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DET NORSKE VERITAS Energy Report Ballast Tank Coating Test of JOTACOTE UNIVERSAL 80 on MUKI Z 2001 Jotun AS DNV Reg. No. / Report No. 128OB65-7 / 2009-5730 Rev. No. 00, 2010-01-21

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DET NORSKE VERITAS

Energy Report

Ballast Tank Coating Test of JOTACOTE UNIVERSAL 80 on

MUKI Z 2001

Jotun AS

DNV Reg. No. / Report No. 128OB65-7 / 2009-5730

Rev. No. 00, 2010-01-21

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Report for Jotun A/S

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DNV Reg. No.: 128OB65-7 Revision No.: 00 Date : 2010-01-21 Page ii of ii

Table of Contents

1 INTRODUCTION ............................................................................................................. 1

2 SCOPE OF WORK ........................................................................................................... 1

3 WORK CARRIED OUT PRIOR TO EXPOSURE ....................................................... 1

3.1 Primary surface preparation ....................................................................................... 1

3.2 Application ................................................................................................................. 2 3.2.1 Application procedure....................................................................................... 2 3.2.2 Panel coding...................................................................................................... 4 3.2.3 Dry film thickness............................................................................................. 5

3.3 Pinhole detection ........................................................................................................ 7

4 EXPOSURE........................................................................................................................ 7

5 PRODUCT IDENTIFICATION ...................................................................................... 7

6 EXAMINATIONS AND TESTS CARRIED OUT AFTER EXPOSURE.................... 8

7 EVALUATION OF TEST RESULTS ............................................................................. 9

8 CONCLUSION .................................................................................................................. 9

9 REFERENCES ................................................................................................................ 10

Appendix A Meteorological data of weathering period Appendix B Infrared spectra Appendix C Detailed test results Appendix D Photo documentation

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1 INTRODUCTION The coating system, JOTACOTE UNIVERSAL 80, applied to steel panels shop primed with Muki Z 2001 has been tested in accordance with the IMO Performance Standard for Protective Coatings /1/.

2 SCOPE OF WORK The following work and tests have been performed by JOTUN AS at the JOTUN AS test laboratory in Sandefjord, Norway, partly under supervision of a representative from DNV: • Surface preparations as described in Table 1 and 2 • Application processes as documented in Table 3 • Two months outdoor weathering of the shop primed test panels The following work and tests have been performed by DNV at the DNV Energy laboratory in Bergen, Norway: • Identification of the coating system by means of determination of density and infrared (IR)

spectra • Total dry film thickness measurements and pinhole detection on the test panels before testing • 180 days exposure in an exposure tank with wave movement (confer Figure 1 for details) • 180 days in dry heat (confer Figure 1 for details) • 180 days in condensation chamber (confer Figure 1 for details) • Evaluation of testing performed after exposure, including visual check for rust and blisters,

undercutting from scribe, adhesion measurements and coating flexibility • Evaluation of cathodic protection during wave tank exposure

3 WORK CARRIED OUT PRIOR TO EXPOSURE 3.1 Primary surface preparation

The primary surface preparation was carried out as described in Table 1.

Table 1 Primary surface preparation data* Surface preparation date November 2008 Surface preparation method Blast cleaning with Alsil. A3

Blasting standard Sa 2½

Roughness Rmax: 50-75 microns

Water soluble salts Standard used: ISO 8502: The Bresle Method, measured 15 mg/m2

Dust and abrasive inclusions No dust or abrasive contaminations were observed on the surface

* Data given by Jotun AS

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3.2 Application 3.2.1 Application procedure MUKI Z 2001 was applied to the test panels according to the application data given in Table 3.

The shop primed test panels were weathered outdoors for two months. Details on the weathering process and followed cleaning of the test panels is provided in Table 2, while further meteorological data of the weathering period is attached as Appendix A.

