for inspection purposes only.appendix iii: certificates and process detail form.....24 opinions and...
TRANSCRIPT
Document No: SHGATL5080818 Licence Number: P0650-03 Visit No: 3 Licence Holder: Zinc Processors Ltd. Year: 2018 Facility Location: Drombana, Co.Limerick Office: Limerick Version No: 1
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Report Title Air Emissions Compliance Monitoring Emissions Report
Company address Air Scientific Ltd., Unit 5, Caherdavin Business Centre, Caherdavin,
Park, Ennis Road, Limerick V94 NT63.
Stack Emissions Testing Report Commissioned by Zinc Processors Limited Trading As Shannonside Galvanising
Facility Name Zinc Processors Limited Trading As Shannonside Galvanising
Contact Person Dermot O’ Brien
EPA Licence Number P0650-03
Licence Holder Zinc Processors Limited Trading As Shannonside Galvanising
Stack Reference Number A1-1 & A1-2
Dates of the Monitoring Campaign 08-08-2018
Job Reference Number SHGATL5080818
Report Written By Mr. Robert O’Brien
Report Approved by Mark McGarry
Stack Testing Team Mr. Robert O’Brien & Mr. Michéal Ryan
Report Date 18-09-2018
Report Type Test Report Compliance Monitoring
Version 1
Signature of Approver Operations Manager
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Contents
1.0 Executive Summary ................................................................................................................................................................................ 3 1.1 Overall aim of the monitoring campaign ................................................................................................................................................ 3 1.2 Summary of substances to be monitored at each emission point .......................................................................................................... 3 1.3 Special Requirements ............................................................................................................................................................................. 3 1.4 Summary of Results ................................................................................................................................................................................ 4 Emission Point Number: A1-1 ........................................................................................................................................................................... 4 Emission Point Number: A1-2 ........................................................................................................................................................................... 5 1.5 Operating Information ........................................................................................................................................................................... 6 Please reference Process Details as per Appendix III attached. ........................................................................................................................ 6 1.6 Monitoring Deviations ............................................................................................................................................................................ 6 1.7 Reference Documents ............................................................................................................................................................................ 6 1.8 Revision History ...................................................................................................................................................................................... 6 Part 2: Supporting Information ........................................................................................................................................................................ 7 Appendix I ......................................................................................................................................................................................................... 8 1.1 Monitoring Personnel ............................................................................................................................................................................. 8 1.2 Equipment Inventory .............................................................................................................................................................................. 9 Appendix II ...................................................................................................................................................................................................... 10 2.1 Stack Emission Point Reference: A1-1 .................................................................................................................................................. 10 2.1.1 Suitability of Sample Location: ........................................................................................................................................................ 10 2.1.2 Stack Diagram ................................................................................................................................................................................. 11 2.1.3 Stack Raw Data ............................................................................................................................................................................... 12 2.2 Stack Emission Point Reference: A1-2 .................................................................................................................................................. 19 2.2.1 Suitability of Sample Location: ........................................................................................................................................................ 19 2.2.2 Stack Diagram ................................................................................................................................................................................. 20 2.2.3 Stack Raw Data ............................................................................................................................................................................... 21 Appendix III: Certificates and Process Detail Form .................................................................................................................................... 24
Opinions and interpretations expressed herein will be outside the scope of Air Scientific Limited INAB accreditation. This test report shall not be reproduced, without the written approval of Air Scientific Limited.
All sampling and reporting is completed in accordance with Environmental Protection Agency Air Guidance Note 2 requirements.
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1.0 Executive Summary
1.1 Overall aim of the monitoring campaign
The aim of the monitoring campaign was to demonstrate compliance with a set of emission limit values as specified
in the site licence.
1.2 Summary of substances to be monitored at each emission point
Stack Name: A1-1
Total Particulate Matter
Chloride (as HCl)
Ammonium Chloride
Metals (Lead, Cadmium, Zinc)
Volumetric Flow Rate (Ref)
Stack Name: A1-2
Total Particulate Matter
Total Gaseous Organic Compounds
Volumetric Flow Rate (Ref)
1.3 Special Requirements
There were no special requirements
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1.4 Summary of Results
Emission Point Number: A1-1
Parameter Method Units Result MU +/- Limit O2 Ref.
