etay hailu sugar power point
TRANSCRIPT
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Sugar processing
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Cane supply
Cane transportation starts immediately after cutting
Therefore cane transportation and storage time should always be
kept to a minimum
Deterioration is accelerated by high temperature, light, loss of
moisture, all of which factors are greater under tropical
conditions.
To minimize the delay time a close cooperation between
harvesting crew and factory people is essential
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Raw materials and its accessories
• The raw materials used in the every sugar factory is
sugar cane.Howeverthere are accessories material
used for dierent purpases
• For instance Sulphur dioxide-used in clarication
process to make
- rapid setting of uice
- fast !oiling of massecuite- fast crystali"ation of sucrose
- market improvement of suger colour
- !etter elimination of phosphates and waxes
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• #ime$%a&'-also used during clarication to(
neuterili"e the free organic acids present in a uice
for the pricipitation of colouring matters
• )ater-used for
*m!i!ition(process in which water is applied to the crushed
cane to enhance the extraction of the uice at the next mill!
Steam generation
Sugar wash . . .etc
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Cane cutting method
• "and cutting
• #echanical cutting
1. Hand Cutting$
. %ndoubtedly, hand cut cane is better suited for factory processing
than mechanically harvested cane
. &ecause a hand cut cane is cleaner and its purities are higher
since in general cane is cut lower to the ground by hand than by
machine
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The highest sugar content is known to be in the lowest part of the
cane stalk, the poorest part being the top.
The cane toping is also properly done by hand cutting
2. Mechanical Cutting$
#echanically cutting and loading is a faster process.
The main problem with machine handling of cane is usually
damage to the field, harming future cane crop
particularly this occurs when harvesting is done during the rainy
season in which damage to the next years cane can be appreciable.
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• 'hen the cane is cut, rapid deterioration of the cane begins.
• Therefore, unlike sugar beets, sugarcane cannot be stored for later
processing without excessive deterioration of the sucrose content.
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Cane preparation
The preparation of the cane is accomplished by several ways.
&y revolving cane knives that cut the cane into chips but extracts
no uice.
&y shredders that tears the cane into shreds, but extract no uice.
&y crusher that break and crush the structure of the cane
extracting a large proportion of the uice.
&y combination of any or all of the means ust enumerated. we use
combination of and )
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• *reparation of the cane has three main obectives.
To increase capacity by increase of bulk density of the feed.
To assist extraction at the mills by breaking down the structure of
the cane.
To render the uice more readily available for the action of
+mbibition by breaking and opening cane cells
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Separation of Juice from Cane
The sugar content of cane is dissolved in uice contained in millions
of plant cells.
There are two different systems of extracting the sugar containing
uice from the cane. uch methods of extraction are$ -
a. &y means of pressure in a number of mills provided with three
rollers through which the cane is forced
b. &y means of diffusion, extracting uice by applying heat and
immersion in water and sueezing of the baggasse
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Milling process
• The classical combination of three rollers arranged in a triangular
form is the standard milling unit for industry
• The milling process may be separated into two steps
The preparation of cane by breaking down the hard structure and
rupturing the cells
The actual grinding of the cane
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+illing ,iagram
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• /or the grinding, or milling, of the crushed cane, multiple sets of
three-roller mills are most commonly used although some mills
consist of four, five, or six rollers in multiple sets
• Conveyors transport the crushed cane from one mill to the next.
• +mbibition is the process in which water or uice is applied to the
crushed cane to enhance the extraction of the uice at the next mill
• The crushed cane exiting the last mill is called bagasse
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elt conveyor
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Screw conveyor
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0ir unit (pump!
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Juice Screening
• #ixed uice from the milling tandem contains a large amount
of cane fiber that falls out with the uice between the rollers
of the mills.
• The process in which the fiber is separated from the uice is
called uice screening
Juice Screening Equipments
• 0 stationary and vibrating or rotating wire mesh screen.
• 0n inclined wedge-wire screen (D#!
• 0 rubber-lined Dorr clone (cyclone! system
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Extraction
• The term extraction is generally used to mean total sugar extracted
by the milling tandem, a percent of sugar in cane
Juice Weighing
• +n a sugar mill, the main material whose weight must be determined
is cane.