Table 2 Secondary surface preparation and weathering details

Weathering site (outdoor) At the JOTUN AS site in Sandefjord, Norway

Start of weathering 2008-12-29

Stop of weathering 2009-03-01

Preparation of test panel after the weathering period Washed with fresh water. 12 mg/m2 water soluble salts measured

One coat of JOTACOTE UNIVERSAL 80 (Al/Bronze) and one coat of JOTACOTE UNIVERSAL 80 (Al) were applied to the weathered and cleaned shop primed test panels. The complete application data are given in Table 3.

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Table 3 Application data

Coating data Shop primer 1st coat 2nd coat

MUKI Z 2001 JOTACOTE UNIVERSAL 80

JOTACOTE UNIVERSAL 80 Paint system

Grey Al/Bronze Al

Manufacturer JOTUN AS

Date 2008-12-16 2009-04-23 2009-04-23

Time 13:35 09:30 15:10

Batch no. Liquid / Comp A: P3781055

Base / Comp A: Lab made 19.1.2009

Base / Comp A: Lab made 19.1.2009

Batch no. Paste / Comp B : P3781054

Hardener / Comp B : Lab made 19.1.2009

Hardener / Comp B : Lab made 19.1.2009

Thinner name (if used) NA Jotun no. 17 Jotun no. 17

Batch no. thinner NA NA NA

Method of application Airless spray Airless spray Airless spray

Equipment used (pressure ratio) WIWA (60:1) WIWA (60:1) WIWA (60:1)

Air pressure at nozzle [bar] 150 150 150

Size nozzle [inch] 0.017 0.019 0.017

Fan width [º] 60 60 60

Mix. ratio [weight%] A:B = 40:60 A:B = 100:20 A:B = 100:20 Volume solids [%] 28 80 80

Wet film thickness [µm] 70 225 200

Dry film thickness [µm] 20 Average ca 160 Confer Table 4

Thinner [volume%] 0 10 10

Air temperature [ºC] 23 19 26

Humidity [% RH] 46 42 40

Steel temp. [ºC] 21 19 26

Dew point [ºC] ≈ 11 ≈ 6 ≈ 11 Comments: Present during the application of shop primer: Terje Aamodt, Reidar J. Pettersen, Cecilie Clasen, Odd Arntzen and Phuoc van Hoang – Jotun AS. Nedim Kaniza, Bodycote. Present during the application of 1st and 2nd coat: Reidar J. Pettersen, Cecilie Clasen, Odd Arntzen and Terje Aamodt – Jotun AS. Vidar Kvamme – Det Norske Veritas.

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3.2.2 Panel coding

The panels were coded with the unique DNV system name J24Z followed by a suffix specific for every panel’s position during the six-month exposure testing as shown in Figure 1.

Figure 1 Panel coding

H

W1 top

C1 C2 R1

W4 side (not cooled)

W3 side (cooled)

W2 bottom

Wave tank (size: 400x200 mm)

Condensation chamber (size: 150x150 mm)

Heating cabinet (size: 400x200 mm)

anode

artificial holiday

scribe scribe

U-beam U-beam

scribe

Reference (size: 150x150 mm)

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3.2.3 Dry film thickness The dry film thickness (DFT) measurements of the total coat were carried out by means of a calibrated PosiTector 6000 using the template shown in Figure 2. Table 4 shows the results from the measurements of the total dry film thickness.

Panel coding on the reverse side

21 3

54 6

87 9

1110 12

1413 15

Panel coding on the reverse side

1 2 3

7 8 9

4 5 6

Figure 2 DFT measurements locations

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Table 4 Results from the DFT measurements of the total coat, values are given in µm (20 µm subtracted for shop primer)