(%)
Moisture
Ref.(%) Compliant Blanks Date Time on Time off
Accreditation
Sampling Analysis
HCL EN 1911 mg.m-3 <0.191 0.009 10 N/a N/a Yes 0.1 08/08/2018 09:45 10:15 Yes Yes
NH4CL EN 14791 mg.m-3 <0.917 0.045 10 N/a N/a Yes 0.2 08/08/2018 09:45 10:15 No No
Lead EN 14385 mg.m-3 <0.06569 0.00231 2 N/a N/a Yes 0.00104 08/08/2018 10:24 10:56 Yes Yes
Cadmium EN 14385 mg.m-3 <0.00126 0.00004 0.01 N/a N/a Yes 0.00118 08/08/2018 10:24 10:56 Yes Yes
Zinc EN 14385 mg.m-3 <4.01578 0.14149 5 N/a N/a Yes 0.04216 08/08/2018 10:24 10:56 No No
Particulate Matter EN 13284-1 mg.m-3 5.41 0.58 5 N/a N/a No 0.61 08/08/2018 11:31 12:10 Yes Yes
Volumetric Flow Rate (Ref) EN 16911 m3.h-1 25,172 1,081 25,500 N/a N/a Yes N/a 08/08/2018 11:31 12:10 Yes N/a
Note 1: All results are normalised to standard temperature and pressure (0OC and 101.3kPa)
Note 2: All results are reported in the format as defined by the EPA in guidance note AG2:2017.
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Document No: SHGATL5080818 Licence Number: P0650-03 Visit No: 3 Licence Holder: Zinc Processors Ltd. Year: 2018 Facility Location: Drombana, Co.Limerick Office: Limerick Version No: 1
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Emission Point Number: A1-2
Parameter Method Units Result MU +/- Limit O2 Ref.
(%)
Moisture
Ref (%) Compliant Blanks Date Time on Time off
Accreditation
Sampling Analysis
Total Organic Compounds EN 12619 mg.m-3 30.8 1.12 150 N/a N/a Yes N/a 08/08/2018 14:40 15:09 No N/a
Particulate Matter EN 13284-1 mg.m-3 1.87 0.71 5 N/a N/a Yes 0.79 08/08/2018 14:55 15:30 Yes Yes
Volumetric Flow Rate (Ref) EN 16911 m3.h-1 13,958 985 18,800 N/a N/a Yes N/a 08/08/2018 14:55 15:30 Yes N/a
Note 1: All results are normalised to standard temperature and pressure (0OC and 101.3kPa)
Note 2: All results are reported in the format as defined by the EPA in guidance note AG2:2017.
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1.5 Operating Information
Please reference Process Details as per Appendix III attached.
1.6 Monitoring Deviations
Stack Name: A1-1
Parameter Deviation
Total Particulate Matter Blank > 10% of ELV due to low ELV.
Hydrogen Chloride (as HCl) None
Metals (Lead, Cadmium, Zinc) None
Ammonium Chloride None
Volumetric Flow Rate (Ref) EN 16911 - in accordance with MID 16911-1
Stack Name: A1-2
Parameter Deviation
Total Particulate Matter Straight length before sample point <5 hydraulic diameters. Straight length after sample point <5 hydraulic diameters. Blank > 10% of ELV due to low ELV.
Total Gaseous Organic Compounds None
Volumetric Flow Rate (Ref) EN 16911 - in accordance with MID 16911-1. Straight length before sample point <5 hydraulic diameters. Straight length after sample point <5 hydraulic diameters
1.7 Reference Documents
Risk Assessment (RA) SOP 1011
Site Review (SR) SOP 1015
Site Specific Protocol (SSP) SOP 1015
1.8 Revision History
Revision Number Changes to the report
1 Original version of the report
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EPA Export 27-11-2018:03:52:32
Document No: SHGATL5080818 Licence Number: P0650-03 Visit No: 3 Licence Holder: Zinc Processors Ltd. Year: 2018 Facility Location: Drombana, Co.Limerick Office: Limerick Version No: 1
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Part 2: Supporting Information
Report Title Air Emissions Compliance Monitoring Emissions Report
Company address Air Scientific Ltd., Unit 5, Caherdavin Business Centre, Caherdavin,
Park, Ennis Road, Limerick V94 NT63.
