gc accessories - phenomenex · detector noise, ghost peaks and even column damage. oxygen is...

326 Phenomenex

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GC ACCESSORIES

CAPILLARY uNIONS AND SPLITTERS• Connect fused silica capillary tubing of the same or different diameter, from 0.25 to 0.53 mm ID

• Patented laser-formed Linear Taper™

• Provides leak-free seal without tools, glue or fittings

• Stays sealed even at high temperatures and pressures

• Laser-cut smooth ends prevent column damage during insertion

POLYIMIDE RESIN• Permanently connects unions and splitters to capillary tubing

• Prevents connections from dislodging due to vibration or shock

• Stable to 350 °C

ORDERING INFORMATION

Capillary Unions and SplittersPart no. Description Unit Price

AG0-4716 I Universal Capillary Column Union, Borosilicate I 5/pk I AG0-4717 Universal Capillary Column Y-connector, Borosilicate ea

Polyimide ResinPart no. Description Unit Price

AG0-5722 I Polyimide Resin, 0.5 mL I ea I

Ceramic Scoring WafersPart no. Description Unit Price

AG0-4718 I Ceramic Scoring Wafer I 2/pk I

Use the Union for:• Connecting a guard column to an analytical column• Connecting columns of different selectivities• Connecting transfer lines to e.g., mass spec• Repairing a broken column

Use the Y-connector (splitter) for:• Splitting a sample onto two columns (perform confirmational analysis in a single injection)• Splitting the column eluent to two detectors



See p. 25 for GC Retention Gaps and Guard Column Kits.

CERAMIC SCORING WAFERS• High quality ceramic cutting tool for fused silica capillary columns

327Phenomenex

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GC ACCESSORIES

GC FITTINGS• For capillary column connections to both Agilent injectors and GC detectors (not MS)

• Interchangeable with original Agilent nuts

• Standard length nut uses short Agilent ferrules (1.65 mm)

• Extended length (deep well) nut uses standard ferrules (2.4 mm)

GC Fittings Similar to Part no. Description Mfr. no.* Unit Price

AG0-5152 I Agilent GC Standard Capillary Nut, I 5181-8830 I 2/pk I 1/16” Hex stainless steel, uses short Agilent ferrules (1.65 mm length) AG0-5153 Agilent GC Deep Well Capillary Nut, 5020-8292 2/pk 1/16” Hex stainless steel, uses standard ferrules (2.4 mm length)


Selection Guide:• Connecting similar sized columns or tubing: Select the union with inside diameter large enough to accommodate the tubing in question.• Connecting dissimilar sized columns or tubing: Select the union with inside diameter large enough to accommodate the smaller of the two sizes.

Applications:• Connecting a guard column to an analytical column• Connecting columns of different selectivities• Connecting transfer lines to, e.g., mass spec• Repairing a broken column

CAPILLARY COLuMN MINI uNIONS• High-precision unions for capillary GC columns

• Connect capillary columns of same or dissimilar sizes

• Connect high temperature polyimide-coated and metal capillaries, which is not possible with glass unions

• Inert and precise glass-lined bore

• Low dead volume

Capillary Column Mini UnionsPart no. Description Unit Price

AG0-5160 I GC Mini-Unions, GLT/SS, 0.4 mm ID, fits I ea I Col 1 (0.1-0.25 mm), Col 2 (0.1-0.53 mm) AG0-5161 GC Mini-Unions, GLT/SS, 0.5 mm ID, fits ea Col 1 (0.32 mm), Col 2 (0.32-0.53 mm) AG0-5162 GC Mini-Unions, GLT/SS, 0.8 mm ID, fits ea Col 1 (0.45 mm), Col 2 (0.45-0.53 mm)Replacement Ferrules AG0-7033 Ferrule for 0.4 mm ID, GC Mini-Union, 10/pk using 0.1 to 0.25 mm ID capillary tubingAG0-7034 Ferrule for 0.5 mm ID, GC Mini-Union, 10/pk using 0.32 mm ID capillary tubing AG0-7035 Ferrule for 0.8 mm ID, GC Mini-Union, 10/pk using 0.45-0.53 mm ID capillary tubing


See p. 372 for GC Reference Books and Software.

* Similar to but not always an exact equivalent to the original manufacturer's product.

328 Phenomenex

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GC ACCESSORIES

LONG FERRuLES

Graphite Ferrules• High-purity graphite significantly reduces ferrule bleed

• Special construction minimizes "flaking"

• Stable to 450 °C - excellent for high temperature use

• Not for use with GC/MS transfer lines

Vespel/Graphite Ferrules (60/40 %)• High quality, improved universal design

• use for most applications, up to 400 °C

• Seal easily with minimum torque

• Highly reusable (save money)


Graphite Ferrules, Rated to 450 °CPart no. Description Unit Price

0.4 mm Ferrule ID I I AG0-4698 Graphite Ferrule 1/16" to 0.4 mm 10/pk AG0-4699 Graphite Ferrule 1/16" to 0.4 mm 50/pk 0.5 mm Ferrule ID AG0-4701 Graphite Ferrule 1/16" to 0.5 mm 10/pk AG0-4702 Graphite Ferrule 1/16" to 0.5 mm 50/pk 0.8 mm Ferrule ID AG0-4704 Graphite Ferrule 1/16" to 0.8 mm 10/pk AG0-4705 Graphite Ferrule 1/16" to 0.8 mm 50/pk

Vespel/Graphite Ferrules (60/40 %), Rated to 400 °CPart no. Description Unit Price

0.4 mm Ferrule ID I I AG0-4707 Vespel/Graphite Ferrule 1/16" to 0.4 mm 10/pkAG0-4708 Vespel/Graphite Ferrule 1/16" to 0.4 mm 50/pk0.5 mm Ferrule ID AG0-4710 Vespel/Graphite Ferrule 1/16" to 0.5 mm 10/pkAG0-4711 Vespel/Graphite Ferrule 1/16" to 0.5 mm 50/pk0.8 mm Ferrule ID AG0-4713 Vespel/Graphite Ferrule 1/16" to 0.8 mm 10/pkAG0-4714 Vespel/Graphite Ferrule 1/16" to 0.8 mm 50/pk


All Vespel containing ferrules should be pre-shrunk in an oven at 250 °C for at least 4 hours prior to use.

