chlorophenol 2 177 27-123 40IISD 4-chloro-3-methylphenol 22 2 3-97
Mr Dennis Gagne July 24 1990 Page Six Revised August 10 1990
H-0-7-24
Due to matrix spike recoveries less than ten percent the undetected phenol and 2-chlorophenol in aample AT5J1 will be rejected (R) bull The remaining compounds which did not meet matrix spike criteria were not detected in the original aamp1e therefore no action is required
Very truly yours
ROY F WESTON INC
~~ Zoe Horton Ot9anic Data Reviewer
~~tA-o ltA_
Cheryl Blaine
~~~middotFmiddot-Tea Manager ESAT Reqion I
Zh Enclosure(amp)
)
CnnEB GEOROB Case 14355
TABLE I - Recommendations Summary
amp llli A
AT528 A A A AT529 A A A AT530 A A A AT531 A AA
A Accept all data
Accept the reaulta for the aaaple but eatiaate the non-detected 1 1-dichloroethane since calishybration criteria waa not aet Inatruaent rashyaponae to thia coapound ia not atable therefore quantitation aay be affected
Accept the reaulta for the aaaple but reject (R) the undetected phenol and 2-chlorophenol due to low aatrix spike duplicate recoveriea Thia aay indicate that in the original aaaple theae acid coapounda vera not recovered accurately during extraction poaaibly resulting in falae negatives
Charibullbull Georqe Table II - Tentatively Identified Compoundbull (TICbull) awamary
AT529
FURAN TETRAHYDRO
X - CoJapound was detected
)
Data s ummary Xey
A Acceptable data
J The associatec1 nWDerical value is an estimated quantity
R Rej act data due to qual ty control criteria The data are unusable (compound may or may not be present) Reaampl inq and reanalysis is necessary tor verification
u The compound was analyzed tor but was not detected The associated numerical value is the sample quantitation limit
UJ The coapound was analyzed tor but was not detected The saaple quantitfltion liait is an estiaated quantity
The capounc1 Vfla analyzed tor but waa not c1etected The saaple quantitation liait ia the same as the CRQL presentec1
CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL
ADMINISTRAT IVE RECORD
( ) 06ll9 lQDllflrf JnO 0616V9 oI6V9 0616119 06161 on-snvo
Ol bullbull bullbull m l-wJIICIIInliO
---------middotmiddotmiddot-------middotmiddotmiddotmiddot--middotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddot bull-IAJ1 101
-bullbulln -NIIIIAtt11
-bulln-oIO)JUOLmiddotll ll wbullbulln-o101J1bull1
-middotbullbull-z oa -wtd-z-14tt_
s 0middot-middotmiddot S tuldoldDIOJI0-[ 1--bull1
_1011bull1 -l l l __IO__ o
-0-JO Ioi~ IJI
-diDIdDJOIol-10-[ 1-l -
OOIdDJO)IP0-l l
- 1-JoOIPIIIbullbullu l 1I IIV AIIA
111)) Jo0 )1PtJIIIUCiqJI]
_Joell lol-1bull1-1 1 1 _nz
- IOIO)Iol-0-ll
( )UOJ )-Ioll-oIO JI-10 bullll
-ot-oJOllol-10middot 1 1
-ot-oJOl l-10 -1 1
M) 0UDqJI]
JO )Ioll-l Aiol
01 PIJOIfl AIIJA
01 -~~~-middotmiddot 01 __Jo01]
l[SIY oun llSJY _ ~~~ d j JI
I[SIr oun
WI _11110A OIOQIeampAI~H)JIIQ
~
CHARLES GEORGE LAND RECLAMATION TRUS T LANDFI LL
AOHINISTRATI VE RECORD
()
ann usn oun
_11_
6lSU
lllnll middot[ -~O~Dl~WObulll
_~~~~~
middot~middotlbullllllod lllj~-
lll~liimiddotZ -1bull11~1fMuoH1Jrpz
1-pHIIPI~I -Sl loHIJII~~Imiddotl
-~ludoiHI)IPft
-~~~PMgtJAIIImiddotZ -lodIIII~ [ middot OHI)ICbull
-~~~IIQOHIJIPftOI
OII J)jueGHIJIQbull
_bull lfdtl
-n-qoo~OJIPI~I middottll
1-lfdioHI)II~IOmiddotl
-~~~-liiIOiji-HIIIO middotZgtbullIq
P71 ~011101
p~~ ~bullmiddotz
~---~bullu-z
~---middot -NiqO~I1
-1HIJIPObull
-IbullAdold-U-Pmiddot-~~11bull1
1-lfIIAIII
~bull1110 ( iildoJdoOjOHIIOmiddotl)Ojq
1-lod AII1middotl
-NiqOHI JIPI Omiddotll
10110~ jA NOI
-NOqOHI JIP0middot1
-laqiiIHI JIP 0middot [ 1
_- o z
~Otf10 (1Aij1MHii10middotllbull lq
lliMIIIoiOIAOIY1
MIUfXI1 Jl IZS OIIOS
w bull bull ~bullbulll~bulloo bullbullll
_
CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL
AOHINISTRATI VE RECORD
~----~__ filii
til
tltMoshy
( I