Panel Measuring point

(according to Figure 2) W1 W2 W3 W4 H C1 C2 R1 Total

1 322 328 328 320 326 334 331 368

2 364 340 321 352 346 321 330 336

3 334 322 322 330 320 320 323 308

4 324 322 298 352 320 323 351 355

5 340 350 326 330 326 320 336 348

6 296 326 322 320 282 332 314 352

7 310 310 322 328 282 323 324 379

8 350 352 329 324 340 290 328 382

9 324 320 320 308 322 325 332 354

10 336 322 322 360 328

11 344 340 356 330 338

12 322 326 320 324 326

13 320 322 321 320 330

14 330 326 329 366 368

15 322 296 289 346 324

Max 364 352 356 366 368 334 351 382 382

Min 296 296 289 308 282 290 314 308 282

Average 329 327 322 334 325 321 330 354 329

StDev 17 14 15 17 22 13 10 23 18

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3.3 Pinhole detection

Pinhole detection was performed on the coated test panel before the tank exposure. The detection was carried out by means of an Elcometer 269 Pinhole detector at 90 volts. The results from the pinhole detection are presented in Table 6.

4 EXPOSURE The exposure in the simulated ballast wave, condensation chamber and heating cabinet was carried out according to the IMO Performance Standard for Protective Coatings /1/. The exposure was started 2008-06-15 and terminated 2009-12-11.

5 PRODUCT IDENTIFICATION

The density of each component of the coating system as described in Table 3 was determined by means of an Erichsen Mod. 290/1 pyknometer based on ISO 2811-1 /5/. Furthermore, IR spectra of all components were recorded on a Nicolet Protégé 460 FT-IR spectrometer. The results from the paint identification are listed in Table 5 and Appendix B respectively.

Table 5 Product identification analysis

Product Batch no. Density [g/ml] Infrared identification

P3781054 2.07* Confer Appendix B, Figure B1 MUKI Z 2001 (Paste / Comp B)

FR156121971** 2.06** NA

MUKI Z 2001 (Liquid / Comp A)

P3781055 0.91 Confer Appendix B, Figure B2

JOTACOTE UNIVERSAL 80, Al/Bronze (Base / Comp A)

Lab made 19.01.2009 1.62 Confer Appendix B, Figure B3

JOTACOTE UNIVERSAL 80, Al/Bronze (Hardener / Comp B)

Lab made 19.01.2009 0.98 Confer Appendix B, Figure B4

Lab made 19.01.2009 NA*** Confer Appendix B, Figure B5 JOTACOTE UNIVERSAL 80,

Al (Base / Comp A) Lab made 2009.07.01** 1.62** NA

JOTACOTE UNIVERSAL 80, Al (Hardener / Comp B)

Lab made 19.01.2009 0.98 Confer Appendix B, Figure B6

* Sample of MUKI Z 2001, batch P3781054, provided DNV by Jotun AS. This sample was found not proper, due to low viscosity. Density of this product was measured by Jotun AS, and stated to be 2.07 g/ml. ** Sample provided by Jotun AS, analysis performed by DNV. *** Jotun AS did not provide DNV with enough paint to perform density analysis.

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6 EXAMINATIONS AND TESTS CARRIED OUT AFTER EXPOSURE

The visual inspection for blisters and rust as well as the adhesion testing were carried out according to specifications and standards referred to in the IMO Performance Standard for Protective Coatings /1/. In addition, the evaluation of cathodic protection was performed in accordance with ISO 15711:2003 /5/, ASTM G8:1996 /6/ and further IACS Rec. No. 101 /7/, interpretation details are given in the present report. The results of the examinations are schematically given in Table 6 and more detailed in Appendix C. Pictures of the panels after exposure as well as pictures of the adhesion tests are enclosed as Appendix D.

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7 EVALUATION OF TEST RESULTS

The test results have been evaluated in accordance with the requirements for epoxy-based systems on shop primed and two-month weathered steel substrate stated in the Performance Standard for Protective Coatings /1/. The results from this evaluation are presented in Table 6.