SHORT FERRuLES

(For Agilent/HP 5890 & 6890 GC’s)


Vespel/Graphite (85/15 %) Short Ferrules (not for GC/MS), Rated to 350 °C Similar toPart no. Description Mfr. no.* Unit PriceAG0-7318 l Vespel/Graphite (85/15 %) l 5181-3323 l 10/pk l Short Ferrules, 1/16" to 0.4 mm (for 0.10 to 0.25 mm ID columns) AG0-7319 Vespel/Graphite (85/15 %) 5062-3514 10/pk Short Ferrules, 1/16" to 0.5 mm (for 0.32 ID columns) AG0-7320 Vespel/Graphite (85/15 %) 5062-3512 10/pk Short Ferrules, 1/16" to 0.8 mm (for 0.45 to 0.53 mm ID columns)

Vespel/Graphite (85/15 %) GC/MS Compatible, Rated to 350 °C Similar to Part no. Description Mfr. no.* Unit PriceAG0-7321 l Vespel/Graphite (85/15 %) GC/MS l 5181-3322 l 10/pk l Short Ferrules, 1/16" to 0.4 mm (for 0.10 to 0.25 mm ID columns) AG0-7322 Vespel/Graphite (85/15 %) GC/MS 5062-3513 10/pk Short Ferrules, 1/16" to 0.5 mm (for 0.32 ID columns) AG0-7323 Vespel/Graphite (85/15 %) GC/MS 5062-3511 10/pk Short Ferrules, 1/16" to 0.8 mm (for 0.45 to 0.53 mm ID columns)


Select the correct ferrule for your capillary column as follows:

GC Capillary ID (mm) Ferrule Hole Size (mm)

0.10 to 0.25 0.40.28 to 0.35 0.50.45 to 0.53 0.8

NOTE: Other types of ferrules are available upon request, please call.

*Similar to but not always an exact equivalent to the original manufacturer’s product.

329Phenomenex

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GC ACCESSORIES

Injection Port Cleaning kit• Includes 4 stainless steel brush sizes 1/8, 3/16,

1/4 and 3/8"

• Also includes a scraper-pick combo for hard septum residues and septum removal

• Easy to use with twisted wire handles and a convenient wire ring to keep parts together

FERRuLE REMOVER TOOL kIT• Simple and convenient tools effectively remove stuck ferrules from fittings• Special spiral-cut rachet design slides in and grabs ferrule tight• Includes two tools for removing capillary ferrules from 0.4 to 0.8 mm ID


Ferrule Remover Tool KitPart no. Description Unit Price

AD0-4725 I GC Ferrule Remover Tool Kit I ea I

Injection Port Cleaning KitPart no. Description Unit Price

AD0-4724 I GC Injection Port Cleaning Kit I ea I


CLEANING kITS

Flame Detector Jet Cleaning kit• For routine maintenance of Flame Ionization Detectors• Includes: • Set of 3 jet reamers 0.008, 0.08 and 0.02" • 1 Stainless steel and 1 brass brush • 1 Dual-ended pin vise for holding reamers and brushes• use after the flame jet has been taken apart or while installed in the GC

Flame Detector Jet Cleaning KitPart no. Description Unit Price

AD0-4723 I GC Flame Detector Jet Cleaning Kit I ea I


FID Flame Jet for Agilent Technologies (HP) Similar to Part no. Description Mfr. no.* Unit Price

AD0-7324 I Flame Jet Kit I 19244-80560 I ea I

for Agilent/HP 5890, 5710/30/90A and 5830/40A (65 mm Jet)AD0-7331 Flame Jet Kit G1531-80560 ea for Agilent/HP 6890/6850 (42.5 mm Jet)AGO-7325 Replacement Ferrules 10/pk


FID FLAME JET kITS


330 Phenomenex

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MOISTuRE, OxYGEN AND HYDROCARBON GAS TRAPS/PuRIFIERS• Improve analytical reliability (identification and quantitation results)

• Protect capillary columns from irreversible damage

• Extend column lifetimes and save money

• Reliable and affordable high-capacity, high- performance purifiers

Gas traps/purifiers are recommended, even with ultra-high purity gases. Trace contaminants can cause unstable baselines, high detector noise, ghost peaks and even column damage. Oxygen is especially detrimental to more-polar columns and can cause oxidation of the stationary phase, column bleed, loss of retention as well as reduced column lifetimes.

Keep trace impurities in your system gases below 1 ppm by "scrubbing" moisture first with a high capacity moisture trap. Follow this with a high capacity hydrocarbon trap for removal of hydrocarbons/organics. Then, finally and most importantly, remove oxygen impurities from the gas stream with a high performance oxygen trap.

Hydrocarbon Traps• Improves baselines and analytical sensitivity

• Integral 40 µm frits prevent particle contamination

• Removes trace organics from carrier gases, air and hydrogen

Indicating Oxygen Traps• Improves analytical sensitivity

• Reduces O2 to less than 1 ppb

• Adsorbs moisture and other polar or polarizable molecules

• Color indicator warns of saturation

Hydrocarbon TrapsPart no. Description Unit Price

100cc I I I AG0-4770 Hydrocarbon Trap, capillary grade, 1/8" fittings ea AG0-4771 Hydrocarbon Trap, capillary grade, 1/4" fittings ea 200cc AG0-4772 Hydrocarbon Trap, 1/8" fittings ea AG0-4773 Hydrocarbon Trap, 1/4" fittings ea AG0-5618 Hydrocarbon Trap Refill, 1 pint, 2 recharges ea

Indicating Oxygen Traps

Part no. Description Unit Price 50cc I I I AG0-4774 Indicating Oxygen Trap,1/8" fittings ea AG0-4775 Indicating Oxygen Trap,1/4" fittings ea 150cc AG0-4776 Large Indicating Oxygen Trap,1/8" fittings ea AG0-4777 Large Indicating Oxygen Trap,1/4" fittings ea


Indicating Glass Moisture Traps

Part no. Description Unit Price100cc I I I

AG0-4766 Glass Indicating Moisture Trap,1/8" fittings ea 250cc AG0-4768 Large Glass Indicating Moisture Trap,1/8" fittings ea AG0-4769 Large Glass Indicating Moisture Trap,1/4" fittings ea

Indicating Glass Moisture Traps• Reduces noise for high-sensitivity GC detectors: GC/MS, MSD, ECD, Hall EC, Ion Trap

• Heavy-wall borosilicate glass tube prevents O2 and H2O infusion

• Pre-purged with ultra-high purity helium for rapid equilibration/stabilization



Technical SpecificationsPacking: Impregnated carbon filter mediaIndicator: no Max pressure: 250 psi (1724 kPa)Efficiency: Excellent to none (call for specific compound ratings)Fittings: 1/8 or 1/4"Purge Gas: Helium, ultra-high purity

For maximum efficiency, flow rates for any trap should not exceed 3 L/min. Trapping efficiency will drop-off rapidly as flow rates increase.

