environmental impact statement minago project … · appendix l7.3 certified laboratory reports for...
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ENVIRONMENTAL IMPACT STATEMENT
MINAGO PROJECT
VOLUME III – Part I
LABORATORY CERTIFIED REPORTS
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VICTORY NICKEL INC.
MINAGO PROJECT Environmental Impact Statement
ii
VOLUME III - LIST OF APPENDICES
Volume III - Part I: APPENDIX L7.3 Certified Laboratory Reports for Soils - 2007 Results (Jul. 2007)
APPENDIX L7.5 Certified Laboratory Reports for Surface Water Quality
Appendix L7.5-A: Data Quality Objectives – ALS Vancouver & Summary of Data Analysis for Water Samples with Higher reported Dissolved versus
Total Element Concentrations Appendix L7.5-B:
Summary of 2006 Trip Blank Water Quality Results Summary of Sept.- Oct 2007 & May 2008 Blanks Water Quality Results Summary of March 2008 Blanks Water Quality Results
Appendix L7.5-C: May 2006 Results Appendix L7.5-D: June 2006 Results Appendix L7.5-E: July 2006 Results Appendix L7.5-F: August 2006 Results Appendix L7.5-G: September 2006 Results Appendix L7.5-H: October 2006 Results Appendix L7.5-I: May 2007 Results Appendix L7.5-J: June 2007 Results Appendix L7.5-K: July 2007 Results Appendix L7.5-L: August 2007 Results Appendix L7.5-M: September 2007 Results Appendix L7.5-N: October 2007 Results
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APPENDIX L7.3 Certified Laboratory Reports for Soils
2007 Results (Jul. 2007)
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ANALYTICAL REPORT CASH CLIENTS-WINNIPEG
ATTN: DR. DAVID MCHAINA Reported On: 29-OCT-07 01:38 PM Revision: 1 VICTORY NICKEL INC.
STE 1802 -80 RICHMOND ST W TORONTO ON M5H 2A4
L533759 Lab Work Order #: Date Received: 25-JUL-07
Project P.O. #: Job Reference: MINAGO Legal Site Desc: CofC Numbers:
Other Information:
Comments:
APPROVED BY: ____________________________________________ MARILYN BELL
Project Manager
THIS REPORT SHALL NOT BE REPRODUCED EXCEPT IN FULL WITHOUT THE WRITTEN AUTHORITY OF THE LABORATORY. ALL SAMPLES WILL BE DISPOSED OF AFTER 30 DAYS FOLLOWING ANALYSIS. PLEASE CONTACT THE LAB IF YOU REQUIRE ADDITIONAL SAMPLE STORAGE TIME.
1329 Niakwa Road East, Unit 12, Winnipeg, MB R2J 3T4 Phone: +1 204 255 9720 Fax: +1 204 255 9721 www.alsglobal.com
A Campbell Brothers Limited Company
L7.3–1
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MINAGO L533759 CONTD.... 2 of 9 PAGE
ALS LABORATORY GROUP ANALYTICAL REPORT
Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed By Batch
L533759-1 MINAGO SAMPLE 1 (0 - 15 CM) Sampled By: LT / DMM on 18-JUL-07 Matrix: SOIL
Cyanide, Total mg/kg 08-AUG-07 15-AUG-07 17 1 DXN R561492 Loss on Ignition @ 550 C % 07-AUG-07 07-AUG-07 87.7 0 MMC R558484
Metals Silver (Ag)-Total mg/kg 08-AUG-07 08-AUG-07 <1 1 DAG R558986 Aluminum (Al)-Total mg/kg 08-AUG-07 08-AUG-07 446 3 DAG R558986 Arsenic (As)-Total mg/kg 08-AUG-07 08-AUG-07 2.52 0.03 DAG R558986 Boron (B)-Total mg/kg 08-AUG-07 08-AUG-07 14.5 0.6 DAG R558986 Barium (Ba)-Total mg/kg 08-AUG-07 08-AUG-07 RAMB 74.2 0.04 DAG R558986 Beryllium (Be)-Total mg/kg 08-AUG-07 08-AUG-07 <0.06 0.06 DAG R558986 Bismuth (Bi)-Total mg/kg 08-AUG-07 08-AUG-07 0.06 0.02 DAG R558986 Calcium (Ca)-Total mg/kg 08-AUG-07 08-AUG-07 RAMB 33200 7 DAG R558986 Cadmium (Cd)-Total mg/kg 08-AUG-07 08-AUG-07 0.18 0.02 DAG R558986 Cobalt (Co)-Total mg/kg 08-AUG-07 08-AUG-07 1.25 0.01 DAG R558986 Chromium (Cr)-Total mg/kg 08-AUG-07 08-AUG-07 1.6 0.1 DAG R558986 Copper (Cu)-Total mg/kg 08-AUG-07 08-AUG-07 4.5 0.2 DAG R558986 Iron (Fe)-Total mg/kg 08-AUG-07 08-AUG-07 1810 6 DAG R558986 Potassium (K)-Total mg/kg 08-AUG-07 08-AUG-07 231 7 DAG R558986 Magnesium (Mg)-Total mg/kg 08-AUG-07 08-AUG-07 5600 2 DAG R558986 Manganese (Mn)-Total mg/kg 08-AUG-07 08-AUG-07 RAMB 1310 0.09 DAG R558986 Molybdenum (Mo)-Total mg/kg 08-AUG-07 08-AUG-07 0.60 0.02 DAG R558986 Sodium (Na)-Total mg/kg 08-AUG-07 08-AUG-07 RAMB 139 2 DAG R558986 Nickel (Ni)-Total mg/kg 08-AUG-07 08-AUG-07 15.6 0.2 DAG R558986 Lead (Pb)-Total mg/kg 08-AUG-07 08-AUG-07 10.1 0.05 DAG R558986 Selenium (Se)-Total mg/kg 08-AUG-07 08-AUG-07 0.5 0.1 DAG R558986 Tin (Sn)-Total mg/kg 08-AUG-07 08-AUG-07 <4 4 DAG R558986 Strontium (Sr)-Total RAMB mg/kg 08-AUG-07 08-AUG-07 68.6 0.02 DAG R558986 Titanium (Ti)-Total mg/kg 08-AUG-07 08-AUG-07 16.7 0.03 DAG R558986 Thallium (Tl)-Total mg/kg 08-AUG-07 08-AUG-07 <0.2 0.2 DAG R558986 Uranium (U)-Total mg/kg 08-AUG-07 08-AUG-07 0.05 0.02 DAG R558986 Vanadium (V)-Total mg/kg 08-AUG-07 08-AUG-07 2.18 0.06 DAG R558986 Zinc (Zn)-Total mg/kg 08-AUG-07 08-AUG-07 RAMB 48 2 DAG R558986
Package 4 Ag. Soil Avail Micronutrients (Cu,Fe,Zn,Mn) ug/cc
Copper (Cu) ug/cc 07-AUG-07 07-AUG-07 0.30 0.02 0 R558096 Iron (Fe) ug/cc 07-AUG-07 07-AUG-07 62 2 0 R558096 Manganese (Mn) ug/cc 07-AUG-07 07-AUG-07 11.1 0.04 0 R558096 Zinc (Zn) ug/cc 07-AUG-07 07-AUG-07 2.8 0.2 0 R558096 Boron (B), Hot Water Ext. ug/cc 07-AUG-07 07-AUG-07 0.6 0.1 DAD R557913 Available Chloride ug/cc 07-AUG-07 07-AUG-07 3.0 0.2 BFE R557940 Available Nitrate-N ug/cc 07-AUG-07 07-AUG-07 3.6 0.4 BFE R558175
Available Phosphate & Potassium (ug/cc) Available Phosphate-P ug/cc 07-AUG-07 07-AUG-07 1 1 BFE R558066 Available Potassium ug/cc 07-AUG-07 07-AUG-07 14 2 BFE R558066 Available Sulfate-S RRA ug/cc 07-AUG-07 07-AUG-07 8 2 DAD R558074 Hand Texture 07-AUG-07 07-AUG-07 Organic 0 BMD R558557
pH & EC 1:2 soil to water (Ag. Method) pH (1:2 soil:water) pH 07-AUG-07 07-AUG-07 6.8 0.1 BMD R557999 Conductivity (1:2) ds m-1 07-AUG-07 07-AUG-07 0.10 0.01 BMD R557999
L533759-2 MINAGO SAMPLE 1 (15 - 30 CM) Sampled By: LT / DMM on 18-JUL-07 Matrix: SOIL
L7.3–2
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MINAGO L533759 CONTD.... 3 of 9 PAGE
ALS LABORATORY GROUP ANALYTICAL REPORT
Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed By Batch
L533759-2 MINAGO SAMPLE 1 (15 - 30 CM) Sampled By: LT / DMM on 18-JUL-07 Matrix: SOIL
Cyanide, Total mg/kg 08-AUG-07 15-AUG-07 27 1 DXN R561492 Loss on Ignition @ 550 C % 07-AUG-07 07-AUG-07 80.5 0 MMC R558484
