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GTE1544-VENM01 VENM INSPECTION MEMO Client: Hannas Job No: GTE1544 Project: Industrial Subdivision By: J.George Location: Lot 37 Prospect Highway, Pemulwuy Our Ref No: VENM01 Contact: Joel Hewitt Date: 3/04/2018 As requested, Ground Technologies undertook a sampling and testing of the western batter soil material contained within lot 37, Prospect Highway Pemulwuy. The site is being developed as an industrial estate and approximately 40,000m 3 of material will need to be excavated and disposed off site for the proposed development works. 1. Introduction In January 2018, PSM consultants carried out a geotechnical investigation of the QuarryWest Estate (Geotechnical Report-PSM3528-001L REV1). This site was part of the Boral Quarry in the past and their offices were located on the building pad till 2014. As part of the investigation seven (7) trenches were excavated up to a depth of 0.5m on the batters below approximately 101 RL. These trenches were still exposed at the time of our site investigation on 20 th March 2018. An inspection of the exposed trenches was conducted as part of this investigation and one sample was retrieved from each of the trenches. The proposed site location is given in Figure 1 and the areas of the exposed trenches are marked in Figure 2. Figure 1- Site Location 2. Site History Aerial photographs indicate the site was previously part of the Quarry site and an office building/warehouse and two smaller buildings were located on the existing building pad. The site of the excavated trenches (batter) was located to the west of the site structures. From the aerial photographs on the following pages, it is GROUND TECHNOLOGIES Geotechnical . Environmental . Laboratories Ground Technologies Pty Ltd ABN 25 089 213 294 19 Bernera Road, Prestons NSW 2170 PO Box 1121 Green Valley NSW 2168 Ph: (02) 8783 8200 Fax: (02) 8783 8210 Email: [email protected]

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Page 1: Ground Technologies Pty Ltd GROUND TECHNOLOGIES Ph: (02

GTE1544-VENM01

VENM INSPECTION MEMO Client: Hannas Job No: GTE1544

Project: Industrial Subdivision By: J.George

Location: Lot 37 Prospect Highway, Pemulwuy Our Ref No: VENM01

Contact: Joel Hewitt Date: 3/04/2018

As requested, Ground Technologies undertook a sampling and testing of the western batter soil material contained within lot 37, Prospect Highway Pemulwuy. The site is being developed as an industrial estate and approximately 40,000m3 of material will need to be excavated and disposed off site for the proposed development works.

1. Introduction In January 2018, PSM consultants carried out a geotechnical investigation of the QuarryWest Estate (Geotechnical Report-PSM3528-001L REV1). This site was part of the Boral Quarry in the past and their offices were located on the building pad till 2014. As part of the investigation seven (7) trenches were excavated up to a depth of 0.5m on the batters below approximately 101 RL. These trenches were still exposed at the time of our site investigation on 20th March 2018. An inspection of the exposed trenches was conducted as part of this investigation and one sample was retrieved from each of the trenches. The proposed site location is given in Figure 1 and the areas of the exposed trenches are marked in Figure 2.

Figure 1- Site Location

2. Site History Aerial photographs indicate the site was previously part of the Quarry site and an office building/warehouse and two smaller buildings were located on the existing building pad. The site of the excavated trenches (batter) was located to the west of the site structures. From the aerial photographs on the following pages, it is

GROUND TECHNOLOGIES

Geotechnical . Environmental . Laboratories

Ground Technologies Pty Ltd ABN 25 089 213 294 19 Bernera Road, Prestons NSW 2170 PO Box 1121 Green Valley NSW 2168 Ph: (02) 8783 8200 Fax: (02) 8783 8210 Email: [email protected]

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understood that the buildings on site were demolished sometime in 2014. It is understood that these buildings were on site for a long time as part of the quarry.

Figure 2 – Aerial Photograph of Site (2009)

Figure 3 – Aerial Photograph of Site (2013)

Figure 4 – Aerial Photograph of Site (2015)

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3. Assessment of Acid Sulphate Soils Data from the Department of Land and Water Conservation indicates that the subject site is situated in a region with no known occurrence of acid sulfate soils. Furthermore, no alluvial soils were encountered during the investigation.

4. Site Observations & Subsurface Investigation The exposed trenches were located on the western batters dipping towards the east. The existing geometry of the western batters are located within the area to the west of the existing building pad with a relatively flat slope above RL101m and a steep cut batter at approximately 45 degrees below this elevation.