Technical SpecificationsPacking: Molecular sieve 13XIndicator: yes, 4A indicating molecular sieveMax pressure: 100 psi (690 kPa)Efficiency: ≤10 ppb H2OCapacity: 100 cc unit: 10 standard “A” cylinders with up to 300 ppm H2OFittings: 1/8 or 1/4"

Technical SpecificationsPacking: ProprietaryIndicator: yesMax pressure: 50 psi (345 kPa) Efficiency: ≤1 ppb O2

Fittings: 1/8 or 1/4"Frit: 40 μm stainless steel

331Phenomenex

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LabClear OxiClear™ Gas Purifiers• High performance, high capacity purifier

• Removes oxygen and trace amounts of water and organics from carrier gases

• Popular, affordable and disposable

Combination Oxygen/Moisture Traps• Improves analytical sensitivity of GC/MS, MSD, ECD

• Reduces O2/H2O to less than 15 ppb

• Pre-purged with ultra-high purity helium for rapid equilibration/stabilization

• High capacity capillary grade

The Combo™ Oxygen/Moisture Trap incorporates a revolutionary new scrubbing media with twice the surface area for high capacity. Discover how you can improve analytical results using high sensitivity GC-MS and ECD detectors when oxygen and moisture are efficiently removed from the gas stream. Remember, even trace levels of these "bad actors" in your carrier gas can degrade your separation or even destroy your capillary column, particularly columns composed of more polar phases and/or thicker films. Their sensitivity to oxygen increases approximately one order of magnitude for every 20 °C increase in operating temperature. At the typical upper temperature limits of these phases (200 to 240 °C) even minute traces of oxygen and water will cause severe degradation/damage to the column.

The Combo Trap is a one-piece, aluminum canister that contains a highly active, metal-based, inlet support reagent capable of scrubbing oxygen in the gas stream to less than 15 ppb. Up to 2 g of moisture can also be removed by this trap with no effect on the oxygen-removing capacity. Filled under a heated flow of ultra-high purity helium, this trap is ready to go to work.

Excellent for argon-methane mixtures used with ECDs, this trap effectively prevents degradation of the detector's radioactive source. For GC-MS applications, no extensive purging is necessary as with other traps prepared with nitrogen. In addition to inert gases (nitrogen, helium, argon and krypton) the Phenomenex Combo Trap treats streams of hydrogen, alkanes, alkenes, aliphatic hydrocarbon gases, low boiling aromatics, carbon dioxide and carbon monoxide.

A 40 µm stainless steel frit is pressed into each end fitting and the unit is tested to 2000 psi for integrity. Available with 1/8" or 1/4" fittings, the popular Combo Trap is highly dependable and a very cost-effective option for your system.

OxiClear Gas PurifiersPart no. Description Unit Price

5½ x 2" I I I AG0-4792 OxiClear Disposable Gas Purifier,1/8" fittings ea AG0-4791 OxiClear Disposable Gas Purifier,1/4" fittings ea


Combination Oxygen/Moisture TrapsPart no. Description Unit Price

AG0-4778 I Combo Oxygen / Moisture Trap,1/8" fittings I ea I

AG0-4779 Combo Oxygen / Moisture Trap,1/4" fittings ea


Technical SpecificationsPacking: ProprietaryIndicator: noMax pressure: 2000 psi (13,789 kPa)Efficiency: ≤15 ppb O2 and H2OCapacity: 2 g H2O Fittings: 1/8 or 1/4"

Technical SpecificationsPacking: ProprietaryIndicator: noMax pressure: 250 psi (1723 kPa)Max recommended flow: 3 mL/min @ 35 psiEfficiency: ≤5 ppb O2 when incoming O2 concentration is 15 ppm or lessCapacity: ≥1200 cubic ft. standard grade gasFittings: 1/8 or 1/4" (nickle plated brass)

332 Phenomenex

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SEPTA

Silicone Rubber Inlet Septa• Advanced silicone formulations reduce coring and increase septum lifetime

• Enhanced durability and re-sealing capabilities

• Precision formed and cut to exacting specifications

• Reduced needle damage

• General purpose and specialty low bleed, high temperature septa available

PhenoGrey-250

This general purpose silicone rubber septum is designed for use up to 250 °C for extended periods of time. With a durometer reading of 40-45, septum puncture is easy (fewer bent needles) for up to 100 injections.

PhenoBlue-300

This low-bleed septum is designed from a recent technology advance in the silicone field. Thoroughly tested and evaluated, the high durometer rating of 50-60 guarantees over 100 injections at 300 °C, but is actually heat-stable to 350 °C to give you even greater confidence when the oven heats up!

PhenoRed-400

Fire brick red, with a 50 durometer rating, this specially formulated high-temperature, low-bleed silicone rubber septum is designed and conditioned for high sensitivity analysis where the demands for low bleed and heat stability are critical. Say goodbye to ghost peaks! Temperature-rated to 400 °C, even continuous injection port temperatures of 350 °C rarely change this septum's physical properties. Typical injection life is 150 punctures. Tested against some of the leading septa, the PhenoRed-400 has proven itself to be one of the best in its class.

PhenoGreen-400

Long life, high-temperature green septum, rated to 400 °C. GuideRight™ through-hole to guide the needle during injection.

Septa Sizes by GC Instrument Manufacturer

I Instrument Model

I Septa Diameter

Agilent (HP) 5850, 5880, 5890, 6850, 6890 7/16" (11 mm) 5700 series, 5880A 3/8" (9.5 mm)

Antek All 3/8" (9.5 mm)

Finnigan 9600 3/8" (9.5 mm)

Finnigan/Tremetics 9000, 9500 1/2" (12.7 mm)

Fisons/Carlo Erba 8000 series 21/32" (17 mm)

GOW-MAC All 3/8" (9.5 mm)

HNU Portable GC 3/8" (9.5 mm)

PerkinElmer Sigma series, 900, 9900, 8000, Autosampler 7/16" (11 mm)

Shimadzu All plug

Tracor 220, 222 1/2" (12.7 mm) 540 11/24" (11.5 mm) 550, 560 3/8" (9.5 mm)

Varian Packed column injectors 3/8" (9.5 mm) SPI 7/16" (11 mm) 3700 / Vista capillary injectors 7/16" (11 mm) or Saturn GC/MS 11/24" (11.5 mm)


Silicone Rubber SeptaPart no. Description Unit Price Part no. Description Unit Price PhenoGrey 3/8" (9.5 mm) Diameter

I

PhenoGrey 7/16" (11 mm) Diameter

I

AG0-4686 PhenoGrey-250 Injector Septa 50/pk AG0-4692 PhenoGrey-250 Injector Septa 50/pkAG0-4687 PhenoGrey-250 Injector Septa 100/pk AG0-4693 PhenoGrey-250 Injector Septa 100/pkPhenoBlue PhenoBlue AG0-4688 PhenoBlue-300 Injector Septa 50/pk AG0-4694 PhenoBlue-300 Injector Septa 50/pkAG0-4689 PhenoBlue-300 Injector Septa 100/pk AG0-4695 PhenoBlue-300 Injector Septa 100/pkPhenoRed PhenoRed AG0-4690 PhenoRed-400 Injector Septa 50/pk AG0-4696 PhenoRed-400 Injector Septa 50/pkAG0-4691 PhenoRed-400 Injector Septa 100/pk AG0-4697 PhenoRed-400 Injector Septa 100/pk

See p. 335-337 for injection port inlet liners.