• The weight of cane is the most important information, since other
materials are always related to cane weigh
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• #ixed uice is normally weighed or measured.
• +f the uice is measured samples of each measuring tank is taken to
obtain an average density of the measured uice and find the
correct specific gravity.
• The volume of the uice is converted to weight by multiplying it by
its specific gravity
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• 1enerally, mixed uice weighing is the starting point for control of
the whole factory.
• 0ccurate weighing, sampling and analysis of uice for sucrose is
essential for determination of extraction, boiling house recovery
and boiling house efficiency
Juice Heating
• 2uice heating is excited in a number of vessels called uice heaters
or preheaters
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Heat Transfer Rate
• The fundamental heat transfer euation describes how heat is
transferred across the heating surface.
• The total heat flux across the heating surface of a heater is given by
a usual formula.
3 4 %0 ∆t
'here 3 4 Total heat flux, heat transferred, in ' or, 5Cal6hr!
% 4 7verall heat transfer coefficient in (5Cal6hr6m869C!
0 4 0rea of heating surface (ft8, m8!
∆t 4 Temperature drop of condensing steam to boiling uice. +n 5, oC.
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• The main purpose of such heating is the following.
Due to application of heat to the 2uice, certain organic constituents
like proteins are coagulated
"eat destroys microorganisms and enzymes preventing loss of
sucrose by microbiological activity
"eat accelerates the reaction rate between the uice acids and the
lime, which will be subseuently added
types of Juice Heaters
There are two main types of heaters.
• The *late "eat :xchangers
• 0 hell and Tube Type (;ertical and "orizontal!
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a. The Plate Heat Exchangers
. These types heaters are made up of a number of thin corrugated
or dimpled sheets separated by gaskets and held in place by an
adustable framework
. They are widely used for heating and cooling liuid sugars
(sucrose syrup and invert sugar solutions!
. The unit provides counter current or concurrent liuid-liuid heat
exchange, or vapor to liuid heat exchange or combined heatingand regenerative cooling in the same heat frame
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b. Shell and Tube T!pe "#erticaland Hori$ontal%-
+t is a uice heater consists of a cylindrical mild steel shell with a
heating tube, tube plate and header at each end.
The tube plates are perforated to receive the tubes, which are
expanded into them.
The shell is extended at both ends beyond the tube plates into
heaters, which are divided by baffles into compartments
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Juice clari&cation
• +n uice clarification process the elimination of non-sugars has to
be done in such a way that
• +norganic non-sugars are removed and not produced afresh when
the clarifying agents are used
• +f agents are not used under proper condition, color and ash are
produced afresh
•
<either sucrose nor reducing sugars are destroyed in considerableuantity
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• The main obects of cane uice clarification are$-
To separate soluble and insoluble matter that can precipitate
To reduce color and turbidity of the uice
To produce clear uice of correct p" (=.>!
To kill or inactivate microorganisms in the uice by heat treatment
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Methods of Juice Clarification
• Depending on the type of final product to be produced, there are
different methods of uice clarification
Carbonation process
Defecation *rocess
ulfitation *rocess
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Caronation !rocess$ The main clarifying agents in the carbonation
process are lime and C78 gas. The process consists of precipitating
calcium carbonate.
Ca (7"!8 ? C78 @ CaC7) ? "87
• The precipitate (Calcium Carbonate! adsorbs coloring matter and
gums
• +t is easily filterable. The raw uice is heated to a temperature A> B
AA>
C and pumped into the carbonation tank where lime is addedand mixed thoroughly.
• The uice is neutralized with C78 gas
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'efecation Process
Clarification by heat and lime is known as a simple defecation
process. ufficient lime is added to neutralize the organic acids
present in the uice, after which the temperature is raised >C
(boiling point!.
The treatment causes formation of heavy precipitate of complex
composition.
The flocculent precipitate carries with it most of the finely
suspended material of the uice that has escaped mechanical
screening.
