hplc suction filter with mobile phase cleaning function glc ......glc suction filter 2 0.0 1.0 2.0...

1
GLC Suction Filter 2 HPLC Suction filter with mobile phase cleaning function ■ Removes contaminants at the most upstream of HPLC system ■ Does not affect system volume ■ Available for LC/MS Removal Effect of GLC Suction Filter 2 for LC/MS The GLC Suction Filter 2 is the most upstream consumable part of a HPLC system and is useful for removing contaminants in the mobile phase. The product is easy to install and can be replaced by the user. Removal of contaminants in the mobile phase by GLC Suction Filter 2 was evaluated. A mixture of acetonitrile and water (1/9, 5/5, 9/1) was used as the mobile phases. In all case, the removal of contaminants was confirmed and the noise level of the TIC was also reduced. Features [email protected] https://solutions.shimadzu.co.jp/glc 5F CS-Tower Bldg., 5-20-8, Asakusabashi, Taito-ku, Tokyo 111-0053, Japan MK-FL-20-E0001A Product Information Please read the manual carefully and pre-condition before use. *The suction tube is not included. *3mm outer diameter suction tube can be connected. *When using ion-pair reagents in the mobile phase, the ion-pair reagent is retained in the product, and retention time and peak shape may be affected. *Bleed noise from this product may be seen. *This product does not remove all impurities. *If impurities are not retained, ghost peaks may be detected. In this case, replace the product. *The recommended replacement period is after passing 60L of mobile phase or 1 year after use. Column Detector Degasser GLC Suction Filter 2 Pump Attachment Position Activated charcoal SUS Sintered Filter Flow Normal Suction Filter 0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 min 0.0 2.5 5.0 (x1,000,000) 2:TIC(-) 1:TIC(+) 2:TIC(-) 1:TIC(+) 250 500 750 1000 1250 1500 1750 m/z 0.0 2.5 Inten. (x10,000) 119 279 1937 704 379 614 907 1368 1777 976 1224 1531 1674 1060 250 500 750 1000 1250 1500 1750 m/z 0.0 2.5 Inten. (x10,000) 103 743 864 271 655 1938 1675 1236 524 1785 1475 1107 974 1368 360 1571 GLC Suction Filter 2 0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 min 0.0 2.5 5.0 (x1,000,000) 2:TIC(-) 1:TIC(+) 2:TIC(-) 1:TIC(+) 250 500 750 1000 1250 1500 1750 m/z 0.0 2.5 Inten. (x10,000) 100 473 879 512 605 696 361 256 832 964 1118 1377 1687 1230 1523 250 500 750 1000 1250 1500 1750 m/z 0.0 2.5 Inten. (x10,000) 100 255 459 325 700 1158 911 1024 837 1507 1320 1873 1683 Mobile Phase : Water : Acetonitrile = 10 : 90 Mobile Phase : Water : Acetonitrile = 50 : 50 0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 min 0.0 2.5 5.0 (x1,000,000) 2:TIC(-) 1:TIC(+) 2:TIC(-) 1:TIC(+) 250 500 750 1000 1250 1500 1750 m/z 0.0 2.5 Inten. (x10,000) 100 342 471 579 563 883 976 1409 1054 1635 717 1223 1807 1927 1541 250 500 750 1000 1250 1500 1750 m/z 0.0 2.5 Inten. (x10,000) 100 311 459 555 954 1324 1064 1202 814 1493 1939 1696 0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 min 0.0 2.5 5.0 (x1,000,000) 2:TIC(-) 1:TIC(+) 2:TIC(-) 1:TIC(+) 250 500 750 1000 1250 1500 1750 m/z 0.0 2.5 Inten. (x10,000) 119 279 812 1501 371 1089 527 971 1256 1932 642 1606 1376 1804 250 500 750 1000 1250 1500 1750 m/z 0.0 2.5 Inten. (x10,000) 103 649 1845 736 879 1653 1462 342 1286 495 265 412 1128 1018 Mobile Phase : Water : Acetonitrile = 90 : 10 0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 min 0.0 2.5 5.0 (x1,000,000) 2:TIC(-) 1:TIC(+) 2:TIC(-) 1:TIC(+) 250 500 750 1000 1250 1500 1750 m/z 0.0 2.5 Inten. (x10,000) 100 279 579 580 991 391 1330 1653 1910 1104 815 744 1509 1799 1196 250 500 750 1000 1250 1500 1750 m/z 0.0 2.5 Inten. (x10,000) 119 1754 241 999 1266 1517 326 700 1114 539 402 1861 917 847 0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 min 0.0 2.5 5.0 (x1,000,000) 2:TIC(-) 1:TIC(+) 2:TIC(-) 1:TIC(+) 250 500 750 1000 1250 1500 1750 m/z 0.0 2.5 Inten. (x10,000) 279 119 1922 722 1004 1416 472 1641 1757 1537 591 913 1274 250 500 750 1000 1250 1500 1750 m/z 0.0 2.5 Inten. (x10,000) 103 1391 1643 1084 1961 1248 646 941 426 1840 219 341 766 1500 Analytical Conditions Instruments : Nexera X2 Flow Rate : 0.2 mL /min Detection : MS (ESI), Scan Mode (100 to 2000 m/z , positive, negative) P/N Internal Volume Qty. 370-02010-01 0.7mL 1

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Page 1: HPLC Suction filter with mobile phase cleaning function GLC ......GLC Suction Filter 2 0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 min 0.0 2.5 5.0 (x1,0 00,000) 2:TIC(-) 1:TIC(+) 2:TIC(-)

GLC Suction Filter 2HPLC Suction filter with mobile phase cleaning function

■ Removes contaminants at the most upstream of HPLC system■ Does not affect system volume■ Available for LC/MS

Removal Effect of GLC Suction Filter 2 for LC/MS

The GLC Suction Filter 2 is the most upstream

consumable part of a HPLC system and is

useful for removing contaminants in the

mobile phase. The product is easy to install

and can be replaced by the user.