Table 6 Results from evaluation of the coated test samples

Test parameter Acceptance criteria /1/ Test results Evaluation

Blisters on panel 1) No blisters No blisters Passed

Rust on panel 1) No rust No rust Passed

Number of pinholes 2) 0 0 Passed

8.4 Adhesion values – average wave tank panels [MPa] 3)

> 3.5 adhesive failure ≥ 3 cohesive failure Total adhesive: 0 %

Total cohesive: 100 %

Passed

8.1 Adhesion values –average condensation chamber panels [MPa] 4)

> 3.5 adhesive failure ≥ 3 cohesive failure Total adhesive: 0 %

Total cohesive: 100 %

Passed

Current demand – wave tank bottom panel [mA/m2] 5) < 5 1.83 Passed

Cathodic disbondment – wave tank bottom panel [mm] 5) < 8 3 - 4 Passed

Undercutting from scribes – average maxima of wave tank panels [mm] 6) < 8 ≈ 1.7 Passed

U-bar / U-beam

Any defects, cracking or detachment at the angle or weld will lead to system being failed.

No defects, cracking or detachment

Passed

1) Confer Appendix C, Table C1 for details 2) Confer chapter 3.3 for details 3) Confer Appendix C, Table C2 for details 4) Confer Appendix C, Table C3 for details 5) Confer Appendix C, Table C5 for details 6) Confer Appendix C, Table C6 for details

8 CONCLUSION Based on the results and evaluations described in the present report, the coating system, one coat of JOTACOTE UNIVERSAL 80 (Al/Bronze) and one coat of JOTACOTE UNIVERSAL 80 (Al), applied to steel panels shop primed with MUKI Z 2001, all products by JOTUN AS, has passed the test requirements given in the IMO Performance Standard for Protective Coatings /1/.

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9 REFERENCES

/1/ IMO MSC.215(82):2006 Performance Standard for Protective Coatings for dedicated sea water ballast tanks in all types of ships and double-side skin spaces of bulk carriers (including all official standards referred to therein).

/2/ ISO 8503-4:1988 Preparation of steel substrates before application of paints and related products - Surface roughness characteristics of blast-cleaned steel substrates - Part 4: Method for the calibration of ISO surface profile comparators and for the determination of surface profile - Stylus instrument procedure.

/3/ ISO 8502-6:2006 Preparation of steel substrates before application of paints and related products – Tests for the assessment of surface cleanliness – Part 6: Extraction of soluble contaminants for analysis - The Bresle method.

ISO 8502-9:1998 Preparation of steel substrates before application of paints and related products – Tests for the assessment of surface cleanliness Part 9: Field method for the conductometric determination of water-soluble salts.

/4/ ISO 2811-1:1997 Paint and varnishes - Determination of density – Part 1: Pyknometer method.

/5/ ISO 15711-2:2002 Paints and varnishes - Determination of resistance to cathodic disbonding of coatings exposed to sea water.

/6/ ASTM G8:1996 Standard test method for cathodic disbonding of pipeline coats

/7/ IACS Rec. No. 101: 2008 Model Report for IMO Resolution MSC.215(82) Annex 1 “Test Procedures for Coating Qualification”.

/8/ ISO 4628-2:2003 Paint and varnishes - Evaluation of degradation of coatings - Designation of quantity and size of defects, and of intensity of uniform changes in appearance - Part 2: Assessment of degree of blistering.

/9/ ISO 4628-3:2003 Paint and varnishes - Evaluation of degradation of coatings - Designation of quantity and size of defects, and of intensity of uniform changes in appearance - Part 3: Assessment of degree of rusting.

/10/ ISO 4628-8:2005, (section 5.3.1) Paints and varnishes - Evaluation of degradation of coatings - Designation of intensity, quantity and size of common types of defects, and of intensity of uniform changes in appearance - Part 8: Assessment of degree of delamination and corrosion around a scribe.

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APPENDIX A

METEOROLOGICAL DATA OF WEATHERING PERIOD

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The weathering of the shop primed test panel was carried out at the JOTUN AS site in Sandefjord, Norway. The meteorological data was obtained from the Norwegian Meteorological Institute. Melsom is the name of the nearest weather station that records temperature. Melsom is located a few km from Sandefjord.

