dr. m. shahid, · fig. crystal structure of the novel organotin(iv) compound, fig. mossbauer...

12
Dr. M. SHAHID, Assistant Professor Department of Chemistry, AMU, Aligarh, India Residence: Flat No. 11, Aisha Apartments Opp. S.S. House, ADM compound, Aligarh Mobile: +91 9359264128 Ph. 0571-2700920 (ext) 3350 E -Mail: [email protected] Educational Qualifications Ph.D. in Inorganic Chemistry from AMU, Aligarh in 2011. M.Sc. in Chemistry from CSJM Kanpur with First division and First position. B.Sc. in Chemistry (with Physics & Maths) from CSJM Kanpur with First Division. Intermediate (Maths) from UPB with First Divisions & Distinctions. High Schooling from UPB with First Divisions & Distinctions. Junior Research Fellowship & National Eligibility Test (JRF-NET) organized by CSIR-UGC in 2009. Graduate Aptitude Test in Engineering (GATE) organized by IIT Kanpur in 2007. Selected Achievements & Awards Fast Track Young Scientist awarded by SERB-DST, New Delhi, 2012. Research Associate awarded by CSIR, New Delhi, 2012. Certificate of Appreciation in online competition of Kepler’s Mission, NASA, USA, 2009. Affiliate Member, Royal Society of Chemistry (AMRSC), London. Member- American Chemical Society (ACS), Inorganic Chemistry Division. Member, Editorial Board, Pharmacologia: A Science Magazine, London, UK. Academic Editor of PLOS ONE, an international Journal of repute. Associate Editor: International Journal of Chemical Synthesis and Reactions (ChemPub) Member-Editorial Board: Journal of Transition Metal Complexes IASc-INSA-NASI fellowship awarded by Indian Academy of Science, 2015. Teaching Experience Guest Lecturer July 2003-May 2005, Govt. Polytechnic, UPTU, Hardoi. Guest Lecturer July 2010- March 2011, Department of Chemistry, AMU, Aligarh Assistant Professor (AdHoc) Sep 2011- Oct 2011, Department of Chemistry, AMU, Aligarh Guest Lecturer Oct 2011- March 2012, Department of Chemistry, AMU, Aligarh Assistant Professor (AdHoc) Aug 2012- Sep 2012, Department of Chemistry, AMU, Aligarh Guest Lecturer Sep 2012 – Sep 2013, Department of Chemistry, AMU, Aligarh Assistant Professor (AdHoc) Aug 2013 – Sep 2013, Department of Chemistry, AMU, Aligarh Guest Lecturer Sep 2013- Jan 2014, Department of Chemistry, AMU, Aligarh Assistant Professor Feb 2014- onwards, Department of Chemistry, AMU, Aligarh Courses taught: B.Sc. - Advanced Organic and Inorganic Chemistry,

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Page 1: Dr. M. SHAHID, · Fig. Crystal structure of the novel organotin(IV) compound, Fig. Mossbauer Spectra of a bimetallic complex at RT & LNT a potential antitumor agent isolated by Dr

Dr M SHAHID Assistant Professor Department of Chemistry AMU Aligarh India

Residence Flat No 11 Aisha Apartments Opp SS House ADM compound Aligarh Mobile +91 9359264128 Ph 0571-2700920 (ext) 3350 E -Mail shahid81chemgmailcom Educational Qualifications

PhD in Inorganic Chemistry from AMU Aligarh in 2011 MSc in Chemistry from CSJM Kanpur with First division and First position BSc in Chemistry (with Physics amp Maths) from CSJM Kanpur with First Division Intermediate (Maths) from UPB with First Divisions amp Distinctions High Schooling from UPB with First Divisions amp Distinctions Junior Research Fellowship amp National Eligibility Test (JRF-NET) organized by CSIR-UGC in 2009 Graduate Aptitude Test in Engineering (GATE) organized by IIT Kanpur in 2007

Selected Achievements amp Awards

Fast Track Young Scientist awarded by SERB-DST New Delhi 2012 Research Associate awarded by CSIR New Delhi 2012 Certificate of Appreciation in online competition of Keplerrsquos Mission NASA USA 2009 Affiliate Member Royal Society of Chemistry (AMRSC) London Member- American Chemical Society (ACS) Inorganic Chemistry Division Member Editorial Board Pharmacologia A Science Magazine London UK Academic Editor of PLOS ONE an international Journal of repute Associate Editor International Journal of Chemical Synthesis and Reactions (ChemPub) Member-Editorial Board Journal of Transition Metal Complexes IASc-INSA-NASI fellowship awarded by Indian Academy of Science 2015

Teaching Experience

Guest Lecturer July 2003-May 2005 Govt Polytechnic UPTU Hardoi Guest Lecturer July 2010- March 2011 Department of Chemistry AMU Aligarh Assistant Professor (AdHoc) Sep 2011- Oct 2011 Department of Chemistry AMU Aligarh Guest Lecturer Oct 2011- March 2012 Department of Chemistry AMU Aligarh Assistant Professor (AdHoc) Aug 2012- Sep 2012 Department of Chemistry AMU Aligarh Guest Lecturer Sep 2012 ndash Sep 2013 Department of Chemistry AMU Aligarh Assistant Professor (AdHoc) Aug 2013 ndash Sep 2013 Department of Chemistry AMU Aligarh Guest Lecturer Sep 2013- Jan 2014 Department of Chemistry AMU Aligarh Assistant Professor Feb 2014- onwards Department of Chemistry AMU Aligarh

Courses taught BSc - Advanced Organic and Inorganic Chemistry

MSc - Ist semester-Inorganic Reaction Mechanism MSc - IIIrd Semester- Organometallic Chemistry

Fellowships availed

Junior Research Fellowship (JRF) by UGC from Oct 2009 to July 2010 UGC fellowship for central Universities from 2007 to Sep 2009

Research Profile

Summary of PhD work

Title of Thesis Synthesis amp Physico-chemical Investigations of Binary and Ternary Complexes of Metal Ions Mentor Prof Zafar A Siddiqi Significant outcomes

The chemistry of functionalized polycarboxylic acid and their binary and ternary complexes of metal ions has been taken under investigation The coordination chemistry of functionalized polycarboxylic acid ligands viz pyridinedicarboxylic acid (H2pda) iminodiacetic acid (H2imda) oxydiacetic acid (H2oda) or nitrilotriacetic acid (H3nta) has attracted special focus of inorganic and bioinorganic chemists over the past decades These ligands are very important tridentate chelating agents The flexibility of these ligands makes them useful for the formation of the complexes differing in coordination numbers conformations and 3-D architectures It is well known that in binary and ternary mixed ligand metal carboxylate complexes the carboxylate ligands play an important role to construct novel metal-organic frame works (MOFs) and supramolecular frameworks

Fig (a) A supramolecular network of the complex [Cu(IDA)(Phen)H2O]2H2O constructed from H-bonding (b) Two layers of the complex showing πndashπ interactions between phenanthroline rings and forming a supramolecular framework [Eur J Med Chem 44 (2009) 2517ndash2522]

I during my PhD focused on the study and design of mixed-ligand ternary metal iminodiacetate

complexes and their possible structural diversities and to pursue in-vitro antimicrobial antitumoral and superoxide dismutase (SOD) activities Ternary complexes of iminodiacetate containing an α-diimine as

auxiliary ligand have been widely used as models for several mono and polynuclear metal-enzymes and therefore I have concentrated on the synthesis characterization and the structure-activity correlations of the mixed ligand complexes of transition lanthanide and tin metal ions Moreover due to the flexible nature of iminodiacetic acid ligand we have investigated various H-bonding and π-π interactions existing in these complexes which result in 1D 2D and 3D supramolecular network These supramolecular networks have been characterized using X-ray crystallography

Fig Crystal structure of the novel organotin(IV) compound Fig Mossbauer Spectra of a bimetallic complex at RT amp LNT a potential antitumor agent isolated by Dr Shahid [J Organomet Chem 694 (2009) 3768ndash3774]

Fig Crystal structure of 1D coordination polymeric structure of [Cu(dipic)(4-picoline)]n isolated by us [Eur J Med Chem 45 (2010) 264ndash269]

Fig Crystal structure of the dinuclear complex Fig Crystal structure of 1D coordination polymeric structure of (colouring scheme by symmetry equivalence) isolated [Cu(2-pa)2]middot2H2On isolated by us [Eur J Med Chem 57(2012) 102] by us [Spectrochim Acta Part A 93 (2012) 280]

Current Research Interests

Designing and magnetic studies of Molecule Based MAGNETS called Single Molecule Magnets (SMMs) having High Spin and Large Anisotropy Such molecules show slow relaxation of magnetization amp also QTM and can be used for Data Storage and Quantum Computations

Designing of Molecular Magnetic Coolants or Refrigerants These are the molecules which show Magneto-Caloric Effects (MCE) at low temperature and can be used to produce cooling

Synthesis of polynuclear metal clusters of 3d 3d-4f and 4f metal ions and their Single crystal X-ray studies

Metal-Organic Frameworks (MOFs) and their applications in sensing and dye adsorption through molecular recognition

Luminescence and magnetic studies of transition metal and Lanthanide complexes

Research Project(s) completedongoing = 04

1 SERB-DST Fast Track Young Scientist Project of Rs 1835 Lac funded by SERB-DST New Delhi

(Title Coordination polymers as single molecule magnets (SMMs) Design magnetic properties structural and electrochemical investigations) (Duration 2012-2015) Completed

2 UGC Start Up Grant Project of Rs 6 Lac funded by UGC New Delhi

(Title Novel polynuclear metal clusters as single molecule magnets (SMMs) Synthesis structural characterization electrochemical and magnetic studies) (Duration 2014-2016) Completed

3 SERB-DST project under EMR (Individual Centric) Schemes for Faculty on Molecular coolers (2017-2020)

Title Exploring new molecular magnetic refrigerants with Cu-Gd systems Ongoing 4 ICMR major research Project (2019-2022)

Title Design of new molecules for neurodegenerative disease (eg Alzeimerrsquos Parkinsonrsquos Disease)

Ongoing

List of International Publications

Published = 70 2020

1 Exploring catecholase activity in dinuclear Mn(II) and Cu(II) complexes An experimental and theoretical approach M S Ahmad M Khalid M S Khan M Shahid M Ahmad Monika A Ansari M Ashafaq New J Chem 2020 Accepted

2 Catalytic activity of Mn(III) and Co(III) complexes Evaluation of catechol oxidase enzymatic and photodegradation property M S Khan M Khalid M S Ahmad M Shahid M Ahmad Res Chem Inter 2020 accepted

3 A novel self-assembly NaCu12Zn4 as a multifunctional material First report of a discrete coordination compound for detection of Ca2+ ion and selective adsorption of cationic dye in water Khushboo Iman M Shahid and Musheer Ahmad Dalton Trans (RSC) 2020 Just Accepted (IF = 40)

4 Two dimensional (2D) molecular frameworks for rapid and selective adsorption of hazardous aromatic dyes from aqueous phase Mantasha I Sameer Hussain Musheer Ahmad M Shahid Sep Pur Tech (Elsevier) 2020 Accepted (IF = 52)

5 Exploring solvent dependent catecholase activity in transition metal complexes An experimental and theoretical approach Mantasha I M Shahid A Ansari M Kumar M N Akhtar M A AlDamen You Song M Ahmad New J Chem 2020 Just Accepted

6 Effect of cabergoline on cognitive impairments in transgenic Drosophila model of Parkinsonrsquos Disease Y H Siddique M Shahid Lett Drug Des Discov 2020 Accepted

2019

7 Topology magnetism and dye adsorption properties of metal organic frameworks (MOFs) synthesized from bench chemicals K Iman M Shahid M S Khan M Ahmad and F Sama CrystEngComm 2019 Accepted DOI 101039C9CE01041F

8 Three-in-one is really better Exploring sensing and adsorption properties in a newly designed metal-organic system incorporating copper(II) ion M S Khan M Khalid M S Ahmad M Shahid M Ahmad Dalton Trans 2019 Accepted

9 Synthesis characterization theoretical studies and catecholase like activities of [MO6] type complexes M N Ahamad M Kumar A Ansari Mantasha I M Ahmad M Shahid New J Chem 2019 Accepted

10 Tetrazole based porous metal organic framework (MOF) topological analysis and dye adsorption properties Abeda Mariyam M Shahid Mantasha I M Shahnawaz Khan M Shahwaz Ahmad J Inorg Organomet Poly Mat 2019 Accepted

11 Zein film functionalized with gold nanoparticles and the factors affecting its mechanical propertiesM Ajmal P Y A Jayaprakash S Ghosh V S Jaswal K SinghS Mandal M Shahid M Yadav S Das and P Kumar RSC Adv 2019 Accepted

12 A dinuclear paddle-wheel Cu(II) complex [Cu2(L)4(H2O)2]2H2O [HL=2(methoxycarbonyl)benzoic acid)] crystallographic magnetic and theoretical analysis F Vakil Mantasha I M Shahid M Ahmad J Struct Chem (Springer) Accepted 2019

13 Design and characterization of a Cu(II) coordination polymer based on a-diimine Evaluation of the biomimetic activity J Struct Chem Accepted 2019

14 Unprecedented isolation of a dinuclear tin(II) complex stabilized by pyridine-26-dimethanol structure DFT and in vitro screening of cytotoxic properties Mantasha I M K Raza M Shahid A Ansari M Ahmad I M Khan Applied Organomet Chem (Wiley) 2019 Accepted

15 A combined experimental and theoretical approach to structure magnetic properties and DNA binding affinity of a homodinuclear Cu(II) complex M N Ahamad M Shahid A Ansari M Kumar I M Khan M Ahmad Rahisuddin and R Arif New J Chem (RSC) 2019 Accepted 101039c9nj00228f

16 Cu(II) MOFs based on bipyridyls topology magnetism and exploring sensing ability towards multiple nitro aromatic explosives MOHD NAQI AHAMAD Mohammad Shahid Musheer Ahmad Farasha Sama ACS Omega2019447738-7749

17 Crystal engineering and magnetostructural properties of newly designed azideacetate bridged Mn12 coordination polymers Cryst Growth Des (ACS) 2019 accepted

18 Fe6 Cclusters of tripodal polyalcohol ligands synthesis structures and magnetostructural properties M Ashafaq M Khalid M Raizada M Shahid M Ahmad Polyhedron 2019 Just accepted

19 Life sensors Current advances in oxygen sensing by lanthanide complexes K Iman M Shahid New J Chem (Perspective) 2019 Accepted

20 Synthesis crystal structures photoluminescence magnetic and antioxidant properties and theoretical analysis of Zn(II) and Cu(II) complexes of an aminoalcohol ligand supported by benzoate counter anions Mantasha I M Shahid M Ahmad Rahisuddin R Arif S Tasneem F Sama I A Ansari New J Chem 2019 Accepted

21 Therapeutic potential of luteolin in transgenic Drosophila model of Alzheimerrsquos disease F Ali Rahul S Jyoti F Naz M Ashafaq M Shahid Y H Siddique Neuroscience Letters (Elsevier) 692 (2019) 90-99

22 Synthesis structure and DNA binding properties of a homodinuclear Cu(II) complex An experimental and theoretical approach Farasha Sama Mukul Raizada Mo Ashafaq M Naqi Ahamad Mantasha I Khushboo Iman M Shahid Rahisuddin Rizwan Arif Naseer A Shah Hatem AM Saleh J Mol Struct (Elsevier) 1176 (2019) 283-289

23 Synthesis spectral and crystallographic study DNA binding and molecular docking studies of homo dinuclear Co(II) and Ni(II) complexes M S Khan M Khalid M S Ahmad M Ahmad M Ashafaq Rahisuddin R Arif M Shahid J Mol Struct (Elsevier) 1175 (2019) 889-899

2018 24 Spectroscopic investigations on La3+ Pr3+ Nd3+ and Gd3+ complexes with a multidentate ligating system

Luminescence properties and biological activities M Shahid Armeen Siddique Mo Ashafaq Mukul Raizada Farasha Sama M Naqi Ahamad I Mantasha Istikhar A Ansari Ishaat M Khan Pankaj Kumar Kehkeshan Fatma Zafar A Siddiqi J Mol Struct (Elsevier) 1173 918-930

25 Synthesis structure and magnetic studies of lanthanide metalndashorganic frameworks (LnndashMOFs) Aqueous phase highly selective sensors for picric acid as well as the arsenic aion M Raizada F Sama M Ashafaq M Shahid M Khalid M Ahmad Z A Siddiqi Polyhedron (Elsevier) (2018) 139 131-141

26 Structural characterization magnetic studies and catecholase-like activities of Mn12 clusters M Ashafaq M Raizada M Khalid M Shahid M Ahmad Z A Siddiqi J Coord Chem 71 2018 2118

27 Synthesis molecular docking and DNA binding studies of phthalimide-based copper(II) complex In vitro antibacterial hemolytic and antioxidant assessment Rizwan Arif Pattan Sirajuddin Nayab Istikhar A Ansari M Shahid Mohammad Irfan Shadab Alam Mohammad Abid Rahisuddin J Mol Struct (Elsevier) 1160 (2018) 142-153

28 Experimental and theoretical characterization of organic salt 2-((4-bromophenyl)amino) pyrido[12- a ] quinoxalin-11-ium bromide monohydrate synthesized via oxidative cyclization MSH Faizi MJ Alam A Haque S Ahmad M Shahid M Ahmad J Mol Struct(Invited Article) 2018 1156 457-464

2017 29 A new hybrid material of polyoxovanadate-Cu complex with VmiddotmiddotmiddotH interactions and dual aqueous phase sensing

properties for picric acid as well as Pd2+ X-ray magnetic and theoretical studies and mechanistic insights of sensing M Raizada F Sama M Ashafaq M Shahid M Ahmad Z A Siddiqi J Mat Chem C (RSC) (2017) 69 (22) 3336-3353 IF = 53

30 A disc-like Co7 cluster with a solvent dependent catecholase activity MN Ahamad F Sama MN Akhtar YC Chen ML Tong M Ahmad New J Chem 2017 41 (23) 14057-14061

31 Spectral characterization crystal structures and biological activities of iminodiacetate ternary complexes M Shahid Anjuli Sana Tasneem Mantasha I M Naqi Ahamad Farasha Sama K Fatma Z A Siddiqi J Mol Struct 2017 1146 424

32 Amino alcohols and benzoates-Friends or foes Tuning nuclearity of Cu(II) complexes structures magnetism DFT and TD-DFT studies and catecholase like activities Farasha Sama Ashish Kumar Dhara Muhammad Nadeem Akhtar Yan-Cong Chen Ming-Liang Tong Istikhar A Ansari Mukul Raizada Musheer Ahmad M Shahid Zafar A Siddiqi Dalton Trans 2017 46 9801

33 Synthesis and spectral characterization of 2-((2-hydroxybenzylidene)amino)-2-methylpropane-13-diol derived complexes molecular docking and antimicrobial studies I A Ansari F Sama M Raizada M Shahid R K Rajpoot Z A Siddiqi J Mol Struct (Elsevier) 1127 (2017) 479-488

34 Design structures and study of non-covalent interactions of mono- di- and tetranuclear complexes of a bifurcated quadridentate tripod ligand N-(aminopropyl)-diethanolamine F Sama I A Ansari M Raizada M Ahmad C M Nagaraja M Shahid A Kumar K Khan Z A Siddiqi New J Chem (RSC) (2017) 41 (5) 1959-1972

35 Design structural characterization and catalytic activity of incomplete dicubane clusters of N-substituted diethanolamines F Sama I A Ansari M Raizada M Ahmad Mo Ashafaq M Shahid B Das K Shankar Z A Siddiqi J Cluster Sci (Springer) 2017 28 (3) 1355-1377

36 New phthalimide-appended Schiff bases Studies of DNA binding molecular docking and antioxidant activities P S Nayab Rahisuddin I A Ansari A Ali M Shahid Luminescence (Wiley) 2017 32 (5) 829-838

2016

37 Structurally well-characterized new multinuclear Cu(II) and Zn(II) clusters X-ray crystallography theoretical studies and applications in catalysis I A Ansari F Sama M Raizada M Shahid M Ahmad Z A Siddiqi New J Chem (RSC) 2016 40 9840-9852

38 Isolation of proton transfer complexes containing 4‒picolinium as cation and pyridine‒26ndashdicarboxylate complex as anion Crystallographic and spectral investigations antioxidant activities and molecular docking studies Istikhar A Ansari F Sama M Shahid Rahisuddin R Arif M Khalid and Z A Siddiqi RSC Adv (RSC) 2016 6 11088

39 Synthesis crystal structures and spectral characterization of Cu(II) and Mn(II) complexes of 4-hydroxy-3-methoxybenzaldehyde antioxidant properties and molecular docking studies I A Ansari F Sama M Shahid M Ahmad Rahisuddin P S Nayab Z A Siddiqi J Coord Chem (TampF) (2016) 69 3336ndash3353

40 Synthesis Spectral Characterization X-ray and Magnetic Studies of Oxo-bridged Tetranuclear Coordination Polymers of Cobalt I A Ansari F Sama M Shahid M Khalid P K Sharma M Ahmad amp Z A Siddiqi J Inorg Organom Polym Mat 26 (2016) 178

2015

41 Isolation and Spectral Characterization of Complexes [FeL1ClH2O] and [FeL2ClH2O] (H2L1=N-(3-hydroxy-propyl)-2-[(3-hydroxy-propylcarbamoyl)-methyl]-amino-acetamide and H2L2=N-(2-hydroxy-ethyl)-2-[2-hydroxy-ethylcarbamoyl)-methyl]-amino-acetamide) 57Fe Moumlssbauer and Cyclic Voltammetric Investigations M Shahid Anjuli Mukul Raizada Farasha Sama Istikhar A Ansari Mohd Khalid I M Khan M Ahmad ZA Siddiqi Can Chem Trans 3 (2015) 354

42 Synthesis crystal structures and genotoxic studies of cis-micro-12-peroxo dicobalt(III) complexes M Shahid Armeen Siddique Istikhar A Ansari Farasha Sama Sandesh Chibber Mohd Khalid Zafar A Siddiqi Md Serajul Haque Faizi J Coord Chem 68 (2015) 848

2014

43 N1-Phenyl-N4-[(quinolin-2-yl)methylidene]benzene-14-diamine MSH Faizi A Mashrai S Garandel M Shahid Acta Cryst (2014) E70 o905-906

44 2266-Tetrabromo-3445-tetramethoxycyclohexanone MSH Faizi A Mashrai M Shahid Acta Cryst (2014) E70 o826

45 N1-((1H-imidazol)methylene)-N4-phenylbenzene-14-diamine MSH Faizi A Mashrai M Shahid M Ahmad Acta Cryst (2014) E70 o806

46 Isolation of a decavanadate cluster [H2V10O28][4-picH]4bull2H2O (4-pic=4-picoline) Crystal structure electrochemical characterization genotoxic and antimicrobial studies M Shahid PK Sharma Anjuli S Chibber ZA Siddiqi J Cluster Science 2014 (in press)

47 Designing and characterization of Fe(III) complexes of oxydiacetate containing α-diimine as auxiliary ligand 57Fe-

Moumlssbauer and cyclic voltammetric studies M Shahid P K Sharma Z A Siddiqi F Sama I A Ansari M Khalid J Mol Structure 1063 (2014) 313

48 Synthesis and characterization of a carboxylate bridged homodinuclear Co(II) complex Crystal structure of [Co2(Pda)2(H2O)5]middot2H2O (H2Pda = pyridine-26-dicorboxylic acid) Z A Siddiqi I A Ansari F Sama M Shahid IJIRSET 3 (2014) 8673

2013

49 Synthesis crystal structure and magnetic studies of tetranuclear hydroxo and ligand bridged [Co4(micro3-OH)2(micro2-dea)2(L-L)4]4Clmiddot8H2O [L-L= 22prime- bipyridine or 110-phenanthroline] complexes with mixed valence defect dicubane core Z A Siddiqi A Siddique M Shahid M Khalid Anjuli P K Sharma M Ahmad S Kumar Y Lan A K Powell Dalton Trans 42 (2013) 9513-9522

50 Synthesis structural characterization DNA binding studies and antitumor properties of tin(II)-oxydiacetate complexes containing α-diimine as auxiliary ligand Z A Siddiqi P K Sharma M Shahid M Khalid J Photochem Photobiol B Biology 125 (2013) 171-175

51 Spectroscopic Luminescence electrochemical and antimicrobial studies of lanthanide complexes of bis-

benzimidazole derived ligands Z A Siddiqi Anjuli M Shahid M Khalid P K Sharma A Siddique J Mol Structure 1037 (2013) 402-411

52 Synthesis and structural characterization of homo-dinuclear complexes [M2(dea)2(H2O)4] [M2(dea)2(Bipy)2] and [Fe2(dea)2(H2O)2(Cl)2] (M = Co Ni or Cu H2dea = diethanolamine) 57Fe Moumlssbauer and electrochemical investigations Z A Siddiqi A Siddique M Shahid P K Sharma Anjuli M Khalid J Mol Structure 1036 (2013) 209-215

53 H-bonded supramolecular assembly via proton transfer Isolation X-ray crystallographic characterization and SOD mimic activity of [Cu(dipic)2]2[PA-H]45H2O ZA Siddiqi M Khalid M Shahid S Kumar PK Sharma Armeen Siddique Anjuli J Mol Structure 1033 (2013) 98-103

2012

54 Superoxide scavenging and antimicrobial activities of novel transition metal complexes of oxydiacetate dianion as primary ligand Spectral characterization cyclic voltammetric investigations and crystal structure Z A Siddiqi P K Sharma M Shahid Anjuli A Siddique M Khalid and S Kumar Eur J Med Chem 57(2012) 102-111

55 Crystal Structure of a Mixed-Ligand Cu(II) Complex Forming Supramolecular Assembly via an Extensive H-Bonding and RingndashRing πndashπ Interactions ZA Siddiqi M Shahid M Khalid S Kumar Anjuli Armeen Siddique J Chem Crystallography 42 (2012) 1042-1045

56 Novel decavanadate cluster complexes [H2V10O28][LH]4nH2O (L= Imidazole n=2 or 2-methylimidazole n= 0)

Preparation characterization and genotoxic studies Z A Siddiqi Anjuli P K Sharma M Shahid A Siddique M Khalid and S Kumar J Mol Structure 1029 (2012) 86-91

57 Structural electrochemical characterization and SOD mimic activities of 1D chain or 3D network encouraged by unique μ2-bridging by adipate ion in mixed ligand complexes containing α-diimine as auxiliary ligand Z A Siddiqi PK Sharma M Shahid S Kumar Anjuli A Siddique Spectrochim Acta Part A 93 (2012) 280-289

2011

58 Synthesis spectral characterizations and biological studies of transition metal mixed ligand complexes X-ray crystal structures of [Cu(oda)(Bipy)(H2O)]4H2O and [VO(oda)(Bipy)]2H2O ZA Siddiqi PK Sharma M Shahid M Khalid S Kumar J Mol Structure 994 (2011) 295

59 Spectral thermal and electrochemical characterization of novel homo-dinuclear complexes [M2(H3DTPA)(H2O)6]Cl2middotxH2O (M = Cr2+ Mn2+ Co2+ Ni2+ or Cu2+) Z A Siddiqi S Noor M Shahid M Khalid Spectrochimica Acta Part A 78 (2011) 1386

2010

60 Spectral and Physico-chemical investigations of novel homo-bimetallic di-micro2-alkoxo bridged Schiff base complexes 57Fe Moumlssbauer parameters of the Fe(III) complex ZA Siddiqi M Khalid S Kumar M Shahid S Noor Spectrochimica Acta Part A 75 (2010) 841ndash845

61 Synthesis physico-chemical and spectral investigations of novel homo-bimetallic mixed-ligand complexes 57Fe Moumlssbauer parameters of [Fe2(imda)2(H2O)3Cl] ZA Siddiqi M Shahid M Khalid S Noor S Kumar Spectrochimica Acta Part A 75 (2010) 61ndash68

62 Antimicrobial and SOD activities of novel transition metal complexes of pyridine-26-dicarboxylic acid containing 4-picoline as auxiliary ligand ZA Siddiqi M Khalid S Kumar M Shahid S Noor Eur J Med Chem 45 (2010) 264ndash269

2009

63 Synthesis and single crystal X-ray structure of 4-picoline-(pyridine-26-dicarboxylato-NOOrsquo)copper(II) ZA Siddiqi M Khalid S Kumar M Shahid X-ray structure analysis online 9 (2009) 71ndash72

64 Novel homo-bimetallic complexes of [N10] macrocyclic ligand modified with tetrapeptide function biological activities spectral and cyclic voltammetric studies Z A Siddiqi S Kumar M Khalid M Shahid Spectrochimica Acta Part A 72 (2009) 970ndash974

65 Synthesis and spectral investigations of mononuclear [N6] [N8] and dinuclear [N10] complexes of polyamide macrocycles 57Fe Moumlssbauer parameters of Fe(III) complexes ZA Siddiqi S Kumar M Khalid M Shahid Spectrochimica Acta Part A 72 (2009) 616ndash620