0 uice clarified does the separation of this precipitate from the uice
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Sul&tation Process
• +n the sulfitation system clarification is done by heat lime and
sulphurdioxide gas
• The mixed uice is heated to =A >C, more lime slurry is added to the
raw uice and the excess of lime is neutralized by 78 gas.
• The process is called after the name of the acid used for
neutralization of excess lime EsulphitationF
• The treated uice is heated to >
C and separation of flocculated
non-sugars takes place in a continuous settler.
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• /rom the settler the clear uice continues in the process and the
underflow mud is a filtered on continuous drum filter and the
filtrate is recycled to the measured raw uice
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Juice (lashing
• The treated uice delivered by one of the suited pump and heated at
a temperature of about >8 9C - >A 9C
• contain air bubbles which retard setting in the further process.
• 'hile the under pressure uice enter tangentially in to cylindrical
(vertical! tank which has a large vent to the atmosphere called flash
tank, the bubbles attached to the suspended particles of the uice is
flash out.
• Tangential entrance of the uice used to give a circular movement of
the uice inside the flash tank and this benefit the separation of air
and this avoid the loss of uice through the escaping air
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(locculent
/locculent is materials of high molecular weight purchased in
powder form and it acts as abridge between two or more particles
present in the uice to unit the solid particles in to a loose porous
state
/locculent must be free flowing (solution! for mixing with the
uice
There are two flocculent tanks each has a capacity of G m) for
preparation of flocculent solution and to store the prepared one
The normal dosage in uice clarification is 8 B G ppm on weight of
uice
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Juice Setting
+n the clarifier, the suspended solids are allowed to settle out from
the uice
The uice flows upward at a velocity low enough to allow the
precipitate to settle
The precipitate are falling down against rising streams if uice
going to the overflow point
7bviously, for effective separation, the settling rate must be faster
than all of the up-flow streams of uice so that net direction of
particle movement is downward
f i i d f l f h l ifi
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• +f uice is drawn from only one compartment of the clarifier, a
very high upward velocities of uice exists which restricts the
falling rate of the precipitate or particles entertainment to the over
flow clear uice occurs
• clarifiers have a settling tray, which are supposed to segregate the
setting uice into compartments
• Hiuid-solid separation occurs utilizing the cross sectional area of
each tray
• This system reduces the overall up-flow velocity dividing it by the
number of settling trays
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'here$ ; - falling velocity of the particle (m6sec!
D - diameter of the particles (Cm!
d - density of the solid particle (gm6Cm)!
d8 - density of the liuid (gm6Cm)!
g - gravity constant Cm6sec8
u - viscosity of the liuid (poises!
The above euation is for a particle of spherical shape.
This is expressed by stokesI Haw
The settling rate of the particles depends on the size and density
of the particles as well as density and viscosity of the uice
u
g d d DV
D
!( 8
8−
=
E ti
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E)aporation
The evaporation process is the process of concentration of the
solids in uice with removed of the water, without substantial
changes in the composition or character of the solids in the
solution
+n the clarification, process impurities are removed from uice as
far as possible
The clarified uice contains about ) B J solids, depending on
the concentration of the original uice in the cane and the
imbibition practice employed
T d h f l i h b
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• To produce sugar, the water content of clear uice has to be
removed almost entirely
•
This is the obective of evaporation
• "ence the evaporation process is separated into two phases
a. :vaporation so called, which proceeds from clear uice to syrup,
and during which only liuid material is handled.
b. The sugar boiling (pan boiling!, in which further concentration is
carried out so that crystals form and are grown under controlled
conditions to the desired size
i ff i
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multiple Effect E"aporation
:vaporation in open pots over a fire had already been
abandoned and evaporation of uice by heating with steam
had been commenced
team is used for heating uice to evaporate the water which it
contains.
'ith steam at >>C, pressure >.G 5g6Cm8 uice at
atmospheric pressure may be heated and evaporated
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• the vapor of uice so boiling at atmospheric pressure is at >> >C.