Figure A1 Temperature variations [ºC] for January 2009

Figure A2 Daily precipitation [mm] for January 2009

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Figure A3 Temperature variations [ºC] for February 2009

Figure A4 Daily precipitation [mm] for February 2009

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APPENDIX B

INFRARED SPECTRA

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3999,7 3600 3200 2800 2400 2000 1800 1600 1400 1200 1000 800 649,90,000

0,01

0,02

0,03

0,04

0,05

0,06

0,07

0,08

0,09

0,10

0,11

0,12

0,13

0,14

0,15

0,16

0,17

0,18

0,19

0,20

0,21

0,22

0,23

0,24

0,25

0,26

0,271

1/cm

ARBITRARY

Figure B1 IR spectra of MUKI Z 2001 (binder phase of paste), batch no. P3781054

3999,7 3600 3200 2800 2400 2000 1800 1600 1400 1200 1000 800 649,90,000

0,02

0,04

0,06

0,08

0,10

0,12

0,14

0,16

0,18

0,20

0,22

0,24

0,26

0,28

0,30

0,32

0,34

0,36

0,38

0,40

0,42

0,44

0,46

0,48

0,50

0,52

0,54

0,56

0,58

0,600,611

1/cm

ARBITRARY

Figure B2 IR spectra of MUKI Z 2001 (liquid), batch no. P3781055

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3999,7 3600 3200 2800 2400 2000 1800 1600 1400 1200 1000 800 649,90,000

0,02

0,04

0,06

0,08

0,10

0,12

0,14

0,16

0,18

0,20

0,22

0,24

0,26

0,28

0,30

0,32

0,34

0,36

0,372

1/cm

ARBITRARY

Figure B3 IR spectra of JOTACOTE UNIVERSAL 80 (binder phase of base, Al/Bronze), batch no.: Lab made 19.01.2009

3999,7 3600 3200 2800 2400 2000 1800 1600 1400 1200 1000 800 649,90,000

0,01

0,02

0,03

0,04

0,05

0,06

0,07

0,08

0,09

0,10

0,11

0,12

0,13

0,14

0,15

0,16

0,17

0,178

1/cm

ARBITRARY

Figure B4 IR spectra of JOTACOTE UNIVERSAL 80 (hardener, Al/Bronze), batch no.: Lab made 19.01.2009

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3999,7 3600 3200 2800 2400 2000 1800 1600 1400 1200 1000 800 649,90,000

0,02

0,04

0,06

0,08

0,10

0,12

0,14

0,16

0,18

0,20

0,22

0,24

0,26

0,28

0,30

0,32

0,34

0,359

1/cm

ARBITRARY

Figure B5 IR spectra of JOTACOTE UNIVERSAL 80 (binder phase of base, Al), batch no.: Lab made 19.01.2009

3999,7 3600 3200 2800 2400 2000 1800 1600 1400 1200 1000 800 649,90,000

0,01

0,02

0,03

0,04

0,05

0,06

0,07

0,08

0,09

0,10

0,11

0,12

0,13

0,14

0,15

0,16

0,17

0,178

1/cm

ARBITRARY

Figure B6 IR spectra of JOTACOTE UNIVERSAL 80 (hardener, Al), batch no.: Lab made 19.01.2009

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APPENDIX C

DETAILED TEST RESULTS

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Table C1 Development of blisters and rust after exposure

Panel Blisters7) Rust 8) Other defects

W1 0 0 0

W2 0 0 0

W3 0 0 0

W4 0 0 0

H 0 0 0

C1 0 0 0

C2 0 0 0

7) The of the degree of blistering was performed according to ISO 4628-2 /8/ 8) The evaluation of degree of rusting was performed according to ISO 4628-3 /9/

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Table C2 Results of the pull-off adhesion test: wave tank and heat panels Panel

Adhesion test no.9)

Adhesion strength [MPa] 10) Fracture [%] 11)

