durability of bonded aerospace structures...6300 psi! toughened ! film! cytec fm 300-2k (0.08 psf)!...

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JAMS 2014 Technical Review March 25-26, 2014 Durability of Bonded Aerospace Structures Dr. Lloyd Smith Harrison Scarborough Washington State University

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Page 1: Durability of Bonded Aerospace Structures...6300 psi! Toughened ! Film! Cytec FM 300-2K (0.08 psf)! 35 in-lb/in! Metal to Metal Climbing Drum! 5900 psi! Brittle! Film! Hysol EA 9394!

JAMS 2014 Technical Review March 25-26, 2014

Durability of Bonded Aerospace Structures Dr. Lloyd Smith Harrison Scarborough Washington State University

Page 2: Durability of Bonded Aerospace Structures...6300 psi! Toughened ! Film! Cytec FM 300-2K (0.08 psf)! 35 in-lb/in! Metal to Metal Climbing Drum! 5900 psi! Brittle! Film! Hysol EA 9394!

Introduction

Why use adhesives? •  High strength •  Low weight •  Reduced holes or no holes •  Join thin materials •  Join dissimilar materials •  High fatigue resistance

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Significant use aboard current and future aircraft.

Low confidence in our ability to

describe durability.

Page 3: Durability of Bonded Aerospace Structures...6300 psi! Toughened ! Film! Cytec FM 300-2K (0.08 psf)! 35 in-lb/in! Metal to Metal Climbing Drum! 5900 psi! Brittle! Film! Hysol EA 9394!

Introduction

•  Aim

–  Consider the relation between adhesive quasi-static and fatigue performance. §  Shear and peel stress §  Toughened and brittle systems

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Page 4: Durability of Bonded Aerospace Structures...6300 psi! Toughened ! Film! Cytec FM 300-2K (0.08 psf)! 35 in-lb/in! Metal to Metal Climbing Drum! 5900 psi! Brittle! Film! Hysol EA 9394!

Literature Review

•  Fatigue response of double cantilever beam specimen – Azari et al.

•  Variable amplitude fatigue testing of single Lap shear specimen – Shenoy et al.

•  Fatigue performance versus scarf angle – Jen

None address the role of toughness

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Page 5: Durability of Bonded Aerospace Structures...6300 psi! Toughened ! Film! Cytec FM 300-2K (0.08 psf)! 35 in-lb/in! Metal to Metal Climbing Drum! 5900 psi! Brittle! Film! Hysol EA 9394!

•  Wide Area Lap Shear

•  Double Cantilever Beam

Quasi-static Testing

Number of Coupons   Adherend   Adhesive  

Qua

si-S

tatic

 

5   2024-T3   FM300-2  

WA

LS  5   2024-T3   EA9696  

5   2024-T3   EA9394  

5   2024-T3   EA9380.05  

5   2024-T3   FM300-2  

DC

B  5   2024-T3   EA9696  

5   2024-T3   EA9394  

5   2024-T3   EA9380.05  

5

adopted from [2]

Page 6: Durability of Bonded Aerospace Structures...6300 psi! Toughened ! Film! Cytec FM 300-2K (0.08 psf)! 35 in-lb/in! Metal to Metal Climbing Drum! 5900 psi! Brittle! Film! Hysol EA 9394!

•  Double Cantilever Beam

•  Scarf

Fatigue Testing

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Number of Coupons   Adherend   Adhesive  

Fatig

ue  

5   2024-T3   FM300-2  

DC

B  5   2024-T3   EA9696  

5   2024-T3   EA9394  

5   2024-T3   EA9380.05  

25   2024-T3   FM300-2  

Sca

rf Jo

int  

25   2024-T3   EA9696  

25   2024-T3   EA9394  

25   2024-T3   EA9380.05  adopted from [1]

adopted from [2]

Page 7: Durability of Bonded Aerospace Structures...6300 psi! Toughened ! Film! Cytec FM 300-2K (0.08 psf)! 35 in-lb/in! Metal to Metal Climbing Drum! 5900 psi! Brittle! Film! Hysol EA 9394!

Adhesive Selection

•  65% variation in Peel Strength •  33% variation in Lap Shear Strength

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Adhesive   Peel Strength   Peel Test  

Tensile Lap Shear Strength  

Toughness   Form  

Hysol EA 9696 (0.060 psf)   100 in-lb/in   Metal to Metal Climbing Drum   6300 psi   Toughened   Film  

Cytec FM 300-2K (0.08 psf)   35 in-lb/in   Metal to Metal Climbing Drum   5900 psi   Brittle   Film  

Hysol EA 9394   20 lb/in   Floating Roller Peel Strength   4200 psi   Brittle   Paste  

Hysol EA 9380.05   *   *   *   Toughened   Paste  

*No data available

Page 8: Durability of Bonded Aerospace Structures...6300 psi! Toughened ! Film! Cytec FM 300-2K (0.08 psf)! 35 in-lb/in! Metal to Metal Climbing Drum! 5900 psi! Brittle! Film! Hysol EA 9394!

Adherend Selection

•  2024-T3 Aluminum –  High fatigue resistance –  Higher stiffness compared to 6061-T6 –  Lower corrosion resistance

§  Phosphoric acid anodized per BAC5555 both sides §  Primed per BAC5514-589 using Cytec Engineered Materials

BR6747-1 Bonding Primer

–  Common in aerospace structures

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Page 9: Durability of Bonded Aerospace Structures...6300 psi! Toughened ! Film! Cytec FM 300-2K (0.08 psf)! 35 in-lb/in! Metal to Metal Climbing Drum! 5900 psi! Brittle! Film! Hysol EA 9394!

Finite Element Analysis (FEA)

•  Abaqus

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1”x0.25”x6” – 2,000 lb load

Page 10: Durability of Bonded Aerospace Structures...6300 psi! Toughened ! Film! Cytec FM 300-2K (0.08 psf)! 35 in-lb/in! Metal to Metal Climbing Drum! 5900 psi! Brittle! Film! Hysol EA 9394!

Finite Element Analysis (FEA)

•  Peel stress along line A-B

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A  

B  

C  

10 degree scarf joint will provide shear stress testing with minimal

peel stresses. -­‐1400  

-­‐1200  

-­‐1000  

-­‐800  

-­‐600  

-­‐400  

-­‐200  

0  0   5   10   15   20   25   30   35   40   45  

Average  Pe

el  Stress  (psi)  

Scarf  Angle  (degrees)  

Page 11: Durability of Bonded Aerospace Structures...6300 psi! Toughened ! Film! Cytec FM 300-2K (0.08 psf)! 35 in-lb/in! Metal to Metal Climbing Drum! 5900 psi! Brittle! Film! Hysol EA 9394!

Summary

•  Compare static and fatigue response •  Consider the roll of toughness on fatigue •  Consider shear and peel dominated stress

•  Results will lead to improved life prediction methodologies

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