Stack Emissions Testing Report Commissioned by Zinc Processors Limited Trading As Shannonside Galvanising
Facility Name Zinc Processors Limited Trading As Shannonside Galvanising
Contact Person Dermot O’ Brien
EPA Licence Number P0650-03
Licence Holder Zinc Processors Limited Trading As Shannonside Galvanising
Stack Reference Number A1-1 & A1-2
Dates of the Monitoring Campaign 08-08-2018
Job Reference Number SHGATL5080818
Report Written By Mr. Robert O’Brien
Report Approved by Mark McGarry
Stack Testing Team Mr. Robert O’Brien & Mr. Michéal Ryan
Report Date 18-09-2018
Report Type Test Report Compliance Monitoring
Version 1
Signature of Approver Operations Manager
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Appendix I
1.1 Monitoring Personnel
Team Leader Name Robbie O Brien
System approval ASL Team Leader Approved
Technician Name Micheal Ryan
System approval ASL Technician Approved
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1.2 Equipment Inventory
ID Item of Equipment Used ID Item of Equipment Used ID Item of Equipment Used
ASLLK12EQ500 Pump ASLLK12EQ525 Horiba (PG-250) X ASLLK13EQ501 Vernier Calipers
ASLLK12EQ531 Pump ASLLK14EQ501 Horiba-PG 350 ASLLK14EQ503 Vernier Calipers
ASLLK12EQ532 Pump ASLLK14EQ512 Horiba PG250Y ASLLK14EQ507 Vernier Calipers
ASLLK12EQ533 Pump ASLLK16EQ508 Horiba- PG250z ASLLK17EQ533 Vernier Calipers
ASLLK12EQ534 Pump ASLLK17EQ515 Horiba 350 ASLLK18EQ506 Vernier Calipers
ASLLK12EQ535 Pump
ASLLK12EQ536 Pump
ASLLK12EQ537 Pump ASLLK12EQ526 Chiller ASLLK13EQ503 1kg weight
ASLLK12EQ538 Pump ASLLK14EQ513 Chiller ASLLK13EQ508 500g Hafner weight
ASLLK12EQ539 Pump ASLLK16EQ509 Chiller ASLLK13EQ509 500g Hafner weight
ASLLK12EQ540 Pump ASLLK18EQ505 Chiller ASLLK15EQ512 1kg weight
ASLLK12EQ541 Pump ASLLK16EQ511 1kg weight
ASLLK12EQ542 Pump ASLLK16EQ512 500g weight
ASLLK12EQ543 Pump ASLLK14EQ518 Velocity Meter ASLLK17EQ529 500g weight
ASLLK13EQ513 Pump ASLLK16EQ501 Velocity Meter ASLLK17EQ530 1kg weight
ASLLK13EQ514 Pump ASLLK17EQ508 Velocity Meter
ASLLK16EQ518 Pump ASLLK17EQ514 Velocity Meter
ASLLK16EQ519 Pump ASLLK18EQ504 Velocity Meter ASLLK13EQ504 G4
ASLLK17EQ509 Pump ASLLK13EQ515 G4
ASLLK17EQ510 Pump ASLLK15EQ501 G4
ASLLK17EQ525 Pump ASLLK14EQ500 FID ASLLK17EQ534 ST5
ASLLK17EQ526 Pump ASLLK16EQ502 FID ASLLK18EQ503 ST5
ASLLK17EQ522 Pump ASLLK17EQ517 FID
ASLLK17EQ523 Pump ASLLK17EQ535 Signal Cutter
ASLLK17EQ524 Pump ASLLK14EQ510 Digital Protractor
ASLLK14EQ511 Digital Protractor
ASLLK13EQ512 PCDD thermometer ASLLK15EQ505 Digital Protractor
ASLLK12EQ529 Calibrator ASLLK16EQ507 Digital Protractor
ASLLK14EQ502 Calibrator ASLLK17EQ528 Digital Protractor
ASLLK17EQ532 MF Meter ASLLK16EQ510 Measuring Tape ASLLK18EQ507 Digital Protractor
ASLLK17EQ540 MF Meter ASLLK16EQ513 Measuring Tape
ASLLK17EQ541 MF Meter ASLLK16EQ514 Measuring Tape