06R9bull 06ll9 I QJ131111] UYO 0616l9 0616l9 0616ll9 IQ]41fn]1YO
11))-fJIIOUnliO
Ol -)Lecl( )lf l )orut
01 -OJifl(ljI ) NIIq)Q
Ol -Md(PmiddotpoundlI)OUIIpU)
Ol -Md( I )O
II -~~~-l f(~)OIWI
01 -IUUIlf (q)Ollel
111 ) lljd)J110middotUmiddot)0
Ul)l lfllld()JIj)llfUmiddotl)I U
01 -w10
01 -OJif1UI( I )ONII
P) lWqOJO)IP0bullpoundpound
l l l ) llfl lld lAlMCI )Il11
~middot lll)l~jlfdlAIIqmiddotUmiddot0
OS l-lfdoHJifOI4 01 -NiqOJO)IPIIIII 01 Jllj)I)Aulf4middot1Aui~Jbull bull
01 l)aulbull l lldiposoJlUmiddotI
OS 1--PIAbullIl_middot l middotOJ1)U)Qbull9t
OS au10JIUmiddott
Ol J lbulllWIfltllmiddotl~JO)IOmiddott
01 lll)llflfdAij11 )0
_)OIOJI)U)Qmiddottl
0) UljONiqjQ
os bull-fdonu os _lfdoJI UOmiddot middotz
_lry IU1Y OU1Y 6lS1Y n AIOUIOIYl 1101Ul0l Jl4WYS l fSn 0[51Y J8WII JldWS
tlSlY middoto11 CIS SSOI =nn u --o 1 1 1100 -s til OJOq1llluAj lllo U )Ji tQ uu
~ ~--~----4--===================- middot middotc~-====================--_j
- barcode 555910
- barcodetext SDMS Doc ID 555910
)
Mr Dennis Gagne July 24 1990 Page Five Revised August 1 0 1990
H-0-7 - 2 4
It appears that there was a problem during the extracshytion or concentration process tor ATSJlMSD In ATSllMSO two acid s urrogates recovered less than lOt Recoveries ot the two surrogates were within criteria in ATSJl and ATSllMS Since s urrogate recoveries in AT531 were all within criteria and only one surroqate was slightly low in aaaple AT531MS no action will be taken for the original aaaple ATSJl Matrix SpikeMatrix Spike Duplicate
StpiyolatiJa
la t IISUJtl and ATU1JISD QC
IJaitJI
IIUIIall ~ 1BAl RfQ 1BAl RfQ
HSIISD 1 4-dichlorobenzene 2523 36-97 HSIISD n-nitroao-di-n- 3129 41-116
propylamine IISIISD 1 2 4-trichlorobenzene 3431 39-98 HSIISD acenaphthene 3635 46-118 IISD phenol 4 158 12-89 42IISD 2-chlorophenol 2 177 27-123 40IISD 4-chloro-3-methylphenol 22 2 3-97
Mr Dennis Gagne July 24 1990 Page Six Revised August 10 1990
H-0-7-24
Due to matrix spike recoveries less than ten percent the undetected phenol and 2-chlorophenol in aample AT5J1 will be rejected (R) bull The remaining compounds which did not meet matrix spike criteria were not detected in the original aamp1e therefore no action is required
Very truly yours
ROY F WESTON INC
~~ Zoe Horton Ot9anic Data Reviewer
~~tA-o ltA_
Cheryl Blaine
~~~middotFmiddot-Tea Manager ESAT Reqion I
Zh Enclosure(amp)
)
CnnEB GEOROB Case 14355
TABLE I - Recommendations Summary
amp llli A
AT528 A A A AT529 A A A AT530 A A A AT531 A AA
A Accept all data
Accept the reaulta for the aaaple but eatiaate the non-detected 1 1-dichloroethane since calishybration criteria waa not aet Inatruaent rashyaponae to thia coapound ia not atable therefore quantitation aay be affected
Accept the reaulta for the aaaple but reject (R) the undetected phenol and 2-chlorophenol due to low aatrix spike duplicate recoveriea Thia aay indicate that in the original aaaple theae acid coapounda vera not recovered accurately during extraction poaaibly resulting in falae negatives
Charibullbull Georqe Table II - Tentatively Identified Compoundbull (TICbull) awamary
AT529
FURAN TETRAHYDRO
X - CoJapound was detected
)
Data s ummary Xey
A Acceptable data
J The associatec1 nWDerical value is an estimated quantity
R Rej act data due to qual ty control criteria The data are unusable (compound may or may not be present) Reaampl inq and reanalysis is necessary tor verification
u The compound was analyzed tor but was not detected The associated numerical value is the sample quantitation limit
UJ The coapound was analyzed tor but was not detected The saaple quantitfltion liait is an estiaated quantity
The capounc1 Vfla analyzed tor but waa not c1etected The saaple quantitation liait ia the same as the CRQL presentec1
CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL
ADMINISTRAT IVE RECORD