Figure 5 – Location of excavated trenches

An inspection of the existing trenches exposed the following main soil profiles;

• Natural Clayey SAND, orange/brown • Slightly weathered Dolerite, orange brown/grey • Dolerite

Photograph 1– TP5 excavated trench showing cut profile

TP5 TP4 TP3

TP2A

TP2

TP1

TP0

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Photograph 2 – TP3 excavated trench showing cut profile

Photograph 3 – TP2 excavated trench showing cut profile

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Photograph 4 – TP1 excavated trench showing cut profile

Geological units observed in the subsurface profile are listed in Table 1; the trenches are marked the same as given in the PSM report to keep it uniform. There are three main soil profiles which are given below;

Table 1 – Geological Units

Unit Soil Profile TP0(RL)

TP1(RL) TP2(RL) TP2A(RL) TP3(RL) TP4(RL) TS5(RL) A Natural Clayey

Sand, orange/brown,

101.20 101.16 101.36 101.36 101.36 98.81 95.80

B Extremely to slightly weathered Dolerite,(boulders), brown;

96.49 96.74 96.91 96.46 98.53 95.80 93.88

C Dolerite, grey to dark grey and green

92.83 93.4 - - - - -

End of Trench(Toe of the batter)

91.20 91.20 91.40 91.40 91.40 91.20 91.20

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5. Laboratory Analysis - Contamination Whilst the potential for site contamination was low, limited laboratory screening testing was undertaken as a part of this investigation. The Assessment criteria used in this investigation have been obtained from the National Environment Protection (Assessment of Site Contamination) Measure (NEPM, 2013). This document presents risk-based Health Investigation Levels based on a variety of exposure settings for a number of organic and inorganic contaminants. To assess the risk to human health the results of the laboratory analysis are compared against the Health Investigation Levels (HIL) for the exposure setting; ‘standard residential with garden/accessible soil’ (‘A’). Test results are tabulated and presented below (Table 1) along with the relevant assessment criteria. Laboratory test certificates (ES1808431) are located in Appendix A.

Table 1: Laboratory Test Results – VENM Material

Chemicals and other attributes

Sample Number NEPM Health Investigation Level HILs (D)

(mg/kg) E1 E2 E3 E4 E5 E6 E7 Arsenic <5 <5 <5 <5 <5 <5 <5 100 Cadmium <1 <1 <1 <1 <1 <1 <1 20 Chromium (total) 10 5 10 4 8 6 11 100 Copper 108 84 81 29 70 41 60 6,000 Lead <5 <5 <5 <5 <5 <5 <5 300 Nickel 29 15 24 6 24 12 23 400 Zinc 27 16 21 33 20 23 30 7,400 Mercury <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 40 Total PAH <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 300 Carcinogenic PAH <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 3 Benzo(a)pyrene <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 0.7 Benzene <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 10 Toluene <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 65 Ethyl-Benzene <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 40 Xylenes <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 <0.05 1.6 TPH – C6-C10 <10 <10 <10 <10 <10 <10 <10 180 TPH – C10-C16 <50 <50 <50 <50 <50 <50 <50 120 TPH – C16-C34 <100 <100 <100 <100 <100 <100 <100 1300 TPH – C34-C40 <100 <100 <100 <100 <100 <100 <100 5600

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6. Laboratory Analysis – Salinity / Aggressivity Seven (7) screening tests were collected as a part of this assessment in order to gain a view on the risk of saline soils. This assessments is based on the booklet “Site Investigations for Urban Salinity” published by Department of Land and Water Conservation 2002, AS2870 Residential Slabs and Footings and AS2159:2009 Piling – Design and Installation Guidelines

Table 2: Analysis of the Soil Samples (Salinity) Sample EC

µS/cm Texture Factor ECe Salinity Class

E1 17 10 0.17 Non Saline

E2 17 10 0.17 Non Saline

E3 20 10 0.20 Non Saline

E4 18 10 0.18 Non Saline

E5 24 10 0.24 Non Saline

E6 30 10 0.30 Non Saline

E7 41 10 0.41 Non Saline

Table 11: Analysis of the Soil Samples (Aggressiveness)