&ut, with vapor at that temperature it is not possible to boil uice
at the same temperature
• 0 temperature difference is necessary between the heating fluid
and the fluid to be heated
• +t thus became possible to create the necessary temperature
difference and utilize the vapor arising from the uice in the st
vessel to heat the uice in the 8nd vessel, the vapor produce in the
8nd vessel to heat the uice in the )rd vessel, etc
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#apor *leeding"steam econom!%
• +n a multiple effect evaporators, it is possible to enlarge the st
vessel, tap off some of the vapor boiled there (instead of sending
all vapor to the next vessel!, and use that vapor for heating at other
stations like uice heating, pan boiling.
• This practice is called vapor bleeding and it results in further
saving of steam.
• &ut the exhaust steam saved is not eual to the exhaust steam that
would otherwise have had to be used to heat the mixed uice, but
to some fraction of it
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condenser
• 0 condenser is a tank in which the vapor enters near the bottom
and rises to condense on a shower of water droplets falling
through the tank.
• The water containing the condensed vapor leaves the condenser
by displacement through its barometric leg about >.G meter long
pipe
• 0bout G> B A> tons of water is needed to condense ton of vapor.
• The barometric leg of the condenser deeps into a sealing well that
is always filled with water
• +n condensers the total heat contained in vapor is transferred to the
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• +n condensers, the total heat contained in vapor is transferred to the
cooling water or inection water.
•
The inection water reuired per unit vapor can be calculated by theeuation
'here - Total heat in Cal65g of vapor
- Temperature of the in let water (>C!
- Temperature of the discharge water (>C'
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#acuums Pans
The operation known in the sugar factory, as sugar boiling is
essentially the process of crystallization, which is carried out in
single effect vacuum evaporators designed for handling viscous
materials and known as vacuum pans
Thus, the vacuum pan is an evaporative crystallizer in which
degree of super saturation is controlled by evaporating solvent as
the solute crystallizes out
T f #
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Types of #acuum pan
• There are two types of vacuum pans used in sugar boiling, namely
a.The Coil !ans
• The heating surface consists of a series of coils, ) − A in number
placed one upon the other.
• The coils occupy a large position of the cylindrical height.
• :ach coil set has a separate steam trap, a steam inlet and exhaust
value.
• The heating coils are made of copper tubing which are securely
held in position by tie rods.
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. calanderia pans
• +n calanderia pans the tubes are shorter and of larger diameter than
in evaporators.
• 'hether the pan is of coil or calanderia type, the massecuite rises
through the heating surface, between the turns of the coils or
through the tubes of the calanderia
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'etermination of Critical Points
• The different zones of super saturations are determined and
identified by experience.
• The sugar boilers learns by experience and observation to know
when a solution was the right degree of super saturation for
graining or growth of existing grain, though they didnKt think in
terms of super saturation.
• +n modern practice instruments are used which give an indication
of super saturation coefficient
+ i i , th d " i t%
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+raining ,ethods"assignment%
• There are two different techniues for establishing grain.
! 'aiting of pontaneous 1raining #ethod
8! eeding #ethod
a! hock eeding #ethod (Dry ugar Dust eeding #ethod!
b! The lurry #ethod
Crystalli$ation
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Crystalli$ation
Crystallization is a process which consists of mixing the massecuite
for certain time after dropping from the pans, and before passing tothe centrifugals.
The process is with the aim of completing the formation of crystals
and forcing further exhaustion of the mother liuor
The massecuite when discharged from the pan is at a high super
saturation.
+f it is allowed to stand, the sugar still contained in the mother
liuor will continue to be deposited as a crystal, but this masscuite
is very viscous
• Th f th it t b k t i ti i d t h
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• Therefore the masscuite must be kept in motion in order to change
constantly the relative positions of the particles of mother liuor
and crystals until the mother liuor becomes a substantiallyexhausted molasses
T!pes of Cr!stalli$ers
•
There are crystallizer of batch and continuous operation.Depending on the system of cooling there are-
. 0ir Cooled Crystallizers
8. 'ater Cooled Crystallizers
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-. irCooled Cr!stalli$ers
• The massecuite is cooled by the circulation of air from the walls
of crystallizers and from the surface of the massecuite.
• The cooling effect is slow. <owadays the air cooled crystallizers
are commonly used for storing high grade massecuite and their
use for cooling low grade massecuite is not favored
/ Water Cooled Cr!stalli$ers
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/.Water Cooled Cr!stalli$ers
These crystallizers have three arrangements$-
'ater acketed
Cooling coil of rotating type
• 'ater acketed crystallizers are not found very
satisfactory, recently they are not used.