( ) 06ll9 lQDllflrf JnO 0616V9 oI6V9 0616119 06161 on-snvo
Ol bullbull bullbull m l-wJIICIIInliO
---------middotmiddotmiddot-------middotmiddotmiddotmiddot--middotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddot bull-IAJ1 101
-bullbulln -NIIIIAtt11
-bulln-oIO)JUOLmiddotll ll wbullbulln-o101J1bull1
-middotbullbull-z oa -wtd-z-14tt_
s 0middot-middotmiddot S tuldoldDIOJI0-[ 1--bull1
_1011bull1 -l l l __IO__ o
-0-JO Ioi~ IJI
-diDIdDJOIol-10-[ 1-l -
OOIdDJO)IP0-l l
- 1-JoOIPIIIbullbullu l 1I IIV AIIA
111)) Jo0 )1PtJIIIUCiqJI]
_Joell lol-1bull1-1 1 1 _nz
- IOIO)Iol-0-ll
( )UOJ )-Ioll-oIO JI-10 bullll
-ot-oJOllol-10middot 1 1
-ot-oJOl l-10 -1 1
M) 0UDqJI]
JO )Ioll-l Aiol
01 PIJOIfl AIIJA
01 -~~~-middotmiddot 01 __Jo01]
l[SIY oun llSJY _ ~~~ d j JI
I[SIr oun
WI _11110A OIOQIeampAI~H)JIIQ
~
CHARLES GEORGE LAND RECLAMATION TRUS T LANDFI LL
AOHINISTRATI VE RECORD
()
ann usn oun
_11_
6lSU
lllnll middot[ -~O~Dl~WObulll
_~~~~~
middot~middotlbullllllod lllj~-
lll~liimiddotZ -1bull11~1fMuoH1Jrpz
1-pHIIPI~I -Sl loHIJII~~Imiddotl
-~ludoiHI)IPft
-~~~PMgtJAIIImiddotZ -lodIIII~ [ middot OHI)ICbull
-~~~IIQOHIJIPftOI
OII J)jueGHIJIQbull
_bull lfdtl
-n-qoo~OJIPI~I middottll
1-lfdioHI)II~IOmiddotl
-~~~-liiIOiji-HIIIO middotZgtbullIq
P71 ~011101
p~~ ~bullmiddotz
~---~bullu-z
~---middot -NiqO~I1
-1HIJIPObull
-IbullAdold-U-Pmiddot-~~11bull1
1-lfIIAIII
~bull1110 ( iildoJdoOjOHIIOmiddotl)Ojq
1-lod AII1middotl
-NiqOHI JIPI Omiddotll
10110~ jA NOI
-NOqOHI JIP0middot1
-laqiiIHI JIP 0middot [ 1
_- o z
~Otf10 (1Aij1MHii10middotllbull lq
lliMIIIoiOIAOIY1
MIUfXI1 Jl IZS OIIOS
w bull bull ~bullbulll~bulloo bullbullll
_
CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL
AOHINISTRATI VE RECORD
~----~__ filii
til
tltMoshy
( I
06R9bull 06ll9 I QJ131111] UYO 0616l9 0616l9 0616ll9 IQ]41fn]1YO
11))-fJIIOUnliO
Ol -)Lecl( )lf l )orut
01 -OJifl(ljI ) NIIq)Q
Ol -Md(PmiddotpoundlI)OUIIpU)
Ol -Md( I )O
II -~~~-l f(~)OIWI
01 -IUUIlf (q)Ollel
111 ) lljd)J110middotUmiddot)0
Ul)l lfllld()JIj)llfUmiddotl)I U
01 -w10
01 -OJif1UI( I )ONII
P) lWqOJO)IP0bullpoundpound
l l l ) llfl lld lAlMCI )Il11
~middot lll)l~jlfdlAIIqmiddotUmiddot0
OS l-lfdoHJifOI4 01 -NiqOJO)IPIIIII 01 Jllj)I)Aulf4middot1Aui~Jbull bull
01 l)aulbull l lldiposoJlUmiddotI
OS 1--PIAbullIl_middot l middotOJ1)U)Qbull9t
OS au10JIUmiddott
Ol J lbulllWIfltllmiddotl~JO)IOmiddott
01 lll)llflfdAij11 )0
_)OIOJI)U)Qmiddottl
0) UljONiqjQ
os bull-fdonu os _lfdoJI UOmiddot middotz
_lry IU1Y OU1Y 6lS1Y n AIOUIOIYl 1101Ul0l Jl4WYS l fSn 0[51Y J8WII JldWS
tlSlY middoto11 CIS SSOI =nn u --o 1 1 1100 -s til OJOq1llluAj lllo U )Ji tQ uu
~ ~--~----4--===================- middot middotc~-====================--_j
- barcode 555910
- barcodetext SDMS Doc ID 555910
Mr Dennis Gagne July 24 1990 Page Six Revised August 10 1990
H-0-7-24
Due to matrix spike recoveries less than ten percent the undetected phenol and 2-chlorophenol in aample AT5J1 will be rejected (R) bull The remaining compounds which did not meet matrix spike criteria were not detected in the original aamp1e therefore no action is required
Very truly yours
ROY F WESTON INC
~~ Zoe Horton Ot9anic Data Reviewer
~~tA-o ltA_
Cheryl Blaine
~~~middotFmiddot-Tea Manager ESAT Reqion I
Zh Enclosure(amp)
)
CnnEB GEOROB Case 14355
TABLE I - Recommendations Summary
amp llli A
AT528 A A A AT529 A A A AT530 A A A AT531 A AA
A Accept all data
Accept the reaulta for the aaaple but eatiaate the non-detected 1 1-dichloroethane since calishybration criteria waa not aet Inatruaent rashyaponae to thia coapound ia not atable therefore quantitation aay be affected
Accept the reaulta for the aaaple but reject (R) the undetected phenol and 2-chlorophenol due to low aatrix spike duplicate recoveriea Thia aay indicate that in the original aaaple theae acid coapounda vera not recovered accurately during extraction poaaibly resulting in falae negatives