Metals Silver (Ag)-Total mg/kg 08-AUG-07 08-AUG-07 <1 1 DAG R558986 Aluminum (Al)-Total mg/kg 08-AUG-07 08-AUG-07 303 3 DAG R558986 Arsenic (As)-Total mg/kg 08-AUG-07 08-AUG-07 1.15 0.03 DAG R558986 Boron (B)-Total mg/kg 08-AUG-07 08-AUG-07 16.1 0.6 DAG R558986 Barium (Ba)-Total mg/kg 08-AUG-07 08-AUG-07 RAMB 101 0.04 DAG R558986 Beryllium (Be)-Total mg/kg 08-AUG-07 08-AUG-07 <0.06 0.06 DAG R558986 Bismuth (Bi)-Total mg/kg 08-AUG-07 08-AUG-07 <0.02 0.02 DAG R558986 Calcium (Ca)-Total mg/kg 08-AUG-07 08-AUG-07 RAMB 33800 7 DAG R558986 Cadmium (Cd)-Total mg/kg 08-AUG-07 08-AUG-07 0.07 0.02 DAG R558986 Cobalt (Co)-Total mg/kg 08-AUG-07 08-AUG-07 0.34 0.01 DAG R558986 Chromium (Cr)-Total mg/kg 08-AUG-07 08-AUG-07 1.4 0.1 DAG R558986 Copper (Cu)-Total mg/kg 08-AUG-07 08-AUG-07 5.5 0.2 DAG R558986 Iron (Fe)-Total mg/kg 08-AUG-07 08-AUG-07 535 6 DAG R558986 Potassium (K)-Total mg/kg 08-AUG-07 08-AUG-07 229 7 DAG R558986 Magnesium (Mg)-Total mg/kg 08-AUG-07 08-AUG-07 10300 2 DAG R558986 Manganese (Mn)-Total mg/kg 08-AUG-07 08-AUG-07 RAMB 18.1 0.09 DAG R558986 Molybdenum (Mo)-Total mg/kg 08-AUG-07 08-AUG-07 0.37 0.02 DAG R558986 Sodium (Na)-Total mg/kg 08-AUG-07 08-AUG-07 RAMB 179 2 DAG R558986 Nickel (Ni)-Total mg/kg 08-AUG-07 08-AUG-07 1.9 0.2 DAG R558986 Lead (Pb)-Total mg/kg 08-AUG-07 08-AUG-07 1.07 0.05 DAG R558986 Selenium (Se)-Total mg/kg 08-AUG-07 08-AUG-07 0.4 0.1 DAG R558986 Tin (Sn)-Total mg/kg 08-AUG-07 08-AUG-07 <4 4 DAG R558986 Strontium (Sr)-Total RAMB mg/kg 08-AUG-07 08-AUG-07 40.6 0.02 DAG R558986 Titanium (Ti)-Total mg/kg 08-AUG-07 08-AUG-07 12.0 0.03 DAG R558986 Thallium (Tl)-Total mg/kg 08-AUG-07 08-AUG-07 <0.2 0.2 DAG R558986 Uranium (U)-Total mg/kg 08-AUG-07 08-AUG-07 0.07 0.02 DAG R558986 Vanadium (V)-Total mg/kg 08-AUG-07 08-AUG-07 1.21 0.06 DAG R558986 Zinc (Zn)-Total mg/kg 08-AUG-07 08-AUG-07 RAMB 10 2 DAG R558986
Package 4 Ag. Soil Avail Micronutrients (Cu,Fe,Zn,Mn) ug/cc
Copper (Cu) ug/cc 07-AUG-07 07-AUG-07 0.29 0.02 0 R558096 Iron (Fe) RRA ug/cc 07-AUG-07 07-AUG-07 6 2 0 R558096 Manganese (Mn) ug/cc 07-AUG-07 07-AUG-07 RRA 1.29 0.04 0 R558096 Zinc (Zn) ug/cc 07-AUG-07 07-AUG-07 0.9 0.2 0 R558096 Boron (B), Hot Water Ext. ug/cc 07-AUG-07 07-AUG-07 0.6 0.1 DAD R557913 Available Chloride ug/cc 07-AUG-07 07-AUG-07 5.0 0.2 BFE R557940 Available Nitrate-N ug/cc 07-AUG-07 07-AUG-07 2.6 0.4 BFE R558175
Available Phosphate & Potassium (ug/cc) Available Phosphate-P ug/cc 07-AUG-07 07-AUG-07 1 1 BFE R558066 Available Potassium ug/cc 07-AUG-07 07-AUG-07 13 2 BFE R558066 Available Sulfate-S ug/cc 07-AUG-07 07-AUG-07 12 2 DAD R558074 Hand Texture 07-AUG-07 07-AUG-07 Organic 0 BMD R558557
pH & EC 1:2 soil to water (Ag. Method) pH (1:2 soil:water) pH 07-AUG-07 07-AUG-07 7.6 0.1 BMD R557999 Conductivity (1:2) ds m-1 07-AUG-07 07-AUG-07 0.10 0.01 BMD R557999
L533759-3 MINAGO SAMPLE 2 (0 - 15 CM) Sampled By: LT / DMM on 18-JUL-07 Matrix: SOIL
L7.3–3
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MINAGO L533759 CONTD.... 4 of 9 PAGE
ALS LABORATORY GROUP ANALYTICAL REPORT
Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed By Batch
L533759-3 MINAGO SAMPLE 2 (0 - 15 CM) Sampled By: LT / DMM on 18-JUL-07 Matrix: SOIL
Cyanide, Total mg/kg 08-AUG-07 15-AUG-07 41 1 DXN R561492 Loss on Ignition @ 550 C % 07-AUG-07 07-AUG-07 88.4 0 MMC R558484
Metals Silver (Ag)-Total mg/kg 08-AUG-07 08-AUG-07 8 1 DAG R558986 Aluminum (Al)-Total mg/kg 08-AUG-07 08-AUG-07 715 3 DAG R558986 Arsenic (As)-Total mg/kg 08-AUG-07 08-AUG-07 2.34 0.03 DAG R558986 Boron (B)-Total mg/kg 08-AUG-07 08-AUG-07 13.8 0.6 DAG R558986 Barium (Ba)-Total mg/kg 08-AUG-07 08-AUG-07 RAMB 33.7 0.04 DAG R558986 Beryllium (Be)-Total mg/kg 08-AUG-07 08-AUG-07 <0.06 0.06 DAG R558986 Bismuth (Bi)-Total mg/kg 08-AUG-07 08-AUG-07 <0.02 0.02 DAG R558986 Calcium (Ca)-Total mg/kg 08-AUG-07 08-AUG-07 RAMB 30800 7 DAG R558986 Cadmium (Cd)-Total mg/kg 08-AUG-07 08-AUG-07 0.11 0.02 DAG R558986 Cobalt (Co)-Total mg/kg 08-AUG-07 08-AUG-07 0.89 0.01 DAG R558986 Chromium (Cr)-Total mg/kg 08-AUG-07 08-AUG-07 1.2 0.1 DAG R558986 Copper (Cu)-Total mg/kg 08-AUG-07 08-AUG-07 2.9 0.2 DAG R558986 Iron (Fe)-Total mg/kg 08-AUG-07 08-AUG-07 5690 6 DAG R558986 Potassium (K)-Total mg/kg 08-AUG-07 08-AUG-07 142 7 DAG R558986 Magnesium (Mg)-Total mg/kg 08-AUG-07 08-AUG-07 4140 2 DAG R558986 Manganese (Mn)-Total mg/kg 08-AUG-07 08-AUG-07 RAMB 126 0.09 DAG R558986 Molybdenum (Mo)-Total mg/kg 08-AUG-07 08-AUG-07 0.36 0.02 DAG R558986 Sodium (Na)-Total mg/kg 08-AUG-07 08-AUG-07 RAMB 132 2 DAG R558986 Nickel (Ni)-Total mg/kg 08-AUG-07 08-AUG-07 1.9 0.2 DAG R558986 Lead (Pb)-Total mg/kg 08-AUG-07 08-AUG-07 1.24 0.05 DAG R558986 Selenium (Se)-Total mg/kg 08-AUG-07 08-AUG-07 0.7 0.1 DAG R558986 Tin (Sn)-Total mg/kg 08-AUG-07 08-AUG-07 <4 4 DAG R558986 Strontium (Sr)-Total RAMB mg/kg 08-AUG-07 08-AUG-07 69.7 0.02 DAG R558986 Titanium (Ti)-Total mg/kg 08-AUG-07 08-AUG-07 21.5 0.03 DAG R558986 Thallium (Tl)-Total mg/kg 08-AUG-07 08-AUG-07 <0.2 0.2 DAG R558986 Uranium (U)-Total mg/kg 08-AUG-07 08-AUG-07 0.11 0.02 DAG R558986 Vanadium (V)-Total mg/kg 08-AUG-07 08-AUG-07 1.96 0.06 DAG R558986 Zinc (Zn)-Total mg/kg 08-AUG-07 08-AUG-07 RAMB 29 2 DAG R558986
L533759-4 MINAGO SAMPLE 2 (15 - 30 CM) Sampled By: LT / DMM on 18-JUL-07 Matrix: SOIL
Cyanide, Total mg/kg 08-AUG-07 15-AUG-07 9 1 DXN R561492 Loss on Ignition @ 550 C % 07-AUG-07 07-AUG-07 44.7 0 MMC R558484
Metals Silver (Ag)-Total mg/kg 08-AUG-07 08-AUG-07 <1 1 DAG R558986 Aluminum (Al)-Total mg/kg 08-AUG-07 08-AUG-07 2210 3 DAG R558986 Arsenic (As)-Total mg/kg 08-AUG-07 08-AUG-07 1.91 0.03 DAG R558986 Boron (B)-Total mg/kg 08-AUG-07 08-AUG-07 13.1 0.6 DAG R558986 Barium (Ba)-Total RAMB mg/kg 08-AUG-07 08-AUG-07 47.4 0.04 DAG R558986 Beryllium (Be)-Total mg/kg 08-AUG-07 08-AUG-07 0.07 0.06 DAG R558986 Bismuth (Bi)-Total mg/kg 08-AUG-07 08-AUG-07 0.05 0.02 DAG R558986 Calcium (Ca)-Total mg/kg 08-AUG-07 08-AUG-07 RAMB 64800 7 DAG R558986 Cadmium (Cd)-Total mg/kg 08-AUG-07 08-AUG-07 0.09 0.02 DAG R558986 Cobalt (Co)-Total mg/kg 08-AUG-07 08-AUG-07 1.54 0.01 DAG R558986 Chromium (Cr)-Total mg/kg 08-AUG-07 08-AUG-07 10.9 0.1 DAG R558986 Copper (Cu)-Total mg/kg 08-AUG-07 08-AUG-07 4.6 0.2 DAG R558986 Iron (Fe)-Total mg/kg 08-AUG-07 08-AUG-07 2850 6 DAG R558986
L7.3–4
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MINAGO L533759 CONTD.... 5 of 9 PAGE
ALS LABORATORY GROUP ANALYTICAL REPORT
Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed By Batch
L533759-4 MINAGO SAMPLE 2 (15 - 30 CM) Sampled By: LT / DMM on 18-JUL-07 Matrix: SOIL
Metals Potassium (K)-Total mg/kg 08-AUG-07 08-AUG-07 538 7 DAG R558986 Magnesium (Mg)-Total mg/kg 08-AUG-07 08-AUG-07 33900 2 DAG R558986 Manganese (Mn)-Total mg/kg 08-AUG-07 08-AUG-07 RAMB 162 0.09 DAG R558986 Molybdenum (Mo)-Total mg/kg 08-AUG-07 08-AUG-07 0.30 0.02 DAG R558986 Sodium (Na)-Total RAMB mg/kg 08-AUG-07 08-AUG-07 110 2 DAG R558986 Nickel (Ni)-Total mg/kg 08-AUG-07 08-AUG-07 7.7 0.2 DAG R558986 Lead (Pb)-Total mg/kg 08-AUG-07 08-AUG-07 4.17 0.05 DAG R558986 Selenium (Se)-Total mg/kg 08-AUG-07 08-AUG-07 0.3 0.1 DAG R558986 Tin (Sn)-Total mg/kg 08-AUG-07 08-AUG-07 <4 4 DAG R558986 Strontium (Sr)-Total mg/kg 08-AUG-07 08-AUG-07 RAMB 30.5 0.02 DAG R558986 Titanium (Ti)-Total mg/kg 08-AUG-07 08-AUG-07 134 0.03 DAG R558986 Thallium (Tl)-Total mg/kg 08-AUG-07 08-AUG-07 <0.2 0.2 DAG R558986 Uranium (U)-Total mg/kg 08-AUG-07 08-AUG-07 0.16 0.02 DAG R558986 Vanadium (V)-Total mg/kg 08-AUG-07 08-AUG-07 5.11 0.06 DAG R558986 Zinc (Zn)-Total mg/kg 08-AUG-07 08-AUG-07 RAMB 9 2 DAG R558986
L533759-5 MINAGO SAMPLE 3 (0 - 30 CM) Sampled By: LT / DMM on 18-JUL-07 Matrix: SOIL
Cyanide, Total mg/kg 08-AUG-07 15-AUG-07 30 1 DXN R561492 Loss on Ignition @ 550 C % 07-AUG-07 07-AUG-07 85.9 0 MMC R558484
Metals Silver (Ag)-Total mg/kg 08-AUG-07 08-AUG-07 <1 1 DAG R558986 Aluminum (Al)-Total mg/kg 08-AUG-07 08-AUG-07 648 3 DAG R558986 Arsenic (As)-Total mg/kg 08-AUG-07 08-AUG-07 18.6 0.03 DAG R558986 Boron (B)-Total mg/kg 08-AUG-07 08-AUG-07 14.4 0.6 DAG R558986 Barium (Ba)-Total RAMB mg/kg 08-AUG-07 08-AUG-07 365 0.04 DAG R558986 Beryllium (Be)-Total mg/kg 08-AUG-07 08-AUG-07 <0.06 0.06 DAG R558986 Bismuth (Bi)-Total mg/kg 08-AUG-07 08-AUG-07 0.07 0.02 DAG R558986 Calcium (Ca)-Total mg/kg 08-AUG-07 08-AUG-07 RAMB 29400 7 DAG R558986 Cadmium (Cd)-Total mg/kg 08-AUG-07 08-AUG-07 0.35 0.02 DAG R558986 Cobalt (Co)-Total mg/kg 08-AUG-07 08-AUG-07 5.25 0.01 DAG R558986 Chromium (Cr)-Total mg/kg 08-AUG-07 08-AUG-07 1.2 0.1 DAG R558986 Copper (Cu)-Total mg/kg 08-AUG-07 08-AUG-07 7.3 0.2 DAG R558986 Iron (Fe)-Total mg/kg 08-AUG-07 08-AUG-07 9140 6 DAG R558986 Potassium (K)-Total mg/kg 08-AUG-07 08-AUG-07 197 7 DAG R558986 Magnesium (Mg)-Total mg/kg 08-AUG-07 08-AUG-07 4270 2 DAG R558986 Manganese (Mn)-Total mg/kg 08-AUG-07 08-AUG-07 RAMB 5560 0.09 DAG R558986 Molybdenum (Mo)-Total mg/kg 08-AUG-07 08-AUG-07 0.55 0.02 DAG R558986 Sodium (Na)-Total RAMB mg/kg 08-AUG-07 08-AUG-07 62 2 DAG R558986 Nickel (Ni)-Total mg/kg 08-AUG-07 08-AUG-07 1.8 0.2 DAG R558986 Lead (Pb)-Total mg/kg 08-AUG-07 08-AUG-07 3.40 0.05 DAG R558986 Selenium (Se)-Total mg/kg 08-AUG-07 08-AUG-07 0.9 0.1 DAG R558986 Tin (Sn)-Total mg/kg 08-AUG-07 08-AUG-07 <4 4 DAG R558986 Strontium (Sr)-Total mg/kg 08-AUG-07 08-AUG-07 RAMB 67.9 0.02 DAG R558986 Titanium (Ti)-Total mg/kg 08-AUG-07 08-AUG-07 19.9 0.03 DAG R558986 Thallium (Tl)-Total mg/kg 08-AUG-07 08-AUG-07 <0.2 0.2 DAG R558986 Uranium (U)-Total mg/kg 08-AUG-07 08-AUG-07 0.13 0.02 DAG R558986 Vanadium (V)-Total mg/kg 08-AUG-07 08-AUG-07 1.72 0.06 DAG R558986 Zinc (Zn)-Total mg/kg 08-AUG-07 08-AUG-07 RAMB 90 2 DAG R558986
L7.3–5
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MINAGO L533759 CONTD.... 6 of 9 PAGE
ALS LABORATORY GROUP ANALYTICAL REPORT
Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed By Batch
L533759-5 MINAGO SAMPLE 3 (0 - 30 CM) Sampled By: LT / DMM on 18-JUL-07 Matrix: SOIL
L533759-6 MINAGO SAMPLE 4 (0 - 30 CM) Sampled By: LT / DMM on 18-JUL-07 Matrix: SOIL
Cyanide, Total mg/kg 08-AUG-07 15-AUG-07 39 1 DXN R561492 Loss on Ignition @ 550 C % 07-AUG-07 07-AUG-07 85.4 0 MMC R558484
Metals Silver (Ag)-Total mg/kg 08-AUG-07 08-AUG-07 <1 1 DAG R558986 Aluminum (Al)-Total mg/kg 08-AUG-07 08-AUG-07 613 3 DAG R558986 Arsenic (As)-Total mg/kg 08-AUG-07 08-AUG-07 2.15 0.03 DAG R558986 Boron (B)-Total mg/kg 08-AUG-07 08-AUG-07 28.2 0.6 DAG R558986 Barium (Ba)-Total mg/kg 08-AUG-07 08-AUG-07 RAMB 51.8 0.04 DAG R558986 Beryllium (Be)-Total mg/kg 08-AUG-07 08-AUG-07 <0.06 0.06 DAG R558986 Bismuth (Bi)-Total mg/kg 08-AUG-07 08-AUG-07 0.05 0.02 DAG R558986 Calcium (Ca)-Total mg/kg 08-AUG-07 08-AUG-07 RAMB 32500 7 DAG R558986 Cadmium (Cd)-Total mg/kg 08-AUG-07 08-AUG-07 0.16 0.02 DAG R558986 Cobalt (Co)-Total mg/kg 08-AUG-07 08-AUG-07 0.44 0.01 DAG R558986 Chromium (Cr)-Total mg/kg 08-AUG-07 08-AUG-07 1.2 0.1 DAG R558986 Copper (Cu)-Total mg/kg 08-AUG-07 08-AUG-07 5.4 0.2 DAG R558986 Iron (Fe)-Total mg/kg 08-AUG-07 08-AUG-07 3620 6 DAG R558986 Potassium (K)-Total mg/kg 08-AUG-07 08-AUG-07 227 7 DAG R558986 Magnesium (Mg)-Total mg/kg 08-AUG-07 08-AUG-07 5480 2 DAG R558986 Manganese (Mn)-Total mg/kg 08-AUG-07 08-AUG-07 RAMB 566 0.09 DAG R558986 Molybdenum (Mo)-Total mg/kg 08-AUG-07 08-AUG-07 0.39 0.02 DAG R558986 Sodium (Na)-Total mg/kg 08-AUG-07 08-AUG-07 RAMB 103 2 DAG R558986 Nickel (Ni)-Total mg/kg 08-AUG-07 08-AUG-07 2.3 0.2 DAG R558986 Lead (Pb)-Total mg/kg 08-AUG-07 08-AUG-07 5.09 0.05 DAG R558986 Selenium (Se)-Total mg/kg 08-AUG-07 08-AUG-07 0.6 0.1 DAG R558986 Tin (Sn)-Total mg/kg 08-AUG-07 08-AUG-07 <4 4 DAG R558986 Strontium (Sr)-Total RAMB mg/kg 08-AUG-07 08-AUG-07 108 0.02 DAG R558986 Titanium (Ti)-Total mg/kg 08-AUG-07 08-AUG-07 18.6 0.03 DAG R558986 Thallium (Tl)-Total mg/kg 08-AUG-07 08-AUG-07 <0.2 0.2 DAG R558986 Uranium (U)-Total mg/kg 08-AUG-07 08-AUG-07 0.14 0.02 DAG R558986 Vanadium (V)-Total mg/kg 08-AUG-07 08-AUG-07 1.89 0.06 DAG R558986 Zinc (Zn)-Total mg/kg 08-AUG-07 08-AUG-07 RAMB 13 2 DAG R558986
L533759-7 MINAGO SAMPLE 5 (0 - 30 CM) Sampled By: LT / DMM on 18-JUL-07 Matrix: SOIL
Cyanide, Total mg/kg 08-AUG-07 15-AUG-07 23 1 DXN R561492 Loss on Ignition @ 550 C % 07-AUG-07 07-AUG-07 88.2 0 MMC R558484
Metals Silver (Ag)-Total mg/kg 08-AUG-07 08-AUG-07 <1 1 DAG R558986 Aluminum (Al)-Total mg/kg 08-AUG-07 08-AUG-07 782 3 DAG R558986 Arsenic (As)-Total mg/kg 08-AUG-07 08-AUG-07 1.77 0.03 DAG R558986 Boron (B)-Total mg/kg 08-AUG-07 08-AUG-07 9.3 0.6 DAG R558986 Barium (Ba)-Total mg/kg 08-AUG-07 08-AUG-07 RAMB 23.0 0.04 DAG R558986 Beryllium (Be)-Total mg/kg 08-AUG-07 08-AUG-07 <0.06 0.06 DAG R558986 Bismuth (Bi)-Total mg/kg 08-AUG-07 08-AUG-07 0.05 0.02 DAG R558986 Calcium (Ca)-Total mg/kg 08-AUG-07 08-AUG-07 RAMB 23900 7 DAG R558986 Cadmium (Cd)-Total mg/kg 08-AUG-07 08-AUG-07 0.12 0.02 DAG R558986
