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HP 1100 LC/MSD Gsbookl%.fm Page 1 Wednesday, November 1, 2000 1:52 PM

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Page 1: HP 1100 LC/MSD - Chemical Analysis, Life Sciences, and ...€” 2 — Help Help Topics Help Contents Index Find Display Close Print popup Print Cancel Help Topic Open Close I Open

HP 1100LC/MSD

Gsbookl%.fm Page 1 Wednesday, November 1, 2000 1:52 PM

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— 2 —

Help Help

Topics Help

Contents

Index

Find

Display

Close

Print

popup

Print

Cancel Help TopicOpen

Close

IOpen

Help

Contents

Gsbookl%.fm Page 2 Wednesday, November 1, 2000 1:52 PM

Page 3: HP 1100 LC/MSD - Chemical Analysis, Life Sciences, and ...€” 2 — Help Help Topics Help Contents Index Find Display Close Print popup Print Cancel Help Topic Open Close I Open

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View

HP LC/MSD ReferenceCollectionCD ROM

OQ/PV

GLP

EMFLC/MSD CD-ROM

MSDLC/MSD

Gsbookl%.fm Page 3 Wednesday, November 1, 2000 1:52 PM

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LC/MSD DAD

/

Gsbookl%.fm Page 4 Wednesday, November 1, 2000 1:52 PM

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FIA

FIA :• FIA• Edit FIA Series.• Enable FIA Series in Method

FIA .

Single Sample

Sequence

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DAD

LC/MSD

Integration

Gsbookl%.fm Page 6 Wednesday, November 1, 2000 1:52 PM

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UV MS

Calibration.

Signals

Spectral

Gsbookl%.fm Page 7 Wednesday, November 1, 2000 1:52 PM

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:

/

MS

Gsbookl%.fm Page 8 Wednesday, November 1, 2000 1:52 PM

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— 9 —

x

y

Gsbookl%.fm Page 9 Wednesday, November 1, 2000 1:52 PM

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File/Add to Report Styles

Gsbookl%.fm Page 10 Wednesday, November 1, 2000 1:52 PM

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\hpchem\repstyle

SIMPLE.FRP I

NESTED.FRP

SPECTRA.FRP

PURITY.FRP

ESTD.FRP

AREAPCT.FRP

LIBRARY.FRP

Gsbookl%.fm Page 11 Wednesday, November 1, 2000 1:52 PM

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OQ/PV

/

Gsbookl%.fm Page 12 Wednesday, November 1, 2000 1:52 PM

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— 13 —

Verification ViewShowTopToolbar

.

Verification (OQ/PV)

• (OQ)

• (PV)

VWD

DAD*

/ *

* LC/MSD

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CD-ROM

Gsbookl%.fm Page 14 Wednesday, November 1, 2000 1:52 PM

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MSD

MSD

LC/MSD LC/MSD

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LC LC/MSD

1 Method and Run ControlOn

2 LC3 LC/MSD

15

APCI

LC/MSD

1

LC50:50 /

5-102 Off

LC/MSD 20psi3L/min 300 APCI

325 MSLC to Waste(LC )

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— 17 —

LC/MSD

LC/MSD HPLCLC

LC/MSD

•••

LC/MSDLC/MSD

.tun

LC/MSD

LC/MSD4 4

LC/MSD

LC/MSD

1 MSD Tune Tune/ Autotune Autotune

2

LC/MSD

1 Tune / Check Tune.

2Check Tune

•• (<150amu)•

4

1(fragmentor skim2 1 2

2

34

fragmentorfragmentor

Gsbookl%.fm Page 17 Wednesday, November 1, 2000 1:52 PM

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— 18 —

LC/MSD

••• FIA

••••

Method and Run Control

1 Method / Load Method Open Method

2 Method / Edit Entire Method

Help

3 ()

45

DAD VWD

MSD

MSD

6

7 Run Time Checklist( )8 Method / Save

Method As Save Method

9 Start

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— 19 —

Deconvolution

Deconvolution

1 Data Analysis MS

2 Spectral

3 Enter Deconvolution Tool

4 Find Ions

5 Î

ÃFind Ions Options

6 Run Deconvolution

( Specra/Deconvolution

7 Component ±£

8 Preview Deconvolution Report

Print Report

9 Compont ListDelete Componts

4

10

Gaussian

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— 20 —

o

o

o

o MS

o HP 1100Series LC/MSD Maintenance CD-ROM

o Maintenance Logbook EMF

o

o

o

o

o LC/MSD

oZDV

T

o SIM ѣ

o (APCI)1.0ml/min 0.5-1.5 ml/min

( )

SIM

SIM

Gsbookl%.fm Page 20 Wednesday, November 1, 2000 1:52 PM

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— 21 —

LC/MSDLC/MSD

fragmentor

LC/MSD

LC

LC

>18M

LC

LC

MS LC to MSD

Fragmentor

Gsbookl%.fm Page 21 Wednesday, November 1, 2000 1:52 PM

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— 22 —

HP 1100 LC

LC DAD VWD)

Gsbookl%.fm Page 22 Wednesday, November 1, 2000 1:52 PM

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— 23 —

LC

CAN

HP-IB

CAN

Gsbookl%.fm Page 23 Wednesday, November 1, 2000 1:52 PM

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HP 1100 LC/MSD

On/off

þ>

LC

Gsbookl%.fm Page 24 Wednesday, November 1, 2000 1:52 PM

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— 25 —

HP 1100 LC/MSD APCI

APCIOn/off

APCI

APCI

LC

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— 26 —

HP 1100 LC/MSD ( )

MS

LC

Gsbookl%.fm Page 26 Wednesday, November 1, 2000 1:52 PM

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— 27 —

LC/MSD ( , )

LC/MSD

HP-IB

LC/MSD

LC

(N2)

(N2)

Gsbookl%.fm Page 27 Wednesday, November 1, 2000 1:52 PM

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— 28 —

HP 1100 LC/MSD APCI ( )

MS

APCI

APCI

LC

Gsbookl%.fm Page 28 Wednesday, November 1, 2000 1:52 PM

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LC/MSD APCI ( , )

LC/MSD

HP-IB

LC/MSD

LC

(N2)

(N2)

APCI APCI

Gsbookl%.fm Page 29 Wednesday, November 1, 2000 1:52 PM

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LC/MSD

HP

ES

OQ/PV

G1946-85001G1946-85002G1946-85006G1946-85005G1946-85004G1946-85003

, F120 ( PEEK )bal 1/4"

PEEK 0.005", 1/16"

G1946-800099301-139705971-801030100-19200100-15160905-14750101-0941G1946-20177G1946-200975182-34410890-19156040-0834

8660-085205980-600519300-1751

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— 31 —

HP 1100 LC/MSD

HP 1100 LC/MSDIEC 1010 1

LC LC/MSDLC

LC/MSDLC

LC/MSD HP 1100 LC

X Z H P

LC/MSD

LC/MSD

LC/MSD

Gsbookl%.fm Page 31 Wednesday, November 1, 2000 1:52 PM

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, 5/97HP G2710 LC/MSDA.05.01

©1997

. 5/97G1946-97006

Gsbookl%.fm Page 32 Wednesday, November 1, 2000 1:52 PM