•
The cooling coil of stationary type is less efficient due to
poor contact of the massecuite with the cooling surface.
• They are only used because of lower cost
Centrifugal Separation
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Centrifugal Separation
• The final stage of the process of sugar making has now been
peached.
• The sugar crystals mixed with the mother liuor has been obtained.
• 'hat remains is to separate them by the centrifugal force in proper
marketable form.
• uch separation is known as curing, purging by a centrifugal
machine
sugar con"eyor
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sugar con"eyor
ugar conveyors are of three designs
crew or scroll conveyor
1rass-hopper conveyor (shaker conveyor!
&elt or slat conveyor
. Scre% Con"eyors
• are not favored for carrying dry white sugar as crystals are liable to be
grounded there in.
•
crew conveyors are generally used to convey massecuite in horizontaltrough
• 0 full screw may be used, but more often the screw consists of a simple
metal ribbon held in place by steel strips
&elt Con"eyor
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&elt Con"eyor
• The dry sugar is conveyed horizontally by means of a belt conveyor
of 8 B )L inch width which saves the crystals from being rubbed
• The belt conveyor has the lowest power consumption and is only
used for moisture free sugar
Sugar Ele"ator
• The sugar elevator is used for lifting the sugar to a higher level.
• +t consists of a number of buckets attached to the endless
detachable chain
Sugar dr!er
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Sugar dr!er
• The sugar leaving the centrifugals is hot at L> B =>> C and moist >.A
B .AJ moisture and as such it canKt be bagged for sale.
• There are two ways of sugar drying in practice
» Drying sugar in rotary drying
» Drying sugar is centrifugal machines
• 7f the two, drying sugar in centrifugal machines is considered
superior, since in the rotary dryers the crystals lose their moisture
by rubbing action against each other
• /urther, the sugar dust formed means loss of sugar and reuires
additional euipment to recover it
T!pes of 'r!ers
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T!pes of 'r!ers
There are three principle types of sugar dryers
/luidized &ed Dryers
Motating Drum Dryers
'luidi$ed(&ed )ryer$
• The sugar is distributed on the perforated plate. "ot air passes
through this plate and through the sugar layer
• The transmission of heat is very rapid, permitting a very brief time
in the dryer
• "owever the fluidization and the air flow involve abrasion of the
crystal
! Rotary )rum )ryer$
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!. Rotary()rum )ryer$
+t is the most widely used.
+t is cylindrical and set at a slope of A> to the horizontal, which
facilitates the movement of the sugar from end and end of the
drum.
The revolving motion of the drum causes to lift the sugar and fall
from one sloop to other through a countercurrent hot air flow and
reaches the discharge end of the drum.
The drum is often arranged to act as both dryer and cooler.
The cold air enters at the lower end and leaves near the middle of
the drum
Sie"ing and *rading of Sugars
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Sie"ing and *rading of Sugars
• The sugar obtained after drying and cooling consists of a mixture of
heterogeneous crystals and needs to be well sieved and graded
before it is marketed.
• The sieving is done through sifters which are of the following.
Motary Type
#agnetic or ;ibrating Type
a Rotar! T!pe
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a. Rotar! T!pe
• This type of screen is attached to a rigid cylindrical frame carried
on a rollers or control shaft
• The axis of the cylinder is usually inclined to the horizontal, so
that the material is carried forward while rolling over the screen
• usually each screen is bounded with several rings of plates having
different perforations arranged in order of sizes, the smallest being
in the beginning
• The whole arrangement is simple.
b #ibrating T!pe
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b. #ibrating T!pe
• The vibrating movement reduces chocking of screens and works
for a longer period without cleaning.
• creens of various mesh sizes are fixed in frames and arranged one
over the other in order to facilitate grading of sugars
• The frames are vibrated at a very high speed by means of an
eccentric having a small throw >.A B .> inch and are belt driven by
a motor
• The mechanism is placed under the upper part of the box free for
access to the screen
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