L7.3–6
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MINAGO L533759 CONTD.... 7 of 9 PAGE
ALS LABORATORY GROUP ANALYTICAL REPORT
Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed By Batch
L533759-7 MINAGO SAMPLE 5 (0 - 30 CM) Sampled By: LT / DMM on 18-JUL-07 Matrix: SOIL
Metals Cobalt (Co)-Total mg/kg 08-AUG-07 08-AUG-07 0.44 0.01 DAG R558986 Chromium (Cr)-Total mg/kg 08-AUG-07 08-AUG-07 1.4 0.1 DAG R558986 Copper (Cu)-Total mg/kg 08-AUG-07 08-AUG-07 5.8 0.2 DAG R558986 Iron (Fe)-Total mg/kg 08-AUG-07 08-AUG-07 1590 6 DAG R558986 Potassium (K)-Total mg/kg 08-AUG-07 08-AUG-07 262 7 DAG R558986 Magnesium (Mg)-Total mg/kg 08-AUG-07 08-AUG-07 6010 2 DAG R558986 Manganese (Mn)-Total mg/kg 08-AUG-07 08-AUG-07 RAMB 30.9 0.09 DAG R558986 Molybdenum (Mo)-Total mg/kg 08-AUG-07 08-AUG-07 0.72 0.02 DAG R558986 Sodium (Na)-Total RAMB mg/kg 08-AUG-07 08-AUG-07 85 2 DAG R558986 Nickel (Ni)-Total mg/kg 08-AUG-07 08-AUG-07 2.2 0.2 DAG R558986 Lead (Pb)-Total mg/kg 08-AUG-07 08-AUG-07 5.38 0.05 DAG R558986 Selenium (Se)-Total mg/kg 08-AUG-07 08-AUG-07 0.5 0.1 DAG R558986 Tin (Sn)-Total mg/kg 08-AUG-07 08-AUG-07 <4 4 DAG R558986 Strontium (Sr)-Total mg/kg 08-AUG-07 08-AUG-07 RAMB 47.3 0.02 DAG R558986 Titanium (Ti)-Total mg/kg 08-AUG-07 08-AUG-07 28.3 0.03 DAG R558986 Thallium (Tl)-Total mg/kg 08-AUG-07 08-AUG-07 <0.2 0.2 DAG R558986 Uranium (U)-Total mg/kg 08-AUG-07 08-AUG-07 0.19 0.02 DAG R558986 Vanadium (V)-Total mg/kg 08-AUG-07 08-AUG-07 2.02 0.06 DAG R558986 Zinc (Zn)-Total mg/kg 08-AUG-07 08-AUG-07 RAMB 5 2 DAG R558986
L533759-8 MINAGO SAMPLE 6 (0 - 30 CM) Sampled By: LT / DMM on 18-JUL-07 Matrix: SOIL
Cyanide, Total mg/kg 08-AUG-07 15-AUG-07 10 1 DXN R561492 Loss on Ignition @ 550 C % 07-AUG-07 07-AUG-07 33.9 0 MMC R558484
Metals Silver (Ag)-Total mg/kg 08-AUG-07 08-AUG-07 1 1 DAG R558986 Aluminum (Al)-Total mg/kg 08-AUG-07 08-AUG-07 5690 3 DAG R558986 Arsenic (As)-Total mg/kg 08-AUG-07 08-AUG-07 2.48 0.03 DAG R558986 Boron (B)-Total mg/kg 08-AUG-07 08-AUG-07 9.0 0.6 DAG R558986 Barium (Ba)-Total RAMB mg/kg 08-AUG-07 08-AUG-07 67.2 0.04 DAG R558986 Beryllium (Be)-Total mg/kg 08-AUG-07 08-AUG-07 0.26 0.06 DAG R558986 Bismuth (Bi)-Total mg/kg 08-AUG-07 08-AUG-07 0.09 0.02 DAG R558986 Calcium (Ca)-Total mg/kg 08-AUG-07 08-AUG-07 RAMB 51500 7 DAG R558986 Cadmium (Cd)-Total mg/kg 08-AUG-07 08-AUG-07 0.16 0.02 DAG R558986 Cobalt (Co)-Total mg/kg 08-AUG-07 08-AUG-07 4.86 0.01 DAG R558986 Chromium (Cr)-Total mg/kg 08-AUG-07 08-AUG-07 19.8 0.1 DAG R558986 Copper (Cu)-Total mg/kg 08-AUG-07 08-AUG-07 10.9 0.2 DAG R558986 Iron (Fe)-Total mg/kg 08-AUG-07 08-AUG-07 10900 6 DAG R558986 Potassium (K)-Total mg/kg 08-AUG-07 08-AUG-07 1100 7 DAG R558986 Magnesium (Mg)-Total mg/kg 08-AUG-07 08-AUG-07 19700 2 DAG R558986 Manganese (Mn)-Total mg/kg 08-AUG-07 08-AUG-07 RAMB 700 0.09 DAG R558986 Molybdenum (Mo)-Total mg/kg 08-AUG-07 08-AUG-07 0.33 0.02 DAG R558986 Sodium (Na)-Total RAMB mg/kg 08-AUG-07 08-AUG-07 132 2 DAG R558986 Nickel (Ni)-Total mg/kg 08-AUG-07 08-AUG-07 14.6 0.2 DAG R558986 Lead (Pb)-Total mg/kg 08-AUG-07 08-AUG-07 5.65 0.05 DAG R558986 Selenium (Se)-Total mg/kg 08-AUG-07 08-AUG-07 0.4 0.1 DAG R558986 Tin (Sn)-Total mg/kg 08-AUG-07 08-AUG-07 <4 4 DAG R558986 Strontium (Sr)-Total mg/kg 08-AUG-07 08-AUG-07 RAMB 45.8 0.02 DAG R558986 Titanium (Ti)-Total mg/kg 08-AUG-07 08-AUG-07 367 0.03 DAG R558986
L7.3–7
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MINAGO L533759 CONTD.... 8 of 9 PAGE
ALS LABORATORY GROUP ANALYTICAL REPORT
Sample Details/Parameters Result Qualifier* D.L. Units Extracted Analyzed By Batch
L533759-8 MINAGO SAMPLE 6 (0 - 30 CM) Sampled By: LT / DMM on 18-JUL-07 Matrix: SOIL
Metals Thallium (Tl)-Total mg/kg 08-AUG-07 08-AUG-07 <0.2 0.2 DAG R558986 Uranium (U)-Total mg/kg 08-AUG-07 08-AUG-07 1.57 0.02 DAG R558986 Vanadium (V)-Total mg/kg 08-AUG-07 08-AUG-07 16.1 0.06 DAG R558986 Zinc (Zn)-Total mg/kg 08-AUG-07 08-AUG-07 RAMB 33 2 DAG R558986
L533759-9 MINAGO SAMPLE 7 (0 - 30 CM) Sampled By: LT / DMM on 18-JUL-07 Matrix: SOIL
Cyanide, Total mg/kg 08-AUG-07 15-AUG-07 6 1 DXN R561492 Loss on Ignition @ 550 C % 07-AUG-07 07-AUG-07 54.4 0 MMC R558484
Metals Silver (Ag)-Total mg/kg 08-AUG-07 08-AUG-07 <1 1 DAG R558986 Aluminum (Al)-Total mg/kg 08-AUG-07 08-AUG-07 5000 3 DAG R558986 Arsenic (As)-Total mg/kg 08-AUG-07 08-AUG-07 3.20 0.03 DAG R558986 Boron (B)-Total mg/kg 08-AUG-07 08-AUG-07 10.7 0.6 DAG R558986 Barium (Ba)-Total RAMB mg/kg 08-AUG-07 08-AUG-07 72.9 0.04 DAG R558986 Beryllium (Be)-Total mg/kg 08-AUG-07 08-AUG-07 0.23 0.06 DAG R558986 Bismuth (Bi)-Total mg/kg 08-AUG-07 08-AUG-07 0.10 0.02 DAG R558986 Calcium (Ca)-Total RAMB mg/kg 08-AUG-07 08-AUG-07 37500 7 DAG R558986 Cadmium (Cd)-Total mg/kg 08-AUG-07 08-AUG-07 0.16 0.02 DAG R558986 Cobalt (Co)-Total mg/kg 08-AUG-07 08-AUG-07 4.49 0.01 DAG R558986 Chromium (Cr)-Total mg/kg 08-AUG-07 08-AUG-07 15.0 0.1 DAG R558986 Copper (Cu)-Total mg/kg 08-AUG-07 08-AUG-07 11.2 0.2 DAG R558986 Iron (Fe)-Total mg/kg 08-AUG-07 08-AUG-07 9050 6 DAG R558986 Potassium (K)-Total mg/kg 08-AUG-07 08-AUG-07 966 7 DAG R558986 Magnesium (Mg)-Total mg/kg 08-AUG-07 08-AUG-07 11700 2 DAG R558986 Manganese (Mn)-Total RAMB mg/kg 08-AUG-07 08-AUG-07 1060 0.09 DAG R558986 Molybdenum (Mo)-Total mg/kg 08-AUG-07 08-AUG-07 0.59 0.02 DAG R558986 Sodium (Na)-Total mg/kg 08-AUG-07 08-AUG-07 RAMB 317 2 DAG R558986 Nickel (Ni)-Total mg/kg 08-AUG-07 08-AUG-07 14.6 0.2 DAG R558986 Lead (Pb)-Total mg/kg 08-AUG-07 08-AUG-07 7.76 0.05 DAG R558986 Selenium (Se)-Total mg/kg 08-AUG-07 08-AUG-07 0.4 0.1 DAG R558986 Tin (Sn)-Total mg/kg 08-AUG-07 08-AUG-07 <4 4 DAG R558986 Strontium (Sr)-Total mg/kg 08-AUG-07 08-AUG-07 RAMB 37.8 0.02 DAG R558986 Titanium (Ti)-Total mg/kg 08-AUG-07 08-AUG-07 312 0.03 DAG R558986 Thallium (Tl)-Total mg/kg 08-AUG-07 08-AUG-07 <0.2 0.2 DAG R558986 Uranium (U)-Total mg/kg 08-AUG-07 08-AUG-07 1.26 0.02 DAG R558986 Vanadium (V)-Total mg/kg 08-AUG-07 08-AUG-07 14.1 0.06 DAG R558986 Zinc (Zn)-Total RAMB mg/kg 08-AUG-07 08-AUG-07 25 2 DAG R558986
* Refer to Referenced Information for Qualifiers (if any) and Methodology.