ASLLK17EQ542 MF Meter ASLLK17EQ527 Measuring tape ASLLK12EQ522 Balance
ASLLK18EQ508 Measuring tape ASLLK12EQ544 Balance
ASLLK15EQ509 Balance
ASLLK12EQ507 Heated Line ASLLK15EQ510 Balance
ASLLK12EQ527 Heated Line ASLLK16EQ515 Thermocouple K type ASLLK17EQ537 Balance
ASLLK14EQ509 Heated Line ASLLK16EQ516 Thermocouple K type ASLLK17EQ538 Balance
ASLLK14EQ514 Heated Line ASLLK17EQ531 K type Thermocouple
ASLLK17EQ502 Heated Line ASLLK18EQ500 K type Thermocouple
ASLLK17EQ503 Heated Line ASLLK18EQ501 K type Thermocouple
ASLLK17EQ539 Heated Line ASLLK18EQ502 K type Thermocouple
ASLLK12EQ518 S type Pitot Tube ASLLK17EQ518 Stopwatch
ASLLK12EQ520 L Type Pitot tube ASLLK17EQ519 Stopwatch
ASLLK13EQ506 S type Pitot Tube ASLLK17EQ520 Stopwatch
ASLLK14EQ506 Pitot + thermocouple ASLLK17EQ521 Stopwatch
ASLLK16EQ506 S type Pitot Tube ASLLK18EQ509 Stopwatch
ASLLK16EQ517 S type Pitot Tube
ASLLK17EQ536 S type Pitot
ASLLK17EQ507 1 m S type & K type
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Appendix II
2.1 Stack Emission Point Reference: A1-1
2.1.1 Suitability of Sample Location:
General Information A1-1
Permanent/Temporary Permanent
Inside/ Outside Outside
Platform Details
Irish EPA Technical Guidance Note AG1 / BS EN 15259 Platform Requirements
Value Comment
Sufficient Working area to manipulate probe and measuring instruments
Yes -
Platform has 2 handrails (approx. 0.5m & 1.0 m high) Yes -
Platform has vertical base boards (approx. 0.25 m high) Yes -
Platform has chains / self-closing gates at top of ladders Yes -
There are no obstructions present which hamper insertion of sampling equipment
Yes -
Safe Access Available Yes -
Easy Access Available Yes -
Sampling Location / Platform Improvement Recommendations
None
EN 15259 Homogeneity Test Requirements
1
Select Option: 1: There is no requirement to perform a BSEN15259 Homogeneity Test on this stack 2: Test results were obtained from previous Homogeneity test carried out by ASL 3: Test results were obtained from previous Homogeneity test carried out by Alternative contractor 4: Homogeneity Test is required on this stack and the client has been informed of this requirement
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2.1.2 Stack Diagram
Figure 1: A1-1
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2.1.3 Stack Raw Data
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Title: Determination of Metals
Method: EN 14385
Client: Shannonside
Test Date: 08/08/2018 Temperature at Pump 22.7 Deg C
Test Time On: 10:24:15 Pressure at Pump 86.714 kPa
Test Time Off: 10:55 Air Volume at Pump 0.7571 m3
Laboratory Used: CLS Humidity at Pumps 0 %
Stack Name A1-1
Filter I.D. Y-362 Flow Uncertainty 1124 m3/hr
Stack Flow Rate 26178 m3.hr-1 Flow Uncertainty 4 %
Dry Volume of Air Sampled Metals 0.5989 Nm3
Dry Volume of Air Sampled Mercury
Moisture Content 0.00 %