Sample pH Chloride Sulphate Resistivity Aggressivity to Concrete

Aggressivity to Steel pH Units mg/kg mg/kg Ohm.cm

E1 7.2 <10 <10 58800 Non Aggressive Non Aggressive E2 7.4 <10 <10 58800 Non Aggressive Non Aggressive E3 7.7 <10 <10 50000 Non Aggressive Non Aggressive E4 7.7 <10 <10 55600 Non Aggressive Non Aggressive E5 7.6 10 <10 41700 Non Aggressive Non Aggressive E6 7.6 10 <10 33300 Non Aggressive Non Aggressive E7 7.5 10 <10 24400 Non Aggressive Non Aggressive

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7. Conclusion

Based on visual observations and laboratory analysis, the material from the exposed trenches appears to be naturally occurring and free from foreign material as no suspicious odours or obvious signs of contamination were observed. Hence the material on the above site is classified as virgin excavated natural material (VENM) for future use; since it is in accordance with the definition of VENM given under the Protection of the Environments Operations Act 1997 as outlined below: ‘Natural material (such as clay, gravel, sand, soil or rock fines):

• That has been excavated or quarried from areas that are not contaminated with manufactured chemicals or process residues, as a result of industrial, commercial, mining or agricultural activities, and

• That does not contain any sulfidic ores or soils or any other waste.’ The electrical conductivity results indicate that the soil salinity is non saline. The laboratory test values of sulphates, chlorides and pH indicate that the soil is non aggressive to both steel and concrete. For and on behalf of Ground Technologies Pty Ltd

Reviewed By

J.George A.Bennett Environmental Engineer Principal Geotechnical Engineer

Attachment: Certificate of Analysis ES1808431

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APPENDIX A LABORATORY TEST RESULTS

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0 0.00 True

Environmental

CERTIFICATE OF ANALYSISWork Order : Page : 1 of 9ES1808431

:: LaboratoryClient GROUND TECHNOLOGIES Environmental Division Sydney

: :ContactContact MR ANTHONY BENNETT Customer Services ES

:: AddressAddress 16 Weld Street

PRESTONS NSW, AUSTRALIA 2170

277-289 Woodpark Road Smithfield NSW Australia 2164

:Telephone +61 02 8783 8200 :Telephone +61-2-8784 8555

:Project GTE1544, Greystanes Date Samples Received : 20-Mar-2018 11:45

:Order number Date Analysis Commenced : 22-Mar-2018

:C-O-C number ---- Issue Date : 29-Mar-2018 10:55

Sampler : JASMINE GEORGE

Site : ----

Quote number : EN/222/17

7:No. of samples received

7:No. of samples analysed

This report supersedes any previous report(s) with this reference. Results apply to the sample(s) as submitted. This document shall not be reproduced, except in full.

This Certificate of Analysis contains the following information:

l General Comments

l Analytical Results

l Surrogate Control Limits

Additional information pertinent to this report will be found in the following separate attachments: Quality Control Report, QA/QC Compliance Assessment to assist with

Quality Review and Sample Receipt Notification.

SignatoriesThis document has been electronically signed by the authorized signatories below. Electronic signing is carried out in compliance with procedures specified in 21 CFR Part 11.

Signatories Accreditation CategoryPosition

Ankit Joshi Inorganic Chemist Sydney Inorganics, Smithfield, NSW

Edwandy Fadjar Organic Coordinator Sydney Inorganics, Smithfield, NSW

Edwandy Fadjar Organic Coordinator Sydney Organics, Smithfield, NSW

Raymond Commodore Instrument Chemist Sydney Inorganics, Smithfield, NSW

R I G H T S O L U T I O N S | R I G H T P A R T N E R

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General Comments

The analytical procedures used by the Environmental Division have been developed from established internationally recognized procedures such as those published by the USEPA, APHA, AS and NEPM. In house

developed procedures are employed in the absence of documented standards or by client request.

Where moisture determination has been performed, results are reported on a dry weight basis.

Where a reported less than (<) result is higher than the LOR, this may be due to primary sample extract/digestate dilution and/or insufficient sample for analysis.

Where the LOR of a reported result differs from standard LOR, this may be due to high moisture content, insufficient sample (reduced weight employed) or matrix interference.

When sampling time information is not provided by the client, sampling dates are shown without a time component. In these instances, the time component has been assumed by the laboratory for processing

purposes.

Where a result is required to meet compliance limits the associated uncertainty must be considered. Refer to the ALS Contact for details.

CAS Number = CAS registry number from database maintained by Chemical Abstracts Services. The Chemical Abstracts Service is a division of the American Chemical Society.