L7.3–8
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MINAGO L533759 CONTD.... 9 PAGE 9 of
Reference Information
Sample Parameter Qualifier key listed: Qualifier Description
RAMB Result Adjusted For Method Blank
RRA Reported Result Is The Average Of 2 Or More Analyses
Methods Listed (if applicable): ALS Test Code Matrix Test Description Preparation Method Reference(Based On) Analytical Method Reference(Based On)
B-HOTW-AG-SK Soil Available Boron, Hot water (ug/cc) Methods of Soil Analysis (1996) SSSA CL-AG-SK Soil Available Chloride (ug/cc) NCR-13 (1998) P.26 CN-TOT-WP Soil Cyanide, Total EPA 9013A
Total Cyanides in Soil, Vegetation and Tissue: The sample is extracted with a strong base for 16 hours, then filtered. The filtrate is then analyzed for total cyanide as follows: Simple cyanides are converted to hydrogen cyanide (HCN) by distillation. Complex cyanides are not easily decomposed. Low power UV radiation is used to break down organic, metallic and alkali complexed compounds to free cyanide. The distillation step isolates HCN from simple cyanides under specific acidic conditions. The liberated HCN is converted to cyanogen chloride with chloramine-T. This further reacts with barbituric acid and isonicotinic acid to form a highly coloured complex.
LOI-550-SK Soil Loss on Ignition @ 550 C CSSS (1993) p.461-462
M.R. Carter (ed.). Soil Sampling and Methods of Analysis, Canadian Society of Soil Science (1993).p.461 & 462. Lewis Publishers Ann Arbor, MI METAL-DTPA-AG-SK Soil Avail Micronutrients CSSS 1993
(Cu,Fe,Zn,Mn) ug/cc METAL-LOW-EXD-WP Soil Metals EPA SW846 3050B Rev 2 1996 NO3-AG-SK Soil Available Nitrate-N (ug/cc) CSSS 1993 PH,EC-AG-SK Soil pH & EC 1:2 soil to water (Ag. CSSS 16.3,18.3.1 - 1:2 water extract
Method) PO4/K-AG-SK Soil Available Phosphate & Potassium COMM SOIL SCI 25 5&6
(ug/cc) SO4-AG-SK Soil Available Sulfate-S (ug/cc) NCR-13 (1998) P35-39 TEXTURE-HAND-SK Soil Qualitative Soil Texture- manual Qualitative
** Laboratory Methods employed follow in-house procedures, which are generally based on nationally or internationally accepted methodologies.
Chain of Custody numbers:
The last two letters of the above test code(s) indicate the laboratory that performed analytical analysis for that test. Refer to the list below:
Laboratory Definition Code Laboratory Location Laboratory Location Laboratory Definition Code
SK WP ALS LABORATORY GROUP - ALS LABORATORY GROUP - SASKATOON, SASKATCHEWAN, WINNIPEG, MANITOBA, CANADA CANADA
GLOSSARY OF REPORT TERMS Surr - A surrogate is an organic compound that is similar to the target analyte(s) in chemical composition and behavior but not normally detected in environmental samples. Prior to sample processing, samples are fortified with one or more surrogate compounds. The reported surrogate recovery value provides a measure of method efficiency. The Laboratory control limits are determined under column heading D.L. mg/kg (units) - unit of concentration based on mass, parts per million. mg/L (units) - unit of concentration based on volume, parts per million. < - Less than. D.L. - The reporting limit. N/A - Result not available. Refer to qualifier code and definition for explanation.
Test results reported relate only to the samples as received by the laboratory. UNLESS OTHERWISE STATED, ALL SAMPLES WERE RECEIVED IN ACCEPTABLE CONDITION. UNLESS OTHERWISE STATED, SAMPLES ARE NOT CORRECTED FOR CLIENT FIELD BLANKS. Although test results are generated under strict QA/QC protocols, any unsigned test reports, faxes, or emails are considered preliminary.
ALS Laboratory Group has an extensive QA/QC program where all analytical data reported is analyzed using approved referenced procedures followed by checks and reviews by senior managers and quality assurance personnel. However, since the results are obtained from chemical measurements and thus cannot be guaranteed, ALS Laboratory Group assumes no liability for the use or
interpretation of the results.
L7.3–9
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L7.3–10
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APPENDIX L7.5 Certified Laboratory Reports for Surface Water Quality
Page
Appendix L7.5-A: Data Quality Objectives – ALS Vancouver & Summary of Data Analysis for Water Samples with higher reported Dissolved versus Total Elemental Concentrations L7.5-1
Appendix L7.5-B: Summary of 2006 Trip Blank Water Quality Results
Summary of Sept.-Oct. 2007 & May 2008 Blanks WQ Results Summary of March 2008 Blanks Water Quality Results L7.5-7
Appendix L7.5-C: May 2006 Results L7.5-11 Appendix L7.5-D: June 2006 Results L7.5-36 Appendix L7.5-E: July 2006 Results L7.5-61 Appendix L7.5-F: August 2006 Results L7.5-94 Appendix L7.5-G: September 2006 Results L7.5-117 Appendix L7.5-H: October 2006 Results L7.5-140
Appendix L7.5-I: May 2007 Results L7.5-161 Appendix L7.5-J: June 2007 Results L7.5-194 Appendix L7.5-K: July 2007 Results L7.5-240 Appendix L7.5-L: August 2007 Results L7.5-280 Appendix L7.5-M: September 2007 Results L7.5-328 Appendix L7.5-N: October 2007 Results L7.5-433
Appendix L7.5-O: March 2008 Results L7.5-495 Appendix L7.5-P: May 2008 Results L7.5-516
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APPENDIX L7.5-A Data Quality Objectives – ALS Vancouver
&
Summary of Data Analysis for Water Samples with Higher
reported Dissolved versus Total Element Concentrations
L7.5–1
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Data Quality Objectives – ALS Vancouver
L7.5–2
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L7.5–3
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Summary of Data Analysis for Water Samples with Higher reported Dissolved versus Total Element Concentrations
Issue: Dissolved element concentrations reported by the testing laboratories were at times higher than the reported total element concentrations. In theory, dissolved element concentrations are never higher than the total element concentrations.
Investigation: As part of the investigation of this finding, error bounds were calculated for all of the Minago WQ data based on the Data Quality Objectives (DQO) for precision provided by the ALS Vancouver Laboratory. Precision was assumed to be the absolute value of the Relative Percent Difference (RPD) for laboratory duplicate samples plus/minus the additional value of square root of 2 multiplied by the detection limit (DL) to deal with variability of the two results near the detection limit. Thus, the difference between results was assumed to
be: )2( DLmeanRPD ×+×≤ . A sample calculation of the error bounds is
given below.
Example Calculation of Error Bounds:
Aug. 2007 data for aluminum recorded at MRW1:
Total Aluminum (T-Al) 0.0210 ± ∆ T-Al mg/L
Difference: -0.0068 mg/L Dissolved Aluminum (D-Al) 0.0278 ± D D-Al mg/L
1. Assume RPD% for aluminum is 20%, thus the RPD factor is 0.2.
2. In this example: Mean = 0.0210 mg/L for Total aluminum Mean = 0.0278 mg/L for Dissolved aluminum
3. In this example: DL = 0.001 mg/L. Allowable Difference (Error): ∆ T-Al = 0.2 x 0.0210 + 0.00141 = 0.00561 mg/L Allowable Difference (Error): ∆ D-Al = 0.2 x 0.0278 + 0.00141 = 0.00697 mg/L Thus, the range for Total Aluminum (T-AL ± ∆T-Al) is: 0.01539 mg/L < T-Al < 0.02661 mg/L, and the range for Dissolved Aluminum (D-AL ± ∆D-Al) is: 0.02083 mg/L < D-Al < 0.03477 mg/L.
Therefore, T-AL and D-Al share the same region and are not significantly different.
L7.5–4
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Error Bound Calculations:
The error bounds were calculated for all Minago water quality data in a similar fashion to the sample calculation presented above. The following assumptions were made in the error bound calculations and comparisions of dissolved and total element concentrations:
• if the measured concentration of an element was below the detection limit, the value for that concentration was set to half of the detection limit;
• if no replicate laboratory data existed for a parameter or if the measured RPD% value was greater than 20%, the RPD% value was set to 20% in the first set of calculations;
• in another set of calculations, all RPD% values were set to 20%.
