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NAM E

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10 7 . 848 1 1 . 50880E+01 2 .39250E-02 ACENAPHTHEN E11 12 .510 1 1 . 50000E+01 2 .46750E-02 ANTHRACENE.12 28 . 7 48 1 1 . 50000E+01 2 . 98,580E-82 CHRYSEN E13 2_ .830 1 6 .eO800E+00 3 .51-750E-02 BENZ(B)FLUOR

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LIST DIET I TEM PDET 1 TE MP'=348°C ,ETF'T= 340° E

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1990 .'

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HDMSe00037560

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15 :10 MAR 89 198 2

RT AREA T`i'PE CAL AMOUNT NAME

0.34 16 0 a"1 til8 E 06811 .55 1 7 . 08 88 0.11318 .02 233 .95 EH 1;.578

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RT AREA TYPE CAL AMUL1 T NAM E

88 1059 4 .9507 . 45 455 .92 SY 2 4 .285 FiCENAPHTHYL E

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£hP3 5888 MANURL INJECTION @ 16 :50 MAR 8, 1942 .-+'- DUPLICATE A

'ESQID COMPENSATED ANALYSI S

RT AREA TYPE CAL AMOUNT NAME .

0 .34 179400e .00 BV 11$48 .4 k0 .53 16.8'9 .12 vv 1c+ ,

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11 .03 2 .46 BB 1 .621E-0211 .54 2'9 .10 68 0 .19211 .86 12 .36 G B 8 . 151E-0214 4 .16 Be 2 . 746E-0214 .31 15 .40 6B 0 .10214 .40 12 .41 BB 8 . 180E-@216 .16 45 .50 B6 0 .300

17 .09 3 .3 .53 BP 0 .224 PYRENE

17 .47 20 .21 PP 0 . 13317 .81 .5- P6 i . 674E-8218 .43 49 .56 BY 0 .330

18 .69 21 .76 V P 0 .15019 .56 196 .39 PV 1 .29628 .38 10.3 . vv 0 .68620 .73 173 . y r, V B 1 576 CHRYSEN E21 .21 14 .2'151 E',T , 485E-0221 .47 65 .50 V13V 0 .43221 .84 40 .54 '.1P 0 .268

MULTIPLIER = 0 .2

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LIT RE POR T£hP•3 5830A MANUAL INJ, EC T IOH 0d 1r~~ 50 MAR 8n 19822-47-82, DUPLICATE RESTD COMPENSATED ANALYSI S

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HDMSe00037563

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08 :30 OVEN TEMP 10 0

AVAILABLE MEMCIR'i C B''i` T E'3 ? : 18304

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CLOCK TIME 530 1 TEMP ON

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CLOCK TIME 640 DETECTOR B 171 ri

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AVAILABLE MEMORY (BYTES : 182-72,

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RT AREA TYPE CAL 1 1 E a fl f'1 E

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9 . ?7 1225 . 06 BB 3 FLUEHE

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LIST REPOR TKhPI 5880A MANUAL2 IJL STD #1

@ Of" : 39 MAR 9a 1982

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9-

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R.EL RLI E

LIST REPOR TChP1 5 8 A MANUAL INJECTION L 87 :39 r1 RR 91 19822 UL :STD # 1ESTD COMPENSATED ANALYSI S

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0 .33 17919413 0O BB 59134 .8803 .43 943 . 90 BB 1 40 .000 HAPRTh..ALLNE7 . 39 103t, . 85 BY 2 4 +, ► A-10 ACENAPHTHYLE

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1 4 .4~ . . ., _ 54 411 1 1 . 8 81 .35 200 .261 .67 149 . 255 .50 189 . e 77.41 359.57

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2 .86 14" .7 43.+df 343 . 5 1 124 . 78. . .