66 Spectral studies of Fe(III) complexes of dipodal tridentate chelating agents ZA Siddiqi S Kumar M Khalid

M Shahid Spectrochimica Acta Part A 71 (2009) 1845ndash1850

67 Spectroscopic and antimicrobial studies of La3+ Pr3+ Nd3+ and Gd3+ complexes of a dipodal [NNN] chelating ligand ZA Siddiqi M Shahid M Khalid S Noor S Kumar Spectrochimica Acta Part A 74 (2009) 391ndash397

68 Synthesis crystal structure and in-vitro antitumor activity of carboxylate bridged dinuclear organotin(IV) complexes ZA Siddiqi M Shahid S Kumar M Khalid S Noor J Organomet Chem 694 (2009) 3768ndash3774

69 Antimicrobial and SOD activities of novel transition metal ternary complexes of iminodiacetic acid containing α-diimine as auxiliary ligand ZA Siddiqi M Shahid M Khalid S Kumar Eur J Med Chem 44 (2009) 2517ndash2522

Communicated papers

Polyhedron (2019) Inorg Chem Front (2019) MatChemFront (2019) Dalton Trans (2019) CrystGrowth Des (2019)

Conferences (Papers Read)

1 Emerging Trends in Advanced Chemistry (ETAC-08) held at Centre of Advanced Study Department of Chemistry University of Rajasthan Jaipur 8-10 March 2008 (Oral)

Title ldquoSpectroscopic and X-Ray Crystallographic Characterization of a Cu(II)- Mixed Ligand Iminodiacetaterdquo

2 Interdisciplinary Science Conference lsquoInterface between Chemistry and Biologyrsquo held at Centre for Interdisciplinary Research in Basic Sciences Jamia Millia Islamia (JMI) New Delhi 8th October 2009 (Poster) Title ldquoA novel pathway to synthesize polynuclear organotin(IV) supramolecular complexes Spectroscopic X-ray crystallographic and in-vitro cytotoxic studiesrdquo

3 12th CRSI National Symposium in Chemistry held at Indian Institute of Chemical Technology (IICT) Hyderabad 5thndash7th February 2010 (Poster)

Title ldquoSynthesis crystal structures and cytotoxic studies of novel benzimidazole derived complexes [Mn(BIm)(CH3OH)Cl2] and [Cu(BIm)Cl2]rdquo

4 National Symposium on Recent Trends in Chemical Sciences (NSRTCS-2010) held on 24-25th Feb 2010 at Department of Chemistry AMU Aligarh (Poster)

Title A novel homo-dinuclear mixed-valent [FeIII-FeII] ferredoxin analogue [Fe2(imda)2(H2O)3Cl] Synthesis Moumlssbauer and EPR spectral characterization

5 International Satellite Symposium on lsquoFree Radicals in Health and Diseasersquo Satellite Free Radical Research (SFRR) held at Department of Biochemistry AMU Aligarh (Poster) March 17-18 2009 Title ldquoSOD A natural antioxidant and its comparison with a synthetic antioxidant prepared in the laboratoryrdquo

6 International Conference on Chemistry Frontiers and Challenges 5-6 March 2011 Deptt of Chemistry

AMU Aligarh (Poster) Title Synthesis and X-ray crystallographic analyses of novel transition metal ternary complexes bearing 1D chains

and 3D supramolecular networks

7 National Conference on New Vistas In chemistry Daptt Of Chemistry AMU Aligarh 2-3 March 2012 (Poster) Title Synthesis and spectral investigations of oxydiacetate complexes containing heterocycle as auxiliary ligand 57Moumlssbauer genotoxic and antimicrobial studies

8 International Conference on Chemistry Frontiers and Challenges 2-3 March 2013 Deptt of Chemistry AMU Aligarh (Poster)

Title Heterometallic polynuclear Mnx-Lny clusters showing Single Molecule Magnet (SMM) behaviour Crystallography magnetism and cyclic voltammetric investigations

9 National Symposium on free radical research 6 March 2014 Department of Biochemistry AMU Aligarh (Poster)

Title Superoxide scavenging activities of novel transition metal complexes of oxydiacetate Crystal structure and cyclic voltammetric studies

10 National Symposium of Chemistry 22 March 2014 Department of Chemistry AMU Aligarh (Poster) Title Designing of mono- and di-nuclear high spin Fe(III) complexes of oxydiacetate ligand 57Fe-Moumlssbauer and

magnetic studies 11 National Conference on Interdisciplinary approach in chemical sciences Jamia millia islamia New Delhi 2015

(ORAL) Title Synthesis and spectral and X-ray crystallographic studies of proton transfer complexes of 4-picoline and pyridine-26ndashdicarboxylic acid

12 National Seminar on intellectual Property Right (IPR) University Polytechnic AMU Aligarh 2015 13 International Conference on recent advances in chemical sciences Department of Chemistry AMU Aligarh29-30

March 2016 (Poster) Title Single molecules magnets Designing strategies

14 Recent Advances in Chemical Sciences March 25-26 2017 Dept of Chemistry AMU Aligarh (Poster) Title Synthesis and structural characterization of polynuclear metal clusters

15 National Seminar on intellectual Property Right (IPR) University Polytechnic AMU Aligarh 2017 16 Emerging trends in chemical sciences 24-25 Feb 2018 Department of Chemistry Amu Aligarh (Poster) Title Structural investigation on some Cu-Gd complexes 17 Indo-French workshop cum conference on magnetism of molecules Solid State amp Structural Chemistry Unit (SSCU)

Indian Institute of Science (IISc) Bangalore 26-30 Nov 2018 (Poster) Title A novel Mn12Na2 polymer exhibiting single chain magnet (SCM) behavior

18 Emerging trends in Chemical Sciences 24-25 Feb 2019 Department of Chemistry AMU Aligarh (Attended)

Dr M Shahid

Page 2: Dr. M. SHAHID, · Fig. Crystal structure of the novel organotin(IV) compound, Fig. Mossbauer Spectra of a bimetallic complex at RT & LNT a potential antitumor agent isolated by Dr

MSc - Ist semester-Inorganic Reaction Mechanism MSc - IIIrd Semester- Organometallic Chemistry

Fellowships availed

Junior Research Fellowship (JRF) by UGC from Oct 2009 to July 2010 UGC fellowship for central Universities from 2007 to Sep 2009

Research Profile

Summary of PhD work

Title of Thesis Synthesis amp Physico-chemical Investigations of Binary and Ternary Complexes of Metal Ions Mentor Prof Zafar A Siddiqi Significant outcomes

The chemistry of functionalized polycarboxylic acid and their binary and ternary complexes of metal ions has been taken under investigation The coordination chemistry of functionalized polycarboxylic acid ligands viz pyridinedicarboxylic acid (H2pda) iminodiacetic acid (H2imda) oxydiacetic acid (H2oda) or nitrilotriacetic acid (H3nta) has attracted special focus of inorganic and bioinorganic chemists over the past decades These ligands are very important tridentate chelating agents The flexibility of these ligands makes them useful for the formation of the complexes differing in coordination numbers conformations and 3-D architectures It is well known that in binary and ternary mixed ligand metal carboxylate complexes the carboxylate ligands play an important role to construct novel metal-organic frame works (MOFs) and supramolecular frameworks

Fig (a) A supramolecular network of the complex [Cu(IDA)(Phen)H2O]2H2O constructed from H-bonding (b) Two layers of the complex showing πndashπ interactions between phenanthroline rings and forming a supramolecular framework [Eur J Med Chem 44 (2009) 2517ndash2522]

I during my PhD focused on the study and design of mixed-ligand ternary metal iminodiacetate

complexes and their possible structural diversities and to pursue in-vitro antimicrobial antitumoral and superoxide dismutase (SOD) activities Ternary complexes of iminodiacetate containing an α-diimine as

auxiliary ligand have been widely used as models for several mono and polynuclear metal-enzymes and therefore I have concentrated on the synthesis characterization and the structure-activity correlations of the mixed ligand complexes of transition lanthanide and tin metal ions Moreover due to the flexible nature of iminodiacetic acid ligand we have investigated various H-bonding and π-π interactions existing in these complexes which result in 1D 2D and 3D supramolecular network These supramolecular networks have been characterized using X-ray crystallography

Fig Crystal structure of the novel organotin(IV) compound Fig Mossbauer Spectra of a bimetallic complex at RT amp LNT a potential antitumor agent isolated by Dr Shahid [J Organomet Chem 694 (2009) 3768ndash3774]

Fig Crystal structure of 1D coordination polymeric structure of [Cu(dipic)(4-picoline)]n isolated by us [Eur J Med Chem 45 (2010) 264ndash269]

Fig Crystal structure of the dinuclear complex Fig Crystal structure of 1D coordination polymeric structure of (colouring scheme by symmetry equivalence) isolated [Cu(2-pa)2]middot2H2On isolated by us [Eur J Med Chem 57(2012) 102] by us [Spectrochim Acta Part A 93 (2012) 280]

Current Research Interests

Designing and magnetic studies of Molecule Based MAGNETS called Single Molecule Magnets (SMMs) having High Spin and Large Anisotropy Such molecules show slow relaxation of magnetization amp also QTM and can be used for Data Storage and Quantum Computations

Designing of Molecular Magnetic Coolants or Refrigerants These are the molecules which show Magneto-Caloric Effects (MCE) at low temperature and can be used to produce cooling

Synthesis of polynuclear metal clusters of 3d 3d-4f and 4f metal ions and their Single crystal X-ray studies

Metal-Organic Frameworks (MOFs) and their applications in sensing and dye adsorption through molecular recognition

Luminescence and magnetic studies of transition metal and Lanthanide complexes

Research Project(s) completedongoing = 04

1 SERB-DST Fast Track Young Scientist Project of Rs 1835 Lac funded by SERB-DST New Delhi

(Title Coordination polymers as single molecule magnets (SMMs) Design magnetic properties structural and electrochemical investigations) (Duration 2012-2015) Completed

2 UGC Start Up Grant Project of Rs 6 Lac funded by UGC New Delhi

(Title Novel polynuclear metal clusters as single molecule magnets (SMMs) Synthesis structural characterization electrochemical and magnetic studies) (Duration 2014-2016) Completed

3 SERB-DST project under EMR (Individual Centric) Schemes for Faculty on Molecular coolers (2017-2020)

Title Exploring new molecular magnetic refrigerants with Cu-Gd systems Ongoing 4 ICMR major research Project (2019-2022)

Title Design of new molecules for neurodegenerative disease (eg Alzeimerrsquos Parkinsonrsquos Disease)

Ongoing

List of International Publications

Published = 70 2020

1 Exploring catecholase activity in dinuclear Mn(II) and Cu(II) complexes An experimental and theoretical approach M S Ahmad M Khalid M S Khan M Shahid M Ahmad Monika A Ansari M Ashafaq New J Chem 2020 Accepted

2 Catalytic activity of Mn(III) and Co(III) complexes Evaluation of catechol oxidase enzymatic and photodegradation property M S Khan M Khalid M S Ahmad M Shahid M Ahmad Res Chem Inter 2020 accepted

3 A novel self-assembly NaCu12Zn4 as a multifunctional material First report of a discrete coordination compound for detection of Ca2+ ion and selective adsorption of cationic dye in water Khushboo Iman M Shahid and Musheer Ahmad Dalton Trans (RSC) 2020 Just Accepted (IF = 40)

4 Two dimensional (2D) molecular frameworks for rapid and selective adsorption of hazardous aromatic dyes from aqueous phase Mantasha I Sameer Hussain Musheer Ahmad M Shahid Sep Pur Tech (Elsevier) 2020 Accepted (IF = 52)

5 Exploring solvent dependent catecholase activity in transition metal complexes An experimental and theoretical approach Mantasha I M Shahid A Ansari M Kumar M N Akhtar M A AlDamen You Song M Ahmad New J Chem 2020 Just Accepted

6 Effect of cabergoline on cognitive impairments in transgenic Drosophila model of Parkinsonrsquos Disease Y H Siddique M Shahid Lett Drug Des Discov 2020 Accepted

2019

7 Topology magnetism and dye adsorption properties of metal organic frameworks (MOFs) synthesized from bench chemicals K Iman M Shahid M S Khan M Ahmad and F Sama CrystEngComm 2019 Accepted DOI 101039C9CE01041F

8 Three-in-one is really better Exploring sensing and adsorption properties in a newly designed metal-organic system incorporating copper(II) ion M S Khan M Khalid M S Ahmad M Shahid M Ahmad Dalton Trans 2019 Accepted

9 Synthesis characterization theoretical studies and catecholase like activities of [MO6] type complexes M N Ahamad M Kumar A Ansari Mantasha I M Ahmad M Shahid New J Chem 2019 Accepted

10 Tetrazole based porous metal organic framework (MOF) topological analysis and dye adsorption properties Abeda Mariyam M Shahid Mantasha I M Shahnawaz Khan M Shahwaz Ahmad J Inorg Organomet Poly Mat 2019 Accepted

11 Zein film functionalized with gold nanoparticles and the factors affecting its mechanical propertiesM Ajmal P Y A Jayaprakash S Ghosh V S Jaswal K SinghS Mandal M Shahid M Yadav S Das and P Kumar RSC Adv 2019 Accepted

12 A dinuclear paddle-wheel Cu(II) complex [Cu2(L)4(H2O)2]2H2O [HL=2(methoxycarbonyl)benzoic acid)] crystallographic magnetic and theoretical analysis F Vakil Mantasha I M Shahid M Ahmad J Struct Chem (Springer) Accepted 2019

13 Design and characterization of a Cu(II) coordination polymer based on a-diimine Evaluation of the biomimetic activity J Struct Chem Accepted 2019

14 Unprecedented isolation of a dinuclear tin(II) complex stabilized by pyridine-26-dimethanol structure DFT and in vitro screening of cytotoxic properties Mantasha I M K Raza M Shahid A Ansari M Ahmad I M Khan Applied Organomet Chem (Wiley) 2019 Accepted

15 A combined experimental and theoretical approach to structure magnetic properties and DNA binding affinity of a homodinuclear Cu(II) complex M N Ahamad M Shahid A Ansari M Kumar I M Khan M Ahmad Rahisuddin and R Arif New J Chem (RSC) 2019 Accepted 101039c9nj00228f

16 Cu(II) MOFs based on bipyridyls topology magnetism and exploring sensing ability towards multiple nitro aromatic explosives MOHD NAQI AHAMAD Mohammad Shahid Musheer Ahmad Farasha Sama ACS Omega2019447738-7749

17 Crystal engineering and magnetostructural properties of newly designed azideacetate bridged Mn12 coordination polymers Cryst Growth Des (ACS) 2019 accepted

18 Fe6 Cclusters of tripodal polyalcohol ligands synthesis structures and magnetostructural properties M Ashafaq M Khalid M Raizada M Shahid M Ahmad Polyhedron 2019 Just accepted

19 Life sensors Current advances in oxygen sensing by lanthanide complexes K Iman M Shahid New J Chem (Perspective) 2019 Accepted

20 Synthesis crystal structures photoluminescence magnetic and antioxidant properties and theoretical analysis of Zn(II) and Cu(II) complexes of an aminoalcohol ligand supported by benzoate counter anions Mantasha I M Shahid M Ahmad Rahisuddin R Arif S Tasneem F Sama I A Ansari New J Chem 2019 Accepted

21 Therapeutic potential of luteolin in transgenic Drosophila model of Alzheimerrsquos disease F Ali Rahul S Jyoti F Naz M Ashafaq M Shahid Y H Siddique Neuroscience Letters (Elsevier) 692 (2019) 90-99

22 Synthesis structure and DNA binding properties of a homodinuclear Cu(II) complex An experimental and theoretical approach Farasha Sama Mukul Raizada Mo Ashafaq M Naqi Ahamad Mantasha I Khushboo Iman M Shahid Rahisuddin Rizwan Arif Naseer A Shah Hatem AM Saleh J Mol Struct (Elsevier) 1176 (2019) 283-289

23 Synthesis spectral and crystallographic study DNA binding and molecular docking studies of homo dinuclear Co(II) and Ni(II) complexes M S Khan M Khalid M S Ahmad M Ahmad M Ashafaq Rahisuddin R Arif M Shahid J Mol Struct (Elsevier) 1175 (2019) 889-899

2018 24 Spectroscopic investigations on La3+ Pr3+ Nd3+ and Gd3+ complexes with a multidentate ligating system

Luminescence properties and biological activities M Shahid Armeen Siddique Mo Ashafaq Mukul Raizada Farasha Sama M Naqi Ahamad I Mantasha Istikhar A Ansari Ishaat M Khan Pankaj Kumar Kehkeshan Fatma Zafar A Siddiqi J Mol Struct (Elsevier) 1173 918-930

25 Synthesis structure and magnetic studies of lanthanide metalndashorganic frameworks (LnndashMOFs) Aqueous phase highly selective sensors for picric acid as well as the arsenic aion M Raizada F Sama M Ashafaq M Shahid M Khalid M Ahmad Z A Siddiqi Polyhedron (Elsevier) (2018) 139 131-141

26 Structural characterization magnetic studies and catecholase-like activities of Mn12 clusters M Ashafaq M Raizada M Khalid M Shahid M Ahmad Z A Siddiqi J Coord Chem 71 2018 2118

27 Synthesis molecular docking and DNA binding studies of phthalimide-based copper(II) complex In vitro antibacterial hemolytic and antioxidant assessment Rizwan Arif Pattan Sirajuddin Nayab Istikhar A Ansari M Shahid Mohammad Irfan Shadab Alam Mohammad Abid Rahisuddin J Mol Struct (Elsevier) 1160 (2018) 142-153

28 Experimental and theoretical characterization of organic salt 2-((4-bromophenyl)amino) pyrido[12- a ] quinoxalin-11-ium bromide monohydrate synthesized via oxidative cyclization MSH Faizi MJ Alam A Haque S Ahmad M Shahid M Ahmad J Mol Struct(Invited Article) 2018 1156 457-464

2017 29 A new hybrid material of polyoxovanadate-Cu complex with VmiddotmiddotmiddotH interactions and dual aqueous phase sensing

properties for picric acid as well as Pd2+ X-ray magnetic and theoretical studies and mechanistic insights of sensing M Raizada F Sama M Ashafaq M Shahid M Ahmad Z A Siddiqi J Mat Chem C (RSC) (2017) 69 (22) 3336-3353 IF = 53

30 A disc-like Co7 cluster with a solvent dependent catecholase activity MN Ahamad F Sama MN Akhtar YC Chen ML Tong M Ahmad New J Chem 2017 41 (23) 14057-14061

31 Spectral characterization crystal structures and biological activities of iminodiacetate ternary complexes M Shahid Anjuli Sana Tasneem Mantasha I M Naqi Ahamad Farasha Sama K Fatma Z A Siddiqi J Mol Struct 2017 1146 424

32 Amino alcohols and benzoates-Friends or foes Tuning nuclearity of Cu(II) complexes structures magnetism DFT and TD-DFT studies and catecholase like activities Farasha Sama Ashish Kumar Dhara Muhammad Nadeem Akhtar Yan-Cong Chen Ming-Liang Tong Istikhar A Ansari Mukul Raizada Musheer Ahmad M Shahid Zafar A Siddiqi Dalton Trans 2017 46 9801

33 Synthesis and spectral characterization of 2-((2-hydroxybenzylidene)amino)-2-methylpropane-13-diol derived complexes molecular docking and antimicrobial studies I A Ansari F Sama M Raizada M Shahid R K Rajpoot Z A Siddiqi J Mol Struct (Elsevier) 1127 (2017) 479-488

34 Design structures and study of non-covalent interactions of mono- di- and tetranuclear complexes of a bifurcated quadridentate tripod ligand N-(aminopropyl)-diethanolamine F Sama I A Ansari M Raizada M Ahmad C M Nagaraja M Shahid A Kumar K Khan Z A Siddiqi New J Chem (RSC) (2017) 41 (5) 1959-1972

35 Design structural characterization and catalytic activity of incomplete dicubane clusters of N-substituted diethanolamines F Sama I A Ansari M Raizada M Ahmad Mo Ashafaq M Shahid B Das K Shankar Z A Siddiqi J Cluster Sci (Springer) 2017 28 (3) 1355-1377

36 New phthalimide-appended Schiff bases Studies of DNA binding molecular docking and antioxidant activities P S Nayab Rahisuddin I A Ansari A Ali M Shahid Luminescence (Wiley) 2017 32 (5) 829-838

2016

37 Structurally well-characterized new multinuclear Cu(II) and Zn(II) clusters X-ray crystallography theoretical studies and applications in catalysis I A Ansari F Sama M Raizada M Shahid M Ahmad Z A Siddiqi New J Chem (RSC) 2016 40 9840-9852

38 Isolation of proton transfer complexes containing 4‒picolinium as cation and pyridine‒26ndashdicarboxylate complex as anion Crystallographic and spectral investigations antioxidant activities and molecular docking studies Istikhar A Ansari F Sama M Shahid Rahisuddin R Arif M Khalid and Z A Siddiqi RSC Adv (RSC) 2016 6 11088

39 Synthesis crystal structures and spectral characterization of Cu(II) and Mn(II) complexes of 4-hydroxy-3-methoxybenzaldehyde antioxidant properties and molecular docking studies I A Ansari F Sama M Shahid M Ahmad Rahisuddin P S Nayab Z A Siddiqi J Coord Chem (TampF) (2016) 69 3336ndash3353

40 Synthesis Spectral Characterization X-ray and Magnetic Studies of Oxo-bridged Tetranuclear Coordination Polymers of Cobalt I A Ansari F Sama M Shahid M Khalid P K Sharma M Ahmad amp Z A Siddiqi J Inorg Organom Polym Mat 26 (2016) 178

2015

41 Isolation and Spectral Characterization of Complexes [FeL1ClH2O] and [FeL2ClH2O] (H2L1=N-(3-hydroxy-propyl)-2-[(3-hydroxy-propylcarbamoyl)-methyl]-amino-acetamide and H2L2=N-(2-hydroxy-ethyl)-2-[2-hydroxy-ethylcarbamoyl)-methyl]-amino-acetamide) 57Fe Moumlssbauer and Cyclic Voltammetric Investigations M Shahid Anjuli Mukul Raizada Farasha Sama Istikhar A Ansari Mohd Khalid I M Khan M Ahmad ZA Siddiqi Can Chem Trans 3 (2015) 354

42 Synthesis crystal structures and genotoxic studies of cis-micro-12-peroxo dicobalt(III) complexes M Shahid Armeen Siddique Istikhar A Ansari Farasha Sama Sandesh Chibber Mohd Khalid Zafar A Siddiqi Md Serajul Haque Faizi J Coord Chem 68 (2015) 848

2014

43 N1-Phenyl-N4-[(quinolin-2-yl)methylidene]benzene-14-diamine MSH Faizi A Mashrai S Garandel M Shahid Acta Cryst (2014) E70 o905-906

44 2266-Tetrabromo-3445-tetramethoxycyclohexanone MSH Faizi A Mashrai M Shahid Acta Cryst (2014) E70 o826

45 N1-((1H-imidazol)methylene)-N4-phenylbenzene-14-diamine MSH Faizi A Mashrai M Shahid M Ahmad Acta Cryst (2014) E70 o806

46 Isolation of a decavanadate cluster [H2V10O28][4-picH]4bull2H2O (4-pic=4-picoline) Crystal structure electrochemical characterization genotoxic and antimicrobial studies M Shahid PK Sharma Anjuli S Chibber ZA Siddiqi J Cluster Science 2014 (in press)

47 Designing and characterization of Fe(III) complexes of oxydiacetate containing α-diimine as auxiliary ligand 57Fe-

Moumlssbauer and cyclic voltammetric studies M Shahid P K Sharma Z A Siddiqi F Sama I A Ansari M Khalid J Mol Structure 1063 (2014) 313

48 Synthesis and characterization of a carboxylate bridged homodinuclear Co(II) complex Crystal structure of [Co2(Pda)2(H2O)5]middot2H2O (H2Pda = pyridine-26-dicorboxylic acid) Z A Siddiqi I A Ansari F Sama M Shahid IJIRSET 3 (2014) 8673

2013

49 Synthesis crystal structure and magnetic studies of tetranuclear hydroxo and ligand bridged [Co4(micro3-OH)2(micro2-dea)2(L-L)4]4Clmiddot8H2O [L-L= 22prime- bipyridine or 110-phenanthroline] complexes with mixed valence defect dicubane core Z A Siddiqi A Siddique M Shahid M Khalid Anjuli P K Sharma M Ahmad S Kumar Y Lan A K Powell Dalton Trans 42 (2013) 9513-9522

50 Synthesis structural characterization DNA binding studies and antitumor properties of tin(II)-oxydiacetate complexes containing α-diimine as auxiliary ligand Z A Siddiqi P K Sharma M Shahid M Khalid J Photochem Photobiol B Biology 125 (2013) 171-175

51 Spectroscopic Luminescence electrochemical and antimicrobial studies of lanthanide complexes of bis-

benzimidazole derived ligands Z A Siddiqi Anjuli M Shahid M Khalid P K Sharma A Siddique J Mol Structure 1037 (2013) 402-411

52 Synthesis and structural characterization of homo-dinuclear complexes [M2(dea)2(H2O)4] [M2(dea)2(Bipy)2] and [Fe2(dea)2(H2O)2(Cl)2] (M = Co Ni or Cu H2dea = diethanolamine) 57Fe Moumlssbauer and electrochemical investigations Z A Siddiqi A Siddique M Shahid P K Sharma Anjuli M Khalid J Mol Structure 1036 (2013) 209-215

53 H-bonded supramolecular assembly via proton transfer Isolation X-ray crystallographic characterization and SOD mimic activity of [Cu(dipic)2]2[PA-H]45H2O ZA Siddiqi M Khalid M Shahid S Kumar PK Sharma Armeen Siddique Anjuli J Mol Structure 1033 (2013) 98-103

2012

54 Superoxide scavenging and antimicrobial activities of novel transition metal complexes of oxydiacetate dianion as primary ligand Spectral characterization cyclic voltammetric investigations and crystal structure Z A Siddiqi P K Sharma M Shahid Anjuli A Siddique M Khalid and S Kumar Eur J Med Chem 57(2012) 102-111

55 Crystal Structure of a Mixed-Ligand Cu(II) Complex Forming Supramolecular Assembly via an Extensive H-Bonding and RingndashRing πndashπ Interactions ZA Siddiqi M Shahid M Khalid S Kumar Anjuli Armeen Siddique J Chem Crystallography 42 (2012) 1042-1045

56 Novel decavanadate cluster complexes [H2V10O28][LH]4nH2O (L= Imidazole n=2 or 2-methylimidazole n= 0)

Preparation characterization and genotoxic studies Z A Siddiqi Anjuli P K Sharma M Shahid A Siddique M Khalid and S Kumar J Mol Structure 1029 (2012) 86-91

57 Structural electrochemical characterization and SOD mimic activities of 1D chain or 3D network encouraged by unique μ2-bridging by adipate ion in mixed ligand complexes containing α-diimine as auxiliary ligand Z A Siddiqi PK Sharma M Shahid S Kumar Anjuli A Siddique Spectrochim Acta Part A 93 (2012) 280-289

2011

58 Synthesis spectral characterizations and biological studies of transition metal mixed ligand complexes X-ray crystal structures of [Cu(oda)(Bipy)(H2O)]4H2O and [VO(oda)(Bipy)]2H2O ZA Siddiqi PK Sharma M Shahid M Khalid S Kumar J Mol Structure 994 (2011) 295

59 Spectral thermal and electrochemical characterization of novel homo-dinuclear complexes [M2(H3DTPA)(H2O)6]Cl2middotxH2O (M = Cr2+ Mn2+ Co2+ Ni2+ or Cu2+) Z A Siddiqi S Noor M Shahid M Khalid Spectrochimica Acta Part A 78 (2011) 1386

2010

60 Spectral and Physico-chemical investigations of novel homo-bimetallic di-micro2-alkoxo bridged Schiff base complexes 57Fe Moumlssbauer parameters of the Fe(III) complex ZA Siddiqi M Khalid S Kumar M Shahid S Noor Spectrochimica Acta Part A 75 (2010) 841ndash845

61 Synthesis physico-chemical and spectral investigations of novel homo-bimetallic mixed-ligand complexes 57Fe Moumlssbauer parameters of [Fe2(imda)2(H2O)3Cl] ZA Siddiqi M Shahid M Khalid S Noor S Kumar Spectrochimica Acta Part A 75 (2010) 61ndash68

62 Antimicrobial and SOD activities of novel transition metal complexes of pyridine-26-dicarboxylic acid containing 4-picoline as auxiliary ligand ZA Siddiqi M Khalid S Kumar M Shahid S Noor Eur J Med Chem 45 (2010) 264ndash269

2009

63 Synthesis and single crystal X-ray structure of 4-picoline-(pyridine-26-dicarboxylato-NOOrsquo)copper(II) ZA Siddiqi M Khalid S Kumar M Shahid X-ray structure analysis online 9 (2009) 71ndash72