Results of the Investigation re. Higher Dissolved versus Total Element Concentrations
All Minago water samples for which the reported dissolved element concentrations were higher than the total element concentrations were identified. For these water samples, an analysis was undertaken to determine whether those differences were actually significant based on the calculated error bounds (as was illustrated above). For the vast majority of water samples, the differences between the measured total and dissolved element concentrations were not significant. However, for some of the water samples the differences were significant. Table L7.5-1 summarizes the number of test results for which the differences were significantly different and could not solely be explained with the error bounds. Details of the element concentrations for these water samples and their error bounds are presented at the end of each of the appendices containing the laboratory certified reports.
MRW1 Aug. 2007 Data
0.0000.0050.0100.0150.0200.0250.0300.0350.040
Total Al Dissolved AlC
once
ntra
tion
(mg/
L)
L7.5–5
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Table L7.5-1 Number of Test Results with Significant Higher Dissolved versus Total Concentrations
Sampling Date
Number of Results that could not be fully explained with the error bounds assuming
RPD as measured or 20% for which no RPD existed
Number of Results that could not be
fully explained with the error
bounds assuming RPD
was 20%
Consultant / Lab
03-May-06 1 1 Wardrop / Maxxam 16-May-06 5 0 Wardrop / Maxxam 20-Jun-06 0 0 Wardrop / Maxxam 18-Jul-06 18 0 Wardrop / Maxxam 22-Aug-06 3 0 Wardrop / Maxxam 19-Sep-06 6 0 Wardrop / Maxxam 12-Oct-06 3 0 Wardrop / Maxxam
15-May-07 5 3 URS / ALS Vancouver 12-Jun-07 1 0 URS / ALS Vancouver 15-Jul-07 4 0 URS / ALS Vancouver 15-Aug-07 6 5 URS / ALS Vancouver 12-Sep-07 3 2 KR Design / ALS Vancouver 15-Oct-07 0 0 KR Design / ALS Vancouver 11-Mar-08 1 0 KR Design / ALS Vancouver 6-9 May-08 32 0 KR Design / ALS Vancouver
For samples were the differences were significant, the error might be due to laboratory method variability as well as other factors such as:
• field sampling method variability;
• bias introduced during general handling, storage, transportation and/or analysis of the sample;
• field sample grab bias - where separate grab samples are processed to produce total and dissolved samples.
L7.5–6
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APPENDIX L7.5-B
Summary of 2006 Trip Blank Water Quality Results
Summary of Sept.-Oct. 2007 & May 2008 Blanks WQ Results Summary of March 2008 Blanks Water Quality Results
L7.5–7
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SUMMARY OF TRIP BLANK RESULTS FOR 2006 WATER QUALITY ANALYSES July 18-20, August 22- September October 12,
May 3, 2006 June 20, 2006 2006 24, 2006 19-20, 2006 2006 Units RDL
Physical/Chemical Properties Alkalinity (PP as CaCO3) mg/L 0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Alkalinity (Total as CaCO3) mg/L 0.5 0.7 0.6 <0.5 0.8 1.8 <0.5 Total Dissolved Solids mg/L 1 <1 <1 <1 <1 1 <1 Total Hardness (CaCO3) mg/L 0.5 <0.5 <0.5 <0.5 <0.5 0.5 <0.5 Total Suspended Solids mg/L 1 <1 <1 <1 <1 <1 <1 True Colour Col. Unit 5 <5 <5 <5 <5 <5 <5 Turbidity NTU 0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 Major Ions Dissolved Calcium (Ca) mg/L 0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 Dissolved Chloride (Cl) mg/L 0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Dissolved Magnesium (Mg) mg/L 0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 Dissolved Potassium (K) mg/L 0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 Dissolved Sodium (Na) mg/L 0.05 <0.05 <0.05 <0.05 <0.05 <0.5 <0.05 Dissolved Sulphate (SO4) mg/L 0.5 <0.5 0.6 <5 ( 1 ) <0.5 <0.5 <0.5 Fluoride (F) mg/L n/a n/a <0.01 <0.01 0.01 0.01 Nutrients Ammonia (N) mg/L 0.005 <0.005 <0.005 <0.005 0.007 0.005 0.007 Dissolved Inorganic Carbon (C) mg/L 0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Dissolved Organic Carbon (C) mg/L 0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Dissolved Phosphorus (P) mg/L 0.002 <0.002 <0.002 <0.002 <0.002 <0.002 <0.002 Nitrate (N) mg/L 0.02 <0.02 0.02 <0.02 <0.02 0.02 <0.02 Nitrite (N) mg/L 0.005 0.047 <0.005 <0.005 <0.005 0.005 <0.005 Total Inorganic Carbon (C) mg/L 0.5 <0.5 <0.5 <0.5 0.6 <0.5 <0.5 Total Kjeldahl Nitrogen (Calc) mg/L 0.02 <0.02 <0.02 0.02 <0.02 <0.02 <0.02 Total Organic Carbon (C) mg/L 0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Total Phosphorus (P) mg/L 0.002 0.002 <0.002 0.003 <0.002 <0.002 <0.002 Radiochemical Radium 226 Bq/L 0.01 <0.01 <0.01 <0.01 < 0.01 <0.01 0.02 Dissolved Metals Aluminum (Al) mg/L 0.0002 <0.0002 0.0004 0.0003 <0.0002 0.0003 <0.0002 Antimony (Sb) mg/L 0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 Arsenic (As) mg/L 0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 Barium (Ba) mg/L 0.00002 <0.00002 <0.00002 <0.00002 <0.00002 <0.00002 <0.00002 Beryllium (Be) mg/L 0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 Bismuth (Bi) mg/L 0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 Boron (B) mg/L 0.008 <0.008 <0.008 <0.008 <0.008 <0.008 <0.008 Cadmium (Cd) mg/L 0.00001 0.00003 <0.00001 <0.00001 <0.00001 <0.00001 <0.00001 Chromium (Cr) mg/L 0.0002 <0.0002 0.0002 0.0004 <0.0002 <0.0002 <0.0002 Cobalt (Co) mg/L 0.00002 <0.00002 <0.00002 <0.00002 <0.00002 <0.00002 <0.00002 Copper (Cu) mg/L 0.0001 <0.0001 0.0001 0.0002 <0.0001 <0.0001 <0.0001 Iron (Fe) mg/L 0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 Lead (Pb) mg/L 0.00002 <0.00002 <0.00002 <0.00002 <0.00002 <0.00002 <0.00002 Lithium (Li) mg/L 0.0002 <0.0002 0.0003 <0.0002 <0.0002 <0.0002 <0.0002 Manganese (Mn) mg/L 0.00002 <0.00002 0.00002 <0.00002 <0.00002 <0.00002 <0.00002 Mercury (Hg) mg/L 0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 Molybdenum (Mo) mg/L 0.00002 <0.00002 <0.00002 <0.00002 <0.00002 <0.00002 <0.00002 Nickel (Ni) mg/L 0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 Selenium (Se) mg/L 0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 Silicon (Si) mg/L 0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 Silver (Ag) mg/L 0.00001 <0.00001 <0.00001 <0.00001 <0.00001 <0.00001 <0.00001 Strontium (Sr) mg/L 0.00001 0.00004 <0.00001 0.00002 <0.00001 <0.00001 0.00003 Thallium (Tl) mg/L 0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 Tin (Sn) mg/L 0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 Titanium (Ti) mg/L 0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 Uranium (U) mg/L 0.00001 <0.00001 <0.00001 <0.00001 <0.00001 <0.00001 <0.00001 Vanadium (V) mg/L 0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 Zinc (Zn) mg/L 0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 Total Metals Aluminum (Al) mg/L 0.0002 <0.0002 0.0018 0.0010 0.0019 0.0007 <0.0002 Antimony (Sb) mg/L 0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 Arsenic (As) mg/L 0.0001 <0.0001 <0.0001 <0.0001 <0.0001 <0.0001 0.0002 Barium (Ba) mg/L 0.00002 <0.00002 0.00005 0.00003 0.00004 0.00010 <0.00002 Beryllium (Be) mg/L 0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 Bismuth (Bi) mg/L 0.00005 <0.00005 <0.00005 0.00005 0.00009 <0.00005 <0.00005 Boron (B) mg/L 0.008 <0.008 <0.008 <0.008 <0.008 <0.008 <0.008 Cadmium (Cd) mg/L 0.00001 0.00003 <0.00001 <0.00001 <0.00001 <0.00001 <0.00001 Calcium (Ca) mg/L 0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 Chromium (Cr) mg/L 0.0002 <0.0002 0.0010 0.0005 0.0006 0.0007 <0.0002 Cobalt (Co) mg/L 0.00002 <0.00002 0.00003 <0.00002 <0.00002 0.00022 <0.00002 Copper (Cu) mg/L 0.0001 <0.0001 0.0002 0.0001 0.0001 <0.0001 <0.0001 Iron (Fe) mg/L 0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 Lead (Pb) mg/L 0.00002 <0.00002 <0.00002 0.00002 <0.00002 <0.00002 <0.00002 Lithium (Li) mg/L 0.0002 <0.0002 <0.0002 <0.0002 <0.0002 <0.0002 <0.0002 Magnesium (Mg) mg/L 0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 Manganese (Mn) mg/L 0.00002 <0.00002 0.00023 0.00012 0.00007 0.00004 0.00002 Mercury (Hg) mg/L 0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 Molybdenum (Mo) mg/L 0.00002 <0.00002 0.00006 <0.00002 <0.00002 <0.00002 <0.00002 Nickel (Ni) mg/L 0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 Potassium (K) mg/L 0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 Selenium (Se) mg/L 0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 Silicon (Si) mg/L 0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 Silver (Ag) mg/L 0.00001 <0.00001 <0.00001 <0.00001 0.00001 <0.00001 <0.00001 Sodium (Na) mg/L 0.05 0.06 <0.05 <0.05 <0.05 <0.05 <0.05 Strontium (Sr) mg/L 0.00001 <0.00001 0.00003 0.00006 0.00002 0.00002 0.00004 Thallium (Tl) mg/L 0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 Tin (Sn) mg/L 0.00005 <0.00005 0.00007 0.00006 <0.00005 <0.00005 <0.00005 Titanium (Ti) mg/L 0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 Uranium (U) mg/L 0.00001 <0.00001 <0.00001 <0.00001 0.00001 <0.00001 <0.00001 Vanadium (V) mg/L 0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 <0.00005 Zinc (Zn) mg/L 0.0005 <0.0005 <0.0005 0.0006 0.0005 <0.0005 <0.0005
L7.5–8
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File 39548827
MINAGO MINAGO MINAGO MINAGO MINAGO MINAGO Sample ID TRAVEL FIELD TRAVEL TRAVEL EQUIP RINSE FIELD BLANK BLANK BLANK BLANK BLANK
Date Sampled 12-SEP-07 12-SEP-07 Oct. 2007 Oct. 2007 08-May-08 09-May-08
ALS Sample ID L557035-2 L557035-3 L569390-22 L569390-23 L632454-12 L632454-13 Matrix Water Water Water Water Water Water
Physical Tests Hardness (as CaCO3) mg/L 0.5 0.5 <0.50 <0.50 <0.50 <0.50