.3 .67 7 ` .5 13.89 79.864. i5 Q .9 15. ill. 1 1 4 . 466 . 35 .:.4 . 9e-,,60 1 08' - 7 3

9 .38 ;F. . 7 5

9 94 22. . 7 210.79 163.3 .318.51 69.99

MULTIPLIER 3 . 2

EDT CEtLIE: --4 HERDING

--49- 2

2--51-2

.5 1

OWNED BY C

HDMSe0003757 4

AMOUNT NrM E

1 .9 3 6J . J L

5 .11 91 .999

Vv lvv . 83Vt k3 . 942VP w? . 3 r ri

PV 1 1 . 1361vv 0. 525

VV 0 .755BV 1. 558VV 0.71lip 13. 583PV 3 2.330 FLUOREHEVP 1.470Pe ` . 6E;B 6.46.E

;ETPT=183t;C Li. N1II' = 330 C

r 22 . 723 .4 3

F ,,T : :.-T i OP RU N

K ,r7 cSBOA MANUAL ? f-l .JECTIOR . i ; 1 NOR 9 191

E' TD COMP ENSATE D ANALYSI S

R T AREA T "(PE '-PL RMcl Y .H T NAM E

3 .45 1054 . 06 V,'"Y 1 . .'•? NNNAAPHufu, .

4 . 00 7018 . 9 .3 W 5 . 2'i7

4 . 60 3 7 Fri . 6 1 W'V 2 . 4464 .79 445 . 68 v 9425 .11 231 .62 Y# 1 . 5305 .31 199 .63 YB 1 . 3 1 86 .21 344 .37 v Ya - . 27'y

6 .51 531 .45 Y V 3 .5086 .88 245 .1 YP 1 . 618 t

7 .63 55 . 7w PV X3 .3747 .96 185 . 79 VV 10 1 .184 RCENAF : 4THEN E_ .94 61 .70 PV 0 .4079 .38 172 .23 YY I .1aS FLUOREtIL.

9 .85 55. . 1 0 YP 8. 37 410.85

11 .345

156 .74PV

VP

0 .45 21 . 03 5

12 .35 280 .75 r8 4 1 .834 PHEHAHTHREH E13 .87 38 4 .56 vv 2 .53 814 .14 128 .18 vv 0.84614 .62 88 .17 VV' 0 . 5~3

5 . 9t 257 5 =1Y 1 , ? o

15 .29 123 .39 vv 0 .81 415 . 54 107 . : 5 VV 0 . 71 216 .78 126 52 BY 0 .791 PYRENE17 .48 120 .04 EP 0 .79218 .17 1 19 . 22 PV 0 . 78718 .48 247 .11 VP 1 .63 119 .4 720 .33

199 . 8 3179 .41

P BBY

1 .31 91 . 082 BE ly"i

21 .37 89 . 6 1 BE 0 .59 122 .71 92 .32 Be

MULTIP LIER t 0

LI OVEN T E'I POVEN TE M P=10t0 9ETPT=10@"C LIMIT = 330 0 C

EDIT C i -4

-4 HEADING,

2-52-8-22

e

ri

0

HDMSe00037575

Ao- j,L TE D

UN'LI TFiE.LE c;ETPCIIHT

~JFdL1 YTN SETPOIN

Tt, Mr,

RUN TIME = 31 .0 ci'- 30 .k-,,Q MIN'T : STOP RU N

[hP] 5880A MHk4URL INJECTION @ 1.4 :25 NA P2-52-82ESTD COMPENSATED Hi'(AL 'S-I Si

AREJ € `iFE CAL r!t'4U!E I4 T

.t, 61 .4 17 0.4065 .19 101 .75 vv 0 .67 25 . 36 '0 .70 IV .€ 0 .59 95 . r€ . VV 0 . 4506 .29 75 .06 vv 0 . 495- .87 226 . vv 1 . 505

cis 55 . 48 0 . 3667 .8.1 vv i0t 0 .51 85 .1i3 5 . 1 vv 0 .3953 .95 6t• . I pp 0 .4379 .39 109 .66 Py 3 0 .71 7