Wet Volume of Air Sampled Metals 0.5989 m3
Wet Volume of Air Sampled Mercury 0 m3
Emission Limit Value 5 mg.m-3
Leak Check Results Result % Leak
Before Blank 0.09 cc/min 0.4
After Blank 0.09 cc/min 0.4
Before Sample 1 0.09 cc/min 0.4
After Sample 1 0.09 cc/min 0.4
Average Flow Rate 21 cc/min 0.4
Standard Maximum 0.42 cc/min 2%
Back Pressure 69 bar or kPa
Standard Criteria to be Met Result Standard Requirement
Angle of Flow Pass <15 Degrees Probe material Titanium
Negative Flow in the Stack Pass None Filter housing Titanium
Pitot Pressure Difference Pass >5Pa Positioning of filter Out Stack
Ratio of Flow Measurement Pass <3:1 Filter Size & Material 47mm Quartz
Stagnation Check Pass <10 Pa
Pitot Tube Leak Check Result
Positive Pressure Pass -
Negative Pressure Pass -
Number of Ports 2 2
Straight length before sample point Pass > 5 Hydraulic Diameters
Straight length after sample point Pass > 5 HD from fan or bend / >2 from stack exit
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Sample Calculations
Filter Imp 1 & 2 Imp 3 Total Metal
ug / filter ug/L ug/L ug
Cadmium 0.5 0.5 0.5 0.8
Lead 38 3.2 0.3 39.3
Zinc 2300 250 25 2405.1
Run 1
Impinger 1 & 2 Total Volume (Incl Rinse) 410 mls
Impinger 3 Total Volume (Incl Rinse) 102 mls
Concentration Calculation
mg.m-3 Uncertainty
Cadmium 0.00126 0.000044
Lead 0.06569 0.002314
Zinc 4.01578 0.141485
Total Metals 4.08273 0.143844
Total Cd 0.00126 0.000044
Remaining Metals 4.08147 0.143800
Blank Calculations
Filter Impingers Total Metals Concentration
ug / filter ug/L ug mg.m-3
Cadmium 0.5 0.5 0.705 0.00118
Lead 0.5 0.3 0.623 0.00104
Zinc 15 25 25.250 0.04216
% of ELV
Total Metals 0.0444 0.8876
Blank < 10% of the Emission Limit Values Yes Yes / No
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PITOT DATA SPECIFICATION
Name p0.83
Velocity [m/sec] 5 0.83
Velocity [m/sec] 10 0.83
Velocity [m/sec] 20 0.83
Velocity [m/sec] 30 0.83
Velocity [m/sec] 40 0.83
DUCT AND GAS SPECIFICATION
Name SHAN A1-1
Section Circular
Diameter [m] 0.74
Area [m2] 0.43
Port B [#] 2
Points P [#] 4
Density ρn [kg/m3] 1.286
Carbon dioxide CO2 [%] 0
Oxygen O2 [%] 20.9
Water vapor ratio rw [0;1] 0.01
Nozzle nz [mm] 5
Turbolence factor ft [sec] 9
DUCT FLOW RATE
Dry actual QVa [m3/h] 29743
Moist actual Q'Va [m3/h] 30044
Moist standard [Tnorm Pnorm] Q'Vn [m3/h] 26178
Dry standard [Tnorm Pnorm] QVn [m3/h] 25916
AVERAGE VALUES
Total Points [#] 2
Velocity v'a [m/sec] 19.405
Stack temperature ta [°C] 37.794
Stack Static Pressure Pastatic [kPa] 100.459
Isokinetic Deviation DI [%] 1
Velocity at nozzle v'N [m/sec] 19.614
Probe temperature tprobe [°C] 124.255
Box temperature tbox [°C] 115.566
Stack Differential Pitot Pressure dPpitot [Pa] 326.544
Ambient Pressure Pamb [kPa] 100.29
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Title: Determination of Total Particulates
Method: EN 13284-1