64 Novel homo-bimetallic complexes of [N10] macrocyclic ligand modified with tetrapeptide function biological activities spectral and cyclic voltammetric studies Z A Siddiqi S Kumar M Khalid M Shahid Spectrochimica Acta Part A 72 (2009) 970ndash974

65 Synthesis and spectral investigations of mononuclear [N6] [N8] and dinuclear [N10] complexes of polyamide macrocycles 57Fe Moumlssbauer parameters of Fe(III) complexes ZA Siddiqi S Kumar M Khalid M Shahid Spectrochimica Acta Part A 72 (2009) 616ndash620

66 Spectral studies of Fe(III) complexes of dipodal tridentate chelating agents ZA Siddiqi S Kumar M Khalid

M Shahid Spectrochimica Acta Part A 71 (2009) 1845ndash1850

67 Spectroscopic and antimicrobial studies of La3+ Pr3+ Nd3+ and Gd3+ complexes of a dipodal [NNN] chelating ligand ZA Siddiqi M Shahid M Khalid S Noor S Kumar Spectrochimica Acta Part A 74 (2009) 391ndash397

68 Synthesis crystal structure and in-vitro antitumor activity of carboxylate bridged dinuclear organotin(IV) complexes ZA Siddiqi M Shahid S Kumar M Khalid S Noor J Organomet Chem 694 (2009) 3768ndash3774

69 Antimicrobial and SOD activities of novel transition metal ternary complexes of iminodiacetic acid containing α-diimine as auxiliary ligand ZA Siddiqi M Shahid M Khalid S Kumar Eur J Med Chem 44 (2009) 2517ndash2522

Communicated papers

Polyhedron (2019) Inorg Chem Front (2019) MatChemFront (2019) Dalton Trans (2019) CrystGrowth Des (2019)

Conferences (Papers Read)

1 Emerging Trends in Advanced Chemistry (ETAC-08) held at Centre of Advanced Study Department of Chemistry University of Rajasthan Jaipur 8-10 March 2008 (Oral)

Title ldquoSpectroscopic and X-Ray Crystallographic Characterization of a Cu(II)- Mixed Ligand Iminodiacetaterdquo

2 Interdisciplinary Science Conference lsquoInterface between Chemistry and Biologyrsquo held at Centre for Interdisciplinary Research in Basic Sciences Jamia Millia Islamia (JMI) New Delhi 8th October 2009 (Poster) Title ldquoA novel pathway to synthesize polynuclear organotin(IV) supramolecular complexes Spectroscopic X-ray crystallographic and in-vitro cytotoxic studiesrdquo

3 12th CRSI National Symposium in Chemistry held at Indian Institute of Chemical Technology (IICT) Hyderabad 5thndash7th February 2010 (Poster)

Title ldquoSynthesis crystal structures and cytotoxic studies of novel benzimidazole derived complexes [Mn(BIm)(CH3OH)Cl2] and [Cu(BIm)Cl2]rdquo

4 National Symposium on Recent Trends in Chemical Sciences (NSRTCS-2010) held on 24-25th Feb 2010 at Department of Chemistry AMU Aligarh (Poster)

Title A novel homo-dinuclear mixed-valent [FeIII-FeII] ferredoxin analogue [Fe2(imda)2(H2O)3Cl] Synthesis Moumlssbauer and EPR spectral characterization

5 International Satellite Symposium on lsquoFree Radicals in Health and Diseasersquo Satellite Free Radical Research (SFRR) held at Department of Biochemistry AMU Aligarh (Poster) March 17-18 2009 Title ldquoSOD A natural antioxidant and its comparison with a synthetic antioxidant prepared in the laboratoryrdquo

6 International Conference on Chemistry Frontiers and Challenges 5-6 March 2011 Deptt of Chemistry

AMU Aligarh (Poster) Title Synthesis and X-ray crystallographic analyses of novel transition metal ternary complexes bearing 1D chains

and 3D supramolecular networks

7 National Conference on New Vistas In chemistry Daptt Of Chemistry AMU Aligarh 2-3 March 2012 (Poster) Title Synthesis and spectral investigations of oxydiacetate complexes containing heterocycle as auxiliary ligand 57Moumlssbauer genotoxic and antimicrobial studies

8 International Conference on Chemistry Frontiers and Challenges 2-3 March 2013 Deptt of Chemistry AMU Aligarh (Poster)

Title Heterometallic polynuclear Mnx-Lny clusters showing Single Molecule Magnet (SMM) behaviour Crystallography magnetism and cyclic voltammetric investigations

9 National Symposium on free radical research 6 March 2014 Department of Biochemistry AMU Aligarh (Poster)

Title Superoxide scavenging activities of novel transition metal complexes of oxydiacetate Crystal structure and cyclic voltammetric studies

10 National Symposium of Chemistry 22 March 2014 Department of Chemistry AMU Aligarh (Poster) Title Designing of mono- and di-nuclear high spin Fe(III) complexes of oxydiacetate ligand 57Fe-Moumlssbauer and

magnetic studies 11 National Conference on Interdisciplinary approach in chemical sciences Jamia millia islamia New Delhi 2015

(ORAL) Title Synthesis and spectral and X-ray crystallographic studies of proton transfer complexes of 4-picoline and pyridine-26ndashdicarboxylic acid

12 National Seminar on intellectual Property Right (IPR) University Polytechnic AMU Aligarh 2015 13 International Conference on recent advances in chemical sciences Department of Chemistry AMU Aligarh29-30

March 2016 (Poster) Title Single molecules magnets Designing strategies

14 Recent Advances in Chemical Sciences March 25-26 2017 Dept of Chemistry AMU Aligarh (Poster) Title Synthesis and structural characterization of polynuclear metal clusters

15 National Seminar on intellectual Property Right (IPR) University Polytechnic AMU Aligarh 2017 16 Emerging trends in chemical sciences 24-25 Feb 2018 Department of Chemistry Amu Aligarh (Poster) Title Structural investigation on some Cu-Gd complexes 17 Indo-French workshop cum conference on magnetism of molecules Solid State amp Structural Chemistry Unit (SSCU)

Indian Institute of Science (IISc) Bangalore 26-30 Nov 2018 (Poster) Title A novel Mn12Na2 polymer exhibiting single chain magnet (SCM) behavior

18 Emerging trends in Chemical Sciences 24-25 Feb 2019 Department of Chemistry AMU Aligarh (Attended)

Dr M Shahid

Page 3: Dr. M. SHAHID, · Fig. Crystal structure of the novel organotin(IV) compound, Fig. Mossbauer Spectra of a bimetallic complex at RT & LNT a potential antitumor agent isolated by Dr

auxiliary ligand have been widely used as models for several mono and polynuclear metal-enzymes and therefore I have concentrated on the synthesis characterization and the structure-activity correlations of the mixed ligand complexes of transition lanthanide and tin metal ions Moreover due to the flexible nature of iminodiacetic acid ligand we have investigated various H-bonding and π-π interactions existing in these complexes which result in 1D 2D and 3D supramolecular network These supramolecular networks have been characterized using X-ray crystallography

Fig Crystal structure of the novel organotin(IV) compound Fig Mossbauer Spectra of a bimetallic complex at RT amp LNT a potential antitumor agent isolated by Dr Shahid [J Organomet Chem 694 (2009) 3768ndash3774]

Fig Crystal structure of 1D coordination polymeric structure of [Cu(dipic)(4-picoline)]n isolated by us [Eur J Med Chem 45 (2010) 264ndash269]

Fig Crystal structure of the dinuclear complex Fig Crystal structure of 1D coordination polymeric structure of (colouring scheme by symmetry equivalence) isolated [Cu(2-pa)2]middot2H2On isolated by us [Eur J Med Chem 57(2012) 102] by us [Spectrochim Acta Part A 93 (2012) 280]

Current Research Interests

Designing and magnetic studies of Molecule Based MAGNETS called Single Molecule Magnets (SMMs) having High Spin and Large Anisotropy Such molecules show slow relaxation of magnetization amp also QTM and can be used for Data Storage and Quantum Computations

Designing of Molecular Magnetic Coolants or Refrigerants These are the molecules which show Magneto-Caloric Effects (MCE) at low temperature and can be used to produce cooling

Synthesis of polynuclear metal clusters of 3d 3d-4f and 4f metal ions and their Single crystal X-ray studies

Metal-Organic Frameworks (MOFs) and their applications in sensing and dye adsorption through molecular recognition

Luminescence and magnetic studies of transition metal and Lanthanide complexes

Research Project(s) completedongoing = 04

1 SERB-DST Fast Track Young Scientist Project of Rs 1835 Lac funded by SERB-DST New Delhi

(Title Coordination polymers as single molecule magnets (SMMs) Design magnetic properties structural and electrochemical investigations) (Duration 2012-2015) Completed

2 UGC Start Up Grant Project of Rs 6 Lac funded by UGC New Delhi

(Title Novel polynuclear metal clusters as single molecule magnets (SMMs) Synthesis structural characterization electrochemical and magnetic studies) (Duration 2014-2016) Completed

3 SERB-DST project under EMR (Individual Centric) Schemes for Faculty on Molecular coolers (2017-2020)

Title Exploring new molecular magnetic refrigerants with Cu-Gd systems Ongoing 4 ICMR major research Project (2019-2022)

Title Design of new molecules for neurodegenerative disease (eg Alzeimerrsquos Parkinsonrsquos Disease)

Ongoing

List of International Publications

Published = 70 2020

1 Exploring catecholase activity in dinuclear Mn(II) and Cu(II) complexes An experimental and theoretical approach M S Ahmad M Khalid M S Khan M Shahid M Ahmad Monika A Ansari M Ashafaq New J Chem 2020 Accepted

2 Catalytic activity of Mn(III) and Co(III) complexes Evaluation of catechol oxidase enzymatic and photodegradation property M S Khan M Khalid M S Ahmad M Shahid M Ahmad Res Chem Inter 2020 accepted

3 A novel self-assembly NaCu12Zn4 as a multifunctional material First report of a discrete coordination compound for detection of Ca2+ ion and selective adsorption of cationic dye in water Khushboo Iman M Shahid and Musheer Ahmad Dalton Trans (RSC) 2020 Just Accepted (IF = 40)

4 Two dimensional (2D) molecular frameworks for rapid and selective adsorption of hazardous aromatic dyes from aqueous phase Mantasha I Sameer Hussain Musheer Ahmad M Shahid Sep Pur Tech (Elsevier) 2020 Accepted (IF = 52)

5 Exploring solvent dependent catecholase activity in transition metal complexes An experimental and theoretical approach Mantasha I M Shahid A Ansari M Kumar M N Akhtar M A AlDamen You Song M Ahmad New J Chem 2020 Just Accepted

6 Effect of cabergoline on cognitive impairments in transgenic Drosophila model of Parkinsonrsquos Disease Y H Siddique M Shahid Lett Drug Des Discov 2020 Accepted

2019

7 Topology magnetism and dye adsorption properties of metal organic frameworks (MOFs) synthesized from bench chemicals K Iman M Shahid M S Khan M Ahmad and F Sama CrystEngComm 2019 Accepted DOI 101039C9CE01041F

8 Three-in-one is really better Exploring sensing and adsorption properties in a newly designed metal-organic system incorporating copper(II) ion M S Khan M Khalid M S Ahmad M Shahid M Ahmad Dalton Trans 2019 Accepted

9 Synthesis characterization theoretical studies and catecholase like activities of [MO6] type complexes M N Ahamad M Kumar A Ansari Mantasha I M Ahmad M Shahid New J Chem 2019 Accepted

10 Tetrazole based porous metal organic framework (MOF) topological analysis and dye adsorption properties Abeda Mariyam M Shahid Mantasha I M Shahnawaz Khan M Shahwaz Ahmad J Inorg Organomet Poly Mat 2019 Accepted

11 Zein film functionalized with gold nanoparticles and the factors affecting its mechanical propertiesM Ajmal P Y A Jayaprakash S Ghosh V S Jaswal K SinghS Mandal M Shahid M Yadav S Das and P Kumar RSC Adv 2019 Accepted

12 A dinuclear paddle-wheel Cu(II) complex [Cu2(L)4(H2O)2]2H2O [HL=2(methoxycarbonyl)benzoic acid)] crystallographic magnetic and theoretical analysis F Vakil Mantasha I M Shahid M Ahmad J Struct Chem (Springer) Accepted 2019

13 Design and characterization of a Cu(II) coordination polymer based on a-diimine Evaluation of the biomimetic activity J Struct Chem Accepted 2019

14 Unprecedented isolation of a dinuclear tin(II) complex stabilized by pyridine-26-dimethanol structure DFT and in vitro screening of cytotoxic properties Mantasha I M K Raza M Shahid A Ansari M Ahmad I M Khan Applied Organomet Chem (Wiley) 2019 Accepted

15 A combined experimental and theoretical approach to structure magnetic properties and DNA binding affinity of a homodinuclear Cu(II) complex M N Ahamad M Shahid A Ansari M Kumar I M Khan M Ahmad Rahisuddin and R Arif New J Chem (RSC) 2019 Accepted 101039c9nj00228f

16 Cu(II) MOFs based on bipyridyls topology magnetism and exploring sensing ability towards multiple nitro aromatic explosives MOHD NAQI AHAMAD Mohammad Shahid Musheer Ahmad Farasha Sama ACS Omega2019447738-7749

17 Crystal engineering and magnetostructural properties of newly designed azideacetate bridged Mn12 coordination polymers Cryst Growth Des (ACS) 2019 accepted

18 Fe6 Cclusters of tripodal polyalcohol ligands synthesis structures and magnetostructural properties M Ashafaq M Khalid M Raizada M Shahid M Ahmad Polyhedron 2019 Just accepted

19 Life sensors Current advances in oxygen sensing by lanthanide complexes K Iman M Shahid New J Chem (Perspective) 2019 Accepted

20 Synthesis crystal structures photoluminescence magnetic and antioxidant properties and theoretical analysis of Zn(II) and Cu(II) complexes of an aminoalcohol ligand supported by benzoate counter anions Mantasha I M Shahid M Ahmad Rahisuddin R Arif S Tasneem F Sama I A Ansari New J Chem 2019 Accepted

21 Therapeutic potential of luteolin in transgenic Drosophila model of Alzheimerrsquos disease F Ali Rahul S Jyoti F Naz M Ashafaq M Shahid Y H Siddique Neuroscience Letters (Elsevier) 692 (2019) 90-99

22 Synthesis structure and DNA binding properties of a homodinuclear Cu(II) complex An experimental and theoretical approach Farasha Sama Mukul Raizada Mo Ashafaq M Naqi Ahamad Mantasha I Khushboo Iman M Shahid Rahisuddin Rizwan Arif Naseer A Shah Hatem AM Saleh J Mol Struct (Elsevier) 1176 (2019) 283-289

23 Synthesis spectral and crystallographic study DNA binding and molecular docking studies of homo dinuclear Co(II) and Ni(II) complexes M S Khan M Khalid M S Ahmad M Ahmad M Ashafaq Rahisuddin R Arif M Shahid J Mol Struct (Elsevier) 1175 (2019) 889-899

2018 24 Spectroscopic investigations on La3+ Pr3+ Nd3+ and Gd3+ complexes with a multidentate ligating system

Luminescence properties and biological activities M Shahid Armeen Siddique Mo Ashafaq Mukul Raizada Farasha Sama M Naqi Ahamad I Mantasha Istikhar A Ansari Ishaat M Khan Pankaj Kumar Kehkeshan Fatma Zafar A Siddiqi J Mol Struct (Elsevier) 1173 918-930

25 Synthesis structure and magnetic studies of lanthanide metalndashorganic frameworks (LnndashMOFs) Aqueous phase highly selective sensors for picric acid as well as the arsenic aion M Raizada F Sama M Ashafaq M Shahid M Khalid M Ahmad Z A Siddiqi Polyhedron (Elsevier) (2018) 139 131-141

26 Structural characterization magnetic studies and catecholase-like activities of Mn12 clusters M Ashafaq M Raizada M Khalid M Shahid M Ahmad Z A Siddiqi J Coord Chem 71 2018 2118

27 Synthesis molecular docking and DNA binding studies of phthalimide-based copper(II) complex In vitro antibacterial hemolytic and antioxidant assessment Rizwan Arif Pattan Sirajuddin Nayab Istikhar A Ansari M Shahid Mohammad Irfan Shadab Alam Mohammad Abid Rahisuddin J Mol Struct (Elsevier) 1160 (2018) 142-153

28 Experimental and theoretical characterization of organic salt 2-((4-bromophenyl)amino) pyrido[12- a ] quinoxalin-11-ium bromide monohydrate synthesized via oxidative cyclization MSH Faizi MJ Alam A Haque S Ahmad M Shahid M Ahmad J Mol Struct(Invited Article) 2018 1156 457-464

2017 29 A new hybrid material of polyoxovanadate-Cu complex with VmiddotmiddotmiddotH interactions and dual aqueous phase sensing

properties for picric acid as well as Pd2+ X-ray magnetic and theoretical studies and mechanistic insights of sensing M Raizada F Sama M Ashafaq M Shahid M Ahmad Z A Siddiqi J Mat Chem C (RSC) (2017) 69 (22) 3336-3353 IF = 53

30 A disc-like Co7 cluster with a solvent dependent catecholase activity MN Ahamad F Sama MN Akhtar YC Chen ML Tong M Ahmad New J Chem 2017 41 (23) 14057-14061

31 Spectral characterization crystal structures and biological activities of iminodiacetate ternary complexes M Shahid Anjuli Sana Tasneem Mantasha I M Naqi Ahamad Farasha Sama K Fatma Z A Siddiqi J Mol Struct 2017 1146 424

32 Amino alcohols and benzoates-Friends or foes Tuning nuclearity of Cu(II) complexes structures magnetism DFT and TD-DFT studies and catecholase like activities Farasha Sama Ashish Kumar Dhara Muhammad Nadeem Akhtar Yan-Cong Chen Ming-Liang Tong Istikhar A Ansari Mukul Raizada Musheer Ahmad M Shahid Zafar A Siddiqi Dalton Trans 2017 46 9801

33 Synthesis and spectral characterization of 2-((2-hydroxybenzylidene)amino)-2-methylpropane-13-diol derived complexes molecular docking and antimicrobial studies I A Ansari F Sama M Raizada M Shahid R K Rajpoot Z A Siddiqi J Mol Struct (Elsevier) 1127 (2017) 479-488

34 Design structures and study of non-covalent interactions of mono- di- and tetranuclear complexes of a bifurcated quadridentate tripod ligand N-(aminopropyl)-diethanolamine F Sama I A Ansari M Raizada M Ahmad C M Nagaraja M Shahid A Kumar K Khan Z A Siddiqi New J Chem (RSC) (2017) 41 (5) 1959-1972

35 Design structural characterization and catalytic activity of incomplete dicubane clusters of N-substituted diethanolamines F Sama I A Ansari M Raizada M Ahmad Mo Ashafaq M Shahid B Das K Shankar Z A Siddiqi J Cluster Sci (Springer) 2017 28 (3) 1355-1377

36 New phthalimide-appended Schiff bases Studies of DNA binding molecular docking and antioxidant activities P S Nayab Rahisuddin I A Ansari A Ali M Shahid Luminescence (Wiley) 2017 32 (5) 829-838

2016

37 Structurally well-characterized new multinuclear Cu(II) and Zn(II) clusters X-ray crystallography theoretical studies and applications in catalysis I A Ansari F Sama M Raizada M Shahid M Ahmad Z A Siddiqi New J Chem (RSC) 2016 40 9840-9852

38 Isolation of proton transfer complexes containing 4‒picolinium as cation and pyridine‒26ndashdicarboxylate complex as anion Crystallographic and spectral investigations antioxidant activities and molecular docking studies Istikhar A Ansari F Sama M Shahid Rahisuddin R Arif M Khalid and Z A Siddiqi RSC Adv (RSC) 2016 6 11088

39 Synthesis crystal structures and spectral characterization of Cu(II) and Mn(II) complexes of 4-hydroxy-3-methoxybenzaldehyde antioxidant properties and molecular docking studies I A Ansari F Sama M Shahid M Ahmad Rahisuddin P S Nayab Z A Siddiqi J Coord Chem (TampF) (2016) 69 3336ndash3353

40 Synthesis Spectral Characterization X-ray and Magnetic Studies of Oxo-bridged Tetranuclear Coordination Polymers of Cobalt I A Ansari F Sama M Shahid M Khalid P K Sharma M Ahmad amp Z A Siddiqi J Inorg Organom Polym Mat 26 (2016) 178

2015

41 Isolation and Spectral Characterization of Complexes [FeL1ClH2O] and [FeL2ClH2O] (H2L1=N-(3-hydroxy-propyl)-2-[(3-hydroxy-propylcarbamoyl)-methyl]-amino-acetamide and H2L2=N-(2-hydroxy-ethyl)-2-[2-hydroxy-ethylcarbamoyl)-methyl]-amino-acetamide) 57Fe Moumlssbauer and Cyclic Voltammetric Investigations M Shahid Anjuli Mukul Raizada Farasha Sama Istikhar A Ansari Mohd Khalid I M Khan M Ahmad ZA Siddiqi Can Chem Trans 3 (2015) 354

42 Synthesis crystal structures and genotoxic studies of cis-micro-12-peroxo dicobalt(III) complexes M Shahid Armeen Siddique Istikhar A Ansari Farasha Sama Sandesh Chibber Mohd Khalid Zafar A Siddiqi Md Serajul Haque Faizi J Coord Chem 68 (2015) 848

2014

43 N1-Phenyl-N4-[(quinolin-2-yl)methylidene]benzene-14-diamine MSH Faizi A Mashrai S Garandel M Shahid Acta Cryst (2014) E70 o905-906

44 2266-Tetrabromo-3445-tetramethoxycyclohexanone MSH Faizi A Mashrai M Shahid Acta Cryst (2014) E70 o826

45 N1-((1H-imidazol)methylene)-N4-phenylbenzene-14-diamine MSH Faizi A Mashrai M Shahid M Ahmad Acta Cryst (2014) E70 o806

46 Isolation of a decavanadate cluster [H2V10O28][4-picH]4bull2H2O (4-pic=4-picoline) Crystal structure electrochemical characterization genotoxic and antimicrobial studies M Shahid PK Sharma Anjuli S Chibber ZA Siddiqi J Cluster Science 2014 (in press)

47 Designing and characterization of Fe(III) complexes of oxydiacetate containing α-diimine as auxiliary ligand 57Fe-

Moumlssbauer and cyclic voltammetric studies M Shahid P K Sharma Z A Siddiqi F Sama I A Ansari M Khalid J Mol Structure 1063 (2014) 313

48 Synthesis and characterization of a carboxylate bridged homodinuclear Co(II) complex Crystal structure of [Co2(Pda)2(H2O)5]middot2H2O (H2Pda = pyridine-26-dicorboxylic acid) Z A Siddiqi I A Ansari F Sama M Shahid IJIRSET 3 (2014) 8673

2013

49 Synthesis crystal structure and magnetic studies of tetranuclear hydroxo and ligand bridged [Co4(micro3-OH)2(micro2-dea)2(L-L)4]4Clmiddot8H2O [L-L= 22prime- bipyridine or 110-phenanthroline] complexes with mixed valence defect dicubane core Z A Siddiqi A Siddique M Shahid M Khalid Anjuli P K Sharma M Ahmad S Kumar Y Lan A K Powell Dalton Trans 42 (2013) 9513-9522

50 Synthesis structural characterization DNA binding studies and antitumor properties of tin(II)-oxydiacetate complexes containing α-diimine as auxiliary ligand Z A Siddiqi P K Sharma M Shahid M Khalid J Photochem Photobiol B Biology 125 (2013) 171-175

51 Spectroscopic Luminescence electrochemical and antimicrobial studies of lanthanide complexes of bis-

benzimidazole derived ligands Z A Siddiqi Anjuli M Shahid M Khalid P K Sharma A Siddique J Mol Structure 1037 (2013) 402-411

52 Synthesis and structural characterization of homo-dinuclear complexes [M2(dea)2(H2O)4] [M2(dea)2(Bipy)2] and [Fe2(dea)2(H2O)2(Cl)2] (M = Co Ni or Cu H2dea = diethanolamine) 57Fe Moumlssbauer and electrochemical investigations Z A Siddiqi A Siddique M Shahid P K Sharma Anjuli M Khalid J Mol Structure 1036 (2013) 209-215

53 H-bonded supramolecular assembly via proton transfer Isolation X-ray crystallographic characterization and SOD mimic activity of [Cu(dipic)2]2[PA-H]45H2O ZA Siddiqi M Khalid M Shahid S Kumar PK Sharma Armeen Siddique Anjuli J Mol Structure 1033 (2013) 98-103

2012

54 Superoxide scavenging and antimicrobial activities of novel transition metal complexes of oxydiacetate dianion as primary ligand Spectral characterization cyclic voltammetric investigations and crystal structure Z A Siddiqi P K Sharma M Shahid Anjuli A Siddique M Khalid and S Kumar Eur J Med Chem 57(2012) 102-111

55 Crystal Structure of a Mixed-Ligand Cu(II) Complex Forming Supramolecular Assembly via an Extensive H-Bonding and RingndashRing πndashπ Interactions ZA Siddiqi M Shahid M Khalid S Kumar Anjuli Armeen Siddique J Chem Crystallography 42 (2012) 1042-1045

56 Novel decavanadate cluster complexes [H2V10O28][LH]4nH2O (L= Imidazole n=2 or 2-methylimidazole n= 0)

Preparation characterization and genotoxic studies Z A Siddiqi Anjuli P K Sharma M Shahid A Siddique M Khalid and S Kumar J Mol Structure 1029 (2012) 86-91

57 Structural electrochemical characterization and SOD mimic activities of 1D chain or 3D network encouraged by unique μ2-bridging by adipate ion in mixed ligand complexes containing α-diimine as auxiliary ligand Z A Siddiqi PK Sharma M Shahid S Kumar Anjuli A Siddique Spectrochim Acta Part A 93 (2012) 280-289

2011

58 Synthesis spectral characterizations and biological studies of transition metal mixed ligand complexes X-ray crystal structures of [Cu(oda)(Bipy)(H2O)]4H2O and [VO(oda)(Bipy)]2H2O ZA Siddiqi PK Sharma M Shahid M Khalid S Kumar J Mol Structure 994 (2011) 295

59 Spectral thermal and electrochemical characterization of novel homo-dinuclear complexes [M2(H3DTPA)(H2O)6]Cl2middotxH2O (M = Cr2+ Mn2+ Co2+ Ni2+ or Cu2+) Z A Siddiqi S Noor M Shahid M Khalid Spectrochimica Acta Part A 78 (2011) 1386

2010

60 Spectral and Physico-chemical investigations of novel homo-bimetallic di-micro2-alkoxo bridged Schiff base complexes 57Fe Moumlssbauer parameters of the Fe(III) complex ZA Siddiqi M Khalid S Kumar M Shahid S Noor Spectrochimica Acta Part A 75 (2010) 841ndash845

61 Synthesis physico-chemical and spectral investigations of novel homo-bimetallic mixed-ligand complexes 57Fe Moumlssbauer parameters of [Fe2(imda)2(H2O)3Cl] ZA Siddiqi M Shahid M Khalid S Noor S Kumar Spectrochimica Acta Part A 75 (2010) 61ndash68

62 Antimicrobial and SOD activities of novel transition metal complexes of pyridine-26-dicarboxylic acid containing 4-picoline as auxiliary ligand ZA Siddiqi M Khalid S Kumar M Shahid S Noor Eur J Med Chem 45 (2010) 264ndash269

2009

63 Synthesis and single crystal X-ray structure of 4-picoline-(pyridine-26-dicarboxylato-NOOrsquo)copper(II) ZA Siddiqi M Khalid S Kumar M Shahid X-ray structure analysis online 9 (2009) 71ndash72

64 Novel homo-bimetallic complexes of [N10] macrocyclic ligand modified with tetrapeptide function biological activities spectral and cyclic voltammetric studies Z A Siddiqi S Kumar M Khalid M Shahid Spectrochimica Acta Part A 72 (2009) 970ndash974

65 Synthesis and spectral investigations of mononuclear [N6] [N8] and dinuclear [N10] complexes of polyamide macrocycles 57Fe Moumlssbauer parameters of Fe(III) complexes ZA Siddiqi S Kumar M Khalid M Shahid Spectrochimica Acta Part A 72 (2009) 616ndash620

66 Spectral studies of Fe(III) complexes of dipodal tridentate chelating agents ZA Siddiqi S Kumar M Khalid

M Shahid Spectrochimica Acta Part A 71 (2009) 1845ndash1850

67 Spectroscopic and antimicrobial studies of La3+ Pr3+ Nd3+ and Gd3+ complexes of a dipodal [NNN] chelating ligand ZA Siddiqi M Shahid M Khalid S Noor S Kumar Spectrochimica Acta Part A 74 (2009) 391ndash397

68 Synthesis crystal structure and in-vitro antitumor activity of carboxylate bridged dinuclear organotin(IV) complexes ZA Siddiqi M Shahid S Kumar M Khalid S Noor J Organomet Chem 694 (2009) 3768ndash3774