1 8.9 30C, 70D

2 8.1 45C, 55D W1

3 8.8 25C, 75D

4 8.6 30C, 70D

5 8.6 25C, 75D W2

6 8.4 25C, 75D

7 7.3 5C, 95D

8 7.9 30C, 70D W3

9 8.3 25C, 75D

10 8.4 55C, 45D

11 8.6 65C, 35D W4

12 8.6 30C, 70D

13 8.1 5C, 95D

14 8.9 5C, 95D H

15 8.7 5C, 95D

Average 8.4 Total adhesive: 0 % Total cohesive: 100 %

Maximum 8.9

Minimum 7.3 9) Number of test specimen per panel in accordance with IACS Rec. No. 101 /7/. 10) Adhesion tests were carried out with a DeFlesko PosiTest AT adhesion tester. Dollies with 20 mm diameter were used. The coating surface and dollies were softly grinded with FEPA P#320 SiC paper and rinsed with technical alcohol. The dollies were glued to the coated surface with 3M DP410 adhesive. The curing of the adhesive was carried out according to manufacturer’s recommendations. A whole saw was employed to carefully cut through the coating down to bare steel before pulling off the dollies.

11) A/B: Fracture between the steel surface and the shop primer

B: Fracture in the shop primer

B/C: Fracture between the shop primer and the first coat

C: Fracture in the first coat

C/D: Fracture between the first coat the second coat

D: Fracture in the second coat

-/Y: Fracture between the second coat and the glue

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Table C3 Results of the pull-off adhesion test: condensation chamber panels Panel

Adhesion test no.9)

Adhesion strength [MPa] 10) Fracture [%] 11)

16 7.9 1C, 99D

17 8.0 10C, 90D C1

18 7.5 7C, 93D

19 7.8 20C, 80D

20 9.0 20C, 80D C2

21 8.3 30C, 70D

Average 8.1 Total adhesive: 0 % Total cohesive: 100 %

Maximum 9.0

Minimum 7.5 9) Number of test specimen per panel in accordance with IACS Rec. No. 101 /7/. 10) Adhesion tests were carried out with a DeFlesko PosiTest AT adhesion tester. Dollies with 20 mm diameter were used. The coating surface and dollies were softly grinded with FEPA P#320 SiC paper and rinsed with technical alcohol. The dollies were glued to the coated surface with 3M DP410 adhesive. The curing of the adhesive was carried out according to manufacturer’s recommendations. A whole saw was employed to carefully cut through the coating down to bare steel before pulling off the dollies.

11) A/B: Fracture between the steel surface and the shop primer

B: Fracture in the shop primer

B/C: Fracture between the shop primer and the first coat

C: Fracture in the first coat

C/D: Fracture between the first coat the second coat

D: Fracture in the second coat

-/Y: Fracture between the second coat and the glue

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Table C4 Results of the pull-off adhesion test: reference panels (for information only) Panel

Adhesion test no.9)

Adhesion strength [MPa] 10) Fracture [%] 11)

22 9.5 99C, 1D

23 8.1 85C, 8D, 7-/Y

24 7.2 80C, 15D, 5-/Y

25 7.9 96C, 2D, 2-/Y

26 6.8 92C, 5D, 3-/Y

R1

27 8.2 92C, 4D, 4-/Y

Average 8.0 Total adhesive: ≈ 3.5 % Total cohesive: ≈ 96.5 %

Maximum 9.5

Minimum 6.8 9) Number of test specimen per panel in accordance with IACS Rec. No. 101 /7/ 10) Adhesion tests were carried out with a DeFlesko PosiTest AT adhesion tester. Dollies with 20 mm diameter were used. The coating surface and dollies were softly grinded with FEPA P#320 SiC paper and rinsed with technical alcohol. The dollies were glued to the coated surface with 3M DP410 adhesive. The curing of the adhesive was carried out according to manufacturer’s recommendations. A whole saw was employed to carefully cut through the coating down to bare steel before pulling off the dollies.

