hnmr spectrum of stage-1 - royal society of chemistry · 2018-04-19 · of 0265/c01/e00502/005 in...
TRANSCRIPT
![Page 1: HNMR Spectrum of Stage-1 - Royal Society of Chemistry · 2018-04-19 · of 0265/C01/E00502/005 in DMSO-d6 Released on 70 60 20 10 O ppm 100 90 30 160 150 50 40 30 140 130 120 110](https://reader033.vdocument.in/reader033/viewer/2022060217/5f064f6a7e708231d4175a00/html5/thumbnails/1.jpg)
1HNMR Spectrum of Stage-1
Electronic Supplementary Material (ESI) for RSC Advances.This journal is © The Royal Society of Chemistry 2018
![Page 2: HNMR Spectrum of Stage-1 - Royal Society of Chemistry · 2018-04-19 · of 0265/C01/E00502/005 in DMSO-d6 Released on 70 60 20 10 O ppm 100 90 30 160 150 50 40 30 140 130 120 110](https://reader033.vdocument.in/reader033/viewer/2022060217/5f064f6a7e708231d4175a00/html5/thumbnails/2.jpg)
13CNMR Spectrum of Stage-1
![Page 3: HNMR Spectrum of Stage-1 - Royal Society of Chemistry · 2018-04-19 · of 0265/C01/E00502/005 in DMSO-d6 Released on 70 60 20 10 O ppm 100 90 30 160 150 50 40 30 140 130 120 110](https://reader033.vdocument.in/reader033/viewer/2022060217/5f064f6a7e708231d4175a00/html5/thumbnails/3.jpg)
Mass spectrum of Stage-1
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DSC Thermogram of Stage-1
![Page 5: HNMR Spectrum of Stage-1 - Royal Society of Chemistry · 2018-04-19 · of 0265/C01/E00502/005 in DMSO-d6 Released on 70 60 20 10 O ppm 100 90 30 160 150 50 40 30 140 130 120 110](https://reader033.vdocument.in/reader033/viewer/2022060217/5f064f6a7e708231d4175a00/html5/thumbnails/5.jpg)
HPLC Chromatogram of Stage-1
![Page 6: HNMR Spectrum of Stage-1 - Royal Society of Chemistry · 2018-04-19 · of 0265/C01/E00502/005 in DMSO-d6 Released on 70 60 20 10 O ppm 100 90 30 160 150 50 40 30 140 130 120 110](https://reader033.vdocument.in/reader033/viewer/2022060217/5f064f6a7e708231d4175a00/html5/thumbnails/6.jpg)
1HNMR Spectrum of Stage-2
![Page 7: HNMR Spectrum of Stage-1 - Royal Society of Chemistry · 2018-04-19 · of 0265/C01/E00502/005 in DMSO-d6 Released on 70 60 20 10 O ppm 100 90 30 160 150 50 40 30 140 130 120 110](https://reader033.vdocument.in/reader033/viewer/2022060217/5f064f6a7e708231d4175a00/html5/thumbnails/7.jpg)
13CNMR Spectrum of Stage-2
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Mass Spectrum of Stage-2
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DSC Thermogram of Stage-2
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HPLC Chromatogram of Stage-2
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1HNMR Spectrum of Stage-3
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13 CNMR Spectrum of Stage-3
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Mass Spectrum of Stage-3
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DSC Thermogram of Stage-3
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HPLC Chromatogram of Stage-3 (Chemical purity)
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HPLC Chromatogram of Stage-3 (Chiral purity)
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1HNMR Spectrum of stage-4
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13CNMR Spectrum of stage-4
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Mass Spectrum of stage-4
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DSC Thermogram of stage-4
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HPLC Chromatogram of stage-4
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1HNMR Spectrum of stage-5/ Idelalisib
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13CNMR Spectrum of stage-5/ Idelalisib
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Mass Spectrum of stage-5/ Idelalisib
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DSC Thermogram of stage-5/ Idelalisib
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HPLC Chromatogram of stage-5/ Idelalisib (Chemical purity)
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HPLC Chromatogram of stage-5/ Idelalisib
(Chiral purity)