Charibullbull Georqe Table II - Tentatively Identified Compoundbull (TICbull) awamary
AT529
FURAN TETRAHYDRO
X - CoJapound was detected
)
Data s ummary Xey
A Acceptable data
J The associatec1 nWDerical value is an estimated quantity
R Rej act data due to qual ty control criteria The data are unusable (compound may or may not be present) Reaampl inq and reanalysis is necessary tor verification
u The compound was analyzed tor but was not detected The associated numerical value is the sample quantitation limit
UJ The coapound was analyzed tor but was not detected The saaple quantitfltion liait is an estiaated quantity
The capounc1 Vfla analyzed tor but waa not c1etected The saaple quantitation liait ia the same as the CRQL presentec1
CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL
ADMINISTRAT IVE RECORD
( ) 06ll9 lQDllflrf JnO 0616V9 oI6V9 0616119 06161 on-snvo
Ol bullbull bullbull m l-wJIICIIInliO
---------middotmiddotmiddot-------middotmiddotmiddotmiddot--middotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddot bull-IAJ1 101
-bullbulln -NIIIIAtt11
-bulln-oIO)JUOLmiddotll ll wbullbulln-o101J1bull1
-middotbullbull-z oa -wtd-z-14tt_
s 0middot-middotmiddot S tuldoldDIOJI0-[ 1--bull1
_1011bull1 -l l l __IO__ o
-0-JO Ioi~ IJI
-diDIdDJOIol-10-[ 1-l -
OOIdDJO)IP0-l l
- 1-JoOIPIIIbullbullu l 1I IIV AIIA
111)) Jo0 )1PtJIIIUCiqJI]
_Joell lol-1bull1-1 1 1 _nz
- IOIO)Iol-0-ll
( )UOJ )-Ioll-oIO JI-10 bullll
-ot-oJOllol-10middot 1 1
-ot-oJOl l-10 -1 1
M) 0UDqJI]
JO )Ioll-l Aiol
01 PIJOIfl AIIJA
01 -~~~-middotmiddot 01 __Jo01]
l[SIY oun llSJY _ ~~~ d j JI
I[SIr oun
WI _11110A OIOQIeampAI~H)JIIQ
~
CHARLES GEORGE LAND RECLAMATION TRUS T LANDFI LL
AOHINISTRATI VE RECORD
()
ann usn oun
_11_
6lSU
lllnll middot[ -~O~Dl~WObulll
_~~~~~
middot~middotlbullllllod lllj~-
lll~liimiddotZ -1bull11~1fMuoH1Jrpz
1-pHIIPI~I -Sl loHIJII~~Imiddotl
-~ludoiHI)IPft
-~~~PMgtJAIIImiddotZ -lodIIII~ [ middot OHI)ICbull
-~~~IIQOHIJIPftOI
OII J)jueGHIJIQbull
_bull lfdtl
-n-qoo~OJIPI~I middottll
1-lfdioHI)II~IOmiddotl
-~~~-liiIOiji-HIIIO middotZgtbullIq
P71 ~011101
p~~ ~bullmiddotz
~---~bullu-z
~---middot -NiqO~I1
-1HIJIPObull
-IbullAdold-U-Pmiddot-~~11bull1
1-lfIIAIII
~bull1110 ( iildoJdoOjOHIIOmiddotl)Ojq
1-lod AII1middotl
-NiqOHI JIPI Omiddotll
10110~ jA NOI
-NOqOHI JIP0middot1
-laqiiIHI JIP 0middot [ 1
_- o z
~Otf10 (1Aij1MHii10middotllbull lq
lliMIIIoiOIAOIY1
MIUfXI1 Jl IZS OIIOS
w bull bull ~bullbulll~bulloo bullbullll
_
CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL
AOHINISTRATI VE RECORD
~----~__ filii
til
tltMoshy
( I
06R9bull 06ll9 I QJ131111] UYO 0616l9 0616l9 0616ll9 IQ]41fn]1YO
11))-fJIIOUnliO
Ol -)Lecl( )lf l )orut
01 -OJifl(ljI ) NIIq)Q
Ol -Md(PmiddotpoundlI)OUIIpU)
Ol -Md( I )O
II -~~~-l f(~)OIWI
01 -IUUIlf (q)Ollel
111 ) lljd)J110middotUmiddot)0
Ul)l lfllld()JIj)llfUmiddotl)I U
01 -w10
01 -OJif1UI( I )ONII
P) lWqOJO)IP0bullpoundpound
l l l ) llfl lld lAlMCI )Il11
~middot lll)l~jlfdlAIIqmiddotUmiddot0
OS l-lfdoHJifOI4 01 -NiqOJO)IPIIIII 01 Jllj)I)Aulf4middot1Aui~Jbull bull
01 l)aulbull l lldiposoJlUmiddotI
OS 1--PIAbullIl_middot l middotOJ1)U)Qbull9t
OS au10JIUmiddott
Ol J lbulllWIfltllmiddotl~JO)IOmiddott
01 lll)llflfdAij11 )0
_)OIOJI)U)Qmiddottl
0) UljONiqjQ
os bull-fdonu os _lfdoJI UOmiddot middotz
_lry IU1Y OU1Y 6lS1Y n AIOUIOIYl 1101Ul0l Jl4WYS l fSn 0[51Y J8WII JldWS
tlSlY middoto11 CIS SSOI =nn u --o 1 1 1100 -s til OJOq1llluAj lllo U )Ji tQ uu
~ ~--~----4--===================- middot middotc~-====================--_j
- barcode 555910
- barcodetext SDMS Doc ID 555910
)
CnnEB GEOROB Case 14355
TABLE I - Recommendations Summary
amp llli A
AT528 A A A AT529 A A A AT530 A A A AT531 A AA
A Accept all data