Other septa are available upon request.Shimadzu Injector Septa PlugPart no. Description Unit Price

AG0-7517 I Septa plug for all Shimadzu Injectors I 50/pk I

(9A, 14, 15A, 17A, 2010) Rated to 350 °C


GuideRight™ Injection Hole SeptaThe GuideRight™ through-hole guides the needle during injection. Septum performance and lifetime increase while downtime due to bent needles or dirty injection ports decreases. Choose from either high-temperature PhenoGreen™ or PhenoRed™, both rated to 400 °C.

GuideRight Injection Hole SeptaPart no. Description Unit Price

I PhenoGreen 3/8" (9.5 mm) Diameter I I

AG0-7874 PhenoGreen™ 400 Injector Septa 50/pk PhenoGreen 7/16" (11 mm) Diameter

AG0-7875 PhenoGreen™ 400 Injector Septa 50/pk PhenoRed 3/8" (9.5 mm) Diameter

AG0-7916 PhenoRed™ 400 Injector Septa 50/pk PhenoRed 7/16" (11 mm) Diameter

AG0-7917 PhenoRed™ 400 Injector Septa 50/pk


333Phenomenex

ACCESSORIESHPLC &

GCM

erlin Micro

seal

GC ACCESSORIES

Merlin Microseal™ Septum (for Agilent GC's)• Improves chromatographic performance and quanti- tative results by reducing bleed and ghost peaks

• Save time changing septa, instrument downtime and troubleshooting

• Thousands of injections before seal replacement

• Easier manual injections

• Improves reliability and performance during extended automated runs

• No instrument modification required

The Merlin Microseal Septum is a long-life replacement for the standard septum on the capillary inlet or the purged-packed inlet of Agilent GC systems.

The Microseal is a patented inlet assembly that provides two distinct sealing mechanisms. The first is a double O-ring seal around the syringe that ensures gas leak integrity during time of injection. There is no traditional septum to core or flake, which can cause bleeding and ghost peaks, and less force is required for the user to make a manual injection. The second seal is a spring-assisted duckbill that reliably maintains a high-pressure seal within the injection port at all times.

Since the syringe does not pierce any septum material, seal lifetime is significantly extended – Microseals are typically used for up to one year or more under normal conditions before septum replacement. Many laboratories experience lifetimes of 5,000 to 10,000 injections or more. This means you save tremendously in time changing septa, instrument downtime and troubleshooting.

Syringes for use With the Merlin Microseal™

Chromatographic performance will also improve due to less bleed and fewer ghost peaks, improving quantitation and data reliability.

Instrument Compatibility: The Merlin Microseal systems can be used manually with all Agilent 5800 and 6800 series GCs. However, for autosampler use it is compatible with only the 7673A and 7673B units. Other inlets or autosampler systems from Agilent or other manufacturers are not compatible.


Merlin Microseal Septum (For Agilent GC's)

Part no. Description Unit Price

AG0-5985 I Merlin Microseal High Pressure Septum Standard Kit, includes nut and 2 septa

I ea

I

AG0-5986 Merlin Microseal High Pressure Septum Starter Kit, includes nut and 1 septum ea Replacement Parts AG0-5987 Merlin Microseal High Pressure Septum ea AG0-5988 Merlin Microseal High Pressure Nut Kit, includes 1 nut ea

O-ring seals needle during injection

Spring

Duckbill opens easily, seals reliably

(1) Complete High Pressure Kits include the nut and one or two Microseal septa. All High Pressure Kits are rated for inlet pressures up to 100 psi. For long-term operation (>6 months) with the Microseal septum use the following injection port limits: (a) Agilent 6890, 5890 Series II - 325 °C; (b) Agilent 5890A - 300 °C.

Higher temperatures will result in shorter lifetimes. (2) The Merlin Microseal Septum should only be used with a blunt-tipped, 0.63 mm diameter (0.025”, 23 gauge) syringe needle (typically used with the Agilent 7673 autosampler). Sharp-pointed or sharp-edged needles should not be used as they may slice or pierce the seals.

Part no. Mfr. no. Agilent P/n Description* Capacity (µL) Unit Price Part no. Mfr. no. Description* Vol Range Unit Price

For Agilent 7673 Autosamplers I I I I Removable needles

I I I I

AS0-4386 87987 9301-0892 75ASN (23s/1.71"/HP) 5 ea AS0-4401 7786-01 RN (23s/1.71"/3) 2.5-100 µL 6/pkAS0-4387 80387 9301-0713 701ASN (23s/1.71"/HP) 10 ea AS0-4388 80390 9301-0725 701ASN (23s/1.71"/HP) 10 6/pk AS0-4389 80389 — 701ASN (26s/1.71"/HP) 10 6/pk

NOTE: Replacement needles are available in packs of three. * Values in parentheses denote the following: (gauge/length/point style). “s” after gauge denotes smaller/reduced internal needle diameter.


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GC ACCESSORIES

Sealing Rings for Agilent Inlet Liners Similar to Part no. Description Mfr. no. * Unit PriceAG0-7326 l Sealing ring, Viton, rated to < 300 °C l 5180-4182 l 10/pk l

AG0-7327 Sealing ring, graphite, rated to > 250 °C (450 °C max.) 5180-4168 10/pk


Inlet Base Seals Similar to Part no. Description Mfr. no.* Unit Price

Standard, single groove for splitless applications, 0.8 mm dia. inlet hole l l l AG0-7518 Gold Inlet Base Seal, splitless (single groove), 0.8 mm 18740-20885 2/pk AG0-7519 Gold Inlet Base Seal, splitless (single groove), 0.8 mm 18740-20885 10/pk High Split Flow, cross groove for split applications, 0.8 mm dia. inlet hole AG0-7520 Gold Inlet Base Seal, split (double groove/cross), 0.8 mm 5182-9652 2/pk AG0-7521 Gold Inlet Base Seal, split (double groove/cross), 0.8 mm 5182-9652 10/pk Replacement Inlet Seal Washers AG0-7522 Inlet Seal Washers, for Agilent GC injection port 5061-5869 12/pk

*Similar to but not always an exact equivalent to the original manufacturer's product.

SEALING O-RINGS• Thermally stable

• Graphite suitable for GC/MS

The Viton O-rings below are suitable for all Agilent inlet liners 6.3 mm OD and can be used at temperatures up to 300 °C. Graphite sealing rings are also made to fit 6.3 mm OD inlet liners and can withstand temperatures above 250 °C.