LOR = Limit of reporting

^ = This result is computed from individual analyte detections at or above the level of reporting

ø = ALS is not NATA accredited for these tests.

~ = Indicates an estimated value.

Key :

Benzo(a)pyrene Toxicity Equivalent Quotient (TEQ) is the sum total of the concentration of the eight carcinogenic PAHs multiplied by their Toxicity Equivalence Factor (TEF) relative to Benzo(a)pyrene. TEF values

are provided in brackets as follows: Benz(a)anthracene (0.1), Chrysene (0.01), Benzo(b+j) & Benzo(k)fluoranthene (0.1), Benzo(a)pyrene (1.0), Indeno(1.2.3.cd)pyrene (0.1), Dibenz(a.h)anthracene (1.0),

Benzo(g.h.i)perylene (0.01). Less than LOR results for 'TEQ Zero' are treated as zero, for 'TEQ 1/2LOR' are treated as half the reported LOR, and for 'TEQ LOR' are treated as being equal to the reported LOR.

Note: TEQ 1/2LOR and TEQ LOR will calculate as 0.6mg/Kg and 1.2mg/Kg respectively for samples with non-detects for all of the eight TEQ PAHs.

l

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Analytical Results

E5E4E3E2E1Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

20-Mar-2018 00:0020-Mar-2018 00:0020-Mar-2018 00:0020-Mar-2018 00:0020-Mar-2018 00:00Client sampling date / time

ES1808431-005ES1808431-004ES1808431-003ES1808431-002ES1808431-001UnitLORCAS NumberCompound

Result Result Result Result Result

EA002 : pH (Soils)

7.2 7.4 7.7 7.7 7.6pH Unit0.1----pH Value

EA010: Conductivity

17 17 20 18 24µS/cm1----Electrical Conductivity @ 25°C

EA055: Moisture Content (Dried @ 105-110°C)

6.6 5.7 5.2 2.8 2.8%1.0----Moisture Content

EA080: Resistivity

58800 58800 50000 55600 41700ohm cm1----Resistivity at 25°C

ED040S : Soluble Sulfate by ICPAES

<10Sulfate as SO4 2- <10 <10 <10 <10mg/kg1014808-79-8

ED045G: Chloride by Discrete Analyser

<10Chloride <10 <10 <10 10mg/kg1016887-00-6

EG005T: Total Metals by ICP-AES

<5Arsenic <5 <5 <5 <5mg/kg57440-38-2

<1Cadmium <1 <1 <1 <1mg/kg17440-43-9

10Chromium 5 10 4 8mg/kg27440-47-3

108Copper 84 81 29 70mg/kg57440-50-8

<5Lead <5 <5 <5 <5mg/kg57439-92-1

29Nickel 15 24 6 24mg/kg27440-02-0

27Zinc 16 21 33 20mg/kg57440-66-6

EG035T: Total Recoverable Mercury by FIMS

<0.1Mercury <0.1 <0.1 <0.1 <0.1mg/kg0.17439-97-6

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons

<0.5Naphthalene <0.5 <0.5 <0.5 <0.5mg/kg0.591-20-3

<0.5Acenaphthylene <0.5 <0.5 <0.5 <0.5mg/kg0.5208-96-8

<0.5Acenaphthene <0.5 <0.5 <0.5 <0.5mg/kg0.583-32-9

<0.5Fluorene <0.5 <0.5 <0.5 <0.5mg/kg0.586-73-7

<0.5Phenanthrene <0.5 <0.5 <0.5 <0.5mg/kg0.585-01-8

<0.5Anthracene <0.5 <0.5 <0.5 <0.5mg/kg0.5120-12-7

<0.5Fluoranthene <0.5 <0.5 <0.5 <0.5mg/kg0.5206-44-0

<0.5Pyrene <0.5 <0.5 <0.5 <0.5mg/kg0.5129-00-0

<0.5Benz(a)anthracene <0.5 <0.5 <0.5 <0.5mg/kg0.556-55-3

<0.5Chrysene <0.5 <0.5 <0.5 <0.5mg/kg0.5218-01-9

<0.5Benzo(b+j)fluoranthene <0.5 <0.5 <0.5 <0.5mg/kg0.5205-99-2 205-82-3

<0.5Benzo(k)fluoranthene <0.5 <0.5 <0.5 <0.5mg/kg0.5207-08-9

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Analytical Results

E5E4E3E2E1Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

20-Mar-2018 00:0020-Mar-2018 00:0020-Mar-2018 00:0020-Mar-2018 00:0020-Mar-2018 00:00Client sampling date / time