69 Antimicrobial and SOD activities of novel transition metal ternary complexes of iminodiacetic acid containing α-diimine as auxiliary ligand ZA Siddiqi M Shahid M Khalid S Kumar Eur J Med Chem 44 (2009) 2517ndash2522

Communicated papers

Polyhedron (2019) Inorg Chem Front (2019) MatChemFront (2019) Dalton Trans (2019) CrystGrowth Des (2019)

Conferences (Papers Read)

1 Emerging Trends in Advanced Chemistry (ETAC-08) held at Centre of Advanced Study Department of Chemistry University of Rajasthan Jaipur 8-10 March 2008 (Oral)

Title ldquoSpectroscopic and X-Ray Crystallographic Characterization of a Cu(II)- Mixed Ligand Iminodiacetaterdquo

2 Interdisciplinary Science Conference lsquoInterface between Chemistry and Biologyrsquo held at Centre for Interdisciplinary Research in Basic Sciences Jamia Millia Islamia (JMI) New Delhi 8th October 2009 (Poster) Title ldquoA novel pathway to synthesize polynuclear organotin(IV) supramolecular complexes Spectroscopic X-ray crystallographic and in-vitro cytotoxic studiesrdquo

3 12th CRSI National Symposium in Chemistry held at Indian Institute of Chemical Technology (IICT) Hyderabad 5thndash7th February 2010 (Poster)

Title ldquoSynthesis crystal structures and cytotoxic studies of novel benzimidazole derived complexes [Mn(BIm)(CH3OH)Cl2] and [Cu(BIm)Cl2]rdquo

4 National Symposium on Recent Trends in Chemical Sciences (NSRTCS-2010) held on 24-25th Feb 2010 at Department of Chemistry AMU Aligarh (Poster)

Title A novel homo-dinuclear mixed-valent [FeIII-FeII] ferredoxin analogue [Fe2(imda)2(H2O)3Cl] Synthesis Moumlssbauer and EPR spectral characterization

5 International Satellite Symposium on lsquoFree Radicals in Health and Diseasersquo Satellite Free Radical Research (SFRR) held at Department of Biochemistry AMU Aligarh (Poster) March 17-18 2009 Title ldquoSOD A natural antioxidant and its comparison with a synthetic antioxidant prepared in the laboratoryrdquo

6 International Conference on Chemistry Frontiers and Challenges 5-6 March 2011 Deptt of Chemistry

AMU Aligarh (Poster) Title Synthesis and X-ray crystallographic analyses of novel transition metal ternary complexes bearing 1D chains

and 3D supramolecular networks

7 National Conference on New Vistas In chemistry Daptt Of Chemistry AMU Aligarh 2-3 March 2012 (Poster) Title Synthesis and spectral investigations of oxydiacetate complexes containing heterocycle as auxiliary ligand 57Moumlssbauer genotoxic and antimicrobial studies

8 International Conference on Chemistry Frontiers and Challenges 2-3 March 2013 Deptt of Chemistry AMU Aligarh (Poster)

Title Heterometallic polynuclear Mnx-Lny clusters showing Single Molecule Magnet (SMM) behaviour Crystallography magnetism and cyclic voltammetric investigations

9 National Symposium on free radical research 6 March 2014 Department of Biochemistry AMU Aligarh (Poster)

Title Superoxide scavenging activities of novel transition metal complexes of oxydiacetate Crystal structure and cyclic voltammetric studies

10 National Symposium of Chemistry 22 March 2014 Department of Chemistry AMU Aligarh (Poster) Title Designing of mono- and di-nuclear high spin Fe(III) complexes of oxydiacetate ligand 57Fe-Moumlssbauer and

magnetic studies 11 National Conference on Interdisciplinary approach in chemical sciences Jamia millia islamia New Delhi 2015

(ORAL) Title Synthesis and spectral and X-ray crystallographic studies of proton transfer complexes of 4-picoline and pyridine-26ndashdicarboxylic acid

12 National Seminar on intellectual Property Right (IPR) University Polytechnic AMU Aligarh 2015 13 International Conference on recent advances in chemical sciences Department of Chemistry AMU Aligarh29-30

March 2016 (Poster) Title Single molecules magnets Designing strategies

14 Recent Advances in Chemical Sciences March 25-26 2017 Dept of Chemistry AMU Aligarh (Poster) Title Synthesis and structural characterization of polynuclear metal clusters

15 National Seminar on intellectual Property Right (IPR) University Polytechnic AMU Aligarh 2017 16 Emerging trends in chemical sciences 24-25 Feb 2018 Department of Chemistry Amu Aligarh (Poster) Title Structural investigation on some Cu-Gd complexes 17 Indo-French workshop cum conference on magnetism of molecules Solid State amp Structural Chemistry Unit (SSCU)

Indian Institute of Science (IISc) Bangalore 26-30 Nov 2018 (Poster) Title A novel Mn12Na2 polymer exhibiting single chain magnet (SCM) behavior

18 Emerging trends in Chemical Sciences 24-25 Feb 2019 Department of Chemistry AMU Aligarh (Attended)

Dr M Shahid

Page 4: Dr. M. SHAHID, · Fig. Crystal structure of the novel organotin(IV) compound, Fig. Mossbauer Spectra of a bimetallic complex at RT & LNT a potential antitumor agent isolated by Dr

Current Research Interests

Designing and magnetic studies of Molecule Based MAGNETS called Single Molecule Magnets (SMMs) having High Spin and Large Anisotropy Such molecules show slow relaxation of magnetization amp also QTM and can be used for Data Storage and Quantum Computations

Designing of Molecular Magnetic Coolants or Refrigerants These are the molecules which show Magneto-Caloric Effects (MCE) at low temperature and can be used to produce cooling

Synthesis of polynuclear metal clusters of 3d 3d-4f and 4f metal ions and their Single crystal X-ray studies

Metal-Organic Frameworks (MOFs) and their applications in sensing and dye adsorption through molecular recognition

Luminescence and magnetic studies of transition metal and Lanthanide complexes

Research Project(s) completedongoing = 04

1 SERB-DST Fast Track Young Scientist Project of Rs 1835 Lac funded by SERB-DST New Delhi

(Title Coordination polymers as single molecule magnets (SMMs) Design magnetic properties structural and electrochemical investigations) (Duration 2012-2015) Completed

2 UGC Start Up Grant Project of Rs 6 Lac funded by UGC New Delhi

(Title Novel polynuclear metal clusters as single molecule magnets (SMMs) Synthesis structural characterization electrochemical and magnetic studies) (Duration 2014-2016) Completed

3 SERB-DST project under EMR (Individual Centric) Schemes for Faculty on Molecular coolers (2017-2020)

Title Exploring new molecular magnetic refrigerants with Cu-Gd systems Ongoing 4 ICMR major research Project (2019-2022)

Title Design of new molecules for neurodegenerative disease (eg Alzeimerrsquos Parkinsonrsquos Disease)

Ongoing

List of International Publications

Published = 70 2020

1 Exploring catecholase activity in dinuclear Mn(II) and Cu(II) complexes An experimental and theoretical approach M S Ahmad M Khalid M S Khan M Shahid M Ahmad Monika A Ansari M Ashafaq New J Chem 2020 Accepted

2 Catalytic activity of Mn(III) and Co(III) complexes Evaluation of catechol oxidase enzymatic and photodegradation property M S Khan M Khalid M S Ahmad M Shahid M Ahmad Res Chem Inter 2020 accepted

3 A novel self-assembly NaCu12Zn4 as a multifunctional material First report of a discrete coordination compound for detection of Ca2+ ion and selective adsorption of cationic dye in water Khushboo Iman M Shahid and Musheer Ahmad Dalton Trans (RSC) 2020 Just Accepted (IF = 40)

4 Two dimensional (2D) molecular frameworks for rapid and selective adsorption of hazardous aromatic dyes from aqueous phase Mantasha I Sameer Hussain Musheer Ahmad M Shahid Sep Pur Tech (Elsevier) 2020 Accepted (IF = 52)

5 Exploring solvent dependent catecholase activity in transition metal complexes An experimental and theoretical approach Mantasha I M Shahid A Ansari M Kumar M N Akhtar M A AlDamen You Song M Ahmad New J Chem 2020 Just Accepted

6 Effect of cabergoline on cognitive impairments in transgenic Drosophila model of Parkinsonrsquos Disease Y H Siddique M Shahid Lett Drug Des Discov 2020 Accepted

2019

7 Topology magnetism and dye adsorption properties of metal organic frameworks (MOFs) synthesized from bench chemicals K Iman M Shahid M S Khan M Ahmad and F Sama CrystEngComm 2019 Accepted DOI 101039C9CE01041F

8 Three-in-one is really better Exploring sensing and adsorption properties in a newly designed metal-organic system incorporating copper(II) ion M S Khan M Khalid M S Ahmad M Shahid M Ahmad Dalton Trans 2019 Accepted

9 Synthesis characterization theoretical studies and catecholase like activities of [MO6] type complexes M N Ahamad M Kumar A Ansari Mantasha I M Ahmad M Shahid New J Chem 2019 Accepted

10 Tetrazole based porous metal organic framework (MOF) topological analysis and dye adsorption properties Abeda Mariyam M Shahid Mantasha I M Shahnawaz Khan M Shahwaz Ahmad J Inorg Organomet Poly Mat 2019 Accepted

11 Zein film functionalized with gold nanoparticles and the factors affecting its mechanical propertiesM Ajmal P Y A Jayaprakash S Ghosh V S Jaswal K SinghS Mandal M Shahid M Yadav S Das and P Kumar RSC Adv 2019 Accepted

12 A dinuclear paddle-wheel Cu(II) complex [Cu2(L)4(H2O)2]2H2O [HL=2(methoxycarbonyl)benzoic acid)] crystallographic magnetic and theoretical analysis F Vakil Mantasha I M Shahid M Ahmad J Struct Chem (Springer) Accepted 2019

13 Design and characterization of a Cu(II) coordination polymer based on a-diimine Evaluation of the biomimetic activity J Struct Chem Accepted 2019

14 Unprecedented isolation of a dinuclear tin(II) complex stabilized by pyridine-26-dimethanol structure DFT and in vitro screening of cytotoxic properties Mantasha I M K Raza M Shahid A Ansari M Ahmad I M Khan Applied Organomet Chem (Wiley) 2019 Accepted

15 A combined experimental and theoretical approach to structure magnetic properties and DNA binding affinity of a homodinuclear Cu(II) complex M N Ahamad M Shahid A Ansari M Kumar I M Khan M Ahmad Rahisuddin and R Arif New J Chem (RSC) 2019 Accepted 101039c9nj00228f

16 Cu(II) MOFs based on bipyridyls topology magnetism and exploring sensing ability towards multiple nitro aromatic explosives MOHD NAQI AHAMAD Mohammad Shahid Musheer Ahmad Farasha Sama ACS Omega2019447738-7749

17 Crystal engineering and magnetostructural properties of newly designed azideacetate bridged Mn12 coordination polymers Cryst Growth Des (ACS) 2019 accepted

18 Fe6 Cclusters of tripodal polyalcohol ligands synthesis structures and magnetostructural properties M Ashafaq M Khalid M Raizada M Shahid M Ahmad Polyhedron 2019 Just accepted

19 Life sensors Current advances in oxygen sensing by lanthanide complexes K Iman M Shahid New J Chem (Perspective) 2019 Accepted

20 Synthesis crystal structures photoluminescence magnetic and antioxidant properties and theoretical analysis of Zn(II) and Cu(II) complexes of an aminoalcohol ligand supported by benzoate counter anions Mantasha I M Shahid M Ahmad Rahisuddin R Arif S Tasneem F Sama I A Ansari New J Chem 2019 Accepted

21 Therapeutic potential of luteolin in transgenic Drosophila model of Alzheimerrsquos disease F Ali Rahul S Jyoti F Naz M Ashafaq M Shahid Y H Siddique Neuroscience Letters (Elsevier) 692 (2019) 90-99

22 Synthesis structure and DNA binding properties of a homodinuclear Cu(II) complex An experimental and theoretical approach Farasha Sama Mukul Raizada Mo Ashafaq M Naqi Ahamad Mantasha I Khushboo Iman M Shahid Rahisuddin Rizwan Arif Naseer A Shah Hatem AM Saleh J Mol Struct (Elsevier) 1176 (2019) 283-289

23 Synthesis spectral and crystallographic study DNA binding and molecular docking studies of homo dinuclear Co(II) and Ni(II) complexes M S Khan M Khalid M S Ahmad M Ahmad M Ashafaq Rahisuddin R Arif M Shahid J Mol Struct (Elsevier) 1175 (2019) 889-899

2018 24 Spectroscopic investigations on La3+ Pr3+ Nd3+ and Gd3+ complexes with a multidentate ligating system

Luminescence properties and biological activities M Shahid Armeen Siddique Mo Ashafaq Mukul Raizada Farasha Sama M Naqi Ahamad I Mantasha Istikhar A Ansari Ishaat M Khan Pankaj Kumar Kehkeshan Fatma Zafar A Siddiqi J Mol Struct (Elsevier) 1173 918-930

25 Synthesis structure and magnetic studies of lanthanide metalndashorganic frameworks (LnndashMOFs) Aqueous phase highly selective sensors for picric acid as well as the arsenic aion M Raizada F Sama M Ashafaq M Shahid M Khalid M Ahmad Z A Siddiqi Polyhedron (Elsevier) (2018) 139 131-141

26 Structural characterization magnetic studies and catecholase-like activities of Mn12 clusters M Ashafaq M Raizada M Khalid M Shahid M Ahmad Z A Siddiqi J Coord Chem 71 2018 2118

27 Synthesis molecular docking and DNA binding studies of phthalimide-based copper(II) complex In vitro antibacterial hemolytic and antioxidant assessment Rizwan Arif Pattan Sirajuddin Nayab Istikhar A Ansari M Shahid Mohammad Irfan Shadab Alam Mohammad Abid Rahisuddin J Mol Struct (Elsevier) 1160 (2018) 142-153

28 Experimental and theoretical characterization of organic salt 2-((4-bromophenyl)amino) pyrido[12- a ] quinoxalin-11-ium bromide monohydrate synthesized via oxidative cyclization MSH Faizi MJ Alam A Haque S Ahmad M Shahid M Ahmad J Mol Struct(Invited Article) 2018 1156 457-464

2017 29 A new hybrid material of polyoxovanadate-Cu complex with VmiddotmiddotmiddotH interactions and dual aqueous phase sensing

properties for picric acid as well as Pd2+ X-ray magnetic and theoretical studies and mechanistic insights of sensing M Raizada F Sama M Ashafaq M Shahid M Ahmad Z A Siddiqi J Mat Chem C (RSC) (2017) 69 (22) 3336-3353 IF = 53

30 A disc-like Co7 cluster with a solvent dependent catecholase activity MN Ahamad F Sama MN Akhtar YC Chen ML Tong M Ahmad New J Chem 2017 41 (23) 14057-14061

31 Spectral characterization crystal structures and biological activities of iminodiacetate ternary complexes M Shahid Anjuli Sana Tasneem Mantasha I M Naqi Ahamad Farasha Sama K Fatma Z A Siddiqi J Mol Struct 2017 1146 424

32 Amino alcohols and benzoates-Friends or foes Tuning nuclearity of Cu(II) complexes structures magnetism DFT and TD-DFT studies and catecholase like activities Farasha Sama Ashish Kumar Dhara Muhammad Nadeem Akhtar Yan-Cong Chen Ming-Liang Tong Istikhar A Ansari Mukul Raizada Musheer Ahmad M Shahid Zafar A Siddiqi Dalton Trans 2017 46 9801

33 Synthesis and spectral characterization of 2-((2-hydroxybenzylidene)amino)-2-methylpropane-13-diol derived complexes molecular docking and antimicrobial studies I A Ansari F Sama M Raizada M Shahid R K Rajpoot Z A Siddiqi J Mol Struct (Elsevier) 1127 (2017) 479-488

34 Design structures and study of non-covalent interactions of mono- di- and tetranuclear complexes of a bifurcated quadridentate tripod ligand N-(aminopropyl)-diethanolamine F Sama I A Ansari M Raizada M Ahmad C M Nagaraja M Shahid A Kumar K Khan Z A Siddiqi New J Chem (RSC) (2017) 41 (5) 1959-1972

35 Design structural characterization and catalytic activity of incomplete dicubane clusters of N-substituted diethanolamines F Sama I A Ansari M Raizada M Ahmad Mo Ashafaq M Shahid B Das K Shankar Z A Siddiqi J Cluster Sci (Springer) 2017 28 (3) 1355-1377

36 New phthalimide-appended Schiff bases Studies of DNA binding molecular docking and antioxidant activities P S Nayab Rahisuddin I A Ansari A Ali M Shahid Luminescence (Wiley) 2017 32 (5) 829-838

2016

37 Structurally well-characterized new multinuclear Cu(II) and Zn(II) clusters X-ray crystallography theoretical studies and applications in catalysis I A Ansari F Sama M Raizada M Shahid M Ahmad Z A Siddiqi New J Chem (RSC) 2016 40 9840-9852

38 Isolation of proton transfer complexes containing 4‒picolinium as cation and pyridine‒26ndashdicarboxylate complex as anion Crystallographic and spectral investigations antioxidant activities and molecular docking studies Istikhar A Ansari F Sama M Shahid Rahisuddin R Arif M Khalid and Z A Siddiqi RSC Adv (RSC) 2016 6 11088

39 Synthesis crystal structures and spectral characterization of Cu(II) and Mn(II) complexes of 4-hydroxy-3-methoxybenzaldehyde antioxidant properties and molecular docking studies I A Ansari F Sama M Shahid M Ahmad Rahisuddin P S Nayab Z A Siddiqi J Coord Chem (TampF) (2016) 69 3336ndash3353

40 Synthesis Spectral Characterization X-ray and Magnetic Studies of Oxo-bridged Tetranuclear Coordination Polymers of Cobalt I A Ansari F Sama M Shahid M Khalid P K Sharma M Ahmad amp Z A Siddiqi J Inorg Organom Polym Mat 26 (2016) 178

2015

41 Isolation and Spectral Characterization of Complexes [FeL1ClH2O] and [FeL2ClH2O] (H2L1=N-(3-hydroxy-propyl)-2-[(3-hydroxy-propylcarbamoyl)-methyl]-amino-acetamide and H2L2=N-(2-hydroxy-ethyl)-2-[2-hydroxy-ethylcarbamoyl)-methyl]-amino-acetamide) 57Fe Moumlssbauer and Cyclic Voltammetric Investigations M Shahid Anjuli Mukul Raizada Farasha Sama Istikhar A Ansari Mohd Khalid I M Khan M Ahmad ZA Siddiqi Can Chem Trans 3 (2015) 354

42 Synthesis crystal structures and genotoxic studies of cis-micro-12-peroxo dicobalt(III) complexes M Shahid Armeen Siddique Istikhar A Ansari Farasha Sama Sandesh Chibber Mohd Khalid Zafar A Siddiqi Md Serajul Haque Faizi J Coord Chem 68 (2015) 848

2014

43 N1-Phenyl-N4-[(quinolin-2-yl)methylidene]benzene-14-diamine MSH Faizi A Mashrai S Garandel M Shahid Acta Cryst (2014) E70 o905-906

44 2266-Tetrabromo-3445-tetramethoxycyclohexanone MSH Faizi A Mashrai M Shahid Acta Cryst (2014) E70 o826

45 N1-((1H-imidazol)methylene)-N4-phenylbenzene-14-diamine MSH Faizi A Mashrai M Shahid M Ahmad Acta Cryst (2014) E70 o806

46 Isolation of a decavanadate cluster [H2V10O28][4-picH]4bull2H2O (4-pic=4-picoline) Crystal structure electrochemical characterization genotoxic and antimicrobial studies M Shahid PK Sharma Anjuli S Chibber ZA Siddiqi J Cluster Science 2014 (in press)

47 Designing and characterization of Fe(III) complexes of oxydiacetate containing α-diimine as auxiliary ligand 57Fe-

Moumlssbauer and cyclic voltammetric studies M Shahid P K Sharma Z A Siddiqi F Sama I A Ansari M Khalid J Mol Structure 1063 (2014) 313

48 Synthesis and characterization of a carboxylate bridged homodinuclear Co(II) complex Crystal structure of [Co2(Pda)2(H2O)5]middot2H2O (H2Pda = pyridine-26-dicorboxylic acid) Z A Siddiqi I A Ansari F Sama M Shahid IJIRSET 3 (2014) 8673

2013

49 Synthesis crystal structure and magnetic studies of tetranuclear hydroxo and ligand bridged [Co4(micro3-OH)2(micro2-dea)2(L-L)4]4Clmiddot8H2O [L-L= 22prime- bipyridine or 110-phenanthroline] complexes with mixed valence defect dicubane core Z A Siddiqi A Siddique M Shahid M Khalid Anjuli P K Sharma M Ahmad S Kumar Y Lan A K Powell Dalton Trans 42 (2013) 9513-9522

50 Synthesis structural characterization DNA binding studies and antitumor properties of tin(II)-oxydiacetate complexes containing α-diimine as auxiliary ligand Z A Siddiqi P K Sharma M Shahid M Khalid J Photochem Photobiol B Biology 125 (2013) 171-175

51 Spectroscopic Luminescence electrochemical and antimicrobial studies of lanthanide complexes of bis-

benzimidazole derived ligands Z A Siddiqi Anjuli M Shahid M Khalid P K Sharma A Siddique J Mol Structure 1037 (2013) 402-411

52 Synthesis and structural characterization of homo-dinuclear complexes [M2(dea)2(H2O)4] [M2(dea)2(Bipy)2] and [Fe2(dea)2(H2O)2(Cl)2] (M = Co Ni or Cu H2dea = diethanolamine) 57Fe Moumlssbauer and electrochemical investigations Z A Siddiqi A Siddique M Shahid P K Sharma Anjuli M Khalid J Mol Structure 1036 (2013) 209-215

53 H-bonded supramolecular assembly via proton transfer Isolation X-ray crystallographic characterization and SOD mimic activity of [Cu(dipic)2]2[PA-H]45H2O ZA Siddiqi M Khalid M Shahid S Kumar PK Sharma Armeen Siddique Anjuli J Mol Structure 1033 (2013) 98-103

2012

54 Superoxide scavenging and antimicrobial activities of novel transition metal complexes of oxydiacetate dianion as primary ligand Spectral characterization cyclic voltammetric investigations and crystal structure Z A Siddiqi P K Sharma M Shahid Anjuli A Siddique M Khalid and S Kumar Eur J Med Chem 57(2012) 102-111

55 Crystal Structure of a Mixed-Ligand Cu(II) Complex Forming Supramolecular Assembly via an Extensive H-Bonding and RingndashRing πndashπ Interactions ZA Siddiqi M Shahid M Khalid S Kumar Anjuli Armeen Siddique J Chem Crystallography 42 (2012) 1042-1045

56 Novel decavanadate cluster complexes [H2V10O28][LH]4nH2O (L= Imidazole n=2 or 2-methylimidazole n= 0)

Preparation characterization and genotoxic studies Z A Siddiqi Anjuli P K Sharma M Shahid A Siddique M Khalid and S Kumar J Mol Structure 1029 (2012) 86-91

57 Structural electrochemical characterization and SOD mimic activities of 1D chain or 3D network encouraged by unique μ2-bridging by adipate ion in mixed ligand complexes containing α-diimine as auxiliary ligand Z A Siddiqi PK Sharma M Shahid S Kumar Anjuli A Siddique Spectrochim Acta Part A 93 (2012) 280-289

2011

58 Synthesis spectral characterizations and biological studies of transition metal mixed ligand complexes X-ray crystal structures of [Cu(oda)(Bipy)(H2O)]4H2O and [VO(oda)(Bipy)]2H2O ZA Siddiqi PK Sharma M Shahid M Khalid S Kumar J Mol Structure 994 (2011) 295

59 Spectral thermal and electrochemical characterization of novel homo-dinuclear complexes [M2(H3DTPA)(H2O)6]Cl2middotxH2O (M = Cr2+ Mn2+ Co2+ Ni2+ or Cu2+) Z A Siddiqi S Noor M Shahid M Khalid Spectrochimica Acta Part A 78 (2011) 1386

2010

60 Spectral and Physico-chemical investigations of novel homo-bimetallic di-micro2-alkoxo bridged Schiff base complexes 57Fe Moumlssbauer parameters of the Fe(III) complex ZA Siddiqi M Khalid S Kumar M Shahid S Noor Spectrochimica Acta Part A 75 (2010) 841ndash845

61 Synthesis physico-chemical and spectral investigations of novel homo-bimetallic mixed-ligand complexes 57Fe Moumlssbauer parameters of [Fe2(imda)2(H2O)3Cl] ZA Siddiqi M Shahid M Khalid S Noor S Kumar Spectrochimica Acta Part A 75 (2010) 61ndash68

62 Antimicrobial and SOD activities of novel transition metal complexes of pyridine-26-dicarboxylic acid containing 4-picoline as auxiliary ligand ZA Siddiqi M Khalid S Kumar M Shahid S Noor Eur J Med Chem 45 (2010) 264ndash269

2009

63 Synthesis and single crystal X-ray structure of 4-picoline-(pyridine-26-dicarboxylato-NOOrsquo)copper(II) ZA Siddiqi M Khalid S Kumar M Shahid X-ray structure analysis online 9 (2009) 71ndash72

64 Novel homo-bimetallic complexes of [N10] macrocyclic ligand modified with tetrapeptide function biological activities spectral and cyclic voltammetric studies Z A Siddiqi S Kumar M Khalid M Shahid Spectrochimica Acta Part A 72 (2009) 970ndash974

65 Synthesis and spectral investigations of mononuclear [N6] [N8] and dinuclear [N10] complexes of polyamide macrocycles 57Fe Moumlssbauer parameters of Fe(III) complexes ZA Siddiqi S Kumar M Khalid M Shahid Spectrochimica Acta Part A 72 (2009) 616ndash620

66 Spectral studies of Fe(III) complexes of dipodal tridentate chelating agents ZA Siddiqi S Kumar M Khalid

M Shahid Spectrochimica Acta Part A 71 (2009) 1845ndash1850

67 Spectroscopic and antimicrobial studies of La3+ Pr3+ Nd3+ and Gd3+ complexes of a dipodal [NNN] chelating ligand ZA Siddiqi M Shahid M Khalid S Noor S Kumar Spectrochimica Acta Part A 74 (2009) 391ndash397

68 Synthesis crystal structure and in-vitro antitumor activity of carboxylate bridged dinuclear organotin(IV) complexes ZA Siddiqi M Shahid S Kumar M Khalid S Noor J Organomet Chem 694 (2009) 3768ndash3774

69 Antimicrobial and SOD activities of novel transition metal ternary complexes of iminodiacetic acid containing α-diimine as auxiliary ligand ZA Siddiqi M Shahid M Khalid S Kumar Eur J Med Chem 44 (2009) 2517ndash2522

Communicated papers

Polyhedron (2019) Inorg Chem Front (2019) MatChemFront (2019) Dalton Trans (2019) CrystGrowth Des (2019)

Conferences (Papers Read)

1 Emerging Trends in Advanced Chemistry (ETAC-08) held at Centre of Advanced Study Department of Chemistry University of Rajasthan Jaipur 8-10 March 2008 (Oral)

Title ldquoSpectroscopic and X-Ray Crystallographic Characterization of a Cu(II)- Mixed Ligand Iminodiacetaterdquo

2 Interdisciplinary Science Conference lsquoInterface between Chemistry and Biologyrsquo held at Centre for Interdisciplinary Research in Basic Sciences Jamia Millia Islamia (JMI) New Delhi 8th October 2009 (Poster) Title ldquoA novel pathway to synthesize polynuclear organotin(IV) supramolecular complexes Spectroscopic X-ray crystallographic and in-vitro cytotoxic studiesrdquo

3 12th CRSI National Symposium in Chemistry held at Indian Institute of Chemical Technology (IICT) Hyderabad 5thndash7th February 2010 (Poster)

Title ldquoSynthesis crystal structures and cytotoxic studies of novel benzimidazole derived complexes [Mn(BIm)(CH3OH)Cl2] and [Cu(BIm)Cl2]rdquo

4 National Symposium on Recent Trends in Chemical Sciences (NSRTCS-2010) held on 24-25th Feb 2010 at Department of Chemistry AMU Aligarh (Poster)

Title A novel homo-dinuclear mixed-valent [FeIII-FeII] ferredoxin analogue [Fe2(imda)2(H2O)3Cl] Synthesis Moumlssbauer and EPR spectral characterization

5 International Satellite Symposium on lsquoFree Radicals in Health and Diseasersquo Satellite Free Radical Research (SFRR) held at Department of Biochemistry AMU Aligarh (Poster) March 17-18 2009 Title ldquoSOD A natural antioxidant and its comparison with a synthetic antioxidant prepared in the laboratoryrdquo