Client: Shannonside Test Date: 08/08/2018 Temperature at Pump 20.611 Deg C
Test Time 11:31 Pressure at Pump 86.489 kPa
Laboratory Used: CLS Air Volume at Pump 0.7215 m3
Stack Name A1-1 Humidity at Pumps 0 %
Run I.D. 2 Filter Weight 2.8 mg
Filter I.D. 8-131 Front End Weight 0.3 mg
Moisture Content 0.00 % Stack Flow Rate 25172 Nm3/hr Flow Uncertainty 1081 m3/hr
Volume of Air Sampled 0.573 Nm3 Flow Uncertainty 4.3 %
Leak Check Results Result % Leak
Before Blank 0.19 l/min 0.9
After Blank 0.19 l/min 0.9
Before Sample 1 0 l/min 0.0
After Sample 1 0 l/min 0.0
Average Flow Rate 21 l/min 0.9
Standard Maximum 0.42 l/min 2%
Back Pressure 69 kPa
Standard Criteria to be Met Result Std. Requirement
Angle of Flow Pass <15 Degrees Probe material Stainless Steel
Negative Flow in the Stack Pass None Filter housing Stainless Steel
Pitot Pressure Difference Pass >5Pa Positioning of filter In Stack
Ratio of Flow Measurement Pass <3:1 Filter Size & Material 47mm Quartz
Stagnation Test Pass <10Pa
Pitot Tube Leak Check Result
Positive Pressure Pass -
Negative Pressure Pass -
Number of Ports 2 2
Straight length before sample point Pass > 5 Hydraulic Diameters
Straight length after sample point Pass > 5 Hydraulic Diameters/ >2 from Bend
Sample Calculations
Blank (Filter and Front Wash Combined) 0.35 mg
Sample 1 (Filter and Front Combined) 3.1 mg
Volume of Air Sampled 0.573 Nm3
Blank Result 0.61 mg/Nm3
Sample Result 5.41 mg/Nm3
Uncertainty of Measurement 0.58 mg/Nm3
Emission Limit Value 5 mg/Nm3 Blank as Percentage of ELV 12.2 % Standard Requirement <10% ELV
Isokinetic Criterion Compliance
Isokinetic Variation 0.5 %
Allowable Isokinetic Range I -5 to + 15% %
Isokinetic Acceptable Yes -
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PITOT DATA SPECIFICATION
Name p0.83
Velocity [m/sec] 5 0.83
Velocity [m/sec] 10 0.83
Velocity [m/sec] 20 0.83
Velocity [m/sec] 30 0.83
Velocity [m/sec] 40 0.83
DUCT AND GAS SPECIFICATION
Name SHAN A1-1
Section Circular
Diameter [m] 0.74
Area [m2] 0.43
Port B [#] 2
Points P [#] 4
Density ρn [kg/m3] 1.286
Carbon dioxide CO2 [%] 0
Oxygen O2 [%] 20.9
Water vapor ratio rw [0;1] 0.01
Nozzle nz [mm] 5
Turbolence factor ft [sec] 9
DUCT FLOW RATE
Dry actual QVa [m3/h] 27494
Moist actual Q'Va [m3/h] 27772
Moist standard [Tnorm Pnorm] Q'Vn [m3/h] 25172
Dry standard [Tnorm Pnorm] QVn [m3/h] 24920
AVERAGE VALUES
Total Points [#] 2
Velocity v'a [m/sec] 17.937
Stack temperature ta [°C] 25.895
Stack Static Pressure Pastatic [kPa] 100.474
Isokinetic Deviation DI [%] 0.5
Velocity at nozzle v'N [m/sec] 18.039
Probe temperature tprobe [°C] 124.379
Box temperature tbox [°C] 89.513
Stack Differential Pitot Pressure dPpitot [Pa] 282.834
Ambient Pressure Pamb [kPa] 100.29
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EPA Export 27-11-2018:03:52:33