Total Elements Aluminum (Al)-Total mg/L <0.0010 <0.0010 <0.0010 <0.0010 <0.0010 <0.0010 Antimony (Sb)-Total mg/L <0.000050 <0.000050 <0.000050 - <0.000050 <0.000050 Arsenic (As)-total mg/L <0.000030 <0.000030 <0.000030 <0.000030 <0.000030 <0.000030 Barium (Ba)-Total mg/L <0.000050 <0.000050 <0.000050 <0.000050 <0.000050 <0.000050 Beryllium (Be)-total mg/L <0.00020 <0.00020 <0.00020 <0.00020 <0.00020 <0.00020 Bismuth (Bi)-Total mg/L <0.00050 <0.00050 <0.00050 <0.00050 <0.00050 <0.00050 Boron (B)-total mg/L <0.0010 <0.0010 <0.0010 <0.0010 <0.0010 <0.0010 Cadmium (Cd)-Total mg/L <0.000017 <0.000017 <0.000017 <0.000017 <0.000017 <0.000017 Calcium (Ca)-Total mg/L 0.050 <0.020 0.182 <0.020 <0.020 <0.020 Chromium (Cr)-Total mg/L <0.00010 <0.00010 <0.00010 <0.00010 <0.00010 <0.00010
Trivalent Chromium (Cr-III) Hexavalent Chromium (Cr-VI)
Cobalt (Co)-Total mg/L <0.00010 <0.00010 <0.00010 <0.00010 <0.00010 <0.00010 Copper (Cu)-Total mg/L <0.00050 <0.00050 <0.00010 <0.00010 <0.00010 <0.00010 Iron (Fe)-Total mg/L <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 Lead (Pb)-Total mg/L <0.000050 <0.000050 <0.000050 <0.000050 <0.000050 <0.000050 Lithium (Li)-Total mg/L <0.0050 <0.0050 <0.0050 <0.0050 <0.0050 <0.0050 Magnesium (Mg)-Total mg/L <0.010 <0.010 <0.0050 <0.0050 <0.0050 <0.0050 Manganese (Mn)-Total mg/L <0.000050 <0.000050 0.000104 <0.000050 <0.000050 <0.000050 Mercury (Hg)-Total mg/L <0.000020 <0.000020 <0.000010 <0.000010 <0.000010 <0.000010
Inorganic Mercury Methylmercury
Molybdenum (Mo)-Total mg/L <0.000050 <0.000050 <0.000050 <0.000050 <0.000050 <0.000050 Nickel (Ni)-Total mg/L <0.00010 <0.00010 <0.00010 <0.00010 <0.00010 <0.00010 Phosphorus (P)-Total mg/L <0.30 <0.30 <0.30 <0.30 <0.30 <0.30 Potassium (K)-Total mg/L <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 Selenium (Se)-Total mg/L <0.00010 <0.00010 <0.00010 <0.00010 <0.00010 <0.00010 Silicon (Si)-Total mg/L <0.050 <0.050 <0.050 <0.050 <0.050 <0.050 Silver (Ag)-Total mg/L <0.00010 <0.00010 <0.000010 <0.000010 <0.000010 <0.000010 Sodium (Na)-Total mg/L <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 Strontium (Sr)-Total mg/L <0.00010 <0.00010 0.00012 <0.00010 <0.00010 <0.00010 Thallium (Tl)-Total mg/L <0.000050 <0.000050 <0.000050 <0.000050 <0.000050 <0.000050 Tin (Sn)-Total mg/L <0.00010 <0.00010 <0.00010 <0.00010 <0.00010 <0.00010 Titanium (Ti)-Total mg/L <0.010 <0.010 <0.010 <0.010 <0.010 <0.010 Uranium (U)-Total mg/L <0.000010 <0.000010 <0.000010 <0.000010 <0.000010 <0.000010 Vanadium (V)-Total mg/L <0.000050 0.000135 <0.000050 <0.000050 <0.000050 <0.000050 Zinc (Zn)-Total mg/L <0.0010 <0.0010 <0.0010 <0.0010 <0.0010 <0.0010
Summary of Sept. & Oct. 2007 and May 2008 Travel and Field Blanks
L7.5–9
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Deionized water for these samples was RESULTS OF ANALYSIS Units prepared by the ALS Winnipeg Lab
Concentrations in the Deionized Water SAMPLE OF
FILTER TRAVEL at the time of Sample ID DEIONIZED FIELD BLANK
BLANK BLANK WATER preparation at ALS
Winnipeg Lab Date Sampled 11-MAR-08 11-MAR-08 11-MAR-08 11-MAR-08 Time Sampled 00:00 00:00 00:00 00:00 ALS Sample ID L610409-4 L610409-5 L610409-6 L610409-7 Matrix Water Water Water Water
Concentrations as measured by ALS Vancouver
Physical Tests Hardness (as CaCO3) mg/L <0.50 <0.50 <0.50 <0.50
Total Elements Aluminum (Al)-Total mg/L - <0.0010 <0.0010 <0.0010 <0.005 Antimony (Sb)-Total mg/L - 0.000844 0.000836 0.000798 <0.001 Arsenic (As)-total mg/L - <0.000030 <0.000030 <0.000030 <0.0005 Barium (Ba)-Total mg/L - <0.000050 <0.000050 <0.000050 <0.0003 Beryllium (Be)-total mg/L - <0.00020 <0.00020 <0.00020 <0.001 Bismuth (Bi)-Total mg/L - <0.00050 <0.00050 <0.00050 <0.0001 Boron (B)-total mg/L - 0.0034 0.0019 0.0018 <0.03 Cadmium (Cd)-Total mg/L - <0.000017 <0.000017 <0.000017 <0.00002 Calcium (Ca)-Total mg/L - <0.020 0.18 <0.020 <0.1 Chromium (Cr)-Total mg/L - 0.00027 <0.00010 <0.00010 <0.001 Cobalt (Co)-Total mg/L - <0.00010 <0.00010 <0.00010 <0.0002 Copper (Cu)-Total mg/L - <0.00010 <0.00010 <0.00010 <0.001 Iron (Fe)-Total mg/L - <0.010 <0.010 <0.010 <0.05 Lead (Pb)-Total mg/L - <0.000050 <0.000050 <0.000050 <0.0005 Lithium (Li)-Total mg/L - <0.0050 <0.0050 <0.0050 <0.01 Magnesium (Mg)-Total mg/L - 0.0327 <0.0050 <0.0050 <0.01 Manganese (Mn)-Total mg/L - <0.000050 <0.000050 <0.000050 <0.0003 Mercury (Hg)-Total mg/L - <0.000010 <0.000010 <0.000010 <0.0001 Molybdenum (Mo)-Total mg/L - <0.000050 <0.000050 <0.000050 <0.0002 Nickel (Ni)-Total mg/L - <0.00010 <0.00010 <0.00010 <0.002 Phosphorus (P)-Total mg/L - <0.30 <0.30 <0.30 <0.05 Potassium (K)-Total mg/L - <0.050 <0.050 <0.050 <0.1 Selenium (Se)-Total mg/L - <0.00010 <0.00010 <0.00010 <0.001 Silicon (Si)-Total mg/L - <0.050 <0.050 <0.050 <0.3 Silver (Ag)-Total mg/L - <0.000010 <0.000010 <0.000010 <0.0001 Sodium (Na)-Total mg/L - <0.010 <0.010 <0.010 <0.03 Strontium (Sr)-Total mg/L - <0.00010 <0.00010 <0.00010 <0.0001 Thallium (Tl)-Total mg/L - <0.000050 <0.000050 <0.000050 <0.0001 Tin (Sn)-Total mg/L - <0.00010 <0.00010 <0.00010 <0.0006 Titanium (Ti)-Total mg/L - <0.010 <0.010 <0.010 <0.0009 Uranium (U)-Total mg/L - <0.000010 <0.000010 <0.000010 <0.0001 Vanadium (V)-Total mg/L - <0.000050 <0.000050 <0.000050 <0.001 Zinc (Zn)-Total mg/L - <0.0010 <0.0010 <0.0010 <0.01
Dissolved Elements Aluminum (Al)-Dissolved mg/L <0.0010 - - - <0.001 Antimony (Sb)-Dissolved mg/L 0.000961 - - - <0.001 Arsenic (As)-Dissolved mg/L <0.000030 - - - <0.0005 Barium (Ba)-Dissolved mg/L <0.000050 - - - <0.0003 Beryllium (Be)-Dissolved mg/L <0.00020 - - - <0.001 Bismuth (Bi)-Dissolved mg/L <0.00050 - - - <0.0003 Boron (B)-Dissolved mg/L 0.0031 - - - <0.02 Cadmium (Cd)-Dissolved mg/L <0.000017 - - - <0.00002 Calcium (Ca)-Dissolved mg/L <0.020 - - - <0.05 Chromium (Cr)-Dissolved mg/L <0.00010 - - - <0.001 Cobalt (Co)-Dissolved mg/L <0.00010 - - - <0.0002 Copper (Cu)-Dissolved mg/L <0.00010 - - - <0.0004 Iron (Fe)-Dissolved mg/L <0.010 - - - <0.01 Lead (Pb)-Dissolved mg/L <0.000050 - - - <0.0001 Lithium (Li)-Dissolved mg/L <0.0050 - - - <0.005 Magnesium (Mg)-Dissolved mg/L 0.0081 - - - <0.01 Manganese (Mn)-Dissolved mg/L <0.000050 - - - <0.0002 Mercury (Hg)-Dissolved mg/L <0.000010 - - - <0.00005 Molybdenum (Mo)-Dissolved mg/L <0.000050 - - - <0.0001 Nickel (Ni)-Dissolved mg/L <0.00010 - - - <0.0002 Phosphorus (P)-Dissolved mg/L <0.30 - - - <0.02 Potassium (K)-Dissolved mg/L <0.050 - - - <0.05 Selenium (Se)-Dissolved mg/L <0.00010 - - - <0.001 Silicon (Si)-Dissolved mg/L <0.050 - - - <0.2 Silver (Ag)-Dissolved mg/L <0.000010 - - - <0.0001 Sodium (Na)-Dissolved mg/L <0.010 - - - <0.02 Strontium (Sr)-Dissolved mg/L <0.00010 - - - <0.0001 Thallium (Tl)-Dissolved mg/L <0.000050 - - - <0.0001 Tin (Sn)-Dissolved mg/L <0.00010 - - - <0.0003 Titanium (Ti)-Dissolved mg/L <0.010 - - - <0.0005 Uranium (U)-Dissolved mg/L <0.000010 - - - <0.0001 Vanadium (V)-Dissolved mg/L <0.000050 - - - <0.001 Zinc (Zn)-Dissolved mg/L <0.0010 - - - <0.005
L7.5–10
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APPENDIX L7.5-C Certified Laboratory Reports for Surface Water Quality
May 2006 Results
L7.5–11
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L7. 5–12
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L7.5–13
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L7.5–14
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L7.5–15
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L7.5–16
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L7.5–17
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L7.5–18
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L7.5–19
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L7.5–20
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L7.5–21
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L7.5–22
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L7.5–23
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L7.5–24
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L7.5–25
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L7.5–26
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L7.5–27
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L7.5–28
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L7.5–29
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L7.5–30
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L7.5–31
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L7.5–32
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L7.5–33
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L7.5–34
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May 3, 2006 Minago Surface Water Quality Datafor which the measured Dissolved concentration was higher than the Total concentration
May 3, 2006 Surface Water Quality Data
0.000000.000500.001000.001500.002000.00250
Total Cu Dissolved Cu
WRStation
Con
cent
ratio
n (m
g/L)
May 16, 2006 Minago Surface Water Quality Datafor which the measured Dissolved concentrations were higher than the Total concentrations
May 16, 2006 Surface Water Quality Data
0
5
10
15
20
25
30
35
40
45
50
Total Ca DissolvedCa
Total Ca DissolvedCa
Total Ca DissolvedCa
Total Mg DissolvedMg
Total Ca DissolvedCa
MRW1 OCW1 OCW-2A OCW-2A OCW-3a
Station
Con
cent
ratio
n (m
g/L)
L7.5–35
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APPENDIX L7.5-D Certified Laboratory Reports for Surface Water Quality
June 2006 Results
L7.5–36
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File 39548827
L7.5–37
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L7.5–38
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L7.5–39
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L7.5–40
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L7.5–41
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L7.5–42
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L7.5–43
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L7.5–44
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L7.5–45
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L7.5–46