6 International Conference on Chemistry Frontiers and Challenges 5-6 March 2011 Deptt of Chemistry

AMU Aligarh (Poster) Title Synthesis and X-ray crystallographic analyses of novel transition metal ternary complexes bearing 1D chains

and 3D supramolecular networks

7 National Conference on New Vistas In chemistry Daptt Of Chemistry AMU Aligarh 2-3 March 2012 (Poster) Title Synthesis and spectral investigations of oxydiacetate complexes containing heterocycle as auxiliary ligand 57Moumlssbauer genotoxic and antimicrobial studies

8 International Conference on Chemistry Frontiers and Challenges 2-3 March 2013 Deptt of Chemistry AMU Aligarh (Poster)

Title Heterometallic polynuclear Mnx-Lny clusters showing Single Molecule Magnet (SMM) behaviour Crystallography magnetism and cyclic voltammetric investigations

9 National Symposium on free radical research 6 March 2014 Department of Biochemistry AMU Aligarh (Poster)

Title Superoxide scavenging activities of novel transition metal complexes of oxydiacetate Crystal structure and cyclic voltammetric studies

10 National Symposium of Chemistry 22 March 2014 Department of Chemistry AMU Aligarh (Poster) Title Designing of mono- and di-nuclear high spin Fe(III) complexes of oxydiacetate ligand 57Fe-Moumlssbauer and

magnetic studies 11 National Conference on Interdisciplinary approach in chemical sciences Jamia millia islamia New Delhi 2015

(ORAL) Title Synthesis and spectral and X-ray crystallographic studies of proton transfer complexes of 4-picoline and pyridine-26ndashdicarboxylic acid

12 National Seminar on intellectual Property Right (IPR) University Polytechnic AMU Aligarh 2015 13 International Conference on recent advances in chemical sciences Department of Chemistry AMU Aligarh29-30

March 2016 (Poster) Title Single molecules magnets Designing strategies

14 Recent Advances in Chemical Sciences March 25-26 2017 Dept of Chemistry AMU Aligarh (Poster) Title Synthesis and structural characterization of polynuclear metal clusters

15 National Seminar on intellectual Property Right (IPR) University Polytechnic AMU Aligarh 2017 16 Emerging trends in chemical sciences 24-25 Feb 2018 Department of Chemistry Amu Aligarh (Poster) Title Structural investigation on some Cu-Gd complexes 17 Indo-French workshop cum conference on magnetism of molecules Solid State amp Structural Chemistry Unit (SSCU)

Indian Institute of Science (IISc) Bangalore 26-30 Nov 2018 (Poster) Title A novel Mn12Na2 polymer exhibiting single chain magnet (SCM) behavior

18 Emerging trends in Chemical Sciences 24-25 Feb 2019 Department of Chemistry AMU Aligarh (Attended)

Dr M Shahid

Page 5: Dr. M. SHAHID, · Fig. Crystal structure of the novel organotin(IV) compound, Fig. Mossbauer Spectra of a bimetallic complex at RT & LNT a potential antitumor agent isolated by Dr

Designing of Molecular Magnetic Coolants or Refrigerants These are the molecules which show Magneto-Caloric Effects (MCE) at low temperature and can be used to produce cooling

Synthesis of polynuclear metal clusters of 3d 3d-4f and 4f metal ions and their Single crystal X-ray studies

Metal-Organic Frameworks (MOFs) and their applications in sensing and dye adsorption through molecular recognition

Luminescence and magnetic studies of transition metal and Lanthanide complexes

Research Project(s) completedongoing = 04

1 SERB-DST Fast Track Young Scientist Project of Rs 1835 Lac funded by SERB-DST New Delhi

(Title Coordination polymers as single molecule magnets (SMMs) Design magnetic properties structural and electrochemical investigations) (Duration 2012-2015) Completed

2 UGC Start Up Grant Project of Rs 6 Lac funded by UGC New Delhi

(Title Novel polynuclear metal clusters as single molecule magnets (SMMs) Synthesis structural characterization electrochemical and magnetic studies) (Duration 2014-2016) Completed

3 SERB-DST project under EMR (Individual Centric) Schemes for Faculty on Molecular coolers (2017-2020)

Title Exploring new molecular magnetic refrigerants with Cu-Gd systems Ongoing 4 ICMR major research Project (2019-2022)

Title Design of new molecules for neurodegenerative disease (eg Alzeimerrsquos Parkinsonrsquos Disease)

Ongoing

List of International Publications

Published = 70 2020

1 Exploring catecholase activity in dinuclear Mn(II) and Cu(II) complexes An experimental and theoretical approach M S Ahmad M Khalid M S Khan M Shahid M Ahmad Monika A Ansari M Ashafaq New J Chem 2020 Accepted

2 Catalytic activity of Mn(III) and Co(III) complexes Evaluation of catechol oxidase enzymatic and photodegradation property M S Khan M Khalid M S Ahmad M Shahid M Ahmad Res Chem Inter 2020 accepted

3 A novel self-assembly NaCu12Zn4 as a multifunctional material First report of a discrete coordination compound for detection of Ca2+ ion and selective adsorption of cationic dye in water Khushboo Iman M Shahid and Musheer Ahmad Dalton Trans (RSC) 2020 Just Accepted (IF = 40)

4 Two dimensional (2D) molecular frameworks for rapid and selective adsorption of hazardous aromatic dyes from aqueous phase Mantasha I Sameer Hussain Musheer Ahmad M Shahid Sep Pur Tech (Elsevier) 2020 Accepted (IF = 52)

5 Exploring solvent dependent catecholase activity in transition metal complexes An experimental and theoretical approach Mantasha I M Shahid A Ansari M Kumar M N Akhtar M A AlDamen You Song M Ahmad New J Chem 2020 Just Accepted

6 Effect of cabergoline on cognitive impairments in transgenic Drosophila model of Parkinsonrsquos Disease Y H Siddique M Shahid Lett Drug Des Discov 2020 Accepted

2019

7 Topology magnetism and dye adsorption properties of metal organic frameworks (MOFs) synthesized from bench chemicals K Iman M Shahid M S Khan M Ahmad and F Sama CrystEngComm 2019 Accepted DOI 101039C9CE01041F

8 Three-in-one is really better Exploring sensing and adsorption properties in a newly designed metal-organic system incorporating copper(II) ion M S Khan M Khalid M S Ahmad M Shahid M Ahmad Dalton Trans 2019 Accepted

9 Synthesis characterization theoretical studies and catecholase like activities of [MO6] type complexes M N Ahamad M Kumar A Ansari Mantasha I M Ahmad M Shahid New J Chem 2019 Accepted

10 Tetrazole based porous metal organic framework (MOF) topological analysis and dye adsorption properties Abeda Mariyam M Shahid Mantasha I M Shahnawaz Khan M Shahwaz Ahmad J Inorg Organomet Poly Mat 2019 Accepted

11 Zein film functionalized with gold nanoparticles and the factors affecting its mechanical propertiesM Ajmal P Y A Jayaprakash S Ghosh V S Jaswal K SinghS Mandal M Shahid M Yadav S Das and P Kumar RSC Adv 2019 Accepted

12 A dinuclear paddle-wheel Cu(II) complex [Cu2(L)4(H2O)2]2H2O [HL=2(methoxycarbonyl)benzoic acid)] crystallographic magnetic and theoretical analysis F Vakil Mantasha I M Shahid M Ahmad J Struct Chem (Springer) Accepted 2019

13 Design and characterization of a Cu(II) coordination polymer based on a-diimine Evaluation of the biomimetic activity J Struct Chem Accepted 2019

14 Unprecedented isolation of a dinuclear tin(II) complex stabilized by pyridine-26-dimethanol structure DFT and in vitro screening of cytotoxic properties Mantasha I M K Raza M Shahid A Ansari M Ahmad I M Khan Applied Organomet Chem (Wiley) 2019 Accepted

15 A combined experimental and theoretical approach to structure magnetic properties and DNA binding affinity of a homodinuclear Cu(II) complex M N Ahamad M Shahid A Ansari M Kumar I M Khan M Ahmad Rahisuddin and R Arif New J Chem (RSC) 2019 Accepted 101039c9nj00228f

16 Cu(II) MOFs based on bipyridyls topology magnetism and exploring sensing ability towards multiple nitro aromatic explosives MOHD NAQI AHAMAD Mohammad Shahid Musheer Ahmad Farasha Sama ACS Omega2019447738-7749

17 Crystal engineering and magnetostructural properties of newly designed azideacetate bridged Mn12 coordination polymers Cryst Growth Des (ACS) 2019 accepted

18 Fe6 Cclusters of tripodal polyalcohol ligands synthesis structures and magnetostructural properties M Ashafaq M Khalid M Raizada M Shahid M Ahmad Polyhedron 2019 Just accepted

19 Life sensors Current advances in oxygen sensing by lanthanide complexes K Iman M Shahid New J Chem (Perspective) 2019 Accepted

20 Synthesis crystal structures photoluminescence magnetic and antioxidant properties and theoretical analysis of Zn(II) and Cu(II) complexes of an aminoalcohol ligand supported by benzoate counter anions Mantasha I M Shahid M Ahmad Rahisuddin R Arif S Tasneem F Sama I A Ansari New J Chem 2019 Accepted

21 Therapeutic potential of luteolin in transgenic Drosophila model of Alzheimerrsquos disease F Ali Rahul S Jyoti F Naz M Ashafaq M Shahid Y H Siddique Neuroscience Letters (Elsevier) 692 (2019) 90-99

22 Synthesis structure and DNA binding properties of a homodinuclear Cu(II) complex An experimental and theoretical approach Farasha Sama Mukul Raizada Mo Ashafaq M Naqi Ahamad Mantasha I Khushboo Iman M Shahid Rahisuddin Rizwan Arif Naseer A Shah Hatem AM Saleh J Mol Struct (Elsevier) 1176 (2019) 283-289

23 Synthesis spectral and crystallographic study DNA binding and molecular docking studies of homo dinuclear Co(II) and Ni(II) complexes M S Khan M Khalid M S Ahmad M Ahmad M Ashafaq Rahisuddin R Arif M Shahid J Mol Struct (Elsevier) 1175 (2019) 889-899

2018 24 Spectroscopic investigations on La3+ Pr3+ Nd3+ and Gd3+ complexes with a multidentate ligating system

Luminescence properties and biological activities M Shahid Armeen Siddique Mo Ashafaq Mukul Raizada Farasha Sama M Naqi Ahamad I Mantasha Istikhar A Ansari Ishaat M Khan Pankaj Kumar Kehkeshan Fatma Zafar A Siddiqi J Mol Struct (Elsevier) 1173 918-930

25 Synthesis structure and magnetic studies of lanthanide metalndashorganic frameworks (LnndashMOFs) Aqueous phase highly selective sensors for picric acid as well as the arsenic aion M Raizada F Sama M Ashafaq M Shahid M Khalid M Ahmad Z A Siddiqi Polyhedron (Elsevier) (2018) 139 131-141

26 Structural characterization magnetic studies and catecholase-like activities of Mn12 clusters M Ashafaq M Raizada M Khalid M Shahid M Ahmad Z A Siddiqi J Coord Chem 71 2018 2118

27 Synthesis molecular docking and DNA binding studies of phthalimide-based copper(II) complex In vitro antibacterial hemolytic and antioxidant assessment Rizwan Arif Pattan Sirajuddin Nayab Istikhar A Ansari M Shahid Mohammad Irfan Shadab Alam Mohammad Abid Rahisuddin J Mol Struct (Elsevier) 1160 (2018) 142-153

28 Experimental and theoretical characterization of organic salt 2-((4-bromophenyl)amino) pyrido[12- a ] quinoxalin-11-ium bromide monohydrate synthesized via oxidative cyclization MSH Faizi MJ Alam A Haque S Ahmad M Shahid M Ahmad J Mol Struct(Invited Article) 2018 1156 457-464

2017 29 A new hybrid material of polyoxovanadate-Cu complex with VmiddotmiddotmiddotH interactions and dual aqueous phase sensing

properties for picric acid as well as Pd2+ X-ray magnetic and theoretical studies and mechanistic insights of sensing M Raizada F Sama M Ashafaq M Shahid M Ahmad Z A Siddiqi J Mat Chem C (RSC) (2017) 69 (22) 3336-3353 IF = 53

30 A disc-like Co7 cluster with a solvent dependent catecholase activity MN Ahamad F Sama MN Akhtar YC Chen ML Tong M Ahmad New J Chem 2017 41 (23) 14057-14061

31 Spectral characterization crystal structures and biological activities of iminodiacetate ternary complexes M Shahid Anjuli Sana Tasneem Mantasha I M Naqi Ahamad Farasha Sama K Fatma Z A Siddiqi J Mol Struct 2017 1146 424

32 Amino alcohols and benzoates-Friends or foes Tuning nuclearity of Cu(II) complexes structures magnetism DFT and TD-DFT studies and catecholase like activities Farasha Sama Ashish Kumar Dhara Muhammad Nadeem Akhtar Yan-Cong Chen Ming-Liang Tong Istikhar A Ansari Mukul Raizada Musheer Ahmad M Shahid Zafar A Siddiqi Dalton Trans 2017 46 9801

33 Synthesis and spectral characterization of 2-((2-hydroxybenzylidene)amino)-2-methylpropane-13-diol derived complexes molecular docking and antimicrobial studies I A Ansari F Sama M Raizada M Shahid R K Rajpoot Z A Siddiqi J Mol Struct (Elsevier) 1127 (2017) 479-488

34 Design structures and study of non-covalent interactions of mono- di- and tetranuclear complexes of a bifurcated quadridentate tripod ligand N-(aminopropyl)-diethanolamine F Sama I A Ansari M Raizada M Ahmad C M Nagaraja M Shahid A Kumar K Khan Z A Siddiqi New J Chem (RSC) (2017) 41 (5) 1959-1972

35 Design structural characterization and catalytic activity of incomplete dicubane clusters of N-substituted diethanolamines F Sama I A Ansari M Raizada M Ahmad Mo Ashafaq M Shahid B Das K Shankar Z A Siddiqi J Cluster Sci (Springer) 2017 28 (3) 1355-1377

36 New phthalimide-appended Schiff bases Studies of DNA binding molecular docking and antioxidant activities P S Nayab Rahisuddin I A Ansari A Ali M Shahid Luminescence (Wiley) 2017 32 (5) 829-838

2016

37 Structurally well-characterized new multinuclear Cu(II) and Zn(II) clusters X-ray crystallography theoretical studies and applications in catalysis I A Ansari F Sama M Raizada M Shahid M Ahmad Z A Siddiqi New J Chem (RSC) 2016 40 9840-9852

38 Isolation of proton transfer complexes containing 4‒picolinium as cation and pyridine‒26ndashdicarboxylate complex as anion Crystallographic and spectral investigations antioxidant activities and molecular docking studies Istikhar A Ansari F Sama M Shahid Rahisuddin R Arif M Khalid and Z A Siddiqi RSC Adv (RSC) 2016 6 11088

39 Synthesis crystal structures and spectral characterization of Cu(II) and Mn(II) complexes of 4-hydroxy-3-methoxybenzaldehyde antioxidant properties and molecular docking studies I A Ansari F Sama M Shahid M Ahmad Rahisuddin P S Nayab Z A Siddiqi J Coord Chem (TampF) (2016) 69 3336ndash3353

40 Synthesis Spectral Characterization X-ray and Magnetic Studies of Oxo-bridged Tetranuclear Coordination Polymers of Cobalt I A Ansari F Sama M Shahid M Khalid P K Sharma M Ahmad amp Z A Siddiqi J Inorg Organom Polym Mat 26 (2016) 178

2015

41 Isolation and Spectral Characterization of Complexes [FeL1ClH2O] and [FeL2ClH2O] (H2L1=N-(3-hydroxy-propyl)-2-[(3-hydroxy-propylcarbamoyl)-methyl]-amino-acetamide and H2L2=N-(2-hydroxy-ethyl)-2-[2-hydroxy-ethylcarbamoyl)-methyl]-amino-acetamide) 57Fe Moumlssbauer and Cyclic Voltammetric Investigations M Shahid Anjuli Mukul Raizada Farasha Sama Istikhar A Ansari Mohd Khalid I M Khan M Ahmad ZA Siddiqi Can Chem Trans 3 (2015) 354

42 Synthesis crystal structures and genotoxic studies of cis-micro-12-peroxo dicobalt(III) complexes M Shahid Armeen Siddique Istikhar A Ansari Farasha Sama Sandesh Chibber Mohd Khalid Zafar A Siddiqi Md Serajul Haque Faizi J Coord Chem 68 (2015) 848

2014

43 N1-Phenyl-N4-[(quinolin-2-yl)methylidene]benzene-14-diamine MSH Faizi A Mashrai S Garandel M Shahid Acta Cryst (2014) E70 o905-906

44 2266-Tetrabromo-3445-tetramethoxycyclohexanone MSH Faizi A Mashrai M Shahid Acta Cryst (2014) E70 o826

45 N1-((1H-imidazol)methylene)-N4-phenylbenzene-14-diamine MSH Faizi A Mashrai M Shahid M Ahmad Acta Cryst (2014) E70 o806

46 Isolation of a decavanadate cluster [H2V10O28][4-picH]4bull2H2O (4-pic=4-picoline) Crystal structure electrochemical characterization genotoxic and antimicrobial studies M Shahid PK Sharma Anjuli S Chibber ZA Siddiqi J Cluster Science 2014 (in press)

47 Designing and characterization of Fe(III) complexes of oxydiacetate containing α-diimine as auxiliary ligand 57Fe-

Moumlssbauer and cyclic voltammetric studies M Shahid P K Sharma Z A Siddiqi F Sama I A Ansari M Khalid J Mol Structure 1063 (2014) 313

48 Synthesis and characterization of a carboxylate bridged homodinuclear Co(II) complex Crystal structure of [Co2(Pda)2(H2O)5]middot2H2O (H2Pda = pyridine-26-dicorboxylic acid) Z A Siddiqi I A Ansari F Sama M Shahid IJIRSET 3 (2014) 8673

2013

49 Synthesis crystal structure and magnetic studies of tetranuclear hydroxo and ligand bridged [Co4(micro3-OH)2(micro2-dea)2(L-L)4]4Clmiddot8H2O [L-L= 22prime- bipyridine or 110-phenanthroline] complexes with mixed valence defect dicubane core Z A Siddiqi A Siddique M Shahid M Khalid Anjuli P K Sharma M Ahmad S Kumar Y Lan A K Powell Dalton Trans 42 (2013) 9513-9522

50 Synthesis structural characterization DNA binding studies and antitumor properties of tin(II)-oxydiacetate complexes containing α-diimine as auxiliary ligand Z A Siddiqi P K Sharma M Shahid M Khalid J Photochem Photobiol B Biology 125 (2013) 171-175

51 Spectroscopic Luminescence electrochemical and antimicrobial studies of lanthanide complexes of bis-

benzimidazole derived ligands Z A Siddiqi Anjuli M Shahid M Khalid P K Sharma A Siddique J Mol Structure 1037 (2013) 402-411

52 Synthesis and structural characterization of homo-dinuclear complexes [M2(dea)2(H2O)4] [M2(dea)2(Bipy)2] and [Fe2(dea)2(H2O)2(Cl)2] (M = Co Ni or Cu H2dea = diethanolamine) 57Fe Moumlssbauer and electrochemical investigations Z A Siddiqi A Siddique M Shahid P K Sharma Anjuli M Khalid J Mol Structure 1036 (2013) 209-215

53 H-bonded supramolecular assembly via proton transfer Isolation X-ray crystallographic characterization and SOD mimic activity of [Cu(dipic)2]2[PA-H]45H2O ZA Siddiqi M Khalid M Shahid S Kumar PK Sharma Armeen Siddique Anjuli J Mol Structure 1033 (2013) 98-103

2012

54 Superoxide scavenging and antimicrobial activities of novel transition metal complexes of oxydiacetate dianion as primary ligand Spectral characterization cyclic voltammetric investigations and crystal structure Z A Siddiqi P K Sharma M Shahid Anjuli A Siddique M Khalid and S Kumar Eur J Med Chem 57(2012) 102-111

55 Crystal Structure of a Mixed-Ligand Cu(II) Complex Forming Supramolecular Assembly via an Extensive H-Bonding and RingndashRing πndashπ Interactions ZA Siddiqi M Shahid M Khalid S Kumar Anjuli Armeen Siddique J Chem Crystallography 42 (2012) 1042-1045

56 Novel decavanadate cluster complexes [H2V10O28][LH]4nH2O (L= Imidazole n=2 or 2-methylimidazole n= 0)

Preparation characterization and genotoxic studies Z A Siddiqi Anjuli P K Sharma M Shahid A Siddique M Khalid and S Kumar J Mol Structure 1029 (2012) 86-91

57 Structural electrochemical characterization and SOD mimic activities of 1D chain or 3D network encouraged by unique μ2-bridging by adipate ion in mixed ligand complexes containing α-diimine as auxiliary ligand Z A Siddiqi PK Sharma M Shahid S Kumar Anjuli A Siddique Spectrochim Acta Part A 93 (2012) 280-289

2011

58 Synthesis spectral characterizations and biological studies of transition metal mixed ligand complexes X-ray crystal structures of [Cu(oda)(Bipy)(H2O)]4H2O and [VO(oda)(Bipy)]2H2O ZA Siddiqi PK Sharma M Shahid M Khalid S Kumar J Mol Structure 994 (2011) 295

59 Spectral thermal and electrochemical characterization of novel homo-dinuclear complexes [M2(H3DTPA)(H2O)6]Cl2middotxH2O (M = Cr2+ Mn2+ Co2+ Ni2+ or Cu2+) Z A Siddiqi S Noor M Shahid M Khalid Spectrochimica Acta Part A 78 (2011) 1386

2010

60 Spectral and Physico-chemical investigations of novel homo-bimetallic di-micro2-alkoxo bridged Schiff base complexes 57Fe Moumlssbauer parameters of the Fe(III) complex ZA Siddiqi M Khalid S Kumar M Shahid S Noor Spectrochimica Acta Part A 75 (2010) 841ndash845

61 Synthesis physico-chemical and spectral investigations of novel homo-bimetallic mixed-ligand complexes 57Fe Moumlssbauer parameters of [Fe2(imda)2(H2O)3Cl] ZA Siddiqi M Shahid M Khalid S Noor S Kumar Spectrochimica Acta Part A 75 (2010) 61ndash68

62 Antimicrobial and SOD activities of novel transition metal complexes of pyridine-26-dicarboxylic acid containing 4-picoline as auxiliary ligand ZA Siddiqi M Khalid S Kumar M Shahid S Noor Eur J Med Chem 45 (2010) 264ndash269

2009

63 Synthesis and single crystal X-ray structure of 4-picoline-(pyridine-26-dicarboxylato-NOOrsquo)copper(II) ZA Siddiqi M Khalid S Kumar M Shahid X-ray structure analysis online 9 (2009) 71ndash72

64 Novel homo-bimetallic complexes of [N10] macrocyclic ligand modified with tetrapeptide function biological activities spectral and cyclic voltammetric studies Z A Siddiqi S Kumar M Khalid M Shahid Spectrochimica Acta Part A 72 (2009) 970ndash974

65 Synthesis and spectral investigations of mononuclear [N6] [N8] and dinuclear [N10] complexes of polyamide macrocycles 57Fe Moumlssbauer parameters of Fe(III) complexes ZA Siddiqi S Kumar M Khalid M Shahid Spectrochimica Acta Part A 72 (2009) 616ndash620

66 Spectral studies of Fe(III) complexes of dipodal tridentate chelating agents ZA Siddiqi S Kumar M Khalid

M Shahid Spectrochimica Acta Part A 71 (2009) 1845ndash1850

67 Spectroscopic and antimicrobial studies of La3+ Pr3+ Nd3+ and Gd3+ complexes of a dipodal [NNN] chelating ligand ZA Siddiqi M Shahid M Khalid S Noor S Kumar Spectrochimica Acta Part A 74 (2009) 391ndash397

68 Synthesis crystal structure and in-vitro antitumor activity of carboxylate bridged dinuclear organotin(IV) complexes ZA Siddiqi M Shahid S Kumar M Khalid S Noor J Organomet Chem 694 (2009) 3768ndash3774

69 Antimicrobial and SOD activities of novel transition metal ternary complexes of iminodiacetic acid containing α-diimine as auxiliary ligand ZA Siddiqi M Shahid M Khalid S Kumar Eur J Med Chem 44 (2009) 2517ndash2522

Communicated papers

Polyhedron (2019) Inorg Chem Front (2019) MatChemFront (2019) Dalton Trans (2019) CrystGrowth Des (2019)

Conferences (Papers Read)

1 Emerging Trends in Advanced Chemistry (ETAC-08) held at Centre of Advanced Study Department of Chemistry University of Rajasthan Jaipur 8-10 March 2008 (Oral)

Title ldquoSpectroscopic and X-Ray Crystallographic Characterization of a Cu(II)- Mixed Ligand Iminodiacetaterdquo

2 Interdisciplinary Science Conference lsquoInterface between Chemistry and Biologyrsquo held at Centre for Interdisciplinary Research in Basic Sciences Jamia Millia Islamia (JMI) New Delhi 8th October 2009 (Poster) Title ldquoA novel pathway to synthesize polynuclear organotin(IV) supramolecular complexes Spectroscopic X-ray crystallographic and in-vitro cytotoxic studiesrdquo

3 12th CRSI National Symposium in Chemistry held at Indian Institute of Chemical Technology (IICT) Hyderabad 5thndash7th February 2010 (Poster)

Title ldquoSynthesis crystal structures and cytotoxic studies of novel benzimidazole derived complexes [Mn(BIm)(CH3OH)Cl2] and [Cu(BIm)Cl2]rdquo

4 National Symposium on Recent Trends in Chemical Sciences (NSRTCS-2010) held on 24-25th Feb 2010 at Department of Chemistry AMU Aligarh (Poster)

Title A novel homo-dinuclear mixed-valent [FeIII-FeII] ferredoxin analogue [Fe2(imda)2(H2O)3Cl] Synthesis Moumlssbauer and EPR spectral characterization

5 International Satellite Symposium on lsquoFree Radicals in Health and Diseasersquo Satellite Free Radical Research (SFRR) held at Department of Biochemistry AMU Aligarh (Poster) March 17-18 2009 Title ldquoSOD A natural antioxidant and its comparison with a synthetic antioxidant prepared in the laboratoryrdquo

6 International Conference on Chemistry Frontiers and Challenges 5-6 March 2011 Deptt of Chemistry

AMU Aligarh (Poster) Title Synthesis and X-ray crystallographic analyses of novel transition metal ternary complexes bearing 1D chains

and 3D supramolecular networks

7 National Conference on New Vistas In chemistry Daptt Of Chemistry AMU Aligarh 2-3 March 2012 (Poster) Title Synthesis and spectral investigations of oxydiacetate complexes containing heterocycle as auxiliary ligand 57Moumlssbauer genotoxic and antimicrobial studies

8 International Conference on Chemistry Frontiers and Challenges 2-3 March 2013 Deptt of Chemistry AMU Aligarh (Poster)

Title Heterometallic polynuclear Mnx-Lny clusters showing Single Molecule Magnet (SMM) behaviour Crystallography magnetism and cyclic voltammetric investigations

9 National Symposium on free radical research 6 March 2014 Department of Biochemistry AMU Aligarh (Poster)

Title Superoxide scavenging activities of novel transition metal complexes of oxydiacetate Crystal structure and cyclic voltammetric studies

10 National Symposium of Chemistry 22 March 2014 Department of Chemistry AMU Aligarh (Poster) Title Designing of mono- and di-nuclear high spin Fe(III) complexes of oxydiacetate ligand 57Fe-Moumlssbauer and

magnetic studies 11 National Conference on Interdisciplinary approach in chemical sciences Jamia millia islamia New Delhi 2015

(ORAL) Title Synthesis and spectral and X-ray crystallographic studies of proton transfer complexes of 4-picoline and pyridine-26ndashdicarboxylic acid

12 National Seminar on intellectual Property Right (IPR) University Polytechnic AMU Aligarh 2015 13 International Conference on recent advances in chemical sciences Department of Chemistry AMU Aligarh29-30

March 2016 (Poster) Title Single molecules magnets Designing strategies

14 Recent Advances in Chemical Sciences March 25-26 2017 Dept of Chemistry AMU Aligarh (Poster) Title Synthesis and structural characterization of polynuclear metal clusters

15 National Seminar on intellectual Property Right (IPR) University Polytechnic AMU Aligarh 2017 16 Emerging trends in chemical sciences 24-25 Feb 2018 Department of Chemistry Amu Aligarh (Poster) Title Structural investigation on some Cu-Gd complexes 17 Indo-French workshop cum conference on magnetism of molecules Solid State amp Structural Chemistry Unit (SSCU)

Indian Institute of Science (IISc) Bangalore 26-30 Nov 2018 (Poster) Title A novel Mn12Na2 polymer exhibiting single chain magnet (SCM) behavior

18 Emerging trends in Chemical Sciences 24-25 Feb 2019 Department of Chemistry AMU Aligarh (Attended)

Dr M Shahid

Page 6: Dr. M. SHAHID, · Fig. Crystal structure of the novel organotin(IV) compound, Fig. Mossbauer Spectra of a bimetallic complex at RT & LNT a potential antitumor agent isolated by Dr