Document No: SHGATL5080818 Licence Number: P0650-03 Visit No: 3 Licence Holder: Zinc Processors Ltd. Year: 2018 Facility Location: Drombana, Co.Limerick Office: Limerick Version No: 1
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Title: Determination of Inorganic Compounds
Method: EN1911 EN14791
Test Date: 07/08/2018
Test Time Started: 09:45 09:45
Test Time Finished: 10:15 10:15
Laboratory Used: CLS
Stack Reference: A1-1
Leak Check Results HCL NH4CL
Prior to test: 0 0 l/min
Post Test: 0 0 l/min
Sample Volume Flow Rate: 2.09 2.09 l/min
Standard Requirement: <2 <2 %
Test Result: 0.0 0.0 %
Test Status Pass / Fail Pass / Fail
Reference Details
Stack Moisture Content 0 %
Calibration Details HCL NH4CL
Pump Number: ASLLK17EQ525 ASLLK17EQ524
Calibration Unit: ASLLK17EQ542 ASLLK17EQ542
Calibration Rate Before Test: 2.1 2.1 l/min
Calibration Rate After Test: 2.1 2.1 l/min
Average sample Volume: 2.1 2.1 l/min
Sample Test Time: 30 30 minutes
Pump Gas Temperature: 21 21 OC
Pump Sample Pressure: 101.3 101.3 kPa
Actual Sample Volume: 0.063 0.063 m3
Normalised Gas Volume: 0.058 0.058 Nm3
Normalised Wet Gas Volume: 0.058 0.058 Nm3
Sample Details HCL NH4CL
Impinger Solution DI Water 0.1N H2SO4
Solution ID Number: Run 1 Run 1
Blank Identification Number: Run 1 Run 1
Impinger Material PTFE PTFE
Breakthrough Occurred No No
Transport Temp meets Standard Yes Yes
Analysed Within Specified Timeframe Yes Yes
Transport Container Airtight Yes Yes
Exposed to Sunlight No No
Calculations HCL NH4CL
Laboratory Result Imp 1 / 2 0.06 0.4 ug/ml
Laboratory Result Imp Final 0.05 0.1 ug/ml
Impinger Final Volume Imp 1 / 2 122 115 ml
Impinger Final Volume Imp Final 70 74 ml
Combined Concentration 0.0 0.1 mg
Factor 1.028 1
Concentration 0.0 0.1 mg
Air Sample Volume 0.058 0.058 Nm3
Emissions Concentration 0.191 0.917 mg.m-3
Uncertainty 0.009 0.045 mg.m-3
Licence Limits 10 10 mg.m-3
Blank Calculation HCL NH4CL
Laboratory Impinger / Rinse Result 0.05 0.1 ug/ml
Factor 1.028 1 -
Blank Concentration 0.1 0.2 mg.m-3
% of Licence Limit 1.1 2.0 %
Field Blank <10% ELV Yes Yes mg.m-3
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2.2 Stack Emission Point Reference: A1-2
2.2.1 Suitability of Sample Location:
General Information A1-2
Permanent/Temporary Permanent
Inside/ Outside Outside
Platform Details
Irish EPA Technical Guidance Note AG1 / BS EN 15259 Platform Requirements
Value Comment
Sufficient Working area to manipulate probe and measuring instruments
Yes -
Platform has 2 handrails (approx. 0.5m & 1.0 m high) Yes -
Platform has vertical base boards (approx. 0.25 m high) Yes -
Platform has chains / self-closing gates at top of ladders Yes -
There are no obstructions present which hamper insertion of sampling equipment
Yes -
Safe Access Available Yes -
Easy Access Available Yes -
Sampling Location / Platform Improvement Recommendations
None
EN 15259 Homogeneity Test Requirements
1.