10 . S3 tE1 _Aq Lad

9 . 1582

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23 .43

ACE dHFHTHENL

FLUUREHE

HDMSe00037576

15 . Ct n. . . -i 19, 1 4 ~, ~'f

15 .57 . 6o . 39 111 P

16 .7417 .43 50 .83 S

6 V15 .44 204 .1'3 V P19,47 60 .00 S F23 .35 224 .48 E `r.

20 .73 1 •t . ~ 5

vv1 2

198',,3 :1

91 . re

MULTIPLIER: 13 .2

OVEN TEMP POST VALUE.OVEN TEMP POST TIME 0

OVEN TEMP POST TIME 5

E: 3

! 59 5

0 .3-1:11 9

1

1 5°9

L I :ST AL ;r; 2 TEM PAUX 2 TEMP=340C :SETPT=13G'E- ; L=P? : INIT=4€o50 c

LIST AU ;; 1 TL 1PALl. i D-C SETPT='. 1U^C:(CIPP ) _ii1IT C:

START

READY FOR INJECTIO N

SIGNALLIST Ft u„ : TEMPA112 TEND=4S'E__ SETF'T-SU ,D C(O1FF .) LIMIT=405`} C

START

READ ;' FOR INJECTION

LIST OVEN TEMP LIt`Ii T'P ERRO : "EHT_F:" f<= :E'V EXPECTED

LIST OVEN TEMP POST VALU EOVEN TEMP POST VALUE 320"'C

LIST OVEN TEMP POST TIM EOVEN TEMP POST TIME 5 .01 MJI F

LIST RLI~; 2 TEM PAUX 2 TEMP=640C SETPT E.F-i .C OFF LIMIT=415-tC

EDIT CALIS - 4-4 HEADING

2-52 .322-50-S2

LIST : EM TEt 1OVEN T Er1P =1o0_•G -~ETPT 1 ^C LIMY T=3310x

-~-w • .

yr

HDMSe00037577

21 .4 3

23 .53

Ri : STOP RUIA

ItiPI 5880A MANUFL INJECTIONSO-02

ESTD COMFEU -FTED ANiLYSI ;

3 .203 .473 . 73

4 . -"

4 .564 .925 .215 .746 .2511, .87

185121 .43

E 17 . 20

te1949 .72

705 .072189 .95

1444 .32

2109 .531356 .39G 10 i 28

2226 .102154 . ?p:

2590 .1 2

79 .2566 . i 2

MULTIP LIER = 0 .2

5 .39416 .576 NAF'HTHi L E.NE.

4 .65 314 .454

9 .53313 . 92 3

8 .952

13 .908

14 .692

14 .222417 .0950 .5230 .43 6

(OFF) LIMIT =4 0 5"C:

LIST OVEN TEM POVEN TEMP = 328 °C SETPT =32@cG LIMIT=33@°c

HDMSe0003757 8

AU> 2 TEMP=6 "F: _ETPT= 8'=C < O

18 .51

5 ;45 MAR 9 s 19$2

,ETI- ! _ i ,C[ iJFF :- LIMIT= 4I 5 C

EDIT CALIE; --4 HEAD I14 C

2-5a-82

14 . CC1'4 .E ~

1 RT : S, TOP FW-H

141 58B 0 A NAHUAL INJECTION @ 1E. :31 MAR 9~ 1982METHOD ABORTE DAREA COMPENSATED ANALYSI S

TOTAL AREA = .00MULTIPLIER = @ . L

EDIT CALK--4 HEA DiFaso

HDMSe0003757 9

2-43-82

RUN TIME = 330 a 65 MI N

P NSTBRPRBUST TIME + .0 .O8 MI MM

[hp7 5880A MAN UAL IM ..1ECTIOM @ 17-15 MAR 1METHOD ABDRTE DAREA COMPEN5-ATED SALE _;

RT AREA TYPE AREAi %

OVEN TEMP POST TINE 5

LI°= T

OVEN TEMP=24 C LSE i F i ,Ln-

:C L101-1=7-.300CECUIO TIME = 3 .00 MI N

OVEN T EMP PRO FILE : AHNUTAT10€ 4 €O1FF )INITIAL VALUE = 111 =r~INITIAL TIME = 0 . €P,3 MI NLEVEL I

FRGF1 RATE i•iIt t lFINA LFINAL

VALU ETIME = 3t . r•_1U M I N

POST VALUE = 32000POST TIME = 5 .00 MIN

HDMSe00037580

IT~FC i n '4 3 i_ _,ET , 40l:T ~

3•j.L 2 E 3't e-I49 :~,_: '3ETPT =1 ScC CIFF !