Tip for Agilent GCs: The critical seal for Agilent GCs is at the top of the inlet sleeve. Injection liner O-rings are made to seal leak tight on both split and splitless liners, but do require frequent replacement in order to ensure sealing integrity and optimal performance.

INLET BASE SEALS• Prevents analyte adsorption

• Improves detection sensitivity

• Improves method reproducibility

• Fits all Agilent 5890/6890 systems

Phenomenex offers high-quality replacement inlet base seals for Agilent split/splitless injection ports. These precision-machined, low-cost seals reduce the need for cleaning and reuse, saving you time and money. The seals are gold plated, providing exceptional inertness to active compounds with better sealing properties than conventional uncoated steel.

• Guaranteed replacement to equivalent Agilent part numbers

In Agilent split/splitless injection ports, the inlet seal sits at the base of the injector. Non-volatile residues, septum fragments, and other contaminates dirty this inlet seal, which can severely degrade chromatographic performance. The result can be analyte adsorption and breakdown as well as higher background noise, degraded quantitation and reproducibility.

335Phenomenex

ACCESSORIESHPLC &

GCInlet Liners

GC ACCESSORIES

Tapered FocusLiners

Description

INJECTION PORT INLET LINERS • Fit standard instrument manufacturers’ inlets

• Popular designs at excellent prices

• Reduce analyte discrimination

• Improve reproducibility and results

• Clean, non-adsorptive/non-reactive surface

The Tapered FocusLiner™ can markedly improve reproducibility and results. In the original FocusLiner design a glass wool plug is held fast in the ideal position in the injection liner to provide extra surface area for vaporization as well as wipe the needle of any residual sample once withdrawn. The wool also traps any nonvolatile sample residue, maintaining a cleaner column inlet. Now markedly improved by adding a narrow taper at the bottom of the liner, sample loading using the Tapered FocusLiner is more even (i.e., less discrimination) for samples with a wide range of boilers. Made with a consistent, high-quality deactivation process, the Tapered FocusLiner offers enhanced analytical precision for even the higher molecular weight components of your sample.

4 mm ID Liner with Glass Wool

% RSD comparison of 15 consecutive injections on 2 types of inlet liners

4 mm ID FocusLiner™

FocusLiner™ Design Improves Analytical Precision

Description

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Agilent Technologies (HP) I I I I I I I I

Split / Splitless 5880/5890/6890 4 x 78.5 x 6.3 B (y) Y 092002 AG0-7515 5/pk 092219 AG0-7582 25/pk Single Taper / Gooseneck Liner 5880/5890/6890 4 x 78.5 x 6.3 B (y) Y 092003 AG0-4680 5/pk 092011 AG0-7514 25/pk PerkinElmer Single Taper / Gooseneck Liner AutoSystem™ 4 x 92 x 6.2 B (y) Y 092095 AG0-4681 5/pk & Clarus 500 09209525 AG0-7864 25/pk Split / Splitless AutoSystem™ 4 x 92 x 6.2 B (y) Y 092092 AG0-7639 5/pk & Clarus 500 09209225 AG0-7865 25/pk Shimadzu Single Taper / Gooseneck Liner 17B 3.4 x 95 x 5 B (y) Y 092068 AG0-4683 5/pk

Thermo Electron (Carlo Erba) Single Taper / Gooseneck Liner 8000 series 5 x 105 x 8.0 B (y) Y 092046 AG0-4679 5/pk 09204625 AG0-7863 25/pk Varian Single Taper / Gooseneck Liner 1075/77 4 x 72 x 6.3 B (y) Y 092025 AG0-4684 5/pk

Double Taper / Gooseneck Liner 1078/79 3.4 x 54 x 5 B (y) Y 092036 AG0-4685 5/pk

* *B= Borosilicate; Deactivated = Yes (y) or No (n)


% R

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Injection Port Inlet Liners (cont'd)


Cup Splitter, Gooseneck and Straight Liners

Description

* B= Borosilicate; Deactivated = Yes (y) or No (n). ** Similar to but not always an exact equivalent to the original manufacturer’s product.

Co

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ea5/pk

25/pk

ea5/pk

25/pk

ea5/pk

25/pk

ea5/pk

25/pk

ea5/pk

25/pk

ea5/pk

25/pk

ea5/pk

25/pk

ea5/pk

25/pk

ea5/pk

25/pk

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ea5/pk

25/pk

ea5/pk

25/pk

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ea5/pk

25/pk

Split / Splitless, Single Taper with wool

Split / Splitless Liner with wool

Splitless, Double Taper/Gooseneck Liner

Split Liner with wool

Single Taper Direct Connect with Side Hole (bottom)

Single Taper Direct Connect with Side Hole (top)

Split / Splitless, Recessed Gooseneck Liner with wool

Direct Liner

Split / Splitless Single Taper/Gooseneck Liner with wool

Split / Splitless Liner with wool

Split / Splitless, Single Taper/Gooseneck Liner

Split / Splitless with Single Taper

Splitless Liner

Splitless Liner

Cup Splitter / Split Liner with wool

Cup Splitter / Split LinerAgilent Technologies (HP) I I I I I I I I I

5880/5890/6890 4 x 78.5 x 6.3 B (n) N HP 18740-80190 — 5183-4699 20710 AG0-4647 5/pk 25/pk 5183-4700 — AG0-4648 25/pk

5880/5980/6890 4 x 78.5 x 6.3 B (n) Y Like HP 18740-80190, but with wool 5183-4699 AG0-7853 5/pk 5183-4700 2048205 5880/5890/6890 2 x 78.5 x 6.3 B (n) N HP 18740-80220 — 5181-8818 — 5183-4703 20713 AG0-4649 5/pk 5183-4704 20714 AG0-4650 25/pk 5880/5890/6890 4 x 78.5 x 6.3 B (n) N 210-3003 — 210-3003-5 20773 AG0-4651 5/pk 20774 AG0-4652 25/pk 5880/5890/6890 4 x 78.5 x 6.3 B (y) N 5181-3316 — 5183-4695 20799 AG0-7516 5/pk 5183-4696 20800 AG0-7640 25/pk 5880/5890/6890 2 x 78.5 x 6.3 B (n) N 5181-3316 — 5183-4695 20796 AG0-4653 5/pk 5183-4696 20797 AG0-4654 25/pk 5880/5890/6890 4 x 78.5 x 6.3 B (y) Y 19251-60540 — 5183-4691 20782 AG0-4655 5/pk 5183-4692 20783 AG0-4656 25/pk 5880/5890/6890 4 x 78.5 x 6.3 B (y) Y 5062-3587 — 5183-4693 22406 AG0-4657 5/pk 5183-4694 22407 AG0-4658 25/pk 5880/5890/6890 1.5 x 78.5 x 6.3 B (y) N 18740-80200 — 5183-4709 20973 AG0-4659 5/pk 5183-4710 — AG0-4660 25/pk 5880/5890/6890 4 x 78.5 x 6.3 B (y) Y 19251-60540 — 5183-4691 22409 AG0-4661 5/pk 5183-4692 22410 AG0-4662 25/pk 5880/5980/6890 4 x 78.5 x 6.3 B (y) N — 21055 AG0-7850 5/pk 20998