ES1808431-005ES1808431-004ES1808431-003ES1808431-002ES1808431-001UnitLORCAS NumberCompound

Result Result Result Result Result

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons - Continued

<0.5Benzo(a)pyrene <0.5 <0.5 <0.5 <0.5mg/kg0.550-32-8

<0.5Indeno(1.2.3.cd)pyrene <0.5 <0.5 <0.5 <0.5mg/kg0.5193-39-5

<0.5Dibenz(a.h)anthracene <0.5 <0.5 <0.5 <0.5mg/kg0.553-70-3

<0.5Benzo(g.h.i)perylene <0.5 <0.5 <0.5 <0.5mg/kg0.5191-24-2

<0.5^ <0.5 <0.5 <0.5 <0.5mg/kg0.5----Sum of polycyclic aromatic hydrocarbons

<0.5^ <0.5 <0.5 <0.5 <0.5mg/kg0.5----Benzo(a)pyrene TEQ (zero)

0.6^ 0.6 0.6 0.6 0.6mg/kg0.5----Benzo(a)pyrene TEQ (half LOR)

1.2^ 1.2 1.2 1.2 1.2mg/kg0.5----Benzo(a)pyrene TEQ (LOR)

EP080/071: Total Petroleum Hydrocarbons

<10 <10 <10 <10 <10mg/kg10----C6 - C9 Fraction

<50 <50 <50 <50 <50mg/kg50----C10 - C14 Fraction

<100 <100 <100 <100 <100mg/kg100----C15 - C28 Fraction

<100 <100 <100 <100 <100mg/kg100----C29 - C36 Fraction

<50^ <50 <50 <50 <50mg/kg50----C10 - C36 Fraction (sum)

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions

<10C6 - C10 Fraction <10 <10 <10 <10mg/kg10C6_C10

<10^ C6 - C10 Fraction minus BTEX

(F1)

<10 <10 <10 <10mg/kg10C6_C10-BTEX

<50 <50 <50 <50 <50mg/kg50---->C10 - C16 Fraction

<100 <100 <100 <100 <100mg/kg100---->C16 - C34 Fraction

<100 <100 <100 <100 <100mg/kg100---->C34 - C40 Fraction

<50^ <50 <50 <50 <50mg/kg50---->C10 - C40 Fraction (sum)

<50^ <50 <50 <50 <50mg/kg50---->C10 - C16 Fraction minus Naphthalene

(F2)

EP080: BTEXN

<0.2Benzene <0.2 <0.2 <0.2 <0.2mg/kg0.271-43-2

<0.5Toluene <0.5 <0.5 <0.5 <0.5mg/kg0.5108-88-3

<0.5Ethylbenzene <0.5 <0.5 <0.5 <0.5mg/kg0.5100-41-4

<0.5meta- & para-Xylene <0.5 <0.5 <0.5 <0.5mg/kg0.5108-38-3 106-42-3

<0.5ortho-Xylene <0.5 <0.5 <0.5 <0.5mg/kg0.595-47-6

<0.2^ <0.2 <0.2 <0.2 <0.2mg/kg0.2----Sum of BTEX

<0.5^ <0.5 <0.5 <0.5 <0.5mg/kg0.5----Total Xylenes

<1Naphthalene <1 <1 <1 <1mg/kg191-20-3

EP075(SIM)S: Phenolic Compound Surrogates

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Analytical Results

E5E4E3E2E1Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

20-Mar-2018 00:0020-Mar-2018 00:0020-Mar-2018 00:0020-Mar-2018 00:0020-Mar-2018 00:00Client sampling date / time

ES1808431-005ES1808431-004ES1808431-003ES1808431-002ES1808431-001UnitLORCAS NumberCompound