]J-4J I TEMP E C SETV`T=28 0 : C• L_ 11 i T=4E1Lj" L CO

1NJ 2 TEMP=16r c '3ETPT=l00'C OFF) LIMIT=405"CFUX 1 TEHP=Grf.: SETPT 21 ;0°CE;OFF? LIMIT=40540FiU ; 2 TEHP-1304 SETPT=2.0'C'CoFF ;F WMIT=4050C

DEVICE Z- G ; ERMIHAL I r

CHART SPEED _ 0 .50 CM'MIt!AATTH = 2T:OFD SET 10ZERO = 8 .7 3

E I T

LIST DETECTOR BDETECTOR E: FLAME IONIZATION

CALIBRATION : H=1 44443 10. L1=i3751 S

LIST PEAK: WIDTHPEAK WIDTH =

LI'T THRESHOLDTHRESHOLD = 4

O'v E N TEMP 25

LIST RUN TBLRUN TABLE :

32 .00 STOP

AVAILABLE 01EMOR-`l' (BYTES) 19136

LIST REPORT TBLREPORT TABLE

L2 ~- 1376

0 . 00 RE UL- €" !E+073 .00 REJECT 50

A'VAILA8L E MEMORY (eYTES) : 19136

LI'= ICALI BCAL

CALI BTABLE. :

F:T LEVEL AMT RMT'FwREA REF NAM E

1 3 .4E.9 1 . F=jRt000E+01 4 .25126E-02 NAPHTHALEN E2 7 .432. 1 4 . 0000E+01 3 .85778E-02 ACEHAPHTNYI-E3 9 .342 1 4 .OEt00OE+0 1 3 .26514E-02 FLUOREI4 E4 12 .385 1 4 .00000E+01 6625E-02 PHEN'ANTHREI1 E5 16 .774 i 4 .0000@E+01 3 . 12520E-02 PYRENE

20 .55;7 1 4 . OO00E•€ 1 3 . 01638E-02 BENZ<AkHr-4TH .7 2 + 24 .739 1 4 . 00000E 01 3 . 52 9.59E-02 BEHZ ( R)PY R8 28 .02 : 1 4 .00000E+01 95086. E;-92 DIBEN(AH?AM T9 28 .911 1 4 . i304 £~E+€~i1 3 .31863F--02 8EN(H 1 ) PER

10 7 .840 1 1 . 50U80E+01 3 .18711E-02 ACEHAPHTHEM Ei 12 . 510 1 1 .50080E+01 20358E--02 ANTHPACEH E

12 20 .740 F 1 .50000E+61 4 . OOSOO L-02 CHRY SSEU E13 1 6 .0000@E+00 4 . 01 .339E--02 BENZ(B ) FLUO R

L.ALIB PFiPAIIS :0 MULTIPLIER = 0 .2I O'FF w TFifif41 = ;4 -

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HDMSe00037581

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AVAILfELE MEMIQRY :BE) : 191 :F6.v I

DET I TEM P OFF

HDMSe00037582`

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LF _ . .ft{

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L 1

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P= 4 o

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F'TE11 c':I_rF' t lr'MIT= 4

F T= - C, 1 .-FF.' =40Z. TF . L''}€ (TIFF? (L i.MI =4 i 5

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L_ 1 . T IHL I B -AE:L E

11 PF` ~''1 = ;_rv,rn1

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f'i .H 1 rE R

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HDMSe00037584

L E:T LEVEL F+MM T

5 . F~ 1 F_31_1 0 E +L7 1

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1 E1 . 208 1 F . E~i~iFi}'~1~ E+01

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WINDOW =

r- E 1f'RY 2 , T

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7 . JJL J _ E-

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