2019

7 Topology magnetism and dye adsorption properties of metal organic frameworks (MOFs) synthesized from bench chemicals K Iman M Shahid M S Khan M Ahmad and F Sama CrystEngComm 2019 Accepted DOI 101039C9CE01041F

8 Three-in-one is really better Exploring sensing and adsorption properties in a newly designed metal-organic system incorporating copper(II) ion M S Khan M Khalid M S Ahmad M Shahid M Ahmad Dalton Trans 2019 Accepted

9 Synthesis characterization theoretical studies and catecholase like activities of [MO6] type complexes M N Ahamad M Kumar A Ansari Mantasha I M Ahmad M Shahid New J Chem 2019 Accepted

10 Tetrazole based porous metal organic framework (MOF) topological analysis and dye adsorption properties Abeda Mariyam M Shahid Mantasha I M Shahnawaz Khan M Shahwaz Ahmad J Inorg Organomet Poly Mat 2019 Accepted

11 Zein film functionalized with gold nanoparticles and the factors affecting its mechanical propertiesM Ajmal P Y A Jayaprakash S Ghosh V S Jaswal K SinghS Mandal M Shahid M Yadav S Das and P Kumar RSC Adv 2019 Accepted

12 A dinuclear paddle-wheel Cu(II) complex [Cu2(L)4(H2O)2]2H2O [HL=2(methoxycarbonyl)benzoic acid)] crystallographic magnetic and theoretical analysis F Vakil Mantasha I M Shahid M Ahmad J Struct Chem (Springer) Accepted 2019

13 Design and characterization of a Cu(II) coordination polymer based on a-diimine Evaluation of the biomimetic activity J Struct Chem Accepted 2019

14 Unprecedented isolation of a dinuclear tin(II) complex stabilized by pyridine-26-dimethanol structure DFT and in vitro screening of cytotoxic properties Mantasha I M K Raza M Shahid A Ansari M Ahmad I M Khan Applied Organomet Chem (Wiley) 2019 Accepted

15 A combined experimental and theoretical approach to structure magnetic properties and DNA binding affinity of a homodinuclear Cu(II) complex M N Ahamad M Shahid A Ansari M Kumar I M Khan M Ahmad Rahisuddin and R Arif New J Chem (RSC) 2019 Accepted 101039c9nj00228f

16 Cu(II) MOFs based on bipyridyls topology magnetism and exploring sensing ability towards multiple nitro aromatic explosives MOHD NAQI AHAMAD Mohammad Shahid Musheer Ahmad Farasha Sama ACS Omega2019447738-7749

17 Crystal engineering and magnetostructural properties of newly designed azideacetate bridged Mn12 coordination polymers Cryst Growth Des (ACS) 2019 accepted

18 Fe6 Cclusters of tripodal polyalcohol ligands synthesis structures and magnetostructural properties M Ashafaq M Khalid M Raizada M Shahid M Ahmad Polyhedron 2019 Just accepted

19 Life sensors Current advances in oxygen sensing by lanthanide complexes K Iman M Shahid New J Chem (Perspective) 2019 Accepted

20 Synthesis crystal structures photoluminescence magnetic and antioxidant properties and theoretical analysis of Zn(II) and Cu(II) complexes of an aminoalcohol ligand supported by benzoate counter anions Mantasha I M Shahid M Ahmad Rahisuddin R Arif S Tasneem F Sama I A Ansari New J Chem 2019 Accepted

21 Therapeutic potential of luteolin in transgenic Drosophila model of Alzheimerrsquos disease F Ali Rahul S Jyoti F Naz M Ashafaq M Shahid Y H Siddique Neuroscience Letters (Elsevier) 692 (2019) 90-99

22 Synthesis structure and DNA binding properties of a homodinuclear Cu(II) complex An experimental and theoretical approach Farasha Sama Mukul Raizada Mo Ashafaq M Naqi Ahamad Mantasha I Khushboo Iman M Shahid Rahisuddin Rizwan Arif Naseer A Shah Hatem AM Saleh J Mol Struct (Elsevier) 1176 (2019) 283-289

23 Synthesis spectral and crystallographic study DNA binding and molecular docking studies of homo dinuclear Co(II) and Ni(II) complexes M S Khan M Khalid M S Ahmad M Ahmad M Ashafaq Rahisuddin R Arif M Shahid J Mol Struct (Elsevier) 1175 (2019) 889-899

2018 24 Spectroscopic investigations on La3+ Pr3+ Nd3+ and Gd3+ complexes with a multidentate ligating system

Luminescence properties and biological activities M Shahid Armeen Siddique Mo Ashafaq Mukul Raizada Farasha Sama M Naqi Ahamad I Mantasha Istikhar A Ansari Ishaat M Khan Pankaj Kumar Kehkeshan Fatma Zafar A Siddiqi J Mol Struct (Elsevier) 1173 918-930

25 Synthesis structure and magnetic studies of lanthanide metalndashorganic frameworks (LnndashMOFs) Aqueous phase highly selective sensors for picric acid as well as the arsenic aion M Raizada F Sama M Ashafaq M Shahid M Khalid M Ahmad Z A Siddiqi Polyhedron (Elsevier) (2018) 139 131-141

26 Structural characterization magnetic studies and catecholase-like activities of Mn12 clusters M Ashafaq M Raizada M Khalid M Shahid M Ahmad Z A Siddiqi J Coord Chem 71 2018 2118

27 Synthesis molecular docking and DNA binding studies of phthalimide-based copper(II) complex In vitro antibacterial hemolytic and antioxidant assessment Rizwan Arif Pattan Sirajuddin Nayab Istikhar A Ansari M Shahid Mohammad Irfan Shadab Alam Mohammad Abid Rahisuddin J Mol Struct (Elsevier) 1160 (2018) 142-153

28 Experimental and theoretical characterization of organic salt 2-((4-bromophenyl)amino) pyrido[12- a ] quinoxalin-11-ium bromide monohydrate synthesized via oxidative cyclization MSH Faizi MJ Alam A Haque S Ahmad M Shahid M Ahmad J Mol Struct(Invited Article) 2018 1156 457-464

2017 29 A new hybrid material of polyoxovanadate-Cu complex with VmiddotmiddotmiddotH interactions and dual aqueous phase sensing

properties for picric acid as well as Pd2+ X-ray magnetic and theoretical studies and mechanistic insights of sensing M Raizada F Sama M Ashafaq M Shahid M Ahmad Z A Siddiqi J Mat Chem C (RSC) (2017) 69 (22) 3336-3353 IF = 53

30 A disc-like Co7 cluster with a solvent dependent catecholase activity MN Ahamad F Sama MN Akhtar YC Chen ML Tong M Ahmad New J Chem 2017 41 (23) 14057-14061

31 Spectral characterization crystal structures and biological activities of iminodiacetate ternary complexes M Shahid Anjuli Sana Tasneem Mantasha I M Naqi Ahamad Farasha Sama K Fatma Z A Siddiqi J Mol Struct 2017 1146 424

32 Amino alcohols and benzoates-Friends or foes Tuning nuclearity of Cu(II) complexes structures magnetism DFT and TD-DFT studies and catecholase like activities Farasha Sama Ashish Kumar Dhara Muhammad Nadeem Akhtar Yan-Cong Chen Ming-Liang Tong Istikhar A Ansari Mukul Raizada Musheer Ahmad M Shahid Zafar A Siddiqi Dalton Trans 2017 46 9801

33 Synthesis and spectral characterization of 2-((2-hydroxybenzylidene)amino)-2-methylpropane-13-diol derived complexes molecular docking and antimicrobial studies I A Ansari F Sama M Raizada M Shahid R K Rajpoot Z A Siddiqi J Mol Struct (Elsevier) 1127 (2017) 479-488

34 Design structures and study of non-covalent interactions of mono- di- and tetranuclear complexes of a bifurcated quadridentate tripod ligand N-(aminopropyl)-diethanolamine F Sama I A Ansari M Raizada M Ahmad C M Nagaraja M Shahid A Kumar K Khan Z A Siddiqi New J Chem (RSC) (2017) 41 (5) 1959-1972

35 Design structural characterization and catalytic activity of incomplete dicubane clusters of N-substituted diethanolamines F Sama I A Ansari M Raizada M Ahmad Mo Ashafaq M Shahid B Das K Shankar Z A Siddiqi J Cluster Sci (Springer) 2017 28 (3) 1355-1377

36 New phthalimide-appended Schiff bases Studies of DNA binding molecular docking and antioxidant activities P S Nayab Rahisuddin I A Ansari A Ali M Shahid Luminescence (Wiley) 2017 32 (5) 829-838

2016

37 Structurally well-characterized new multinuclear Cu(II) and Zn(II) clusters X-ray crystallography theoretical studies and applications in catalysis I A Ansari F Sama M Raizada M Shahid M Ahmad Z A Siddiqi New J Chem (RSC) 2016 40 9840-9852

38 Isolation of proton transfer complexes containing 4‒picolinium as cation and pyridine‒26ndashdicarboxylate complex as anion Crystallographic and spectral investigations antioxidant activities and molecular docking studies Istikhar A Ansari F Sama M Shahid Rahisuddin R Arif M Khalid and Z A Siddiqi RSC Adv (RSC) 2016 6 11088

39 Synthesis crystal structures and spectral characterization of Cu(II) and Mn(II) complexes of 4-hydroxy-3-methoxybenzaldehyde antioxidant properties and molecular docking studies I A Ansari F Sama M Shahid M Ahmad Rahisuddin P S Nayab Z A Siddiqi J Coord Chem (TampF) (2016) 69 3336ndash3353

40 Synthesis Spectral Characterization X-ray and Magnetic Studies of Oxo-bridged Tetranuclear Coordination Polymers of Cobalt I A Ansari F Sama M Shahid M Khalid P K Sharma M Ahmad amp Z A Siddiqi J Inorg Organom Polym Mat 26 (2016) 178

2015

41 Isolation and Spectral Characterization of Complexes [FeL1ClH2O] and [FeL2ClH2O] (H2L1=N-(3-hydroxy-propyl)-2-[(3-hydroxy-propylcarbamoyl)-methyl]-amino-acetamide and H2L2=N-(2-hydroxy-ethyl)-2-[2-hydroxy-ethylcarbamoyl)-methyl]-amino-acetamide) 57Fe Moumlssbauer and Cyclic Voltammetric Investigations M Shahid Anjuli Mukul Raizada Farasha Sama Istikhar A Ansari Mohd Khalid I M Khan M Ahmad ZA Siddiqi Can Chem Trans 3 (2015) 354

42 Synthesis crystal structures and genotoxic studies of cis-micro-12-peroxo dicobalt(III) complexes M Shahid Armeen Siddique Istikhar A Ansari Farasha Sama Sandesh Chibber Mohd Khalid Zafar A Siddiqi Md Serajul Haque Faizi J Coord Chem 68 (2015) 848

2014

43 N1-Phenyl-N4-[(quinolin-2-yl)methylidene]benzene-14-diamine MSH Faizi A Mashrai S Garandel M Shahid Acta Cryst (2014) E70 o905-906

44 2266-Tetrabromo-3445-tetramethoxycyclohexanone MSH Faizi A Mashrai M Shahid Acta Cryst (2014) E70 o826

45 N1-((1H-imidazol)methylene)-N4-phenylbenzene-14-diamine MSH Faizi A Mashrai M Shahid M Ahmad Acta Cryst (2014) E70 o806

46 Isolation of a decavanadate cluster [H2V10O28][4-picH]4bull2H2O (4-pic=4-picoline) Crystal structure electrochemical characterization genotoxic and antimicrobial studies M Shahid PK Sharma Anjuli S Chibber ZA Siddiqi J Cluster Science 2014 (in press)

47 Designing and characterization of Fe(III) complexes of oxydiacetate containing α-diimine as auxiliary ligand 57Fe-

Moumlssbauer and cyclic voltammetric studies M Shahid P K Sharma Z A Siddiqi F Sama I A Ansari M Khalid J Mol Structure 1063 (2014) 313

48 Synthesis and characterization of a carboxylate bridged homodinuclear Co(II) complex Crystal structure of [Co2(Pda)2(H2O)5]middot2H2O (H2Pda = pyridine-26-dicorboxylic acid) Z A Siddiqi I A Ansari F Sama M Shahid IJIRSET 3 (2014) 8673

2013

49 Synthesis crystal structure and magnetic studies of tetranuclear hydroxo and ligand bridged [Co4(micro3-OH)2(micro2-dea)2(L-L)4]4Clmiddot8H2O [L-L= 22prime- bipyridine or 110-phenanthroline] complexes with mixed valence defect dicubane core Z A Siddiqi A Siddique M Shahid M Khalid Anjuli P K Sharma M Ahmad S Kumar Y Lan A K Powell Dalton Trans 42 (2013) 9513-9522

50 Synthesis structural characterization DNA binding studies and antitumor properties of tin(II)-oxydiacetate complexes containing α-diimine as auxiliary ligand Z A Siddiqi P K Sharma M Shahid M Khalid J Photochem Photobiol B Biology 125 (2013) 171-175

51 Spectroscopic Luminescence electrochemical and antimicrobial studies of lanthanide complexes of bis-

benzimidazole derived ligands Z A Siddiqi Anjuli M Shahid M Khalid P K Sharma A Siddique J Mol Structure 1037 (2013) 402-411

52 Synthesis and structural characterization of homo-dinuclear complexes [M2(dea)2(H2O)4] [M2(dea)2(Bipy)2] and [Fe2(dea)2(H2O)2(Cl)2] (M = Co Ni or Cu H2dea = diethanolamine) 57Fe Moumlssbauer and electrochemical investigations Z A Siddiqi A Siddique M Shahid P K Sharma Anjuli M Khalid J Mol Structure 1036 (2013) 209-215

53 H-bonded supramolecular assembly via proton transfer Isolation X-ray crystallographic characterization and SOD mimic activity of [Cu(dipic)2]2[PA-H]45H2O ZA Siddiqi M Khalid M Shahid S Kumar PK Sharma Armeen Siddique Anjuli J Mol Structure 1033 (2013) 98-103

2012

54 Superoxide scavenging and antimicrobial activities of novel transition metal complexes of oxydiacetate dianion as primary ligand Spectral characterization cyclic voltammetric investigations and crystal structure Z A Siddiqi P K Sharma M Shahid Anjuli A Siddique M Khalid and S Kumar Eur J Med Chem 57(2012) 102-111

55 Crystal Structure of a Mixed-Ligand Cu(II) Complex Forming Supramolecular Assembly via an Extensive H-Bonding and RingndashRing πndashπ Interactions ZA Siddiqi M Shahid M Khalid S Kumar Anjuli Armeen Siddique J Chem Crystallography 42 (2012) 1042-1045

56 Novel decavanadate cluster complexes [H2V10O28][LH]4nH2O (L= Imidazole n=2 or 2-methylimidazole n= 0)

Preparation characterization and genotoxic studies Z A Siddiqi Anjuli P K Sharma M Shahid A Siddique M Khalid and S Kumar J Mol Structure 1029 (2012) 86-91

57 Structural electrochemical characterization and SOD mimic activities of 1D chain or 3D network encouraged by unique μ2-bridging by adipate ion in mixed ligand complexes containing α-diimine as auxiliary ligand Z A Siddiqi PK Sharma M Shahid S Kumar Anjuli A Siddique Spectrochim Acta Part A 93 (2012) 280-289

2011

58 Synthesis spectral characterizations and biological studies of transition metal mixed ligand complexes X-ray crystal structures of [Cu(oda)(Bipy)(H2O)]4H2O and [VO(oda)(Bipy)]2H2O ZA Siddiqi PK Sharma M Shahid M Khalid S Kumar J Mol Structure 994 (2011) 295

59 Spectral thermal and electrochemical characterization of novel homo-dinuclear complexes [M2(H3DTPA)(H2O)6]Cl2middotxH2O (M = Cr2+ Mn2+ Co2+ Ni2+ or Cu2+) Z A Siddiqi S Noor M Shahid M Khalid Spectrochimica Acta Part A 78 (2011) 1386

2010

60 Spectral and Physico-chemical investigations of novel homo-bimetallic di-micro2-alkoxo bridged Schiff base complexes 57Fe Moumlssbauer parameters of the Fe(III) complex ZA Siddiqi M Khalid S Kumar M Shahid S Noor Spectrochimica Acta Part A 75 (2010) 841ndash845

61 Synthesis physico-chemical and spectral investigations of novel homo-bimetallic mixed-ligand complexes 57Fe Moumlssbauer parameters of [Fe2(imda)2(H2O)3Cl] ZA Siddiqi M Shahid M Khalid S Noor S Kumar Spectrochimica Acta Part A 75 (2010) 61ndash68

62 Antimicrobial and SOD activities of novel transition metal complexes of pyridine-26-dicarboxylic acid containing 4-picoline as auxiliary ligand ZA Siddiqi M Khalid S Kumar M Shahid S Noor Eur J Med Chem 45 (2010) 264ndash269

2009

63 Synthesis and single crystal X-ray structure of 4-picoline-(pyridine-26-dicarboxylato-NOOrsquo)copper(II) ZA Siddiqi M Khalid S Kumar M Shahid X-ray structure analysis online 9 (2009) 71ndash72

64 Novel homo-bimetallic complexes of [N10] macrocyclic ligand modified with tetrapeptide function biological activities spectral and cyclic voltammetric studies Z A Siddiqi S Kumar M Khalid M Shahid Spectrochimica Acta Part A 72 (2009) 970ndash974

65 Synthesis and spectral investigations of mononuclear [N6] [N8] and dinuclear [N10] complexes of polyamide macrocycles 57Fe Moumlssbauer parameters of Fe(III) complexes ZA Siddiqi S Kumar M Khalid M Shahid Spectrochimica Acta Part A 72 (2009) 616ndash620

66 Spectral studies of Fe(III) complexes of dipodal tridentate chelating agents ZA Siddiqi S Kumar M Khalid

M Shahid Spectrochimica Acta Part A 71 (2009) 1845ndash1850

67 Spectroscopic and antimicrobial studies of La3+ Pr3+ Nd3+ and Gd3+ complexes of a dipodal [NNN] chelating ligand ZA Siddiqi M Shahid M Khalid S Noor S Kumar Spectrochimica Acta Part A 74 (2009) 391ndash397

68 Synthesis crystal structure and in-vitro antitumor activity of carboxylate bridged dinuclear organotin(IV) complexes ZA Siddiqi M Shahid S Kumar M Khalid S Noor J Organomet Chem 694 (2009) 3768ndash3774

69 Antimicrobial and SOD activities of novel transition metal ternary complexes of iminodiacetic acid containing α-diimine as auxiliary ligand ZA Siddiqi M Shahid M Khalid S Kumar Eur J Med Chem 44 (2009) 2517ndash2522

Communicated papers

Polyhedron (2019) Inorg Chem Front (2019) MatChemFront (2019) Dalton Trans (2019) CrystGrowth Des (2019)

Conferences (Papers Read)

1 Emerging Trends in Advanced Chemistry (ETAC-08) held at Centre of Advanced Study Department of Chemistry University of Rajasthan Jaipur 8-10 March 2008 (Oral)

Title ldquoSpectroscopic and X-Ray Crystallographic Characterization of a Cu(II)- Mixed Ligand Iminodiacetaterdquo

2 Interdisciplinary Science Conference lsquoInterface between Chemistry and Biologyrsquo held at Centre for Interdisciplinary Research in Basic Sciences Jamia Millia Islamia (JMI) New Delhi 8th October 2009 (Poster) Title ldquoA novel pathway to synthesize polynuclear organotin(IV) supramolecular complexes Spectroscopic X-ray crystallographic and in-vitro cytotoxic studiesrdquo

3 12th CRSI National Symposium in Chemistry held at Indian Institute of Chemical Technology (IICT) Hyderabad 5thndash7th February 2010 (Poster)

Title ldquoSynthesis crystal structures and cytotoxic studies of novel benzimidazole derived complexes [Mn(BIm)(CH3OH)Cl2] and [Cu(BIm)Cl2]rdquo

4 National Symposium on Recent Trends in Chemical Sciences (NSRTCS-2010) held on 24-25th Feb 2010 at Department of Chemistry AMU Aligarh (Poster)

Title A novel homo-dinuclear mixed-valent [FeIII-FeII] ferredoxin analogue [Fe2(imda)2(H2O)3Cl] Synthesis Moumlssbauer and EPR spectral characterization

5 International Satellite Symposium on lsquoFree Radicals in Health and Diseasersquo Satellite Free Radical Research (SFRR) held at Department of Biochemistry AMU Aligarh (Poster) March 17-18 2009 Title ldquoSOD A natural antioxidant and its comparison with a synthetic antioxidant prepared in the laboratoryrdquo

6 International Conference on Chemistry Frontiers and Challenges 5-6 March 2011 Deptt of Chemistry

AMU Aligarh (Poster) Title Synthesis and X-ray crystallographic analyses of novel transition metal ternary complexes bearing 1D chains

and 3D supramolecular networks

7 National Conference on New Vistas In chemistry Daptt Of Chemistry AMU Aligarh 2-3 March 2012 (Poster) Title Synthesis and spectral investigations of oxydiacetate complexes containing heterocycle as auxiliary ligand 57Moumlssbauer genotoxic and antimicrobial studies

8 International Conference on Chemistry Frontiers and Challenges 2-3 March 2013 Deptt of Chemistry AMU Aligarh (Poster)

Title Heterometallic polynuclear Mnx-Lny clusters showing Single Molecule Magnet (SMM) behaviour Crystallography magnetism and cyclic voltammetric investigations

9 National Symposium on free radical research 6 March 2014 Department of Biochemistry AMU Aligarh (Poster)

Title Superoxide scavenging activities of novel transition metal complexes of oxydiacetate Crystal structure and cyclic voltammetric studies

10 National Symposium of Chemistry 22 March 2014 Department of Chemistry AMU Aligarh (Poster) Title Designing of mono- and di-nuclear high spin Fe(III) complexes of oxydiacetate ligand 57Fe-Moumlssbauer and

magnetic studies 11 National Conference on Interdisciplinary approach in chemical sciences Jamia millia islamia New Delhi 2015

(ORAL) Title Synthesis and spectral and X-ray crystallographic studies of proton transfer complexes of 4-picoline and pyridine-26ndashdicarboxylic acid

12 National Seminar on intellectual Property Right (IPR) University Polytechnic AMU Aligarh 2015 13 International Conference on recent advances in chemical sciences Department of Chemistry AMU Aligarh29-30

March 2016 (Poster) Title Single molecules magnets Designing strategies

14 Recent Advances in Chemical Sciences March 25-26 2017 Dept of Chemistry AMU Aligarh (Poster) Title Synthesis and structural characterization of polynuclear metal clusters

15 National Seminar on intellectual Property Right (IPR) University Polytechnic AMU Aligarh 2017 16 Emerging trends in chemical sciences 24-25 Feb 2018 Department of Chemistry Amu Aligarh (Poster) Title Structural investigation on some Cu-Gd complexes 17 Indo-French workshop cum conference on magnetism of molecules Solid State amp Structural Chemistry Unit (SSCU)

Indian Institute of Science (IISc) Bangalore 26-30 Nov 2018 (Poster) Title A novel Mn12Na2 polymer exhibiting single chain magnet (SCM) behavior

18 Emerging trends in Chemical Sciences 24-25 Feb 2019 Department of Chemistry AMU Aligarh (Attended)

Dr M Shahid

Page 7: Dr. M. SHAHID, · Fig. Crystal structure of the novel organotin(IV) compound, Fig. Mossbauer Spectra of a bimetallic complex at RT & LNT a potential antitumor agent isolated by Dr

23 Synthesis spectral and crystallographic study DNA binding and molecular docking studies of homo dinuclear Co(II) and Ni(II) complexes M S Khan M Khalid M S Ahmad M Ahmad M Ashafaq Rahisuddin R Arif M Shahid J Mol Struct (Elsevier) 1175 (2019) 889-899

2018 24 Spectroscopic investigations on La3+ Pr3+ Nd3+ and Gd3+ complexes with a multidentate ligating system

Luminescence properties and biological activities M Shahid Armeen Siddique Mo Ashafaq Mukul Raizada Farasha Sama M Naqi Ahamad I Mantasha Istikhar A Ansari Ishaat M Khan Pankaj Kumar Kehkeshan Fatma Zafar A Siddiqi J Mol Struct (Elsevier) 1173 918-930

25 Synthesis structure and magnetic studies of lanthanide metalndashorganic frameworks (LnndashMOFs) Aqueous phase highly selective sensors for picric acid as well as the arsenic aion M Raizada F Sama M Ashafaq M Shahid M Khalid M Ahmad Z A Siddiqi Polyhedron (Elsevier) (2018) 139 131-141

26 Structural characterization magnetic studies and catecholase-like activities of Mn12 clusters M Ashafaq M Raizada M Khalid M Shahid M Ahmad Z A Siddiqi J Coord Chem 71 2018 2118

27 Synthesis molecular docking and DNA binding studies of phthalimide-based copper(II) complex In vitro antibacterial hemolytic and antioxidant assessment Rizwan Arif Pattan Sirajuddin Nayab Istikhar A Ansari M Shahid Mohammad Irfan Shadab Alam Mohammad Abid Rahisuddin J Mol Struct (Elsevier) 1160 (2018) 142-153

28 Experimental and theoretical characterization of organic salt 2-((4-bromophenyl)amino) pyrido[12- a ] quinoxalin-11-ium bromide monohydrate synthesized via oxidative cyclization MSH Faizi MJ Alam A Haque S Ahmad M Shahid M Ahmad J Mol Struct(Invited Article) 2018 1156 457-464

2017 29 A new hybrid material of polyoxovanadate-Cu complex with VmiddotmiddotmiddotH interactions and dual aqueous phase sensing

properties for picric acid as well as Pd2+ X-ray magnetic and theoretical studies and mechanistic insights of sensing M Raizada F Sama M Ashafaq M Shahid M Ahmad Z A Siddiqi J Mat Chem C (RSC) (2017) 69 (22) 3336-3353 IF = 53

30 A disc-like Co7 cluster with a solvent dependent catecholase activity MN Ahamad F Sama MN Akhtar YC Chen ML Tong M Ahmad New J Chem 2017 41 (23) 14057-14061

31 Spectral characterization crystal structures and biological activities of iminodiacetate ternary complexes M Shahid Anjuli Sana Tasneem Mantasha I M Naqi Ahamad Farasha Sama K Fatma Z A Siddiqi J Mol Struct 2017 1146 424

32 Amino alcohols and benzoates-Friends or foes Tuning nuclearity of Cu(II) complexes structures magnetism DFT and TD-DFT studies and catecholase like activities Farasha Sama Ashish Kumar Dhara Muhammad Nadeem Akhtar Yan-Cong Chen Ming-Liang Tong Istikhar A Ansari Mukul Raizada Musheer Ahmad M Shahid Zafar A Siddiqi Dalton Trans 2017 46 9801

33 Synthesis and spectral characterization of 2-((2-hydroxybenzylidene)amino)-2-methylpropane-13-diol derived complexes molecular docking and antimicrobial studies I A Ansari F Sama M Raizada M Shahid R K Rajpoot Z A Siddiqi J Mol Struct (Elsevier) 1127 (2017) 479-488

34 Design structures and study of non-covalent interactions of mono- di- and tetranuclear complexes of a bifurcated quadridentate tripod ligand N-(aminopropyl)-diethanolamine F Sama I A Ansari M Raizada M Ahmad C M Nagaraja M Shahid A Kumar K Khan Z A Siddiqi New J Chem (RSC) (2017) 41 (5) 1959-1972

35 Design structural characterization and catalytic activity of incomplete dicubane clusters of N-substituted diethanolamines F Sama I A Ansari M Raizada M Ahmad Mo Ashafaq M Shahid B Das K Shankar Z A Siddiqi J Cluster Sci (Springer) 2017 28 (3) 1355-1377

36 New phthalimide-appended Schiff bases Studies of DNA binding molecular docking and antioxidant activities P S Nayab Rahisuddin I A Ansari A Ali M Shahid Luminescence (Wiley) 2017 32 (5) 829-838

2016

37 Structurally well-characterized new multinuclear Cu(II) and Zn(II) clusters X-ray crystallography theoretical studies and applications in catalysis I A Ansari F Sama M Raizada M Shahid M Ahmad Z A Siddiqi New J Chem (RSC) 2016 40 9840-9852

38 Isolation of proton transfer complexes containing 4‒picolinium as cation and pyridine‒26ndashdicarboxylate complex as anion Crystallographic and spectral investigations antioxidant activities and molecular docking studies Istikhar A Ansari F Sama M Shahid Rahisuddin R Arif M Khalid and Z A Siddiqi RSC Adv (RSC) 2016 6 11088

39 Synthesis crystal structures and spectral characterization of Cu(II) and Mn(II) complexes of 4-hydroxy-3-methoxybenzaldehyde antioxidant properties and molecular docking studies I A Ansari F Sama M Shahid M Ahmad Rahisuddin P S Nayab Z A Siddiqi J Coord Chem (TampF) (2016) 69 3336ndash3353