5880/5980/6890 4 x 78.5 x 6.3 B (y) N G1544-80730 20771 AG0-7851 5/pk 5880/5890/6890 4 x 78.5 x 6.3 B (y) Y 5183-4647 — 5183-4701 21033 AG0-8172 5/pk 5183-4702 — 5880/5890/6890 4 x 78.5 x 6.3 B (y) N 5181-3315 — 5183-4705 20785 AG0-8173 5/pk 5183-4706 20786

5880/5890/6890 4 x 78.5 x 6.3 B (y) Y — AG0-8174 5/pk

5880/5980/6890 4 x 78.5 x 6.3 B (y) Y 5183-4711 — 5183-4712 22406 AG0-8175 5/pk 5183-4713 22407

GCM

odel

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Price

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337Phenomenex

ACCESSORIESHPLC &

GCInlet Liners

GC ACCESSORIES

GCM

odel

No.

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Mat

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Num

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*

Part

No.

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Price

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(dea

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ool(

Y/N)

Injection Port Inlet Liners (cont'd)


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n In

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his

End

5/pk

5/pk

—

5/pk

5/pk 25/pk

5/pk

25/pk

5/pk

ea5/pk

25/pknot

deactivated

ea5/pk

25/pk

ea5/pk

25/pknot

deactivated

Cup Splitter, Gooseneck and Straight Liners (cont'd)

Description

PerkinElmer I I I I I I I I I Autosystem 3.5 x 100 x 5 B (n) N 0330-5181 20740 AG0-4663 5/pk

Autosystem 4 x 92 x 6 B (n) N N610-1052 20836 AG0-4665 5/pk

Shimadzu 17A, 17B, 2010 2.6 x 95.5 x 5.0 B (y) N — AG0-4667 5/pk

9A/16A 3.4 x 139 x 5.0 B (y) N — 20749 AG0-4669 5/pk Thermo Electron (Carlo Erba) 6000 Series 3 x 79.5 x 5.0 B (y) N 45300400 20815 AG0-4643 5/pk

20816

Thermo Electron (Finnigan) 8000 Series 3 x 105 x 8.0 B (y) N — 20937 AG0-4645 5/pk

20938

8000 5 x 105 x 8.0 B (y) N 45350033 AG0-7852 5/pk

Varian 1075/1077 2 x 74 x 6.3 B (n) N 01-900109-05 20722 AG0-4671 5/pk 03-949437-09 20723 1075/1077 4 x 74 x 6.3 B (n) N 01-900109-05 20905 AG0-4673 5/pk 20906

1093/1094I 0.5 x 54 x 4.7 B (y) N 01-900109-06 20776 AG0-4675 5/pk — 20777 03-918332-01

1093/1094I 0.8 x 54 x 4.7 B (y) N 01-900109-07 20779 AG0-4677 5/pk

Split / Splitless Liner

Splitless Liner

Splitless / Single Taper LinerTrace / Trace

Splitless Liner

Splitless Liner

Splitless Liner

Splitless Liner

Split / Splitless Liner

Cup Splitter / Split Liner

SPI (septum-equipped programmable injector) Liner

SPI (septum-equipped programmable injector) Liner

* B= Borosilicate; Deactivated = Yes (y) or No (n). ** Similar to but not always an exact equivalent to the original manufacturer’s product.

338 Phenomenex

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Zephyr™ 500HR

DIGITAL GAS FLOW METER• Accurate - NIST Traceable calibration with up to 0.01 mL/min resolution

• Precise - unaffected by temperature or pressure

• Versatile - Measure Air, Nitrogen, Oxygen, Hydrogen, Helium, and 5 % Argon/Methane up to 500 mL/min and Carbon Dioxide up to 300 mL/min

Reliable, Accurate Flow MeasurementThe Phenomenex Zephyr™ 500HR Digital Gas Flow Meter is an excellent choice for all your flow applications. The unit provides reliable accurate real-time measurements for all your gas streams. With seven gas NIST-traceable calibrations, 2 % of reading accuracy, and a measuring range from 0.01-500 mL/min, one flow meter replaces several separate flow meters for GC, SFC, SFE, industrial hygiene, biotechnology and general laboratory applications.

The flow meter works equally well with positive and negative (vacuum) flow sources and may be placed in-line for continuous flow measurement. Use it to monitor flow to traps, sorbent tubes, incubators, fermentors, or reaction vessels without interrupting gas flow.

Compared to most other general-purpose flow meters, the Zephyr offers a wider flow range and higher resolution (0.01 mL/min), and with the accuracy and precision you need at low flowrates. Don’t waste money purchasing any other flow meter. The unit’s auto-ranging display shows two decimal places (0.01 mL/min resolution) for reading less than 10 mL/min. It is good for setting capillary GC flow or for leak testing. Its high sensitivity easily detects even the smallest of leaks.

Rugged and ReproducibleThe rugged solid-state sensor with microprocessor controller measures true mass flow without the ambient temperature and pressure change errors that affect soap film and acoustic sensor meters. There’s also no water-vapor error (up to 5 %) that plagues soap film techniques. You’ll obtain precise, accurate flow measurement with no liquids, no bubbles, no waiting and no hassles!

Unlike competitive flowmeters, the Zephyr 500HR Digital Gas Flow Meter tolerates water vapor, making it suitable for purge and trap applications. If the sensor is exposed to an exceedingly moist sample, simply purge the sensor with dry gas for several minutes to restore performance.

Each unit’s straight-through gas flow path reduces backpressure, internal volume, and sensor purge time. Readings stabilize quickly and measurements at low flow rate are accurate and precise.

Versatile Fittings & Flow AdaptorsThe flow meter includes interchangeable fittings and 1/32” and 1/8” ID tubing. Use the smaller tubing for low-flow measurements. The larger tubing minimizes backpressure for high-flow measurements.

Flow adaptors make convenient, leak-free connections to all of your flow sources. The unit includes General Purpose and Agilent split vent adaptors. The General Purpose adaptor connects to Agilent FID, split vent traps, packed GC columns, and gas lines. The Agilent split vent adaptor connects to Agilent GC split vents. The unit also includes a capillary column adaptor.

nIST Traceable CalibrationThe Zephyr 500HR Digital Gas Flow Meter is calibrated with seven gases using NIST traceable standards. An economical recalibration service maintains the unit’s performance, and includes minor repairs and an NIST-traceable calibration certificate. The certificate includes percent error data indicating how far your meter was out of calibration, helping you meet ISO, GLP, GMP and other quality system requirements. The unit is CE approved.