Removal of contaminants in the mobile phase by GLC Suction Filter 2 was

evaluated. A mixture of acetonitrile and water (1/9, 5/5, 9/1) was used as the

mobile phases. In all case, the removal of contaminants was confirmed and

the noise level of the TIC was also reduced.

Features

[email protected]://solutions.shimadzu.co.jp/glc5F CS-Tower Bldg., 5-20-8, Asakusabashi, Taito-ku, Tokyo 111-0053, Japan

MK-FL-20-E0001A

Product Information Please read the manual carefully and pre-condition before use.*The suction tube is not included.*3mm outer diameter suction tube can be connected.*When using ion-pair reagents in the mobile phase, the ion-pair reagent is retained in the product, and retention time and peak shape may be affected.*Bleed noise from this product may be seen.*This product does not remove all impurities.*If impurities are not retained, ghost peaks may be detected. In this case, replace the product.*The recommended replacement period is after passing 60L of mobile phase or 1 year after use.

Column

Detector

Degasser

GLC Suction Filter 2

Pump

Attachment Position

Activated charcoal

SUS Sintered Filter

Flow

Normal Suction Filter

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 min0.0

2.5

5.0

(x1,000,000)

2:TIC(-)1:TIC(+)2:TIC(-)1:TIC(+)

250 500 750 1000 1250 1500 1750 m/z0.0

2.5

Inten.(x10,000)

119

2791937

704379 614 907 1368 1777976 1224 1531 16741060

250 500 750 1000 1250 1500 1750 m/z0.0

2.5

Inten.(x10,000)

103

743 864271 6551938

16751236524 178514751107974 1368360 1571

GLC Suction Filter 2

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 min0.0

2.5

5.0

(x1,000,000)

2:TIC(-)1:TIC(+)2:TIC(-)1:TIC(+)

250 500 750 1000 1250 1500 1750 m/z0.0

2.5

Inten.(x10,000)100 473

879512 605696361256 832 964 1118 1377 16871230 1523

250 500 750 1000 1250 1500 1750 m/z0.0

2.5

Inten.(x10,000)100

255 459325 700 1158911 1024837 15071320 18731683

Mobile Phase : Water : Acetonitrile = 10 : 90 Mobile Phase : Water : Acetonitrile = 50 : 50

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 min0.0

2.5

5.0

(x1,000,000)

2:TIC(-)1:TIC(+)2:TIC(-)1:TIC(+)

250 500 750 1000 1250 1500 1750 m/z0.0

2.5

Inten.(x10,000)100 342

471579

563 883 976 14091054 1635717 1223 18071927

1541

250 500 750 1000 1250 1500 1750 m/z0.0

2.5

Inten.(x10,000)100

311 459 555 954 13241064 1202814 14931939

1696

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 min0.0

2.5

5.0

(x1,000,000)

2:TIC(-)1:TIC(+)2:TIC(-)1:TIC(+)

250 500 750 1000 1250 1500 1750 m/z0.0

2.5

Inten.(x10,000)

119

279 812 1501371 1089527 971 12561932

642 16061376 1804

250 500 750 1000 1250 1500 1750 m/z0.0

2.5

Inten.(x10,000)

103

649 1845736 879 16531462342 1286495265 412 11281018

Mobile Phase : Water : Acetonitrile = 90 : 10

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 min0.0

2.5

5.0

(x1,000,000)

2:TIC(-)1:TIC(+)2:TIC(-)1:TIC(+)

250 500 750 1000 1250 1500 1750 m/z0.0

2.5

Inten.(x10,000)100 279

579

580 991391 1330 1653 19101104815744 1509 17991196

250 500 750 1000 1250 1500 1750 m/z0.0

2.5

Inten.(x10,000)

119

1754241 999 1266 1517326 700 1114539402 1861917847

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 min0.0

2.5

5.0

(x1,000,000)

2:TIC(-)1:TIC(+)2:TIC(-)1:TIC(+)

250 500 750 1000 1250 1500 1750 m/z0.0

2.5

Inten.(x10,000)

279119

1922722 1004 1416472 1641 17571537591 913 1274

250 500 750 1000 1250 1500 1750 m/z0.0

2.5

Inten.(x10,000)

103

1391 164310841961

1248646 941426 1840219 341 766 1500

Analytical ConditionsInstruments : Nexera X2Flow Rate : 0.2 mL /minDetection : MS (ESI), Scan Mode (100 to 2000 m/z , positive, negative)

P/N Internal Volume Qty.370-02010-01 0.7mL 1