Select Option: 1: There is no requirement to perform a BSEN15259 Homogeneity Test on this stack 2: Test results were obtained from previous Homogeneity test carried out by ASL 3: Test results were obtained from previous Homogeneity test carried out by Alternative contractor 4: Homogeneity Test is required on this stack and the client has been informed of this requirement
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2.2.2 Stack Diagram
Figure 2: A1-2
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2.2.3 Stack Raw Data
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Title: Determination of Total Particulates
Method: EN 13284-1
Client: Shannonside Test Date: 08/08/2018 Temperature at Pump 16.889 Deg C
Test Time 14:55 Pressure at Pump 91.796 kPa
Laboratory Used: CLS Air Volume at Pump 0.5188 m3
Stack Name A1-2 Humidity at Pumps 0 %
Run I.D. 1 Filter Weight 0.53 mg
Filter I.D. 8-122 Front End Weight 0.3 mg
Moisture Content 0.00 % Stack Flow Rate 13958 Nm3/hr Flow Uncertainty 985 m3/hr
Volume of Air Sampled 0.4428 Nm3 Flow Uncertainty 7.1 %
Leak Check Results Result % Leak
Before Blank 0 l/min 0.0
After Blank 0 l/min 0.0
Before Sample 1 0 l/min 0.0
After Sample 1 0 l/min 0.0
Average Flow Rate 14.765 l/min 0.0
Standard Maximum 0.2953 l/min 2%
Back Pressure 69 kPa
Standard Criteria to be Met Result Std. Requirement
Angle of Flow Pass <15 Degrees Probe material Stainless Steel
Negative Flow in the Stack Pass None Filter housing Stainless Steel
Pitot Pressure Difference Pass >5Pa Positioning of filter In Stack
Ratio of Flow Measurement Pass <3:1 Filter Size & Material 47mm Quartz
Stagnation Test Pass <10Pa
Pitot Tube Leak Check Result
Positive Pressure Pass -
Negative Pressure Pass -
Number of Ports 2 2
Straight length before sample point No > 5 Hydraulic Diameters
Straight length after sample point No > 5 Hydraulic Diameters/ >2 from Bend
Sample Calculations
Blank (Filter and Front Wash Combined) 0.35 mg
Sample 1 (Filter and Front Combined) 0.83 mg
Volume of Air Sampled 0.4428 Nm3
Blank Result 0.79 mg/Nm3
Sample Result 1.87 mg/Nm3
Uncertainty of Measurement 0.71 mg/Nm3
Emission Limit Value 5 mg/Nm3 Blank as Percentage of ELV 15.8 % Standard Requirement <10% ELV
Isokinetic Criterion Compliance
Isokinetic Variation 1.7 %
Allowable Isokinetic Range I -5 to + 15% %
Isokinetic Acceptable Yes -
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Name p0.83
Velocity [m/sec] 5 0.83
Velocity [m/sec] 10 0.83
Velocity [m/sec] 20 0.83
Velocity [m/sec] 30 0.83
Velocity [m/sec] 40 0.83
DUCT AND GAS SPECIFICATION
Name SHAN A1-2
Section Rectangular
Size [m]x[m] 0.700 x 1.140
Area [m2] 0.797
Port B [#] 2
Points P [#] 4
Density ρn [kg/m3] 1.286
Carbon dioxide CO2 [%] 0
Oxygen O2 [%] 20.9
Water vapor ratio rw [0;1] 0.01
Nozzle nz [mm] 8
Turbolence factor ft [sec] 9
DUCT FLOW RATE
Dry actual QVa [m3/h] 14942
Moist actual Q'Va [m3/h] 15093
Moist standard [Tnorm Pnorm] Q'Vn [m3/h] 13958
Dry standard [Tnorm Pnorm] QVn [m3/h] 13818
AVERAGE VALUES
Total Points [#] 2
Velocity v'a [m/sec] 5.254
Stack temperature ta [°C] 19.99
Stack Static Pressure Pastatic [kPa] 100.551
Isokinetic Deviation DI [%] 1.7
Velocity at nozzle v'N [m/sec] 5.346
Probe temperature tprobe [°C] 19.27
Box temperature tbox [°C] 19.547
Stack Differential Pitot Pressure dPpitot [Pa] 24.898
Ambient Pressure Pamb [kPa] 100.574
SAMPLED VOLUMES
Elapsed time et [hh:mm:ss] 00:30:00
Total encoder impulses [#] 43236
Standard Volume [Tnorm Pnorm] Vgn [m3] 0.4428
Moist Volume at stack conditions V'ga [m3] 0.4824
Volume at dgm conditions Vdgm [m3] 0.5188
Gas meter temperature tgm [°C] 16.889
Gas Meter Pressure Pdgm [kPa] 91.796
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Appendix III: Certificates and Process Detail Form
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