SpecificationsFlow Range: 0.01-500 SCCM Air, N2, H2, O2, He & 5 % Ar/CH4 Auto-ranging

0.01 - 300 SCCM CO2Accuracy: 0.01 - 9.99 SCCM: 0.01 SCCM or +/-2 % of reading

10.0 - 500 SCCM: 0.1 SCCM or +/-2 % of readingSensor Type: Solid-state mass flow, silicon on ceramicCalibration: Multi-point, NIST Traceable, all gases, Certificate supplied

with % Error DataModes: Standard flow range: mass flow, linear velocity & split ratio

Low flow range: mass flow & split ratiosDisplay: 16-Character Alpha-Numeric LCD, Auto-rangingPower: 9-Volt (alkaline) automatic power off 5 minutes after last

key stroke, low battery warningDimensions: 190.5 x 57.4 x 101.6 mm (7.5" x 2.26" x 4.0")Safety: CE mark certification to EN55011, EN5502 & EN50082-1Warranty: 1 year parts & labor. Does not cover recalibration of unit.

Digital Gas Flow Meter

Part no. Description Unit Price

EG0-7332 I Zephyr 500HR Digital Gas Flow Meter, 0.01-500 mL/min,

I ea

I

9V battery powerReplacement AccessoriesAG0-7344 1/16" (1.6 mm) Barbed Inlet/Outlet Fitting 2/pk AG0-7345 1/8" (3.8 mm) Barbed Inlet/Outlet Fitting 2/pk AG0-7346 Split Vent Adaptor ea AG0-7347 General Purpose Flow Adaptor ea AG0-7348 Capillary Column Adaptor ea AG0-7349 1/32" (0.8 mm) ID Connecting Tubing, 10 ft. ea AG0-7350 1/8" (3.8 mm) ID Connecting Tubing, 1 meter ea AG0-7351 Replacement Septa for Capillary Column Flow Adaptor 25/pk (1/4" Cylindrical septa)Recalibration ServiceAG0-7352 Recalibration Service for the Zephyr 500HR ea


Note: Zephyr 500HR Digital Gas Flow Meter includes A, B, E, F, G, H & I

ABEFGHI

Note: SCCM = Standard Cubic Centimeters per Minute

339Phenomenex

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Syring

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SYRINGES

Hamilton Syringes

Needle Dimensions: 26s Gauge; Point Style #2; 2" Long

1000 Series Gastight Syringes

The Hamilton 1000 Series GASTIGHT syringes with Teflon Luer lock tip are available in volumes from 1.0 to 100 mL (Luer lock needle not included).

Part no. Mfr. no. Model no. Capacity (mL) Unit Price

AS0-1907 I 81320 I 1001 TLL I 1.0 I ea I

AS0-1908 81420 1002 TLL 2.5 ea AS0-1909 81520 1005 TLL 5.0 ea AS0-1910 81620 1010 TLL 10.0 ea Luer Lock needles with Fluorocarbon Hub, 2" long, #2 pt style AS0-1914 90126 KF 726 26 gauge 6/pk AS0-1915 90122 KF 722 22 gauge 6/pk AS0-1916 90116 KF 716 16 gauge 6/pk

Removable Needles

Replacement needles are available in packs of three.

Part no. Mfr. no. Description* Vol. Range Unit Price

AS0-1904 I 7758-04 I RN (26/2"/2) I 2.5-100 µL I 6/pk I

AS0-1905 7758-01 RN (22/2"/2) 2.5-100 µL 6/pk AS0-4392 7758-02 RN (26/2"/2) 25-100 µL 6/pk AS0-4393 7758-03 RN (22s/2"/2) 25-100 µL 6/pk AS0-4395 7779-01 RN (22/2"/2) 250 µL-10 mL 6/pk AS0-4398 7779-03 RN (22s/2"/2) 250 µL-10 mL 6/pk AS0-4396 7770-02 RN (22/2"/3) 2.5-100 µL 6/pk AS0-4394 7770-01 RN (22s/2"/3)1 2.5-100 µL 6/pk AS0-4397 7780-04 RN (22/2"/3)1 250 µL-10 mL 6/pk AS0-4400 7780-03 RN (22s/2"/3)1 250 µL-10 mL 6/pk AS0-4402 8648-01 RN (25s/1.97"/3)2 250 µL-10 mL 6/pk AS0-4401 7786-01 RN (23s/1.71"/AS)2 2.5-100 µL 6/pk 1 for Rheodyne Injectors 2 for Waters U6K Injectors 3 for Agilent 7673 Autosampler * RN = Removable Needle Values in parentheses denote the following: (Gauge/Length/Point Style)."s" after Gauge denotes smaller/reduced internal needle diameter.

1700 Series Gastight Syringes

The Hamilton 1700 Series GASTIGHT syringes are available in volumes from 10-500 µL. The 1700 series GASTIGHT syringe with removable needle in either point style #2 (22° bevel) or #3 (90°) is a universally popular style for most GC & HPLC applications.

Part no. Mfr. no. Description* Capacity (µL) Unit Price

needle Point Style #2 I I

I I

AS0-1898 80030 1701RN (26s/2"/2) 10 eaAS0-1899 80230 1702RN (22s/2"/2) 25 eaAS0-1900 80930 1705RN (22s/2"/2) 50 ea AS0-1901 81030 1710RN (22s/2"/2) 100 eaAS0-1902 81130 1725RN (22s/2"/2) 250 eaAS0-1903 81230 1750RN (22s/2"/2) 500 eaneedle Point Style #3 AS0-4380 80065 1701RN (22s/2"/3) 10 eaAS0-4381 80265 1702RN (22s/2"/3) 25 eaAS0-4382 80965 1705RN (22s/2"/3) 50 eaAS0-4383 81065 1710RN (22s/2"/3) 100 eaAS0-4384 81165 1725RN (22s/2"/3) 250 eaAS0-4385 81265 1750RN (22/2"/3) 500 ea

The Hamilton 1700 Series syringes are also available with Teflon Luer lock tip, from 50 to 500 µL sizes.

For HP 7673 Autosamplers

Agilent Part no. Mfr. no. P/n** Description* Capacity (µL) Unit Price

AS0-4386 I 87987 I 9301-0892 I 75ASN I 5 I ea I

(23s/1.71"/HP)

AS0-7641 87990 — 75ASN 5 6/pk (23s/1.71"/HP)AS0-4387 80387 9301-0713 701ASN 10 ea (23s/1.71"/HP)AS0-4388 80390 9301-0725 701ASN 10 6/pk (23s/1.71"/HP)AS0-4389 80389 — 701ASN 10 6/pk (26s/1.71"/HP)


GC Injector Syringes

For HP 7670, 7671, 7672 GC Manual Injectors

Part no. Mfr. no. Description* Capacity (µL) Unit Price

AS0-4390 I 87900 I 75N (26s/2"/2) I 5 I ea I

AS0-0077 80300 701N (26s/2"/2) 10 ea AS0-0016 80366 701N (26s/2"/2) 10 6/pk AS0-4391 80000 1701N (26s/2"/2) 10 ea AS0-1899 80230 1702RN (22s/2"/2) 25 ea AS0-1902 81130 1725RN (22s/2"/2) 250 ea

See p. 361 for HPLC Syringes.