Accept the reaulta for the aaaple but eatiaate the non-detected 1 1-dichloroethane since calishybration criteria waa not aet Inatruaent rashyaponae to thia coapound ia not atable therefore quantitation aay be affected
Accept the reaulta for the aaaple but reject (R) the undetected phenol and 2-chlorophenol due to low aatrix spike duplicate recoveriea Thia aay indicate that in the original aaaple theae acid coapounda vera not recovered accurately during extraction poaaibly resulting in falae negatives
Charibullbull Georqe Table II - Tentatively Identified Compoundbull (TICbull) awamary
AT529
FURAN TETRAHYDRO
X - CoJapound was detected
)
Data s ummary Xey
A Acceptable data
J The associatec1 nWDerical value is an estimated quantity
R Rej act data due to qual ty control criteria The data are unusable (compound may or may not be present) Reaampl inq and reanalysis is necessary tor verification
u The compound was analyzed tor but was not detected The associated numerical value is the sample quantitation limit
UJ The coapound was analyzed tor but was not detected The saaple quantitfltion liait is an estiaated quantity
The capounc1 Vfla analyzed tor but waa not c1etected The saaple quantitation liait ia the same as the CRQL presentec1
CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL
ADMINISTRAT IVE RECORD
( ) 06ll9 lQDllflrf JnO 0616V9 oI6V9 0616119 06161 on-snvo
Ol bullbull bullbull m l-wJIICIIInliO
---------middotmiddotmiddot-------middotmiddotmiddotmiddot--middotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddot bull-IAJ1 101
-bullbulln -NIIIIAtt11
-bulln-oIO)JUOLmiddotll ll wbullbulln-o101J1bull1
-middotbullbull-z oa -wtd-z-14tt_
s 0middot-middotmiddot S tuldoldDIOJI0-[ 1--bull1
_1011bull1 -l l l __IO__ o
-0-JO Ioi~ IJI
-diDIdDJOIol-10-[ 1-l -
OOIdDJO)IP0-l l
- 1-JoOIPIIIbullbullu l 1I IIV AIIA
111)) Jo0 )1PtJIIIUCiqJI]
_Joell lol-1bull1-1 1 1 _nz
- IOIO)Iol-0-ll
( )UOJ )-Ioll-oIO JI-10 bullll
-ot-oJOllol-10middot 1 1
-ot-oJOl l-10 -1 1
M) 0UDqJI]
JO )Ioll-l Aiol
01 PIJOIfl AIIJA
01 -~~~-middotmiddot 01 __Jo01]
l[SIY oun llSJY _ ~~~ d j JI
I[SIr oun
WI _11110A OIOQIeampAI~H)JIIQ
~
CHARLES GEORGE LAND RECLAMATION TRUS T LANDFI LL
AOHINISTRATI VE RECORD
()
ann usn oun
_11_
6lSU
lllnll middot[ -~O~Dl~WObulll
_~~~~~
middot~middotlbullllllod lllj~-
lll~liimiddotZ -1bull11~1fMuoH1Jrpz
1-pHIIPI~I -Sl loHIJII~~Imiddotl
-~ludoiHI)IPft
-~~~PMgtJAIIImiddotZ -lodIIII~ [ middot OHI)ICbull
-~~~IIQOHIJIPftOI
OII J)jueGHIJIQbull
_bull lfdtl
-n-qoo~OJIPI~I middottll
1-lfdioHI)II~IOmiddotl
-~~~-liiIOiji-HIIIO middotZgtbullIq
P71 ~011101
p~~ ~bullmiddotz
~---~bullu-z
~---middot -NiqO~I1
-1HIJIPObull
-IbullAdold-U-Pmiddot-~~11bull1
1-lfIIAIII
~bull1110 ( iildoJdoOjOHIIOmiddotl)Ojq
1-lod AII1middotl
-NiqOHI JIPI Omiddotll
10110~ jA NOI
-NOqOHI JIP0middot1
-laqiiIHI JIP 0middot [ 1
_- o z
~Otf10 (1Aij1MHii10middotllbull lq
lliMIIIoiOIAOIY1
MIUfXI1 Jl IZS OIIOS
w bull bull ~bullbulll~bulloo bullbullll
_
CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL
AOHINISTRATI VE RECORD
~----~__ filii
til
tltMoshy
( I
06R9bull 06ll9 I QJ131111] UYO 0616l9 0616l9 0616ll9 IQ]41fn]1YO
11))-fJIIOUnliO
Ol -)Lecl( )lf l )orut
01 -OJifl(ljI ) NIIq)Q
Ol -Md(PmiddotpoundlI)OUIIpU)
Ol -Md( I )O
II -~~~-l f(~)OIWI
01 -IUUIlf (q)Ollel
111 ) lljd)J110middotUmiddot)0
Ul)l lfllld()JIj)llfUmiddotl)I U
01 -w10
01 -OJif1UI( I )ONII
P) lWqOJO)IP0bullpoundpound
l l l ) llfl lld lAlMCI )Il11
~middot lll)l~jlfdlAIIqmiddotUmiddot0
OS l-lfdoHJifOI4 01 -NiqOJO)IPIIIII 01 Jllj)I)Aulf4middot1Aui~Jbull bull
01 l)aulbull l lldiposoJlUmiddotI
OS 1--PIAbullIl_middot l middotOJ1)U)Qbull9t
OS au10JIUmiddott
Ol J lbulllWIfltllmiddotl~JO)IOmiddott
01 lll)llflfdAij11 )0
_)OIOJI)U)Qmiddottl
0) UljONiqjQ
os bull-fdonu os _lfdoJI UOmiddot middotz
_lry IU1Y OU1Y 6lS1Y n AIOUIOIYl 1101Ul0l Jl4WYS l fSn 0[51Y J8WII JldWS