Result Result Result Result Result

EP075(SIM)S: Phenolic Compound Surrogates - Continued

83.4Phenol-d6 75.3 79.2 76.4 77.8%0.513127-88-3

82.02-Chlorophenol-D4 77.1 86.4 76.5 81.8%0.593951-73-6

63.42.4.6-Tribromophenol 51.0 58.8 51.0 48.8%0.5118-79-6

EP075(SIM)T: PAH Surrogates

88.82-Fluorobiphenyl 73.2 88.1 88.3 86.6%0.5321-60-8

97.3Anthracene-d10 89.0 96.9 96.5 96.1%0.51719-06-8

96.44-Terphenyl-d14 94.0 113 97.1 83.1%0.51718-51-0

EP080S: TPH(V)/BTEX Surrogates

99.21.2-Dichloroethane-D4 105 99.6 101 86.4%0.217060-07-0

105Toluene-D8 113 107 108 110%0.22037-26-5

97.84-Bromofluorobenzene 103 98.0 99.2 107%0.2460-00-4

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Analytical Results

------------E7E6Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

------------20-Mar-2018 00:0020-Mar-2018 00:00Client sampling date / time

------------------------ES1808431-007ES1808431-006UnitLORCAS NumberCompound

Result Result ---- ---- ----

EA002 : pH (Soils)

7.6 7.5 ---- ---- ----pH Unit0.1----pH Value

EA010: Conductivity

30 41 ---- ---- ----µS/cm1----Electrical Conductivity @ 25°C

EA055: Moisture Content (Dried @ 105-110°C)

3.6 5.3 ---- ---- ----%1.0----Moisture Content

EA080: Resistivity

33300 24400 ---- ---- ----ohm cm1----Resistivity at 25°C

ED040S : Soluble Sulfate by ICPAES

<10Sulfate as SO4 2- <10 ---- ---- ----mg/kg1014808-79-8

ED045G: Chloride by Discrete Analyser

10Chloride 10 ---- ---- ----mg/kg1016887-00-6

EG005T: Total Metals by ICP-AES

<5Arsenic <5 ---- ---- ----mg/kg57440-38-2

<1Cadmium <1 ---- ---- ----mg/kg17440-43-9

6Chromium 11 ---- ---- ----mg/kg27440-47-3

41Copper 60 ---- ---- ----mg/kg57440-50-8

<5Lead <5 ---- ---- ----mg/kg57439-92-1

12Nickel 23 ---- ---- ----mg/kg27440-02-0

23Zinc 30 ---- ---- ----mg/kg57440-66-6

EG035T: Total Recoverable Mercury by FIMS

<0.1Mercury <0.1 ---- ---- ----mg/kg0.17439-97-6

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons

<0.5Naphthalene <0.5 ---- ---- ----mg/kg0.591-20-3

<0.5Acenaphthylene <0.5 ---- ---- ----mg/kg0.5208-96-8

<0.5Acenaphthene <0.5 ---- ---- ----mg/kg0.583-32-9

<0.5Fluorene <0.5 ---- ---- ----mg/kg0.586-73-7

<0.5Phenanthrene <0.5 ---- ---- ----mg/kg0.585-01-8

<0.5Anthracene <0.5 ---- ---- ----mg/kg0.5120-12-7

<0.5Fluoranthene <0.5 ---- ---- ----mg/kg0.5206-44-0

<0.5Pyrene <0.5 ---- ---- ----mg/kg0.5129-00-0

<0.5Benz(a)anthracene <0.5 ---- ---- ----mg/kg0.556-55-3

<0.5Chrysene <0.5 ---- ---- ----mg/kg0.5218-01-9

<0.5Benzo(b+j)fluoranthene <0.5 ---- ---- ----mg/kg0.5205-99-2 205-82-3

<0.5Benzo(k)fluoranthene <0.5 ---- ---- ----mg/kg0.5207-08-9

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Analytical Results

------------E7E6Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

------------20-Mar-2018 00:0020-Mar-2018 00:00Client sampling date / time

------------------------ES1808431-007ES1808431-006UnitLORCAS NumberCompound

Result Result ---- ---- ----

EP075(SIM)B: Polynuclear Aromatic Hydrocarbons - Continued

<0.5Benzo(a)pyrene <0.5 ---- ---- ----mg/kg0.550-32-8

<0.5Indeno(1.2.3.cd)pyrene <0.5 ---- ---- ----mg/kg0.5193-39-5

<0.5Dibenz(a.h)anthracene <0.5 ---- ---- ----mg/kg0.553-70-3

<0.5Benzo(g.h.i)perylene <0.5 ---- ---- ----mg/kg0.5191-24-2

<0.5^ <0.5 ---- ---- ----mg/kg0.5----Sum of polycyclic aromatic hydrocarbons

<0.5^ <0.5 ---- ---- ----mg/kg0.5----Benzo(a)pyrene TEQ (zero)