**Similar to but not always an exact equivalent to the original manufacturer’s product.

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Syr

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SGE Syringes For Valco®, Rheodyne®, Waters®, PerkinElmer®, and CTC/LeapThe syringes are fitted with a special dome-tipped removable needle to prevent needle seal damage in the valve and are of a specific length to avoid rotor damage. A low-cost 10 µL syringe, with fixed needle and replaceable plunger, is available for all valves.

SGE Gastight Luer Lock SyringesThe Gastight (GT) range of gas- and liquid-tight syringes has all the excellent features necessary to perform exacting tasks in GC, HPLC, and other applications, particularly where inertness and accuracy are of paramount importance. Replaceable plungers are fitted with PTFE tips which have been machined to provide a precision fit into the glass barrel.

Syringe capacities from 1 to 100 mL also have PTFE coated plunger stems. In addition, 1 to 100 mL syringes can be purchased with a PTFE center male Luer to accept Luer Lock needles. Luer Lock needles are not provided and must be ordered separately. Needles are provided in packages (see below).


SGE Syringes

Part no. Mfr. no. Description Capacity (µL) Unit Price

Syringes for Rheodyne/Valco (2" Fixed needle) I I I

AS0-0142 002301 10F-LC 10 eaAS0-0143 003300 25F-LC 25 eaAS0-0144 004300 50F-LC 50 eaAS0-0145 005300 100F-LC 100 eaAS0-0146 006300 250F-LC 250 eaAS0-0147 007300 500F-LC 500 eaSyringes for Rheodyne/Valco (2" Removable needle) AS0-4370 002313 10R-GT-LC(SS) 10 eaAS0-4371 003312 25R-GT-LC(SS) 25 eaAS0-4372 004312 50R-GT-LC(SS) 50 eaAS0-4373 005312 100R-GT-LC(SS) 100 eaAS0-4374 006312 250R-GT-LC(SS) 250 eaAS0-4375 007312 500R-GT-LC(SS) 500 eaAS0-4376 037250 Replacement Needles N10-LC, #2/0.028" OD/2" — (5/pk) AS0-4377 038250 Replacement Needles N25/500-LC, #2/0.028" OD/2" — (5/pk) Syringes for PerkinElmer(Fixed needle) AS0-7636 001957 SF-PE-GT-0.63 5 eaSyringes for CTC/Leap (Fixed needle) AS0-7638 002981 10F-C/F-S/O.63 10 ea

SGE Luer Lock Syringes

Part no. Mfr. no. Capacity (mL) Description Unit Price

AS0-0120 I 008025 I 1 I 1MF-LL-GT I ea I

AS0-0121 008760 5 5MDR-LL-GT ea AS0-0122 008960 10 10MDR-LL-GT ea Luer Lock and Luer Tip needles AS0-2016 039802 Needles 50 mm length, 5/pk 23 gauge, 20° bevel tip (style #2) AS0-2017 039803 Needles 50 mm length, 2/pk 23 gauge, side hole with dome tip (style #5)


341Phenomenex

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Syring

es

SGE Syringes For Agilent AutosamplersTapered 23-26s (Dual Gauge)

• Designed to Agilent specifications for the 7673, 7683 and 6850 autosamplers

• Proven reliability and performance better than 1 %

• Accuracy and precision better than 1 %

• Cone tip design for optimization of injection

This durable and accurate syringe configuration is very popular. Tapered needle syringes offer the strength of 23 gauge (0.63 mm) OD on the upper portion of the needle, while the 26 gauge (0.47 mm) lower portion allows the syringe to be used for on-column injection into 0.53 mm ID capillary columns as well as split/splitless, direct and packed injection.

VICI Series A-2 Gas Syringes• Push-button valve and smaller volumes

• Pressure-Lok® design offers gas-tight injections

• Inject without carrier backflushing to sharpen peaks and improve separations

• Leak-tight to 250 psi - liquids and gases

• No plunger "blow out" at elevated pressures

The A-2 features a push-button valve, which allows sample storage up to 250 psi in syringes as small as 25 µL. This is useful with small liquid samples containing low-boiling components that would be lost through evaporation using ordinary syringes.

The positive rear stop (in 100 µL and larger sizes) prevents plunger blowout at elevated pressures, protecting against sample loss or operator injury. Like the Series A gas syringe, the A-2 has all the standard Pressure-Lok features such as a PTFE plunger tip, PTFE-sealed needle and ultra-smooth bore. Replacement components are available for easy repair.

VICI Precision Sampling SyringesPart no. Mfr. no. Description Capacity (µL) Unit Price

AS0-4739 I 050023 I Series A-2 Syringe I 25 I ea I

AS0-4740 050024 Series A-2 Syringe 50 ea AS0-4741 050025 Series A-2 Syringe 100 ea AS0-4742 050031 Series A-2 Syringe 250 ea AS0-4743 050032 Series A-2 Syringe 500 ea AS0-4744 050033 Series A-2 Syringe 1000 (1 mL) ea AS0-4745 050034 Series A-2 Syringe 2000 (2 mL) ea AS0-4746 050035 Series A-2 Syringe 5000 (5 mL) ea

NOTES: (1) All other VICI Precision Sampling products not listed are available. (2) Removable needle: 0.028" x 0.005" x 2.00", bevel, open end on 25, 50 and 100 µL (p/n 943050, 3/pk); 0.029" x 0.012" x 2.00", bevel, open end on all others (p/n 943051, 3/pk).

SGE Syringes for Agilent Autosamplers

Similar to Capacity Part no. Mfr. no. Agilent/ P/n* Description (µL) Unit Price

AS0-5208 I 001821 I 5181-1273

I 5F-HP-0.63/0.47 I 5 I ea I AS0-5209 002826 5181-1267 10F-HP-GT-63/47 10 ea AS0-7637 002804 — SK-10F-HP-47 10 6/pk AS0-5210 002827 5181-3361 SK10F-HP-GT-0.63/0.47 10 6/pk

NOTES: (1) All other SGE syringes and accessories not listed are available. (2) All syringes listed above are fixed needle syringes with tapered 23-26s dual gauge, 42 mm length needles. Only the 5 µL capacity syringe is not gas-tight.

ORDERING INFORMATION ORDERING INFORMATION


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