tlSlY middoto11 CIS SSOI =nn u --o 1 1 1100 -s til OJOq1llluAj lllo U )Ji tQ uu
~ ~--~----4--===================- middot middotc~-====================--_j
- barcode 555910
- barcodetext SDMS Doc ID 555910
Charibullbull Georqe Table II - Tentatively Identified Compoundbull (TICbull) awamary
AT529
FURAN TETRAHYDRO
X - CoJapound was detected
)
Data s ummary Xey
A Acceptable data
J The associatec1 nWDerical value is an estimated quantity
R Rej act data due to qual ty control criteria The data are unusable (compound may or may not be present) Reaampl inq and reanalysis is necessary tor verification
u The compound was analyzed tor but was not detected The associated numerical value is the sample quantitation limit
UJ The coapound was analyzed tor but was not detected The saaple quantitfltion liait is an estiaated quantity
The capounc1 Vfla analyzed tor but waa not c1etected The saaple quantitation liait ia the same as the CRQL presentec1
CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL
ADMINISTRAT IVE RECORD
( ) 06ll9 lQDllflrf JnO 0616V9 oI6V9 0616119 06161 on-snvo
Ol bullbull bullbull m l-wJIICIIInliO
---------middotmiddotmiddot-------middotmiddotmiddotmiddot--middotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddot bull-IAJ1 101
-bullbulln -NIIIIAtt11
-bulln-oIO)JUOLmiddotll ll wbullbulln-o101J1bull1
-middotbullbull-z oa -wtd-z-14tt_
s 0middot-middotmiddot S tuldoldDIOJI0-[ 1--bull1
_1011bull1 -l l l __IO__ o
-0-JO Ioi~ IJI
-diDIdDJOIol-10-[ 1-l -
OOIdDJO)IP0-l l
- 1-JoOIPIIIbullbullu l 1I IIV AIIA
111)) Jo0 )1PtJIIIUCiqJI]
_Joell lol-1bull1-1 1 1 _nz
- IOIO)Iol-0-ll
( )UOJ )-Ioll-oIO JI-10 bullll
-ot-oJOllol-10middot 1 1
-ot-oJOl l-10 -1 1
M) 0UDqJI]
JO )Ioll-l Aiol
01 PIJOIfl AIIJA
01 -~~~-middotmiddot 01 __Jo01]
l[SIY oun llSJY _ ~~~ d j JI
I[SIr oun
WI _11110A OIOQIeampAI~H)JIIQ
~
CHARLES GEORGE LAND RECLAMATION TRUS T LANDFI LL
AOHINISTRATI VE RECORD
()
ann usn oun
_11_
6lSU
lllnll middot[ -~O~Dl~WObulll
_~~~~~
middot~middotlbullllllod lllj~-
lll~liimiddotZ -1bull11~1fMuoH1Jrpz
1-pHIIPI~I -Sl loHIJII~~Imiddotl
-~ludoiHI)IPft
-~~~PMgtJAIIImiddotZ -lodIIII~ [ middot OHI)ICbull
-~~~IIQOHIJIPftOI
OII J)jueGHIJIQbull
_bull lfdtl
-n-qoo~OJIPI~I middottll
1-lfdioHI)II~IOmiddotl
-~~~-liiIOiji-HIIIO middotZgtbullIq
P71 ~011101
p~~ ~bullmiddotz
~---~bullu-z
~---middot -NiqO~I1
-1HIJIPObull
-IbullAdold-U-Pmiddot-~~11bull1
1-lfIIAIII
~bull1110 ( iildoJdoOjOHIIOmiddotl)Ojq
1-lod AII1middotl
-NiqOHI JIPI Omiddotll
10110~ jA NOI
-NOqOHI JIP0middot1
-laqiiIHI JIP 0middot [ 1
_- o z
~Otf10 (1Aij1MHii10middotllbull lq
lliMIIIoiOIAOIY1
MIUfXI1 Jl IZS OIIOS
w bull bull ~bullbulll~bulloo bullbullll
_
CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL
AOHINISTRATI VE RECORD
~----~__ filii
til
tltMoshy
( I
06R9bull 06ll9 I QJ131111] UYO 0616l9 0616l9 0616ll9 IQ]41fn]1YO
11))-fJIIOUnliO
Ol -)Lecl( )lf l )orut
01 -OJifl(ljI ) NIIq)Q
Ol -Md(PmiddotpoundlI)OUIIpU)
Ol -Md( I )O
II -~~~-l f(~)OIWI
01 -IUUIlf (q)Ollel
111 ) lljd)J110middotUmiddot)0
Ul)l lfllld()JIj)llfUmiddotl)I U
01 -w10
01 -OJif1UI( I )ONII
P) lWqOJO)IP0bullpoundpound
l l l ) llfl lld lAlMCI )Il11
~middot lll)l~jlfdlAIIqmiddotUmiddot0
OS l-lfdoHJifOI4 01 -NiqOJO)IPIIIII 01 Jllj)I)Aulf4middot1Aui~Jbull bull
01 l)aulbull l lldiposoJlUmiddotI
OS 1--PIAbullIl_middot l middotOJ1)U)Qbull9t
OS au10JIUmiddott
Ol J lbulllWIfltllmiddotl~JO)IOmiddott
01 lll)llflfdAij11 )0
_)OIOJI)U)Qmiddottl
0) UljONiqjQ
os bull-fdonu os _lfdoJI UOmiddot middotz
_lry IU1Y OU1Y 6lS1Y n AIOUIOIYl 1101Ul0l Jl4WYS l fSn 0[51Y J8WII JldWS
tlSlY middoto11 CIS SSOI =nn u --o 1 1 1100 -s til OJOq1llluAj lllo U )Ji tQ uu
~ ~--~----4--===================- middot middotc~-====================--_j
- barcode 555910
- barcodetext SDMS Doc ID 555910
)
Data s ummary Xey
A Acceptable data