40 Synthesis Spectral Characterization X-ray and Magnetic Studies of Oxo-bridged Tetranuclear Coordination Polymers of Cobalt I A Ansari F Sama M Shahid M Khalid P K Sharma M Ahmad amp Z A Siddiqi J Inorg Organom Polym Mat 26 (2016) 178

2015

41 Isolation and Spectral Characterization of Complexes [FeL1ClH2O] and [FeL2ClH2O] (H2L1=N-(3-hydroxy-propyl)-2-[(3-hydroxy-propylcarbamoyl)-methyl]-amino-acetamide and H2L2=N-(2-hydroxy-ethyl)-2-[2-hydroxy-ethylcarbamoyl)-methyl]-amino-acetamide) 57Fe Moumlssbauer and Cyclic Voltammetric Investigations M Shahid Anjuli Mukul Raizada Farasha Sama Istikhar A Ansari Mohd Khalid I M Khan M Ahmad ZA Siddiqi Can Chem Trans 3 (2015) 354

42 Synthesis crystal structures and genotoxic studies of cis-micro-12-peroxo dicobalt(III) complexes M Shahid Armeen Siddique Istikhar A Ansari Farasha Sama Sandesh Chibber Mohd Khalid Zafar A Siddiqi Md Serajul Haque Faizi J Coord Chem 68 (2015) 848

2014

43 N1-Phenyl-N4-[(quinolin-2-yl)methylidene]benzene-14-diamine MSH Faizi A Mashrai S Garandel M Shahid Acta Cryst (2014) E70 o905-906

44 2266-Tetrabromo-3445-tetramethoxycyclohexanone MSH Faizi A Mashrai M Shahid Acta Cryst (2014) E70 o826

45 N1-((1H-imidazol)methylene)-N4-phenylbenzene-14-diamine MSH Faizi A Mashrai M Shahid M Ahmad Acta Cryst (2014) E70 o806

46 Isolation of a decavanadate cluster [H2V10O28][4-picH]4bull2H2O (4-pic=4-picoline) Crystal structure electrochemical characterization genotoxic and antimicrobial studies M Shahid PK Sharma Anjuli S Chibber ZA Siddiqi J Cluster Science 2014 (in press)

47 Designing and characterization of Fe(III) complexes of oxydiacetate containing α-diimine as auxiliary ligand 57Fe-

Moumlssbauer and cyclic voltammetric studies M Shahid P K Sharma Z A Siddiqi F Sama I A Ansari M Khalid J Mol Structure 1063 (2014) 313

48 Synthesis and characterization of a carboxylate bridged homodinuclear Co(II) complex Crystal structure of [Co2(Pda)2(H2O)5]middot2H2O (H2Pda = pyridine-26-dicorboxylic acid) Z A Siddiqi I A Ansari F Sama M Shahid IJIRSET 3 (2014) 8673

2013

49 Synthesis crystal structure and magnetic studies of tetranuclear hydroxo and ligand bridged [Co4(micro3-OH)2(micro2-dea)2(L-L)4]4Clmiddot8H2O [L-L= 22prime- bipyridine or 110-phenanthroline] complexes with mixed valence defect dicubane core Z A Siddiqi A Siddique M Shahid M Khalid Anjuli P K Sharma M Ahmad S Kumar Y Lan A K Powell Dalton Trans 42 (2013) 9513-9522

50 Synthesis structural characterization DNA binding studies and antitumor properties of tin(II)-oxydiacetate complexes containing α-diimine as auxiliary ligand Z A Siddiqi P K Sharma M Shahid M Khalid J Photochem Photobiol B Biology 125 (2013) 171-175

51 Spectroscopic Luminescence electrochemical and antimicrobial studies of lanthanide complexes of bis-

benzimidazole derived ligands Z A Siddiqi Anjuli M Shahid M Khalid P K Sharma A Siddique J Mol Structure 1037 (2013) 402-411

52 Synthesis and structural characterization of homo-dinuclear complexes [M2(dea)2(H2O)4] [M2(dea)2(Bipy)2] and [Fe2(dea)2(H2O)2(Cl)2] (M = Co Ni or Cu H2dea = diethanolamine) 57Fe Moumlssbauer and electrochemical investigations Z A Siddiqi A Siddique M Shahid P K Sharma Anjuli M Khalid J Mol Structure 1036 (2013) 209-215

53 H-bonded supramolecular assembly via proton transfer Isolation X-ray crystallographic characterization and SOD mimic activity of [Cu(dipic)2]2[PA-H]45H2O ZA Siddiqi M Khalid M Shahid S Kumar PK Sharma Armeen Siddique Anjuli J Mol Structure 1033 (2013) 98-103

2012

54 Superoxide scavenging and antimicrobial activities of novel transition metal complexes of oxydiacetate dianion as primary ligand Spectral characterization cyclic voltammetric investigations and crystal structure Z A Siddiqi P K Sharma M Shahid Anjuli A Siddique M Khalid and S Kumar Eur J Med Chem 57(2012) 102-111

55 Crystal Structure of a Mixed-Ligand Cu(II) Complex Forming Supramolecular Assembly via an Extensive H-Bonding and RingndashRing πndashπ Interactions ZA Siddiqi M Shahid M Khalid S Kumar Anjuli Armeen Siddique J Chem Crystallography 42 (2012) 1042-1045

56 Novel decavanadate cluster complexes [H2V10O28][LH]4nH2O (L= Imidazole n=2 or 2-methylimidazole n= 0)

Preparation characterization and genotoxic studies Z A Siddiqi Anjuli P K Sharma M Shahid A Siddique M Khalid and S Kumar J Mol Structure 1029 (2012) 86-91

57 Structural electrochemical characterization and SOD mimic activities of 1D chain or 3D network encouraged by unique μ2-bridging by adipate ion in mixed ligand complexes containing α-diimine as auxiliary ligand Z A Siddiqi PK Sharma M Shahid S Kumar Anjuli A Siddique Spectrochim Acta Part A 93 (2012) 280-289

2011

58 Synthesis spectral characterizations and biological studies of transition metal mixed ligand complexes X-ray crystal structures of [Cu(oda)(Bipy)(H2O)]4H2O and [VO(oda)(Bipy)]2H2O ZA Siddiqi PK Sharma M Shahid M Khalid S Kumar J Mol Structure 994 (2011) 295

59 Spectral thermal and electrochemical characterization of novel homo-dinuclear complexes [M2(H3DTPA)(H2O)6]Cl2middotxH2O (M = Cr2+ Mn2+ Co2+ Ni2+ or Cu2+) Z A Siddiqi S Noor M Shahid M Khalid Spectrochimica Acta Part A 78 (2011) 1386

2010

60 Spectral and Physico-chemical investigations of novel homo-bimetallic di-micro2-alkoxo bridged Schiff base complexes 57Fe Moumlssbauer parameters of the Fe(III) complex ZA Siddiqi M Khalid S Kumar M Shahid S Noor Spectrochimica Acta Part A 75 (2010) 841ndash845

61 Synthesis physico-chemical and spectral investigations of novel homo-bimetallic mixed-ligand complexes 57Fe Moumlssbauer parameters of [Fe2(imda)2(H2O)3Cl] ZA Siddiqi M Shahid M Khalid S Noor S Kumar Spectrochimica Acta Part A 75 (2010) 61ndash68

62 Antimicrobial and SOD activities of novel transition metal complexes of pyridine-26-dicarboxylic acid containing 4-picoline as auxiliary ligand ZA Siddiqi M Khalid S Kumar M Shahid S Noor Eur J Med Chem 45 (2010) 264ndash269

2009

63 Synthesis and single crystal X-ray structure of 4-picoline-(pyridine-26-dicarboxylato-NOOrsquo)copper(II) ZA Siddiqi M Khalid S Kumar M Shahid X-ray structure analysis online 9 (2009) 71ndash72

64 Novel homo-bimetallic complexes of [N10] macrocyclic ligand modified with tetrapeptide function biological activities spectral and cyclic voltammetric studies Z A Siddiqi S Kumar M Khalid M Shahid Spectrochimica Acta Part A 72 (2009) 970ndash974

65 Synthesis and spectral investigations of mononuclear [N6] [N8] and dinuclear [N10] complexes of polyamide macrocycles 57Fe Moumlssbauer parameters of Fe(III) complexes ZA Siddiqi S Kumar M Khalid M Shahid Spectrochimica Acta Part A 72 (2009) 616ndash620

66 Spectral studies of Fe(III) complexes of dipodal tridentate chelating agents ZA Siddiqi S Kumar M Khalid

M Shahid Spectrochimica Acta Part A 71 (2009) 1845ndash1850

67 Spectroscopic and antimicrobial studies of La3+ Pr3+ Nd3+ and Gd3+ complexes of a dipodal [NNN] chelating ligand ZA Siddiqi M Shahid M Khalid S Noor S Kumar Spectrochimica Acta Part A 74 (2009) 391ndash397

68 Synthesis crystal structure and in-vitro antitumor activity of carboxylate bridged dinuclear organotin(IV) complexes ZA Siddiqi M Shahid S Kumar M Khalid S Noor J Organomet Chem 694 (2009) 3768ndash3774

69 Antimicrobial and SOD activities of novel transition metal ternary complexes of iminodiacetic acid containing α-diimine as auxiliary ligand ZA Siddiqi M Shahid M Khalid S Kumar Eur J Med Chem 44 (2009) 2517ndash2522

Communicated papers

Polyhedron (2019) Inorg Chem Front (2019) MatChemFront (2019) Dalton Trans (2019) CrystGrowth Des (2019)

Conferences (Papers Read)

1 Emerging Trends in Advanced Chemistry (ETAC-08) held at Centre of Advanced Study Department of Chemistry University of Rajasthan Jaipur 8-10 March 2008 (Oral)

Title ldquoSpectroscopic and X-Ray Crystallographic Characterization of a Cu(II)- Mixed Ligand Iminodiacetaterdquo

2 Interdisciplinary Science Conference lsquoInterface between Chemistry and Biologyrsquo held at Centre for Interdisciplinary Research in Basic Sciences Jamia Millia Islamia (JMI) New Delhi 8th October 2009 (Poster) Title ldquoA novel pathway to synthesize polynuclear organotin(IV) supramolecular complexes Spectroscopic X-ray crystallographic and in-vitro cytotoxic studiesrdquo

3 12th CRSI National Symposium in Chemistry held at Indian Institute of Chemical Technology (IICT) Hyderabad 5thndash7th February 2010 (Poster)

Title ldquoSynthesis crystal structures and cytotoxic studies of novel benzimidazole derived complexes [Mn(BIm)(CH3OH)Cl2] and [Cu(BIm)Cl2]rdquo

4 National Symposium on Recent Trends in Chemical Sciences (NSRTCS-2010) held on 24-25th Feb 2010 at Department of Chemistry AMU Aligarh (Poster)

Title A novel homo-dinuclear mixed-valent [FeIII-FeII] ferredoxin analogue [Fe2(imda)2(H2O)3Cl] Synthesis Moumlssbauer and EPR spectral characterization

5 International Satellite Symposium on lsquoFree Radicals in Health and Diseasersquo Satellite Free Radical Research (SFRR) held at Department of Biochemistry AMU Aligarh (Poster) March 17-18 2009 Title ldquoSOD A natural antioxidant and its comparison with a synthetic antioxidant prepared in the laboratoryrdquo

6 International Conference on Chemistry Frontiers and Challenges 5-6 March 2011 Deptt of Chemistry

AMU Aligarh (Poster) Title Synthesis and X-ray crystallographic analyses of novel transition metal ternary complexes bearing 1D chains

and 3D supramolecular networks

7 National Conference on New Vistas In chemistry Daptt Of Chemistry AMU Aligarh 2-3 March 2012 (Poster) Title Synthesis and spectral investigations of oxydiacetate complexes containing heterocycle as auxiliary ligand 57Moumlssbauer genotoxic and antimicrobial studies

8 International Conference on Chemistry Frontiers and Challenges 2-3 March 2013 Deptt of Chemistry AMU Aligarh (Poster)

Title Heterometallic polynuclear Mnx-Lny clusters showing Single Molecule Magnet (SMM) behaviour Crystallography magnetism and cyclic voltammetric investigations

9 National Symposium on free radical research 6 March 2014 Department of Biochemistry AMU Aligarh (Poster)

Title Superoxide scavenging activities of novel transition metal complexes of oxydiacetate Crystal structure and cyclic voltammetric studies

10 National Symposium of Chemistry 22 March 2014 Department of Chemistry AMU Aligarh (Poster) Title Designing of mono- and di-nuclear high spin Fe(III) complexes of oxydiacetate ligand 57Fe-Moumlssbauer and

magnetic studies 11 National Conference on Interdisciplinary approach in chemical sciences Jamia millia islamia New Delhi 2015

(ORAL) Title Synthesis and spectral and X-ray crystallographic studies of proton transfer complexes of 4-picoline and pyridine-26ndashdicarboxylic acid

12 National Seminar on intellectual Property Right (IPR) University Polytechnic AMU Aligarh 2015 13 International Conference on recent advances in chemical sciences Department of Chemistry AMU Aligarh29-30

March 2016 (Poster) Title Single molecules magnets Designing strategies

14 Recent Advances in Chemical Sciences March 25-26 2017 Dept of Chemistry AMU Aligarh (Poster) Title Synthesis and structural characterization of polynuclear metal clusters

15 National Seminar on intellectual Property Right (IPR) University Polytechnic AMU Aligarh 2017 16 Emerging trends in chemical sciences 24-25 Feb 2018 Department of Chemistry Amu Aligarh (Poster) Title Structural investigation on some Cu-Gd complexes 17 Indo-French workshop cum conference on magnetism of molecules Solid State amp Structural Chemistry Unit (SSCU)

Indian Institute of Science (IISc) Bangalore 26-30 Nov 2018 (Poster) Title A novel Mn12Na2 polymer exhibiting single chain magnet (SCM) behavior

18 Emerging trends in Chemical Sciences 24-25 Feb 2019 Department of Chemistry AMU Aligarh (Attended)

Dr M Shahid

Page 8: Dr. M. SHAHID, · Fig. Crystal structure of the novel organotin(IV) compound, Fig. Mossbauer Spectra of a bimetallic complex at RT & LNT a potential antitumor agent isolated by Dr

35 Design structural characterization and catalytic activity of incomplete dicubane clusters of N-substituted diethanolamines F Sama I A Ansari M Raizada M Ahmad Mo Ashafaq M Shahid B Das K Shankar Z A Siddiqi J Cluster Sci (Springer) 2017 28 (3) 1355-1377

36 New phthalimide-appended Schiff bases Studies of DNA binding molecular docking and antioxidant activities P S Nayab Rahisuddin I A Ansari A Ali M Shahid Luminescence (Wiley) 2017 32 (5) 829-838

2016

37 Structurally well-characterized new multinuclear Cu(II) and Zn(II) clusters X-ray crystallography theoretical studies and applications in catalysis I A Ansari F Sama M Raizada M Shahid M Ahmad Z A Siddiqi New J Chem (RSC) 2016 40 9840-9852

38 Isolation of proton transfer complexes containing 4‒picolinium as cation and pyridine‒26ndashdicarboxylate complex as anion Crystallographic and spectral investigations antioxidant activities and molecular docking studies Istikhar A Ansari F Sama M Shahid Rahisuddin R Arif M Khalid and Z A Siddiqi RSC Adv (RSC) 2016 6 11088

39 Synthesis crystal structures and spectral characterization of Cu(II) and Mn(II) complexes of 4-hydroxy-3-methoxybenzaldehyde antioxidant properties and molecular docking studies I A Ansari F Sama M Shahid M Ahmad Rahisuddin P S Nayab Z A Siddiqi J Coord Chem (TampF) (2016) 69 3336ndash3353

40 Synthesis Spectral Characterization X-ray and Magnetic Studies of Oxo-bridged Tetranuclear Coordination Polymers of Cobalt I A Ansari F Sama M Shahid M Khalid P K Sharma M Ahmad amp Z A Siddiqi J Inorg Organom Polym Mat 26 (2016) 178

2015

41 Isolation and Spectral Characterization of Complexes [FeL1ClH2O] and [FeL2ClH2O] (H2L1=N-(3-hydroxy-propyl)-2-[(3-hydroxy-propylcarbamoyl)-methyl]-amino-acetamide and H2L2=N-(2-hydroxy-ethyl)-2-[2-hydroxy-ethylcarbamoyl)-methyl]-amino-acetamide) 57Fe Moumlssbauer and Cyclic Voltammetric Investigations M Shahid Anjuli Mukul Raizada Farasha Sama Istikhar A Ansari Mohd Khalid I M Khan M Ahmad ZA Siddiqi Can Chem Trans 3 (2015) 354

42 Synthesis crystal structures and genotoxic studies of cis-micro-12-peroxo dicobalt(III) complexes M Shahid Armeen Siddique Istikhar A Ansari Farasha Sama Sandesh Chibber Mohd Khalid Zafar A Siddiqi Md Serajul Haque Faizi J Coord Chem 68 (2015) 848

2014

43 N1-Phenyl-N4-[(quinolin-2-yl)methylidene]benzene-14-diamine MSH Faizi A Mashrai S Garandel M Shahid Acta Cryst (2014) E70 o905-906

44 2266-Tetrabromo-3445-tetramethoxycyclohexanone MSH Faizi A Mashrai M Shahid Acta Cryst (2014) E70 o826

45 N1-((1H-imidazol)methylene)-N4-phenylbenzene-14-diamine MSH Faizi A Mashrai M Shahid M Ahmad Acta Cryst (2014) E70 o806

46 Isolation of a decavanadate cluster [H2V10O28][4-picH]4bull2H2O (4-pic=4-picoline) Crystal structure electrochemical characterization genotoxic and antimicrobial studies M Shahid PK Sharma Anjuli S Chibber ZA Siddiqi J Cluster Science 2014 (in press)

47 Designing and characterization of Fe(III) complexes of oxydiacetate containing α-diimine as auxiliary ligand 57Fe-

Moumlssbauer and cyclic voltammetric studies M Shahid P K Sharma Z A Siddiqi F Sama I A Ansari M Khalid J Mol Structure 1063 (2014) 313

48 Synthesis and characterization of a carboxylate bridged homodinuclear Co(II) complex Crystal structure of [Co2(Pda)2(H2O)5]middot2H2O (H2Pda = pyridine-26-dicorboxylic acid) Z A Siddiqi I A Ansari F Sama M Shahid IJIRSET 3 (2014) 8673

2013

49 Synthesis crystal structure and magnetic studies of tetranuclear hydroxo and ligand bridged [Co4(micro3-OH)2(micro2-dea)2(L-L)4]4Clmiddot8H2O [L-L= 22prime- bipyridine or 110-phenanthroline] complexes with mixed valence defect dicubane core Z A Siddiqi A Siddique M Shahid M Khalid Anjuli P K Sharma M Ahmad S Kumar Y Lan A K Powell Dalton Trans 42 (2013) 9513-9522

50 Synthesis structural characterization DNA binding studies and antitumor properties of tin(II)-oxydiacetate complexes containing α-diimine as auxiliary ligand Z A Siddiqi P K Sharma M Shahid M Khalid J Photochem Photobiol B Biology 125 (2013) 171-175

51 Spectroscopic Luminescence electrochemical and antimicrobial studies of lanthanide complexes of bis-

benzimidazole derived ligands Z A Siddiqi Anjuli M Shahid M Khalid P K Sharma A Siddique J Mol Structure 1037 (2013) 402-411

52 Synthesis and structural characterization of homo-dinuclear complexes [M2(dea)2(H2O)4] [M2(dea)2(Bipy)2] and [Fe2(dea)2(H2O)2(Cl)2] (M = Co Ni or Cu H2dea = diethanolamine) 57Fe Moumlssbauer and electrochemical investigations Z A Siddiqi A Siddique M Shahid P K Sharma Anjuli M Khalid J Mol Structure 1036 (2013) 209-215

53 H-bonded supramolecular assembly via proton transfer Isolation X-ray crystallographic characterization and SOD mimic activity of [Cu(dipic)2]2[PA-H]45H2O ZA Siddiqi M Khalid M Shahid S Kumar PK Sharma Armeen Siddique Anjuli J Mol Structure 1033 (2013) 98-103

2012

54 Superoxide scavenging and antimicrobial activities of novel transition metal complexes of oxydiacetate dianion as primary ligand Spectral characterization cyclic voltammetric investigations and crystal structure Z A Siddiqi P K Sharma M Shahid Anjuli A Siddique M Khalid and S Kumar Eur J Med Chem 57(2012) 102-111

55 Crystal Structure of a Mixed-Ligand Cu(II) Complex Forming Supramolecular Assembly via an Extensive H-Bonding and RingndashRing πndashπ Interactions ZA Siddiqi M Shahid M Khalid S Kumar Anjuli Armeen Siddique J Chem Crystallography 42 (2012) 1042-1045

56 Novel decavanadate cluster complexes [H2V10O28][LH]4nH2O (L= Imidazole n=2 or 2-methylimidazole n= 0)

Preparation characterization and genotoxic studies Z A Siddiqi Anjuli P K Sharma M Shahid A Siddique M Khalid and S Kumar J Mol Structure 1029 (2012) 86-91

57 Structural electrochemical characterization and SOD mimic activities of 1D chain or 3D network encouraged by unique μ2-bridging by adipate ion in mixed ligand complexes containing α-diimine as auxiliary ligand Z A Siddiqi PK Sharma M Shahid S Kumar Anjuli A Siddique Spectrochim Acta Part A 93 (2012) 280-289

2011

58 Synthesis spectral characterizations and biological studies of transition metal mixed ligand complexes X-ray crystal structures of [Cu(oda)(Bipy)(H2O)]4H2O and [VO(oda)(Bipy)]2H2O ZA Siddiqi PK Sharma M Shahid M Khalid S Kumar J Mol Structure 994 (2011) 295

59 Spectral thermal and electrochemical characterization of novel homo-dinuclear complexes [M2(H3DTPA)(H2O)6]Cl2middotxH2O (M = Cr2+ Mn2+ Co2+ Ni2+ or Cu2+) Z A Siddiqi S Noor M Shahid M Khalid Spectrochimica Acta Part A 78 (2011) 1386

2010

60 Spectral and Physico-chemical investigations of novel homo-bimetallic di-micro2-alkoxo bridged Schiff base complexes 57Fe Moumlssbauer parameters of the Fe(III) complex ZA Siddiqi M Khalid S Kumar M Shahid S Noor Spectrochimica Acta Part A 75 (2010) 841ndash845

61 Synthesis physico-chemical and spectral investigations of novel homo-bimetallic mixed-ligand complexes 57Fe Moumlssbauer parameters of [Fe2(imda)2(H2O)3Cl] ZA Siddiqi M Shahid M Khalid S Noor S Kumar Spectrochimica Acta Part A 75 (2010) 61ndash68

62 Antimicrobial and SOD activities of novel transition metal complexes of pyridine-26-dicarboxylic acid containing 4-picoline as auxiliary ligand ZA Siddiqi M Khalid S Kumar M Shahid S Noor Eur J Med Chem 45 (2010) 264ndash269

2009

63 Synthesis and single crystal X-ray structure of 4-picoline-(pyridine-26-dicarboxylato-NOOrsquo)copper(II) ZA Siddiqi M Khalid S Kumar M Shahid X-ray structure analysis online 9 (2009) 71ndash72

64 Novel homo-bimetallic complexes of [N10] macrocyclic ligand modified with tetrapeptide function biological activities spectral and cyclic voltammetric studies Z A Siddiqi S Kumar M Khalid M Shahid Spectrochimica Acta Part A 72 (2009) 970ndash974

65 Synthesis and spectral investigations of mononuclear [N6] [N8] and dinuclear [N10] complexes of polyamide macrocycles 57Fe Moumlssbauer parameters of Fe(III) complexes ZA Siddiqi S Kumar M Khalid M Shahid Spectrochimica Acta Part A 72 (2009) 616ndash620

66 Spectral studies of Fe(III) complexes of dipodal tridentate chelating agents ZA Siddiqi S Kumar M Khalid

M Shahid Spectrochimica Acta Part A 71 (2009) 1845ndash1850

67 Spectroscopic and antimicrobial studies of La3+ Pr3+ Nd3+ and Gd3+ complexes of a dipodal [NNN] chelating ligand ZA Siddiqi M Shahid M Khalid S Noor S Kumar Spectrochimica Acta Part A 74 (2009) 391ndash397

68 Synthesis crystal structure and in-vitro antitumor activity of carboxylate bridged dinuclear organotin(IV) complexes ZA Siddiqi M Shahid S Kumar M Khalid S Noor J Organomet Chem 694 (2009) 3768ndash3774

69 Antimicrobial and SOD activities of novel transition metal ternary complexes of iminodiacetic acid containing α-diimine as auxiliary ligand ZA Siddiqi M Shahid M Khalid S Kumar Eur J Med Chem 44 (2009) 2517ndash2522

Communicated papers

Polyhedron (2019) Inorg Chem Front (2019) MatChemFront (2019) Dalton Trans (2019) CrystGrowth Des (2019)

Conferences (Papers Read)

1 Emerging Trends in Advanced Chemistry (ETAC-08) held at Centre of Advanced Study Department of Chemistry University of Rajasthan Jaipur 8-10 March 2008 (Oral)

Title ldquoSpectroscopic and X-Ray Crystallographic Characterization of a Cu(II)- Mixed Ligand Iminodiacetaterdquo

2 Interdisciplinary Science Conference lsquoInterface between Chemistry and Biologyrsquo held at Centre for Interdisciplinary Research in Basic Sciences Jamia Millia Islamia (JMI) New Delhi 8th October 2009 (Poster) Title ldquoA novel pathway to synthesize polynuclear organotin(IV) supramolecular complexes Spectroscopic X-ray crystallographic and in-vitro cytotoxic studiesrdquo

3 12th CRSI National Symposium in Chemistry held at Indian Institute of Chemical Technology (IICT) Hyderabad 5thndash7th February 2010 (Poster)

Title ldquoSynthesis crystal structures and cytotoxic studies of novel benzimidazole derived complexes [Mn(BIm)(CH3OH)Cl2] and [Cu(BIm)Cl2]rdquo

4 National Symposium on Recent Trends in Chemical Sciences (NSRTCS-2010) held on 24-25th Feb 2010 at Department of Chemistry AMU Aligarh (Poster)

Title A novel homo-dinuclear mixed-valent [FeIII-FeII] ferredoxin analogue [Fe2(imda)2(H2O)3Cl] Synthesis Moumlssbauer and EPR spectral characterization

5 International Satellite Symposium on lsquoFree Radicals in Health and Diseasersquo Satellite Free Radical Research (SFRR) held at Department of Biochemistry AMU Aligarh (Poster) March 17-18 2009 Title ldquoSOD A natural antioxidant and its comparison with a synthetic antioxidant prepared in the laboratoryrdquo

6 International Conference on Chemistry Frontiers and Challenges 5-6 March 2011 Deptt of Chemistry

AMU Aligarh (Poster) Title Synthesis and X-ray crystallographic analyses of novel transition metal ternary complexes bearing 1D chains

and 3D supramolecular networks

7 National Conference on New Vistas In chemistry Daptt Of Chemistry AMU Aligarh 2-3 March 2012 (Poster) Title Synthesis and spectral investigations of oxydiacetate complexes containing heterocycle as auxiliary ligand 57Moumlssbauer genotoxic and antimicrobial studies

8 International Conference on Chemistry Frontiers and Challenges 2-3 March 2013 Deptt of Chemistry AMU Aligarh (Poster)

Title Heterometallic polynuclear Mnx-Lny clusters showing Single Molecule Magnet (SMM) behaviour Crystallography magnetism and cyclic voltammetric investigations

9 National Symposium on free radical research 6 March 2014 Department of Biochemistry AMU Aligarh (Poster)

Title Superoxide scavenging activities of novel transition metal complexes of oxydiacetate Crystal structure and cyclic voltammetric studies

10 National Symposium of Chemistry 22 March 2014 Department of Chemistry AMU Aligarh (Poster) Title Designing of mono- and di-nuclear high spin Fe(III) complexes of oxydiacetate ligand 57Fe-Moumlssbauer and

magnetic studies 11 National Conference on Interdisciplinary approach in chemical sciences Jamia millia islamia New Delhi 2015

(ORAL) Title Synthesis and spectral and X-ray crystallographic studies of proton transfer complexes of 4-picoline and pyridine-26ndashdicarboxylic acid

12 National Seminar on intellectual Property Right (IPR) University Polytechnic AMU Aligarh 2015 13 International Conference on recent advances in chemical sciences Department of Chemistry AMU Aligarh29-30

March 2016 (Poster) Title Single molecules magnets Designing strategies

14 Recent Advances in Chemical Sciences March 25-26 2017 Dept of Chemistry AMU Aligarh (Poster) Title Synthesis and structural characterization of polynuclear metal clusters