0.6^ 0.6 ---- ---- ----mg/kg0.5----Benzo(a)pyrene TEQ (half LOR)

1.2^ 1.2 ---- ---- ----mg/kg0.5----Benzo(a)pyrene TEQ (LOR)

EP080/071: Total Petroleum Hydrocarbons

<10 <10 ---- ---- ----mg/kg10----C6 - C9 Fraction

<50 <50 ---- ---- ----mg/kg50----C10 - C14 Fraction

<100 <100 ---- ---- ----mg/kg100----C15 - C28 Fraction

<100 <100 ---- ---- ----mg/kg100----C29 - C36 Fraction

<50^ <50 ---- ---- ----mg/kg50----C10 - C36 Fraction (sum)

EP080/071: Total Recoverable Hydrocarbons - NEPM 2013 Fractions

<10C6 - C10 Fraction <10 ---- ---- ----mg/kg10C6_C10

<10^ C6 - C10 Fraction minus BTEX

(F1)

<10 ---- ---- ----mg/kg10C6_C10-BTEX

<50 <50 ---- ---- ----mg/kg50---->C10 - C16 Fraction

<100 <100 ---- ---- ----mg/kg100---->C16 - C34 Fraction

<100 <100 ---- ---- ----mg/kg100---->C34 - C40 Fraction

<50^ <50 ---- ---- ----mg/kg50---->C10 - C40 Fraction (sum)

<50^ <50 ---- ---- ----mg/kg50---->C10 - C16 Fraction minus Naphthalene

(F2)

EP080: BTEXN

<0.2Benzene <0.2 ---- ---- ----mg/kg0.271-43-2

<0.5Toluene <0.5 ---- ---- ----mg/kg0.5108-88-3

<0.5Ethylbenzene <0.5 ---- ---- ----mg/kg0.5100-41-4

<0.5meta- & para-Xylene <0.5 ---- ---- ----mg/kg0.5108-38-3 106-42-3

<0.5ortho-Xylene <0.5 ---- ---- ----mg/kg0.595-47-6

<0.2^ <0.2 ---- ---- ----mg/kg0.2----Sum of BTEX

<0.5^ <0.5 ---- ---- ----mg/kg0.5----Total Xylenes

<1Naphthalene <1 ---- ---- ----mg/kg191-20-3

EP075(SIM)S: Phenolic Compound Surrogates

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Analytical Results

------------E7E6Client sample IDSub-Matrix: SOIL

(Matrix: SOIL)

------------20-Mar-2018 00:0020-Mar-2018 00:00Client sampling date / time

------------------------ES1808431-007ES1808431-006UnitLORCAS NumberCompound

Result Result ---- ---- ----

EP075(SIM)S: Phenolic Compound Surrogates - Continued

73.2Phenol-d6 75.8 ---- ---- ----%0.513127-88-3

74.82-Chlorophenol-D4 76.1 ---- ---- ----%0.593951-73-6

47.82.4.6-Tribromophenol 47.1 ---- ---- ----%0.5118-79-6

EP075(SIM)T: PAH Surrogates

75.62-Fluorobiphenyl 73.9 ---- ---- ----%0.5321-60-8

87.9Anthracene-d10 89.0 ---- ---- ----%0.51719-06-8

93.04-Terphenyl-d14 104 ---- ---- ----%0.51718-51-0

EP080S: TPH(V)/BTEX Surrogates

1081.2-Dichloroethane-D4 94.6 ---- ---- ----%0.217060-07-0

106Toluene-D8 101 ---- ---- ----%0.22037-26-5

95.54-Bromofluorobenzene 92.7 ---- ---- ----%0.2460-00-4

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Surrogate Control Limits

Recovery Limits (%)Sub-Matrix: SOIL

Compound CAS Number Low High

EP075(SIM)S: Phenolic Compound Surrogates

Phenol-d6 13127-88-3 63 123

2-Chlorophenol-D4 93951-73-6 66 122

2.4.6-Tribromophenol 118-79-6 40 138

EP075(SIM)T: PAH Surrogates

2-Fluorobiphenyl 321-60-8 70 122

Anthracene-d10 1719-06-8 66 128

4-Terphenyl-d14 1718-51-0 65 129

EP080S: TPH(V)/BTEX Surrogates

1.2-Dichloroethane-D4 17060-07-0 73 133

Toluene-D8 2037-26-5 74 132

4-Bromofluorobenzene 460-00-4 72 130