J The associatec1 nWDerical value is an estimated quantity
R Rej act data due to qual ty control criteria The data are unusable (compound may or may not be present) Reaampl inq and reanalysis is necessary tor verification
u The compound was analyzed tor but was not detected The associated numerical value is the sample quantitation limit
UJ The coapound was analyzed tor but was not detected The saaple quantitfltion liait is an estiaated quantity
The capounc1 Vfla analyzed tor but waa not c1etected The saaple quantitation liait ia the same as the CRQL presentec1
CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL
ADMINISTRAT IVE RECORD
( ) 06ll9 lQDllflrf JnO 0616V9 oI6V9 0616119 06161 on-snvo
Ol bullbull bullbull m l-wJIICIIInliO
---------middotmiddotmiddot-------middotmiddotmiddotmiddot--middotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddot bull-IAJ1 101
-bullbulln -NIIIIAtt11
-bulln-oIO)JUOLmiddotll ll wbullbulln-o101J1bull1
-middotbullbull-z oa -wtd-z-14tt_
s 0middot-middotmiddot S tuldoldDIOJI0-[ 1--bull1
_1011bull1 -l l l __IO__ o
-0-JO Ioi~ IJI
-diDIdDJOIol-10-[ 1-l -
OOIdDJO)IP0-l l
- 1-JoOIPIIIbullbullu l 1I IIV AIIA
111)) Jo0 )1PtJIIIUCiqJI]
_Joell lol-1bull1-1 1 1 _nz
- IOIO)Iol-0-ll
( )UOJ )-Ioll-oIO JI-10 bullll
-ot-oJOllol-10middot 1 1
-ot-oJOl l-10 -1 1
M) 0UDqJI]
JO )Ioll-l Aiol
01 PIJOIfl AIIJA
01 -~~~-middotmiddot 01 __Jo01]
l[SIY oun llSJY _ ~~~ d j JI
I[SIr oun
WI _11110A OIOQIeampAI~H)JIIQ
~
CHARLES GEORGE LAND RECLAMATION TRUS T LANDFI LL
AOHINISTRATI VE RECORD
()
ann usn oun
_11_
6lSU
lllnll middot[ -~O~Dl~WObulll
_~~~~~
middot~middotlbullllllod lllj~-
lll~liimiddotZ -1bull11~1fMuoH1Jrpz
1-pHIIPI~I -Sl loHIJII~~Imiddotl
-~ludoiHI)IPft
-~~~PMgtJAIIImiddotZ -lodIIII~ [ middot OHI)ICbull
-~~~IIQOHIJIPftOI
OII J)jueGHIJIQbull
_bull lfdtl
-n-qoo~OJIPI~I middottll
1-lfdioHI)II~IOmiddotl
-~~~-liiIOiji-HIIIO middotZgtbullIq
P71 ~011101
p~~ ~bullmiddotz
~---~bullu-z
~---middot -NiqO~I1
-1HIJIPObull
-IbullAdold-U-Pmiddot-~~11bull1
1-lfIIAIII
~bull1110 ( iildoJdoOjOHIIOmiddotl)Ojq
1-lod AII1middotl
-NiqOHI JIPI Omiddotll
10110~ jA NOI
-NOqOHI JIP0middot1
-laqiiIHI JIP 0middot [ 1
_- o z
~Otf10 (1Aij1MHii10middotllbull lq
lliMIIIoiOIAOIY1
MIUfXI1 Jl IZS OIIOS
w bull bull ~bullbulll~bulloo bullbullll
_
CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL
AOHINISTRATI VE RECORD
~----~__ filii
til
tltMoshy
( I
06R9bull 06ll9 I QJ131111] UYO 0616l9 0616l9 0616ll9 IQ]41fn]1YO
11))-fJIIOUnliO
Ol -)Lecl( )lf l )orut
01 -OJifl(ljI ) NIIq)Q
Ol -Md(PmiddotpoundlI)OUIIpU)
Ol -Md( I )O
II -~~~-l f(~)OIWI
01 -IUUIlf (q)Ollel
111 ) lljd)J110middotUmiddot)0
Ul)l lfllld()JIj)llfUmiddotl)I U
01 -w10
01 -OJif1UI( I )ONII
P) lWqOJO)IP0bullpoundpound
l l l ) llfl lld lAlMCI )Il11
~middot lll)l~jlfdlAIIqmiddotUmiddot0
OS l-lfdoHJifOI4 01 -NiqOJO)IPIIIII 01 Jllj)I)Aulf4middot1Aui~Jbull bull
01 l)aulbull l lldiposoJlUmiddotI
OS 1--PIAbullIl_middot l middotOJ1)U)Qbull9t
OS au10JIUmiddott
Ol J lbulllWIfltllmiddotl~JO)IOmiddott
01 lll)llflfdAij11 )0
_)OIOJI)U)Qmiddottl
0) UljONiqjQ
os bull-fdonu os _lfdoJI UOmiddot middotz
_lry IU1Y OU1Y 6lS1Y n AIOUIOIYl 1101Ul0l Jl4WYS l fSn 0[51Y J8WII JldWS
tlSlY middoto11 CIS SSOI =nn u --o 1 1 1100 -s til OJOq1llluAj lllo U )Ji tQ uu
~ ~--~----4--===================- middot middotc~-====================--_j
- barcode 555910
- barcodetext SDMS Doc ID 555910
CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL
ADMINISTRAT IVE RECORD
( ) 06ll9 lQDllflrf JnO 0616V9 oI6V9 0616119 06161 on-snvo
Ol bullbull bullbull m l-wJIICIIInliO
---------middotmiddotmiddot-------middotmiddotmiddotmiddot--middotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddot bull-IAJ1 101
-bullbulln -NIIIIAtt11
-bulln-oIO)JUOLmiddotll ll wbullbulln-o101J1bull1
-middotbullbull-z oa -wtd-z-14tt_