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L7.5–47
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L7.5–48
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L7.5–49
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L7.5–50
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L7.5–51
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L7.5–52
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L7.5–53
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L7.5–54
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L7.5–55
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L7.5–56
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L7.5–57
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L7.5–58
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L7.5–59
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L7.5–60
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APPENDIX L7.5-E Certified Laboratory Reports for Surface Water Quality
July 2006 Results
L7.5–61
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File 39548827
L7.5–62
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L7.5–63
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L7.5–64
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L7.5–65
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L7.5–66
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L7.5–67
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L7.5–68
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L7.5–69
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L7.5–70
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L7.5–71
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L7.5–72
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L7.5–73
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L7.5–74
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L7.5–75
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L7.5–76
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L7.5–77
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L7.5–78
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L7.5–79
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L7.5–80
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L7.5–81
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L7.5–82
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L7.5–83
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L7.5–84
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L7.5–85
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L7.5–86
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L7.5–87
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L7.5–88
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L7.5–89
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L7.5–90
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L7.5–91
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July 18-20, 2006 Minago Surface Water Quality Datafor which the measured Dissolved concentrations were higher than the Total concentrations
July 18-20, 2006 Surface Water Quality Data (Series 1)
0.0000
0.0100
0.0200
0.0300
0.0400
0.0500
0.0600
Total Ba DissolvedBa
Total Ba DissolvedBa
Total Sr DissolvedSr
Total Sr DissolvedSr
Total Sr DissolvedSr
OCW1 OCW-2A MRW1 OCW1 OCW-2A
Station
Con
cent
ratio
n (m
g/L)
July 18-20, 2006 Surface Water Quality Data (Series 2)
0
1
2
3
4
5
6
Total Si DissolvedSi
Total Si DissolvedSi
Total Si DissolvedSi
Total Si DissolvedSi
Total Na DissolvedNa
MRW1 OCW1 OCW-2A OCW-3A MRW1
Station
Con
cent
ratio
n (m
g/L)
L7.5–92
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July 18-20, 2006 Minago Surface Water Quality Datafor which the measured Dissolved concentrations were higher than the Total concentrations
July 18-20, 2006 Surface Water Quality Data (Series 3)
0
10
20
30
40
50
60
70
Tota
l Ca
Dis
solv
edC
a
Tota
l Ca
Dis
solv
edC
a
Tota
l Ca
Dis
solv
edC
a
Tota
l Ca
Dis
solv
edC
a
Tota
l Mg
Dis
solv
edM
g
Tota
l Mg
Dis
solv
edM
g
Tota
l Mg
Dis
solv
edM
g
Tota
l Mg
Dis
solv
edM
g
MRW1 OCW1 OCW-2A OCW-3A MRW1 OCW1 OCW-2A OCW-3A
Station
Con
cent
ratio
n (m
g/L)
L7.5–93
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APPENDIX L7.5-F Certified Laboratory Reports for Surface Water Quality
August 2006 Results
L7.5–94
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L7.5–95
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L7.5–96
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L7.5–97
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L7.5–98
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L7.5–99
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L7.5–100
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L7.5–101
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L7.5–102
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L7.5–103
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L7.5–104
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L7.5–105
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L7.5–106
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L7.5–107
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L7.5–108
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L7.5–109
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L7.5–110
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L7.5–111
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L7.5–112
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L7.5–113
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L7.5–114
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L7.5–115
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Aug. 22-24, 2006 Minago Surface Water Quality Data
for which the measured Dissolved concentrations were higher than the Total concentrations
Aug. 22-24, 2006 Surface Water Quality Data
0
10
20
30
40
50
60
70
Total Ca Dissolved Ca Total Ca Dissolved Ca Total Mg DissolvedMg
MRW1 OCW1 OCW1
Station
Con
cent
ratio
n (m
g/L)
L7.5–116
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APPENDIX L7.5-G Certified Laboratory Reports for Surface Water Quality
September 2006 Results
L7.5–117
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File 39548827
L7.5–118
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L7.5–119
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L7.5–120
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L7.5–121
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L7.5–122
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L7.5–123
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L7.5–124
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L7.5–125
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L7.5–126
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L7.5–127
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L7.5–128
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L7.5–129
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L7.5–130
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L7.5–131
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L7.5–132
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L7.5–133
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L7.5–134
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L7.5–135
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L7.5–136
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L7.5–137
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L7.5–138
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Sept. 19-21, 2006 Minago Surface Water Quality Datafor which the measured Dissolved concentrations were higher than the Total concentrations
Sept. 19-21, 2006 Surface Water Quality Data (Series 1)
0102030405060
Tota
l Ca
Dis
solv
edC
a
Tota
l Mg
Dis
solv
edM
g
Tota
l Ca
Dis
solv
edC
a
Tota
l Mg
Dis
solv
edM
g
Tota
l Mg
Dis
solv
edM
g
MRW1 MRW1 OCW-2A OCW-2A OCW-3A
Station
Con
cent
ratio
n (m
g/L)
Sept. 19-21, 2006 Surface Water Quality Data (Series 2)
0.00
0.01
0.02
0.03
0.04
0.05
0.06
Total Sr Dissolved Sr
OCW-2A
Station
Con
cent
ratio
n (m
g/L)
L7.5–139
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APPENDIX L7.5-H Certified Laboratory Reports for Surface Water Quality
October 2006 Results
L7.5–140
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File 39548827
L7.5–141
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L7.5–142
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L7.5–143
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L7.5–144
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L7.5–145
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L7.5–146
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L7.5–147
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L7.5–148
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L7.5–149
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L7.5–150
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L7.5–151
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L7.5–152
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L7.5–153
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L7.5–154
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L7.5–155
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L7.5–156
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L7.5–157
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L7.5–158
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L7.5–159
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Oct. 12, 2006 Minago Surface Water Quality Datafor which the measured Dissolved concentrations were higher than the Total concentrations
Oct. 12, 2006 Surface Water Quality Data
0.0000.0050.0100.0150.0200.0250.0300.0350.040
Total Ba DissolvedBa
Total Ba DissolvedBa
Total Sr DissolvedSr
OCW-2A OCW-3A OCW-3A
Station
Con
cent
ratio
n (m
g/L)
L7.5–160