11) A/B: Fracture between the steel surface and the shop primer

B: Fracture in the shop primer

B/C: Fracture between the shop primer and the first coat

C: Fracture in the first coat

C/D: Fracture between the first coat the second coat

D: Fracture in the second coat

-/Y: Fracture between the second coat and the glue

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Table C5 Cathodic protection

Cathodic disbondment [mm] 12) Zinc anode weight loss [g] Current demand [mA/m2] 13)

3 – 4 0.6797 1.83

12) “Assess loss of adhesion at the artificial holiday by using a sharp knife to make two cuts through the coating to the substrates, intersection at the holiday. With the point of the knife, attempt to lift and peel back the coating from around the holiday. Record whether the adhesion of the coating to the substrate has been reduced and the approximate distance, in millimetres, that the coating can be peeled.” (From ISO 15711:2003 /5/) Additionally IACS interpretation of IMO PSPC: Repeat the cutting and lifting all around the artificial holiday to find the maximum loss of adhesion. Disbonding from artificial holiday can be either loss of adhesion to the steel substrate or between the shop primer and the epoxy coating and shall be less than 8 mm for epoxy based systems to be acceptable (compatibility test). Cohesive adhesion failure in the shop primer is not to be included as part of the loss of adhesion. (From IACS Rec. No. 101 /7/) 13) Exposure time: 119 days submerged in natural seawater during total 180 days of cyclic exposure as defined in /1/ Utilisation factor: 0.8

Consumption rate for Zn-anodes: 11.3 kg/A year

Table C6 Undercutting from scribes Panel Undercutting from scribes [mm] 14)

W1 2

W3 1.5

W4 1.5

Average ≈ 1.7 14) “Rinse the test panel with fresh water immediately after exposure, […], and inspect for visible changes. Carefully remove any loose coating using a knife blade held at an angle, positioning the blade at the coating/ substrate interface and lifting the coating away from the substrate.” (From ISO 4628-8:2005, section 5.3.1 /10/) Addionally IACS interpretation: Undercutting from scribe can be either corrosion of the steel substrate or delamination between the shop primer and the epoxy coating (compatibility test). For PSPC maximum width is used (MSC.215(82), Appendix 1, section 2.2.6). The average of three maximum records of three panels with scribe is used for acceptance. Cohesive adhesion failure in the shop primer is not to be included as part of the delamination. (From IACS Rec. No. 101 /7/)

Table C7 Flexibility (for information only)

Panel Diameter of Mandrel [mm] 15) Elongation [%] 16) Comments

W1 300 1 Many small cracks was observed

R1 300 1 Many small cracks was observed

15) Maximum diameter of mandrel for which any cracking in the coating occurs 16) Calculated respectively to the diameter of the mandrel for which any cracking occurs.

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APPENDIX D

PHOTO DOCUMENTATION

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Figure D1 Overview picture of the wave tank panels (above from left to right: W1, W2,

W3, W4 and H) and the condensation chamber panels (below from left to right: C1 and C2) after exposure

Figure D2 Small cracks in the coating after flexibility test (above W1 and below R1)

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Figure D3 Undercut scribe on the top wave tank panel (W1)

Figure D4 Artificial holiday and cathodic disbondment from the artificial holiday on

the wave tank bottom panel (W2)

Figure D5 Undercut scribe on the side wave tank panel with cooling (W3)

Figure D6 Undercut scribe on the side wave tank panel (W4)

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Figure D7 Adhesion test no. 1, 2 and 3

Figure D8 Adhesion test no. 4, 5 and 6

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Figure D9 Adhesion test no. 7, 8 and 9

Figure D10 Adhesion test no. 10, 11 and 12

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Figure D11 Adhesion test no. 13, 14 and 15

Figure D12 Adhesion test no. 16, 17 and 18

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Figure D13 Adhesion test no. 19, 20 and 21

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Figure D28 Adhesion test no. 22

Figure D29 Adhesion test no. 23

Figure D30 Adhesion test no. 24

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Figure D31 Adhesion test no. 25

Figure D32 Adhesion test no. 26

Figure D33 Adhesion test no. 27

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