s 0middot-middotmiddot S tuldoldDIOJI0-[ 1--bull1
_1011bull1 -l l l __IO__ o
-0-JO Ioi~ IJI
-diDIdDJOIol-10-[ 1-l -
OOIdDJO)IP0-l l
- 1-JoOIPIIIbullbullu l 1I IIV AIIA
111)) Jo0 )1PtJIIIUCiqJI]
_Joell lol-1bull1-1 1 1 _nz
- IOIO)Iol-0-ll
( )UOJ )-Ioll-oIO JI-10 bullll
-ot-oJOllol-10middot 1 1
-ot-oJOl l-10 -1 1
M) 0UDqJI]
JO )Ioll-l Aiol
01 PIJOIfl AIIJA
01 -~~~-middotmiddot 01 __Jo01]
l[SIY oun llSJY _ ~~~ d j JI
I[SIr oun
WI _11110A OIOQIeampAI~H)JIIQ
~
CHARLES GEORGE LAND RECLAMATION TRUS T LANDFI LL
AOHINISTRATI VE RECORD
()
ann usn oun
_11_
6lSU
lllnll middot[ -~O~Dl~WObulll
_~~~~~
middot~middotlbullllllod lllj~-
lll~liimiddotZ -1bull11~1fMuoH1Jrpz
1-pHIIPI~I -Sl loHIJII~~Imiddotl
-~ludoiHI)IPft
-~~~PMgtJAIIImiddotZ -lodIIII~ [ middot OHI)ICbull
-~~~IIQOHIJIPftOI
OII J)jueGHIJIQbull
_bull lfdtl
-n-qoo~OJIPI~I middottll
1-lfdioHI)II~IOmiddotl
-~~~-liiIOiji-HIIIO middotZgtbullIq
P71 ~011101
p~~ ~bullmiddotz
~---~bullu-z
~---middot -NiqO~I1
-1HIJIPObull
-IbullAdold-U-Pmiddot-~~11bull1
1-lfIIAIII
~bull1110 ( iildoJdoOjOHIIOmiddotl)Ojq
1-lod AII1middotl
-NiqOHI JIPI Omiddotll
10110~ jA NOI
-NOqOHI JIP0middot1
-laqiiIHI JIP 0middot [ 1
_- o z
~Otf10 (1Aij1MHii10middotllbull lq
lliMIIIoiOIAOIY1
MIUfXI1 Jl IZS OIIOS
w bull bull ~bullbulll~bulloo bullbullll
_
CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL
AOHINISTRATI VE RECORD
~----~__ filii
til
tltMoshy
( I
06R9bull 06ll9 I QJ131111] UYO 0616l9 0616l9 0616ll9 IQ]41fn]1YO
11))-fJIIOUnliO
Ol -)Lecl( )lf l )orut
01 -OJifl(ljI ) NIIq)Q
Ol -Md(PmiddotpoundlI)OUIIpU)
Ol -Md( I )O
II -~~~-l f(~)OIWI
01 -IUUIlf (q)Ollel
111 ) lljd)J110middotUmiddot)0
Ul)l lfllld()JIj)llfUmiddotl)I U
01 -w10
01 -OJif1UI( I )ONII
P) lWqOJO)IP0bullpoundpound
l l l ) llfl lld lAlMCI )Il11
~middot lll)l~jlfdlAIIqmiddotUmiddot0
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~ ~--~----4--===================- middot middotc~-====================--_j
- barcode 555910
- barcodetext SDMS Doc ID 555910
CHARLES GEORGE LAND RECLAMATION TRUS T LANDFI LL
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CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL
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OS l-lfdoHJifOI4 01 -NiqOJO)IPIIIII 01 Jllj)I)Aulf4middot1Aui~Jbull bull
01 l)aulbull l lldiposoJlUmiddotI
OS 1--PIAbullIl_middot l middotOJ1)U)Qbull9t
OS au10JIUmiddott
Ol J lbulllWIfltllmiddotl~JO)IOmiddott
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tlSlY middoto11 CIS SSOI =nn u --o 1 1 1100 -s til OJOq1llluAj lllo U )Ji tQ uu
~ ~--~----4--===================- middot middotc~-====================--_j
- barcode 555910
- barcodetext SDMS Doc ID 555910
_
CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL
AOHINISTRATI VE RECORD
~----~__ filii
til
tltMoshy
( I
06R9bull 06ll9 I QJ131111] UYO 0616l9 0616l9 0616ll9 IQ]41fn]1YO
11))-fJIIOUnliO
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01 -OJifl(ljI ) NIIq)Q
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Ol -Md( I )O
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01 -w10
01 -OJif1UI( I )ONII
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l l l ) llfl lld lAlMCI )Il11
~middot lll)l~jlfdlAIIqmiddotUmiddot0
OS l-lfdoHJifOI4 01 -NiqOJO)IPIIIII 01 Jllj)I)Aulf4middot1Aui~Jbull bull
01 l)aulbull l lldiposoJlUmiddotI
OS 1--PIAbullIl_middot l middotOJ1)U)Qbull9t
OS au10JIUmiddott
Ol J lbulllWIfltllmiddotl~JO)IOmiddott
01 lll)llflfdAij11 )0
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0) UljONiqjQ
os bull-fdonu os _lfdoJI UOmiddot middotz
_lry IU1Y OU1Y 6lS1Y n AIOUIOIYl 1101Ul0l Jl4WYS l fSn 0[51Y J8WII JldWS
tlSlY middoto11 CIS SSOI =nn u --o 1 1 1100 -s til OJOq1llluAj lllo U )Ji tQ uu
~ ~--~----4--===================- middot middotc~-====================--_j
- barcode 555910
- barcodetext SDMS Doc ID 555910