15 National Seminar on intellectual Property Right (IPR) University Polytechnic AMU Aligarh 2017 16 Emerging trends in chemical sciences 24-25 Feb 2018 Department of Chemistry Amu Aligarh (Poster) Title Structural investigation on some Cu-Gd complexes 17 Indo-French workshop cum conference on magnetism of molecules Solid State amp Structural Chemistry Unit (SSCU)

Indian Institute of Science (IISc) Bangalore 26-30 Nov 2018 (Poster) Title A novel Mn12Na2 polymer exhibiting single chain magnet (SCM) behavior

18 Emerging trends in Chemical Sciences 24-25 Feb 2019 Department of Chemistry AMU Aligarh (Attended)

Dr M Shahid

Page 9: Dr. M. SHAHID, · Fig. Crystal structure of the novel organotin(IV) compound, Fig. Mossbauer Spectra of a bimetallic complex at RT & LNT a potential antitumor agent isolated by Dr

47 Designing and characterization of Fe(III) complexes of oxydiacetate containing α-diimine as auxiliary ligand 57Fe-

Moumlssbauer and cyclic voltammetric studies M Shahid P K Sharma Z A Siddiqi F Sama I A Ansari M Khalid J Mol Structure 1063 (2014) 313

48 Synthesis and characterization of a carboxylate bridged homodinuclear Co(II) complex Crystal structure of [Co2(Pda)2(H2O)5]middot2H2O (H2Pda = pyridine-26-dicorboxylic acid) Z A Siddiqi I A Ansari F Sama M Shahid IJIRSET 3 (2014) 8673

2013

49 Synthesis crystal structure and magnetic studies of tetranuclear hydroxo and ligand bridged [Co4(micro3-OH)2(micro2-dea)2(L-L)4]4Clmiddot8H2O [L-L= 22prime- bipyridine or 110-phenanthroline] complexes with mixed valence defect dicubane core Z A Siddiqi A Siddique M Shahid M Khalid Anjuli P K Sharma M Ahmad S Kumar Y Lan A K Powell Dalton Trans 42 (2013) 9513-9522

50 Synthesis structural characterization DNA binding studies and antitumor properties of tin(II)-oxydiacetate complexes containing α-diimine as auxiliary ligand Z A Siddiqi P K Sharma M Shahid M Khalid J Photochem Photobiol B Biology 125 (2013) 171-175

51 Spectroscopic Luminescence electrochemical and antimicrobial studies of lanthanide complexes of bis-

benzimidazole derived ligands Z A Siddiqi Anjuli M Shahid M Khalid P K Sharma A Siddique J Mol Structure 1037 (2013) 402-411

52 Synthesis and structural characterization of homo-dinuclear complexes [M2(dea)2(H2O)4] [M2(dea)2(Bipy)2] and [Fe2(dea)2(H2O)2(Cl)2] (M = Co Ni or Cu H2dea = diethanolamine) 57Fe Moumlssbauer and electrochemical investigations Z A Siddiqi A Siddique M Shahid P K Sharma Anjuli M Khalid J Mol Structure 1036 (2013) 209-215

53 H-bonded supramolecular assembly via proton transfer Isolation X-ray crystallographic characterization and SOD mimic activity of [Cu(dipic)2]2[PA-H]45H2O ZA Siddiqi M Khalid M Shahid S Kumar PK Sharma Armeen Siddique Anjuli J Mol Structure 1033 (2013) 98-103

2012

54 Superoxide scavenging and antimicrobial activities of novel transition metal complexes of oxydiacetate dianion as primary ligand Spectral characterization cyclic voltammetric investigations and crystal structure Z A Siddiqi P K Sharma M Shahid Anjuli A Siddique M Khalid and S Kumar Eur J Med Chem 57(2012) 102-111

55 Crystal Structure of a Mixed-Ligand Cu(II) Complex Forming Supramolecular Assembly via an Extensive H-Bonding and RingndashRing πndashπ Interactions ZA Siddiqi M Shahid M Khalid S Kumar Anjuli Armeen Siddique J Chem Crystallography 42 (2012) 1042-1045

56 Novel decavanadate cluster complexes [H2V10O28][LH]4nH2O (L= Imidazole n=2 or 2-methylimidazole n= 0)

Preparation characterization and genotoxic studies Z A Siddiqi Anjuli P K Sharma M Shahid A Siddique M Khalid and S Kumar J Mol Structure 1029 (2012) 86-91

57 Structural electrochemical characterization and SOD mimic activities of 1D chain or 3D network encouraged by unique μ2-bridging by adipate ion in mixed ligand complexes containing α-diimine as auxiliary ligand Z A Siddiqi PK Sharma M Shahid S Kumar Anjuli A Siddique Spectrochim Acta Part A 93 (2012) 280-289

2011

58 Synthesis spectral characterizations and biological studies of transition metal mixed ligand complexes X-ray crystal structures of [Cu(oda)(Bipy)(H2O)]4H2O and [VO(oda)(Bipy)]2H2O ZA Siddiqi PK Sharma M Shahid M Khalid S Kumar J Mol Structure 994 (2011) 295

59 Spectral thermal and electrochemical characterization of novel homo-dinuclear complexes [M2(H3DTPA)(H2O)6]Cl2middotxH2O (M = Cr2+ Mn2+ Co2+ Ni2+ or Cu2+) Z A Siddiqi S Noor M Shahid M Khalid Spectrochimica Acta Part A 78 (2011) 1386

2010

60 Spectral and Physico-chemical investigations of novel homo-bimetallic di-micro2-alkoxo bridged Schiff base complexes 57Fe Moumlssbauer parameters of the Fe(III) complex ZA Siddiqi M Khalid S Kumar M Shahid S Noor Spectrochimica Acta Part A 75 (2010) 841ndash845

61 Synthesis physico-chemical and spectral investigations of novel homo-bimetallic mixed-ligand complexes 57Fe Moumlssbauer parameters of [Fe2(imda)2(H2O)3Cl] ZA Siddiqi M Shahid M Khalid S Noor S Kumar Spectrochimica Acta Part A 75 (2010) 61ndash68

62 Antimicrobial and SOD activities of novel transition metal complexes of pyridine-26-dicarboxylic acid containing 4-picoline as auxiliary ligand ZA Siddiqi M Khalid S Kumar M Shahid S Noor Eur J Med Chem 45 (2010) 264ndash269

2009

63 Synthesis and single crystal X-ray structure of 4-picoline-(pyridine-26-dicarboxylato-NOOrsquo)copper(II) ZA Siddiqi M Khalid S Kumar M Shahid X-ray structure analysis online 9 (2009) 71ndash72

64 Novel homo-bimetallic complexes of [N10] macrocyclic ligand modified with tetrapeptide function biological activities spectral and cyclic voltammetric studies Z A Siddiqi S Kumar M Khalid M Shahid Spectrochimica Acta Part A 72 (2009) 970ndash974

65 Synthesis and spectral investigations of mononuclear [N6] [N8] and dinuclear [N10] complexes of polyamide macrocycles 57Fe Moumlssbauer parameters of Fe(III) complexes ZA Siddiqi S Kumar M Khalid M Shahid Spectrochimica Acta Part A 72 (2009) 616ndash620

66 Spectral studies of Fe(III) complexes of dipodal tridentate chelating agents ZA Siddiqi S Kumar M Khalid

M Shahid Spectrochimica Acta Part A 71 (2009) 1845ndash1850

67 Spectroscopic and antimicrobial studies of La3+ Pr3+ Nd3+ and Gd3+ complexes of a dipodal [NNN] chelating ligand ZA Siddiqi M Shahid M Khalid S Noor S Kumar Spectrochimica Acta Part A 74 (2009) 391ndash397

68 Synthesis crystal structure and in-vitro antitumor activity of carboxylate bridged dinuclear organotin(IV) complexes ZA Siddiqi M Shahid S Kumar M Khalid S Noor J Organomet Chem 694 (2009) 3768ndash3774

69 Antimicrobial and SOD activities of novel transition metal ternary complexes of iminodiacetic acid containing α-diimine as auxiliary ligand ZA Siddiqi M Shahid M Khalid S Kumar Eur J Med Chem 44 (2009) 2517ndash2522

Communicated papers

Polyhedron (2019) Inorg Chem Front (2019) MatChemFront (2019) Dalton Trans (2019) CrystGrowth Des (2019)

Conferences (Papers Read)

1 Emerging Trends in Advanced Chemistry (ETAC-08) held at Centre of Advanced Study Department of Chemistry University of Rajasthan Jaipur 8-10 March 2008 (Oral)

Title ldquoSpectroscopic and X-Ray Crystallographic Characterization of a Cu(II)- Mixed Ligand Iminodiacetaterdquo

2 Interdisciplinary Science Conference lsquoInterface between Chemistry and Biologyrsquo held at Centre for Interdisciplinary Research in Basic Sciences Jamia Millia Islamia (JMI) New Delhi 8th October 2009 (Poster) Title ldquoA novel pathway to synthesize polynuclear organotin(IV) supramolecular complexes Spectroscopic X-ray crystallographic and in-vitro cytotoxic studiesrdquo

3 12th CRSI National Symposium in Chemistry held at Indian Institute of Chemical Technology (IICT) Hyderabad 5thndash7th February 2010 (Poster)

Title ldquoSynthesis crystal structures and cytotoxic studies of novel benzimidazole derived complexes [Mn(BIm)(CH3OH)Cl2] and [Cu(BIm)Cl2]rdquo

4 National Symposium on Recent Trends in Chemical Sciences (NSRTCS-2010) held on 24-25th Feb 2010 at Department of Chemistry AMU Aligarh (Poster)

Title A novel homo-dinuclear mixed-valent [FeIII-FeII] ferredoxin analogue [Fe2(imda)2(H2O)3Cl] Synthesis Moumlssbauer and EPR spectral characterization

5 International Satellite Symposium on lsquoFree Radicals in Health and Diseasersquo Satellite Free Radical Research (SFRR) held at Department of Biochemistry AMU Aligarh (Poster) March 17-18 2009 Title ldquoSOD A natural antioxidant and its comparison with a synthetic antioxidant prepared in the laboratoryrdquo

6 International Conference on Chemistry Frontiers and Challenges 5-6 March 2011 Deptt of Chemistry

AMU Aligarh (Poster) Title Synthesis and X-ray crystallographic analyses of novel transition metal ternary complexes bearing 1D chains

and 3D supramolecular networks

7 National Conference on New Vistas In chemistry Daptt Of Chemistry AMU Aligarh 2-3 March 2012 (Poster) Title Synthesis and spectral investigations of oxydiacetate complexes containing heterocycle as auxiliary ligand 57Moumlssbauer genotoxic and antimicrobial studies

8 International Conference on Chemistry Frontiers and Challenges 2-3 March 2013 Deptt of Chemistry AMU Aligarh (Poster)

Title Heterometallic polynuclear Mnx-Lny clusters showing Single Molecule Magnet (SMM) behaviour Crystallography magnetism and cyclic voltammetric investigations

9 National Symposium on free radical research 6 March 2014 Department of Biochemistry AMU Aligarh (Poster)

Title Superoxide scavenging activities of novel transition metal complexes of oxydiacetate Crystal structure and cyclic voltammetric studies

10 National Symposium of Chemistry 22 March 2014 Department of Chemistry AMU Aligarh (Poster) Title Designing of mono- and di-nuclear high spin Fe(III) complexes of oxydiacetate ligand 57Fe-Moumlssbauer and

magnetic studies 11 National Conference on Interdisciplinary approach in chemical sciences Jamia millia islamia New Delhi 2015

(ORAL) Title Synthesis and spectral and X-ray crystallographic studies of proton transfer complexes of 4-picoline and pyridine-26ndashdicarboxylic acid

12 National Seminar on intellectual Property Right (IPR) University Polytechnic AMU Aligarh 2015 13 International Conference on recent advances in chemical sciences Department of Chemistry AMU Aligarh29-30

March 2016 (Poster) Title Single molecules magnets Designing strategies

14 Recent Advances in Chemical Sciences March 25-26 2017 Dept of Chemistry AMU Aligarh (Poster) Title Synthesis and structural characterization of polynuclear metal clusters

15 National Seminar on intellectual Property Right (IPR) University Polytechnic AMU Aligarh 2017 16 Emerging trends in chemical sciences 24-25 Feb 2018 Department of Chemistry Amu Aligarh (Poster) Title Structural investigation on some Cu-Gd complexes 17 Indo-French workshop cum conference on magnetism of molecules Solid State amp Structural Chemistry Unit (SSCU)

Indian Institute of Science (IISc) Bangalore 26-30 Nov 2018 (Poster) Title A novel Mn12Na2 polymer exhibiting single chain magnet (SCM) behavior

18 Emerging trends in Chemical Sciences 24-25 Feb 2019 Department of Chemistry AMU Aligarh (Attended)

Dr M Shahid

Page 10: Dr. M. SHAHID, · Fig. Crystal structure of the novel organotin(IV) compound, Fig. Mossbauer Spectra of a bimetallic complex at RT & LNT a potential antitumor agent isolated by Dr

57 Structural electrochemical characterization and SOD mimic activities of 1D chain or 3D network encouraged by unique μ2-bridging by adipate ion in mixed ligand complexes containing α-diimine as auxiliary ligand Z A Siddiqi PK Sharma M Shahid S Kumar Anjuli A Siddique Spectrochim Acta Part A 93 (2012) 280-289

2011

58 Synthesis spectral characterizations and biological studies of transition metal mixed ligand complexes X-ray crystal structures of [Cu(oda)(Bipy)(H2O)]4H2O and [VO(oda)(Bipy)]2H2O ZA Siddiqi PK Sharma M Shahid M Khalid S Kumar J Mol Structure 994 (2011) 295

59 Spectral thermal and electrochemical characterization of novel homo-dinuclear complexes [M2(H3DTPA)(H2O)6]Cl2middotxH2O (M = Cr2+ Mn2+ Co2+ Ni2+ or Cu2+) Z A Siddiqi S Noor M Shahid M Khalid Spectrochimica Acta Part A 78 (2011) 1386

2010

60 Spectral and Physico-chemical investigations of novel homo-bimetallic di-micro2-alkoxo bridged Schiff base complexes 57Fe Moumlssbauer parameters of the Fe(III) complex ZA Siddiqi M Khalid S Kumar M Shahid S Noor Spectrochimica Acta Part A 75 (2010) 841ndash845

61 Synthesis physico-chemical and spectral investigations of novel homo-bimetallic mixed-ligand complexes 57Fe Moumlssbauer parameters of [Fe2(imda)2(H2O)3Cl] ZA Siddiqi M Shahid M Khalid S Noor S Kumar Spectrochimica Acta Part A 75 (2010) 61ndash68

62 Antimicrobial and SOD activities of novel transition metal complexes of pyridine-26-dicarboxylic acid containing 4-picoline as auxiliary ligand ZA Siddiqi M Khalid S Kumar M Shahid S Noor Eur J Med Chem 45 (2010) 264ndash269

2009

63 Synthesis and single crystal X-ray structure of 4-picoline-(pyridine-26-dicarboxylato-NOOrsquo)copper(II) ZA Siddiqi M Khalid S Kumar M Shahid X-ray structure analysis online 9 (2009) 71ndash72

64 Novel homo-bimetallic complexes of [N10] macrocyclic ligand modified with tetrapeptide function biological activities spectral and cyclic voltammetric studies Z A Siddiqi S Kumar M Khalid M Shahid Spectrochimica Acta Part A 72 (2009) 970ndash974

65 Synthesis and spectral investigations of mononuclear [N6] [N8] and dinuclear [N10] complexes of polyamide macrocycles 57Fe Moumlssbauer parameters of Fe(III) complexes ZA Siddiqi S Kumar M Khalid M Shahid Spectrochimica Acta Part A 72 (2009) 616ndash620

66 Spectral studies of Fe(III) complexes of dipodal tridentate chelating agents ZA Siddiqi S Kumar M Khalid

M Shahid Spectrochimica Acta Part A 71 (2009) 1845ndash1850

67 Spectroscopic and antimicrobial studies of La3+ Pr3+ Nd3+ and Gd3+ complexes of a dipodal [NNN] chelating ligand ZA Siddiqi M Shahid M Khalid S Noor S Kumar Spectrochimica Acta Part A 74 (2009) 391ndash397

68 Synthesis crystal structure and in-vitro antitumor activity of carboxylate bridged dinuclear organotin(IV) complexes ZA Siddiqi M Shahid S Kumar M Khalid S Noor J Organomet Chem 694 (2009) 3768ndash3774

69 Antimicrobial and SOD activities of novel transition metal ternary complexes of iminodiacetic acid containing α-diimine as auxiliary ligand ZA Siddiqi M Shahid M Khalid S Kumar Eur J Med Chem 44 (2009) 2517ndash2522

Communicated papers

Polyhedron (2019) Inorg Chem Front (2019) MatChemFront (2019) Dalton Trans (2019) CrystGrowth Des (2019)

Conferences (Papers Read)

1 Emerging Trends in Advanced Chemistry (ETAC-08) held at Centre of Advanced Study Department of Chemistry University of Rajasthan Jaipur 8-10 March 2008 (Oral)

Title ldquoSpectroscopic and X-Ray Crystallographic Characterization of a Cu(II)- Mixed Ligand Iminodiacetaterdquo

2 Interdisciplinary Science Conference lsquoInterface between Chemistry and Biologyrsquo held at Centre for Interdisciplinary Research in Basic Sciences Jamia Millia Islamia (JMI) New Delhi 8th October 2009 (Poster) Title ldquoA novel pathway to synthesize polynuclear organotin(IV) supramolecular complexes Spectroscopic X-ray crystallographic and in-vitro cytotoxic studiesrdquo

3 12th CRSI National Symposium in Chemistry held at Indian Institute of Chemical Technology (IICT) Hyderabad 5thndash7th February 2010 (Poster)

Title ldquoSynthesis crystal structures and cytotoxic studies of novel benzimidazole derived complexes [Mn(BIm)(CH3OH)Cl2] and [Cu(BIm)Cl2]rdquo

4 National Symposium on Recent Trends in Chemical Sciences (NSRTCS-2010) held on 24-25th Feb 2010 at Department of Chemistry AMU Aligarh (Poster)

Title A novel homo-dinuclear mixed-valent [FeIII-FeII] ferredoxin analogue [Fe2(imda)2(H2O)3Cl] Synthesis Moumlssbauer and EPR spectral characterization

5 International Satellite Symposium on lsquoFree Radicals in Health and Diseasersquo Satellite Free Radical Research (SFRR) held at Department of Biochemistry AMU Aligarh (Poster) March 17-18 2009 Title ldquoSOD A natural antioxidant and its comparison with a synthetic antioxidant prepared in the laboratoryrdquo

6 International Conference on Chemistry Frontiers and Challenges 5-6 March 2011 Deptt of Chemistry

AMU Aligarh (Poster) Title Synthesis and X-ray crystallographic analyses of novel transition metal ternary complexes bearing 1D chains

and 3D supramolecular networks

7 National Conference on New Vistas In chemistry Daptt Of Chemistry AMU Aligarh 2-3 March 2012 (Poster) Title Synthesis and spectral investigations of oxydiacetate complexes containing heterocycle as auxiliary ligand 57Moumlssbauer genotoxic and antimicrobial studies

8 International Conference on Chemistry Frontiers and Challenges 2-3 March 2013 Deptt of Chemistry AMU Aligarh (Poster)

Title Heterometallic polynuclear Mnx-Lny clusters showing Single Molecule Magnet (SMM) behaviour Crystallography magnetism and cyclic voltammetric investigations

9 National Symposium on free radical research 6 March 2014 Department of Biochemistry AMU Aligarh (Poster)

Title Superoxide scavenging activities of novel transition metal complexes of oxydiacetate Crystal structure and cyclic voltammetric studies

10 National Symposium of Chemistry 22 March 2014 Department of Chemistry AMU Aligarh (Poster) Title Designing of mono- and di-nuclear high spin Fe(III) complexes of oxydiacetate ligand 57Fe-Moumlssbauer and

magnetic studies 11 National Conference on Interdisciplinary approach in chemical sciences Jamia millia islamia New Delhi 2015

(ORAL) Title Synthesis and spectral and X-ray crystallographic studies of proton transfer complexes of 4-picoline and pyridine-26ndashdicarboxylic acid

12 National Seminar on intellectual Property Right (IPR) University Polytechnic AMU Aligarh 2015 13 International Conference on recent advances in chemical sciences Department of Chemistry AMU Aligarh29-30

March 2016 (Poster) Title Single molecules magnets Designing strategies

14 Recent Advances in Chemical Sciences March 25-26 2017 Dept of Chemistry AMU Aligarh (Poster) Title Synthesis and structural characterization of polynuclear metal clusters

15 National Seminar on intellectual Property Right (IPR) University Polytechnic AMU Aligarh 2017 16 Emerging trends in chemical sciences 24-25 Feb 2018 Department of Chemistry Amu Aligarh (Poster) Title Structural investigation on some Cu-Gd complexes 17 Indo-French workshop cum conference on magnetism of molecules Solid State amp Structural Chemistry Unit (SSCU)

Indian Institute of Science (IISc) Bangalore 26-30 Nov 2018 (Poster) Title A novel Mn12Na2 polymer exhibiting single chain magnet (SCM) behavior

18 Emerging trends in Chemical Sciences 24-25 Feb 2019 Department of Chemistry AMU Aligarh (Attended)

Dr M Shahid

Page 11: Dr. M. SHAHID, · Fig. Crystal structure of the novel organotin(IV) compound, Fig. Mossbauer Spectra of a bimetallic complex at RT & LNT a potential antitumor agent isolated by Dr

69 Antimicrobial and SOD activities of novel transition metal ternary complexes of iminodiacetic acid containing α-diimine as auxiliary ligand ZA Siddiqi M Shahid M Khalid S Kumar Eur J Med Chem 44 (2009) 2517ndash2522

Communicated papers

Polyhedron (2019) Inorg Chem Front (2019) MatChemFront (2019) Dalton Trans (2019) CrystGrowth Des (2019)

Conferences (Papers Read)

1 Emerging Trends in Advanced Chemistry (ETAC-08) held at Centre of Advanced Study Department of Chemistry University of Rajasthan Jaipur 8-10 March 2008 (Oral)

Title ldquoSpectroscopic and X-Ray Crystallographic Characterization of a Cu(II)- Mixed Ligand Iminodiacetaterdquo

2 Interdisciplinary Science Conference lsquoInterface between Chemistry and Biologyrsquo held at Centre for Interdisciplinary Research in Basic Sciences Jamia Millia Islamia (JMI) New Delhi 8th October 2009 (Poster) Title ldquoA novel pathway to synthesize polynuclear organotin(IV) supramolecular complexes Spectroscopic X-ray crystallographic and in-vitro cytotoxic studiesrdquo

3 12th CRSI National Symposium in Chemistry held at Indian Institute of Chemical Technology (IICT) Hyderabad 5thndash7th February 2010 (Poster)

Title ldquoSynthesis crystal structures and cytotoxic studies of novel benzimidazole derived complexes [Mn(BIm)(CH3OH)Cl2] and [Cu(BIm)Cl2]rdquo

4 National Symposium on Recent Trends in Chemical Sciences (NSRTCS-2010) held on 24-25th Feb 2010 at Department of Chemistry AMU Aligarh (Poster)

Title A novel homo-dinuclear mixed-valent [FeIII-FeII] ferredoxin analogue [Fe2(imda)2(H2O)3Cl] Synthesis Moumlssbauer and EPR spectral characterization

5 International Satellite Symposium on lsquoFree Radicals in Health and Diseasersquo Satellite Free Radical Research (SFRR) held at Department of Biochemistry AMU Aligarh (Poster) March 17-18 2009 Title ldquoSOD A natural antioxidant and its comparison with a synthetic antioxidant prepared in the laboratoryrdquo

6 International Conference on Chemistry Frontiers and Challenges 5-6 March 2011 Deptt of Chemistry

AMU Aligarh (Poster) Title Synthesis and X-ray crystallographic analyses of novel transition metal ternary complexes bearing 1D chains

and 3D supramolecular networks

7 National Conference on New Vistas In chemistry Daptt Of Chemistry AMU Aligarh 2-3 March 2012 (Poster) Title Synthesis and spectral investigations of oxydiacetate complexes containing heterocycle as auxiliary ligand 57Moumlssbauer genotoxic and antimicrobial studies

8 International Conference on Chemistry Frontiers and Challenges 2-3 March 2013 Deptt of Chemistry AMU Aligarh (Poster)

Title Heterometallic polynuclear Mnx-Lny clusters showing Single Molecule Magnet (SMM) behaviour Crystallography magnetism and cyclic voltammetric investigations

9 National Symposium on free radical research 6 March 2014 Department of Biochemistry AMU Aligarh (Poster)

Title Superoxide scavenging activities of novel transition metal complexes of oxydiacetate Crystal structure and cyclic voltammetric studies

10 National Symposium of Chemistry 22 March 2014 Department of Chemistry AMU Aligarh (Poster) Title Designing of mono- and di-nuclear high spin Fe(III) complexes of oxydiacetate ligand 57Fe-Moumlssbauer and

magnetic studies 11 National Conference on Interdisciplinary approach in chemical sciences Jamia millia islamia New Delhi 2015

(ORAL) Title Synthesis and spectral and X-ray crystallographic studies of proton transfer complexes of 4-picoline and pyridine-26ndashdicarboxylic acid

12 National Seminar on intellectual Property Right (IPR) University Polytechnic AMU Aligarh 2015 13 International Conference on recent advances in chemical sciences Department of Chemistry AMU Aligarh29-30

March 2016 (Poster) Title Single molecules magnets Designing strategies

14 Recent Advances in Chemical Sciences March 25-26 2017 Dept of Chemistry AMU Aligarh (Poster) Title Synthesis and structural characterization of polynuclear metal clusters

15 National Seminar on intellectual Property Right (IPR) University Polytechnic AMU Aligarh 2017 16 Emerging trends in chemical sciences 24-25 Feb 2018 Department of Chemistry Amu Aligarh (Poster) Title Structural investigation on some Cu-Gd complexes 17 Indo-French workshop cum conference on magnetism of molecules Solid State amp Structural Chemistry Unit (SSCU)

Indian Institute of Science (IISc) Bangalore 26-30 Nov 2018 (Poster) Title A novel Mn12Na2 polymer exhibiting single chain magnet (SCM) behavior

18 Emerging trends in Chemical Sciences 24-25 Feb 2019 Department of Chemistry AMU Aligarh (Attended)

Dr M Shahid

Page 12: Dr. M. SHAHID, · Fig. Crystal structure of the novel organotin(IV) compound, Fig. Mossbauer Spectra of a bimetallic complex at RT & LNT a potential antitumor agent isolated by Dr

7 National Conference on New Vistas In chemistry Daptt Of Chemistry AMU Aligarh 2-3 March 2012 (Poster) Title Synthesis and spectral investigations of oxydiacetate complexes containing heterocycle as auxiliary ligand 57Moumlssbauer genotoxic and antimicrobial studies

8 International Conference on Chemistry Frontiers and Challenges 2-3 March 2013 Deptt of Chemistry AMU Aligarh (Poster)

Title Heterometallic polynuclear Mnx-Lny clusters showing Single Molecule Magnet (SMM) behaviour Crystallography magnetism and cyclic voltammetric investigations

9 National Symposium on free radical research 6 March 2014 Department of Biochemistry AMU Aligarh (Poster)

Title Superoxide scavenging activities of novel transition metal complexes of oxydiacetate Crystal structure and cyclic voltammetric studies

10 National Symposium of Chemistry 22 March 2014 Department of Chemistry AMU Aligarh (Poster) Title Designing of mono- and di-nuclear high spin Fe(III) complexes of oxydiacetate ligand 57Fe-Moumlssbauer and

magnetic studies 11 National Conference on Interdisciplinary approach in chemical sciences Jamia millia islamia New Delhi 2015

(ORAL) Title Synthesis and spectral and X-ray crystallographic studies of proton transfer complexes of 4-picoline and pyridine-26ndashdicarboxylic acid

12 National Seminar on intellectual Property Right (IPR) University Polytechnic AMU Aligarh 2015 13 International Conference on recent advances in chemical sciences Department of Chemistry AMU Aligarh29-30

March 2016 (Poster) Title Single molecules magnets Designing strategies

14 Recent Advances in Chemical Sciences March 25-26 2017 Dept of Chemistry AMU Aligarh (Poster) Title Synthesis and structural characterization of polynuclear metal clusters

15 National Seminar on intellectual Property Right (IPR) University Polytechnic AMU Aligarh 2017 16 Emerging trends in chemical sciences 24-25 Feb 2018 Department of Chemistry Amu Aligarh (Poster) Title Structural investigation on some Cu-Gd complexes 17 Indo-French workshop cum conference on magnetism of molecules Solid State amp Structural Chemistry Unit (SSCU)

Indian Institute of Science (IISc) Bangalore 26-30 Nov 2018 (Poster) Title A novel Mn12Na2 polymer exhibiting single chain magnet (SCM) behavior

18 Emerging trends in Chemical Sciences 24-25 Feb 2019 Department of Chemistry AMU Aligarh (Attended)

Dr M Shahid